WQ0000485_Monitoring - 11-2022_20221229

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
Type *
GW-59
WQ0000485
Darling Ingredients - Rose Hill Division
Year:* 2022
Upload Document*
scan 2022-11 WQ0000485
GW-59 DIRH.pdf
PDF Only
4.97MB
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
Confirmation Email Address:* [e-mail]
Name of Submitter: * Corey Lanier
Signature:
Date of submittal: 12/29/2022
This will be filled in automatically
Initial Review
Reviewer: Gerald, Wanda

Is the project number correct?* WQ0000485
Is the monitoring report accepted?* - Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 1/19/2023

G -59A tu°t"tP llPt.IILA,NCE Illfll� 0111l]" III+"0ftltf Pervirmwt"# W00000485
(,V.b,.if Pt.N.tt", srwh xwm,wi?OrdsMwr,Pa",y„c^u.Idan}dv h du flV"39fc,—,)
1
Enter date monitoring results were due. (1213112022) Will this monitoring report (GW-59 and GW-59A)
be submitted after the established due date?
No
2
Was any required information missing on the GW-59 report forms?
No
IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and explain the
problems encountered in obtaining the required information.
MW-8A was damaged by farm equipment and is scheduled to be closed and replaced by Register Well Co, INC; moving the
replacement well 10'due North per DEQ direction.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missingidentificalion
plate, area overgrown, etc.)? Ifthe answer is "Yes ", contact the Regional Officefor guidance.
No
4
Are any monitored constituents equal to or above the established standards?
YES
If the answer to question 4 is "NO", skip to section 8,
If the answer to question 4 is "YES" list the affected wells individually with constiluent(s) and concentration(s) exceeding
standards in the space provided below.,
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
5
For the constituents identified in question 4 above, have standards been exceeded previously for the same
constituent(s) in the same well(s) in the last two years?
YES
If the answer to question 5 is "NO", skip to section 8,
lithe answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards,
concentration(s) reported, and sample collection date for each occurrence (for the last two years).
SEE ATTACHED GROUNDWATER MONITORING WELL 2 YR EXCEEDANCE HISTORY REPORT
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE
IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the
Regional Office.
7
Is the perrnittee implementing previously approved actions required by the Division involving this groundwater quality
problem?
YES
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO" contact the Regional Office within 90 da s• an evaluation ma be
re aired io determine the im ct the waste dis. osal s stem is ha-1-at floe review and csrm Irance
boundaries surrounding this facility, Failure to do so may sub act the ermdtee to a Not}ce of hliotatlon,
fines, and/or enaides.
Additional monitoring was performed to identify constituents of TOC in MW No.9. The facility has been
communicating with Mr. Geoff Kegley in the Wilmington Regional Office,
8
The person completing this portion (G W-59A) of the monitoring report should sign below and submit this form with
GW-59 forms for required wells to the address provided at the top of the current G W-59 form.
I hereby acknowledge that the above information was evaluated and the information submitted in this report
(Compliance Report GWpp-59A) is true and complete to the best of my knowledge.
�1.n.tu.
of Permittee (or Authorized Agent) Date

SUBMIT FORM ON YELLOW PAPER ONLY
ROUNDWATER QUALITY MONITORING:
OMPLIANOE REPORT FORM
acility Name:
ermit Name (if different):
acility Address:
Rose Hill, INC 28458
Contact Person:
Well Location/Site Name
Please Print Clearly or Type
Vallev Proteins Inc.- Rose Hill
Lanier
469 Yellow Cut Rd.
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 11
WELL ID NUMBER (from Permit): MWA Date sample collected:
Well Depth: 12.46 ft. Well Diameter:
Depth to Water Level 82546: 6.6 Screened Interval:
Measuring Point is 1.17 ft. above land surface Relative M.P. Elevation:
Volume of water pumped/bailed before sampling: 5.0 gallons
11 /12/2022
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
2 in.
12.46 ft. to 2.46 ft.
ft.
Samples for metals were collected unfiltered: X YES I-1 NO and field acidified: X YES I —I NO
FIELD ANALYSES:
pH4500HB 5.60 units
Spec. Cond. 00094:
Odor 00085:
Appearance
Temp. 000lo: 21 9 oC
uMhos
None
Clear
Date sample analyzed:
11/12/2022-11/30/2022
Laboratory Name:
Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values
should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620
0.28 mg/L
Zn - Zinc 01092 mg/L
Coliform° MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.04 mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)_
)issolved Solids -Total 70300
106.00
mg/L
Al - Aluminum 01105
mg/L
Sodium 7.26 mg/L
pH (Lab) 00403
5.60
units
Ba - Barium 01007
ug/L
TOC 00680
1.5
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
10
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945
44
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ® Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 78732: method # SM 6200C
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625
0.5
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Permittee (or Authorized Aqent) Name and Title - Please print or tvpe
Authorized Agent)
If WELL
DRY at
time of
sampling,
checl�
harm
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
•i1fi711NM+i i NATURAL
GROUNDWATER QUALITY MONITORING:
ir%t?r
COMPLIANCE REPORT FORM
• •'�
�� r t' [�RJ �� 1,x s3 t� n-sa;F1r
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins Inc.- Rose Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458
County Duplin
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(frwn Pest
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-2
Date sample collected: 11/12/2022
FIELD ANALYSES:
WAS
Well Depth: 31.00 ft.
Well Diameter: 2 in.
pH4500HB 6.50 units Temp. 000lo: 20 °C
DRY at
Depth to Water Level 82546: 15.7 ft. below measuring point
Screened Interval: 30.15 ft. to 20.15 ft. Spec, Cond. 00094: µMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 000m None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Tan
check
here:
Samples for metals were collected unfiltered:
X YES ❑
NO and field acidified: X YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed_ 11/12/2022-11/30/2022
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N oo615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (1103) as N 00620 0.13
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 <0.04
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 284.00
mg/L
Al - Aluminum 01105
mg/L Sodium 12.1 m /L
pH (Lab) 00403 6.50
units
Ba - Barium 01007
ug/L
TOC 00680 0.9
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 9
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 9
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? E Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
GW-59 Rev.8/2013

SUBMIT FORM ON YELLOW PAPER ONLY
-uu�Tr,i~sttsRMATro
�1ATi�itAL i �E
T QF EN iRi?NMENT &51
GROUNDWATER QUALITY MONITORING:
>�cEsr��IT.
COMPLIANCE REPORT FORM
Et=1t 1 s? t�tte ?�iosss
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: W00000485 Expiration Date: 3/31 /2025
Facility Name:
Valley Proteins
Inc.- Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd,
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
Rose Hill, NC 28458 County Duplin
:Y
(Z.�,,
X Spray Field ❑ Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-4
Date sample collected: 11/12/2022
FIELD ANALYSES: WAS
Well Depth: 28.93 ft.
Well Diameter: 2 in
pH4500HB 6.30 units Temp. 000lo: 21.1 oC DRY at
Depth to Water Level 82546: 9.6 ft. below measuring point
Screened Interval: 28.93 ft. to 18.93ft.
Spec. Cond. 00094: µMhos time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Clear check
here.
Samples for metals were collected unfiltered:
X YES 0
NO and field acidified: X YES NO
LABORATORY INFORMATION
Date sample analyzed: 11/12/2022-11/30/2022
Laboratory Name: Environmental Chemists, Inc, Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620 <0.02
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 <0.04
mg/L
(Note- Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids. -Total 70300 223.00
mg/L
Al - Aluminum o11o5
mg/L Sodium 11.2 mg/L
pH (Lab) 00403 6.30
units
Ba - Barium 01007
ug/L
TOC 00680 0.70
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 <5,0
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 <5.0
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? E Yes (0) ❑ No (0)
pecific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 78732: method # SM 6200C
Total Ammonia 000lo <0.2
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen, NH3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L , method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Larry Holt - General Manager
Permittee (or Authorized Aqent) Name and Title - Please print or tvl)e
GW-59 Rev, 8/2013

1NDWATER QUALITY MONITORING:
#LIANCE REPORT FORM
TY INFORMATION Please Print Clearly or Type
Name: Valley Proteins Inc.- Rose Hill
Name (if different):
Address: 469 Yellow Cut Rd.
ME
County Duplin
act Person: Corey Lanier Telephone#: [phone]
Location/Site Name: No. of wells to be sampled: 11
_.. _. (from Permit)
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-7A
Date sample collected: 11/12/2022
FIELD ANALYSES:
WAS
Well Depth: 16 ft,
Well Diameter: 2 in.
pH4500HB 3.86 units Temp. 000lo: 21.7 °C
DRY at
Depth to Water Level 62546: 6.0 ft. below measuring point
Screened Interval: 16 ft. to 6 ft.
Spec. Cond. 00094: µMhos
time of
Measuring Point is 2.42 ft. above land surface
Relative M.P. Elevation: ft,
Odor 00085 None
sampling,
Volume of water pumped/bailed before sampling: 5.0 gallons
SamDles for metals were collected unfiltered: X YES r 1 NO and field acidified: X YES I —I NO
Appearance Tan
check
here
Date sample analyzed:
11/12/2022-11/30/2022
Laboratory Name:
Environmental Chemists, Inc.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOZ) as N 00615
<0.02 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616
<1 /100mL
Nitrate (NO3) as N 00620
<0.02 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.04 mg/L
Certification No. DWQ#94
ug/L
mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
Dissolved Solids:Total 70300 297.00 mg/L Al - Aluminum 01105 mg/L Sodium 36.4 mg/L
pH (Lab) 00403
3.86 units
Ba - Barium 01007
ug/L
TOC 00680
1.3 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
117 mg/L
Cd - Cadmium 01027
ug/L
Arsenic olow
ug/L
Chromium: Total0103a
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 20
mg/L
Hg - Mercury71900
ug/L
Lab Report Attached? MYes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 76732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; Naas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L
method #
mg/L Effluent Total

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd.
Rose Hill, NC 2458
County Duplin
act Person: Corey Lanier Telephone#: [phone]
Location/Site Name Field 5 - damaged by farm equip / to replace No. of wells to be sampled: 11
(from Permit)
ID NUMBER (from Permit):
MW-8A Date sample collected: 11/12/2022
PERMIT Number. W00000485 Expiration Date: 3/3112025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
FIELD ANALYSES:
Well Depth: 16 ft. Well Diameter: 2 in. pH4500HB 4.20
Depth to Water Level 62546: 7.0 ft. below measuring point Screened Interval: 16 ft. to 6 ft. Spec. Cond. ©o
Measuring Point is 2.5 ft. above land surface Relative M.P. Elevation: ft. ! Odor 000m:
Volume of water pumped/bailed before sam 0 5.0 gallons Appearance
Samples for metals were collected unfiltered: X YES LJ NO and field acidified: X YES ❑ NO
Date sample analyzed:
11/12/2022-11/30/2022
Laboratory Name:
Environmental Chemists, Inc.
PARAMETERS NOTE: Values
should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616
<1 /100mL
Nitrate (NO3) as N 00620
1.42 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.04 mg/L
units Temp.00010: 21.9 oC
W uMhos
None
Tan
Certification No. DWQ#94
ug/L
mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):.
)issolved Solids:Total 70300 86.00 mg/L Al -Aluminum 01105 mg/L Sodium 2.32 mg/L
pH (Lab) 00403
4.20 units
Ba - Barium 01007
ug/L
TOC 006e0
0.60 mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
8 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 23
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? M Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
VOC 76732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NFIas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N 00625 <0.5
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: rng/L Effluent Total V"OCs: mg1L VOC Removal%
Larry Holt - General Manager
Pennittee (or Authorized Agent) Name and Title - Please print or type
If WELL
WAS
DRY at
time of
sampling,
check
here:

GROUNDWATER QUALITY MONITORING -
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd.
Rose Hill, NC 28458
Contact Person: Corey Lanier
Well Location/Site Name
County Du
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
ERMIT Number: WQ00004 5 Expiration Date_ 313112025
on -Discharge UIC
PLIES Other
YPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-9
Date sample collected: 11/12/2022
FIELD ANALYSES:
WAS
Well Depth: 13.73 ft.
Well Diameter: 2 in.
pH4500r18 6.00 units Temp. 000lo: 19.6 °C
DRY at
Depth to Water Level 82546: 8 ft. below measuring point
Screened Interval: 13.73 ft. to 3.73 ft.
Spec, Cond =94:: µMhos
time of
Measuring Point is 3.50 ft. above land surface
Relative M.P. Elevation: ft.
Odor o0om: None
sampling,
Volume of water pumped/bailed before sampling: 5.0
gallons
Appearance None
check
Samples for metals were collected unfiltered: X YES I-1
NO and field acidified: X YES ❑ NO
here:
Date sample analyzed:
11/12/2022-11/30/2022
Laboratory Name:
Environmental Chemists, Inc.
PARAMETERS NOTE: Values
should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
0.11 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616
<1 /100mL
Nitrate (NO3) as N 00620
1.75 mg/L Zn - Zinc 01092
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
0.12 mg/L
Certification No. DWQ#94
ug/L
mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 374.00 mg/L Al -Aluminum o1105 mg/L Sodium 5.19 mg/L
pH (Lab) 00403
6.00 units
Ba - Barium 01007
ug/L
TOC 00660
27.6 mg/L
Ca - Calcium oo916
mg/L
Chloride 00940
35 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 22
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 000m
µMhos
K - Potassium 00937
mg/L
VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; Ni;as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 1.7
mg/L
Ni - Nickel 01067
ug/L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: _ m /L Effluent Total VOCs_ m /L VOC Removal%
Larry Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type
of Permittee (or Aothorized Agent)

GROUNDWATER QUALITY MONITORING:
bR
COMPLIANCE REPORT FORM
PERMIT Number: W00000485 Expiration Date-, 3f3112025
FACILITY INFORMIATION Please Print Clearly or Type
Facility Name:
Valley_�� Rose Hill
Non -Discharge UIC
NPDES Other
Permit Name (if different):
Facility Address:
469 Yellow Cut Rd.
TYPE OF PERMITTED OPERATION BEING MONITORED
E] Lagoon E] Remediation: Infiltration Gallery
Rose Hilt, NC 28458 County Duplin
—
Contact Person: Corey Lanier
Telephone#: [phone]
E] Rotary Distributor Ej Land Application of Sludge
Well Location/Site Name
—
No. of wells to be sampled: 11
E] Water Source Heat Pump F-1 Other:
(from Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-10A
Date sample collected: 11/12/2022 FIELD ANALYSES:
WAS
Well Depth: 16 ft
Well Diameter: 2 in.
pH4500HB 3.67 units Temp. 000ll: 205 oc
DRY at
Depth to Water Level 82546: 5.3 ft. below measuring point
Screened Interval: 16 ft.
to 6 ft. Spec. Cond. 00094:
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation:
_gMhos
ft. Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Brown
Samples for metals were collected unfiltered:
X YES M
NO and field acidified: X YES
NO
LABORATORY INFORMATION
Date sample analyzed� 11 /12/2022-11/30/2022
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and
colloidal concentrations.
C0Do03a
mg/L
Nbhte(NOu) aoNo061s <0,02
mg/L Pb Loadmmn ug/L
Coliform: MFFecal mmo ^1
/100mL
Nitrate(NO3) as 00620 <0,02
mg/L Zn Zincm092 mg/L
Co|donn: MFTotal o1mm
/100mL Phosphorus: Total anPo06o
mg/L
(No*. use MPN method for highly turbid samples)
Orthuphouphater05o
mg/L Other (Specify Compounds and Concentration Unho):
)i000|vou8onuu:Tma|r0000 833.00
mg/L
Al A|uminumv,1vn
mg/L Sodium 138 mg/L
pH(Lob)ocwno 3.67
units
oo'Barium o1uor
ug/L
TOCoosou 3.6
mg/L
Ca Ca|ciumvvv10
mg/L
Ch|o,idovvn^v noa
mg/L
Cd'Cadmium o1o2r
ug/L
Amenico1oox
ug/L
Chromium: Total u1on*
ug/L
Grease and Oils ounou
mg/L
Cu Coppo,v1vm
mg/L ORGANICS: (by GC, sc/Ma.npLC)
Phenol ocmo
ug/L
Fa |mnv1w*s
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Su|fam,00*m 137
mg/L
Mg Momuryr1yoo
ug/L Lab Report Attached? 0Yes (0) [] N»(0)
SpooihcConductance 0000n
4Mxoo
K Putaooiumooyor
mg/L vOCrorxc. .motxou# SIM 6200C
Total Ammonia 00610 0.50
mg/L
Mg Magnoniumonozr
mg/L .mothod#
(Ammonia Nitrogen. wm"sw;Ammonia Nitrogen, Total)
Mn'Manganese o1oon
ug/L .mothod#
TKmaow000us 0.80
mg/L
Ni'Nickel o1oor
ug/L .mathod#
Reports): Influent Total

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
Facility Name:
Permit Name (if different):
Facility Address:
Rose Hill. NC 28458
Please Fruit Clearly or Type
Vallev Proteins Inc.- Rose Hill
Contact Person- Corey Lanier
Well Location/Site Name
469 Yellow Cut Rd,
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
on -Discharge UIC
PDES Other
yPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-11A
Date sample collected:
11/12/2022
FIELD ANALYSES:
WAS
IWetl Depth: 16 ft.
Well Diameter:
2 in.
pH4500HB 4.10 units Temp. 000l( 21.5 °C
DRY at
Depth to Water Level 82546: 7.7
Screened Interval:
16 ft.
to 6 ft.
Spec. Cond. 00094: uMhos
time of
Measuring Point is 3.3 ft. above land surface
Relative M.P. Elevation:
ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling.
5.0
gallons
Appearance Clear
check
here:
Sam les for metals were collected unfiltered:
XYESM NO and field acidified: X YES
NO
LABORATORY INFORMATION
Date sample analyzed: 11/12/2022-11/30/2022
Laboratory Name_
Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect
dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02
mg/L
Pb - Lead 01051 ug/L
Coliform: MF Fecal 31616 <1
/100mL
Nitrate (NO3) as N 00620
0.6
mg/L
Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.04
mg/L
(Note- Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units)_
lissolved Solids:Total 70300 583.00
mg/L
Al - Aluminum 01105
mg/L
Sodium 72.4 mg/L
pH (Lab) 00403 4.10
units
Ba - Barium 01007
ug/L
TOC 00680 2.50
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 145
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 186.0
mg/L
Hg - Mercury 71900
ug/L
Lab Report Attached? ,Yes (0) ❑ No (0)
ipecific Conductance 00095
uMhos
K - Potassium 00937
mg/L
VOC 78732: method # SM 6200C
Total Ammonia 00610 <0.2
mg/L
Mg - Magnesium 00927
mg/L
method #
(Ammonia Nitrogen; NFJas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
method #
TKN as N 00625 <0.5
mg/L
Ni- Nickel 01067
ug/L
method #
For Re mediation Systems Only (Attach Lab Report): Influent Total VO s; mg/L Effluent Total VOCs: M WL VOIL; KeMOV l"
Larry Holt - General Manager
Perrnittee (or Authorized Agent) Name and Title - Please print or type

HATER QUALITY MONITORING:
NCE REPORT FORM
Facility Name:
Permit Name (if d
Facility Address:
Contact Person:
Well Location/Site Name:
Please Print Clearly or Type
fallev Proteins Inc.- Rose Hill
Hill, NC, 28458
Corev Lanier
469 Yellow Cut Rd.
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
WELL ID NUMBER (from Permit): MW-12B Date sample collected: 11/12/2022
Well Depth: 16 ft. Well Diameter: 2 in,
Depth to Water Level 82546: 7.4 ft. below measuring point Screened Interval: 20 ft. to 10 ft.
Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft.
Volume of water pumped/bailed before sampling: 5.0 gallons
Samples for metals were collected unfiltered:. X YES p NO and field acidified: X YES n NO
LABORATORY INFORMATION
FRMIT Number W00000485 Expiration Date: 3131/ 0 5
on -Discharge UIC
PDES Other
(PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
If WELL
FIELD ANALYSES: WAS
pH45 H13: 3.70 units Temp. 000lo: 21 6 °C DRY at
Spec Cond. os4; µMhos time of
Odor 00085: None sampling,
Appearance Clear check
here:
Date sample analyzed: 11/12/2022-11/30/2022 Laboratory Name: Environmental Chemists,_ Inc.
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615
<0.02 mg/L
Coliform: MF Fecal 31616
<1
/100mL
Nitrate (NO3) as N 00620
0.10 mg/L
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
0.05 mg/L
(Note: Use MPN method for highly
turbid samples)
Orthophosphate 70507
mg/L
Dissolved Solids:Total 70300
309,00
mg/L
Al -Aluminum 01105
mg/L
pH (Lab) 00403
3.70
units
Ba - Barium 01007
ug/L
TOC 00680
1.70
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
81
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
Sulfate 00945
93
mg/L
Hg - Mercury 71900
ug/L
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L
Total Ammonia 00610
<0.2
mg/L
Mg - Magnesium 00927
mg/L
(Amm; n;a Nitrogen, Nh as N. Ammonia
Ni, oger! Total!
Mn - Manganese 01055
ug/L
TKN as N 00625
<0.5
mg/L
Ni - Nickel 01067
ug/L
For Remediation Svstems Only (Attach Lab R oor '):
Certification No. DWQ#94
Pb - Lead 01051 ug/L
Zn - Zinc 01092 mg/L
Other (Specify Compounds and Concentration Units):
Sodium 58.4 mq/L
ORGANICS: (by GC, GC/MS, HPLC)
(Specify test and method #. ATTACH LAB REPORT.)
Lab Report Attached? ■ Yes (0) ❑ No (0)
VOC 78732: method # SM 6200C
method #
method #
method #
mq/L Effluent Total VOCs:

GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
FACILITY INFORMATION Please Print Clearly or Type
Facility Name: Valley Proteins Inc.- Rose Hill
Permit Name (if different):
Facility Address: 469 Yellow Cut Rd.
Rose Hill, NC 28458
act Person: Corey Lanier
Location/Site Name:
County Duplin
Telephone#: [phone]
No. of wells to be sampled: 11
(from Permit)
PERMIT Number: WQ0000485 Expiration Date: 3131/2025
Non -Discharge UIC
NPDES Other
TYPE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
X Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump ❑ Other:
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): MW-13A
Date sample collected: 11/12/2022
FIELD ANALYSES:
WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH45wHB 4,40 units Temp. 00010: 222 oc
DRY at
Depth to Water Level 82546: 7.6 ft. below measuring point
Screened Interval: 16 ft. to 6 ft.
Spec- Cond. 00094_ uMhos
time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None
sampling,
Volume of water pumped/bailed before sampling: 5.0
gallons
Appearance Clear
check
SamDles for metals were collected unfiltered: X YES rt NO and field acidified: X YES n NO
here'E
Date sample analyzed:
11/12/2022-11/30/2022
Laboratory Name:
Environmental Chemists. Inc.
PARAMETERS NOTE: Values
should reflect dissolved
and colloidal concentrations.
COD 00335
mg/L
Nitrite (NOZ) as N 00615
<0.02 mg/L Pb - Lead 01051
Coliform: MF Fecal 31616
<1 /100mL
Nitrate (NO3) as N oo62o
0.03 mg/L Zn - Zinc 01092'
Coliform: MF Total 31504
/100mL
Phosphorus: Total as P 00665
<0.04 mg/L
Certification No. DWQ#94
ug/L
mg/L
(Note: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units):
)issolved Solids:Total 70300 66.00 mg/L Al -Aluminum o11o5 mg/L Sodium 5.7 mg/L
pH (Lab) 00403
4.40 units
Ba - Barium 01007
ug/L
TOC oosso
<0.5 mg/L
Ca - Calcium oo916
mg/L
Chloride 00940
6 mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 6.00
mg/L
Hg - Mercury7190o
ug/L
Lab Report Attached? M Yes (0) ❑ No (0)
Specific Conductance 00095
uMhos
K - Potassium 00937
mg/L
VOC 78732 method # SM 6200C
Total Ammonia oosso <0.20
mg/L
Mg - Magnesium 00927
mg/L
_
method #
(Ammonia Nitrogen; NFSas N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L
, method #
TKN as N oo625 <0.50
mg/L
Ni - Nickel 01067
ug/L
method #
For Rarnediation Systems
Lar Holt - General Manager
Permittee (or Authorized Agent) Name and Title - Please print or type

GROUNDWATER QUALITY MONITORING:
boom Mwr
COMPLIANCE REPORT FORM
FACILITY INFORMATION
Please Pdntclearly orType
PERMIT Number: WQ0000485 Expiration Date: 3/31/2025
Facility Name:
Valley Proteins
Inc.- Rose Hill
Non -Discharge UIC
Permit Name (if different):
NPDES Other
Facility Address:
469 Yellow Cut Rd,
TYKE OF PERMITTED OPERATION BEING MONITORED
Rose Hill, NC 28458
County Duplin
❑ Lagoon ❑ Remediation: Infiltration Gallery
pity) ;S, e
X Spray Field ❑Remediation:
Contact Person: Corey Lanier
Telephone#: [phone]
❑ Rotary Distributor ❑ Land Application of Sludge
Well Location/Site Name
No. of wells to be sampled: 11
❑ Water Source Heat Pump ❑ Other:
(From Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit):
MW-14A
Date sample collected 11/12/2022
FIELD ANALYSES: WAS
Well Depth: 16 ft.
Well Diameter: 2 in.
pH4500HB 4.70 units Temp. 0001c 21'9 °C DRY at
Depth to Water Level 82546: 6.8 ft. below measuring point
Screened Interval: 10 ft. to
2.5 ft. Spec. Cond. 00094: µMhos time of
Measuring Point is 3 ft. above land surface
Relative M.P. Elevation: ft.
Odor 00085: None sampling,
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance Red/Tan check
here:0
Samples for metals were collected unfiltered:
X YES
NO and field acidified: X YES NO
LABORATORY INFORMATION
Date sample analyzed 11/12/2022-11/30/2022
Laboratory Name: Environmental Chemists, Inc. Certification No. DWQ#94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD 00335
mg/L
Nitrite (NO2) as N 00615 <0.02
mg/L Pb - Lead o1o51 ug/L
Coliform: MF Fecal 31616 <1.0
/100mL
Nitrate (NO3) as N 00620 3.00
mg/L Zn - Zinc 01092 mg/L
Coliform: MF Total 31504
/100mL Phosphorus:
Total as P 00665 <0.04
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 944.00
mg/L
Al - Aluminum 01105
mg/L Sodium 85.2 mg/L
pH (Lab) 00403 4.70
units
Ba - Barium 01007
ug/L
TOC 00680 3.50
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940 350
mg/L
Cd - Cadmium 01027
ug/L
Arsenic 01002
ug/L
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper 01042
mg/L ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
ug/L (Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 133
mg/L
Hg - Mercury 71900
ug/L Lab Report Attached? 0 Yes (0) ❑ No (0)
Specific Conductance 00095
µMhos
K - Potassium 00937
mg/L VOC 76732: method # SM 6200C
Total Ammonia 00610 <0.20
mg/L
Mg - Magnesium 00927
mg/L method #
(Ammonia Nitrogen; NF3as N; Ammonia Nitrogen, Total)
Mn - Manganese 01055
ug/L method #
TKN as N 00625 0.60
mg/L
Ni - Nickel 01067
ug/L method #
For Remedlation Systems Only (Attach Lab Reports): Influent Total VOCs_ mg/L Utluent I otal VOUS: mg/L VUU Kernoval _r.
Larry Holt - General Manager
Perrnittee (or Authorized Agent) Name and Title - Please print or type

Valley Proteins, Inc - Rose Hill (WQ0000485) Groundwater Monitoring Well 2 Year Exceedance History Report
TDS 500
10A
11A
14A
November-22
833
583
944
July-22
772
510
1280
i March-22
783
527
1100
November-21
801
722
1230
July-21
706
522
1010
March-21
684
866
November-20
642
844
pH 6.5-8.5
2
4
7A
8A
9
10A
11A
12B
13A
14A
November-22
6
6.3
3.86
4.2
6
3.67
4.1
3.7
4.4
4.7
July-22
6.40
6.3
5.1
5.3
6.4
4.2
4.6
4
5.1
4.9
March-22
6.40
5.9
4.7
4.6
4.6
4.4
4.2
4.7
5.2
November-21
5.50
4.30
4.50
6.30
4.00
4.30
4.20
4.20
5.00
July-21
6.10
5.60
4.90
4.60
5.90
4.70
1 4.60
5.40
5.00
March-21
6.40
5.70
4.90
4.70
5.30
5.00
5.10
5.90
5.40
November-20
6.40
4.50
5.00
4.60
5.00
4.80
5.30
5.70
TOC 10
November-22
July-22
9
27.6
45.1
March-22
34.9
November-21
26.4
July-21
25.9
March-21
32.9
November-20
43.2
Chloride 250
10A
14A
November-22 2
July-22
305
261
350
356
March-22
294
325
November-21
353
July-21
425
275
March-21
November-20
295
285

ANALYTICAL & CONSULTING CHEMISTS
Environmental e iss, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28W 0 910.347.5843 Lab/Fax
info@environmentalchemismcom
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55556 Site: MW-1
11/12/2022
11:30 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
11/12/2022
Depth to water, ft.
Depth to water, Ft.
6.6 feet
11/12/2022
Sodium
EPA200.7, Rev 4.4,1994
7.26mg/L
11/21/2022
Sulfate
EPA 300.0, Rev.2.1, 1993
44 mg/L
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.Ogallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
106 mg/L
11/14/2022
Temperature
SM 2550 B-2010
21.9 C
11/12/2022
pH
SM 4500 H B-2011
5.6 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11 /23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
1.5 mg/L
11/15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
10 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 646 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1, 1, 1 -Trichloroethane
SW 846 Method 826oD/50308
<0.5 pg/L
11/15/2022
1,1,2,2-Tetrachloroethane
SW 846 Method8260D/5030B
<0.5 pg/L
11/15/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,1-Dichloroethane
SW 846 Method 826010/50308
<0.5 pg/L
11/15/2022
1,1-Dichloroethene
SW 846 Method8260D/5030B
<0.5pg/L
11/15/2022
1,1-Dichloropropene
SW 846 Method828OD/5030B
<0.5pg/L
11/15/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2, 3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2,4-Trichlorobenzene
SW 846 Method 626OD15030B
<0.5 pg/L
11/15/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Report #:: 2022-22633 Pagel or 33

Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO M
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report M 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8280D/5030B
<0.5 pg/L
11/15/2022
1,2-Dichlorobenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
11/15/2022
1,2-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1,2-Dichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1,3,5-Trimethylbenzene
SW 840 Method 82BOD/5030B
<0.5 pg/L
11/15/2022
1,3-Dichlorobenzene
SW 045 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1, 3-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
2-Chlorotoluene
SW 846 Method 8260DIS0308
<0.5 pg/L
11/15/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Bromobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/15/2022
Bromochloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Bromoform
SW 846 Method 82600/5030B
<0.5 pg/L
11/15/2022
Bromomethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/15/2022
Carbon tetrachloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Chlorobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
Chloroethene
SW 848 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chloroform
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/15/2022
Chloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
cis- 1,2-Dich loroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
Dibromomethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/15/2022
Dichlorodifluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Ethylbenzene
SW B46 Method 82BODIS030B
<0.5 pg/L
11 /15/2022
Hexachlorobutadiene
SW 846 Method 82600150308
<0.5 pg/L
11/15/2022
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Report#:: 2022-22633
Page 2 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmental a .s s, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 826OD/5030B
<1.0 pg/L
11/15/2022
Methylene chloride
SW 646 Method 826OD/5030B
<0.5 pg/L
11/15/2022
Naphthalene
SW 846 Method 826oD/5030B
<0.5 pg/L
11/15/2022
n-Butylbenzene
SW 846 Method 828DD15030B
<0.5 pg/L
11/15/2022
n-Propylbenzene
SW 846 Method 626013/50308
<0.5 pg/L
11/15/2022
ortho-Xylene
SW 846 Method 626013/50308
<0.5 pg/L
11/15/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
sec-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
Styrene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/15/2022
tert-Butylbenzene
SW 646 Method 826013/50308
<0.5 pg/L
11/15/2022
Tetrachloroethene
SW 646 Method 826OD/5030B
<0.5 pg/L
11/15/2022
Toluene
SW 846 Method 826013/503013
<0.5 pg/L
11/15/2022
Trans-1,2-Dichloroethene
SW 646 Method 826OD15030B
<0.5 pg/L
11/15/2022
Trans-1,3-dichloropropene
SW 646 Method 82BOD15030B
<0.5 pg/L
11/15/2022
Trichloroethene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/15/2022
Trichlorofluoromethane
SW 846 Method 826013/50308
<0.5 pg/L
11/15/2022
Vinyl chloride
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0,1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.28 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
0.28 mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0,1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11 /30/2022
Report it:: 2022-22633 Page 3 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentale is s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55557 Site: MW-2
11/12/2022
11:10 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
color
Tan
11/12/2022
Depth to water, ft.
Depth to water, Ft.
15.7 feet
11/12/2022
Sodium
EPA200.7, Rev4.4, 1994
12.1 mg/L
11/29/2022
Sulfate
EPA300.0, Rev.2.1, 1993
9 mg/L
11/17/2022
Ammonia Nitrogen
EPA350.1, Rev. 2.0,1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2640 C-2015
284 mg/L
11/14/2022
Temperature
SM 2550 B-2010
20.0 C
11/12/2022
pH
SM 4500 H B-2011
6.5 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/23/2022
Total Organic Carbon (TOC)
SM5310 B-2014
0.9mg/L
11/15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
9 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 Ng/L
11/15/2022
1, 1, 1 -Trichloroethane
SW 846 Method 826010/50308
<0.5 pg/L
11/15/2022
1,1,2,2-Tetrachloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/15/2022
1,1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /15/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,1-Dichloroethene
SW 846 Method 826013/50308
<0.5 pg/L
11/15/2022
1,1-Dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
1,2, 3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
Report #:: 2022-22633 Page 4 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmental Chemists, c.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 " 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/15/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1,2-Dichloropropane
SW 846 Method 8280D/50308
<0.5 pg/L
11/15/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1, 3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,4-Dichlorobenzene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/15/2022
2,2-Dichloropropane
SW 845 Method 82BOD/5030B
<0.5 pg/L
11/15/2022
2-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Benzene
SW 846 Method 8260D1503013
<0.5 pg/L
11/15/2022
Bromobenzene
SW 848 Method 8260D/50308
<0.5 pg/L
11/15/2022
Bromochloromethane
SW 846 Method B260D/50308
<0.5 pg/L
11/15/2022
Bromodichloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
Bromoform
SW 846 Method 826013/50308
<0.5 pg/L
11/15/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chloroform
SW 846 Method 8260015030B
<0.5 pg/L
11/15/2022
Chloromethane
SW 846 Method 826013/50306
<0.5 pg/L
11/15/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
cis-1,3-Dichloropropene
SW 845 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Dibromomethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Ethylbenzene
SW 846 Method 826013/503013
<0.5 pg/L
11/15/2022
Hexachlorobutadiene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
Isopropylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Report #:: 2022-22633 Page 5 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmental Cis s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ` 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November- Monitoring Wells
M+P Xylene
SW 845 Method 828013I503013
<1.0 pg/L
11/15/2022
Methylene chloride
SW 846 Method 8260DIS0309
<0.5 pg/L
11/15/2022
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
11/15/2022
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 Ng/L
11/15/2022
n-Propylbenzene
SW 846 Method 826013/503013
<0.5 pg/L
11 /15/2022
ortho-Xylene
SW 846 Method 826013/50308
<0.5 Ng/L
11/15/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 Ng/L
11/15/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Styrene
SW 846 Method 826OD150308
<0.5 Ng/L
11/15/2022
tert-Butylbenzene
SW 846 Method 8280D/5030B
<0.5 Ng/L
11/15/2022
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/15/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 Ng/L
11/15/2022
Trans-1,3-dichloropropene
SW 846 Method 8260DIS0300
<0.5 pg/L
11/15/2022
Trichloroethene
SW 846 Method 826OD15030B
<0.5 Ng/L
11/15/2022
Trichlorofluoromethane
SW 846 Method 82GODI5030B
<0.5 Ng/L
11/15/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0.1993
0.13 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
0.13 mg/L
11 /30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11/30/2022
Report #:: 2022-22633 Page 6 of 33

ANALYTICAL & CONSULTING CHEMISTS
entO Chemists, c.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-55558 Site: MW-4 11/12/2022 10:35 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Clear
11/12/2022
Depth to water, ft.
Depth to Water. Ft
9.6 feet
11 /12/2022
Sodium
EPA 200.7, Rev 4.4. 1994
11.2 mg/L
11/29/2022
Sulfate
EPA 300 0, Rev. 2 1.1993
<5 mg/L
11 /17/2022
Ammonia Nitrogen
EPA 350 1, Rev. 20. 1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
223 mg/L
11 /14/2022
Temperature
SM2550B-2010
21.1 C
11/12/2022
pH
SM 4500 H B-2011
6.3 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
0.7 mg/L
11/15/2022
Fecal Coliform
SM 9222 D-201 5 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
< 5 mg/L
11 /14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
1,1,2-Trichloroethane
SW 845 Method 826013/5030B
<0.5 pg/L
11/15/2022
1,1-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,1-Dichloroethene
SW 846 Method826OD15030B
<0.5pg/L
11/15/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2,3-Trichlorobenzene
SW 846 Method 82800/5030B
<0.5 pg/L
11/15/2022
1,2,3-Trichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1,2,4-Trimethylbenzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/15/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Report #:: 2022-22633 Page 7 of 33

ion
j�j � �'l�lY'�IC�IE'�� j . 1 • . 1, 1 1 1
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report M 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 62BOD/5030B
<0.5 pg/L
11/15/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
1,2-Dichloroethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/15/2022
1,2-Dichloropropane
SW 846 Method 626OD/50308
<0.5 pg/L
11/15/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
1, 3-Dichlorobenzene
SW 846 Method B260D15030B
<0.5 pg/L
11/15/2022
1,3-Dichloropropane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/15/2022
1,4-Dichlorobenzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/15/2022
2,2-Dichloropropane
SW 545 Method 8260D/50308
<0.5 pg/L
11/15/2022
2-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
4-Chlorotoluene
SW 846 Method 6260D/5030B
<0.5 pg/L
11/15/2022
Benzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11 /15/2022
Bromobenzene
SW 846 Method 82GOD150308
<0.5 pg/L
11/15/2022
Bromochloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Bromodichloromethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/15/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Bromomethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chlorobenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/15/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
cis-1,3-Dichloropropene
SW 846 Method 6260D/5030B
<0.5 pg/L
11/15/2022
Dibromochloromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/15/2022
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Dichlorodifluoromethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
Ethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Hexachlorobutadiene
SW 846 Method 6260D/50308
<0.5 pg/L
11/15/2022
Isopropyl benzene
SW 848 Method 8260D15030B
<0.5 pg/L
11/15/2022
Reportk 2022-22633
Page 8 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentale .s s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ® 910.392.0223 Lab * 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 82601)/503013
<1.0 pg/L
11/15/2022
Methylene chloride
SW 848 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Naphthalene
SW 846 Method 826OD15030B
<0.5 pg/L
11/15/2022
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/15/2022
n-Propylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
p-Isopropyltoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/15/2022
sec-Butylbenzene
SW 846 Method 82SOD15030B
<0.5 pg/L
11/15/2022
Styrene
SW 846 Method 826013/503013
<0.5 pg/L
11/15/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Tetrachloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/15/2022
Trans-1 ,2-Dichloroethene
SW 846 Method 82600/5030B
<0.5 pg/L
11/15/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/15/2022
Trichloroethene
SW 846 Method B260D15030B
<0.5 pg/L
11/15/2022
Trichlorofluoromethane
SW 846 Method 826OD150308
<0.5 pg/L
11/15/2022
Vinyl chloride
SW 846 Method 826OD/50308
<0.5 pg/L
11/15/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2-0, 1993
< 0.02 mg/L
11/1412022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
<0.02mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11/30/2022
Report V 2022-22633 Page 9 of 33

ANALYTICAL & CONSULTING CHEMISTS
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Lab ID Sample ID:
22-55559 Site: MW-7A
Test
Color
Depth to water, ft.
Sodium
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
1, 1, 1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1, 1 -Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2, 3-Trichlorobenzene
1,2, 3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
Environmental Chemists, c.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Date of Report: Dec 21, 2022
Customer PO M
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Collect Date/Time Matrix
11/12/2022 12:00 PM Water
Method
Color
Depth to Water, Ft.
EPA 200.7, Rev 4.4, 1994
EPA 300.0, Rev. 2.1, 1993
EPA 350.1, Rev. 2.0. 1993
Gallons Balled before sampling
Qualitative
SM 2540 C-2015
SM 2550 B-2010
SM 4500 H B-2011
SM 4500 P (F-H)-2011
SM 5310 B-2014
SM 9222 D-2015 MF
SM4500 CI E-2011
SW 846 Method 826010/5030B
SW 846 Method 8260D/5030B
SW 846 Method 826010/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8280D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 846 Method 826010/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 626013/5030B
Results
Sampled by
jcb/envirochern
Date Analyzed
Tan
11/12/2022
6.0 feet
11/12/2022
36.4 mg/L
11 /29/2022
20 mg/L
11/17/2022
< 0.2 mg/L
11/18/2022
5.0gallons
11/12/2022
None
11/1212022
297 mg/L
11/14/2022
21.7 C
11/12/2022
3.86estunits
11/12/2022
< 0.04 mg/L
11/23/2022
1.3mg/L
11/15/2022
<1 Colonies/100ml-
11/12/2022
117 mg/L
11/14/2022
<0.5pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5 Ng/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 10 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentale s s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO M
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report M 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 826DD/6030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 646 Method 8260D/50308
<0.5 Ng/L
11/16/2022
4-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 828oD/5030B
<0.5 pg/L
11 /16/2022
Bromodichloromethane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Chloroform
SW 845 Method 8260D15030B
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
cis-1,3-Dichloropropene
SW 848 Method 826OD15030B
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 848 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 828oD/50308
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Isopropylbenzene
SW 845 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 71 of 33

Darling Ingredients - Rose HIII
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 8260D/50308
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 62BOD/5030B
<0.5 pg/L
11/16/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 82BOD150308
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 826oD/50308
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev.2.0,1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev.2.0, 1993
< 0.02 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev 2.0. 1993
< 0.5 mg/L
11 /23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11/30/2022
Report p:: 2022-22633 Page 12 of 33

ANALYTICAL & CONSULTING CHEMISTS
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Lab ID Sample ID:
22-55560 Site: MW-8A
Test
Color
Depth to water, ft.
Sodium
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2, 3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
Environmental Chemists, c.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab ® 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ® 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
info@environmentalchemismcom
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Collect Date/Time Matrix
11/12/2022 12:15 PM Water
Method
Color
Depth to Water, Ft.
EPA 200.7, Rev 4.4, 1994
EPA 300.0, Rev. 2.1. 1993
EPA 350.1, Rev. 2.0, 1993
Gallons Bailed before sampling
Qualitative
SM 2640 C-2015
SM 2550 B-2010
SM 4500 H B-2011
SM 4500 P (F-H)-2011
SM 5310 B-2014
SM 9222 D-2015 MF
SM4500 CI E-2011
SW 846 Method 8260D/5030B
SW 846 Method 8260D15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8280D/5030B
SW 845 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8280D/5030B
SW 846 Method 826OD15030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
Results
Sampled by
jcb/envirochem
Date Analyzed
Tan
11/12/2022
7.0 feet
11/12/2022
2.32 mg/L
12/17/2022
23 mg/L
11/17/2022
< 0.2 mg/L
11/18/2022
5.0gallons
11/12/2022
None
11/12/2022
86 mg/L
11/14/2022
21.9 C
11 /1212022
4.2units
11/12/2022
<0.04mg/L
11/23/2022
0.6 mg/L
11 /15/2022
<1 Colonies/100ml-
11/12/2022
8 mg/L
11/14/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5pg/L
11/16/2022
Report #:: 2022-22633 Page 13 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentale is s,
6602 Windmill Way, Wilmington, NC 28405 ' 910.392,0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info@environmentalchemismcom
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW B46 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 826013I503013
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Bromobenzene
SW B46 Method 826013/50308
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 82SOD15030B
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 82BODI6030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 846 Method 828013/50308
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 626013/503013
<0.5 pg/L
11/16/2022
Isopropylbenzene
SW 846 Method 828013/503013
<0.5 pg/L
11/16/2022
Report #:: 2022-22633
Page 14 of 33

Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method a260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 826013/5030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/1612022
n-Butylbenzene
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 848 Method 8280D/50308
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 828013/503013
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
sec-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 848 Method 8260D/50308
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 828oD/50308
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0,1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
1.42 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
1.42 mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA351.2, Rev.20, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
1.4 mg/L
11/30/2022
Report #:: 2022-22633 Page 15 of 33

ANALYTICAL & CONSULTING CHEMISTS
e � Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55561 Site: MW-9
11/12/2022
10:50 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
None
11/12/2022
Depth to water, ft.
Depth to water, Ft.
8.0 feet
11/12/2022
Sodium
EPA200.7, Rev 4.4,1994
5.19mg/L
11/29/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
22 mg/L
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev, 2.0, 1993
< 0.2 mg/L
11 /18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
374 mg/L
11/14/2022
Temperature
SM 2550 B-2010
19.6 C
11/12/2022
pH
SM 4500 H B-2011
6.0 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
0.12 mg/L
11/23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
27.6 mg/L
11 /15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
35 mg/L
11/14/2022
1. 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1,2-Trichloroethane
SW 846 Method 826oD/5030B
<0.5 pg/L
11/16/2022
1, 1 -Dichloroethane
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1-Dichloropropene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2, 3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,4-Trichlorobenzene
SW 848 Method 826OD15030B
<0.5 pg/L
11/16/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Report P: 2022-22633 Page 16 of 33

Environmental Chemists, Inc.
Wilmington,6602 Windmill Way, 28405 910.392.0223
710 CONSULTING
ANALYTICAL & o@
Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /16/2022
1,2-Dichloropropane
SW 846 Method 826OD/503OB
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 845 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 845 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 845 Method 8260DI5030B
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 828oD/5030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Carbon tetrachloride
5W 846 Method 826oD15030B
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
CIS-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Isopropylbenzene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Report #:: 2022-22633
Page 17 of 33

Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November- Monitoring Wells
M+P Xylene
SW 846 Method 8280D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 848 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
tert-B utyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 626013/50308
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 7-0,1993
0.11 mg/L
11 /14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
1.86 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
1.75mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA351.2, Rev. 2.0,1993
1.7 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
3.6 mg/L
11/30/2022
Report #:: 2022-22633 Page 18 of 33

Environmental
CONSULTINGANALYTICAL & •@
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55562 Site: MW-10A
11/12/2022
10:15 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
color
Brown
11/12/2022
Depth to water, ft.
Depth to Water, Ft.
5.3 feet
11 /12/2022
Sodium
EPA 200.7, Rev 4.4, 1994
138 mg/L
12/17/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
137 mg/L
11 /17/2022
Ammonia Nitrogen
EPA 350.1. Rev. 2.0, 1993
0.5 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
833 mg/L
11/14/2022
Temperature
SM 2550 B-2010
20.5 C
11/12/2022
pH
SM 4500 H B-2011
3.67est. units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
3.6 mg/L
11/15/2022
Fecal Coliform
SM 9222 1 -2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
305 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1, 1, 1 -Trichloroethane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
1,1,2,2-Tetrachloroethane
SW 646 Method 826OD15030B
<0.5 pg/L
11/16/2022
1,1,2-Trichloroethane
SW 846 Method 825OD150308
<0.5 pg/L
11/16/2022
1,1-Dichloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1,1-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,1-Dichloropropene
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,3-Trichloropropane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,4-Trimethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11 /16/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 19 of 33

nvironmental Chemists, Inc.
4ilwoc-
ANALYTICAL & CONSULTING CHEMISTS •@
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 845 Method 826OD/5030B
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D150308
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 846 Method 820DD/5030B
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 848 Method 826oD/5030B
<0.5 pg/L
11 /16/2022
2-Chlorotoluene
SW 846 Method 826oD/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 828oD/50308
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 845 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
lsopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633
Page 20 of 33

Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW B46 Method 8260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 82600/50308
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 82600/50308
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 8260015030E
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 826013150308
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
sec-Butylbenzene
SW 846 Method 82600/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 82GOD/5030B
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260D150308
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0,1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
< 0.02 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2 0. 1993
0.9mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
0.9 mg/L
11/30/2022
Report #:: 2022-22633 Page 21 of 33

i
ANALYTICAL & CONSULTING CHEMISTS
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Lab ID Sample ID:
22-55563 Site: MW-11A
Test
Color
Depth to water, ft.
Sodium
Sulfate
Ammonia Nitrogen
Gallons bailed before sampling
Odor
Total Dissolved Solids (TDS)
Temperature
pH
Total Phosphorus
Total Organic Carbon (TOC)
Fecal Coliform
Chloride
1, 1, 1,2-Tetrachloroethane
1,1,1-Trichloroethane
1,1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1, 1 -Dichloroethene
1,1-Dichloropropene
1,2,3-Trichlorobenzene
1,2,3-Trichloropropane
1,2,4-Trichlorobenzene
1,2,4-Trimethylbenzene
1,2-Dibromo-3-Chloropropane
Eninironmental Chemists, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
71.0 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 " 910.347.5843 Lab/Fax
info®environmentalchemists.com
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Collect Date/Time Matrix
11/12/2022 9:30 AM Water
Method
Color
Depth to Water, Ft.
EPA 200.7, Rev 4.4, 1994
EPA 300.0, Rev. 2.1, 1993
EPA 350.1, Rev. 2.0, 1993
Gallons Bailed before sampling
Qualitative
SM 2540 C-2015
SM 2550 B-2010
SM 4500 H 8-2011
SM 4500 P (F-H)-2011
SM 5310 B-2014
SM 9222 D-2015 MF
SM4500 Cl E-2011
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260W5030B
SW 846 Method 82GOD/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 82601315030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 846 Method 8260D/5030B
SW 648 Method 82BOD/5030B
SW 846 Method 6260D/5030B
Results
Sampled by
jcb/envirochem
Date Analyzed
Clear
11/12/2022
7.7 feet
11/12/2022
72.4mg/L
11/29/2022
186 mg/L
11/17/2022
< 0.2 mg/L
11/18/2022
5.0 gallons
11/12/2022
None
11/12/2022
583 mg/L
11/14/2022
21.5 C
11/12/2022
4.1 units
11/12/2022
< 0.04 mg/L
11/23/2022
2.5mg/L
11/15/2022
<1 Colonies/100ml-
11/12/2022
145 mg/L
11/14/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
<0.5 pg/L
11/16/2022
Report A: 2022-22633 Page 22 of 33

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ANALYTICAL &CONSULTING CHEMISTS
Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
1, 3,5-Trimethylbenzene
SW 846 Method 8260D/50309
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 848 Method 8280D/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 848 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromodichloromethene
SW 846 Method 826oD/5030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 046 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Isopropyl benzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633
Page 23 of 33

Environmental
CONSULTINGANALYTICAL & .@
Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 828013/50306
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 826oD/5030B
<0.5 pg/L
11/16/2022
sec -Butyl benzene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA353.2, Rev. 2.0, 1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
0.60 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
0.60 mg/L
11 /30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
0.6 mg/L
11/30/2022
Report #:: 2022-22833 Page 24 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentalsts,
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab m 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ` 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55564 Site: MW-12B
11/12/2022
10:00 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
11/12/2022
Depth to water, ft.
Depth to Water, Ft.
7.4 feet
11/12/2022
Sodium
EPA200.7, Rev4.4, 1994
58.4mg/L
11/29/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
93 mg/L
11/17/2022
Ammonia Nitrogen
EPA350.1, Rev. 2.0, 1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
309 mg/L
11 /14/2022
Temperature
SM 2550 B-2010
21.6 C
11/12/2022
pH
SM 4500 H B-2011
3.70est. units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
0.05 mg/L
11 /23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
1.7 mg/L
11/15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 CI E-2011
81 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
1,1,1-Trichloroethane
SW 846 Method8260D15030B
<0.5pg/L
11/16/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
1,1,2-Trichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
1,1-Dichloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
1,2,3-Trichloropropane
SW 846 Method 826013/5030B
<0.5 pg/L
11/16/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,4-Trimethylbenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 25 of 33

0
ANALYTICAL & CONSULTING CHEMISTS
Environmentale iss, Inc.
6602 Windmill Way, Wilmington, NC 28405 * 910.392.0223 Lab ` 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 848 Method 82BOD/50308
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 82SOD15030B
<0.5 pg/L
11/16/2022
1, 3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 82SOD15030B
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Bromochloromethane
sw 846 Method 02GOD15030B
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 848 Method 8260W5030B
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 82SOD15030B
<0.5 pg/L
11/16/2022
Chloroethane
SW 848 Method 826OD/50308
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
cis- 1, 3-Dichloropropene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 828oD/50308
<0.5 pg/L
11/16/2022
Isopropylbenzene
SW 846 Method 8260D/50300
<0.5 pg/L
11/16/2022
Report #.: 2022-22633
Page 26 of 33

ANALYTICAL 8 CONSULTING CHEMISTS
Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, I ianteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 646 Method 8260D/5030B
<0.5 pg/L
11 /1612022
n-Butylbenzene
SW 846 Method 8260131503013
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 82a0D/5030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1 ,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 826oD/5030B
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 0260D/5030B
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0. 1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0,1993
0.10 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
0.10 mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11 /30/2022
Report #:: 2022-22633 Page 27 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmentale is s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Post Office Box 1026
Rose Hill NC 28458
Attention:
Date of Report: Dec 21, 2022
Customer PO #:
Customer ID: 08100027
Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-55565 Site: MW-13A
11/12/2022
9:45 AM Water jcb/envirochem
Test
Method
Results Date Analyzed
Color
Color
Clear
11/12/2022
Depth to water, ft.
Depth to Water, Ft.
7.6 feet
11/12/2022
Sodium
EPA200.7, Rev 4,4, 1994
5.70 mg/L
11/29/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
6 mg/L
11/17/2022
Ammonia Nitrogen
EPA350.1, Rev. 2.0,1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Bailed before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 0-2015
66 mg/L
11 /14/2022
Temperature
SM 2550 B-2010
22.2 C
11/12/2022
pH
SM 4500 H B-2011
4.4 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/23/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
<0.5 mg/L
11 /15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100mL
11/12/2022
Chloride
SM4500 Cl E-2011
6 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 828OD/5030B
<0.5 pg/L
11/16/2022
1, 1, 1 -Trichloroethane
SW 846 Method 82600/5030B
<0.5 pg/L
11/16/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,1,2-Trichloroethane
SW 845 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,1-Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
1,1-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,1-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2,3-Trichlorobenzene
SW 846 Method 82600150308
<0.5 pg/L
11/16/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
1,2,4-Trimethylbenzene
SW 848 Method 8260D15030B
<0.5 pg/L
11/16/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/503013
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 28 of 33

Environmental Chemists, Inc.
ANALYTICAL & CONSULTING CHFMISTS oi
Darting Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO M
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report M 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 82GODI5030B
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichlorobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
1, 3-Dichloropropane
SW 846 Method 6260DI5030B
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 628oD/5030B
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 8260DIS0308
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 82GOD15030B
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /16/2022
Carbon tetrachloride
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 82600/503013
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloromethane
SW 845 Method 826OD/50308
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
cis-1,3-Dichloropropene
SW 845 Method 82SOD/5030B
<0.5pg/L
11/16/2022
Dibromochloromethane
SW 646 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 8260DIS030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Isopropylbenzene
SW 840 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633
Page 29 of 33

ANALYTICAL & CONSULTING CHEMISTS
EnvironmentalChemists,Inc.
Wi 6602 ndW Way, Wiirning tong NC 28405 ' 910.398.0223 Lab * 910.392.4424 Fax
71013owsertown Road, lVlanteo, NC 27954 `" 252..473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 848 Method 8260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
ortho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
sec -Butyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 8260D/50308
<0.5 Ng/L
11/16/2022
Toluene
SW 846 Method 8260D/50306
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA353.2, Rev. 2.0, 1993
0.03 mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
0.03mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
< 0.5 mg/L
11/23/2022
Total Nitrogen
Total Nitrogen
<0.5 mg/L
11/30/2022
Report P: 2022-22633 Page 30 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmental a is s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473,5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill Date of Report: Dec 21, 2022
Post Office Box 1026 Customer PO #:
Rose Hill NC 28458 Customer ID: 08100027
Attention: Report #: 2022-22633
Project ID: November - Monitoring Wells
Lab ID Sample ID: Collect Date/Time Matrix Sampled by
22-55566 Site: MW-14A 11/12/2022 11:45 AM Water jcb/envirochem
Test Method Results Date Analyzed
Color
color
Red/Tan
11/12/2022
Depth to water, ft.
Depth to water, Ft.
6.8 feet
11/12/2022
Sodium
EPA 200.7, Rev 4.4,1994
85.2 mg/L
11/29/2022
Sulfate
EPA 300.0, Rev. 2.1. 1993
133 mg/L
11/17/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
< 0.2 mg/L
11/18/2022
Gallons bailed before sampling
Gallons Balled before sampling
5.0 gallons
11/12/2022
Odor
Qualitative
None
11/12/2022
Total Dissolved Solids (TDS)
SM 2540 c-2015
944 mg/L
11 /14/2022
Temperature
SM 2550 B-2010
21.9 C
11/12/2022
pH
SM 4500 H B-2011
4.7 units
11/12/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
11/2312022
Total Organic Carbon (TOC)
SM 5310 B-2014
3.5 mg/L
11/15/2022
Fecal Coliform
SM 9222 D-2015 MF
<1 Colonies/100ml-
11/12/2022
Chloride
SM4500 Cl E-2011
350 mg/L
11/14/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1,1,1-Trichloroethane
SW 846 Method8280D/5030B
<0.5pg/L
11/16/2022
1,1,2,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1,2-Trichloroethane
SW 846 Method8260D/5030B
<0.5pg/L
11/16/2022
1,1-Dichloroethane
SW 846 Method 826010/5030B
<0.5 pg/L
11/16/2022
1,1-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,1-Dichloropropene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,2,3-Trichlorobenzene
SW 646 Method 826013/5030B
<0.5 Ng/L
11/16/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 Ng/L
11/16/2022
1,2,4-Trichlorobenzene
SW 846 Method 6260D/5030B
<0.5 pg/L
11/16/2022
1,2,4-Trimethylbenzene
SW 646 Method 8260D/5030B
<0.5 Ng/L
11/16/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 6260D/5030B
<0.5 pg/L
11/16/2022
Report #:: 2022-22633 Page 31 of 33

�i �p%iii�iiiiiiiii • /�rf %gipp% rr /���
ANALYTICAL & CONSULTING CHEMISTS
Environmental e is s, Inc.
6602 WindmM Way, Wilmington, NC 28405 ' 910.392.0223 Lab " 910.392.4424 Fax
710 Bowsetrtown load, Manteo, NC 27954 * 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
[e-mail]
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
1,2-Dibromoethane
SW B46 Method 8260D15030B
<0.5 pg/L
11/16/2022
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/16/2022
1,2-Dichloroethane
SW 846 Method 82GOD/50308
<0.5 pg/L
11/16/2022
1,2-Dichloropropane
SW 846 Method 82BOD/50308
<0.5 Ng/L
11/16/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/6030B
<0.5 pg/L
11/16/2022
1, 3-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
1,3-Dichloropropane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
2,2-Dichloropropane
SW 846 Method 826OD/50308
<0.5 pg/L
11/16/2022
2-Chlorotoluene
SW 846 Method 8280D/5030B
<0.5 pg/L
11/16/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Benzene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Bromobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Bromochloromethane
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Bromodichloromethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Bromoform
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Bromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Carbon tetrachloride
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Chlorobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/16/2022
Chloroethane
SW 846 Method 8260DI50308
<0.5 pg/L
11/16/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Chloromethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/16/2022
cis-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 ug/L
11/16/2022
cis-1,3-Dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dibromochloromethane
SW 846 Method 8280D/50308
<0.5 pg/L
11/16/2022
Dibromomethane
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Dichlorodifluoromethane
SW 846 Method 82BOD/50308
<0.5 pg/L
11/16/2022
Ethylbenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
Hexachlorobutadiene
SW 846 Method 8280D/5030B
<0.5 Ng/L
11/16/2022
Isopropylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Report 9: 2022-22633
Page 32 of 33

ANALYTICAL & CONSULTING CHEMISTS
Environmental e is s, Inc.
6602 Windmill Way, Wilmington, NC 28405 ' 910.392.0223 Lab ' 910.392.4424 Fax
710 Bowsertown Road, Manteo, NC 27954 ' 252.473.5702 Lab/Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ' 910.347.5843 Lab/Fax
info@environmentalchemismcom
Darling Ingredients - Rose Hill
Date of Report: Dec 21, 2022
Post Office Box 1026
Customer PO #:
Rose Hill NC 28458
Customer ID: 08100027
Attention:
Report #: 2022-22633
Project ID: November - Monitoring Wells
M+P Xylene
SW 846 Method 8260D/5030B
<1.0 pg/L
11/16/2022
Methylene chloride
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
n-Butylbenzene
SW 846 Method 82801350308
<0.5 pg/L
11/16/2022
n-Propylbenzene
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
oltho-Xylene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
p-Isopropyltoluene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/16/2022
sec-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Styrene
SW 846 Method 826013/50308
<0.5 pg/L
11/16/2022
tert-Butylbenzene
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
Tetrachloroethene
SW 846 Method 826013/503013
<0.5 pg/L
11/16/2022
Toluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/16/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D/50308
<0.5 pg/L
11/16/2022
Trichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11 /16/2022
Trichlorofluoromethane
SW 846 Method 82BOD15030B
<0.5 pg/L
11/16/2022
Vinyl chloride
SW 846 Method 8260D15030B
<0.5 pg/L
11/16/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0.1993
< 0.02 mg/L
11/14/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2,Rev. 2.0,1993
3.00mg/L
11/15/2022
Nitrate Nitrogen
Subtraction Method
3.00mg/L
11/30/2022
Total Nitrogen (Calc)
Total Kjeldahl Nitrogen (TKN)
EPA 351.2, Rev. 2.0, 1993
0.6 mg/L
11 /23/2022
Total Nitrogen
Total Nltrogen
3.6 mg/L
11/30/2022
Comment:
Reviewed by:
Report #: 2022-22833 Page 33 of 33

Environmental Chemist, Inc., Wilmington, NC Lab #94 6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Sample Receipt Checklist
... Date.. Report Number: _
ipt
BYES f sample,NO '—§
ECHO/APickup e ry ❑'W UPS ❑' FedEx^q Other ❑
❑
_Y
_ Xmmm
m .. ----- y
l sDeallds re '
_p nt on the cooler?
❑ YES
❑
NO
!e�retcustocly
N/A '2. od seals were resent, were they intact/unbroken?
P
Original temperature upon receipt L) °C Corrected temperature upon receipt � _ �_°C
How temperature taken:
_ ❑ Temperature Blank Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657'W
IR Gun Correction Factor °C: 0.0
YES
❑
NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
YES
❑
NO
4. Were proper custody procedures (relinquished/received) followed?
YES
❑
NO
_T Were sample ID's listed on the COC?
YES
❑
NO
6. Were samples ID's listed on sample containers?
Xr YES
❑
NO
7. Were collection date and time listed on the COO
YES
❑
NO
8. Were tests to be performed listed on the COC?
YES
❑
NO
9. Did samples arrive in proper containers for each test?
YES
❑
NO
10. Did samples arrive in good condition for each test?
YES
❑
NO
11. Was adequate sample volume availableT
YES
❑
NO
12. Were samples received within proper holding time for requested tests?
YES
❑
NO
13. Were acid preserved samples received at a pH of <2?
YES
❑
NO
14. Were cyanide samples received at a pH >12?
❑ YES
❑
NO
15. Were sulfide samples received at a pH >9?
YES
❑
NO
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 rI **
171 YES iD
NO
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
❑ YES
❑
NO
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
Time of preservation,; _ If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s)were received with headspace
COMMENTS:
DOC. QA.002 Rev 1

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