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Home My WebLink AboutWQ0000455_Monitoring (Report)_202301113. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §26I.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Environmental Chemists, Inc. and Date of analysis: 12/7/22 Passed corrosivity test: Ej yes ❑ no. pH: s.u. (2 <pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: >157 °F (> 140°F) Passed reactivity test: ❑ yes ❑no. HCN: <1.0 mg/kg (<250) & H2S: 0.20 mg/kg (<500) TCLP Parameter Limit (mg/l) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <1.0 Hexachlorobenzene 0.13 <0.050 Barium 100.0 <1.0 Hexachloro-1,3-Butadiene 0.5 <0.050 Benzene 0.5 <0.01 Hexachloroethane 3.0 <0.050 Cadmium 1.0 <1.0 Lead 5.0 <1.0 Carbon Tetrachloride 0.5 <0.01 Lindane 0.4 <0.0005 Chlordane 0.03 <0.02 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.01 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.01 Methyl Ethyl Ketone 200.0 <0.05 Chromium 5.0 <1.0 Nitrobenzene 2.0 <0.050 m-Cresol 200.0 <0.050 Pentachlorophenol 100.0 <0.250 o-Cresol 200.0 <0.050 Pyridine 5.0 <0.050 p-Cresol 200.0 <0.050 Selenium 1.0 <1.0 Cresol 200.0 <0.050 Silver 5.0 <1.0 2,4-D 10.0 <0.003 Tetrachloroethylene 0.7 <0.01 1,4-Dichlorobenzene 7.5 <0.050 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.01 Trichloroethylene 0.5 <0.01 1,1-Dichloroethylene 0.7 <0.01 2,4,5-Trichlorophenol 400.0 <0.050 2,4-Dinitrotoluene 0.13 <0.050 2,4,6-Trichlorophenol 2.0 <0.050 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0,003 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.01 FORM: RSC 06-16 Page 2 of 5 ANALYTICAL & CONSULTING CHEMISTS The Village Of Bald Head Island 106 Lighthouse Wynd Bald Head Island NC 28461 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 e 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 e 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 a 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Jan 10, 2023 Customer PO #: Customer ID: 08100149 Report #: 2022-24387 Project ID: Sludge Lab ID 22-60019 Test Sample ID: Site: Sludge Method Collect Date/Time 12/7/2022 8:00 AM Matrix Solid/Sludge Results Chlordane (TCLP) Endrin (TCLP) Heptachlor (TCLP) Heptachlor epoxide (TCLP) Lindane (TCLP) Methoxychlor (TCLP) Toxaphene (TCLP) 2,4,5-TP (TCLP) 2,4-D (TCLP) 1,4-Dichlorobenzene (TCLP) 2,4,5-Trichlorophenol (TCLP) 2,4,6-Trichlorophenol (TCLP) 2,4-Dinitrotoluene (TCLP) Cresol (TCLP) Hexachloro-1,3-butadiene (TCLP) Hexachlorobenzene (TCLP) Hexachloroethane (TCLP) m + p-Cresol (TCLP) Nitrobenzene (TCLP) o-Cresol (TCLP) Pentachlorophenol (TCLP) Pyridine (TCLP) 1,1-Dichloroethylene (TCLP) 1,2-Dichloroethane (TCLP) Benzene (TCLP) Carbon Tetrachloride (TCLP) SW-846 8081 B SW-846 8081 B SW-846 8081 8 SW-846 8081 B SW-846 8081 B SW-846 8081 8 SW-846 8081 B SW-846 8151 A SW-846 8151 A SW-846 8270 E SW-846 8270 E SW-846 8270 E SW-846 8270 E S W-846 8270 E SW-846 8270 E SW-846 8270 E SW-846 8270 E SW-846 8270 E SW-846 6270 E SW-846 8270 E SW-846 8270 E SW-846 8270 E SW-846 Method 8260D SW-846 Method 8260D SW-846 Method 8260D SW-846 Method 8260D Sampled by Jason Jacobs Date Analyzed <0.02 mg/L 12/15/2022 <0.0005 mg/L 12/15/2022 <0.0005 mg/L 12/15/2022 <0.0005 mg/L 12/15/2022 <0.0005 mg/L 12/15/2022 <0.0005 mg/L 12/15/2022 <0.05 mg/L 12/15/2022 <0.003 mg/L 12/14/2022 <0.003 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.250 mg/L 12/14/2022 <0.050 mg/L 12/14/2022 <0.01 mg/L 12/20/2022 <0.01 mg/L 12/20/2022 <0.01 mg/L 12/20/2022 <0.01 mg/L 12/20/2022 Report k:: 2022-24387 Page 1 of 3 ANALYTICAL & CONSULTING CHEMISTS The Village Of Bald Head Island 106 Lighthouse Wynd Bald Head Island NC 28461 Attention: Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Mantel:), NC 27954 0 252.473.5702 Lab/Fax 255-A Wilmington Nighway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com Date of Report: Jan 10, 2023 Customer PO #: Customer ID: 08100149 Report #: 2022-24387 Project ID: Sludge Chlorobenzene (TCLP) Chloroform (TCLP) Methyl ethyl ketone (TCLP) Tetrachloroethylene (TCLP) Trichloroethylene (TCLP) Vinyl Chloride (TCLP) RCI Cyanide Sulfide Ignitability Sludge Residuals Aluminum Arsenic Cadmium Calcium Chromium Copper Lead Magnesium Molybdenum Nickel Potassium Selenium Sodium Zinc N itrate+N itrite-Nitrogen Total Solids (%) Ammonia Nitrogen Total Kjeldahl Nitrogen (TKN) Total Phosphorus SW-846 Method 8260D SW-846 Method 8260D SW-846 Method 8260D SW-846 Method 82600 SW-846 Method 8260D SW-846 Method 8260D SM 4500 CN D-2016 SM 4500 5 D SW 846 method 1010 EPA 200 7. Rev 4 4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7. Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev, 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 353.2 SM 2540 B SM 4500 NH3 C-2011 SM 4500 Norg B-2011 SM 4500 P (F-H)-2011 <0.01 mg/L <0.01 mg/L <0.05 mg/L <0.01 mg/L <0.01 mg/L <0.01 mg/L <1.0 mg/kg 0.20 mg/kg >157°F 25900 mg/kg <37.9 mg/kg <7.58 mg/kg 18100 mg/kg 32.0 mg/kg 325 mg/kg 7.68 mg/kg 5690 mg/kg <7.58 mg/kg 10.9 mg/kg 6920 mg/kg <7.58 mg/kg 4880 mg/kg 877 mg/kg 4780 mg/kg 2.11 % <4.74 mg/kg 45400 mg/kg 45100 mg/kg 12/20/2022 12/20/2022 12/20/2022 12/20/2022 12/20/2022 12/20/2022 12/16/2022 12/19/2022 12/13/2022 01/04/2023 01 /06/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 01/04/2023 12/13/2022 12/08/2022 12/08/2022 12/08/2022 12/19/2022 Report #:: 2022-24387 Page 2 of 3 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab • 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 • 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax info@environmentalchemists.com The Village Of Bald Head Island 106 Lighthouse Wynd Bald Head Island NC 28461 Attention: Customer ID: Report #: Project ID: Sludge Date of Report: Jan 10, 2023 Customer PO #: 08100149 2022-24387 pH SW 846 Method 9045D Result estimated. Analyzed out of 15 minutes hold time. Mercury TCLP Metals Arsenic (TCLP) Barium Cadmium Chromium Lead (TCLP) Selenium Silver Mercury SW-846 7471 B EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 200.7, Rev. 4.4, 1994 EPA 245.1 6.09 units <0.834 mg/kg <1.0mg/L <1.0 <1.0 <1.0 12/13/2022 12/30/2022 12/17/2022 12/17/2022 12/17/2022 12/17/2022 <1.0 mg/L 12/17/2022 <1.0 12/17/2022 <1.0 12/17/2022 <0.0002 12/19/2022 Comment: Results, except pH, reported on a dry weight basis. pH reported on a as received basis. Reviewed by: ) ,{ ., Report #.. 2022-24387 Page 3 of 3 Environmental Chemist, Inc., Wilmington, NC Lab #94 Ghent • Sample Receipt Checklist Date! �/ _, Report Number: 2022- - l 1_d1_ pIcS_rii U;i inc cori:: r Jre. N/A 12. If custody seals were present, were they in ❑ YES I❑ NO Original temperature upon receipt ,)---°C Corrected temperatu.ire upon receipt Hol`! temperature taken: 0 Temperature Blanb: IR Gun iD: Thomas Traceable IR Gun Correction S/N 192511657 Against Bottle; Factor'C: 0.0 p YES ❑ NO 3. If temperature of cooler exceeded 6'C, was Project Mgr./QA notified? q YES ❑ NO 1 4. Were proper custody procedures (relinquished/received) followed? ® YES 0 NO 5. \JVere sample ID's listed on the COC? YES 0 NO 6. Were samples ID's listed on sample containers? Ca YE5 0 NO 7. l'.'ere collection date and time listed on the COC? GI YES 0 NO E. V.'-ere tests to be performed listed on the COC? --- YES 0 NO 5. D ,' samples arrive in proper containers for each test? 10 NO ir.i r?'_. samples arrive in good condition for each test? --....lo No ---- -_— i J. ::c> adequate sample volume + a mailable. I❑ O —''_.. rc: sanin1es rrCei;'ad within proper holding time. D YES NO,_•,,. .� � forr,_i_r_�:_ai.-�:_;. '❑ 1_,. Sere acid preserved samples received at a pH of <2? ❑ YES i❑ NO .,.ere cyanide samples received at a pH >12? — -- — ` —` O YES I❑ I0 1 I .. .,. c !Ir`i;i�- samples received -- - I .. - •; •;,'�iJ�rPieria( rEC?Ii,,rl at a CIIiJ!lilf_ re_•a.! i - _« 0 (E5 0 Ii0 I17. i�ere SJ(fi-e/Cyanide received at a chlorine residual of <0.5 in,'_ ❑ YES 0 NO f ia. ,.'•Jere orthophosphate samples filtered in the field within 15 m gags? 6602 Windmill Way Wilmington, NC 28405 910 392.0223 YE5 YES a YES E•=...c� • i 3r ; a�_ R._ _li c'la'y51� ai recorded On i' Sample Preservation: Sample(s) by adding (circle one): Time of preservation: ':lust be completed for any sample(s) incorrectly preserved or :.'ith headspace) ::'ere received incorrectlye preserved and:`1Erc a.,justed accortilnaly H SJ_ HNO: HCi NaOH ii more than one preservative is needed n0ta = in comments below vere received .vith headspa__ COMMENTS: "C DOC. QA..002 Rev 0 0 pp� Ll�I l�--v 0 5 a w h z 0 H U LL 1— w U 0) J V) 2 S ❑ U z z 0 H U LT. H w U 0 z w U z O Z 0 a1 PHONE/FAX: tQ E N PROJECT NAME: WWTP Sludge samples CONTACT NAME: Nate Lindsay, ORC REPORT TO: COPY TO: CLIENT: The village of Bald Head Utilities ADDRESS: 11 I I ANALYSIS REQUESTED Full TCLP/Nutrients/Metals/RCI E ra 0 ' a W V Lb U c PRESERVATION L13H10 OIHJ. HOVN CONN tOSZH 10H 3NON X - el3SIMIN 019V1 0 �9 E E +• 16 (J, vi P ----- t' t' • I \ r .... 111 116w au!Jo140 (0JOd) Jaulewo0 0_ 0 d 0 a 0 0_ O a 0 a 0 0_ 0 0_ 0 CL 0 CL O geJO JO ailsodwo0 U 0 0 0 0 CO 0 0 0 0 0(.9 0 0 0 0 0 0 0 0 ,�� Relinquished By: I 1 j 4 ,,t adAj aldweS C a E m O 0 O 0 ') P. S w .1 ' Sample Identification Sludge Transfer r o L c 4 W r i i [f 1 Q N N A CO 'L7 U) w U w LY Delivered By: