090099_NOV-2020-DV-0518 Enforcement Packet w photos_20201203

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2.65w
PS Form 3800, April 2015 PSN 7530-02-000-9047
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1. Article Addressed to:
41 S cu,L' TI-)-ST)
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lull
mill
1111111111
9590 9402 5878 0038 2330 32
2. Article Number (Transfer from service label)
7019 0700 0000 3643 4787
A. Signature
X D Agent
A Q It l Di r� 1rr U ns ❑ Addressee
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tem
If YES, enfer delivery address below: ❑ No
/tee) tV1-e- - ,..177
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PS Form 3800, April 2015 (Reverse) PSN 7530-02-000-9047
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USPS TRACKING #
111
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9590 9402 58?8 0038 2330 32
United States
Postal Service
First -Class Mail
Postage & Fees Paid
USPS
Permit No. G-10
• Sender: Please print your name, address, and ZIP+4® in this box*
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NOTICE OF VIOLATION AND/OR
NOTICE OF INTENT

ROY COOPER
Governor
MICHAEL S. REGAN
Secretary
S. DANIEL SMITH
Director
NORTH CAROLINA
Environmental Quality
December 3, 2020
CERTIFIED MAIL
RETURN RECEIPT REQUESTED 7019 0700 0000 3643 4787
Barry Billups
415 Culbreth-Smith Road
Elizabethtown NC 28337
Subject: NOTICE OF VIOLATION/NOTICE OF INTENT
Administrative Code 15A NCAC 2T .1304
NOV-2020-DV-0518
Barry Billups Facility Number 09-99
Permit AWS090099
Bladen County
Dear Barry D Billups,
On November 16, 2020, staff of the NC Department of Environmental Quality (DEQ) Division
of Water Resources (DWR), Water Quality Regional Operations Section (WQROS) inspected
the Barry Billups Farm and the permitted waste disposal system. We wish to thank Mr. Barry
Billups for his assistance during this inspection.
As a result of this inspection, you are hereby notified that, having been permitted to have a non -
discharge permit for the subject animal waste disposal system pursuant to 15A NCAC 2T .1304,
you have been found to be in violation of your permit as follows:
LD_E
a lm nt ofE JNA
Oaparhnenl o<Envlmmmenla49uality
North Carolina Department of Environmental Quality I Division of Water Resources
Fayetteville Regional Office 1225 Green Street, Suite 714 I Fayetteville, North Carolina 28301
910.433.3300

Page 2
Barry Billups
December 3, 2020
Violation 1:
Failure to prevent discharge of waste to surface waters of wetlands. N.C.G.S. 143-215.10C - (Permit No.
AWG100000 Section Conditions I 1).
On November 16, 2020 during an inspection site visit, DWR staff noticed evidence that waste was
ponded in the spray field and waste was in a drainage area next to the lagoon leading to a ditch that flows
offsite. After further investigation of the ditch, DWR staff documented with pictures and samples that
waste was in the ditch and flowed to an unnamed tributary that flows into Turn Bull Creek.
Required Corrective Action for Violation 1:
If you have not done so, recover all waste and return it to your lagoon, and document the amount of waste
recovered. In the future, monitor the permitted spay fields and application equipment during spray events
as required by your permit to prevent the discharge of waste. Explain to anyone applying waste the
importance of reporting to you anytime there is any problems with the waste collection, treatment, storage
and application system operated under this General Permit.
Violation 2:
Failure to prevent excessive ponding or any runoff during any given land application event. [15A NCAC
02T- .1304(b)] (Permit No. AWG100000 Section Conditions II 5).
On November 16, 2020 during a routine compliance inspection site visit, DWR staff noticed evidence of
ponded waste in the spray field next to the lagoon. Waste was ponded in several locations in front of the
gun carts, gun cart pulls, and various other areas in the spray field. DWR staff was able to take multiple
photos of the various areas of the ponded waste. The ponded waste was able to be seen with very little
effort. In addition, waste was observed flowing into an unnamed tributary that flows to Turn Bull Creek.
Pictures and water samples were taken of the waste in the field as well as in the ditch.
Required Corrective Action for Violation 2:
In the future, monitor the permitted spay fields and application equipment during spray events as
required by your permit to prevent the ponding and runoff of waste. If you have not done so, recover all
waste and return it to your lagoon or dry areas of your spray field, and document the amount of waste
recovered. You should report to DWR anytime there is a problem with the waste collection, treatment,
storage or application system that is under this General Permit.

Page 3
Barry Billups
December 3, 2020
Violation 3:
Failure of the Operator in Charge (OIC) or a person under the supervision of an OIC to inspect the land
application as often as necessary to ensure that the animal waste is land applied in accordance with the
CAWMP. In no case, shall the time between inspections be more than 120 minutes during the application
of waste. Inspection shall include but not be limited to visual observation of application equipment, spray
fields, subsurface drain outlets, ditches, and drainage ways for any discharge of waste. (Permit No.
AWG100000 Section II 17).
On November 16, 2020 during your routine compliance inspection, DWR staff was able to document the
violations stated above with very little effort. It is reasonable to assume that whoever operated the waste
application equipment should have seen the ponded waste if they had conducted the 120 inspection as
specified in the permit.
Required Corrective action for Violation 3:
In the future, require the OIC or a person under the supervision of an OIC to inspect the land application
site as often as necessary to ensure that the animal waste is land applied in accordance with the CAWMP.
The Division of Water Resources requests that, in addition to the specified corrective action
above, please submit the following items on or before (January 3, 2021):
1. An explanation from the OIC for this farm regarding how these violations occurred.
2. A list from the OIC concerning the steps that will be taken to prevent these violations
from occurring in the future.
You are required to take any necessary action to correct the above violations on or before
January 3, 2021 and to provide a written response to this Notice by January 3, 2021. Please
include in your response all corrective actions already taken and a schedule for completion of
any corrective actions not addressed.

Page 4
Barry Billups
December 3, 2020
As a result of the violations in this Notice, this office is considering a
recommendation for a civil penalty assessment to the Director of the Division. If you
wish to present an explanation for the violations cited, or if you believe there are other
factors, which should be considered, please send such information to me in writing
within ten (10) days following receipt of this letter. Your response will be reviewed,
and, if an enforcement action is still deemed appropriate, it will be forwarded to the
Director and included for consideration.
Failure to comply with conditions in a permit may result in a recommendation of enforcement
action, to the Director of the Division of Water Quality who may issue a civil penalty assessment
of not more that twenty-five thousand ($25,000) dollars against any "person" who violates or
fails to act in accordance with the terms, conditions, or requirements of a permit under authority
of G.S. 143-215.6A.
If you have any questions concerning this Notice, please contact Katie Fontenot [phone]
or me at [phone].
Sincerely,
EDocuSigneddby:
n n __
5189C2D3DD5C42B...
J. Trent Allen
Regional Supervisor
Water Quality Regional Operations Section
Division of Water Resources
cc: FRO Compliance Animal Files-Laserfiche
Smithfield Pork

INSPECTION REPORT / NOTES

Facility Number
Division of Water Resources
0 Division of Soil and Water Conservation
0 Other Agency
Type of Visit: ) ompliance Inspection
0 Operation Review O'Structure Evaluation 0 Technical Assistance
Reason for Visit: 0 Routine 0 Complaint 0 Follow-up 0 Referral 0 Emergency Other 0 Denied Access
Date of Visit:
Farm Name:
Owner Name:
Mailing Address:
Physical Address:
Facility Contact:
Arrival Time:
Departure Time:
• ,.
5 T
Owner Email:
Phone:
County:
Region:
iI
Onsite Representative:
Certified Operator:
Back-up Operator:
Location of Farm:
Title:
Latitude:
Integrator:
Phone:
Certification Number:
Certification Number:
Longitude:
Swine
Design Current
Capacity Pop.
Wean to Finish
Wean to Feeder
i/.Feeder to Finish
t
Farrow to Wean
Farrow to Feeder
Farrow to Finish
Gilts
Boars
Other
Other
Wet Poultry
Design Current
Capacity Pop.
Layer
Non -Layer
Dry Poultr
Design Current
Capacity Pop.''
Layers
Non -Layers
Pullets
Turkeys
Turkey Poults
Other
Cattle'
Design Current
Capacity Pop.
Dairy Cow
Dairy Calf
Dairy Heifer
Dry Cow
Non -Dairy
Beef Stocker
Beef Feeder
Beef Brood Cow
Discharges and Stream Impacts
1. Is any discharge observed from any part of the operation'?
Discharge originated at: ❑ Structure 0 pplication Field ❑ Other:
a. Was the conveyance man-made?
b. Did the discharge reach waters of the State? (If yes, notify DWR)
c. What is the estimated volume that reached waters of the State (gallons)?
d. Does the discharge bypass the waste management system? (If yes, notify DWR)
2. Is there evidence of a past discharge from any part of the operation?
3. Were there any observable adverse impacts or potential adverse impacts to the waters
of the State other than from a discharge'?
Yes 0 No ❑ NA ❑ NE
0-Yes 0 No
,Yes ❑ No
y! ' tip jrj ....
❑NA ❑NE
❑NA ❑NE
/�
,1` � ._ J � , f ed 4.
Q" Yes
❑ Yes
n Yes
❑ No ❑ NA ❑ NE
"No ❑ NA ❑ NE
0-No DNA ❑NE
Page 1 of'3
2/4/2015 Continued

Waste Collection & Treatment
4. Is storage capacity (structural plus storm storage plus heavy rainfall) less than adequate?
a. If yes, is waste level into the structural freeboard?
Identifier:
Spillway?:
Designed Freeboard (in):
Observed Freeboard (in):
Structure 1
/
i}
Structure 2 Structure 3
[Yeso ❑ NA ❑ NE
❑° es ❑ No ❑ NA ❑ NE
Structure 4 Structure 5 Structure 6
5. Are there any immediate threats to the integrity of any of the structures observed?
(i.e., large trees, severe erosion, seepage, etc.)
6. Are there structures on -site which are not properly addressed and/or managed through a
waste management or closure plan?
If any of questions 4-6 were answered yes, and the situation poses an immediate public health or environmental threat, notify DWR
7. Do any of the structures need maintenance or improvement? ❑ Yes ❑ No ❑ NA ❑ NE
8. Do any of the structures lack adequate markers as required by the permit? ri Yes ErNo ❑ NA ❑ NE
(not applicable to roofed pits, dry stacks, and/or wet stacks)
9. Does any part of the waste management system other than the waste structures require ❑ Yes ❑ No ❑ NA ❑ NE
maintenance or improvement?
Waste Application
10. Arc there any required buffers, setbacks, or compliance alternatives that need
maintenance or improvement?
11. Is there evidence of incorrect land application? If yes, check the appropriate box below.
❑ Yes O'No ❑ NA ❑ NE
❑ Yes ❑ No ❑ NA ❑ NE
❑ Yes ❑'No ❑ NA ❑ NE
Yes ❑ No ❑ NA ❑ NE
DE-xcessive Ponding n Hydraulic Overload ❑ Frozen Ground ❑ Heavy Metals (Cu, Zn, etc.)
❑ PAN ❑ PAN > 10% or 10 lbs. ❑ Total Phosphorus ❑ Failure to Incorporate Manure/Sludge into Bare Soil
❑ Outside of Acceptable Crop Window ❑ Evidence of Wind Drift
12. Crop Type(s):
13. Soil Type(s):
❑ Application Outside of Approved Area
14. Do the receiving crops differ from those designated in the CAWMP? ❑ Yes [o ❑ NA ❑ NE
15. Does the receiving crop and/or land application site need improvement? 12<es ❑ No ❑ NA ❑ NE
16. Did the facility fail to secure and/or operate per the irrigation design or wettable ❑ Yes ENo ❑ NA ❑ NE
acres determination?
17. Does the facility lack adequate acreage for land application? ❑ Yes 'No ❑ NA ❑ NE
18. Is there a lack of properly operating waste application equipment? ❑ Yes [N ❑ NA 0 NE
Required Records & Documents
19. Did the facility fail to have the Certificate of Coverage & Permit readily available? ❑ Yes ❑ No ❑ NA 0-N-E
20. Does the facility fail to have all components of the CAWMP readily available? If yes, check ❑ Yes ❑ No ❑ NA ❑ NE
the appropriate box.
❑ WUP ❑ Checklists ❑ Design ❑ Maps ❑ Lease Agreements ❑ Other:
21. Does record keeping need improvement? If yes, check the appropriate box below. ❑ Yes ❑ No ❑ NA ErS1 E
❑ Waste Application ❑ Weekly Freeboard ❑ Waste Analysis ❑ Soil Analysis ❑ Waste Transfers ❑ Weather Code
❑ Rainfall ❑ Stocking ❑ Crop Yield ❑ 120 Minute Inspections ❑ Monthly and 1" Rainfall Inspections ❑ Sludge Survey
22. Did the facility fail to install and maintain a rain gauge? ❑ Ycs ❑ No ❑ NA f E
23. If selected, did the facility fail to install and maintain rainbreakers on irrigation equipment`? ❑ Yes ❑ No ❑ NA ❑-NE
Page 2 of 3 2/4/2015 Continued

Lacility Number:
-
Date of Inspection: /l—%spa
24. Did the facility fail to calibrate waste application equipment as required by the permit?
25. Is the facility out of compliance with permit conditions related to sludge? If yes, check
the appropriate box(es) below.
O Failure to complete annual sludge survey ❑ Failure to develop a POA for sludge levels
❑ Non -compliant sludge levels in any lagoon
List structure(s) and date of first survey indicating non-compliance:
26. Did the facility fail provide documentation of an actively certified operator in charge? n Ycs ❑ No ❑ NA [E'NE
27. Did the facility fail to secure a phosphorus loss assessments (PLAT) certification? n Yes ❑ No 0 NA agE
Other Issues
28. Did the facility fail to properly dispose of dead animals with 24 hours and/or document 0 Yes 0-No ❑ NA ❑ NE
and report mortality rates that were higher than normal?
29. At the time of the inspection did the facility pose an odor or air quality concern? ❑ Yes E' No ❑ NA ❑ NE
If yes, contact a regional Air Quality representative immediately.
30. Did the facility fail to notify the Regional Office of emergency situations as required by the EF-Ners ❑ No 0 NA 0 NE
permit? (i.e., discharge, freeboard problems, over -application)
31. Do subsurface tile drains exist at the facility?If es check the appropriate box below. Yes No NA Er NE
Y❑ ❑ ❑
O Application Field 0 Lagoon/Storage Pond ❑ Other:
❑ Yes No ❑NA N—E
❑ Yes ❑ No ❑ NA [ TE
32. Were any additional problems noted which cause non-compliance of the permit or CAWMP?
33. Did the Reviewer/Inspector fail to discuss review/inspection with an on -site representative?
34. Does the facility require a follow-up visit by the same agency?
Comments (refer to question # : Explain az
Use drawings of facility to better explain
ffr'J14
_ - a ilf-L-'
/d gq,;
savers Ad/or
use additiona
.dditianal rec
es as necessary)
❑ Yes
❑ Yes
I2 es
idations..
ENo
eNo
❑ No
❑ NA
0 NA
❑ NA
any;, other comments.
Vol/ / X f' 0,,t/d i `.'- `1 Gt ,e ^ s" V it g ' 7eLek //47.4;"- ;/14: • 1), fi re ,
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Ficti} e2,A ad-0 F-
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144y'7 ,6j'
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❑ NE
❑ NE
❑ NE
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c)Gf--tiff � '7" .. ,1_ it T- / Y i '--' le % CIA
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Reviewer/Inspector Name:
Reviewer/Inspector Signature:
Page 3 of •3
. )A"t. 1��1 � f� z' 1 �- / �- 1 T3
Phone:
Date:
2/4/2015

Facility Number: — ) ?
Date of Inspection W//-J , r` )
Additional. Comments and/orDrawings:
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VIOLATORS RESPONSE AND NOTES

KtUItIVtU
DEQ/DWR
F .g 0 3 2021
February 1, 20201
WQROS
Division of Water Resources PAYETTEVIU!_FRF(IONAL OFFICE
Fayetteville Regional Office
Dear Mr. Allen and Ms. Fontenot,
This letter is in regards to the notice of violation for facility 9-99. I received a hand delivered
copy from Steve Guyton in January. This discharge resulted from getting 11 inches of rain in
November after the tropical storm. This is the first time since I have had the farms that I have
had a discharge or violation. I try to do things correctly because me and my family lives near
that farm and 1 want to do the right thing when pumping. I spent over $23,000 in pump and
haul charges to get the lagoon back into compliance. We did pump and haul a second time
because of the rain and the wet field conditions.
Violation 1— All waste water has been pumped back into the lagoon within 2 days of finding the
water. In the future, I will monitor spray events to prevent discharges/ponding. I added a berm
with 12 loads of clay — 4 foot high and 8 foot wide in the corner of the lagoon. I added an 8"
pipe with a plug to collect water the berm will hold back and then I can pull the plug and let rain
water back in the ditch or pump waste water back in the lagoon. I will re -level that field to
prevent ruts which allowed the discharge/ponding to occur. The lagoon is currently at 27.5" as
of today.
Violation 2 — In the future, I will re -level the field to prevent ruts which allowed ponding. I will
run the equipment for reduced times to prevent ponding. I will set a timer on my phone and
turn the system off within 1-2 hours of pumping when the ground may be wetter than desired
as weather permits.
Violation 3 — In the future, I will inspect land application sites every 120 minutes or more often
to ensure that no ponding or run-off occurs. I will set a timer on my phone to make sure that I
am inspecting the system in a timely manner. I also can set a timer on the pump to run for 2
hours.
Thank you for revieing my comments and I am trying to improve this situation as quickly as
can. I am willing to do whatever I need to do to get back into compliance.
Sincerely,
Barry D. Billups

SAMPLE RESULTS/DATA

ENVIRONMENTAL CHEMISTS, INC
P.O. BOX 1037
WRIGHTSVILLE BEACH, NC 28480
Voice: 910-392-0223
Fax: [phone]
E-Mail: [e-mail]
Bill To:
NCDENR - DWQ - FAYETTEVILLE
225 GREEN STREET
SUITE 714
FAYETTEVILLE, NC 28301
PLEASE USE THE P.O. BOX FOR
ALL REMITTANCES. THANK YOU.
INVOICE NUMBER
176866
Invoice Date:
Nov 20, 2020
Page:
1
Customer ID
Customer PO Payment Terms
19020022
9-14, 9-99 Net 30 Days
ENVIROCHEM'S FEDERAL ID #
Ship Date Due Date
56-1894379 11 / 16/20
12/20/20
Quantity
Description Unit Price Amount
REPORT #2020-19506, 2020-19507
WATER: BARRRY BILLUPS 9-99; 9-14
DATE SAMPLED: 11/16/2020
CONTACT - TRENT ALLEN, STEVE GUYTON, KATIE FONTENOT
7.00 FECAL COLIFORM 35.00 245.00
1.00 TRAVEL/PICKUP - AMENDED TO CORRECT - 12/10/2020 - PER JCB - tlw 100.00 100.00
EMAIL INVOICE
REPORT HAS BEEN EMAILED.
PLEASE REFERENCE INVOICE NUMBER ON ALL
REMITTANCES IN ORDER TO PROPERLY APPLY TO
YOUR ACCOUNT. CALL TERESA WOLFE OR FRAN
GODLEY @ 910-392-0223 FOR QUESTIONS.
Subtotal 345.00
Payment/Credit Applied
Total Amount Due $ 345.00

ENVIRONMENTAL CHEMISTS, INC
P.O. BOX 1037
WRIGHTSVILLE BEACH, NC 28480
Voice: 910-392-0223
Fax: [phone]
E-Mail: [e-mail]
Bill To:
NCDENR - DWQ - FAYETTEVILLE
225 GREEN STREET
SUITE 714
FAYETTEVILLE, NC 28301
PLEASE USE THE P.O. BOX FOR
ALL REMITTANCES. THANK YOU.
INVOICE NUMBER
176866
Invoice Date:
Nov 20, 2020
Page:
Customer ID
Customer PO Payment Terms
19020022
9-14, 9-99 Net 30 Days
ENVIROCHEM'S FEDERAL ID #
Ship Date Due Date
56-1894379 11 / 16/20
12/20/20
Quantity
Description Unit Price Amount
REPORT #2020-19506, 2020-19507
WATER: BARRRY BILLUPS 9-99; 9-14
DATE SAMPLED: 11/16/2020
CONTACT - TRENT ALLEN, STEVE GUYTON, KATIE FONTENOT
7.00 FECAL COLIFORM 35.00 245.00
3.00 HOURS TRAVEL/TIME ONSITE 100.00 300.00
EMAIL INVOICE
REPORT HAS BEEN EMAILED.
PLEASE REFERENCE INVOICE NUMBER ON ALL
REMITTANCES IN ORDER TO PROPERLY APPLY TO
YOUR ACCOUNT. CALL TERESA WOLFE OR FRAN
GODLEY @ 910-392-0223 FOR QUESTIONS.
Subtotal 545.00
Payment/Credit Applied
Total Amount Due
$ 545.00

ANALYTICAL & CONSULTING CHEMISTS
NCDFQ/DWR-Fayetteville
225 Green Street
Fayetteville NC
Attention: Trent Allen
viro ent al
e
ists, I c
6C:02 Windmill Way, Wilmington, NC 28405 910,392.0223 Lab o 91.0.392,4 24 Fax
710 owserto,,,,in Road, Manteo, NC 27954 • 252.473.5702 Lab /Fax
255-A Wilmington Highway, Jacksonville, NC 28540 ® 910,347,5843 Lab/Fax
info 9'ienvironrnentalcllernists,com
Date of Report: Nov 18, 2020
Customer P4 #:
28301 Customer ID: 19020022
Report #: 2020-19506
Project ID: Barry Billups 9-99
Lab ID
20-49628
Test
Sample ID:
Site: Upstream
Fecal Coliform
Method
Sa ra 9222D MF
Collect Date/Time Matrix
11/16/2020 1:04 PM Water
Results
Sampled by
Guyton/Fontenot
Date Analyzed
7969 Colonies/100mL 11/16/2020
Lab ID
20-49629
Test
Sample ID:
Site: Source
Method
Collect DatelTime Matrix Sampled by
11/16/2020 1:10 PM Water Guyton/Fontenot
Results
Date Analyzed
Fecal Coliform
Lab ID
20-49630
Test
Sample ID:
Site: Cons/Source
SM 9222D MF
Method
Collect Date/Time
11/16/2020 1;04 PM
>69966 Colonies/190mL 11/16/2020
Matrix
Water
Results
Fecal Conform
SM 92220 MF
Sampled by
Guyton/Fontenot
Date Analyzed
26000Colonies/100mL 11/16/2020
Lab ID
20-49631
Test
Sample ID:
Site: Downstream
Method
Collect Date/Time Matrix
11/16/2020 12:56 PM Water
Results
Sampled by
Guyton/Fontenot
Date Analyzed
Fecal Coliform
Comment:
Reviewed by:
SM 9222D MF
23000Colonies/100r L 11/16/2020
Re ` a s• 2O2D•19
Page 1 of 1

Environmental Chemist, Inc., Wilmington, NC Lab #94
Sample Receipt Checklist
Client: .4 Date:
Receipt of sample:
O YES JD NO
❑ YES ❑ NO
FedEx 0
Other 0
1. Were custody seals present on the cooler?
2. If custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt
How temperature taken: 0 Temperature Blank t( Against Bottles
IR Gun ID: Thomas
0 YES
YES
t YES
f YES
YES
YES
15r� YES
!fit YES
E YES
Ni YES
0 YES
O YES
O YES
O YES
YES
❑ YES
Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ NO
❑ NO
O NO
❑ NO
O NO
O NO
O NO
O NO
O NO
O NO
O NO
O NO
❑ NO
❑ NO
O NO
O NO
3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
4. Were proper custody procedures (relinquished/received) followed?
5. Were sample ID's listed on the COC?
6. Were samples ID's listed on sample containers?
7. Were collection date and time listed on the COC?
8. Were tests to be performed listed on the COC?
9. Did samples arrive in proper containers for each test?
10. Did samples arrive in good condition for each test?
11. Was adequate sample volume available?'
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2? *
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet,
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace)
Sample(s) were received incorrectly preserved and were adjusted accordingly
by adding (circle one): H2SO4 HNO3 HCI NaOH
If more than one preservative is needed, notate in comments below
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Time of preservation:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
Report Number: c.,2o — I 9 So co
ECHEM Pickup' Client Delivery 0 UPS 0
g N/A
k N/A
Volatiles Sample(s)
were received with headspace
DOC. QA.002 Rev 1

Analytical
Consulting Chemists
ADDRESS:,
Sampled By:C t v u 0
Sample Identification
courCe
Temperature when Received 'C:
Delivered By:: -e.V e G
Comments:
Collection
Time
I.
T L C
NCDENR: DWQ CERTIFICATION i 94 NCDHHS: DLS CERTIFICATION # 37729
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME:
CONTACT NAME: PO NO:
REPORT TO: PHONE/FAX:
COPY TO: email:
6502 Windmill Way Wilmington, NC 28405
OFFICE: 910-392-0223 FAX [phone]
info@ env€ronmentalche lsts,com
REPORT NO:
wno )-1- € 110 f SAMPLE TYPE: = Inftuent, E = Effluent, = Weli, ST = Strew , SO w Soits S , Studgey Other:
Accepted:
Received By:
Da Time
4(CC. t,
cted:
PRESERVATION
CC ci
Receh,ed By
ANALYSIS REQUESTED
Resample Requested:
Date: l l 1 tV / 0 Time:
TURNAROUND:

ANALYTICAL & CONSULTING CHEMISTS
vino ental a fists, I c.
6602 Windmill Way, Wilmington, NC 28405 $ 910.392.0223 Lab $ 910,392,4424 Fax
710 Bowsertown Road, Manteo, NC 27954 $ 252,4 3.5702 Lab; Fax
255-A Wilmington Highway, Jacksonville, NC 28540 • 910,3473843 Lab/`Fax
info(a environmenta;'che ists.com
NCDEQJDWR-Fayetteville Date of Report: Nov 18, 2020
225 Green Street Customer PO #:
Fayetteville NC 28301 Customer ID: 19020022
Attention: Trent Allen Report #: 2020-19506
Project ID: Barry Billups 9-99
Lab ID
20-49628
Test
Sample ID:
Site: Upstream
Method
Fecal Coliforrn
Lab ID
20-49629
Test
Sample ID:
Site: Source
SM 92220 MF
Method
Collect Date/Time
11 /16/2020 1:04 PM
Collect Date/Time
Matrix
Water
Results
Sampled by
Guyton/Fontenot
Date Analyzed
7000 Colonies/100mL 11/16/2020
Matrix Sampled by
11/16/2020 1:1 0 PM Water Guyton/Fontenot
Date Analyzed
Results
Fecal Coliform
SM 9222D MF
Lab ID Sample ID:
20-49630 Site: Conic/Source
Test
>60000 Colonies/100m i_ 11 /1 6/2020
Method
Collect Date/Time Matrix Sampled by
11/16/2020 1:04 PM Water Guyton/Fontenot
Results Date Analyzed
Fecal Coiifornn
SM 92220 MFF
Lab ID
20-49631
Tes
Sample ID:
Site: Downstream
Fecal Coil arm
Comment:
Reviewed by:
Method
SM 9222D MF
26000 Colonies/100mL 11/16/2020
Collect Dated" ime Matrix
11/16/2020 12:56 PM Water
Results
Sampled by
Guyton/Fontenot
Date Analyzed
23000 Colonies/100mL 11/16/2020
Report 2.020 1 y 6

Environmental Chemist, Inc., Wilmington, NC Lab #94
Client:
Sample Receipt Checklist
Date:
6602 Windmill Way
Wilmington, NC 28405
910.392.0223
0 Report Number: 19 50(
Receipt of sample: ECHEM Pickup Client Delivery 0
UPS 0 FedEx 0 Other 0
❑ YES
• NO
(4 N/A
1. Were custody seals present on the cooler?
• YES
• NO
q N/A
2. if custody seals were present, were they intact/unbroken?
Original temperature upon receipt °C Corrected temperature upon receipt °C
How temperature taken: • Temperature Blank ' Against Bottles
IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor °C: 0.0
❑ YES
■ NO
3. if temperature of cooler exceeded 6°C, was Project Mgr./QA notified?
tg YES
• NO
4. Were proper custody procedures (relinquished/received) followed? J
1 YES
• NO
5. Were sample ID's listed on the COC?
`X YES
0 NO
6. Were samples ID's listed on sample containers?
k' YES
• NO
7. Were collection date and time listed on the COC?
lil YES
• NO
8. Were tests to be performed listed on the COC?
R YES
• NO
9. Did samples arrive in proper containers for each test?
t,i( YES
0 NO
10. Did samples arrive in good condition for each test?
[i YES
• NO
11. Was adequate sample volume available?'
11/4-21 vcc
ri kin
•
El YES
El YES
❑ YES
ID YES
,tJ YES
Cl YES
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
❑ NO
12. Were samples received within proper holding time for requested tests?
13. Were acid preserved samples received at a pH of <2? *
14. Were cyanide samples received at a pH >12?
15. Were sulfide samples received at a pH >9?
16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? **
17. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L?
18. Were orthophosphate samples filtered in the field within 15 minutes?
* TOC/Volatiles are pH checked at time of analysis and recorded on the benchsheet.
** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet.
Sample Preservation:
Sample(s)
by adding (circle one):
Time of preservation:
(Must be completed for any sample(s) incorrectly preserved or with headspace)
were received incorrectly preserved and were adjusted accordingly
HNO3 HCi NaOH
If more than one preservative is needed, notate in comments below
H 2 S 0 4
Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or
notify the state lab if directed to analyzed by the customer. Who was notified, date and time:
Volatiles Sample(s) were received with headspace
COMMENT
DOC. QA.f}02 Rev 1

Analytical
Consulting Chemists
Client: N c r e- - D
ADDRESS: _.
1
NC€DENR: DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFRCATiON # 37729
COLLECTION AND CHAIN OF CUSTODY
PROJECT NAME:
CONTACT NAME:
REPORT TO:
COPY TO:
Sampled By:G)t ? v n
Sarnple identification
6602 Windmill Way Wilmington, NC 28405
OFFICE: 910 392-0223 FAX [phone]
info@ enviroramentalche€ €sts coal
REPORT NO:
PO NO:
PHONE FAX:
email:
e Fb f1± e l SAMPLE TYPE: l = influent, E = Effluent, W= Weil, ST = Stream , SO = Soi , S Sludge, Other:
Collection
Date Time Temp
4l[14i2c,
DOUrc.
2u�
c
G
0
a c
co
E
PRESERVATION
u
ANALYSIS REQUESTED
G G
Trans
Relinquished By:
............:................
A
Temperature when Received C:
Delivered By: qpt 11 G
Comments:
Date/Time
Received By:
Dat-fTi e
Accepted: R cted: _Resample Requested:
Received By: " ° Date: l i R RV jQ 0 Time:
TURNAROUND:

ENVIRONMENTAL CHEMISTS, INC
P.O. BOX 1037
WRIGHTSVILLE BEACH, NC 28480
Voice: 910-392-0223
Fax: [phone]
E-Mail: [e-mail]
Bill To:
NCDENR - DWQ - FAYETTEVILLE
225 GREEN STREET
SUITE 714
FAYETTEVILLE, NC 28301
Customer ID
19020022
Quantity
REPORT #2020-19506, 2020-19507
WATER: BARRRY BILLUPS 9-99; 9-14
DATE SAMPLED: 11/16/2020
CONTACT - TRENT ALLEN, STEVE GUYTON, KATIE FONTENOT
PLEASE USE THE P.O. BOX FOR
ALL REMITTANCES. THANK YOU.
Customer PO
9-14, 9-99
INVOICE NUMBER
176866
Invoice Date:
Nov 20, 2020
Payment Terms
Net 30 Days
ENVIROCHEM'S FEDERAL ID #
56-1894379
Description
Ship Date
11 / 16/20
Page:
Due Date
12/20/20
Unit Price Amount
7.00 FECAL COLIFORM 35.00 245.00
3.00 HOURS TRAVEL/TIME ONSITE 100.00 300.00
EMAIL INVOICE
REPORT HAS BEEN EMAILED.
PLEASE REFERENCE INVOICE NUMBS.
REMITTANCES IN ORDER TO PROPERLY M.
YOUR ACCOUNT. CALL TERESA WOLFE OR Fi .
GODLEY @ 910-392-0223 FOR QUESTIONS.
�T g
\-)
545.00
$ 545.00

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