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HomeMy WebLinkAboutWQ0005910_Monitoring - 07-2022_20220824 (2)GW-59A COMPLIANCE REPORT FORM Permit #_W Q Qd0911 O (Submit one each monitoring period with GW-59 forms.) 1 Enter date monitoring results were due. 1 Will this monitoring report (GIN-59 and GW-59A) YES NO be submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES" list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. / 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO/ Identification plate, area overgrown, etc.)" 1j the answer is •'Fes", contact the Regional Office for guidance. `// 4 Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: "TVs Avwaw,o..:wtrA 9(0 S: 5.40 a►w �� = -ti0 %J S RO 5 For the constituents identified In question 4 abovq, have standards been exceeded previously for the YES NO same constituent(s) in the same well(s) in the last two years? If the answer to question'5 is NO", skip to section B. If the answer to question 5 is "YES", list in the space provided below, each welt with constituents) exceeding ' standards, concentration(s) reported, and sample toll ction date for each occurrence (for the last two years). MW %% ANwr.oww W it '(Os MvJ S 'CO S 31301 410 ' 313o11�-It.$ 3�x4�?1-9.4� 3thrl 1 Sip h0 $I.0 ��iwllt - 9.9V 1�lal�o= 11.$ Z1z31zo-SSI '�li�ts��'Lotb -tlw124 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer Is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE iMMEDIATELYFOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. 7 Is -the permittee implementing previously approved actions required by the Division involving this YES NO groundwater quality problem? If the answer to question 7 is "YES", describe those actions in the space provided below. If the answer to question 7 is 'NO", contact the Regional Office within 90 days; an evaluation may be disposal system Is having at the review and compliance required to determine the impact the waste boundaries surrounding this facility Failure to do so may subject the permittee to a Notice of Violation. fines and/or penalties. C �J ! i C3 AUG 2 9 2022 e t-2 N S The person completing this portion (GW-59A) *the merit®r_ report should sign below and submit this form with GW-59 forms for required wells to the`tddress proylted at the tap of the current GW-59 form- , cs� ..rnw>r' 'rT. ...,...�,�:... .......:.�asw,...,,,,Y.,-...::•,:,;n-...,, ":..-.�A .rwnr.wu.,.;.. .R.,�:-.-,.M:�,,Su • • r I herbb'y,acknowledge.that;the agoye Infofmatlo►��eva ev (uated and the Infocmatipn bm ed n report,(Compltajic y'ort,-59Aa,.ls true and,complete io;the best of my')Cnowlac�ge�?�,,;,b Signature of Pe e ( A horized Agent) Date SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name:�Crl LLC. Permit Name (if different): Facility Address: 1F v CVv "Z1 I (street) NL 2745i eNT` (City) (Stale) (Zip) County Contact Person: Telephone Well Location/ Site Name: No. of Wells to be Sampled: (Ir6 Well Identification Number (from Permit): VNII.A3 - S For Groundwater Treatment Systems Well Depth: 21-'l ft. Well Diameter: 2. in. Check one: ❑ Influent (98) Screened Interval: t5 ft. to 22- ft. ❑ Effluent (99) Depth to Water Level: LO-S_ft. below measuring point. Measuring Point (M.P.) is: 2- ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: S Date sample collected: ^1-20-22 Field analysis: pH LA-ck'l , Specific Conductance uMhos Temp. 24-S °C, Odor 0rG Appearance DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. INC 27699-1636 Phone: (919) 733-32: PERMIT #: , EXPIRATION DATE: 1O 31 2 y Non -Discharge W Q 00o54 k O UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field Rotary Distributor Other: Remediation: Infiltration Gallery Remedialion: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: Laboratory Name: E�nv►YCLV1yr�¢K1� Certification No. PARAMETERS (Samples for metals were collected unfiltered ✓ YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N OL4 mg/I Coliform: MF Total /100ml Phosphorus: Total as P_ 0.09 ma/I (Note: Use MPN method for highly turbld�samples) Dissolved Solids: Total �5 mg/I pH (when analyzed units TOC 3 • mg/I Chloride mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 0• 09 mg/I TKN as N mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 32.'12 ► mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) In t ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes �/ (1) No (0) VOC : method # = method # = method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name:Awl3ce, LLC- Permit Name (if different): Facility Address:-9)y I Avoca Favw, Rowel tvv (Slreel) NCr 7_ 145-7 Tily) (Stale) (zip) Contact Person: Well Location/ Site Name: County Telephone No_ of Wells to be Sampled: Well Identification Number (from Permit): C'r1J11�� Well Depth: \ q) ft. Well Diameter: 2. Screened Interval: 3 ft. to V 1b ft. Depth to Water Level: � b ft. below measuring point Measuring Point (M.P.) is: 26 ft. above land surface. Gallons of water pumped/bailed before sampling: 5 Field analysis: pH�— , Specific Conductance Temp. 'IS- 3 °C, Odor N 0-f- For Groundwater Treatment Systems in. Check One: ❑ Influent (98) ❑ Effluent (99) Relative M.P. Elevation in ft.: Date sample collected: uMhos Appearance C1 f-ew PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid sa pies) 25� Dissolved Solids: Total mg/I pH (when analyzed units TOC - 0(o mg/I Chloride 32. mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 4 O.Oy mg/I TKN as N mg/I DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT#: • EXPIRATION DATE: tul Non -Discharge W Q 000591 Q UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: -l- A�,-�t� --!j Qb -3-12 Laboratory Name: Er►v 0YOr►wne^A Certification No. V0 ✓ YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N 0 • y-1 mg/I sphorus: Total as P 4.0.04 mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium L4.S 35 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I method # = method # = YES NO) y Ni - Nickel mg/I Pb - Lean mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Di ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. t4tach lab report.) Report Attached? Yes ✓ (1) No (0) VOID : method # = ! 1 9V <. S; A CYIt print or type SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name:Awjocu L.LC. Permit Name (if different): Facility Address: , V v O C.V V F 1, (Street) N �.. Z� 15-7 (City) I(Stale) (zip) County Contact Person: Telephone #: 2S2r4�2-� 133 Well Location/ Site Name: No. of Wells to be Sampled: Well Identification Number (from Permit): tAW- Well Depth: 00 ft. Well Diameter: 2 Screened Interval: 3 ft. to I % ft. Depth to Water Level: 11-1 ft. below measuring point Measuring Point (M.P.) is: Z• ft. above land surface. Gallons of water pumped/bailed before sampling: S Field analysis: pH `• 31 , Specific Conductance Temp. 2-1•a °C, Odor nt, For Groundwater Treatment Systems in. Check One: ❑ Influent (98) El Effluent (99) Relative M.P. Elevation in ft.: Date sample collected:l-'A0-'2'A Appearance PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) Slo 0 Dissolved Solids: Total mg/I pH (when analyzed units TOC 11 • mg/I Chloride 2.1 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 0.(03 mg/I TKN as N mg/I _uMhos C1 c &xv DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phone: (919) 733-32: PERMIT#: EXPIRATION DATE: %O 3: 2 4 Non -Discharge W Q 000154 i 0 UIC 01991:`l TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Spray Field Rotary Distributor Other: Remediation: Infiltration Gallery Remediation: Land Application of Sludge NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: "1-;M 2-A --1 b-3- 2 X Laboratory Name: E.tr'►v ocOy%MC ni Certification No. V) YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N •y mg/1 sphorus: Total as P 1.(o4 mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 34.12S mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I ✓ YES NO) Ni - Nickel mg/I Pb - Lean mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Di ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓ (1) No (0) VOC : method # = method # = : method # = SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: P,rnCu LLC Permit Name (if different): Facility Address: RIJOCCL Faun, V,,�dacl tvv "I11 (Sireel) M(_ 219S7 (Cily) (stale) (zip) Contact Person: Well Location/ Site Name: County 1Sew+%e. _ Telephone #: No. of Wells to be Sampled: Well Identification Number (from Permit): MU- I Well Depth: 2•1-$ ft. Well Di meter: 2. Screened Interval: 10 ft. to 2 ft. Depth to Water Level: 1L1•�J ft. below measuring point. Measuring Point (M.P.) is: ? ft. above land surface. Gallons of water pumped/bailed before sampling: Field analysis: pH (0-,, Specific Conductance Temp. SLi- 3 °C, Odor nt- For Groundwater Treatment Systems in. Check One: ❑ Influent (98) ❑ Effluent (99) DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER RALEIGH. NC 27699-1636 Phone: (9191 733-32. PERMIT #: • EXPIRATION DATE: 10 31 1202q Non -Discharge W Q 000591 Q UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Relative M.P. Elevation in ft.: Date sample collected: "1'10-2� Date sample analyzed: uMhos Laboratory Name: Er►v►1�!]tr►v►r,¢r► Appearance Char Certification No. PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 300 mg/I pH (when analyzed) units TOC (• 9 mg/I Chloride �"1 mg/I Arsenic mg/I Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 4 O •O l,i mg/I TKN as N mg/I method # = method # = If YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N O.SO mg/I sphorus: Total as P O • o `t mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium 4q• S11 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lean mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) nl ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓ (1) No (0) VOC : method # = a - ,, pVcs;dant - Please print or type SUBMIT FORM ON YELLOW PAPER ONLY method # = method # = GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: Pwncu LLC. Permit Name (if different): Facility Ad`dr1ess:Ck , 1F V pc 1 CVV M• I I (SVeel) NL Z,7 7-7 1 Qi� I • Q. (city) (Stale) (Zip) County Contact Person: Telephone Well Location/ Site Name: No. of Wells to be Sampled: _ Well Identification Number (from Permit): (*%4— tD For Groundwater Treatment Systems Well Depth: ZO ft. Well Diameter: 2 in. Check One: ❑ Influent (98) Screened Interval: 3 ft. to ZD ft. ❑ Effluent (99) Depth to Water Level: VPL-_ft. below measuring point. Measuring Point (M.P.) is: Z ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _. Date sample collected: Field analysis: pH � , Specific Conductance uMhos Temp. °C, Odor IVO-C. Appearance CttKf DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER QUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE: 10 31 12 4 Non -Discharge w Q 0005910 UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remedialion: Infiltration Gallery \07—Spray Field Remedialion: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed: 7-11-'17.--% %-I-22 Laboratory Name: �Y ^Ex) ny%yy%s ►i Certification No. V0 PARAMETERS (Samples for metals were collected unfiltered ✓ YES NO and field acidified COD mg/I Nitrite (NO2) as N mg/I Coliform: MF Fecal /100ml Nitrate (NO3) as N L4. mg/I Coliform: MF Total /100ml Phosphorus: Total as P 40. 0`4 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Dissolved Solids: Total LA 10 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC 1.41 mg/I Ca - Calcium 23.3 %o mg/I Chloride 93 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I Phenol mg/I Fe - Iron mg/I Sulfate mg/I Hg - Mercury mg/I Specific Conductance uMhos K - Potassium mg/I Total Ammonia 0.0S mg/I Mg - Magnesium mg/I TKN as N mg/I Mn - Manganese mg/I YES NO) Ni - Nickel mg/I Pb - Lead mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Di ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes,/_(1) No (0) VOC : method # = L — 1 PvrtS%af'y* Please print or type SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: COMPLIANCE REPORT FORM FACILITY INFORMATION Please Print Clearly or Type Facility Name: -QCf., LLC Permit Name (if different): Facility Address: Avoca Favhn Rowel Cvv %.A,% t 1 (Slfeel) NL 2195-7 (City) , (Stale) (Zip) Contact Person: Well Location/ Site Name: County e- _ Telephone #: 2S7_-y82_-A No. of Wells to be Sampled: Well Identification Number (from Permit): (*4W- 1 V For Groundwater Treatment Systems Well Depth: Z.0 ft. Well Diameter: Z in. Check One: ❑ Influent (98) Screened Interval: ft. to 20 ft. ❑ Effluent (99) Depth to Water Level: _ IS-1ft. below measuring point. Measuring Point (M.P.) is: I ft. above land surface. Relative M.P. Elevation in ft.: Gallons of water pumped/bailed before sampling: _5 Date sample collected: Field analysis: pH -l� , Specific Conductance Temp. 'X4- 1 °C, Odor Al 0•. Appearance . PARAMETERS (Samples for metals were collected unfiltered COD mg/I Nitri Coliform: MF Fecal /100ml Nitr Coliform: MF Total /100ml Pho (Note: Use MPN method for highly turbid samples) Dissolved Solids: Total 120 mg/I pH (when analyzed) units TOC -1-LAW mg/I Chloride 2l0 mg/I Arsenic mg/1 Grease and Oils mg/I Phenol mg/I Sulfate mg/I Specific Conductance uMhos Total Ammonia 0--`Aka mg/I TKN as N mg/I uMhos cte'*.i DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES WATER OUALITY DIVISION, GROUNDWATER SECTION 1636 MAIL SERVICE CENTER PERMIT #: • EXPIRATION DATE: Non -Discharge W Q OOO591 O UIC NPDES TYPE OF PERMITTED OPERATION BEING MONITORED Lagoon Remediation: Infiltration Gallery Spray Field Remediation: Rotary Distributor Land Application of Sludge Other: NOTE: Values should reflect dissolved and colloidal concentrations. Date sample analyzed:-1^;1 ;X-.27,-3 'b^3-22 Laboratory Name: - Ey_". ►%CO nvy%e^-k Certification No. ko ✓ YES NO and field acidified to (NO2) as N mg/I ate (NO3) as N 0. o mg/I sphorus: Total as P 'f-10-04 mg/I Orthophosphate mg/I Al - Aluminum mg/I Ba - Barium mg/I Ca - Calcium _1'l . 0 1 mg/I Cd - Cadmium mg/I Chromium: Total mg/I Cu - Copper mg/I Fe - Iron mg/I Hg - Mercury mg/I K - Potassium mg/I Mg - Magnesium mg/I Mn - Manganese mg/I method # = method # = `"e YES NO) 4 Ni - Nickel mg/I Pb - Leant mg/I Zn - Zinc mg/I Ammonia Nitrogen mg/I Other (Specify Compounds and Concentration Units) Di ORGANICS: (GC,GC/MS,HPLC) (Specify test and method #. Attach lab report.) Report Attached? Yes ✓ (1) No (0) VOC : method # = —. ,I P�cs;dctnt print or type E w'nfimgM % hcoo qwn- ho 114 OAKMONT DRIVE GREENVILLE, N.C. 273588 AVOCA, LLC (WASTEWATER) MR. BRIAN CONNER P.O. BOX 129 MERRY HILL, NC 27957 y a Maotevater ZVI. 10 PHONE (2521 756-6208 FAX (2525 756-0633 ID#: 132 DATE COLLECTED: 07/20/22 DATE REPORTED : 08/09/22 REVIEWED BY: Effluent Well #5 Well #7 Well #8 Well #9 Analysis Method PARAMETERS Date Analyst Code BOD, mg/I 1070 07/21/22 HMM 521OB-16 Total Suspended Residue, mg/l 162 07/22/22 DNS 254OD-15 Ammonia Nitrogen as N, mg/l 0.04 0.09 <0.04 0.63 <0.04 07/27/22 KES 350.1 112-93 Total ICjeldahl Nitrogen as N,mg/l 40.50 08/03/22 KES 351.2 112-93 Nitrate+Nitrite as N, mg/l (talc) 0.46 353.2 R2-93 Nitrate Nitrogen as N, mg/l <0.04 <0.04 0.47 0.45 0.50 07/22/22 KES 353.2 112-93 Nitrite Nitrogen as N, mg/l 0.46 07/22/22 KES 353.2 112-93 Total Phosphorus as P, mg/l 5.38 0.09 <0.04 1.64 0.09 08/03/22 BMD 365.4-74 Total Organic Carbon, mg/I 3.37 5.06 11.28 1.09 07/26/22 HMM 531OC-14 Chloride, mg/l 98 33 32 27 27 07/22/22 DNS 4500CLB-11 Total Dissolved Residue, mg/l 2000 590 250 560 300 07/24/22 DNS D5907-13 Calcium, ug/l 29354 32721 4535 34723 49371 07/25/22 LFJ EPA200.7 Magnesium, ug/I 2938 07/25/22 LFJ EPA200.7 Sodium, ug/I 180636 07/25122 LFJ EPA200.7 Sodium Adsorption Ratio (talc) 8.5 Total Nitrogen, mg/I (talc) 40.96 114 OAi4MON T DRIVE GREENVILLE, N.C. 27858 AVOCA, LLC (WASTEWATER) MR. BRIAN CONNER P.O. BOX 129 MERRY HILL, NC 27957 wsstewat*r Z:Ds 10 PHONE (252) 756-6208 FAX (252) 756-0633 ID#: 132 DATE COLLECTED: 07/20/22 DATE REPORTED : 08/09/22 REVIEWED BY: / / `LJ Well #10 Well #11 Analysis Method PARAMETERS Date Analyst Code Ammonia Nitrogen as N, mg/1 0.05 12.96 07/27/22 KES 350.1 R2-93 Nitrate Nitrogen as N, mg/l 4.83 0.08 07/22/22 KES 353.2 R2-93 Total Phosphorus as P, mg/l <0.04 <0.04 08/03/22 BMD 365.4-74 Total Organic Carbon, mg/l 1.43 7.46 07/26/22 RMM 531OC-14 Chloride, mg/l 93 26 07/22/22 DNS 4500CLB-11 Total Dissolved Residue, mg/l 470 720 07/24/22 DNS D5907-13 Calcium, ug/l 23346 17081 07/25/22 LFJ EPA200.7 Environment 1, Inc. CHAIN OF CUSTODY RECORD P.O. Boo-7085. 114 Oakniont Dr. Page I - Greenville NC)7858 environment I inc.corn DISIN17TCTION CHLORINE NEUTRALIZED AT COLLECTION Phone (1.52) 756-6208 a Fax (252) 756-0633 j CHLORINE CLIENT. 132 Week: 33 F-i UV VT L'� 42 pH CHECK (LAB) P P, P1 P P I P1 P1 P P1 P P P1 P I CONTAJNER TYPE, P/G kVOCA, LLC (WASTEWATER) NONE 1M. BRIAN CONNER P.O. BOX 129 CHEMICAL PRESERVATION M[ERRY HILL NC 27957 A A C C C A A C C A A A A A A - NONE D - NACH '252) 482-2133 Ld LU ;�7 -j Uj U) cc LU UJ HNO, E-HCL CC -J CC 0 z C1 LU C - H,SO, F - ZINC ACETATE/NAOH COLLECTION < 0 0 LU -1 CL Uj 0 0 0� 4 + e Z U 0 0 U I- z — LU 2i < G - NA THIOSULFATE CL SAMPLE LOCATION DATE TIME Effluent 8 K".X3 CLASSIFICA T1ION: E WASTEWATER (NPDES) DRINKING HATER welt" Well #5 VI, 24AG 7, . ... .. .... Well #7 I 40 7 DWRIGW Well #8 -1 -x0-7X 11,• 10 21.2 7 SOLID YVASTE SECTION Wen #9 12 ras 24-1 7 'x 11 2.S (#1 7 'g CHAIN OF CUSTODY (SEAL) MAINTAINED Wen #10 DURING SHIPMENT/DELIVERY WeU#ll -1-20-22. 12, 0 9; 4 1 7 N SAMPLES COLLECTED BY., (Please Print? SAMPLES RECEIVED! LAB AT cC. RELINQUISHED B SiG,J iSAtvtPLER, DATFjrIME REC IVED 91Y (StG.I-- COMMIENTS: %CEIVED By (SIG.) DATUIME RECEIVED BY (-5JG,' DAMTIME RELINQUISHED BY (SIG.) DATEITIME RELINQUISHED BY (SIG.) DATE TiNT i Sampler must place a "C" for composite sample or a"G"for PLEASE READ Instructions for completing this form on. the FORM -05 Grab sample in the blocks above for each parameter requested. N-D 411139 ® I Laboratories- LLC a member of The GEL Group INC August 08, 2022 Ms. Ann Brown Environment One, Inc. 114 Oakmont Drive Greenville, North Carolina 27858 Re: Routine Analytical - North Carolina Work Order: 587186 Dear Ms. Brown: 0 PO Qux 3t1712 Chadestan-S029417 2040 U.,-ige Road Ctuidwon. SC 29dtt7 P 3ds.5.�S.Bi%i P 243.766.1 M GEL Laboratories, LLC (GEL) appreciates the opportunity to provide the enclosed analytical results for the sample(s) we received on July 25, 2022. This original data report has been prepared and reviewed in accordance with GEL's standard operating procedures. Test results for NELAP or ISO 17025 accredited tests are verified to meet the requirements of those standards, with any exceptions noted. The results reported relate only to the items tested and to the sample as received by the laboratory. These results may not be reproduced except as full reports without approval by the laboratory. Copies of GEL's accreditation and certifications can be found on our website at www.gel.com. Our policy is to provide high quality, personalized analytical services to enable you to meet your analytical needs on time every time. We trust that you will find everything in order and to your satisfaction. If you have any questions, please do not hesitate to call me at (843) 556-8171, ext. 1614. Sincerely, Delaney Stone Project Manager Purchase Order: PO Chain of Custody: Bromide Enclosures gelxem Page 1 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Report for ENV0001 Environment One, Inc. Client SDG: 587186 GEL Work Order: 587186 The Qualifiers in this report are defined as follows: * A quality control analyte recovery is outside of specified acceptance criteria ** Analyte is a Tracer compound ** Analyte is a surrogate compound U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the Certificate of Analysis. The designation ND, if present, appears in the result column when the analyte concentration is not detected above the limit as defined in the 'U' qualifier above. This data report has been prepared and reviewed in accordance with GEL Laboratories LLC standard operating procedures. Please direct any questions to your Project Manager, Delaney Stone. Reviewed by Page 2 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.corn Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Greenville, North Carolina 27858 Contact: Ms. Ann Brown Project: Routine Analytical - North Carolina Client Sample ID: Effluent Sample ID: 587186001 Matrix: Water Collect Date: 20-JUL-22 12:15 Receive Date: 25-JUL-22 Collector: Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 32.3 1.34 4.00 mg/L 20 HXC 1 07/26/22 0325 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 3 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Contact: Project: Greenville, North Carolina 27858 Ms. Ann Brown Routine Analytical - North Carolina Client Sample ID: Well #5 Sample ID: 587186002 Matrix: Water Collect Date: 20-JUL-22 12:35 Receive Date: 25-JUL-22 Collector: Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 5.46 0.134 0.400 mg/L 2 HXC1 07/26/22 0354 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 4 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company : Environment One, Inc. Address : 114 Oakmont Drive Contact: Project: Greenville, North Carolina 27858 Ms. Ann Brown Routine Analytical - North Carolina Client Sample ID: Well #7 Sample ID: 587186003 Matrix: Water Collect Date: 20-JUL-22 13:40 Receive Date: 25-JUL-22 Collector: Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 16.7 0.670 2.00 m9/L 10 HXC1 07/26/22 0424 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 5 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Greenville, North Carolina 27858 Contact: Ms. Ann Brown Project: Routine Analytical - North Carolina Client Sample ID Sample ID: Matrix: Collect Date: Receive Date: Collector: Well #8 587186004 Water 20-JUL-22 13:10 25-JUL-22 Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 11.4 0.670 2.00 mg/L 10 HXC1 07/26/22 0554 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 6 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Greenville, North -Carolina 27858 Contact: Ms. Ann Brown Proiect: Routine Analvtical - North Carolina Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Well #9 587186005 Water 20-JUL-22 12:55 25-JUL-22 Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 0.294 0.0670 0.200 m9/L 1 HXC 1 07/26/22 0624 2294692 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 7 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Greenville, North Carolina 27858 Contact: Ms. Ann Brown Project: Routine Analytical - North Carolina Client Sample ID: Sample ID: Matrix: Collect Date: Receive Date: Collector: Well #10 587186006 Water 20-JUL-22 13:25 25-JUL-22 Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 0.402 0.0670 0.200 mg/L I HXCI 07/26/22 0654 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments I EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 8 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road" Charleston SC 29407 - (843) 556-8171 - www.gel.com Certificate of Analysis Company: Environment One, Inc. Address : 114 Oakmont Drive Contact: Project: Greenville, North Carolina 27858 Ms. Ann Brown Routine Analytical - North Carolina Client Sample ID: Well #11 Sample ID: 587186007 Matrix: Water Collect Date: 20-JUL-22 12:05 Receive Date: 25-JUL-22 Collector: Client Report Date: August 8, 2022 Project: ENV000101 Client ID: ENV0001 Parameter Qualifier Result DL RL Units PF DF Analyst Date Time Batch Method Ion Chromatography EPA300.0 Bromide Liquid "As Received" Bromide 6.24 0.335 1.00 mg/L 5 HXC1 07/26/22 1601 2294092 1 The following Analytical Methods were performed: Method Description Analyst Comments 1 EPA 300.0 Notes: Column headers are defined as follows: DF: Dilution Factor Lc/LC: Critical Level DL: Detection Limit PF: Prep Factor MDA: Minimum Detectable Activity RL: Reporting Limit MDC: Minimum Detectable Concentration SQL: Sample Quantitation Limit Page 9 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Report Date: August 8, 2022 Environment One, Inc. Page 1 of 114 Oakmont Drive Greenville, North Carolina Contact: Ms. Ann Brown Workorder: 587186 Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time on Chromatography 3atch 2294092 QC1205147521 586558002 DUP Bromide 1 0.184 0.203 mg/L 9.45 ^ (+/-0.200) HXC 1 07/25/22 18:2 QC1205147520 LCS Bromide 1.25 QC1205147519 MB Bromide U QC1205147523 586558002 PS Bromide 1.25 J 0.184 Notes: 1.25 mg/L 0.000 mg/L 1.40 mg/L 100 (90%-110%) 07/25/2217:2 07/25/22 16:5 97.4 (90%-110%) 07/25/2218:5 The Qualifiers in this report are defined as follows: < Result is less than value reported > Result is greater than value reported B The target analyte was detected in the associated blank. E General Chemistry --Concentration of the target analyte exceeds the instrument calibration range H Analytical holding time was exceeded J See case narrative for an explanation J Value is estimated N/A RPD or %Recovery limits do not apply. N 1 See case narrative ND Analyte concentration is not detected above the detection limit NJ Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Q One or more quality control criteria have not been met. Refer to the applicable narrative or DER. R Per section 9.3.4.1 of Method 1664 Revision B, due to matrix spike recovery issues, this result may not be reported or used for regulatory compliance purposes. R Sample results are rejected U Analyte was analyzed for, but not detected above the MDL, MDA, MDC or LOD. X Consult Case Narrative, Data Summary package, or Project Manager concerning this qualifier Z Paint Filter Test --Particulates passed through the filter, however no free liquids were observed. Page 10 of 15 SDG: 587186 GEL LABORATORIES LLC 2040 Savage Road Charleston, SC 29407 - (843) 556-8171 - www.gel.com QC Summary Workorder: 587186 Page 2 of Parmname NOM Sample Qual QC Units RPD% REC% Range Anlst Date Time ^ RPD of sample and duplicate evaluated using +/-RL. Concentrations are <5X the RL. Qualifier Not Applicable for Radiochemistry. d 5-day BOD--The 2:1 depletion requirement was not met for this sample e 5-day BOD--Test replicates show more than 30% difference between high and low values. The data is qualified per the method and can be used for reporting purposes h Preparation or preservation holding time was exceeded N/A indicates that spike recovery limits do not apply when sample concentration exceeds spike cone. by a factor of 4 or more or %RPD not applicable. ^ The Relative Percent Difference (RPD) obtained from the sample duplicate (DUP) is evaluated against the acceptance criteria when the sample is greater than five times (5X) the contract required detection limit (RL). In cases where the duplicate value is less than 5X the RL, a control limit of +/- the RL is used to evaluate the DUP result. * Indicates that a Quality Control parameter was not within specifications. For PS, PSD, and SDILT results, the values listed are the measured amounts, not final concentrations. Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless qualified on the QC Summary. Page 11 of 15 SDG: 587186 General Chemistry Technical Case Narrative Environment One, Inc. SDG #: 587186 Product: Ion Chromatography Analytical Method: EPA 300.0 Analytical Procedure: GL-GC-E-086 REV# 30 Analytical Batch: 2294092 The following samples were analyzed using the above methods and analytical procedure(s). GEL Sample ID# Client Sample Identification 587186001 Effluent 587186002 Well 45 587186003 Well #7 587186004 Well #8 587186005 Well #9 587186006 Well #10 587186007 Well #1 l 1205147519 Method Blank (MB) 1205147520 Laboratory Control Sample (LCS) 1205147521 586558002(NonSDG) Sample Duplicate (DUP) 1205147523 586558002(NonSDG) Post Spike (PS) The samples in this SDG were analyzed on an "as received" basis. Data Summary: All sample data provided in this report met the acceptance criteria specified in the analytical methods and procedures for initial calibration, continuing calibration, instrument controls and process controls where applicable, with the following exceptions. Technical Information Sample Dilutions The following samples 1205147521 (Non SDG 586558002DUP), 1205147523 (Non SDG 586558002PS), 587186001 (Effluent), 581186002 (Well #5), 587186003 (Well #7), 587186004 (Well #8) and 587186007 (Well #11) were diluted because target analyte concentrations exceeded the calibration range. Samples 587186001 (Effluent), 587186002 (Well #5), 587186003 (Well #7), 587186004 (Well #8) and 587186007 (Well #11) were diluted based on historical data. Dilutions may be required for many reasons, including to minimize matrix interferences or to bring over range target analyte concentrations into the linear calibration range. 587186 Analyte 001 002 003 004 007 Bromide 20X I 2X I 10X I 10X I 5X Certification Statement Where the analytical method has been performed under NELAP certification, the analysis has met all of the requirements of the NELAC standard unless otherwise noted in the analytical case narrative. Page 12 of 15 SDG: 587186 KDI , lUNi. I 1=1 C1; kmont [)r. m,>;.n},_ui I inr.cum DISINF'17TION CHLORINE NEUTRALIZED AT COLLECTION (-j-' )7i6-tlb3:; (AIL.ORINt 1 9+: 132 Week: 33 pH CHECK (LAB) J41tA, LLC (WASTEWATER) NONE p p p p p P p p p p H P. ]? CONTAINER TYPE, PiG R�:PRIAN CONNER Ood3OX 129 CHEMICAL PRESERVATION ER12Y HILL NC 27957 A A C C C A A C C A A A A A 01 A -NONE D-NAOH V) 52) 482-21.33 w w `�coB - HNO E - I-ICL rr o w Lr- LU w C- H,SO, F- ZINC ACETATC,NAOH COLLECTION a a o G NATHIOSULfATE s U U ±? SAMPLE LOCATION DATE TIME � o r- tR � � � E ° Cflhient 1 ` CLASSIFICATION WASTEWATER (NPDE5) DRINKINGIVATER F.. "' Well #5 `4-�a-�� \�' 3S Z4,S �1 _ Well #7 -1 10-1� 13'•4 t7 25^j(]�p7 DVJR;'GN! Well #8 —1 -10-1�, 13 :10 v •2 SOLID WASTE SECTION Well #J l_ a- 1 2z. 12 5 2 3 I �i CHAIN OF CUSTODY (SEAL) MAINTAINED Well #Lp i-zv-1z ►3.25 2 •(o ( DURING SHIPM[NT%DELIVERI' Well #11 2Z 12 — __ SAMPLES COLLECTED BY: (Please Print) SAMPLES RECEIVED IN LAB AT ';C iELlh1QUISHED 1:3' SIG.) (SAtvIPLER) DATErrIME REC IVED BY (SIC � - - ATE1TIME 7�21 COMMENTS: �. Pam# �L i32a`7 2zz2 iELlh QUIShi� BY (. IG.1 DATETIME _ze-zz 1-1'.ca ;ELINOUISHED BY (SIG.) DATE;TIME CEI\ D BY iSIG.) TE71ME PLEASE READ Instructions for completing this form on the reverse side. Sampler must place a "C for composite sample or a "G" for -Q 411139 r. A I Grab sample in the blocks above for each parameter requested. N SA11-TPi.F. RF.f F.iP'f J2r RFVTx'W T?f1R�i .1 1�`1 Client SDG/AR/COC/Wut$ Order: 67 Received By: MVH Date Received: Ctrc)c Applicabc: PedEx Express FedEx Ground UPS Field Services Courier Other Carrier and Tracking Number V1 1 0S C),-� /1 �-Att)--� —� S Suspected Hazard hd'drmatinn Z *If Net Counts > 100cpm on samples not marked "radioactive", contact the Radiation Safety Group for further investigation. Hnzatd Class Shipped: UNq: A)SItipped as a DO'r Hazaialuu5? it UN2910, IN the Radioactive Shipment Survey Compliant? Yes_ No_ B) Did the client' desigtmte the s:unples are to be COC notation or radioactive stickers on containers, equal client designation. received as radioactive C) Did the RSO classify (lie samples as Maxim in Net Counts Observed" (Observed Counts- Area Background Counts): CPNI I mR/Hr radioactive? Classified its: Rad I Rad 2 Rad 3 COC notation or hazard labels on containers equal client designation. D) Did the client desi nie samples are hazardous? If D or E is yes, select Hazards below. E) Did the RSO identify possible hazin-W PCBs Flammable Foreign Soil RCRA Asbestos Beryllium Other. Sample Receipt Criteria ^ Z Z Couuuents/Qualifiers (Required for Non -Conforming Items) Shipping containers received intact and Circle Applicable: Setdx broken Damateed container I-eaking container Other (describe) I sealed? 2 Chain of custody documents included Circle Appgenble: Client conincied rand provided CDC COC created upon receipt with shipment'? Preservation Method: Wet Ice Ice Puke Dry ice None ther. 3 Samples requiring cold preservation ':dl temperatures are recorded in Celsius TB11'IPt within (0 < 6 den. C)?b 4 Daily check performed and passed on IR Temperature Device Serial M: IR2-21 temperature gun? Secondary Temperature Device Serial 9 (If Applicable): eals Circle Applicable: Sbroken Damaged containLe er aking container other (describe) 5 Sample containers intact and sealed? Samples requiring chemical preservation Sample ID's and Cnotaincrx Affected: 6 at proper pH? If Prcsemiflon added, I oM,, Il' Yes, arc Encores or Soil Kits present for solids? Yes_ N(L_ NA_(.If ),es, take to VOA Freezer) Do any samples requiro Volatile Fri liquid VOA vials contain acid preservation? Yes_ No_. NA_ftf unknown. select No) 7 Analysis'? Are liquid VOA vials freeof beadspuce?Yes_ No_ NA_ Sumple ID's and containers affected: TD's and tests affected: 8 Samples received within holding time? 9 Sample ID's on CDC mulch ID's on IDS and containers affected: battles? Date & time on COC rants date & time Circle Applicable: No dates on containers o limes on con COC missing info Other (describe) 10 on bottles? t Number of containers received match Circle Applicable: No container count on CDC Other (deu-ribc) I I number indicated on COC? 12 Are sample containers identifiable as GL-L provided by use of GEL labels? 1.3 COC form is properly signed in trcle Applicable: Not relinquished Other (describe) relinquished/received sections? Comments (Use Continuation Foam if needed): I'M(or PMA)rcvicw" litiritlsda t,Ny Dale "t' L/T P:g, I of� GL-CHL-SR-001 Rev 7 Page 14 of 15 SDG: 587186 It - List of current GEL Certifications as of 08 August 2022 State Certification Alabama 42200 Alaska 17-018 Alaska Drinking Water SC00012 Arkansas 88-0651 CLIA 42D0904046 California 2940 Colorado SC00012 Connecticut PH-0169 DoD ELAP/ ISO]7025 A2LA 2567.01 Florida NELAP E87156 Foreign Soils Permit P330-15-00283, P330-15-00253 Georgia SC00012 Georgia SDWA 967 Hawaii SC00012 Idaho SC00012 Illinois NELAP 200029 Indiana C—SC-01 Kansas NELAP E-10332 Kentucky SDWA 90129 Kentucky Wastewater 90129 Louisiana Drinking Water LA024 Louisiana NELAP 03046 (A133904) Maine 2019020 Maryland 270 Massachusetts M—SC012 Massachusetts PFAS Approv Letter Michigan 9976 Mississippi SC00012 Nebraska NE—OS-26-13 Nevada SC000122022-5 New Hampshire NELAP 2054 New Jersey NELAP SC002 New Mexico SC00012 New York NELAP 11501 North Carolina 233 North Carolina SDWA 45709 North Dakota R-158 Oklahoma 2019-165 Pennsylvania NELAP 68-00485 Puerto Rico SC00012 S. Carolina Radiochem 10120002 Sanitation Districts of L 9255651 South Carolina Chemistry 10120001 Tennessee TN 02934 Texas NELAP T104704235-22-20 Utah NELAP SC000122021-36 Vermont VT87156 Virginia NELAP 460202 Washington C780 Page 15 of 15 SDG: 587186