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HomeMy WebLinkAbout820634_NOV-2021-DV-0169 Enforcement Packet w photos_20210812U.S. POSTAL SERVICE CERTIFIED MAIL RECIEPT LISPS Certified Mail - A receipt (this portion of tetyrtC d provides the • A unique identifier folio win lectronic verification of r ilptece. delivery, delivery or attempted • A record of delivery (including the recipient's signature) that is retained by the Postal Service'" for a specified period. Important Reminders: • You may purchase Certified Mail service First -Class Mail®, First -Class packs with or Priority Mail® service. Package Service® ■ Certified Mail service is notavailable for international mail. • In E fierfor • yo label) nce covers requires the si oted delivery Service, with Certified coverage is notavailable forand provides delve to be at least 21 which of Certified Mail service. However, thpurchase delivery to the addressees years of age Mail service does Purchase by name, or to the addressee's authorized specified insurance covers not change the (not available certain Priori ge automatically inclu • To ' For an additional hfee, and included with endorsement on the with a Proper the followingmailpiece, you may request services; - Return receipt service, which provides a record of delivery (including the recipient's signature). You can request a hardCop yFor return receiptOanr complete PS Form 3a � rdcopy returreceipt, Receipt, attach PS ��' Domestic Return 3811 to your mailpiece; 3$ for an electronic returngbenefits: associate for assistance.receipt see a retail return receipt for no To receive a duplicate LISPS®. additional fee, P chts retail associate.arked Certified Mail receipt tento the - Restricted delivery service, which provides delivery to the addressee specified by name, or to the addressee's authorized agent. - Adult signature service, which requires the signee to be at least 21 years of age (not available at retail). - Adult signature restri Form PS F 00, April 2015 (Reverse) PSN 7530-02-000- s0a7 receipt for your records. CKING # F. l �tllA 9590 9402 6135 0209 3298 II United States �� Postal Service ure that your Certified Mail receipt is accepted as legal proof of mailing, it should bear a LISPS postmark, If you u would like a postmark on this Certified Certified Mail receipt, please item at a Post Office' present your postmarking. If you don't need for Certified Mail receipt, detach the Postmark on of this label, affix it to the barappl this appropriate postage,mailpiece, opl Portion and deposit the y mailpiece. IMPONTANP Save this First -Class Mail Postage & Fees Paid USPS Permit No. G-10 • Sender: Please print your name, address ZIP�4® NCDEQ _ DIV. OF WATER RESOUR in this box• ATTN: KATIE FONTENOT URCES 225 GREEN STREET, SUITE 714 FAYETTEVILLE NC 28301-5095 diljg/gijjllijlj j�`Z j iij j IT' C1 CI ru D IL U.S. Postal ServiceTM CERTIFIED MAIL° RECEIPT Domestic Mail Only For delivery information, visit our website at www.usps.com®. Certified Mail Fee Extra Services & Fees (check box, add fee as appropriate) ❑ Retum Receipt (hardcopy)ID $ Return Receipt (electronic) $ ❑Certified Mall Restricted Delivery $ DAdult Signature Required ❑Adult5ignature Restricted Delivery $ Postage Total Pos ge end Fees $ I" ` 1 r Sent To Postmark Here City, State ZlP ----....---------- -_ ..... .... 1 :�- PS Form 3800, April 20'15 PSN 7530-02.coo.00a7 SENDER: COMPLETE THIS SECTION ■ Complete items 1, 2, and 3. ■ Print your name and address on the reverse so that we can return the card to you. ■ Attach this card to the back of the mailpiece, or on the front if space permits. 1. Article Addressed to: TAMMY BUTLER PETERSON 10444 N US 421 HWY CLINTON, NC 28328 ssso saoz si3s ozos azse oa 2. Article Number (Transfer from service label) 7020 0090 0001 7206 7340 PS Form 3811, July 2015 PSN 7530-02-000-9053 See Reverse for Instructions COMPLETE THIS SECTION ON DELIVERY A. Signature X_ .� B. Receive • by (Printed Name) ❑ Age ❑ 1;uaressee C. Date of Delivery D. Is delivery address different from item 1? 0 Yes If YES, enter delivery address below: 0 No 3. Service Type ❑ Adult Signature ❑ Adult Signature Restricted Delivery on Certified Mail® ❑ Certified Mail Restricted Delivery ❑ Collect on Delivery ❑ Collect on Delivery Restricted Delivery lail Restricted Delivery o Priority Mall Express® ❑ Registered Ma1ITM 0 Registered Mail Restricted )(Relivery eturn Receipt for Merchandise ❑ Signature ConfirmationTM ❑ Signature Confirmation Restricted Delivery Domestic Return Receipt NOTICE OF VIOLATION AND/OR NOTICE OF INTENT ROY COOPER Governor DIONNE DELLI-GATTI Secretory S. DANIEL SMITH Director NORTH CAROLINA Environmental Quality April 30, 2021 CERTIFIED MAIL RETURN RECEIPT REQUESTED 7020 0090 0001 7206 7340 Tammy Butler Peterson 10444 N US 421 Hwy Clinton NC 28328 Subject: NOTICE OF VIOLATION/NOTICE OF INTENT Administrative Code 15A NCAC 2T .1304 NOV-2021-DV-0169 Tammy Peterson Farm Facility Number 82-634 Permit AWS820634 Sampson County Dear Tammy Peterson, On February 25, 2021, staff of the NC Department of Environmental Quality (DEQ) Division of Water Resources (DWR), Water Quality Regional Operations Section (WQROS) inspected the Tammy Peterson Farm and the permitted waste disposal system. We wish to thank Mr. Curtis Barwick for his assistance during this inspection. As a result of this inspection, you are hereby notified that, having been permitted to have a non - discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2T .1304, you have been found to be in violation of your permit as follows: North Carolinsi De°n to Fa}'ctte:ille Regional ()I1 9i0.4:33„ :500 ironmental i)uolity Division ofWater Resources xrc°c n Streel, Suite 714 Fayetteville, North Carolina 28:301 Page 2 Tammy Peterson April 30, 2021 Violation 1: The collection, treatment and storage facilities, and the land application equipment and fields shall be properly operated and maintained at all times. — [15A NCAC 02T. 1304(b)]. (Permit No. AWG 100000 Section Conditions II 1). On February 25, 2021, DWR staff surveyed the lagoon due to the lagoon being reported as not in compliance. The freeboard marker was reported reading 7 inches". During the lagoon survey, DWR staff noticed waste had appeared to have flowed from the foundation of house two (2) into the drainage system designed to divert rain water away from the lagoon. DWR staff noticed there was multiple trenched paths that allowed the waste to flow into the ditch at the corner of the lagoon that runs behind the lagoon. DWR documented with pictures and water samples that the waste entered the ditch. Once waste mixes with rainwater is its now considered to be waste. Mr. John Peterson stated on February 26, 2021 that the discharge pipe going to the lagoon has a blockage that caused the waste to flow out of the hog house. Based on the amount of waste still between the buildings this could have happened multiple times. Required Corrective Action for Violation 1: In the future, monitor the permitted storage facilities and collections systems. In the event that there is waste that leaves your storage facility or waste collection system, contain the waste and prevent waste from leaving and entering surface waters. Waste should never be allowed to flow into surface waters intentionally. Mr. John Peterson stated on February 26, 2021 that the discharge pipe going to the lagoon has a blockage, but a farm employee had cleared the blockage. In the future, make sure your employees understand the importance of reporting any issues with your waste collection system. Violation 2: Any discharge of waste that reaches surface waters or wetlands is prohibited except as otherwise provided in this General Permit and associated statutory and regulatory provisions. Waste shall not reach surface waters or wetlands by runoff, drift, manmade conveyance, direct application, direct discharge or through ditches, terraces, or grassed waterways not otherwise classified as state waters. The waste collection, treatment, storage and application system operated under this General Permit shall be effectively maintained and operated as a non -discharge system to prevent the discharge of pollutants to surface waters or wetlands. Application of waste to terraces and grassed waterways is acceptable as long as it is applied in accordance with Natural Resources Conservation Service (MRCS) Standards and does not result in a discharge of waste to surface waters or wetlands. (Permit No. AWGI 00000 Section Conditions I 1). North Carolina Department of Environmental Quality l Division of Water Resources Fayetteville Regional Office 225 Green Street. Suite 7I•1 Fayetteville. North Carolina Zi 301 910.433.3 00 Page 3 Tammy Peterson April 30, 2021 On February 25, 2021 during the site evaluation, DWR staff was able to document with pictures and water samples that waste entered a ditch. There were multiple manmade conveyances that were trenched that would allow for waste to flow into the ditch located at the corner of the lagoon that flows behind the lagoon out into the woods. It appeared that waste flowed from the foundation of house two (2) into the drainage system that is designed for rain water and ponded in a low area at the corner of the lagoon near the ditch; which then was trenched to flow in the ditch. Once waste mixes with standing rain water it now becomes contaminated and is considered waste. Required Corrective action for Violation 2: In the future, return waste to the lagoon or the house. If waste is mixed with rainwater it is still considered waste. In the future don't allow waste to flow into surface waters. In no case should waste ever be diverted to surface waters. In the case where waste leaves a waste collection system, effort must be made to assure waste does not leave. You can return the waste to the lagoon or houses or berms of soil can be added to prevent waste to flow into ditches until the waste can be returned to the collection system. You can contain the waste so it does not leave the site until it can be returned to the lagoon or collection system. In no situation should you divert waste even if it is mixed with rain water to surface waters. Violation 3: The Permittee shall report by telephone to the appropriate Division Regional Office as soon as possible, but in no case more than twenty-four (24) hours following first knowledge of the occurrence of any of the following events: A. failure of any component of the animal waste management system resulting in a discharge to diches, surface waters, or wetlands. — [15A NCAC 02T. 1304(b)]. (Permit No. AWG 100000 Section Conditions III 17 A). Your permit specifically requires notification by telephone within 24 hours and a written report within 5 calendar days following first knowledge of the occurrence of a reportable permit condition. DWR has no record of receiving the 24-hour notification and the 5-day written report concerning the discharge of waste from your hog house. On February 24, 2021, DWR staff conducted a survey of your lagoon because the level was reported to be less than 12 inches. During this inspection, DWR staff documented with pictures and water samples that waste did enter the ditch system around your lagoon. In addition, it documented the conveyance to the ditch was aided by trenches being cut to allow waste and water to flow to the ditch. North Carolina Depot tincnt of Environtnental ('Zualit } Division of Water Resources Fayetteville Regional Office > 25 Green Street, Suite 714 Fayetteville. North Carolina 28301 910.433.3300 Page 4 Tammy Peterson April 30, 2021 Required Corrective action for Violation 3: In the future, notify DWR staff at first knowledge of the occurrence of any issues such as discharge from the storage facilities or waste collection systems. The Division of Water Resources requests that, in addition to the specified corrective action above, please submit the following items on or before (June 4, 2021): 1. An explanation from the OIC for this farm regarding how these violations occurred. 2. A list from the OIC concerning the steps that will be taken to prevent these violations from occurring in the future. You are required to take any necessary action to correct the above violations on or before January 15, 2021 and to provide a written response to this Notice by June 4, 2021. Please include in your response all corrective actions already taken and a schedule for completion of any corrective actions not addressed. North Carolina C)epart n nt of Environmental Quality ' Division of Water Resources Fayetteville Regional Otfice ` 225 Green Strut. Suite 71.1 i Fayetteville. North Carolina 28301 d 10. 133.3300 Page 5 Tammy Peterson April 30, 2021 Failure to comply with conditions in a permit may result in a recommendation of enforcement action, to the Director of the Division of Water Quality who may issue a civil penalty assessment of not more that twenty-five thousand ($25,000) dollars against any "person" who violates or fails to act in accordance with the terms, conditions, or requirements of a permit under authority of G.S. 143-215.6A. If you have any questions concerning this Notice, please contact Katie Fontenot (919) 896-9715 or me at (910) 433-3336. Sincerely, DocuSigned by: "- 5189C2D3DD5C42B... J. Trent Allen Regional Supervisor Water Quality Regional Operations Section Division of Water Resources cc: FRO Compliance Animal Files-Laserfiche Smithfield Pork North Carolina De.part of Environmental Quakty Divisi n of Water Resources Fayetteville Regional Otficc ?2 S Green Street, Suite 71.1 Fayetteville, North Carolina 23301 010.43 3.:33G(') INSPECTION REPORT / NOTES Facility Number }`Division of Water Resources 0 Division of Soil and Water Conservation 0 Other Agency Type of Visit: Reason for Visit: mpliance Inspection 0 Operation Review aStructure Evaluation 0 Technical Assistance outine 0 Complaint aro-How-up 0 Referral 0 Emergency 0 Other 0 Denied Access Date of Visit: _;j•-_'., ( Arrival Time: Farm Name: / co,: r�� j l / Owner Name: / - , �' Mailing Address: Physical Address: Departure Time: Owner Email: Phone: County:. f`. ",— Region: Facility Contact: Onsite Representative: Certified Operator: Back-up Operator: Location of Farm: Title: Latitude: Integrator: Phone: Certification Number: Certification Number: Longitude: Swine Design Current Capacity Pop. Wean to Finish Wean to Feeder Feeder to Finish Farrow to Wean Farrow to Feeder Farrow to Finish Gilts Boars Other Other Wet Poultry Design Current Capacity Pop. Layer Non -Layer Dry' Poultry Design Current Capacity Pop, Layers Non -Layers Pullets Turkeys Turkey Poults Other Cattle Design Current Capacity Pop. Dairy Cow Dairy Calf Dairy Heifer Dry Cow Non -Dairy Beef Stocker Beef Feeder Beef Brood Cow Discharges and Stream Impacts 1. Is any discharge observed from any part of the operation? Discharge originated at: ❑ Structure ❑ Application Field ❑ Other: a. Was the conveyance man-made? b. Did the discharge reach waters of the State? (If yes, notify DWR) c. What is the estimated volume that reached waters of the State (gallons)'? d. Does the discharge bypass the waste management system? (If yes, notify DWR) ❑ Yes ❑ No ❑ NA ❑ NE 2. Is there evidence of a past discharge from any part of the operation? Yes ❑ No, ❑ NA ❑ NE 3. Were there any observable adverse impacts or potential adverse impacts to the waters 0 YesNo ❑ NA 0 NE of the State other than from a discharge? ❑ Yes laICIo 0 NA ❑ NE ❑ Yes ❑ No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA ❑ NE Page 1 of 3 2/4/2015 Continued Waste Collection & Treatment 4. Is storage capacity (structural plus storm storage plus heavy rainfall) less than adequate? a. If yes, is waste level into the structural freeboard? Identifier: Spillway?: Designed Freeboard (in): Observed Freeboard (in): Structure 1 Structure 2 Structure 3 Structure 4 5. Are there any immediate threats to the integrity of any of the structures observed? (i.e., large trees, severe erosion, seepage, etc.) 6. Are there structures on -site which are not properly addressed and/or managed through a waste management or closure plan? If any of questions 4-6 were answered yes, and the situation poses an immediate public health or environmental threat, notify DWR ❑'Yes ❑ Yes Structure 5 No ❑NA ❑NE ❑No ❑NA ❑NE Structure 6 7. Do any of the structures need maintenance or improvement? 8. Do any of the structures lack adequate markers as required by the permit? (not applicable to roofed pits, dry stacks, and/or wet stacks) 9. Does any part of the waste management system other than the waste structures require maintenance or improvement? Waste Application 10. Are there any required buffers, setbacks, or compliance alternatives that need maintenance or improvement? 11. Is there evidence of incorrect land application? If yes, check the appropriate box below. ❑ Yes ❑ No ❑ NA ❑ NE ❑ Yes ❑moo ❑ NA ❑ NE ❑'Yes ❑ No ❑ NA ❑ NE ❑- 'es ❑ No ❑ NA ❑ NE Yes ❑ No ❑ NA ❑ NE n Yes No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA0`NE ❑ Excessive Ponding ❑ Hydraulic Overload ❑ Frozen Ground ❑ Heavy Metals (Cu, Zn, etc.) ❑ PAN ❑ PAN > 10% or 10 lbs. ❑ Total Phosphorus ❑ Failure to Incorporate Manure/Sludge into Bare Soil ❑ Outside of Acceptable Crop Window ❑ Evidence of Wind Drift ❑ Application Outside of Approved Area 12. Crop Type(s): 13. Soil Type(s): 14. Do the receiving crops differ from those designated in the CAWMP? 15. Does the receiving crop and/or land application site need improvement? 16. Did the facility fail to secure and/or operate per the irrigation design or wettable acres determination? 17. Does the facility lack adequate acreage for land application? 18. Is there a lack of properly operating waste application equipment? Required Records & Documents 19. Did the facility fail to have the Certificate of Coverage & Permit readily available? 20. Docs the facility fail to have all components of the CAWMP readily available? If yes, check the appropriate box. ❑ WUP ['Checklists ❑ Design ❑ Maps ❑ Lease Agreements 21. Does record keeping need improvement? If yes, check the appropriate box below. ❑ Waste Application ❑ Weekly Freeboard ❑ Waste Analysis ❑ Soil Analysis ❑ Rainfall ❑ Stocking ❑ Crop Yield ❑ 120 Minute Inspections ❑ Monthly and 1" Ra 22. Did the facility fail to install and maintain a rain gauge? 23. If selected, did the facility fail to install and maintain rainbreakers on irrigation equipment? Page 2 of 3 infall Inspections ❑ Yes ❑ Yes ❑ Yes ❑ No ❑ NA ❑ NE ❑Yes ❑No ❑NA ❑NE fl Yes ❑ No ❑ NA 0 NE ❑ Yes ❑ No ❑ NA 0 NE ❑ Yes ❑ No ❑ NA [] NE ❑ Yes ❑ No ❑ NA ❑ NE ❑ Yes ❑ No ❑ NA ❑ NE ❑ Other: ❑ Yes ❑ No ❑ NA 0 NE n Waste Transfers ❑ Weather Code ❑ Sludge Survey ❑ No ❑ NA ❑ NE ❑ No ❑NA ❑NE 2/4/2015 Continued Facility Number: 24. Did the facility fail to calibrate waste application equipment as required by the permit? 25. Is the facility out of compliance with permit conditions related to sludge? If yes, check the appropriate box(es) below. ❑ Failure to complete annual sludge survey ❑ Failure to develop a POA for sludge levels ❑ Non -compliant sludge levels in any lagoon List structure(s) and date of first survey indicating non-compliance: ❑ Yes ❑'No 0 NA ❑-KE ❑ Yes ❑ No 0 NA ❑ NE 26. Did the facility fail provide documentation of an actively certified operator in charge? 0 Yes ❑ No ❑ NA FINE 27. Did the facility fail to secure a phosphorus loss assessments (PLAT) certification? ❑ Yes ❑ No 0 NA ❑"NE Other Issues 28. Did the facility fail to properly dispose of dead animals with 24 hours and/or document 0 Yes El 'No 0 NA ❑ NE and report mortality rates that were higher than normal? 29. At the time of the inspection did the facility pose an odor or air quality concern? ❑ Yes ❑rNo ❑ NA 0 NE If yes, contact a regional Air Quality representative immediately. 30. Did the facility fail to notify the Regional Office of emergency situations as required by the ❑ Yes ❑ No ❑ NA ❑ NE permit? (i.e., discharge, freeboard problems, over -application) 31. Do subsurface tile drains exist at the facility? If yes, check the appropriate box below. ❑ Yes 0 No ❑ NA ❑ NE ❑ Application Field ❑ Lagoon/Storage Pond n Other: 32. Were any additional problems noted which cause non-compliance of the permit or CAWMP? 33. Did the Reviewer/Inspector fail to discuss review/inspection with an on -site representative? 34. Does the facility require a follow-up visit by the same agency? ❑ Yes ❑allo ❑ NA ❑ NE n Yes No 0 NA ❑ NE ❑ir'Yes ❑No ❑NA ❑NE Comments (refer to question #): Explain any YES answers and/or any additional recommendations or any other comments. Use drawings of facility to better explain situations (use additional pages as necessary). r3" F '( I ., 7 .` I ✓ ` _ , i )'l I, j Reviewer/Inspector Name: V • J t l,(!�'`l_ 4/ L.' i' i, • /, 1.1 I ! 2 Phone: Reviewer/Inspector Signature: Page 3 of•3 , Date: 2/4/2015 VIOLATORS RESPONSE AND NOTES 39/ 08/ 2017 11: 26PM 9105646709 HUBBS FARM PAGE 01/01 May 26, 2021 Tammy Peterson Facility 4 82-634 Additional Statements regarding violations on rebruary 19, 2021 and subsequent NOV/NOI letter dated April 30, 2021. stand by my original statements in the February 26, 2021 letter about the incident on February 19th, The only additional clarification I would like to highlight is that it was never my intent to allow waste to enter the ditch beside the houses. It was only my intent to get the excessive rain water to drain away from the backside of the lagoon berm to avoid water possibly entering the lagoon and to help prevent any possible berm failure. I have never seen our lagoon that high, I had pumped the lagoon down during the summer to a level where the measuring stick was dry. Then to have the amount of rain we had during the fal., and with pumping every opportunity and still losing ground all fall and winter to get to the 7' freeboard was a stress I have never felt in my 15+ years working with the }jogs. Walking behind the houses that day to see the lagoon level was startling. My main train of thought was solely getting as much water off the backside of the berm as possible, Responses to Corrective Action Violation 1- Lagoon level Compliance_ We have contracted and applied to have a center pivot constructed on the farm (S68,000). This will allow us to pump every opportunity and we will have our reels and pump as a backup. Violation 2_. In the previous 25 years of Tammy Warren farm we had not had a discharge escape our farm. if we were to have another discharge from a house we will contain it and return it to the lagoon. I have also thoroughly trained our new employee about reporting anything of the sort to me immediately. Violation 3_. I will report any discharge by phone as soon as possible but not more than 24 hours of first knowledge. I will also present a written report within 5 days of the incident. My mistake was thinking that the survey staff reporting it was sufficient. I realize now, I should have been the one reporting the issue once I realized there was an issue. Summary Once again, it was never my intention to allow waste to enter the ditch. It was in panic that I dug the trenches to drain clear ram water away from backside of the lagoon. It was not until the water had drained that I saw the waste. Once I saw the waste, I looked in the ditch and it appeared clear so I thought it had not entered the ditch. I can't argue the violations, but the letter does read in a way that someone reading it for the first tirne would think it was my intent to put waste in the ditch to hide a spill, I had five days before the surveyors came. I cculd have made many efforts to hide the spill during that time, but did Peterson SAMPLE RESULTS/DATA AC82018 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: T WARREN - SOURCE County: SAMPSON Collector: J BARBER VisitID 3 Region: FRO Report To FRO Location ID: 6P082AWS82 0634 River Basin CPF Collect Date: 02/24/2021 Priority COMPLIANCE Emergency YES Collect Time: 15:20 Sample Matrix: WASTEWATER COC Yes/No Sample Depth 0_1 Loc. Type: OTHER Final Report Sample ID: AC82018 PO Number # Date Received: 02/25/2021 Time Received: 08:25 Labworks LoginlD TASCENZOI Delivery Method NC Courier Final Report Date: 3/10/21 Report Print Date: 03/10/2021 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ CAS # Analyte Name PQL Qualifier LAB Sample temperature at receipt by lab 1.1 Units °C Method Analysis Reference Date Validated by 2/25/21 MSWIFT 7664-41-7 NH3 as N in liquid !C. NUT 0.02 32 mg/L as N EPA 350.1 REV 2 3/2/21 AWILLIAMS E701177 NO2+NO3 as.N in liquid (Ito? 0.2 0.2 U, P mg/L as N EPA 353.2 REV 2 3/2/21 AWILLIAMS 7723-14-0 Phosphorus_total as P in liquid r Z.3 J 0.02 13 mg/L as P EPA 365.1 REV 2 3/3/21 AWILLIAMS TKN_N Total Kjeldahl N as N in liquid i20Lif) 0.3 71 mg/L as N EPA 351.2 REV 2 3/4/21 AWILLIAMS WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 AC82017 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: T WARREN - DRAINAGE WAY County: SAMPSON Collector: J BARBER VisitID 2 Region: FRO Report To FRO Location ID: 6P082AWS82 0634 River Basin CPF Collect Date: 02/24/2021 Priority COMPLIANCE Emergency YES Collect Time: 15:10 Sample Matrix: WASTEWATER COC Yes/No Sample Depth 0_1 Loc. Type: OTHER Final Report Sample ID: AC82017 PO Number # Date Received: 02/25/2021 Time Received: 08:25 Labworks LoginlD TASCENZOI Delivery Method NC Courier Final Report Date: 3/10/21 Report Print Date: 03/10/2021 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ CAS # Analyte Name PQL Qualifier LAB Sample temperature at receipt by lab 1.1 Units °C Method Analysis Reference Date Validated by 2/25/21 MSWIFT 7664-41-7 NH3 as N in liquid l_ ;(p q NUT 0.02 22 mg/L as N EPA 350.1 REV 2 3/2/21 AWILLIAMS E701177 NO2+NO3 as N in liquid 0.2 0.2 U, P mg/L as N EPA 353.2 REV 2 3/2/21 AWILLIAMS 7723-14-0 Phosphorus_total as P in liquid 0.02 6.0 mg/L as P EPA 365.1 REV 2 3/3/21 AWILLIAMS TKN_N Total Kjeldahl N as N in liquid 0.3 34 mg/L as N EPA 351.2 REV 2 3/4/21 AWILLIAMS WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 AC82019 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: T WARREN - SOURCE County: SAMPSON Collector: J BARBER VisitlD 4 Region: FRO Report To FRO Location ID: 6P082AWS82 0634 River Basin CPF Collect Date: 02/24/2021 Priority COMPLIANCE Emergency YES Collect Time: 15:25 Sample Matrix: WASTEWATER COC Yes/No Sample Depth 0_1 Loc. Type: OTHER Final Report Sample ID: AC82019 PO Number # Date Received: 02/25/2021 Time Received: 08:25 Labworks LoginlD TASCENZOI Delivery Method NC Courier Final Report Date: 3/10/21 Report Print Date: 03/10/2021 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ CAS # Analyte Name PQL Qualifier LAB Sample temperature at receipt by lab 1.1 Units °C Method Analysis Reference Date Validated by 2/25/21 MSWIFT 7664-41-7 NH3 as N in liquid NUT 0.02 100 mg/L as N EPA 350.1 REV 2 3/2/21 AWILLIAMS E701177 NO2+NO3 as N in liquid 0.2 0.2 U, P mg/L as N EPA 353.2 REV 2 3/2/21 AWILLIAMS 7723-14-0 Phosphorus_total as P in liquid 0.02 43 mg/L as P EPA 365.1 REV 2 3/3/21 AWILLIAMS TKN_N Total Kjeldahl N as N in liquid 0.3 140 mg/L as N EPA 351.2 REV 2 3/4/21 AWILLIAMS WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 AC82016 North Carolina Division of Water Resources Water Sciences Section Laboratory Results Loc. Descr.: T WARREN - LAGOON #1 County: SAMPSON Collector: J BARBER VisitlD 1 Region: FRO Report To FRO Location ID: 6P082AWS82 0634 River Basin CPF Collect Date: 02/24/2021 Priority COMPLIANCE Emergency YES Collect Time: 15:00 Sample Matrix: WASTEWATER COC Yes/No Sample Depth 0_1 Loc. Type: OTHER Final Report Sample ID: AC82016 PO Number # Date Received: 02/25/2021 Time Received: 08:25 Labworks LoginlD TASCENZOI Delivery Method NC Courier Final Report Date: 3/10/21 Report Print Date: 03/10/2021 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. Result/ CAS # Analyte Name PQL Qualifier LAB Sample temperature at receipt by lab 1.1 Units °C Method Analysis Reference Date Validated by 2/25/21 MSWIFT NUT 7664-41-7 NH3 as N in liquid 0.02 390 mg/L as N EPA 350.1 REV 2 3/2/21 AWILLIAMS E701177 NO2+NO3 as N in liquid 0.2 0.2 U, P mg/L as N EPA 353.2 REV 2 3/2/21 AWILLIAMS 7723-14-0 Phosphorus_total as P in liquid 0.02 54 mg/L as P EPA 365.1 REV 2 3/3/21 AWILLIAMS TKN_N Total Kjeldahl N as N in liquid 0.3 440 mg/L as N EPA 351.2 REV 2 3/4/21 AWILLIAMS WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 AC82020 Loc. Descr.: County: Region: River Basin Emergency COC Yes/No North Carolina Division of Water Resources Water Sciences Section Laboratory Results T WARREN - BLUE LINE DITCH SAMPSON Collector: J BARBER VisitlD 5 FRO Report To FRO Location ID: 6P082AWS82 0634 CPF Collect Date: 02/24/2021 Priority COMPLIANCE YES Collect Time: 15:30 Sample Matrix: WASTEWATER Sample Depth 0.1 Loc. Type: OTHER Final Report Sample ID: AC82020 PO Number # Date Received: 02/25/2021 Time Received: 08:25 Labworks LoginlD TASCENZOI Delivery Method NC Courier Final Report Date: 3/10/21 Report Print Date: 03/10/2021 If this report is labeled preliminary report, the results have not been validated. Do not use for Regulatory purposes. CAS # Analyte Name Sample temperature at receipt by lab PQL Result/ Qualifier LAB 1.1 Units °C Method Analysis Reference Date 2/25/21 Validated by MSWIFT 7664-41-7 NH3 as N in liquid NUT 0.02 1.8 mg/L as N EPA 350.1 REV 2 3/2/21 AWILLIAMS E701177 NO2+NO3 as N in liquid 0.02 2.0 mg/L as N EPA 353.2 REV 2 3/2/21 AWILLIAMS 7723-14-0 Phosphorus_total as P in liquid 0.02 2.0 mg/L as P EPA 365.1 REV 2 3/3/21 AWILLIAMS TKN_N Total Kjeldahl N as N in liquid 0.3 4.2 mg/L as N EPA 351.2 REV 2 3/4/21 AWILLIAMS WSS Chemistry Laboratory» 1623 Mail Service Center, Raleigh, NC 27699-1623 (919) 733-3908 "Not Detected" or "U" does not indicate the sample is analyte free but that the analyte is not detected at or above the PQL. Page 1 of 1 DWR LAGOON SURVEY RESULTS TA 0-7 o9y Luict-1 PE) -Di,..) cRiZen (4t/ARREihi friA,C. 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