WQ0003698_Groundwater Monitoring Report November 2022_20221206

GW-59A COMPLIANCE REPORT FORM Permit # WQOM30of
(Submit one each monitoring period with GW-59 farms.)
I
Enter date monitoring results were due. ( c Ott) Will this monitoring report (GW-59 and GW-59A)
YES
NO
be submitted after the established due date?
X
2
Was any required information missing on the GW-59 report forms?
YES
NO
IF the answer to question f or 2 is "YES", list in the space provided below the well identification number(s) and
explain the problems encountered in obtaining the required information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing;. unlocked or missing cap, missing
YES
NO
identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Ofcefor guidance.
V
4
Are any monitored constituents equal to or above the established standards?
YES
7�
NO
if the answer to question 4 is "NO", skip to section 8.
N the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below.,
Seer A���
5
For the constituents Identified in question 4 'above, have standards been exceeded previously for the
YES
NO
same constituent(s) in the same well(s) in the last two years?
x
If the answer to question 5 is "NO", skip to section 8.
If the answer to question 51s "YES", list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection opts for each occurrence (for the last two years).
See- AitmckeA
6
Are the monitoring wells listed in section 5 located at or beyond the review boundary?
YES
NO
X
nswer is "YES"' a groundwater quality problem may be occurring. CONTACT THE REGIONAL
IMMEDIATELY FOR GUIDANCE. If the answer is "NO" monitoring wells maybe improperly
TADcated;contact the Regional Office.
otal a-�FtCV, CID-- 4A-
7
Is the pennittee implementing previously approved actions required by the Division involving this
YES
NO
groundwater quality problem?
X
If the answer to question 7 is "YES", describe those actions in the space provided below.
If the answer to question 7 is "NO", contact he ealonal Office within 90 days; an evaluation maybe
required to determine the impact the waste disposal system is having at the review and comollance
boundaries surrounding this facility. Failure to do so may subiect the permutes to a Notice of Violation,
fines, andforpenalties.
ei e Tonal coAIMC �
8
The person completing this portion (GW-59) of the monitoring report should sign below and submit this
form with G W-59 forms for required wells to'the address provided at the top of the current Gw4il form.
y l �
2 `D
o V
SsIgnatXofftmitteo
o gent) Date cQ
GW-59A 12/8/2003
fD tv L\
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f^

Question #4
i en neTn WHICH EXCEEDS PERMIT
DATE
MONITORING WELL p
PARAMETER
REPORTED
DATA
11.3.22
1
pH
5.9
2
Ammonia
5.4 mg/L
Iron
27,100ug/L
Manganese
1,250 ug/L
pH
6.4
3
Cobalt
2.5 ug/L
Manganese
98.5 ug/L
pH
5.1
4
Manganese
86 ug/L
pH
4.9

QUESTION #5
LAB DATA WHICH EXCEEDS PERMIT FOR LAST 2 PREVIOUS YEARS
REPORTED
DATE MW # PARAMETER DATA
11/16/2020
1
Iron
0.691 mg/L
Manganese
50!6 ug/L
pH
6
2
Ammonia
5.6 mg/L
Iron
21.6 mg/L
Manganese
1490 ug/L
pH
6.4
3
Nitrate
32.1 mg/L
Iron
1.07 mg/L
Manganese
434 ug/L
pH
1 5
4
Manganese
1Z7 ug/L
pH
,5.1
5/18 & 6/1/2021
1
Iron
0.9 8 mg/L
pH
15.9
2
Ammonia
7. mg/L
Iron
39i5mg/L
Manganese
T-0 0 ug/L
3
Nitrate
21'2mg/L
Iron
0.937mg/L
Manganese
265 ug/L
pH
4.9
4
Manganese
2 7 ug/L
pH
5
11.30.21
1
pH
i 5.9
2
Ammonia
6.0 mg/L
Iron
28.4mg/L
Manganese
1080 ug/L
pH
ii 6
3
Nitrate
12.1mg/L
Manganese
132 ug/L
pH
5
4
Manganese
1 9 ug/L
pH
15.1
5/27-6/9/2022
1
pH
5.7
2
Ammonia
6.4 mg/L
Iron
43'A mg/L
Manganese
1,200 ug/L
pH
6.3

3
Manganese
107 ug/L
4
pH
I5.0
Manganese
17�2 ug/L
pH
5.0
11.3.22
1
pH
5.9
2
Ammonia
5.4 mg/L
Iron
27, 00ug/L
Manganese
1,2 0 ug/L
pH
6.4
3
Cobalt
2.5 ug/L
Manganese
'9815 ug/L
pH
15.1
4
Manganese
8§ ug/L
pH
14.9

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ZeAnalytical'
www.Dacelebs.com
November 28, 2022
Mr. Tim Horton
City of Marion
3982 NC Hwy 226 South
Marion, NC 28752
RE: Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Dear Mr. Horton:
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 03, 2022. The results relate only
to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services -Asheville
• Pace Analytical Services - Charlotte
If you have any questions concerning this report, please feel free to contact me
Sincerely,
Lorri Patton
[e-mail]
1(828)254-7176
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical services, I.L.C.
Pagel of 34

Pace Analytical Services, LLC
1ceAnalyfical0 2225 Riverside Dr.
Asheville, NC 28804
waw.pacelabs.com [phone]
CERTIFICATIONS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Pace Analytical Services Charlotte
South Carolina Laboratory ID: 99006
South Carolina Certification #: 99006001
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Drinking Water Cart. #: 99006003
North Carolina Drinking Water Certification #: 37706
Florida/NELAP Certification #: E87627
North Carolina Field Services Certifcation #: 5342
Kentucky LIST Certification #: 84
North Carolina Wastewater Certification #: 12
Louisiana DoH Drinking Water #: LA029
South Carolina Laboratory ID: 99006
UrginiaA/ELAP Certification #: 460221
Pace Analytical Services Asheville
2225 Riverside Drive, Asheville, NC 28804
South Carolina Laboratory ID: 99030
Flodda/NELAP Certification #: E87648
South Carolina Certification #: 99030001
North Carolina Drinking Water Certification #: 37712
V rginia/VELAP Certification #: 460222
North Carolina Wastewater Certification #: 40
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 34

aceAnalytical o
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Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE SUMMARY
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Lab ID
Sample ID
Matrix
Date Collected
Data Received
92634703001
MW-1R
Water
11/03/22 11:50
11/03/22 17:35
92634703002
MW-2
Water
1110312215:00
11/03/2217:35
92634703003
MW-3
Water
11/0312214:10
11/03/2217:35
92634703004
MW4
Water
11/03/2215:45
11/03/2217:35
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, L.I.C. Page 3 of 34

aceAnalytical e
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SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Monitoring Wells November 2022
92634703
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92634703001
MW-1R
EPA 200.8 Rev 5.4
DB131
6
PASI-A
SM 6200B
SAS
63
PASI-C
EPA 350.1 Rev 2.01993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92634703002
MW-2
EPA 200.8 Rev 5.4
CRW, DBBi
6
PASI-A
SM 6200B
SAS
63
PASI-C
EPA 350.1 Rev 2.01993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92634703003
MW-3
EPA 200.8 Rev 5.4
CRW, DBBi
6
PASI-A
SM 6200B
SAS
63
PASI-C
EPA 350.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 351.2 Rev 2.0 1993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
92634703004
MW4
EPA 200.8 Rev 5.4
DBB1
6
PASI-A
SM 6200B
SAS
63
PASI-C
EPA 360.1 Rev 2.0 1993
ARJ
1
PASI-A
EPA 351.2 Rev 2.01993
MFO
1
PASI-A
EPA 353.2 Rev 2.0 1993
MFO
2
PASI-A
SM 4500-P E-2011
JP1
1
PASI-A
PASI-A = Pace Analytical Services - Asheville
PASI-C = Pace Analytical Services - Charlotte
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of PaceAnaytical Services, LLC. Page 4 of 34

Pace Analytical Services, LLC
aceAnalytical a 2225 Riverside 04
Asheville, NC 28804
www.pecelabsxom
[phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-1R tab ID: 92634703001 Collected: 11/03/2211:50 Received: 11103/2217:35 Matra: Water
Parameters
Monitoring Well Data
Performed by
Collected By
Collected Date
Collected Time
PH
Temperature
Static Water Level
Specific Conductance
Oxygen, Dissolved
Total Well Depth
Turbidity
Odor
Appearance
Results Units PQL MDL OF Prepared
Analytical Method:
Pace Analytical Services - Charlotte
Pace
R. Byes
1113122
11:50
5.9
Std. Units
23.0
deg C
28.46
feet
24.9
umhos/cm
5.6
mg/L
62.62
feet
21.9
NTU
None
White
particulat
as
Analyzed CAS No. Qual
11/10/22 11:37
11/10/22 11:37
11/1022 11:37
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37 778244-7
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37
11/10/22 11:37
200.8 MET ICPMS
Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4
Pace Analytical Services -Asheville
Barium
34.6
ug/L
1.0
0.21
1
11/12/2211:26
11/13/2222:25
7440-39-3
Boron
ND
ug/L
50.0
8.5
1
11/12/2211:26
11/13/2222:25
7440-42-8
Cadmium
ND
ug/L
0.20
0.060
1
11/12/2211:26
11/13/2222:25
744043-9
Cobalt
0.30J
ug/L
1.0
0.050
1
11/12/2211:26
11/13/2222:25
7440484 B
Iron
86.9
ug/L
50.0
20.9
1
1111212211:26
11/13/2222:25
7439-89-6
Manganese
17.5
ug/L
2.0
1.0
1
11/12/22 11:26
11/13/22 22:25
7439-96-5
6200B MSV
Analytical
Method: SM 6200B
Pace Analytical Services - Charlotte
Benzene
NO
ug/L
0.50
0.34
1
11/1312214:07
71-43-2
Bromobenzene
NO
ug/L
0.50
0.29
1
11/13/22 14:07
108-86-1
Bromochloromethane
NO
ug/L
0.50
0.47
1
11/13/22 14:07
74-97-5
Bromodichloromethane
NO
ug/L
0.50
0.31
1
11/13/22 14:07
75-274
Bromoform
NO
ug/L
0.50
0.34
1
11/13/22 14:07
75-25-2
Bromomethane
NO
ug/L
5.0
1.7
1
11/13/22 14:07
74-83-9
n-Butylbenzene
NO
ug/L
0.50
0.49
1
11/1312214:07
104-51-8
sec-Butylbenzene
NO
ug/L
0.50
0.40
1
11/13/22 14:07
135-98-8
tert-Butylbenzene
NO
ug/L
0.50
0.32
1
11/13/22 14:07
98-06-6
Carbon tetrachloride
NO
ug/L
0.50
0.33
1
11/13/22 14:07
56-23-5
Chlorobenzene
NO
ug/L
0.50
0.28
1
11/13/22 14:07
108-90-7
Chloroethane
NO
ug/L
1.0
0.65
1
11/13/22 14:07
75-00-3
Chloroform
NO
ug/L
0.50
0.43
1
11/13/22 14:07
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
11/132214,07
74-87-3
2-Chlorotoluene
NO
ug/L
0.50
0.32
1
11/13/22 14:07
95-49-8
4-Chlorotoluene
NO
ug/L
0.50
0.32
1
11/13/22 14:07
106434
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
0.34
1
11/1312214:07
96-12-8
Dibromochloromethane
NO
ug/L
0.50
0.36
1
11/13/22 14:07
12448-1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1128/2022 12:26 PM without the written consent of Pace Analytical Services, LLC. Page 5 of 34

aceAnalytical e
www.Dacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MWAR Lab ID: 92634703001 Collected: 1110312211:50 Received: 11/03/2217:35 Matra: Water
Parameters Results Units PQL MDL OF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
1,2-Dibromcelhane (EDB)
ND
ug/L
0.50
0.27
1
11/13/22 14:07
106-93-4
Dibrorromethane
NO
ug/L
0.50
0.39
1
11/13/22 14:07
74-95-3
1,2-Dichlorobenzene
NO
ug/L
0.50
0.34
1
11/13/22 14:07
95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
0.34
1
11/13/22 14:07
541-73-1
1,4-Dichlorobenzene
NO
ug/L
0.50
0.33
1
11/13/22 14:07
106-46-7
Dichlorodifluoromethane
NO
ug/L
0.50
0.35
1
11/13/22 14:07
75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
0.37
1
11/13/22 14:07
75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
0.32
1
11/13/22 14:07
107-06-2
1,1-Dichloroethene
NO
ug/L
0.50
0.35
1
11/13/22 14:07
75-354
cis-1,2-Dichloroethene
NO
ug/L
0.50
0.38
1
11/1312214:07
156-59-2
trans-1,2-Dichloroethene
NO
ug/L
0.50
0.40
1
11/13/22 14:07
156-60-5
1,2-Dichloropropane
NO
ug/L
0.50
0.36
1
11/13/22 14:07
78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
0.28
1
11/13/22 14:07
142-28-9
2,2-Dichloropropane
NO
ug/L
0.50
0.39
1
11/13/22 14:07
594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
0.43
1
11/13/22 14:07
563-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
0.36
1
11/13/22 14:07
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
0.50
0.36
1
11/13/22 14:07
10061-02-6
Diisopropyl ether
NO
ug/L
0.60
0.31
1
11/13/22 14:07
108-20-3
Ethylbenzene
NO
ug/L
0.50
0.30
1
11/13/22 14:07
10041-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1.5
1
11/13/22 14:07
87-68-3
Isopropylbenzene(Cumene)
NO
ug/L
0.50
0.33
1
11/13/22 14:07
98-82-8
Methylene Chloride
NO
ug/L
2.0
2.0
1
11/13/22 14:07
75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
0.42
1
11/13/22 14:07
1634-04-4
Naphthalene
NO
ug/L
2.0
0.64
1
11/13/22 14:07
91-20-3
n-Propylbenzene
NO
ug/L
0.50
0.34
1
11/13/22 14:07
103-65-1
Styrene
NO
ug/L
0.50
0.29
1
11/1312214:07
10042-5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
0.31
1
11/13/22 14:07
630-20-6
1, 1,2,2-Tetrachloroethane
NO
ug/L
0.50
0.22
1
11/13/22 14:07
79-34-5
Telrachloroethene
NO
ug/L
0.50
0.29
1
11/13/22 14:07
127-184
Toluene
NO
ug/L
0.50
0.24
1
11/1312214:07
108-88-3
1,2,3-Trichlorobenzene
NO
ug/L
2.0
0.81
1
11/13/22 14:07
87-61-6
1,2,4-Tdchlorobenzene
NO
ug/L
2.0
0.64
1
11/13/22 14:07
120-82-1
1,1,1-Tdchloroethane
NO
ug/L
0.50
0.33
1
11/1322 14:07
71-55-6
1,1,2-Trichlorcethane
NO
ug/L
0.50
0.32
1
11/13/22 14:07
79-00-5
Trichlorcethene
NO
ug/L
0.50
0.38
1
11/13/22 14:07
79-01-6
Trichlorofluoromethane
NO
ug/L
1.0
0.30
1
11/13/22 14:07
75-694
1,2,3-Trichloropropane
NO
ug/L
0.50
0.26
1
11/132214:07
96-184
1,2,4-Trimethylbenzene
NO
ug/L
0.50
0.50
1
11/13/22 14:07
95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
0.33
1
11/13/22 14:07
108-67-8
Vinyl chloride
NO
ug/L
1.0
0.39
1
11/13/22 14:07
75-014
m&p-Xylene
NO
ug/L
1.0
0.71
1
11/13/22 14:07
179601-23-1
o-Xylene
NO
ug/L
0.50
0.34
1
11/13/22 14:07
9547-6
Surrogates
1,2-Dichloroethane-d4 (S)
103
%
70-130
1
11/13/22 14:07
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
1
11/13/22 14:07
460-004
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1128/2022 12:26 PM Wthout the written consent of PaceAnaytical Services, LLC. Page 6 of 34

Pace Analytical services, LLC
ceAnalytical ® 2225 Riverside Dr.
wwalj4i.com Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-1R Lab ID: 92634703001 Collected: 11/03/2211:50 Received: 11/03/2217:35 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qual
6200E MSV Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
Surrogates
Toluene-d8 (S)
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total KJeldahl Nitrogen
Nitrogen, KJeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM450013-E, Phosphate, Ortho
Orthophosphate as P
Date: 11/28/202212:26 PM
102 % 70-130
1
11/13/22 14:07
2037-26-5
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND rtg/L 0.10 0.031
1
11111/2214:07
7664-41-7
Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.50 0.25
1
11/16/22 19:28 11/17/22 05:56
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
0.068 mg/L 0.040 0.010
1
11/04/2203:08
14797-55-8
ND mg/L 0.040 0.031
1
11/04/2203:08
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.026J mg/L 0.050 0.012
1
11/04/2204:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
vothout the vaiden consent of PaceAnalytical Services, L-C.
Page 7 of 34

Pace Analytical Services, LLC
® 2225 Riverside Dr.
aceAnalytical Asheville, NC 28804
www.parolabsxom
[phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-2 Lab ID: 92634703002 Collected: 11/03/2215:00 Received: 11/03/22 17:35 Matra: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical
Method:
Pace Analytical Services
- Charlotte
Performed by
Pace
1
11/10/22 11:39
Collected By
R. Byes
1
11/10/22 11:39
Collected Date
11/3122
1
11/10/22 11:39
Collected Time
15:00
1
11/10/22 11:39
pH
6.4
Std. Units
1
11/10/22 11:39
Temperature
18.5
deg C
1
11/10/22 11:39
Static Water Level
19.37
feet
1
11/10/22 11:39
Specific Conductance
289.3
umhos/cm
1
11/10/22 11:39
Oxygen, Dissolved
0.6
ng/L
1
11/10/22 11:39
7782-44-7
Total Well Depth
38.02
feet
1
11/10/22 11:39
Turbidity
3.9
NTU
1
11/1012211:39
Odor
Sulfur
1
11/10/22 11:39
Appearance
Clear
1
11/10/22 11:39
200.8 MET ICPMS
Analytical
Method: EPA 200.8 Rev 5.4
Preparation Method:
EPA 200.8 Rev 5.4
Pace Analytical
Services
-Asheville
Barium
44.3
ug/L
1.0
0.21
1
11/1212211:26
11/13/2222:29
7440-39-3
Boron
41.OJ
ug/L
50.0
8.5
1
11/12/2211:26
11/13/2222:29
7440-42-8
Cadmium
ND
ug/L
0.20
0.060
1
11/12/2211:26
11/13/2222:29
7440-43-9
Cobalt
0.801
ug/L
1.0
0.050
1
11/1212211:26
11/13/2222:29
7440-48-4
Iron
27100
ug/L
1000
419
20
11/1212211:26
11/14/2217:28
7439-89-6
Manganese
1260
ug/L
40.0
20.4
20
11/1212211:26
11/14/2217:28
7439-96-5
6200B MSV
Analytical
Method: SM 6200B
Pace Analytical
Services - Charlotte
Benzene
NO
ug/L
0.50
0.34
1
11/13/2214:25
71-43-2
Bromobenzene
NO
ug/L
0.50
0.29
1
11/132214:25
108-86-1
Bromochloromethane
NO
ug/L
0.50
0.47
1
11/1312214:25
74-97-5
Bromodichloromethane
NO
ug/L
0.50
0.31
1
11/13/2214:25
75-27-4
Bromoform
ND
ug/L
0.50
0.34
1
11/13/2214:25
75-25-2
Bromomethane
NO
ug/L
5.0
1.7
1
11/13/2214:25
74-83-9
n-Butylbenzene
NO
ug/L
0.50
0.49
1
11/13/2214:25
104-51-8
seo-Butylbenzene
ND
ug/L
0.50
0.40
1
11113/2214:25
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
0.32
1
11/132214,25
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
0.33
1
11/13/22 14:25
56-23-5
Chlorobenzene
NO
ug/L
0.50
0.28
1
11/13/2214:25
108-90-7
Chlorcethane
NO
ug/L
1.0
0.65
1
11/132214:25
75-00-3
Chloroform
NO
ug/L
0.50
0.43
1
11/132214:25
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
11/132214:25
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
0.32
1
11/1312214:25
95-49-8
4-Chlorotoluene
NO
ug/L
0.50
0.32
1
11/132214:25
106-43-4
1,2-Dibromo-3-chloropropane
NO
ug/L
1.0
0.34
1
11/13/2214:25
96-12-8
Dibromochloromethane
NO
ug/L
0.50
0.36
1
11/132214:25
12448-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
0.27
1
11/13/22 14:25
106-93-4
Dibromomethane
ND
ug/L
0.50
0.39
1
11/13/2214:25
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1128/2022 12:26 PM Without the written consent of PaceAnalytical Services, L-C. Page 8 of 34

Pace Analytical Services, LLC
e 2225 Riverside Dr.
aceAnalytical Asheville, NC 28804
www.pacelabs.com
[phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-2 Lab ID: 92634703002 Collected: 11/0312215:00 Received: 11/03/2217:35 Matrix: Water
Parameters Results Units PQL MDL DF Prepared Analyzed CAS No. Qua]
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND
ug/L
0.50
0.34
1
11/13/22 14:25
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
0.34
1
11/13/22 14:26
641-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
0.33
1
11/13/22 14:25
10646-7
Dichlorodifluoromethane
ND
ug/L
0.50
0.35
1
11/13/2214:26
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
0.37
1
11/13/22 14:25
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
0.32
1
11/13/22 14:25
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
0.35
1
11/13/22 14:25
75-35-4
cis-1,2-Dichloroelhene
ND
ug/L
0.50
0.38
1
11/13/22 14:25
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
0.40
1
11/13/22 14:25
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
0.36
1
11/13/22 14:25
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
0.28
1
11/13/22 14:25
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
0.39
1
11/13/22 14:25
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
0.43
1
11/13/22 14:25
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
11/13/22 14:25
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
11/13/22 14:25
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
0.31
1
11/13/22 14:25
108-20-3
Ethylbenzene
ND
ug/L
0.50
0.30
1
11/13/22 14:25
100-41-4
Hexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
111132214:25
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
0.33
1
11/1322 14:25
98-82-8
Methylene Chloride
ND
ug/L
2.0
2.0
1
11/13/22 14:25
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
0.42
1
11/13/22 14:25
1634-04-4
Naphthalene
ND
ug/L
2.0
0.64
1
11/13/22 14:25
91-20-3
n-Propylbenzene
ND
ug/L
0.50
0.34
1
11/13/22 14:25
103-65-1
Styrene
ND
ug/L
0.50
0.29
1
11/13/22 14:25
100-42-5
1,1,1,2-Tetrachloroethane
ND
ug/L
0.50
0.31
1
1111322 14:25
630-20-6
1, 1,2,2-Tetrachloroethane
ND
ug/L
0.50
0.22
1
11/1322 14:25
79-34-5
Tetrachloroethene
ND
ug/L
0.50
0.29
1
11/13/22 14:25
127-184
Toluene
ND
ug/L
0.50
0.24
1
11/1322 14:25
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
0.81
1
11/13/22 14:25
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
0.64
1
11/1322 14:25
120-82-1
1, 1, 1 -Trichloroethane
ND
ug/L
0.50
0.33
1
11/13/22 14:25
71-55-6
1,1,2-Trichloroethane
ND
ug/L
0.50
0.32
1
11/13/22 14:25
79-00-5
Tdchloroethene
ND
ug/L
0.50
0.38
1
11/13/22 14:25
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
11/13/22 14:25
75-69-4
1,2,3-Trichloropropane
ND
ug/L
0.50
0.26
1
11/132214:25
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
0.50
1
11/13/22 14:25
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
0.33
1
11/13/22 14:25
108-67-8
unyl chloride
ND
ug/L
1.0
0.39
1
11/13/22 14:25
75-01-4
m&p-Xylene
ND
ug/L
1.0
0.71
1
11/13/22 14:25
179601-23-1
o-Xylene
ND
ug/L
0.50
0.34
1
11/13/22 14:25
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
106
%
70-130
1
11/13/22 14:25
17060-07-0
4-Bromofluorobenzene (S)
100
%
70-130
1
11/13/22 14:25
460-004
Toluene-d8 (S)
102
%
70-130
1
11/13/22 14:25
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 1128/2022 12:26 PM vnthout the written consent of Pace Analytical Services, LLC. Page 9 of 34

Pace Analytical Services, LLC
® 2225 Riverside Dr.
1c7e Analytical Asheville, NC 28804
www.pacelabs.cam
[phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-2 Lab ID: 92634703002 Collected: 11103/2215:00 Received: 11/03/2217:35 Matra: Water
Parameters
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 11/2812022 12:26 PM
Results Units PQL MDL
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
6.4 mg/L 0.10 0.031
1
11/11/2214:08
7664-41-7
Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993
Pace Analytical Services -Asheville
4.7 mg/L 0.50 0.26
1
11/16/2219:28 11/17/2205:58
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.040 0.010
1
11/04/2203:16
14797-55-8
0.045 ng/L 0.040 0,031
1
11/04/2203:16
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.043J mg/L 0.050 0.012
1
11/04/2204:39
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 10 of 34

® Pace Analytical Services, LLC
�ceMalytical 2225 Riverside
Asheville, NC 2880404
www.pacelabs.cam [phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-3 Lab ID: 92634703003 Collected: 11/03/2214:10 Received: 11103/2217:35 Matra: Water
Parameters
Results
Units
PQL
MDL
DF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical Method:
Pace Analytical Services - Charlotte
Performed by
Pace
1
11/10/2211,41
Collected By
R. Byes
1
11/10/22 11:41
Collected Date
11/3/22
1
11/10/22 11:41
Collected Time
14:10
1
11/10/22 11:41
pH
5.1
Std. Units
1
11/10/22 11:41
Temperature
17.1
deg C
1
11/10/22 11:41
Static Water Level
34.18
feet
1
11/1022 11:41
Specific Conductance
141.8
umhos/cm
1
11/10/22 11:41
Oxygen, Dissolved
3.6
rrg/L
1
11/10/22 11:41
7782-44-7
Total Well Depth
50.02
feet
1
11/10/22 11:41
Turbidity
9.8
NTU
1
11/10/22 11:41
Odor
None
1
11/1022 11:41
Appearance
Clear
1
111102211:41
200.8 MET ICPMS
Analytical
Method: EPA 200.8 Rev 5.4 Preparation
Method: EPA 200.8 Rev 5.4
Pace Analytical Services
- Asheville
Barium
441
ug/L
10.0
2.1
10
11/12/2211:26
11/14/2217:32
7440-39-3
Boron
ND
ug/L
50.0
8.5
1
11/1212211:26
11/13/2222:32
7440-42-8
Cadmium
0.69
ug/L
0.20
0.060
1
11/1212211:26
11/13/2222:32
7440-43-9
Cobalt
2.5
ug/L
1.0
0.050
1
11/1212211:26
11113/2222:32
7440-48-4
Iron
214
ug/L
50.0
20.9
1
11/1212211:26
11/132222:32
7439-89-6
Manganese
98.5
ug/L
2.0
1.0
1
11/1212211:26
11/13/2222:32
7439-96-5
6200E MSV
Analytical
Method: SM 6200B
Pace Analytical
Services
- Charlotte
Benzene
ND
ug/L
0.50
0.34
1
11/132214:43
71-43-2
Bromobenzene
ND
ug/L
0.50
0.29
1
11/13/2214:43
108-86-1
Bromochloromethane
NO
ug/L
0.50
0.47
1
11/1312214:43
74-97-5
Bromodichloromethane
NO
ug/L
0.50
0.31
1
11/13/2214:43
75-27-4
Bromoform
NO
ug/L
0.50
0.34
1
11/13/2214:43
75-25-2
Bromomethane
ND
ug/L
6.0
1.7
1
11/13/2214:43
74-83-9
n-Butylbenzene
ND
ug/L
0.50
0.49
1
11/13/2214:43
104-51-8
sec,Butylbenzene
ND
ug/L
0.50
0.40
1
11/132214:43
135-98-8
tert-Butylbenzene
ND
ug/L
0.50
0.32
1
11113/2214:43
98-06-6
Carbon tetrachloride
ND
ug/L
0.50
0.33
1
11/13/22 14:43
56-23-5
Chlorobenzene
ND
ug/L
0.50
0.28
1
11/13/2214:43
108-9D-7
Chloroethane
ND
ug/L
1.0
0.65
1
11/13/2214:43
75-00-3
Chloroform
ND
ug/L
0.50
0.43
1
11/13/2214:43
67-66-3
Chloromethane
ND
ug/L
1.0
0.54
1
11/13/2214:43
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
0.32
1
11/13/22 14:43
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
0.32
1
11/1322 14:43
106-43-4
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
0.34
1
11/132214:43
96-12-8
Dibromochloromethane
ND
ug/L
0.50
0.36
1
11/13/2214:43
12448-1
1,2-Dibromoethane (EDB)
ND
ug/L
0.50
0.27
1
11/1312214:43
106-93-4
Dibromomethane
NO
ug/L
0.50
0.39
1
11/1312214:43
74-95-3
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11/2812022 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 11 of 34

aceAnalytical e
www.pecolebs.com
ANALYTICAL RESULTS
Project. Monitoring Wells November 2022
Pace Project No.: 92634703
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Sample:
MW-3
Lab ID:
92634703003
Collected:
11/03/22 14:10
Received:
11/03/2217,35
Matrix: Water
Parameters
Results
Units
PQL
MDL DF
Prepared
Analyzed
CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
ND
ug/L
0.50
0.34
1
11/1322 14:43
95-50-1
1,3-Dichlorobenzene
ND
ug/L
0.50
0.34
1
11/13/22 14:43
541-73-1
1,4-Dichlorobenzene
ND
ug/L
0.50
0.33
1
11/13/22 14:43
106-46-7
Dichlorodifluoromethane
ND
ug/L
0.50
0.35
1
11/13/22 14:43
75-71-8
1,1-Dichloroethane
ND
ug/L
0.50
0.37
1
11/13/22 14:43
75-34-3
1,2-Dichloroethane
ND
ug/L
0.50
0.32
1
11/13/22 14:43
107-06-2
1,1-Dichloroethene
ND
ug/L
0.50
0.35
1
11/13/22 14:43
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
0.50
0.38
1
11/13/22 14:43
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
0.50
0.40
1
11/13/22 14:43
156-60-5
1,2-Dichloropropane
ND
ug/L
0.50
0.36
1
11/13/22 14:43
78-87-5
1,3-Dichloropropane
ND
ug/L
0.50
0.28
1
11/13/22 14:43
142-28-9
2,2-Dichloropropane
ND
ug/L
0.50
0.39
1
11/13/22 14:43
594-20-7
1,1-Dichloropropene
ND
ug/L
0.50
0.43
1
11/13/22 14:43
563-58-6
cis-1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
11/13/22 14:43
10061-01-5
trans-1,3-Dichloropropene
ND
ug/L
0.50
0.36
1
11/13/22 14:43
10061-02-6
Diisopropyl ether
ND
ug/L
0.50
0.31
1
11/13/22 14:43
108-20-3
Ethylbenzene
ND
ug/L
0.50
0.30
1
11/13/22 14:43
100-414
Flexachloro-1,3-butadiene
ND
ug/L
2.0
1.5
1
11/1312214:43
87-68-3
Isopropylbenzene (Cumene)
ND
ug/L
0.50
0.33
1
11/13/22 14:43
98-82-8
Methylene Chloride
ND
ug/L
2.0
2.0
1
11/13/22 14:43
75-09-2
Methyl-tert-butyl ether
ND
ug/L
0.50
0.42
1
11/1322 14:43
1634-04-4
Naphthalene
ND
ug/L
2.0
0.64
1
11/13/22 14:43
91-20-3
n-Propylbenzene
ND
ug/L
0.50
0.34
1
11/13/22 14:43
103-65-1
Styrene
ND
ug/L
0.50
0.29
1
11/13/22 14:43
100-42-5
11,12-Tetrachloroethane
ND
ug/L
0.50
0.31
1
11/13/22 14:43
630-20-6
1, 1,2,2-Tetrachloroethane
ND
ug/L
0.50
0.22
1
11/13/22 14:43
79-34-5
Tetrachloroethene
ND
ug/L
0.50
0.29
1
11/13/22 14:43
127-184
Toluene
ND
ug/L
0.50
0.24
1
11/13/22 14:43
108-88-3
1,2,3-Trichlorobenzene
ND
ug/L
2.0
0.81
1
11/13/22 14:43
87-61-6
1,2,4-Trichlorobenzene
ND
ug/L
2.0
0.64
1
11/13/22 14:43
120-82-1
1. 1. 1 -Trichloroethane
ND
ug/L
0.50
0.33
1
11/13/22 14:43
71-55-6
1,1,2-Tdchloroethane
ND
ug/L
0.50
0.32
1
11/13/22 14:43
79-00-5
Trichloroethene
ND
ug/L
0.50
0.38
1
11/13/22 14:43
79-01-6
Trichlorofluoromethane
ND
ug/L
1.0
0.30
1
11/13/22 14:43
75-694
1,2,3-Trichlompropane
ND
ug/L
0.50
0.26
1
111132214:43
96-18-4
1,2,4-Trimethylbenzene
ND
ug/L
0.50
0.50
1
11/13/22 14:43
95-63-6
1,3,5-Trimethylbenzene
ND
ug/L
0.50
0.33
1
11/13/22 14:43
108-67-8
Vinyl chloride
ND
ug/L
1.0
0.39
1
11/1312214:43
75-01-4
m&p-Xylene
ND
ug/L
1.0
0.71
1
11/13/22 14:43
179601-23-1
o-Xylene
ND
ug/L
0.50
0.34
1
11/13/22 14:43
95-47-6
Surrogates
1,2-Dichloroethane-d4 (S)
104
%
70-130
1
11/13/22 14:43
17060-07-0
4-Bromofluorobenzene (S)
99
%
70-130
1
1111322 14:43
460-00-4
Toluene-d8 (S)
103
%
70-130
1
1111322 14:43
2037-26-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM without the written consent of PacsAnalylical Services, LLC. Page 12 of 34

Pace Analytical Services, LLC
® 2225 Riverside Dr.
acemalytical Asheville, NC 28804
www.pacalassxom [phone]
ANALYTICAL RESULTS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-3 Lab ID: 92634703003 Collected: 11/03/2214:10 Received: 11/03/2217:35 Matrix: Water
Parameters
350.1 Ammonia
Nitrogen, Ammonia
351.2 Total Kjeldahl Nitrogen
Nitrogen, Neldahl, Total
363.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 11/28/2022 12:26 PM
Results Units PQL MDL
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services - Asheville
ND mg/L 0.10 0.031
1
11/11/2214:10
7664-41-7
Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.50 0.25
1
11/16/22 19:28 11/17/22 06:00
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
10.0 mg/L 0.20 0.050
5
11/04/2203:38
14797-55-8
ND rrg/L 0.040 0.031
1
11/04/22 03:13
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
ND mg/L 0.050 0,012
1
11/04/2204:38
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 13 of 34

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ANALYTICAL RESULTS
Project. Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW-4 Lab ID: 92634703004 Collected: 11/03/22 15:45 Received:
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Parameters
Results
Units
PQL
MDL
OF
Prepared
Analyzed
CAS No. Qual
Monitoring Well Data
Analytical
Method:
PaceAnalytical Services - Charlotte
Performed by
Pace
1
11/10/22 11:42
Collected By
R. Byes
1
11/10/22 11:42
Collected Date
1113122
1
11/10/22 1142
Collected Time
15:46
1
11/1022 11:42
pH
4.9
Sid. Units
1
11/10/22 11:42
Temperature
16.9
deg C
1
11/10/22 11:42
Static Water Level
21.03
feet
1
11/1022 11:42
Specific Conductance
60.1
umhos/cm
1
11/10/22 11:42
Oxygen, Dissolved
0.7
mg/L
1
11/10/22 11:42
7782-44-7
Total Well Depth
35.37
feet
1
11/1022 11:42
Turbidity
0.8
NTU
1
11/10/22 11:42
Odor
None
1
11/10/22 11:42
Appearance
Clear
1
11/1022 11:42
200.8 MET ICPMS
Analytical
Method: EPA 200.8 Rev 5.4 Preparation
Method: EPA 200.8 Rev 5.4
Pace Analytical
Services
-Asheville
Barium
108
ug/L
1.0
0.21
1
11/1212211:26
11/132222:36
7440-39-3
Boron
NO
ug/L
50.0
8.5
1
11/1212211:26
11/132222:36
744042-8
Cadmium
0.098.1
ug/L
0.20
0.060
1
11/12/2211:26
11/132222:36
7440-43-9
Cobalt
2.5
ug/L
1.0
0.050
1
11/12/2211:26
11/13/2222:36
7440-48-4
Iron
NO
ug/L
50.0
20.9
1
11/1212211:26
11/1312222:36
7439-89-6
Manganese
86.0
ug/L
2.0
1.0
1
11/12/22 11:26
11/13/22 22:36
7439-96-5
6200E MSV
Analytical
Method: SM 6200B
Pace Analytical
Services
- Charlotte
Benzene
NO
ug/L
0.50
0.34
1
111132215:01
7143-2
Bromobenzene
NO
ug/L
0.50
0.29
1
11/132216:01
108-86-1
Bromochloromethane
NO
ug/L
0.50
0.47
1
11/13/2215:01
74-97-5
Bromodichloromethane
NO
ug/L
0.50
0.31
1
11/13/2215:01
75-274
Bromoform
NO
ug/L
0.50
0.34
1
11/13/2215:01
75-25-2
Bromomethane
NO
ug/L
5.0
1.7
1
11/13/2215:01
74-83-9
n-Butylbenzene
ND
ug/L
0.50
0.49
1
11/13/2215:01
104-51-8
sec-Butylbenzene
ND
ug/L
0.50
0.40
1
111132215:01
135-98-8
tert-Butylbenzene
NO
ug/L
0.50
0.32
1
11/132215:01
98-06-6
Carbon tetrachloride
NO
ug/L
0.50
0.33
1
11/1322 15:01
56-23-5
Chlorobenzene
NO
ug/L
0.50
0.28
1
11/13/2215:01
108-90-7
Chloroethane
NO
ug/L
1.0
0.65
1
11/13/2215:01
75-00-3
Chloroform
NO
ug/L
0.50
0.43
1
11/13/2215:01
67-66-3
Chloromethane
NO
ug/L
1.0
0.54
1
11/13/2215:01
74-87-3
2-Chlorotoluene
ND
ug/L
0.50
0.32
1
11/1322 15:01
95-49-8
4-Chlorotoluene
ND
ug/L
0.50
0.32
1
11/132215:01
106-434
1,2-Dibromo-3-chloropropane
ND
ug/L
1.0
0.34
1
11/13/2215:01
96-12-8
Dibromochloromethane
NO
ug/L
0.50
0.36
1
11/13/2215:01
124-48-1
1,2-Dibromoethane (EDB)
NO
ug/L
0.50
0.27
1
11/132216:01
106-93-4
Dibromomethane
NO
ug/L
0.50
0.39
1
11/13/2215:01
74-95-3
REPORT OF LABORATORY ANALYSIS
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Date: 11/28/2022 12:26 PM wihout the written consent of Pace Analytical Services, LLC. Page 14 of 34

a Analytical
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Monitoring Vklls November 2022
Pace Project No.: 92634703
Sample: MW-4 lab ID: 92634703004 Collected: 11103/2215:45 Received: 11/03/22 17:35 Nlatrbc: Water
Parameters Results Units PQL MDL OF Prepared Analyzed CAS No. Qual
6200B MSV
Analytical Method: SM 6200B
Pace Analytical Services - Charlotte
1,2-Dichlorobenzene
NO
ug/L
0.50
0.34
1
11/13/22 15:01
95-50-1
1,3-Dichlorobenzene
NO
ug/L
0.50
0.34
1
11/13/22 15:01
541-73-1
1,4-Dichlorobenzene
NO
ug/L
0.50
0.33
1
11/1322 15:01
106-46-7
Dichlorodifluoromethane
NO
ug/L
0.50
0.35
1
11/13/22 15:01
75-71-8
1,1-Dichloroethane
NO
ug/L
0.50
0.37
1
11/13/2215:01
75-34-3
1,2-Dichloroethane
NO
ug/L
0.50
0.32
1
11/13/22 15:01
107-06-2
1,1-Dichloroethene
NO
ug/L
0.50
0.35
1
11/13/22 15:01
75-35.4
cis-1,2-Dichloroethene
NO
ug/L
0.50
0.38
1
11/132215:01
156-59-2
trans-1,2-Dichlorcethene
NO
ug/L
0.50
0.40
1
11/13/22 15:01
156-60-5
1,2-Dichloropropane
NO
ug/L
0.50
0.36
1
11/13/22 15:01
78-87-5
1,3-Dichloropropane
NO
ug/L
0.50
0.28
1
11/1322 15:01
142-28-9
2,2-Dichloropropane
NO
ug/L
0.50
0.39
1
11/1322 15:01
594-20-7
1,1-Dichloropropene
NO
ug/L
0.50
0.43
1
11/1322 15:01
563-58-6
cis-1,3-Dichloropropene
NO
ug/L
0.50
0.36
1
11/13/22 15:01
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
0.50
0.36
1
11/1322 15:01
10061-02-6
Diisopropyl ether
NO
ug/L
0.50
0.31
1
11/13/22 15:01
108-20-3
Ethylbenzene
NO
ug/L
0.50
0.30
1
11/1312215:01
100-41-4
Hexachloro-1,3-butadiene
NO
ug/L
2.0
1.5
1
11/13/22 15:01
87-68-3
Isopropylbenzene (Cumene)
NO
ug/L
0.50
0.33
1
11/1322 15:01
98-82-8
Methylene Chloride
NO
ug/L
2.0
2.0
1
11/1322 15:01
75-09-2
Methyl-tert-butyl ether
NO
ug/L
0.50
0.42
1
11/1322 15:01
1634-04-4
Naphthalene
NO
ug/L
2.0
0.64
1
11/13/22 15:01
91-20-3
n-Propylbenzene
NO
ug/L
0.50
0.34
1
11/1312215:01
103-65-1
Styrene
NO
ug/L
0.50
0.29
1
11/13/22 15:01
100-42-5
1,1,1,2-Tetrachloroethane
NO
ug/L
0.50
0.31
1
11/13/22 15:01
630-20-6
1, 1,2,2-Tetrachloroethane
NO
ug/L
0.50
0.22
1
11/13/22 15:01
79-34-5
Tetrachlorcethene
NO
ug/L
0.50
0.29
1
11/13/22 15:01
127-184
Toluene
NO
ug/L
0.50
0.24
1
11/13/22 15:01
108-88-3
1,2,3-Trichlorobenzene
NO
ug/L
2.0
0.81
1
11/13/22 15:01
87-61-6
1,2,4-T(chlorobenzene
NO
ug/L
2.0
0.64
1
11/13/22 15:01
120-82-1
1,1,1-Trichloroethane
NO
ug/L
0.50
0.33
1
11/13/22 15:01
71-55-6
1,12-Trichloroethane
NO
ug/L
0.50
0.32
1
11/132215:01
79-OD-5
Trichloroethene
NO
ug/L
0.50
0.38
1
11/13/22 15:01
79.01-6
Trichlorofluoromethane
NO
ug/L
1.0
0.30
1
11/132215:01
75-69-4
1,2,3-Tdchloropropane
NO
ug/L
0.50
0.26
1
11/13/22 15:01
96-18-4
1,2,4-Trimethylbenzene
NO
ug/L
0.50
0.50
1
11/13/22 15:01
95-63-6
1,3,5-Trimethylbenzene
NO
ug/L
0.50
0.33
1
11/13/22 15:01
108-67-8
Vinyl chloride
NO
ug/L
1.0
0.39
1
11/1312215:01
75-01-4
m&p-Xylene
NO
ug/L
1.0
0.71
1
11/13/22 15:01
179601-23-1
o-Xylene
NO
ug/L
0.50
0.34
1
11/13/22 15:01
95-47-6
Surrogates
1,2-Dichloroethaned4 (S)
99
%
70-130
1
11/13/22 15:01
17060-07-0
4-Bromofluorot)enzene (S)
101
%
70-130
1
1111322 15:01
460-00-4
Toluene-d8 (S)
103
%
70-130
1
11/13/22 15:01
2037-26-5
REPORT OF LABORATORY ANALYSIS
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Dale: 11282022 12:26 PM without the wntten consent of PaceAnalytical Services, L-C. Page 15 of 34

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ANALYTICAL RESULTS
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
Sample: MW4 Lab ID: 92634703004 Collected: 11/03/2215:45 Received: 11103/2217:35 Matroc: Water
Parameters
350.1 Ammonia
Nitrogen, Ammonia
361.2 Total Kjeldahl Nitrogen
Nitrogen, Kjeldahl, Total
353.2 Nitrogen, NO2/NO3 unpres
Nitrogen, Nitrate
Nitrogen, Nitrite
SM4500P-E, Phosphate, Ortho
Orthophosphate as P
Date: 11/28/2022 12:26 PM
Results Units PQL MDL
DF
Prepared Analyzed
CAS No. Qual
Analytical Method: EPA 350.1 Rev 2.0 1993
Pace Analytical Services -Asheville
ND mg/L 0.10 0.031
1
11/11/2214:14
766441-7
Analytical Method: EPA 351.2 Rev 2.01993 Preparation Method: EPA 351.2 Rev 2.01993
Pace Analytical Services -Asheville
ND ng/L 0.50 0.25
1
11/16/2219:28 11/17/2206:01
7727-37-9
Analytical Method: EPA 353.2 Rev 2.0 1993
Pace Analytical Services -Asheville
2.9 rrg/L 0.040 0.010
1
11/04/22 03:17
14797-55-8
ND mg/L 0.040 0.031
1
11/04/2203:17
14797-65-0
Analytical Method: SM 4500-P E-2011
Pace Analytical Services -Asheville
0.0151 mg/L 0.050 0,012
1
11/04/2204:40
REPORT OF LABORATORY ANALYSIS
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without the written consent of PaceAnalytical Services, L-C.
Page 16 of 34

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QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 736695 Analysis Method: EPA 200.8 Rev 5.4
QC Batch Method: EPA 200.8 Rev 5.4 Analysis Description: 200.8 MET
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3834138
Matrix:
Water
Associated Lab Samples:
92634703001, 92634703002, 92634703003, 92634703004
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed Qualifiers
Barium
ug/L
ND
1.0
0.21
11/13/2222:18
Boron
ug/L
ND
50.0
8.5
11/13/2222:18
Cadmium
ug/L
ND
0.20
0.060
11/13/2222:18
Cobalt
ug/L
0.12J
1.0
0.050
11/13/22 22:18
Iron
ug/L
ND
50.0
20.9
11/13/2222:18
Manganese
ug/L
ND
2.0
1.0
11/13/2222:18
LABORATORY CONTROL SAMPLE: 3834139
Spike
LCS
LCS
%Rec
Parameter
Units
Conic.
Result
%Rec
Limits Qualifiers
Barium
ug/L
50
48.8
98
85-115
Boron
ug/L
50
48.1J
96
85-115
Cadmium
ug/L
50
50.2
100
85-115
Cobalt
ug/L
50
50.9
102
85-115
Iron
ug/L
1250
1280
102
85-115
Manganese
ug/L
50
50.3
101
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834140
3834141
MS
MSD
92634594005
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Barium
ug/L
ND
50
50
47.8
48.8
96
98
70-130
2
20
Boron
ug/L
NO
50
50
52.5
54.0
97
100
70-130
3
20 CH
Cadmium
ug/L
ND
50
50
49.3
49.9
99
100
70-130
1
20
Cobalt
ug/L
NO
50
50
49.7
50.2
99
100
70-130
1
20
Iron
ug/L
ND
1250
1250
1260
1270
99
101
70-130
1
20
Manganese
ug/L
ND
50
50
49.1
50.1
98
100
70-130
2
20
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834142
3834143
MS
MSD
92634682001 Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter Units Result Conc.
Conc.
Result
Result
%Rec
%Rec
Limits RPD
RPD Qual
Barium ug/L 13.1 50
50
63.3
62.7
100
99
70-130 1
20
Boron ug/L 378 50
50
431
410
107
65
70-130 5
20 CH,E,
M1
Cadmium ug/L ND 50
50
43.4
42.9
87
86
70-130 1
20
Results presented on this page are in the units indicated by the
"Units" column
except where an alternate unit is presented to the right
of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM Wihout the written consent of PaceAnalytical Services, LLC.
Page 17 of 34

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QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Monitoring Wells November 2022
92634703
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834142
3834143
MS
MSD
92634682001
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD RPD Qual
Cobalt
ug/L ND
50
50
47.7
47.2
95
94
70-130
1 20
Iron
ug/L 545
1250
1250
1740
1720
96
94
70-130
1 20
Manganese
ug/L 10
50
50
59.5
58.4
99
97
70-130
2 20
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /28/2022 12:26 PM without the written consent of Pace Analytical Services, I.I.C.
Page 18 of 34

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QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 736729 Analysis Method: SM 6200B
QC Batch Method: SM 6200B Analysis Description: 6200E MSV
Laboratory: Pace Analytical Services - Charlotte
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
METHOD BLANK: 3834279 Matra: Water
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Blank Reporting
Parameter Units Result Limit
MDL
Analyzed
1,1,1,2-Tetrachloroethane
ug/L
ND
0.50
0.31
11/13/22 09:19
1,1,1-Trichlorcethane
ug/L
ND
0.50
0.33
11/13/22 09:19
1,1,2,2-Tetrachloroethane
ug/L
ND
0.60
0.22
11/13/22 09:19
1,1,2-Trichloroethane
ug/L
ND
0.50
0,32
11/13/22 09:19
1,1-Dichloroethane
ug/L
ND
0.50
0.37
11/13/22 09:19
1,1-Dichloroethene
ug/L
ND
0.50
0.35
11/13/22 09:19
1,1-Dichloropropene
ug/L
ND
0.50
0.43
11/13/22 09:19
1,2,3-Trichlorobenzene
ug/L
ND
2.0
0.81
11/13/22 09:19
1,2,3-Trichloropropane
ug/L
ND
0.50
0.26
11/13/22 09:19
1,2,4-Trichlorobenzene
ug/L
NO
2.0
0.64
11/13/22 09:19
1,2,4-Trimethylbenzene
ug/L
NO
0.50
0.50
11/13/22 09:19
1,2-Dibromo-3-chloropropane
ug/L
NO
1.0
0.34
11/13/22 09:19
1,2-Dlbromoethane(EDB)
ug/L
NO
0.50
0.27
11/13/22 09:19
1,2-Dichlorobenzene
ug/L
NO
0.50
0.34
11/13/22 09:19
1,2-Dichloroethane
ug/L
NO
0.50
0.32
11/13/22 09:19
1,2-Dichloropropane
ug/L
NO
0.50
0,36
11/13/22 09:19
1,3,5-Trimethylbenzene
ug/L
NO
0.50
0.33
11/13/22 09:19
1,3-Dichlorobenzene
ug/L
NO
0.50
0.34
11/13/22 09:19
1,3-Dichloropropane
ug/L
NO
0.50
0.28
11/13/22 09:19
1,4-Dichlorobenzene
ug/L
ND
0.50
0.33
11/13/22 09:19
2,2-Dichloropropane
ug/L
ND
0.50
0.39
11/13/22 09:19
2-Chlorotoluene
ug/L
NO
0.50
0.32
11/1312209:19
4-Chlorotoluene
ug/L
NO
0.50
0.32
11/13/22 09:19
Benzene
ug/L
NO
0.50
0.34
11/13/22 09:19
Bromobenzene
ug/L
NO
0.50
0.29
11/13/22 09:19
Bromochloromethane
ug/L
NO
0.50
0.47
11/1312209:19
Bromodichloromethane
ug/L
NO
0.50
0.31
11/13/22 09:19
Bromoform
ug/L
NO
0.50
0.34
11/13/22 09:19
Bromomethane
ug/L
NO
5.0
1.7
11/13/22 09:19
Carbon tetrachloride
ug/L
NO
0.50
0.33
11/13/22 09:19
Chlorobenzene
ug/L
NO
0.50
0.28
11/13/22 09:19
Chlorcethane
ug/L
ND
1.0
0.65
11/13/22 09:19
Chloroform
ug/L
ND
0.50
0.43
11/13/22 09:19
Chloromethane
ug/L
ND
1.0
0.54
11/13/22 09:19
cis-1,2-Dichloroethene
ug/L
ND
0.50
0.38
11/13/22 09:19
cis-1,3-Dichloropropene
ug/L
NO
0.50
0.36
11/13/22 09:19
Dibromochloromethane
ug/L
ND
0.50
0.36
11/13/2209:19
Dibromomethane
ug/L
ND
0.50
0.39
11/13/22 09:19
Dichlorodifluoromethane
ug/L
NO
0.50
0.35
11/13/22 09:19
Diisopropyl ether
ug/L
NO
0.50
0.31
11/13/22 09:19
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are In the units indicated by the "Unit" column except where an alternate unit is presentetl to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM wthout the written consent of Pace Analytical Services, LLC. Page 19 of 34

w
ace Analytical
www.Pacslass.com
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3834279
Matra:
Water
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Blank
Reporting
Parameter
Units
Result
Limit
MDL
Analyzed
Qualifiers
Ethylbenzene
ug/L
ND
0.50
0.30
11/13/22 09:19
Hexachloro-1,3-butadiene
ug/L
ND
2.0
1.5
11/13/22 09:19
Isopropylbenzene(Cumene)
ug/L
ND
0.50
0.33
11/13/22 09:19
m&p-Xylene
ug/L
NO
1.0
0.71
11/13/22 09:19
Methyl-tert-butyl ether
ug/L
NO
0.50
0.42
11/13/22 09:19
Methylene Chloride
ug/L
NO
2.0
2.0
11/13/22 09:19
n-Butylbenzene
ug/L
ND
0.50
0.49
11/13/22 09:19
n-Propylbenzene
ug/L
ND
0.50
0.34
11/13/22 09:19
Naphthalene
ug/L
ND
2.0
0.64
11/1312209:19
o-Xylene
ug/L
ND
0.50
0.34
11/13/2209:19
see-Butylbenzene
ug/L
ND
0.50
0.40
11/13/22 09:19
Styrene
ug/L
ND
0.50
0.29
11/13/22 09:19
tert-Butylbenzene
ug/L
ND
0.50
0.32
11/13/22 09:19
Tetrachloroethene
ug/L
ND
0.50
0.29
11/1312209:19
Toluene
ug/L
ND
0.50
0.24
11/13/22 09:19
trans-1,2-Dichloroethene
ug/L
ND
0.50
0.40
11/13/22 09:19
trans-1,3-Dichloropropene
ug/L
ND
0.50
0.36
11/13/22 09:19
Trichloroethene
ug/L
ND
0.50
0.38
11/13/22 09:19
Trichloro8uoromethane
ug/L
ND
1.0
0.30
11/13/22 09:19
Vinyl chloride
ug/L
ND
1.0
0.39
11/13/22 09:19
1,2-Dichloroethane-d4 (S)
%
102
70-130
11/13/22 09:19
4-Bromofluorobenzene(S)
%
103
70-130
11/13/22 09:19
Toluene-d8 (S)
%
102
70-130
11/13/22 09:19
LABORATORY CONTROL SAMPLE:
3834280
Spike
LCS
LCS
%Rec
Parameter
Units
Conc.
Result
%Rec
Limits Qualifiers
1,1, 1,2-Tetrachloroethane
ug/L
50
53.2
106
60-140
1,1,1-Trichloroethane
ug/L
50
53.9
108
60-140
1, 1,2,2-Tetrachloroethane
ug/L
50
51.8
104
60-140
1,1,2-Trichloroelhane
ug/L
50
50.5
101
60-140
1,1-Dichloroethane
ug/L
50
50.2
100
60-140
1,1-Dichloroethene
ug/L
50
52.6
105
60-140
1,1-Dichloropropene
ug/L
50
57.6
115
60-140
1,2,3-Trichlorobenzene
ug/L
50
47.8
96
60-140
1,2,3-Trichloropropane
ug/L
50
52.2
104
60-140
1,2,4-Trichlorobenzene
ug/L
50
49.5
99
60-140
1,2,4-Trimethylbenzene
ug/L
50
49.7
99
60-140
1,2-Dibromo-3-chloropropane
ug/L
50
48.5
97
60-140
1,2-Dibromoethane (EDB)
ug/L
50
53.1
106
60-140
1,2-Dichlorobenzene
ug/L
50
50.7
101
60-140
1,2-Dichloroethane
ug/L
50
50.3
101
60-140
1,2-Dichloropropane
ug/L
50
49.5
99
60-140
1,3,5-Trimethylbenzene
ug/L
50
52.1
104
60-140
Results presentetl on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM without the written consent of Pace Analytical Services, -LC. Page 20 of 34

aceAnalXical
www.pscelahs.com
QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
LABORATORY CONTROL SAMPLE:
Parameter
3834280
Units
Spike
Conc.
LCS
Result
LCS
%Rec
%Rec
Limits
1,3-Dichlorobenzene
ug/L
50
51.1
102
60-140
1,3-Dichloropropane
ug/L
50
50.7
101
60-140
1,4-Dichlorobenzene
ug/L
50
49.4
99
60-140
2,2-Dichloropropane
ug/L
50
53.8
108
60-140
2-Chlorotoluene
ug/L
50
48.1
96
60-140
4-Chlorotoluene
ug/L
50
48.1
96
60-140
Benzene
ug/L
50
47.8
96
60-140
Bromobenzene
ug/L
50
51.3
103
60-140
Bromochloromethane
ug/L
50
54.1
108
60-140
Bromodichloromethane
ug/L
50
51.8
104
60-140
Bromoform
ug/L
50
55.8
112
60-140
Bromomethane
ug/L
50
47.5
95
60-140
Carbon tetrachloride
ug/L
50
53.1
106
60-140
Chlorobenzene
ug/L
50
51.6
103
60-140
Chloroethane
ug/L
50
46.1
92
60-140
Chloroform
ug/L
50
50.8
102
60-140
Chloromethane
ug/L
50
58.1
116
60-140
cis-1,2-Dichloroethene
ug/L
50
52.0
104
60-140
cis-1,3-Dichloropropene
ug/L
50
52.3
105
60-140
Dibromochloromethane
ug/L
50
53.9
108
60-140
Dibromomethane
ug/L
50
50.2
100
60-140
Dichlorodifluoromelhane
ug/L
50
56.8
114
60-140
Diisopropyl ether
ug/L
50
51.7
103
60-140
Ethylbenzene
ug/L
50
50.4
101
60-140
Hexachloro-1,3-butadiene
ug/L
50
52.6
105
60-140
Isopropylbenzene (Cunene)
ug/L
50
50.7
101
60-140
n&p-Xylene
ug/L
100
102
102
60-140
Methyl-tert-butyl ether
ug/L
50
51.4
103
60-140
Methylene Chloride
ug/L
50
49.5
99
60-140
n-Butylbenzene
ug/L
50
52.1
104
60-140
n-Propylbenzene
ug/L
50
50.4
101
60-140
Naphthalene
ug/L
50
48.8
98
60-140
o-Xylene
ug/L
50
62.1
104
60-140
sec-Butylbenzene
ug/L
50
50.5
101
60-140
Styrene
ug/L
50
52.5
105
60-140
tert-Butylbenzene
ug/L
50
43.8
88
60-140
Tetrachloroethene
ug/L
50
53.0
106
60-140
Toluene
ug/L
50
49.6
99
60-140
trans-1,2-Dichloroethene
ug/L
50
53.2
106
60-140
trans-1,3-Dichloropropane
ug/L
50
51.6
103
60-140
Trichloroethene
ug/L
50
51.9
104
60-140
Trichlorofluoromelhane
ug/L
50
49.1
98
60-140
Vinyl chloride
ug/L
50
57.9
116
60-140
1,2-Dichloroethane-d4 (S)
%
99
70-130
4-Bromofluorobenzene (S)
%
102
70-130
Toluene-d8 (S)
%
98
70-130
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Qualifiers
Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the mull.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/282022 12:26 PM without the written consent of Pace Analytical Services, L-C. Page 21 of 34

aceAnalytical e
www.pecalebs.com
Pace Analytical services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3834648
MS
92634524004 Spike
Parameter Units Result Conc.
1, 1, 1,2-Tetrachloroethane
1, 1, 1 -Trich loroethane
1, 1,2,2-Tetrachloroethane
1,1,2-Trichloroethane
1,1-Dichloroethane
1,1-Dichloroethene
1,1-Dichloropropene
1,2,3-Tdchlorobenzene
1,2,3-Tichooropropane
1,2,4-Trichlorobenzene
1,2,4-Trimelhylbenzene
1,2-Dibromo-3-
chloropropane
1,2-Dibromoethane (EDB)
1,2-Dichlorobenzene
1,2-Dichloroethane
1,2-Dichloropropane
1,3,5-Trimethylbenzene
1,3-Dichlorobenzene
1,3-Dichloropropane
1,4-Dichlorobenzene
2,2-Dichloropropane
2-Chlorotoluene
4-Chlorotoluene
Benzene
Bromobenzene
Bromochloromethane
Bromodich loromethane
Bromoform
Bromomethane
Carbon tetrachloride
Chlorobenzene
Chloroethane
Chloroform
Chloromethane
cis-1, 2-Dichloroethene
cis-1, 3-Dich to rop rope ne
Dibromochloromethane
Dibromomethane
Dich lorodifl uoromethane
Diisopropyl ether
Ethylbenzene
Hexachloro-1, 3-butadiene
Isopropylbenzene
(Cumene)
nAp-Xylene
3834649
MSD
Spike MS MSD MS MSD %Rec
Conc. Result Result %Rec %Rec Limits
ug/L
ND
20
20
21.0
17.5
105
88
60-140
ug/L
ND
20
20
22.2
19.4
111
97
60-140
ug/L
ND
20
20
20.8
17.3
104
87
60-140
ug/L
ND
20
20
20.7
18.5
103
92
60-140
ug/L
ND
20
20
21.0
18.2
105
91
60-140
ug/L
ND
20
20
22.4
19.9
112
99
60-140
ug/L
ND
20
20
24.4
21.2
122
106
60-140
ug/L
ND
20
20
19.5
17.1
97
86
60-140
ug/L
ND
20
20
17.1
15.0
86
75
60-140
ug/L
ND
20
20
19.7
16.6
99
83
60-140
ug/L
ND
20
20
19.8
16.7
99
83
60-140
ug/L
ND
20
20
19.5
15.4
97
77
60-140
Max
RPD RPD Qual
18 30
13 30
19 30
11 30
14 30
12 30
14 30
13 30
13 30
17 30
17 30
24 30
ug/L
ND
20
20
21.1
18.0
106
90
60-140
16
30
ug/L
ND
20
20
19.6
17.1
98
86
60-140
13
30
ug/L
ND
20
20
20.7
18.1
104
91
60-140
13
30
ug/L
ND
20
20
20.2
17.4
101
87
60-140
15
30
ug/L
ND
20
20
21.2
18.0
106
90
60-140
16
30
ug/L
ND
20
20
20.1
17.2
100
86
60-140
16
30
ug/L
ND
20
20
20.2
16.7
101
83
60-140
19
30
ug/L
ND
20
20
19.1
16.7
95
84
60-140
13
30
ug/L
ND
20
20
22.4
18.8
112
94
60-140
18
30
ug/L
ND
20
20
20.5
17.4
103
87
60-140
16
30
ug/L
ND
20
20
20.5
17.4
103
87
60-140
16
30
ug/L
ND
20
20
20.2
17.4
101
87
60-140
15
30
ug/L
ND
20
20
19.9
16.8
100
84
60-140
17
30
ug/L
ND
20
20
21.8
18.9
109
95
60-140
14
30
ug/L
ND
20
20
21.3
18.5
107
92
60-140
14
30
ug/L
ND
20
20
21.3
16.9
107
85
60-140
23
30
ug/L
ND
20
20
22.2
20.5
111
103
60-140
8
30
ug/L
ND
20
20
22.6
19.7
113
98
60-140
14
30
ug/L
ND
20
20
20.8
17.2
104
86
60-140
19
30
ug/L
ND
20
20
24.8
22.2
124
111
60-140
11
30
ug/L
ND
20
20
21.4
18.0
107
90
60-140
18
30
ug/L
ND
20
20
23.7
21.2
119
106
60-140
11
30
ug/L
ND
20
20
21.7
19.0
109
95
60-140
14
30
ug/L
ND
20
20
21.4
18.1
107
90
60-140
17
30
ug/L
ND
20
20
20.6
17.7
103
88
60-140
15
30
ug/L
ND
20
20
21.0
17.6
105
88
60-140
18
30
ug/L
ND
20
20
22.0
19.7
110
98
60-140
11
30
ug/L
ND
20
20
19.9
16.6
99
83
60-140
18
30
ug/L
ND
20
20
20.6
17.7
103
89
60-140
15
30
ug/L
ND
20
20
22.4
19.0
112
95
60-140
16
30
ug/L
ND
20
20
20.6
17.5
103
88
60-140
16
30
ug/L
ND
40
40
41.1
35.0
103
88
60-140
16
30
Results presented on this page are In the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 11/28/2022 12:26 PM without the written consent of PaceAnaytical Services, L-C. Page 22 of 34

aceAnalytical
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QUALITY CONTROL DATA
Pace Analytical services, LLC
2226 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
MATRIX SPIKE & MATRIX SPIKE
DUPLICATE: 3834648
3834649
MS
MSD
92634524004
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Methyl-tert-butyl ether
ug/L
ND
20
20
20.0
17.0
100
85
60-140
17
30
Methylene Chloride
ug/L
ND
20
20
18.1
15.3
91
76
60-140
17
30
n-Butylbenzene
ug/L
ND
20
20
21.6
18.3
108
92
60-140
16
30
n-Propylbenzene
ug/L
ND
20
20
20.8
17.6
104
88
60-140
17
30
Naphthalene
ug/L
ND
20
20
19.7
16.3
98
82
60-140
19
30
o-Xylene
ug/L
ND
20
20
20.8
17.8
104
89
60-140
16
30
sec-Butylbenzene
ug/L
ND
20
20
21.1
17.8
106
89
60-140
17
30
Styrene
ug/L
ND
20
20
19.9
16.7
100
84
60-140
18
30
tert-Butylbenzene
ug/L
ND
20
20
18.6
15.8
93
79
60-140
17
30
Tetrachloroethene
ug/L
ND
20
20
21.0
17.5
105
88
60-140
18
30
Toluene
ug/L
ND
20
20
20.8
17.9
104
90
60-140
15
30
trans-1,2-Dichloroethene
ug/L
ND
20
20
22.3
19.7
111
98
60-140
12
30
trans-1,3-Dichloropropene
ug/L
ND
20
20
21.2
18.1
106
90
60-140
16
30
Trichloroethene
ug/L
ND
20
20
21.6
18.5
108
93
60-140
15
30
Trichlorofluoromelhane
ug/L
ND
20
20
22.3
19.6
111
98
60-140
13
30
Vinyl chloride
ug/L
ND
20
20
24.6
21.2
123
106
60-140
15
30
1,2-Dichloroethane-d4 (S)
%
99
105
70-130
4-Bromofluorobenzene (S)
%
102
102
70-130
Toluene-d8 (S)
%
101
101
70-130
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /28/2022 12:26 PM vAthout the written consent of Pace Analytical Services, -LC. Page 23 of 34

aceAnalyftal e
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QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 736446 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia
Laboratory: PaceAnalytical Services -Asheville
Associated Lab Samples: 92634703001, 92634703002, 92634703003
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3832778 Matrix: Water
Associated Lab Samples: 92634703001, 92634703002, 92634703003
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Ammonia mg/L ND 0.10 0.031 11/11/2213:26
LABORATORY CONTROL SAMPLE: 3832779
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 5.1 103 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832780 3832781
MS MSD
92634724001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Conc. Conc. Result Result %Rec %Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 0.21 5 5 5.7 5.7 110 110 90-110 0 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832782
3832783
MS
MSD
92636033001 Spike
Spike
MS MSD MS MSD
%Rec Max
Parameter Units Result Conc.
Conc.
Result Result %Rec %Rec
Limits RPD RPD Qual
Nitrogen, Ammonia rrg/L NO 5
5
5.4 5.4 106 107
90-110 1 10
Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/282022 12:26 PM without the written consent of PaceAnalytical Services, LLC.
Page 24 of 34

75ceAnalyfical'
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QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 736448 Analysis Method: EPA 350.1 Rev 2.0 1993
QC Batch Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia
Laboratory: PaceAnalytical Services -Asheville
Associated Lab Samples: 92634703004
METHOD BLANK: 3832788
Associated Lab Samples: 92634703004
Parameter
Nitrogen, Ammonia
Matra: Water
Blank Reporting
Units Result Limit
mg/L NO 0.10
LABORATORY CONTROL SAMPLE: 3832789
Spike LCS
Parameter Units Cone. Result
Nitrogen, Ammonia mg/L 5 5.3
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
MDL Analyzed Qualifiers
0.031 11/11/22 14:11
LCS %Rec
%Rec Limits Qualifiers
106 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832790 3832791
MS MSD
92634703004 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qua[
Nitrogen, Ammonia mg/L NO 5 5 5.4 5.4 109 108 90-110 1 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3832792 3832793
MS MSD
92635117001 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual
Nitrogen, Ammonia mg/L 0.40 5 5 5.8 5.8 109 109 90-110 0 10
Results presented on this page are in the units Indicated by the "units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM wihout the wntten consent of PaceAnalytical Services, LLC.
Page 25 of 34

aceAnalytical e
www.pacslaba.cam
QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 737616 Analysis Method: EPA 351.2 Rev 2.0 1993
QC Batch Method: EPA 351.2 Rev 2.01993 Analysis Description: 351.2 TKN
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3838884 Matrix: Water
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Neldahl, Total mg/L ND 0.50 0.25 11/17/22 05:52
LABORATORY CONTROL SAMPLE: 3838885
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Nitrogen, Kjeldahl, Total mg/L 10 9.5 95 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3838886 3838887
MS MSD
92635215002 Spike Spike MS MSD MS MSD %Rec Max
Parameter Units Result Cone. Cone. Result Result %Rec %Rec Limits RPD RPD Qual
Nitrogen, Kjeldahl, Total mg/L ND 10 10 9.2 9.1 89 88 90-110 1 10 Mi
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3838888
3838889
MS
MSD
92635215003 Spike
Spike
MS MSD
MS MSD %Rec Max
Parameter Units Result Cone.
Cone.
Result Result
%Rec %Rec Limits RPD RPD Qual
Nitrogen, Neldahl, Total mg/L 0.90 10
10
10.3 10.9
94 100 90-110 6 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM Without the written consent of Pace Analytical Services, LLC.
Page 26 of 34

1'�7
ceAnalytical
w".pacelabs.com
QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 734865 Analysis Method: EPA 353.2 Rev 2.0 1993
OC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634703001
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3824825
Nlatrb(: Water
Associated Lab Samples: 92634703001
Blank Reporting
Parameter
Units
Result Limit
MDL Analyzed Qualifiers
Nitrogen, Nitrate
mg/L
ND 0.040
0.010 11/04/2202:34
Nitrogen, Nitrite
mg/L
ND 0.040
0.031 11/04/2202:34
LABORATORY CONTROL SAMPLE: 3824826
Spike LCS LCS %Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 99 90-110
Nitrogen, Nitrite mg/L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824827
3824828
MS
MSD
92634699011
Spike
Spike
NIS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Nitrogen, Nitrate
mg/L
5.2
1.5
1.5
6.8
6.7
108
101
90-110
1
10
Nitrogen, Nitrite
nng1L
ND
1
1
1.0
1.0
103
102
90-110
1
10
MATRIX SPIKE & MATRIX
SPIKE DUPLICATE: 3824829
3824830
MS
MSD
92634699014
Spike
Spike
MS
MSD
MS
MSD
%Rec
Max
Parameter
Units
Result
Conc.
Conc.
Result
Result
%Rec
%Rec
Limits
RPD
RPD Qual
Nitrogen, Nitrate
mg/L
1.2
1.5
1.5
2.7
2.7
99
98
90-110
0
10
Nitrogen, Nitrite
mg/L
ND
1
1
1.0
1.0
102
101
90-110
0
10
Results presented on this page are In the units indicated by the "Units' column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 27 of 34

(�157ceAnalyfica(
www.pacalebs.caln
QUALITY CONTROL DATA
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 734866 Analysis Method: EPA 353.2 Rev 2.0 1993
QC Batch Method: EPA 353.2 Rev 2.01993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres.
Laboratory: Pace Analytical Services - Asheville
Associated Lab Samples: 92634703002, 92634703003, 92634703004
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
METHOD BLANK: 3824831 Matrbc: Water
Associated Lab Samples: 92634703002, 92634703003, 92634703004
Blank Reporting
Parameter Units Result Limit MDL Analyzed Qualifiers
Nitrogen, Nitrate mg/L ND 0.040 0.010 11/04/2203:41
Nitrogen, Nitrite rig/L ND 0.040 0.031 11/04/2203:41
LABORATORY CONTROL SAMPLE: 3824832
Spike LCS LCS %Rec
Parameter Units Cone. Result %Rec Limits Qualifiers
Nitrogen, Nitrate mg/L 1.5 1.5 99 90-110
Nitrogen, Nitrite mg/L 1 1.0 100 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824833
3824834
MS
MSD
92634703003
Spike
Spike
MS
MSD
MS MSD %Rec
Max
Parameter
Units
Result
Cone.
Cone.
Result
Result
%Rec %Rec Limits
RPD RPD Qual
Nitrogen, Nitrate
mg/L
10.0
1.5
1.5
11.4
11.5
94 97 90-110
0 10
Nitrogen, Nitrite
r1g/L
NO
1
1
1.0
1.0
100 102 90-110
1 10
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 34

aceAnalytical
www.yecelels.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
QC Batch: 734868
Analysis Method: SM 4500-P E-2011
QC Batch Method: SM 4500-P E-2011
Analysis Description: SM450OP-E Phosphorus, Ortho
Laboratory: Pace Analytical Services -Asheville
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
METHOD BLANK: 3824835
Matra: Water
Associated Lab Samples: 92634703001, 92634703002, 92634703003, 92634703004
Blank Reporting
Parameter Units
Result Limit MDL Analyzed Qualifiers
Orthophosphate as P rrg/L
ND 0.050 0.012 11/04/22 04:27
LABORATORY CONTROL SAMPLE &LCSD: 3824836 3824837
Spike LCS LCSD LCS LCSD %Rec Max
Parameter Units
Conc. Result Result %Rec %Rec Limits RPD RPO
Qualifiers
Orthophosphate as P rrg/L
0.25 0.25 0.26 100 102 90-110 2 10
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824836 3824839
MS MSD
92634534006
Spike Spike MS MSD MS MSD %Rec
Max
Parameter Units Result
Conic. Conic. Result Result %Rec %Rec Limits RPD
RPD Qual
Orthophosphate as P i g/L NO
0.25 0.25 0.27 0.24 93 79 90-110 14
10 M1,R1
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11 /28/2022 12:26 PM without the written consent of PaceAnaytical Services, I.I.C.
Page 29 of 34

Pace Analytical Services, LLC
(15'cemalytical' 2225 Riverside Dr.
Asheville, NC 28804
www.pecelebsxom [phone]
QUALIFIERS
Project: Monitoring Wells November 2022
Pace Project No.: 92634703
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis ofAcrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
'Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI -The NELAC Institute.
ANALYTE QUALIFIERS
B Analyte was detected in the associated method blank.
CH The continuing calibration for this compound is outside of PaceAnalytical acceptance limits. The results may be biased
high.
E Analyte concentration exceeded the calibration range. The reported result is estimated.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
R1 RPD value was outside control limits.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/28/2022 12:26 PM without the written consent of Pace Analytical services, LLC. Page 30 of 34

aceAnalytical
www.psceleb.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Project:
Pace Project No.:
Monitoring Wells November 2022
92634703
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical
Method
Batch
92634703001
MW-1R
92634703002
MW-2
92634703003
MW-3
92634703004
MW41
92634703001
MWAR
EPA 200.8 Rev 5.4
736695
EPA 200.8
Rev 5.4
736721
92634703002
MW-2
EPA 200.8 Rev 5.4
736695
EPA 200.8
Rev 5.4
736721
92634703003
MW-3
EPA 200.8 Rev 5.4
736695
EPA 200.8
Rev 5.4
736721
92634703004
MW-4
EPA 200.8 Rev 5.4
736695
EPA 200.8
Rev 5.4
736721
92634703001
MWAR
SM 6200B
736729
92634703002
MW-2
SM 6200E
736729
92634703003
MW-3
SM 6200B
736729
92634703004
MAi
SM 6200B
736729
92634703001
MWAR
EPA 350.1 Rev 2.01993
736446
92634703002
MW-2
EPA 350.1 Rev 2.0 1993
736446
92634703003
MW-3
EPA 350.1 Rev 2.01993
736446
92634703004
MW4
EPA 350.1 Rev 2.01993
736448
92634703001
MW-1 R
EPA 351.2 Rev 2.0 1993
737616
EPA 351.2
Rev 2.0 1993
737659
92634703002
MW-2
EPA 351.2 Rev 2.0 1993
737616
EPA 351.2
Rev 2.0 1993
737659
92634703003
111
EPA 351.2 Rev 2.0 1993
737616
EPA 351.2
Rev 2.0 1993
737659
92634703004
MW-4
EPA 351.2 Rev 2.0 1993
737616
EPA 351.2
Rev 2.0 1993
737659
92634703001
MWAR
EPA 353.2 Rev 2.01993
734865
92634703002
MW-2
EPA 353.2 Rev 2.01993
734866
92634703003
MW-3
EPA 353.2 Rev 2.0 1993
734866
92634703004
MW-4
EPA 353.2 Rev 2.0 1993
734866
92634703001
MW-1 R
SM 4500-P E-2011
734868
92634703002
MW-2
SM 4500-P E-2011
734868
92634703003
MW-3
SM 4500-P E-2011
734868
92634703004
MW-4
SM 4500-P E-2011
734868
Date: 11/28/2022 12:26 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 31 of 34

ce*
DC# Title: ENV-FRM-HUNI.0083 v01 Sample Condition Upon Receipt
SWII2 MIMS
Effective Date: 05112/202205/12/2022
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ]6 Raleigh❑ Mechanicsville[] Atlanta❑ Kernersville❑
Client Name: Project # O# : 92634703
■
Courier: ❑f Ex I❑U S U�❑USPS ❑Cllent II'.II' I "I (III I I'II
❑ Commercial Pace ❑Other:_
Custody Seal Present? ❑Yes ❑N6 Sealslntact?
Packing Material: []Bubble Wrap Bubble Bags
82634703
Des ffrNo
Date/Initials Person Examining Contents: )
[]None ❑ Other
Thermometry IR Gun un
to: Type of Ice: QWet
Correction Factor:
Cooler Temp: r � Add/Subtractc�(C)
Cooler Temp Corrected ('C): Si t
USDA Regulated Soil (CTN/A, water sample)
Did samples originate in a quarantine zone within the United States: CA, NY, or SC
❑Blue ❑None
Biological Tissue Fro ?
❑Yes ❑No N/A
Temp should be above freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
hasbegun
Did samples originate from a foreign source (internationally,
(check maps)? []Yes []No
Including Hawaii and Puerto Rico)? ❑Yes ❑No
Comments/Discrepancy:
Chain of Custody Present?
Yes
ONO
❑N/A
1.
Samples Arrived within Hold Time?
B<s
ONO
QN A
2.
Short Hold Time Analysis (<72 hr.)?
Yes
ON.
❑N/A
3.
Rush Turn Around Time Requested?
❑Yes
ZN.
UNIA
4.
Sufficient Volume?
2Keses
ONO
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
oGs
es
[:]No
ON.
❑N/A
❑N/A
6.
Containers intact?
es
ONO
❑N/A
7.
Dissolved analysis: Samples Field Filtered?
as
ONO
/A
8.
Sample Labels Match COC?
-Includes Date/Time/ID/Analysis Matrix:
es ONO
(", fJ
❑N/A
9.
Headspace in VOA Vials (>S-6mm)?
QYes
)JUL
❑N/A
10.
Trip Blank Present?
Trip Blank Custody Seats Present?
❑Yes
Oyes
E3No
ONO
❑N/A
/A
11.
COMMENTS/SAMPLE DISCREPANCY
Lot ID of split containers:
CLIENT NOTIFICATION/RESOLUTION
Person contacted:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time:
Field Data Required? ❑Yes ❑NO
Date: I
Date: It / t�
Page 32 of 34
Qualtrax ID: 69614 Page 1 of 2

ace, nLLa
DC#_Title: ENV-FRM-HUN1-0083 v01_Sample Condition Upon Receipt
Effective Date: 051121202205/12/2022
*Check mark top half of box if pH and/or dechlorination is verified and
within the acceptance range for preservation samples,
Exceptions: VOA, Coliform, TOC, Oil and Grease, DRO/8015 (water) DOC, LLHg
**Bottom half of box Is to list number of bottles
***Check all unpreserved Nitrates for chlorine
Projects : 92.634703 ---
M: L1P Due Date: 11/17/22
CLIENT: 83-MARION
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
Amount of Preservative
added
tot It
Now. whenever mere is a discrepancy affecting North Carolina compliance samples, a copy of this form will be sent to the North Carolina DENR Certification Office (Le,
Out of hold, Incorrect preservative, out of temp, incorrect containers.
Page 33 of 34
Qualtrax ID: 69614 Page 2 of 2

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iheuntenl Name: Field datn Rhect
Date Issued: March 6, 2019 '
'
Page: 1 efl
.: 8Cf7Awlylical
Mmunent Number, P•CAR•tl.D•001•rev.03
f0ldlla Alilhodly; Pace Hnntersville Qllnitty
Office
Field Data Sheet
NonleandAffillation(Sampler(s); RA6 Paco
Name and Affiliation (inspector):. N /4
Well Information
Well ID: _ &%--I2
Well Diameter: 1l
Well Locked:
SA Nov.7422
Id Data Sheet Review:
Date: II I o' Wn By: Wa
Constructlon; (PrDReel/Stainless Steel)
Total Well Depth:-�a,_O2_ft MultiFdCtor*:0-10 (!(Radhts/12)2x3.l4x7d61
Static Water Level: 14.46 ft Casing Volume:_gallons
Height of Water Colunm>iN jj_ft Cal. 3 Volumes: (:f•% 1 gallons
PunlpIntake:_ N 60
Pure Information go
DatePurged:__il. _/_ __/Start:. oa4S:Pinish: Purge Rate: ieu.+r5/A:A
A9 1111r: Z
Purging Method: 4 6 e, r'[ PAt Total Volume Purged: _ I ti 2.00.___p (gallons nibs )
Sampling Information
DateCollocted: I(—/2-/_7Z Time Collected: 11 am pill)
SanlplingEquipment Used: f4&e,&+F l4r'L Pik —IT InstrumentlD:llioSbg/7Pv6e64
Bottle Type
aria„rrrci�rr.�-mm�
Preservation
Analysis Required
_M +e.15, T4;iI Aeny«lam,
error r.l..a fTDS, T45
VO Q2,,ot _- f►w4 iheke
Sample'remp (aC): I'inie: 00 'turbidity (ntu): V-1 Time: I 1 S o
DissOxy(mg/L): 5• L ']line: Pe2+mg/L: Thne:
Specific Cond. (us): ZH Time: Res. CI (rng/L)/(Itg/L): Time:__'
Sample pH (s.u.):.�_..�.. 41— Thne:.__.._ —Odor: 1{ 0KP Thee: b (so
ReDox (mV): Thne: Appearance:w--LI4-e r.r+r[4f>� 'rhne:_
ReDox (PH value):YSI PfoPlus+200niV � Other: 'rime: `--
Temp.__6__�_(°F) WindQ- ')_(mph)
Sampler Signature:_ailan__QY"S _._.Date:_ If/
Stabilization Teat
Tinge
Purged
Teenip.
(C)
DissOxy.
(nlg/1.)
Spec
Cond.
( ub)
pH(s.u.)
ReDox
(n1V)
Turbidity
(ntu)
Volume
removed
(gallons ells
L
Water'
level (ft)
Other
og50
11,0
T*L
27.(
5'.7
1%4.7
400
Du
17.p
7,2
71 1
5.7
74, 7
400
2 ,62
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Ihxum eal Name
Field Data Sheet
Document Issued: March 8, 2019
PagAof 2_
aceAtwl3ftaI•
Ducunent Number:
F.CAR-FI.D-00l.rev.03
Issueing Authority:
Pace Huntersvilte Quality Office
client: L •4y of
Location: /nar;04 1N
Project: L •{y of mar;oA Md iA N40v.lo2Z
Well ID: irlw-( 2
Reviewed Date and By: I t- N- d I M Eo—'
Stabilization Test lllt"AlA TO-
1VeH Diameter
Multiplication Factor'
1
0.0409
1.2
0.0918
1.625
0.1030
2
0.1630
3
0.3670
4
0.6530
6
1.4680
3
2.6100
Time
Pufged
Temp.
OlssOxy.
(mg/L)
Spec.
Cond.
PH (s.u.)
ReDox (mV)
Turbidity
(ntu)
Volume Removed
(gallonsIs/)
elie oC
Water level
(ft)
Other
1025
1att,2
5.7
27.2
6.0
NH.Z
3Z0az�
2ar6
13,0Au/n;
1035
la,
,0
Zb.g
4.0
61,2
y o0
-Lfs.7
loks
I IA.
11.0
2 .3
(1.0
57.7
6•t0,0
2
Io5i
5.
2b.
--V&J4
9700
2S 97
110
IM.
5.y
2S,b
S,
200
28.
111
25
Z2.(
3-4,8
1 200
2 ,95
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Dale J.%wcd: March a, 2019
Dwinwnt Nnare: PIMd dala Sheet Page: l of
ACClU7,7ly((c!7/• Issuing Aulborlly:Paco Hantelrville:Qimllty
rkx•ulneni Numher:P-CAH-IO.D-Wt•rev,03 Office
ueiu vaul J
Client: 4i _3 o f o r%a/1_._Locatien;._Me�%oyfit{�-__Pro'ect
N; c'tv oL MH a 1MtM
Review:
Name Affiliatlon (Sanipler(s): A"O eG-i-e;YES
:Dataheet
and -4-J.a t++t;A
Name and Affiliation (Ins;�ector):,�£ / IOvi �a By: �
Well Information
Well ID: fjMw Z
Well Locked:q / FiushmomttWell
Diameter: 1 I
Construction:l/Stainless Steel)
Total Well Depth;
Multi Fector`: 0,10 (r(Rauus/l2)2x 1.14x Zdel
Static Water Level:—IR % _ft
Casing Volmne: 3 •oN gallons
Height of Water Column:_t a . ft
Cal. 3 Volumes: gallons
Pump Intake; / 3 b ft
Purge Information
Date Purged: --jt—/--3—./ z7=Stsrt:—a4Q
Finish-, (HS Purge Rate:_toonN/A,n
PurgingMethod:_?A.-; - If 'L
P�1+—Total Volume Purged: SaO __-.e(gallons inns L)
S nul(t g_Ittfornlatiou
Date Collected: 11 / 3 / Z
Time Collected: 1500 (am nt)
Sampling Equipment Used:Per'I4>i
,'e fl&Af _InstrumentiD; YSIeSba/TPwboail_
Bottle Type
Preservation Analysis Required
meiwa4 Tot+ A, pAei4l ,.
._. fmftol.lol.iTbi T§54
_
Field Measurements/Observations
Sample Temp (°C); f �' S ']'line: 1509
Turbidity (nut): 3 •`a _ Thule:-
1500 _
Diss Oxy (mg/L): 0' (' I'hne:
Pet+nig/L: Tune:
Specific Cond. (uS): .—Time:—
Res. CI(ing/L)/(pg/L): = Time:,
",.�._..
Sample pH (s.u.): _.... 6- _y--Time: •------.—Odor:-__�
h rsL�✓ �Thne:
1500
ReDox (mV): "'' Tilne:
Appeorance: � td. e _'flute:
ReDox (PH value):YSI ProPius+2ooniV
Other: � _� _ Time:-
Ceneral/Weather Observations
(sunny •loudy/rainy) wind 4-5 (
SaniplerS)gnature; Oya-A By sS
Date: (1 /3 /2L --
sA Nov.xo�z
J[a V+++La++W
I 1 GS
o ume
'finite
Tenlp.
Diss t7xy.
Spec,
Cond.
PH (s.u.)
ReDox
Turbidity
remove
Water
Other
Purged
(°C)
(ntg/L)
(us)
(IIIV)
(nul)
(gallons/ nls
level (ft)
t q5
i ,l
o, 9
rig ,
b.4
— -
b• N
Soo
ita+r
btkp
V
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Documeat Name: Field Onto Sheet
bete Issued: Maxis a, 2019
Pop: I of Z
7CC/6lafyflfiil'
Pmaraeat Number: 11-CAR-FID-001•rev.03
Issuing Aldhodty:i-ace Hunletrville Qnnlily
Office
jMr, IWEI�71L'3qt
Name and Affiliation (Sampler(a): Rr^ 8 PA gyp,
Name and Affiliation (Inspector); N / A
Well Information
We]I ID:
Well Diameter: -x n
Total Well Depth; S O Q Z._ft
Static Water Level:_3M.1'b ft
Height of Water C01un1n:- I M LA._ft
Well Locked:
Construction:
,nw sA Not.,2oi�
Itield Data Sheet Review:
II -N, Al ME2
Dater I I l oL l Y, By:
Steel)
MultiPacto'`:—�Io bj�_I•(Rnrpus/12)2x3.1ax7.48)
Casing Volume: 2 S a _ gallons
CaOVolumes: Volumes: -7' 7 5 gallons
Pump Intake, ' 4 4�' R
PuMe Information
Date Purged: ._/ ...—/-� _Start:_-L7.4�_Nlnlsll:. tgo5 PurgeRntc: i0otnif/mot 1
Purging Method: Pao s MOA Sot) /t___Total Volume Purged: _.._.. (gallons/ i s L)
So moltne.htformation
Date Collected: If /3J Z 2 'rinto Colleeted:Lva2 — (all lltt
Sampling Equipment Used:-t%Pj rb_.^onSeon Instrument ID: y %Dgol /riw (-g' j
Bottle Type
Preservation
Analysis Required
�•.eta1� I Tot 2 AmmoA'o-
I K N, N '+ra+e r N-
PA/Aol T011
v,qLjLotsrj or+ko-PkospAs+n
Held Measurgramtt✓Observatlone
Sample Temp (°C):
( -1, 1 I'inte:_ 11T1Q
Turbidity (ntu); .. 9 ,
Time: I t(IJ
Diss Oxy (mg/L):
'Time: _
Fe 2+ mg/L:
Time: �-
Speciflc Cond. (uS):
1`4 1, 9JTints:
Res.
Sample pH (s.u.): _
5 Tlnte: _
P
Th»e: tt( i'O
ReDox (mV):
�" Thne: —
Appearance: a1���
Time:- �-
ReDox(RHvolue):YSIProPlus+200raV
Other: --
Time: -
General/Weather
SamplerSiguature;_I� Lund__ DatO:__ J---
StabilizaUon'1'ee1
Temp.
Diss
Spec.
Cond.
pH (s.u.)
ReDox
Turbidityremoved
(ntu)
o tune
allons nl
(8
Water
level ft
( )
Other
PurTimged
Purged
(°C)
/l,)Oxy
(mg/I,)
(us)
(mV)
L�
Ib
'i
1 I
4•
--
50 �
3N S
175.3
I o
3116
1
I
3.5
To
.�
14?
ZSoU
l I
17.o
3,A
10-51
b6,S
1 450

r Docuurent Name:
Document Issued: March 8, 2019
Field Data Sheet
Pnge2 of i
aCeAnalytical
Document Numlrer;
Issueing Authority:
F-CAR-FLD-001.rev.(U
Pace Huntersville Quality Office
Client: 44-r of Me+pan
Location: M.;-n, N If
Project: C'ir of r,a :%r, My S A Nov. 1-o1,2.
Well ID:
Reviewed Date and By: \ \ - I - I)- M t /t.
StabllilationTest 1 \\ C"1\l'4- TV
fVell Diameter
Multiplication Factor'
1
0.0408
1.2
0.0918
1.625
0.1080
2
0.1630
3
0.3670
4
0.6530
6
1.4680
8
2.6100
IIIIMM
, TurIIdII,

Document Name: 1810d data Shell
Date Issued: March 6, 2019
.. zcahl91yibll
r
Pa e: I of
rkkument Number. M1CAR-PI.D-001-rev.0
IIasuhsg Aulhorlly: Pace fluniersviile Quallly
O((Ice
Field Data Sheet
Name and Affiliation (Sampler(s): RmO P0.1e
Name and Affiliation (inspector): N /A
Well Information
Well ID: MW' N
Well Diameter: 2 1 n
Total Well Depth: 1517 it
Static Water Level: V •01 ft
Height of Water Column: 14.3 L\ ft
Well Locked:
Construction:
Mv154 Now.2022
Field Dnta Sheet Review:
I I -4
Date: 11I oBy: 4-,p
�1(Ya
MUlt,Fnctor''t 4�-('(Radh,s/12)20.tgx2.a91
Casing Volume: Z Aa gallons
Ca1,3Volumes: gallons
Pump Intake: i" 71 --it
Purge Information
Date Purged: 11 Start: ISZS Finish: ISNo Purge Rate: l00M(5/Alt)
Purging Method: I'm o% P Total Volume Purged: 1500 (gallons/( 5Ti.)
e 1�.�`JJ
Sampling Information
Date Collected:_11 / 3 / Z Time Collected:_ I S (a /pm)
Sampling Equipment Used:_�r•,'4i-1+,'1 fk^f! InstrumentiD:_ v4� T w(x g�l
Bottle Type
Field M asurements/Observations
Preservation
Analysis Required
---M at.tir To�.�AMr�p.
IKft� N:+rwtlru+r•Nf
_ekia oh TO- l/-rK$ Thr-W_
b09� pr-t e5 Photo
SampleTemp(aC):--_�S•
"Time:-15Ni_
Turbidity (ntu): 0.8
Time:
1545.
Diss Oxy (mg/4n
• I
Time:
Pe 2+ mg/L: `�
Time:
Specific Cond. (uS):
Tine:
_Res. Cl(mg/LY(1tg/L): ,'rinte:
"—
SamplepH(s,u.):_._g._...Tlme:._._Odor:_--p1A^QTime:
_I54S _
ReDox (mV):
---
Time:
--- Appearance: GI e `r
Time:
!
Rebox (EH value):YSI ProPlus +200mV�—Other:
Time:
`--
(sunny/ oudy/rainy) Temp. _20_("F) Wind a-'
Sam ler Si nalure_R-Yr. --- . 3/ 2 Z
---- — -
Stabilization Test
Time
Temp.
Diss Oxy.
Spec
Cond.
pH (s.u.)
ReDox
Turbidity
Volume
remov
Water
Other ,
Purged
(C)
(nlg/l,)
(t 3)
(mV)
(ntu)
(gallons ills
level (ft)
t
L
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1
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0. 9
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SOO
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1500

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Page 34 of 34