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WQ0000889_Monitoring - 11-2022_20221228 (2)
Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * November Report Information Type * GW-59 GW-59 WQ0000889 PCS Phosphate Company Inc. Year:* 2022 Upload Document* Triannial Groundwater Monitoring Results- Nov 2022.pdf PDF Only Triannial Groundwater Monitoring Results- Nov 2022.pdf PDF Only 3.95MB 3.95MB Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Confirmation Email Address:* brittany.curtis@nutrien.com Name of Submitter: * Brittany Curtis Signature: Date of submittal: Initial Review Reviewer: Gerald, Wanda Is the project number correct?* WQ0000889 Is the monitoring report accepted?* Yes No Regional Office* Washington Reviewer: _anonymous Review Date: 1/18/2023 12/28/2022 This will be filled in automatically CERTIFIED MAIL, December 28, 2022 NC DEQ Division of Water Quality Groundwater Section — Perrnits andCompliance Unit 1636 Mail Service Center Raleigh, N. C. 27699-1636 Re: Triennial Groundwater Monitoring Results, Domestic Wastewater Treatment Plant — Permit No. WQ0000889 PCS Phosphate Company Inc." Beaufort County As required by Monitoring and Reporting Requirements specified in Section IV, 10, of the above referenced pen -nit, please find attached two (2) copies of cornpleted GW-59 forms for the WWMW-1, WWMW-2, WWMW-3, WWMW-4 monitoring wells, laboratory analysis results, and a completed GW-59A forrn. Please do not hesitate to contact me at 252-322-4111 it' I can answer any questions or provide any additional infon-nation. Sincerely, Brittany Curtis Technical Services Specialist Nutrien -- Aurora Attachments pc: 12-04-02 (w/attach) ec: 1-1.13. Mills 1530 NC Hwy 306 South, Awwa, NC USA 278O6 Effective lanuiry 1, 2018, PCS Phosph2le Cognparly, Inc' is all: indirect subs4ary of Notnewl Ltd PCS PhosphAp Company, Inc, remains the legal! ope,raflng e0ity and permiltee Z.7'W-59A COMPLIANCE REPORT FORM Permit # WQOOOOi889 (Submit one each monitoring period with GW-59,forms.) I Enter date monitoring results were due. L12ajtZQ2Z) Will this monitoring report (GW-59 and GW-591A) be YES NO submitted after the established due date? X 2 Was any required !information missing on the GW-59 report forms? YES NO X IFthe answer to question I or2i,9 "YES', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casingi, unlocked or missiongi cap, YES NO missing identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for X Guidance. 14 Are any moniitored constituents equal to or above the established standards? YES INO X ff the answer to question 4 is "NO"', skip to section, 8. If the answer to question 4is "YES', list the affected wells individually with constituent(s) and concentrations(s) exceedino standards in the space provided below" 11 V202-2 VIVVMVV-1 TDS 410 Nolen VNYLINIV NoB m the estabfid background moo tanng wo VV%5""fAVV-2 TDS 420 VVM10VV-3 TDS 660 VVWIAW-4 TDS 630 ,5 For the constituents identified in, question 4 above, have standards been exceeded previous for the same YES NO constituent(s) in the same well(s) X ff the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standardsconcentration(s) reported, and sample collection date for each occurrence (for the last two years,!. 1116)12022 7'/6/20122 11,2022 11,412021 7/20,12021 3/23,12021 11i20i2020 VVVVMVV'-1 TDS 410 370 400 410 390 451 451 VVWMW,2 TDS 42f1 3'20 340 410 390 440 630 WWMW-3 TDS 660 640 640 6180 750 670 672 WWMW-4 TDS 630 640 6C-+0 680 660 660 673 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO X If the answer is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Reuional Office. * Only WWMW No. 1 is located beyond the review boundary. 7 Is the permitted implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? X If the, answer to question 7is "YES", describe those actions in the space provided below. If the answer to question 7 is "NO", jqpgfgct the Regional Office within 90 days an evaluation --i-ma v be required to determine, the Impact the waste disposal system is he viijoA lianput e __Cpmp c _e,k_ jjLrrqLt,a&ag this facifit . Ea the po—rM-At!te—rQ..@..-1V0dc0 of Violatio Denalties, 8 The person completing this portion (GIV-59A) of the monitoring report should sign below and submit this form with 'W-59 forms for required wells to be address provided at the top of the current GW-59 form, 1hereby acknowledge:that the above irlfcJfri.iiiti6riw"evi.o,luate,doindthe information-subm, edit "is.repotl'.. W49A).4true and 1.,' -bi P 't6-tha bts g .10to �pf my ... .... . .... ...................... . .. . ........ ----------- Signature of Permittee (or Authorized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY a DEPARTMENT OF ENVIRONMENTAL O LIALTIY - INV. OF WATERRESOURCES GROUNDWATER QUALITY MONITORING: INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM . a 1617 MAIL SERVICECENTER, RALEIGH, NC 27699-1617 Phone: 910-807-6306 FACILITY INFORMATION Please Print CteanyorType PERMIT Number: WOOGOO889 Expiration Date: 04/30/2028 Facility Name: PCs Phosphate Co. I Nutrien, Inc Non Discharge UIG NPDES Other Permit Name (if different): Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediatiom Infiltration Gallery Aurora NC 28705 County Beaufort Spray Field ❑ Remediat om Contact Person: Brittany Curtis Telephone#: (252)-322-4111 x:8549 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: WWTP No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-1 Date sample collected: 11108/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 0040o: 7.31 units Temp. 00010, 20O °C DRY at Depth to Water Level 82546: 9.36 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 604 gMhos time g li sampling, MeasuringPoint is 2.50 ft. above land surface Relative M.P. Elevation: 20.78 ft. Odor 000t15. Mons check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑ YES ❑ NO 6dN/A Field acidified: ❑ YES ❑ NO ❑ N/A LABORATORY INFORMATION Date sample analyzed: 11/06i2022to 1P'01/2022 Laboratory Name: PCS Phosphate Co. / Environment i,lnc Certification No. # 330 i # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 NIA rrlg/L Nitrite (NO2) as N 00615 NIA mg/L Pb -Lead 01051 NIA ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO.) as N 00620 <0.04 mg/L Zn - Zinc 01092 N A mg/L Coliform: MF Total 31504 N/A /100mL Phosphorus: Total as P 00665 0.017 mg/L (Note: use MPN method for highly turbid samples) Orthophosphate 705o N/A mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Totai 703oo 410 mg/L At - Aluminum oil o5 NIA mg/L Fluoride- 0-76 mglL pH (Lab) 00403 7.71 units Ba - Barium 01007 WA ug/L - TOC 0068o 3,32 mg/L Ca - Calcium o0916 N/A mg/L Chloride o094o 10 mg/L Cd - Cadmium 01027 NIA ug/L Arsenic 01002 NIA ug/L Chromium: Total 01034 NIA ug/L Grease and Oils 00552 NIA mg/L Cu - Cropper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 NIA ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate oo945 N/A mg/L Hg - Mercury 71900 NIA ug/L Lab Report Attached? Q Yes (1) ❑ No (0) Specific Conductance oro95 N/A pMhos K - Potassium 00937 N/A mg/L VOC 7873 method # 6200c-11 Total' Ammonia oo6lo 0.20 mg/L Mg - Magnesium 00927 N/A mg/L method # (Ammonia Nitrogen; NH,as N: Ammonia Nitrogen., Total) Mn - Manganese oio55 N/A ug/L method # TKN as N 00625 NIA mg/L Ni - Nickel 01067 N/A ug/L method ## For Remed ation Systems Only (Attach Lab Reports). Influent Total VOCs N/A mg/L Effluent Total VOCs: NIA mg/L VOC Removal% NIA William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title - Please print or type G-59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY DEPARTMENT OF ENVIRONMENTAL QUALITY - DIV, OF WATER RESOURCES GROUNDWATER QUALITY MONITORING: . . , INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM iat7 t4AlL SERVtCE CENTER RALEIDH, Nc 27699-i311r 'Phone- 91 tti 4G FACILITY INFORMATION Tease Print clearly or Type PERMIT Number: WOO000889 Expiration Date: 0413012028 Facility Name: PCS Phosphate Co. I Nutrien,lnc Non -Discharge X UlC NPDES Other Permit Name (if different): Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED Aurora NC 28706 County Beaufort © Lagoon Remediation: infiltration Gallery E Spray Field El Remediation: Contact Person: Brittany Curtis Telephone#: (252)-322-4111 ext, 8549 0 Rotary Distributor ❑ LandApplication of Sludge Well Location/Site Name: WWTP No. of wells to be sampled: 4 ❑ Water Source. Heat Pump ❑ Other: (from €'emal)_.... SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-2 Date sample collected:. 11/08/2022 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 0040o: 7.56 units Temp. 00010: 20-3 °c DRY at Depth to Water Level 82546: 10-62 ft. below measuring point Screened Interval: 16.0 fL to 21.0 ft. Spec. Cond. 00094: 669 µMhos time ofsampling, Measuring Point is 2.50 ft. above land surface Relative M.P. Elevation: 20.84 ft. Odor 00085. None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑ YES ❑ NO ON/A Field acidified: El YES 71 NO N/A LABORATORY INFORMATION' Date sample analyzed: 11/0812022 to 12/01/2022 LaboratoryName; PCS Phosphate Co. / Environment 1,Inc Certification No. # 330 / # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N 00615 NIA mg/L Pb - Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /1 OOmL Nitrate (NO3) as N 00620 0.75 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 315o4 NIA /100mL Phosphorus: Total as P 00665 0.017 mg/L (Note: use MPN method for highly turbid samples) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units:): issolved Solids:Total 70300 420 mg/L Al - Aluminum o1105 N/A mg/L Fluoride- 0.88 mg/L pH (Lab) 00403 7,87 units Ba - Barium 01007 N/A ug/L TOC 00680 2.63 mg/L Ca - Calcium 00316 NIA mg/L Chloride 00940 46 m /L Cd - Cadmium 01027 NIA ug/L Arsenic 01002 N/A ug/L Chromtiumk Total 01034 N/A ug/L Grease and Oils 00552 NIA mg/L Cu - Copper 01042 NIA mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273o N/A ug/L Fe - iron 01o45 N/A ug/L (Specify test and method #, ATTACH LAB REPORT.) Sulfate 00945 NIA mg/L Hg - Mercury 71900 N/A ug/L Lab Report Attached? Q Yes (1) ❑ No (0) Specific Conductance 00095 N/A µMhos K - Potassium 00937 N/A mg1L VOC 7873 method # 620OC-11 Total Ammonia owo 0.05 mg/L Mg - Magnesium 00927 N/A mg/L method' # (Ammonia Nitrogen,. NH,as N: Ammonia Niirogen, Total) Mn - Manganese 41o55 NIA ug/L method ## TKN as N 00625 N/A mg/L Ni- Nickel 01067 N/A ug1L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A and-t an ne`aG-ratoy=artalytR_ da alwasi U-11 _ a te and imp sonm r now- g William M. Ponton, General Massager Permittee for Authorized Agent) Name and Title - Please print or type mg/L VOC Removal% NIA (Date) GW-59 Rev.05-02.2017 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITYMONITORING: 119 DEPARTMENT OF ENVIRONMENTAL QUAILtTY - DIVY OF WATER ItE$t3URCFS INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 1647 MAIL SERVICE CENTER, RALEIG , NC 27689-1617 'Phone: 9S9 iT-1306 FACILITY INFORMATION Please Print Clearly erType PERMIT Number: W00000889 Expiration Date: Facility Name: PCS Phosphate Co./Nutrien, Inc Non -Discharge X UIC NPDES Other Permit Name (if different): Facility Address: 1530 Hwy 306 South Aurora. NC 27806 TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon E] Remediation: Infiltration Gallery 1530 Hwy 306 South Aurora. NC 27806 County Beaufort © Spray Field ❑ Remediation: Contact Person: BrittanyCurtis Telephone#: (252)-322-4111 x:8540 ❑ Rotary Distributor ElLand Application of Sludge Well Location/Site Name: WWTP No, of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: thorn Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): WWMW-3 Date sample collected: 1 V08/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH 00400: 7.28 units Temp. ooaso: 2€I.0 eC DRY at Depth to Water Level 82546:10.50 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 % Spec. Cond. 00094: 1093 ttMhos time of Measuring Point is 2.5flmpling, g ft. above land surface Relative M.P.Ml'Elevation: 20.15 ft. Odor a003s; Norte check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑ YES ❑ NO WN/A Field acidified: ❑ YES ❑ NO R] N/A LABORATORY INFORMATION Date sample analyzed:11/08/2022 to 12/0/12022 Laboratory Name:. PCS Phosphate Co. / Environment 1, Inc Certification No. # 3301 # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 N/A mg/L Nitrite (NO2) as N € 0615 NIA mg/L Pb - Lead 01051 NIA ug/L Coliform: MF Fecal 31616 < 1.0 t100mL Nitrate (NO3) as N 00620 <0.04 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 NIA 1100mL Phosphorus: Total as P o0665 0.035 mg/L (Note.: Use MPN method for highly turbid samptes) Orthophosphate 70507 N/A mg/L Other (Specify Compounds and Concentration Units): issolved Solids:Total 70300 660 mg/L Al - Aluminum o11€i5 N/A mg/L Fluoride- 0.60 mg/L phi (Lab) oo4o3 7.52 units Ba - Barium 01007 N/A ug/L TOC 00680 2.27 mg/L Ca - Calcium 00916 NIA mg/L Chloride 0o94o 106 mg/L Gd- Cadmium 01027 N/A ug/ Arsenic 01G02 N/A ug/L Chromium: Total o1a34 N/A ug/L Grease and Oils 00552 N/A mg/L Cu - Copper 01042 NIA mg/L ORGANICS: (by GC; GC/MS, HPLC) Phenol 32730 /A ug/L Fe - iron olo45 N/A ug/L (Specify test and method . ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg - Mercury 719oo NIA uglL Lab Report Attached? ❑ Yes (1) ❑ No (0) Specific Conductance 00095 N/A piMhos K - Potassium 00937 N/A mg/L VOC 7873 method # 620OC-11 Total Ammonia 00610 0.13 mgiL Mg - Magnesium 00,327 N/A mg/L method # (firzamonta Nitrogen; NH, as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 N/A ug/L , method # TIN as N 00625 NIA mg/L Ni - Nickel 01067 NIA ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: N/A mg/L Effluent Total VOCs: N/A mg/L VOC Removal% N/A G -59 Rev.05-02-2017 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: ARTMENT of ENVIRONMENTAL QUALITY - CIV. OF WATER RESOURCES INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM .. � 1617 RAIL SERVICE CENTER, RALEIGH,FIB` 271OW1617 Phom:919407 06 FACILITY INFORMATION _ Meese Print Clearly or Type PERMIT Number: W00000889 Expiration Date: 04/30/2028 Facility Name: PCS Phosphate Go, I Nutrien, Inc Non -Discharge X UIC NPDES Other Permit Nara€: (if different): - Facility Address: 1530 Hwy 306 South TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Rernediation: infiltration Gallery Aurora NC 28706 County Beaufort Spray Field ❑ Remediatiom Contact Person: Brittany Curtis Telephone#: (252)-322-4111 ext. 8549 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: VtWTP No. of wells to be sampled: 4 ❑ Water Source Heat Pump ❑ Other: nay, SAMPLING INFORMATION if WELL WELL ID NUMBER (from Permit): WWMW-4 Date sample collected: 11/08/22 FIELD ANALYSES: WAS Well Depth: 21.5 ft. Well Diameter: 2 in. pH oo400: 7.46 units Temp. 000lo: 20.9 oC DRY at Depth to Water Level 82546: 14.45 ft. below measuring point Screened Interval: 16.0 ft. to 21.0 ft. Spec. Cond. 00094: 1127 pMhos time of MeasuringPoint is 2.50 ft. above land surface Relative M.P. Elevation: 20.81 ft. sampling, Odor o0085: None check Volume of water pumped/bailed before sampling: 2100 milliliters Appearance Clear here: Samples for metals were collected unfiltered: ❑ YES ❑ NO ® N/A Field acidified: ❑ YES ❑ NO ❑ N/A LABORATORY INFORMATION - Date sample analyzed: 11/0812022 to 12101i2022 Laboratory Name: PCS Phosphate Co. i Environment 1,Inc Certification No. # 3301 # 10 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. GOD 00335 N/A mg/L Nitrite (NO2) as N 00615 NIA mg/L Pb -Lead 01051 N/A ug/L Coliform: MF Fecal 31616 < 1.0 /100mL Nitrate (NO.) as N 00620 <0.04 mg/L Zn - Zinc 01092 N/A mg/L Coliform: MF Total 31504 N/A /1 OOmL Phosphorus: Total as P 00665 0.051 mg/L (Note: use M N method for highly turbid samples) Orthophosphate 70507 N/A mgiL Other (Specify Compounds and Concentration Units): issolved Solids:Totat 70300 630 mg/L Al - Aluminum 01105 N/A mg/L Fluoride- 2.64 mgiL pH (Lab) 00403 7.66 units Ba - Barium 01007 NIA ug/L TOC 00680 2.28 mg/L Ca - Calcium 00916 N/A mg/L - Chloride oo94o 130 mg/L Cd - Cadmium 01027 NIA ug/L Arsenic 01002 N/A ug/L Chromium: Total 01034 N/A ug/L - Grease and Oils 00552 NIA mg/L Cu - Copper 01042 N/A mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 3273o N/A ug/L Fe - Iron 01045 N/A ug/L (Specify test and method #, ATTACH LAB REPORT.) Sulfate 00945 N/A mg/L Hg - Mercury 719oo N/A ug/L Lab Report Attached? FEI' Yes (1) E No (0) Specific Conductance 00095 NIA pMhos K - Potassium 00937 N/A mg/L VOC 7873 method # 6200G-1I Total Ammonia oo610 0.33 mgiL Mg - Magnesium 00927 NIA rng/L method # (Ammonia Nitrogen: NH3 as N: Ammonia Nitrogen, Total) Mn - Manganese o1055 N/A ug/L method # TKN as IN 00625 NIA mgiL Ni - Nickel 01067 N/A ug/L method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: NIA mg/L Effluent Total VOCs: N/A mg/L VOC Removal% NIA William M. Ponton, General Manager Permittee (or Authorized Agent) Name and Title- Please print or type G-59 Rev.05-02-2017 Tt" Cr�('Lo'- (L)] 114 OAKMONT DWE C32REENVILLE, N C,, 27853 CLIENT: NUTRIEN (WELLS 1-4) MR. BRYAN MILLS 1530 NC HWY. 306 SOUTH AURORA, NC 2'7806 REVIEWED BY: VOLATILE ORGANICS STD. METHODS 620OC-11 wftacawavlmrr xvm Liv PHC)NE (252)756-6208 FAX (252),756-01633 ANALYST: JAP DATE COLLECTED: 11/08/22 Page: 1 DATE REPORTED: 12/01/22 Date Analyze& 11/110/22 11/10/22 I1/21/22 11/16/21 Domestic Domestic Domestic Domestic PARAMETERS, tigil Mwell #1 Mwell #2 Mwell #3 Mwell #4 1. Benzene <0.50 <0.50 <0.50 <0.50 2, Bromobenzene < 0.50 <0.50 <0.50 <0.50' 3. Brortiochloromethane <0.50 <0.50 <0.50 <0.50 4. Bromodiclilorometbane <0150 <0150 <0.50 <0.50 5. Bromofarm <0.50 <0.50 < 0.50 <0.50 6. Bromomethane <0.50' 1 <0.50 <0.50 <0.50 7. N-Butylbenzene <0.50 <0.50 <030 <0.50 I , Sec"Bulylbenzene <0.50' <0.50 <0.50 <0.50 9. Tert-Btitylbenzene <0.50 <030 <0.50 <0.50 10. Carbon Tetrachloride < 0. 50 <0150 <0'.50 <0.50 11. Chlorobenzene <0.50, <01,50 <0.50 <0.50 12. Chloroetbane <0.501 <0.50 <0.50 <0,50 13. Chloroform <0.50 <0.50 <0.50 <0.50 14. Chloromethane < 0.50 <0.50 <0.50 <0.50 15. 2-Chlorotoluene <0.50 <0'.50 <0.50 <0.50 16. 4-Chlorotoluene <0.50 <0.50 <0.50 <0.50 17. Dibromochloromethane <0.50 <0.50 <030 <0.50 18. 1,2-Dibromo-3-Chloropropaue <0.50 < 0.50 <0.50 <0.50 19. 1,2-Dibromoethane <0.50 <0.50 < 0.50 <0.50 20. Dibromomethane <0.50 < 0150 <0.50 <0.50 21. 1,2-Dichlorobenzene <0.50 <0.50 < 0,50 <0.50 22. 1,3-Dichlorobenzene <0.50 <0.50 <0.50 <0.50 23. 1,4-Diclilorobenzene <0.50 <0.50 < 0.50 <0.50 24. Dichlorodifluoromethane <0.50 <0.50 <0.50 < 0.50 25, IJ-Dictiloroethane <0.50 <0.50' <0.50 <0.50 26. 1,2-Dichloroetliane <0.50 <0.50 <0150 <0.50 27. 1,1-Diebloroethene < O'.50 <0.50 <0.,50 <0.50 28. Cis-1,2-Dicliloroethene <0.50 <0.50 <0.50 <0'.50 29, tratis-1,2-Diebloroethene <0.50 <0.50 <0.50 < O'.50 30. 1,2-Dichloropi7opane <0.50 <0.50 < 0 < O'.50 31. 1,3-Dieliloropropane < 01.50 <0.50 <0.50 <0.50: 32. 2,2-Dichloro,propane <0.50 <0.50 <0.50 <0.50 33. 1,1 -Dichloropropene <0.50, <0.50 <0.50, <0.50' 34. Cis-1,3-Dichloropropene <0.50 1 <0.50 <0.50 <0.50 35. trans-1,3-Dieliloropropene <0.50 <0.50 <0.50 <0.50 36. Ethylbenzene <0.50 <0'.50 <0.50 <0.50 37. Hexachlorobtitadiene <0.50 <01,50 <0.50 <0.50 3& Isopropylbenzene <0.50 <01.50 < 0.5'O <0,50 39. 4-1sopropyltoluene <0150 <01.50 <0.50 <0.50 40. Methylene Chloride <0.50 <01.50 <0.50 <0.50 ,41. Naphthalene <0.50 <0.50 <0.50 <0.50 42. Propylbenzene <0.50 <0.50 <0.50 <0.50 43. Styrene <0.50 <0.50 <0.50 <0.50 44. 1, 1, 1,2-Tel rachloroetha tie <0.50 <0.50 <0.50 <0.50 45. 1,1,2,2-Tetracliloroethane <0.50 <0.50 <0.50 <0.50 46. Tetrachloroethene <0.50 <0.50 <0.50 <0.50 47. Toltiene < 0.50 <030 <0.50 <0.50 R vvl'] Fill @ ff I �JNJII (@ E IR r1l, hn( 114 CAKMONT U11WE' GREP'Wfl 11, N.G27�3,58 CLIENT: NUTRIEN (WELLS 1-4:) MR. BRYAN MILLS 1530 KC HWY. 306 SOUTH AURORA, NC 27806 REVIEWED BYt VOLATILE OROAXICS STD. METHODS 6200C-11 F410NE (252) 756-62108 FAX ('252) 756-0633 16015 ANALYST: JAP DATE COLLECTED: 11/08/22 Page: 2 DATE REPORTED: 12/01/22 Date Analyzed: IIII0Y22 11/10/22 11/21/221 11/16/21 Domestic Domestic Domestic Domestic PARAMETERS, ug/1 Mwell #1 Mwell #2 Mwell #3 Mwen 48. 1,2,3-Trichlorobeitzenle <101.50 < 0,50 <0.50 <0.501 49. 1,2,4-Trichlorobenzene <0!150 <0'.50 <0.50 <0.50 501. 1,1,1-Trichloroethane <0.50 <0.50 <0.50 <0.50, 51. 1,1,2-Trichloroethane <0.50 <0.50 <01.501 <0.50 52. Trichloroethene <0.50 < 0,50 <0.50 <0.50 53. Trichlorofluoromethane <0.50 <0.50 <0.50 <0.50 54. 1,2,3-Trichloropropane <0.50 <0.50 <0.50 <030 55. 1,2,4-Trimethylbenzene <0.50 <0.50 <0.50 <0.50 56. 1,3,5-Trimethylbeuzene <0"50 <0.50 <0.50 <0'.50 57. Vinyl Chloride <0.50 <0.50 <0.50 < 0.50 58. Total Xylenes <1100 <1.00 < 1.00 < 1.00 59. Methyl Tert Butyl Ether < 1.00 ........... <1.00 <L00 - . -- J- <1A0 111MI 1,7 It w, 1T1fde_ EA )IFO( 114 OAKMONTMINE' C REENVIULFE, P4,C 27858 NUTRIEN (WELLS 1-4) MR. BRYAN MILLS 1530 NC HWY. 3 0� 6 SOUTH AURORA, NC 27806 Domestic Domestic PARAMETERS Mwell #1 Mwell #2 Fecal Coliform (Nff), /100 Nfls <1 <1 Ammonla Nitrogen as N, rng/l 0.20 0.05 Nitrate Nitrogen as N, mg/l < 0.04 0.75 Total Organic Carbon, ung/l 332 2.63 Chloride, mg1l 10 46 Total Dissolved Residue, mg/1 410 420 �HQNE�'(2'52) 756,62,08 7+" 0633; DATE COLLECTED: 11/08/22 DATE REPORTED : 12/01/22 REVIEWED BY: Domestic Domestic Analysis Method Mwell #3 Mwell #4 Date Analyst Code <1 <1 11/08/22 HMV 922211-15 0,13 0,33 11/09/22 KES 350J R2-93 < 0.04 < 0.04 11/09/22 KES 353.2 R.2-93 2.27 2,28 11/17/22 HMM 531OC-14 106 130 11/14/22 JDJ 4500CLB-11 660 630 11110/22 JDJ D5907-13