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HomeMy WebLinkAbout#5623_2016_1117_JS_FINALINSPECTION REPORT ROUTING SHEET To be attached to all inspection reports in-house only. Laboratory Cert. #: 5623 Laboratory Name: City of Belmont Water Plant Inspection Type: Field Municipal Initial Inspector Name(s): Jason Smith Inspection Date: November 17, 2016 Date Forwarded for Initial December 20, 2016 Review: Initial Review by: Anna Ostendorff Date Initial Review December 20, 2016 Completed: ❑ Insp. Initial ❑ Insp. Reg Cover Letter to use: ❑Insp. No Finding ❑Insp. CP ®Corrected ❑Insp. Reg. Delay (to use: rt click, properties, check) Unit Supervisor/Chemist III: Todd Crawford Date Received: December 29, 2016 Date Forwarded to Admin.: January 5, 2017 Date Mailed: January 12, 2017 Special Mailing Instructions: Copy Wes Bell MRO ROY COOPER r+ fry r'r r Water Resources r.-.nsviraONMEr flat._ QUAU r January 11, 2017 5623 Mr. Joseph Roy City of Belmont Water Plant P.O. Box 431 Belmont, NC 28012 SUBJECT: North Carolina Wastewater/Groundwater Laboratory Certification (NC WW/GW LC) Initial Inspection Dear Mr. Roy: Enclosed is a report for the inspection performed on November 17, 2016 by Jason Smith. Since the Finding(s) cited during the inspection were all corrected prior to the completion of the enclosed report, a response is not required. The staff is commended for taking the initiative in correcting the Findings in such a timely manner. For Certification maintenance, your laboratory must continue to carry out the requirements set forth in 15A NCAC 2H .0800. Copies of the checklists completed during the inspection may be requested from this office. Thank you for your cooperation during the inspection. If you wish to obtain an electronic copy of this report by electronic mail, or if you have questions or need additional information, please contact me at (919) 733- 3908 ext. 251. Sincerely, D� Todd Crawford Technical Assistance & Compliance Specialist NC WW/GW Laboratory Certification Branch Attachment cc: Dana Satterwhite, Jason Smith, Master File 5623 LABORATORY NAME: NPDES PERMIT #: ADDRESS: CERTIFICATE #: DATE OF INSPECTION: TYPE OF INSPECTION: AUDITOR(S): LOCAL PERSON(S) CONTACTED: I. INTRODUCTION: City of Belmont Water Plant NCO077763 205 N. Tenth Street Belmont, NC 28012 5623 November 17, 2016 Field Municipal Initial Jason Smith Joseph Roy and Jennifer Gibson This laboratory was inspected by a representative of the North Carolina Wastewater/Groundwater Laboratory Certification (NC WW/GW LC) program to verify its compliance with the requirements of 15A NCAC 2H .0800 for the analysis of environmental samples. IL GENERAL COMMENTS: The laboratory maintains certification voluntarily. The facility's effluent is discharged to the Belmont WWTP and their NPDES permit is inactive. No samples within the scope of NC WW/GW LC rules have been analyzed since obtaining certification. All required Proficiency Testing (PT) samples have been analyzed for the 2016 PT calendar year and the graded results were 100% acceptable. Current Quality Assurance Policies for Field Laboratories and Approved Procedure documents for the analysis of the facility's currently certified Field Parameters were provided at the time of the inspection. Requirements that reference 15A NCAC 2H .0805 (g) (1), stating "Data pertinent to each analysis must be maintained for five years. Certified Data must consist of date collected, time collected, sample site, sample collector, and sample analysis time. The field benchsheets must provide a space for the signature or initials of the analyst and proper units of measure for all analyses", are intended to be a requirement to document all pertinent information for historical reconstruction of data. It is not intended to imply that existing records are not adequately maintained unless the Finding speaks directly to that. III. FINDINGS REQUIREMENTS COMMENTS AND RECOMMENDATIONS: Documentation Comment: The traceability log did not include the vendor. The NC WW/GW LC Quality Assurance Policies for Field Laboratories document states: All chemicals, reagents, standards Page 2 #5623 City of Belmont Water Plant and consumables used by the laboratory must have the following information documented: Date Received, Date Opened (in use), Vendor, Lot Number, and Expiration Date. Notification of acceptable corrective action (i.e., an updated traceability log including documentation of the vendor with an implementation date of December 5, 2016) was received by email on December 5, 2016. No further response is necessary for this Finding. Quality Assurance Comment: The automatic pipettor used to prepare the PT sample has not been calibrated. This is considered a critical measurement since it is analogous to preparing a standard. The NC WW/GW LC Quality Assurance Policies for Field Laboratories document states: Mechanical volumetric liquid -dispensing devices (e.g., fixed and adjustable auto-pipettors, bottle -top dispensers, etc.), used for critical measurements, must be calibrated at least every twelve months and documented. Each liquid -dispensing device must meet the manufacturer's statement of accuracy. For variable volume devices used at more than one setting, check the accuracy at the maximum, middle and minimum values. Testing at more than three volumes is optional. When a device capable of variable settings is dedicated to dispense a single specific volume, calibration is required at that setting only. Notification of acceptable corrective action (i.e., annual calibration of the automatic pipettor will begin to be performed along with the balance calibration prior to the next critical measurement such as PT preparation) was received by email on December 5, 2016. No further response is necessary for this Finding. Comment: Calibration of the automatic pipettor would not be required if the laboratory uses a Class A volumetric pipet that is the appropriate volume to prepare the PT sample. Chlorine, Total Residual — Hach 10014 (Aqueous) Comment: Instrument identification was not documented on the benchsheet. The NC WW/GW LC Approved Procedure for the Analysis of Total Residual Chlorine document states: The following must be documented in indelible ink whenever sample analysis is performed: Instrument identification. Notification of acceptable corrective action (i.e., an updated benchsheet including the instrument model and serial number with an implementation date of December 15, 2016) was received by email on December 15, 2016. No further response is necessary for this Finding. Comment: The benchsheet did not include a space to document the time and date of sample collection or the sample site. North Carolina Administrative Code, 15A NCAC 2H .0805 (g) (1) states: Data pertinent to each analysis must be maintained for five years. Certified Data must consist of date collected, time collected, sample site, sample collector, and sample analysis time. The field benchsheets must provide a space for the signature or initials of the analyst and proper units of measure for all analyses. This was not documented because the laboratory has only analyzed PT samples which are not collected. The benchsheet must still include a space to document this information to be ready to analyze environmental samples when needed. Notification of acceptable corrective action (i.e., an updated benchsheet including space for the sample site, date collected and time collected with an implementation date of December 15, 2016) was received by email on December 15, 2016. No further response is necessary for this Finding. Comment: A check standard was not being analyzed prior to sample analysis. The NC WW/GW LC Approved Procedure for the Analysis of Total Residual Chlorine document states: When a five -standard annual standard curve verification is used, the laboratory must check the calibration curve each analysis day. To do this, the laboratory must analyze a calibration blank to zero the instrument and analyze a check standard each day that samples are analyzed. The value obtained for the check standard must read within 10% of the true value of the check standard. If Page 3 #5623 City of Belmont Water Plant the obtained value is outside of the ±10% range, corrective action must be taken. General absorbance standard (i.e., DR/check) supplied by some manufacturers cannot be used for the check standard. Gel -type standards may be used for this purpose. These standards must be verified initially and every 12 months thereafter, with the standard curve. Notification of acceptable corrective action (i.e., a calibration log to be used for TRC gel standard analysis with an implementation date of December 5, 2016 and a statement that the gel standard will be analyzed prior to sample analysis) was received by email on December 5, 2016. No further response is necessary for this Finding. IV. PAPER TRAIL INVESTIGATION: No paper trail performed. V. CONCLUSIONS: All Findings noted during the inspection were adequately addressed prior to the completion of this report. The inspector would like to thank the staff for its assistance during the inspection and data review process. No response is required. Report prepared by: Jason Smith Date: December 20, 2016 Report reviewed by: Anna Ostendorff Date: December 20, 2016