NC0005312_Application_20180619 (2)

Water Resources
ENVIRONMENTAL QUALITY
June 19, 2018
Scott Taylor
Duvaltex US Inc
304 E. Main Street
Elkin, NC 28621
Subject: Permit Renewal
Application No. NC0005312
Duvaltex RLAP
Surry County
Dear Applicant:
ROY COOPER
Go"mor
NffCHAEL S. REGAN
Secretrry
LINDA CLTLPEPPER
Jrderim lJhwwr
The Water Quality Permitting Section acknowledges the June 15, 2018 receipt of your permit renewal application and
supporting documentation. Your application will be assigned to a permit writer within the Section's NPDES WW
permitting branch. Per G.S. 15OB-3 your current permit does not expire until permit decision on the application is made.
Continuation of the current permit is contingent on timely and sufficient application for renewal of the current permit.
The permit writer will contact you if additional information is required to complete your permit renewal. Please respond
in a timely manner to requests for additional information necessary to allow a complete review of the application and
renewal of the permit.
Information regarding the status of your renewal application can be found online using the Department of Environmental
Quality's Environmental Application Tracker at:
httl)s•//deq nc gov/permits-regulations/permit-guidance/environmental-application-tracker
If you have any additional questions about the permit, please contact the primary reviewer of the application using the
links available within the Application Tracker.
Sincerely,
�
Wren Thedford
Administrative Assistant
Water Quality Permitting Section
ec: WQPS Lasefiche File w/application (WSRO)
State of North Carolina I Environmental Quality I Water Resources
1617 Mail Service Center I Raleigh, North Carolina 27699-1617
oto.cnv.Avnn

June 11, 2018
Mr. Joe Corporon
NCDEQ- Division of Water Resources
Water Quality Permitting Section- NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Re: Permit Renewal Application
NPDES Permit No. NC0005312
Mr. Corporon,
hart ► hickman
SMARTER ENVIRONMENTAL SOLUTIONS
RECEIVEDIDENRIDWR
JUN 15 2018
Water Resources
Permitting Section
On behalf of Duvaltex (US), Inc. (Duvaltex), Hart and Hickman, PC (H&H) is pleased to
provide (I) Original and (1) copy of an application for renewal of NPDES Wastewater Permit
No. NC0005312.
NPDES permit NC0005312 was reissued on February 5, 2018 to reflect the transfer of ownership
to Duvaltex (US), Inc. from TrueElkin, Inc. The 2012 permit application describes the
downsizing of the facility in 2009, which resulted in the elimination of multiple process
operations. In addition, the 2008 application included effluent information from a neighboring
manufacturing facility not owned or operated by True Elkin, Inc/Duvaltex (US), Inc. This facility
was known as Westpoint Stevens (WPS). WPS remains vacant at the time of writing this letter.
This permit application includes completed EPA Forms 3510-1 and 3510-2c as well as all
required attachments. The data is supported by permit required periodic test results as well as the
2017 priority pollutant analysis.
IJt"�a e lerh�JlI rev. ,jJK ) J r,�L
n ea.(c,4 : `Q d z."Af41- _kk�L -see- -
les
2923 South Tryon Street, Suite 100 3921 Sunset Ridge Rd, Suite 301
Charlotte, NC 28203 Raleigh, NC 27507 www.harthickman.com
704.586.0007 main 919.947.4241 main

Mr. Joe Corporon
June 11, 2018
Should you have any questions or need any additional information, please feel free to call me at
your convenience.
Sincerely,
Hart &Hickman, PC
Greg Kanellis
Senior Project Engineer
Enclosures: (2) Permit Renewal Applications
Cc: Glen Gary, Wastewater Treatment Plant Manager ORC, Duvaltex (US), Inc.
Scott Taylor, Environmental Coordinator, Duvaltex (US), Inc.
S. WAA-Muter Prolens\DwaRex (VCP-0021�OIB S Wmmal\01 AEylicaron Cover Lmer ad Avider
Shave-Fl d.c
hart ► hickman
SMAWEA ENVIRONMENT,-! SOLUTIONS

NPDES
WASTEWATER
APPLICATION
PERMIT RENEWAL
(PERMIT NO. NC0005312)
Duvaltex (US), Inc.
Surry County, North Carolina
June 2018
Submitted to: Joe Corporon
NCDEQ- Division of Water Resources
Water Quality Permitting Section- NPDES
610 East Center Ave., Suite 301
Mooresville, NC 28115
Prepared by: Hart & Hickman, P.C.
3921 Sunset Ridge Road, Suite 301
Raleigh, NC 27607
[phone]
Prepared for: Scott Taylor
Environmental Coordinator
Duvaltex (US), Inc.
P.O. Box 179
Guilford, ME 04443
[phone]

TABLE OF CONTENTS
Section1..............................................................................Form 1
Section2...........................................................................Form 2C
APPENDICIES
AppendixA...............................................................Production Data
Appendix B..................................Whole Effluent Toxicity Tests for 2017
Appendix C......................................Priority Pollutant Analysis for 2017
Appendix D.................................Discharge Monitoring Reports for 2017
Section
Figure 1-1 (Facility Location)............................................................1
Figure 1-2 (Facility Drawing).............................................................I
Figure 1-3 (Production Flow Schematic).................................................2
Figure1-4 (Water Use Schematic).......................................................2
Figure 1-5 (Wastewater Treatment Plant Schematic)................................2

SECTION 1
EPA Form 3510-1
Figure 1-1 Facility Location
Figure 1-2 Facility Site Plan

Please print or type in the unshaded areas only
fill-in areas are spaced for elite type, i.e., 12 chamctersAnch . For Approved. OMB No. 2040-0086. Approval expires 5-31-92
FORM U.S. ENVIRONMENTAL PROTECTION AGENCY I. EPA I.D. NUMBER
�EPA GENERAL INFORMATION S TrA
.►
Consolidated Permits Program F NCO05312 D
GENERAL Read the "General Instructions" before starting.) ' 2 13 1a 5
LABEL ITEMS GENERAL INSTRUCTIONS
I. EPA I.D. NUMBER If a preprinted label has been provided,
affix it in the designated space. Review the
information carefully; if, any of it is
coronet!rrect cross through d and enter the
III. FACILITY NAME correct data in the appropriate fill-in area
below. Also, ff any to the pleorof the
data is
absent (the area information the Iothat
the label
V.FACILITY PLEASE PLACE LABEL IN THIS SPACE appear),please ace Fists pi provide hehproperofill-
MAILING LIST
VI. FACILITY
LOCATION
II. POLLUTANT CHARACTERIM
the supplemental from listed in the
SPECIFIC QUESTIONS ves No FORI
ATTACI
Is this facility a publicly owned treatment works
which results in a discharge to waters of the
U.S.? (FORM 2A)
lrs of the U.S. other man
or B above? FORM 2C 22 2] 24
lity, treat, store, or dispose of
(FORM 3) ® ❑ ❑
uo you or will you infect at mis raanry any
produced water other fluids which are brought to
the surface in connection with conventional oil or
❑
®
1-1
natural gas production, inject fluids used for
enhanced recovery of oil or natural gas, or inject
fluids for storage of liquid hydrocarbons?
34
35
36
FORM4
Is this foci ily a proposed stationary source
which is one of the 28 industrial categones listed
El
®
1-1in
emit
the instructions and which will potentially em
100 tons per year of any air pollutant regulated
under the Clean Air Act and may affect or be
40
41
1 42
located in an attainment areal FORM 51
NAME OF FACILITY
SKIP I Duvaltex (US). Inc.
0
P.O. Box 530
lit any penult application lorms to the EFA. it you answer yes" to any
nthesis following the question. Mark "X" in the box in the third column if
I not submit any of these forms. You may answer "no" If your activity is
ection D of the instructions for definitions of bold-faced terms.
MARK
"X"
SPECIFIC QUESTIONS
YES
NO
FORM
ATTACHED
Does or will this facility (either existing or
proposed) include a concentrated animal
feeding operation or aquatic animal
production facility which results in a discharge
❑
to waters of the U.S.? (FORM 2B)
1e
20
21
Is this proposal facility joinert an hose described
in A or a above) which will result in a discharge
❑
to waters of the U.S.? FORM 2D
25
26
27
Do you or will you inject at this facility industrial or
municipal effluent below the lowermost stratum
containing, within one quarter mile of the well
bore, underground sources of drinking water?
31
32
33
(FORM 4)
Do you or will you inject at this facility Fluids for
special processes such as mining of suffer by the
Fresch process, solution mining of minerals, in
situ combustion of fossil fuel, or recovery of
geothermal energy? (FORM 4)
37
38
39
Is this facility a proposed stationary source
which is NOT one of the 28 industrial categories
in the instructions and which will potentially
Elfisted
0
El
emit 250 tons per year of any air pollutant
regulated under the Clean Air Act and may affect
_
207 1 1 876 1 1 1418
NC 1 128621
NC 1 128621
086
EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

CONTINUED FROM THE FRONT
VII. SIC CODES 4-di it, in order of riori
A. FIRST B. SECOND
c
2262
(sPecdl)
7 2824
(specify)
Finishers of Broadwoven Fabrics of
Manmade Fiber and Silk
7
Manmade Organic Fibers, Except Cellulosic
15
16 17
15 16 19
C. THIRD D. FOURTH
c 2221 (specify) 7 (specify)
7 Manmade Fiber and Silk 7
15 1 16 17 1151 16 t9
Vill. OPERATOR INFORMATION
A. NAME B. Is the name listed in Item
c Duvaltex (US), Inc.
VIII-A also the owner?
8
❑YES ®NO
1a 16 55
C. STATUS OF OPERATOR Enter the appropriate letter into the answer box; if "Other,"s eci
D. PHONE area code & no.
F = FEDERAL M = PUBLIC (other than federal or state)
P
(specify)
c
336
835
0244
A
S = STATE O = OTHER (specify)
66
1s
16 18
t9 n
zz 25
P=PRIVATE
E. STREET OR PO BOX
P.O. Box 530
26 55
F. CITY OR TOWN
G. STATE H. ZIP CODE IX. INDIAN LAND
c Elkin
NC 28621 Is the facility located
on Indian lands?
B
42 42 47 51 ❑YES
®NO
15 16 40
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES (Discharges to Surface Water
D. PSD Air Emissions from Proposed Sources
NC0005312
°
01315R29
9
N
s P
15
16
17 1B 30
15 t6
17
t8 30
B. UIC (Underground injection of Fluids
E. OTHER (specify)
(Specify)
Land Application Permit
1
N/A
7
°
WQ0013982
9
u
9
15 1
16
1 17
18 30
15
18
17
18 30
C. RCRA Hazardous Wastes E. OTHER (specify) (Specify)
cg R ' NCDO03219573 s ° NCG170000 Stormwater Discharge
Permit
15 ,6 A 18 30 15 16 17 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS(provide a brief description)
Duvaltex (US), Inc. leases and operates a textile manufacturing facility and wastewater treatment plant in Elkin,
NC. The facility primarily finishes woven upholstery fabric from primarily manmade and some natural fibers.
Operations include fabric finishing, yarn extrusion and limited weaving for sample fabrics. The WWTP treats
process wastewater from the Duvaltex (US), Inc. The WWTP formerly treated waste from the adjacent former
Westpoint Stevens (WPS) facility. The WPS facility is not owned by Duvaltex (US), Inc. and is currently vacant.
XIII. CERTIFICATION see instructions
i certify under penalty of law that 1 have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information, including the possibil' of fine nd imprisonment.
A. NAME & OFFICIAL TITLE (type or print) B. SIG ATURE
C. DATE SIGNED
/5
J �Aytii<
COMMENTS FOR OFFICIAL USE ONLY
c
C
15
i6 55
EPA FORM 3510-1 (8-90)

( .. .Elkin
SITE
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APPROXIMATE rime
N o z000 a000 SITE LOCATION MAP
SCALE IN FEET PROJECT DUVALTEX (US), INC.. — ELKIN FACILITY
304 EAST MAIN STREET
ELKIN, NORTH CAROLINA
U.S.G.S. QUADRANGLE MAP hart hiekman 29D Snuch Tryon S.t-S.w 106
Ch.1m, North C.Im. 28203
ELKIN SOUTH, NORTH CAROLINA, 1996 SMARTER ENVIRONMENTAL SOIIJTIONS 701 (p) 704-586-0373 (t)
DATE: 5-16-18 REVISION NO: 0
QUADRANGLE
7.5 MINUTE SERIES (TOPOGRAPHIC) JOB NO: VCP-002 FIGURE: 1-1

SECTION 2
EPA Form 3510-2c
Figure 1-3 Production Flow Schematic
Figure 1-4 Water Use Schematic
Figure 1-5 Wastewater Treatment Plant Schematic

Disclaimer
This is an updated PDF document that allows you to type your information
directly into the form. This form is the most updated form currently available.
Note: You cannot save what you have typed unless you have the full Adobe
Professional version.
Instructions:
1. Type in your information
2. Print the completed form
3. Sign and date the printed copy
4. Mail the form to the address stated in the instructions

United States Office of EPA Form 3510-2C
Environmental Protection Enforcement Revised August 1990
Agency Washington, DC 20460 Previous edifions
are obsolete
Permits Division
.="EPA Application Form 2C —
Wastewater Discharge
Information
Consolidated Permits Program
This form must be completed by all persons applying
for an EPA permit to discharge wastewater (existing
manufacturing, commercial, mining, and silvicu@ural
operations).
4�W Printed on regded paper

Paperwork Reduction Act Notice
The public reporting burden for this collection of information is
estimated to average 33 hours per response. This estimate
includes time for reviewing instructions, searching existing
data sources, gathering and maintaining the needed data, and
completing and reviewing the collecttion of information. Send
comments regarding the burden estimate or any other aspect
of this collection of information to the Chief, Information Policy
Branch (PM-223), US Environmental Protection Agency,
1200 Pennsylvania Avenue, NW, Washington, DC 20460, and
to the Office of Information and Regulatory Affairs, Office of
Management and Budget, Washington, DC 20503, marked
Attention: Desk Officer for EPA.

INSTRUCTIONS — FORM 2c
Application for Permit to Discharge Wastewater
EXISTING MANUFACTURING, COMMERCIAL, MINING. AND SILVICULTURAL OPERATIONS
This form must be completed by all applicants who check 'yes" to
item 11-C in Form 1.
Public Availability of Submitted Information.
Your application will not be considered complete unless you answer
every question on this form and on Form 1. If an item does not apply
to you, enter "NA" (for not applicable) to show that you considered
the question.
You may not claim as confidential any information required by this
form or Form 1, whether the information is reported on the forms or
in an attachment. This information will be made available to the
public upon request.
Any information you submit to EPA which goes beyond that required
by this form or Form 1 you may claim as confidential, but claims for
information which is effluent data will be denied. If you do not assert
a claim of confidentiality at the time of submitting the information,
EPA may make the information public without further notice to you.
Claims of confidentiality will be handled in accordance with EPA's
business confidentiality regulations at 40 CFR Part 2.
Definitions
All significant terms used in these instructions and in the form are
defined in the glossary found in the General Instructions which
accompany Form 1.
EPA ID Number
Fill in your EPA Identification Number at the top of each page of
Form 2c. You may copy this number directly from item I of Form 1.
Item I
You may use the map you provided for item XI of Form 1 to
determine the latitude and longitude of each of your outfalls and the
name of the receiving water.
Item 11-A
The line drawing should show generally the route taken by water in
your facility from intake to discharge. Show all operations
contributing wastewater, including process and production areas,
sanitary flows, cooling water, and stormwater runoff. You may group
similar operations into a single unit, labeled to correspond to the
more detailed listing in item II-B. The water balance should show
average flows. Show all significant losses of water to products,
atmosphere, and discharge. You should use actual measurements
whenever available; otherwise use your best estimate. An example
of an acceptable line drawing appears in Figure 2c-1 to these
instructions.
Item II-B
List all sources of wastewater to each outfall. Operations may be
described in general terms (for example, "dye -making reactor' or
"distillation towed. You may estimate the flow contributed by each
source if no date are available. For stormwater discharges you may
estimate the average flow, but you must indicate the rainfall event
upon which the estimate is based and the method of estimation. For
each treatment unit, indicate its size, Flow rate, and retention time,
and describe the ultimate disposal of any solid or liquid wastes not
discharged. Treatment units should be listed in order and you should
select the proper code from Table 2c-1 to fill in column 3-b for each
treatment unit. Insert "XX" into column 3-b d no code corresponds to
a treatment unit you list. If you are applying for a permit for a
privately owned treatment works, you must also identify all of your
contributors in an attached listing.
Item II-C
A discharge is intermittent unless it occurs without interruption during
the operating hours of the facility, except for infrequent shutdowns
for maintenance, process changes, or other similar activities. A
discharge is seasonal if it occurs only during certain parts of the
year. Fill in every applicable column in this item for each source of
intermittent or seasonal discharges. Base your answers on actual
data whenever available; otherwise, provide your best estimate.
Report the highest daily value for flow rate and total volume in the
"Maximum Daily" columns (columns 4-a-2 and 4-b-2). Report the
average of all daily values measured during days when discharge
occurred within the last year in the "Long Term Average" columns
(columns 4-a-1 and 4-b-1).
Item III -A
All effluent guidelines promulgated by EPA appear in the Federal
Register and are published annually in 40 CFR Subchapter N. A
guideline applies to you if you have any operations contributing
process wastewater in any subcategory covered by a BPT, BCT, or
BAT guideline. If you are unsure whether you are covered by a
promulgated effluent guideline, check with your EPA Regional office
(Table 1 in the Form 1 instructions). You must check 'yes" if an
applicable effluent guideline has been promulgated, even if the
guideline limitations are being contested in court. If you believe that a
promulgated effluent guideline has been remanded for
reconsideration by a court and does not apply to your operations,
you may check "no."
Item III-B
An effluent guideline is expressed in terms of production (or other
measure of operation) if the limitation is expressed as mass of
pollutant per operational parameter; for example, "pounds of BOO
per cubic foot of logs from which bark is removed," or "pounds of
TSS per megawatt hour of electrical energy consumed by smelting
furnace." An example of a guideline not expressed in terms of a
measure of operation is one which limits the concentration of
pollutants.
Item III-C
This item must be completed only if you checked "yes" to item III-B.
The production information requested here is necessary to apply
effluent guidelines to your facility and you cannot claim it as
confidential. However, you do not have to indicate how the reported
information was calculated. Report quantities in the units of
measurement used in the applicable effluent guideline. The
production figures provided must be based on actual daily production
and not on design capacity or on predictions of future operations. To
obtain alternate limits under 40 CFR 122.45(b)(2)(ii), you must define
your maximum production capability and demonstrate to the Director
that your actual production is substantially below maximum
production capability and that there is a reasonable potential for an
increase above actual production during the duration of the permit.
Item IV -A
If you check 'yes" to this question, complete all parts of the chart, or
attach a copy of any previous submission you have made to EPA
containing same information.
Item IV-B
You are not required to submit a description of future pollution
control projects if you do not wish to or if none is planned.
Item V-A, B, C, and D
The items require you to collect and report data on the pollutants
discharged for each of your ouffalis. Each part of this item addresses
a different set of pollutants and must be completed in accordance
with the specific instructions for that part. The following general
instructions apply to the entire item.
General Instructions
Part A requires you to report at least one analysis for each pollutant
listed. Parts B and C require you to report analytical data in two
ways. For some pollutants, you may be required to mark "X" in the
"Testing Required" column (column 2-a, Part C), and test (sample
and analyze) and report the levels of the pollutants in your discharge
whether or not you expect them to be present in your discharge. For
all others, you must mark "X" in either the "Believe Present" column
or the "Believe Absent" column (columns 2-a or 2-b, Part B, and
columns 2-15 or 2c, Part C) based on your best estimate, and test for
those which you believe to be present. (See specific instructions on
the form and below for Parts A through D.) Base your determination
that a pollutant is present in or absent from your discharge on your
2C-1

FORM 2c — INSTRUCTIONS (continued)
Item V-A, B, C, and D (continued)
knowledge of your raw materials, maintenance chemicals,
intermediate and final products and byproducts, and any previous
analyses known to you of your effluent or similar effluent. (For
example, if you manufacture pesticides, you should expect those
pesticides to be present in contaminated stormwater runoff) If you
would expect a pollutant to be present solely as a result of its
presence in your intake water, you must mark "Believe Present" but
you are not required to analyze for that pollutant. Instead, mark an
'X' In the "Intake" column.
A. Reporting. All levels must be reported as concentration
and as total mass. You may report some or all of the
required data by attaching separate sheets of paper
instead of filling out pages V-1 to V-9 if the separate sheets
contain all the required information in a format which is
consistent with pages V-1 to V-9 in spacing and in
identification of pollutants and columns. (For example, the
data system used in your GC/MS analysis may be able to
print data in the proper format.) Use the following
abbreviations in the columns headed "Units" (column 3,
Part A, and column 4, Parts B and C).
Concentration Mass
ppm...
....parts permillion
Ibs .........................pounds
mga ...milligrams
per liter
ton ............
tons (English tons)
ppb..........
parts per billion
mg.. .......
...... -....milligrams
ug/l ...
micrograms per liter
9...............................grams
kg ......................kilograms
T...........
tonnes (meMc tons)
All reporting of values for metals must be in terms of "total
recoverable metal," unless:
(1) An applicable, promulgated effluent limitation or standard
specifies the limitation for the metal in dissolved, valent, or total
form; or
(2) All approved analytical methods for the metal inherently
measure only its dissolved form (e.g., hexavalent chromium); or
(3) The permitting authority has determined that in establishing
case -by -case limitations it is necessary to express the
limitations on the metal in dissolved, valent, or total form to
carry out the provisions of the CWA.
If you measure only one daily value, complete only the "Maximum
Daily Values" columns and insert '1' into the "Number of Analyses"
column (columns 2-a and 2-d, Part A, and column 3-a, 3-d, Parts B
and Q. The permitting authority may require you to conduct
additional analyses to further characterize your discharges. For
composite samples, the daily value is the total mass or average
concentration found in a composite sample taken over the operating
hours of the facility during a 24-hour period; for grab samples, the
daily value is the arithmetic or flow -weighted total mass or average
concentration found in a series of at least four grab samples taken
over the operating hours of the facility during a 24-hour period.
If you measure more than one daily value for a pollutant and those
values are representative of your wastestream, you must report
them. You must describe your method of testing and data analysis.
You also must determine the average of all values within the last
year and report the concentration and mass under the "Long Tenn
Average Values" columns (column 2-c, Part A, and column 3-c, Parts
B and C), and the total number of daily values under the "Number of
Analyses" columns (column 2-d, Part A, and columns 3-d, Parts B
and C). Also, determine the average of all daily values taken during
each calendar month, and report the highest average under the
"Maximum 30-day Values" columns (column 2c, Part A, and column
3-b, Parts B and C).
B. Sampling: The collection of the samples for the reported
analyses should be supervised by a person experienced in
performing sampling of industrial wastewater. You may contact your
EPA or Stale permitting authority for detailed guidance on sampling
techniques and for answers to specific questions. Any specific
requirements contained in the applicable analytical methods should
be followed for sample containers, sample preservation, holding
times, the collection of duplicate samples, etc. The time when you
sample should be representative of your normal operation, to the
extent feasible, with all processes which contribute wastewater in
normal operation, and with your treatment system operating property
with no system upsets. Samples should be collected from the center
of the flow channel, where turbulence is at a maximum, at a site
specified in your present permit, or at any site adequate for the
collection of a representative sample.
For pH, temperature, cyanide, total phenols, residual chlorine, oil and
grease, and fecal coliform, grab samples must be used. For all other
pollutants 24-hour composite samples must be used. However, a
minimum of one grab sample may be taken for effluents from holding
ponds or other impoundments with a retention period of greater than
24 hours. For stormwater discharges a minimum of one to four grab
samples may be taken, depending on the duration of the discharge.
One grab must be taken in the first hour (or less) of discharge, with
one additional grab (up to a minimum of lour) taken in each
succeeding hour of discharge for discharges lasting four or more
hours. The Director may waive composite sampling for any outfall for
which you demonstrate that use of an automatic sampler is infeasible
and that a minimum of four grab samples will be representative of
your discharge.
Grab and composite samples are defined as follows:
Grab sample: An individual sample of at least 100 milliliters
collected at a randomly -selected time over a period not exceeding
15 minutes.
Composite sample: A combination of at least 8 sample aliquots
of at least 100 milliliters, collected at periodic intervals during the
operating hours of a facility over a 24 hour period. The composite
must be flow proportional; either the time interval between each
aliquot or the volume of each aliquot must be proportional to either
the stream flow at the time of sampling or the total stream flow
since the collection of the previous aliquot. Aliquots may be
collected manually or automatically. For GC/MS Volatile Organic
Analysis (VOA), aliquots must be combined in the laboratory
immediately before analysis. Four (4) (rather than eight) aliquots
or grab samples should be collected for VOA. These four samples
should be collected during actual hours of discharge over a 24-
hour period and need not be flow proportioned. Only one analysis
is required.
The Agency is currently reviewing sampling requirements in light of
recent research on testing methods. Upon completion of its review,
the Agency plans to propose changes to the sampling requirements.
Data from samples taken in the past may be used, provided that:
All data requirements are met;
Sampling was done no more than three years before submission;
and
All data are representative of the present discharge.
Among the factors which would cause the data to be
unrepresentative are significant charges in production level,
changes in raw materials, processes, or final products, and changes
in wastewater treatment. When the Agency promulgates new
analytical methods in 40 CFR Part 136, EPA will provide information
as to when you should use the new methods to generate data on
your discharges. Of course, the Director may request additional
information, including current quantitative data, if she or he
determines it to be necessary to assess your discharges.
C. Analysis: You must use test methods promulgated in 40 CFR
Part 136; however, if none has been promulgated for a particular
pollutant, you may use any suitable method for measuring the level
of the pollutant in your discharge provided that you submit a
description of the method or a reference to a published method. Your
description should include the sample holding time, preservation
techniques, and the quality control measures which you used. If you
have two or more substantially identical outfalls, you may request
permission from your permitting authority to sample and analyse only
one outfall and submit the results of the analysis for other
substantially identical outfalls. If your request is granted by the
2C-1

FORM 2c — INSTRUCTIONS (continued)
Item V-A, B, C, and D (continued)
permitting authority, on a separate sheet attached to the application
form, identify which ouffall you did test, and describe why the ouffalls
which you did not test are substantially identical to the ouffall which
you did test.
D. Reporting of Intake Data: You are not required to report data
under the "Intake" columns unless you wish to demonstrate your
eligibility for a "net" effluent limitation for one or more pollutants, that
is, an effluent limitation adjusted by subtracting the average level of
the pollutant(s) present in your intake water, NPDES regulations
allow net limitations only in certain circumstances. To demonstrate
your eligibility, under the "Intake" columns report the average of the
results of analyses on your intake water (if your water is treated
before use, test the water after it is treated), and discuss the
requirements for a net limitation with your permitting authority.
Part V-A
Part V-A must be completed by all applicants for all outfalls, inducting
ouffalls containing only noncontad cooling water or storm runoff.
However, at your request, the Director may waive the requirement to
test for one or more of these pollutants, upon a determination that
available information is adequate to support issuance of the permit
with less stringent reporting requirements for these pollutants. You
also may request a waiver for one or more of these pollutants for
your category or subcategory from the Director, Office of Water
Enforcement and Permits. See discussion in General Instructions to
item V for definitions of the columns in Part A. The "Long Term
Average Values" column (column 2-c) and "Maximum 30day
Values" column (column 2-b) are not compulsory but should be filled
out if data are available.
Use composite samples for all pollutants in this Part, except use grab
samples for pH and temperature. See discussion in General
Instructions to Item V for definitions of the columns in Part A. The
"Long Term Average Values" column (column 2c) and "Maximum
30-Day Values" column (column 2-b) are not compulsory but should
be filled out if data are available.
Part V-B
Part V-B must be completed by all applicants for all outfalls, including
outfalls containing only noncontad cooling water or storm runoff. You
must report quantitative data if the pollutant(s) in question is limited
in an effluent limitations guideline either directly, or indirectly but
expressly through limitation on an indicator (e.g., use of TSS as an
indicator to control the discharge of iron and aluminum). For other
discharged pollutants you must provide quantitative data or explain
their presence in your discharge. EPA will consider requests to the
Director of the Office of Water Enforcement and Permits to eliminate
the requirement to test for pollutants for an industrial category or
subcategory. Your request must be supported by data representative
of the industrial category or subcategory in question. The data must
demonstrate that individual testing for each applicant is unnecessary,
because the facilities in the category or subcategory discharge
substantially identical levels of the pollutant or discharge the
pollutant uniformly at sufficiently low levels. Use composite samples
for all pollutants you analyze for in this part, except use grab
samples for residual chlorine, oil and grease, and fecal coliform. The
"Long Term Average Values" column (column 3-c) and "Maximum
30-day Values" column (column 3-b) are not compulsory but should
be filled out if data are available.
Part V-C
Table 2c-2 lists the 34 "primary" industry categories in the lefthand
column. For each ouffall, if any of your processes which contribute
wastewater falls into one of those categories, you must mark "X" in
"Testing Required" column (column 2-a) and test for (1) all of the toxic
metals, cyanide, and total phenols, and (2) the organic toxic
pollutants contained in Table 2c-2 as applicable to your category,
unless you qualify as a small business (see below). The organic toxic
pollutants are listed by GC/MS fractions on pages V-4 to V-9 in Part
V-C. For example, the Organic Chemicals Industry has an asterisk in
all four fractions; therefore, applicants in this category must test for
all organic toxic pollutants in Part V-C. The inclusion of total phenols
in Part V-C is not intended to classify total phenols as a toxic
pollutant. If you are applying for a permit for a privately owned
treatment works, determine your testing requirements on the basis of
the industry categories of your contributors. When you determine
which industry category you are in to find your testing requirements,
you are not determining your category for any other purpose and you
are not giving up your right to challenge your inclusion in that
category (for example, for deciding whether an effluent guideline is
applicable) before your permit is issued. For all other cases
(secondary industries, nonprocess wastewater outfalls, and
nonrequired GC/MS fractions), you must mark "X" in either the
"Believed Present" column (column 2-b) or the "Believed Absent'
column (column 2-c) for each pollutant. For every pollutant you know
or have reason to believe is present in your discharge in
concentrations of 10 ppb or greater, you must report quantitative
data. For acrolein, acrylonitrile, 2, 4 dinitrophenol, and 2-methyl-4, 6
dinitrophenol, where you expect these four pollutants to be
discharged in concentrations of 100 ppb or greater, you must report
quantitative data. For every pollutant expected to be discharged in
concentrations less than the thresholds specified above, you must
either submit quantitative data or briefly describe the reasons the
pollutant is expected to be discharged. At your request the Director,
Office of Water Enforcement and Permits, may waive the
requirement to test for pollutants for an industrial category or
subcategory. Your request must be supported by data
representatives of the industrial category or subcategory in question.
The data must demonstrate that individual testing for each applicant
is unnecessary, because the facilities in question discharge
substantially identical levels of the pollutant, or discharge the
pollutant uniformly at sufficiently low levels. If you quality as a small
business (see below) you are exempt from testing for the organic
toxic pollutants, listed on pages V4 to V-9 in Part C. For pollutants in
intake water, see discussion in General Instructions to this item. The
"Long Term Average Values" column (column 3c) and "Maximum
30-day Values" column (column 3-b) are not compulsory but should
be filled out if data are available. You are required to mark "Testing
Required" for dioxin if you use or manufacture one of the following
compounds:
(a) 2,4,5-tdchlorophenoxy acetic acid, (2,4,5-T);
(b) 2-(2,4,5-lrichlorophenoxy) propanoic acid, (Silvex, 2,4,5-TP)
(c) 2-(2,4,5-lrichlorophenoxy) ethyl 2,2-dichloropropionate, (Erbon)
(d) 0,0dimelhyl 0-(2,4,5-tdchlorophenyl) phosphorothioate, (Ronnel)
(a) 2,4,5, tdchlorophenol, (TCP); or
(f) hexachlorophene, (HCP).
If you mark "Testing Required" or "Believed Present; you must
perform a screening analysis for dioxins, using gas chromotography
with an electron capture detector. A TCDD standard for quanlitabon
is not required. Describe the results of this analysis in the space
provided; for example, "no measurable baseline deflection at the
retention time of TCDD" or "a measurable peak within the tolerances
of the retention time of TCDD:' The permitting authority may require
you to perform a quantitative analysis if you report a positive result.
The Effluent Guidelines Division of EPA has collected and analyzed
samples from some plants for the pollutants listed in Part C in the
course of its BAT guidelines development program. If your effluents
are sampled and analyzed as part of this program in the last three
years, you may use these data to answer Part C provided that the
permitting authority approves, and provided that no process change
or change in raw materials or operating practices has occurred since
the samples were taken that would make the analyses
unrepresentative of your current discharge.
Small Business Exemption: If you qualify as a "small business",
you are exempt from the reporting requirements for the organic toxic
pollutants, listed on pages V-4 to V-9 in Part C. There are two ways
in which you can qualify as a "small business." If your facility is a coal
mine, and if your probable total annual production is less than
100,000 tons per year, you may submit past production data or
estimated future production (such as a schedule of estimated total
production under 30 CFR § 795.14(c)) instead of conducting
analyses for the organic toxic pollutants. If your facility is not a coal
mine, and if your gross total annual sales for the most recent three
years average less than $100,000 per year (in second quarter 1980
2C-1

FORM 2c — INSTRUCTIONS (continued)
Item V-A, B, C, and D (continued)
dollars), you may submit sales data for those years instead of
conducting analyses for the organic toxic pollutants. The production
or sales data must be for the facility which is the source of the
discharge. The data should not be limited to production or sales for
the process or processes which contribute to the discharge, unless
those are the only processes at your facility. For sales data, in
situations involving intracorporate transfer of goods and services, the
transfer price per unit should approximate market prices for those
goods and services as closely as possible. Sales figures for years
after 1980 should be indexed to the second quarter of 1980 by using
the gross national product price deflator (second quarter of
1980=100). This index is available in National Income and Product
Accounts of the United States (Department of Commerce, Bureau of
Economic Analysis).
Part V-D
List any pollutants in Table 2c-3 that you believe to be present and
explain why you believe them to be present. No analysis is required,
but if you have analytical data, you must report it.
Note: Under 40 CFR 117.12(a)(2), certain discharges of hazardous
substances (listed in Table 2c-4 of these instructions) may be
exempted from the requirements of section 311 of CWA, which
establishes reporting requirements, civil penalties and liability for
cleanup costs for spills of oil and hazardous substances. A discharge
of a particular substance may be exempted if the origin, source, and
amount of the discharged substances are identified in the NDPES
permit application or in the permit, if the permit contains a
requirement for treatment of the discharge, and if the treatment is in
place. To apply for an exclusion of the discharge of any hazardous
substance from the requirements of section 311, attach additional
sheets of paper to your form, setting forth the following information:
1. The substance and the amount of each substance which may
be discharged.
2. The origin and source of the discharge of the substance.
3. The treatment which is to be provided for the discharge by:
a. An onsite treatment system separate from any treatment
system treating your normal discharge;
b. A treatment system designed to treat your normal
discharge and which is additionally capable of treating the
amount of the substance identified under paragraph 1
above; or
c. Any combination of the above.
See 40 CFR §117.12(a)(2) and (c) published on August 29, 1979, in
44 FR 50766, or contact your Regional Office (Table 1 on Form 1,
Instructions), for further information on exclusions from section 311.
Item VI
This requirement applies to current use or manufacture of a toxic
pollutant as an intermediate or final product or byproduct. The
Director may waive or modify the requirement if you demonstrate
that it would be unduly burdensome to identify each toxic pollutant
and the Director has adequate information to issue your permit. You
may not claim this information as confidential; however, you do not
have to distinguish between use or production of the pollutants or list
the amounts.
Item VII
Self explanatory. The permitting authority may ask you to provide
additional details after your application is received.
Item IX
The Clean Water Act provides for severe penalties for submitting
false information on this application form.
Section 309(c)(2) of the Clean Water Act provides that "Any person
who knowingly makes any false statement, representation, or
certification in any application,... shall upon conviction, be punished
by a fine of not more than $10,000 or by imprisonment for not more
than six months, or by both."
40 CFR Part 122.22 requires the certification to be signed as follows
(A) For a corporation: by a responsible corporate official. For
purposes of this section, a responsible corporate official means (i) a
president, secretary, treasurer, or vice-president of the corporation in
charge of a principal business function, or any other person who
performs similar policy- or decision -making functions for the
corporation, or (ii) the manager of one or more manufacturing,
production, or operating facilities employing more than 250 persons
or having gross annual sales or expenditures exceeding $25,000,000
(in second-quarter 1980 dollars), if authority to sign documents has
been assigned or delegated to the manager in accordance with
corporate procedures.
Note: EPA does not require specific assignments or delegation of
authority to responsible corporate officers identified in
§122.22(a)(1)(i). The Agency will presume that these responsible
corporate officers have the requisite authority to sign permit
applications unless the corporation has notified the director to the
contrary. Corporate procedures governing authority to sign permit
applications may provide for assignment or delegation to applicable
corporate position under §122.22(a)(1)(ii) rather than to specific
individuals.
(B) For a partnership or sole proprietorship: by a general partner or
the proprietor, respectively; or
(C) For a municipality, State, Federal, or other public agency: by
either a principal executive officer or ranking elected official. For
purposes of this section, a principal executive officer of a Federal
Agency includes (i) the chief executive officer of the Agency, or III) a
senior executive officer having responsibility for the overall
operations of a principal geographic unit of the Agency (e.g.,
Regional Administrators of EPA). Applications for Group II
stormwater dischargers may be signed by a duly authorized
representative (as defined in 40 CFR 122.22(b)) of the individuals
identified above.

CODES FOR TREATMENT UNITS
PHYSICAL TREATMENT PROCESSES
1-A..........
Ammonia Stripping
1-B ..........
Dialysis
1-C ..........
Diatomaceous Earth Filtration
1-0..........
Distillation
1-E .........
Electrodialysis
1-F .........
Evaporation
1-G ..........
Flocculation
1-H ..........
Flotation
1-I ..........
Foam Fractionation
1—t..........
Freezing
1-K..........
Gas -Phase Separation
1-L ..........
Grinding (Comminufors)
2-A..........
Carbon Adsorption
2-B ..........
Chemical Oxidation
2-C ..........
Chemical Precipitation
2-0..........
Coagulation
2-E ..........
Dechlormation
2-F ..........
Disinfection (Chlorine)
3-A.......... Activated Sludge
3-B .......... Aerated Lagoons
3-C.......... Anaerobic Treatment
3-0.......... Nitrification-Denilrification
t-M ..........
Grit Removal
1-N ..........
Microstraining
1-0..........
Mixing
1-P ...........
Moving Bed Filters
1-0...........
Mukimedia Filtration
1-R ..........
Rapid Sand Filtration
1-S ...........
Reverse Osmosis (Hyperfiltration)
1-T. . .........
Screening
1-1.1 ..........
Sedimentation (Settling)
1-V ...........
Slow Sand Filtration
1-W ..........
Solvent Extraction
1-X ...........
Sorption
CHEMICAL TREATMENT PROCESSES
2-G ..........
Disinfection (Ozone)
2-H ..........
Disinfection (Other]
2-1 ...........
Electrochemical Treatment
2-J... .....
... Ion Exchange
2-K ...........
Neutralization
2-L ...........
Reduction
BIOLOGICAL TREATMENT PROCESSES
4-A.......... Discharge to Surface Water
4-B .......... Ocean Discharge Through Outfall
3-E...........
Pre -Aeration
3-F ...........
Spray Irrigation/Land Application
3-G ..........
Stabilization Ponds
3-H ..........
Trickling Filtration
4-C .......... Reuse/Recycle of Treated Effluent
4-D ........... Underground Injection
SLUDGE TREATMENT AND DISPOSAL PROCESSES
5-A ..........
Aerobic Digestion
5-M ..........
Heat Drying
5-B ..........
Anaerobic Digestion
Nl ..........
Heat Treatment
5-C......
.... Bell Filtration
5-0 ..........
Incineration
5-D..........
Centrifugation
5-P ...........
Land Application
5-E ..........
Chemical Conditioning
5-0 ..........
Landfill
5-F ..........
Chlorine Treatment
5-R ..........
Pressure Filtration
5-G..........
Composting
5S ..........
Pyrolysis
5-H ..........
Drying Beds
5-T ..........
Sludge Lagoons
5-I...........
Elutriation
5-1.1 ..........
Vacuum Filtration
5-J ..........
Flotation Thickening
5-V ..........
Vibration
5-K ..........
Freezing
5-W ..........
Wet Oxidation
5-L ..........
Gravity Thickening
Table 2C-1

TESTING REQUIREMENTS FOR ORGANIC TOXIC POLLUTANTS INDUSTRY CATEGORY'
INDUSTRY CATEGORY
Volatile
GC/MS FRACTION'
Acid Base/Neutral
Pesticide
Adhesives and sealants............................................................
X
X
X
-
Aluminumforming.....................................................................
X
X
X
-
Auto and other laundries... ........................................................
X
X
X
X
Battery manufacturing...............................................................
X
-
X
-
Coalmining...............................................................................
X
X
X
X
Coilcoating...............................................................................
X
X
X
Copper forming .........................................................................
X
X
X
-
Electric and electronic compounds ...........................................
X
X
X
X
Electroplating............................................................................
X
X
X
-
Explosives manufacturing ...................................... ......... --......
-
X
X
-
Foundries..................................................................................
X
X
X
-
Gum and wood chemicals.........................................................
X
X
X
X
Inorganic chemicals manufacturing ..........................................
X
X
X
-
Iron and steel manufacturing....................................................
X
X
X
-
Leather tanning and finishing ....................................................
X
X
X
X
Mechanical products manufacturing .......................................-
X
X
X
-
Nonferrous metals manufacturing........- ..................................
X
X
X
X
Oremining................................................................................
X
X
X
X
Organic chemicals manufacturing .............................................
X
X
X
X
Paint and ink formulation..........................................................
X
X
X
X
Pesticides..................................................................................
X
X
X
X
Petroleum refining.....................................................................
X
X
X
X
Pharmaceutical preparations....................................................
X
X
X
-
Photographic equipment and supplies ......................................
X
X
X
X
Plastic and synthetic materials manufacturing ..........................
X
X
X
X
Plastic processing ............... --- ............................................
..- X
-
-
-
Porcelain enameling ................................... -............................
X
-
X
X
Printing and publishing..............................................................
X
X
X
X
Pulp and paperboard mills ........................................................
X
X
X
X
Rubber processing....................................................................
X
X
X
-
Soap and detergent manufacturing ...........................................
X
X
X
-
Steam electric power plants ......................................................
X
X
X
Textile mills ...............................................................................
X
X
X
X
Timber products processing......................................................
X
X
X
X
'See note at conclusion of 40 CFR Part 122, Appendix D (1983) for explanation of effect of suspensions on testing requirements for primary
industry categories.
'The pollutants in each fraction are listed in Item V-C.
X = Testing required.
- = Testing not required.
Tabs 2C-2

TOXIC POLLUTANTS AND HAZARDOUS SUBSTANCES
REQUIRED TO BE IDENTIFIED BY APPLICANTS IF EXPECTED TO BE PRESENT
TOXIC POLLUTANT
HAZARDOUS SUBSTANCES
HAZARDOUS SUBSTANCES
Asbestos
Dichlorvos
Naled
Diethyl amine
Napthenic acid
HAZARDOUS SUBSTANCES
Dimethyl amine
Nitrotoluene
Dintrobenzene
Parathion
Acetaldehyde
Diquat
Phenolsulfonate
Allyl alcohol
Disulfoton
Phosgene
Allyl chloride
Diumn
Propargite
Amyl acetate
Epichlorohydrin
Propylene oxide
Aniline
Ethion
Pyrethdns
Benzonitrile
Ethylene diamine
Quinoline
Benzyl chloride
Ethylene dibromide
Resorcinol
Butyl acetate
Formaldehyde
Strontium
Butylamine
Furfural
Strychnine
Caplan
Guthion
Styrene
Carbaryl
Isoprene
2,4,5-T (2,4,5-Tdchlorophenoxyacetic acid)
Carbofuran
Isopropanolamine
TDE (Tetrachlorodiphenyl ethane)
Carbon disulfide
Kelthane
2,4,5-TP [2-(2,4,5-Trichlorophenoxy) propanoic acid]
Chlorpyrifos
Kepone
Trichlomfon
Coumaphos
Malathion
Triethanolamine
Cresol
Mercaptodimethur
Triethylamine
Crolonaldehyde
Methoxychlor
Trimethylamine
Cyclohexane
Methyl mercaptan
Uranium
2,4-D (2,4-Dichlorophenoxyacetic acid)
Methyl methacrylate
Vanadium
Diazinon
Methyl parathion
Vinyl acetate
Dicamba
Mevinphos
Xylene
Dichlobenil
Mexacarbate
Xylenol
Dichlone
Moncethyl amine
Zirconium
2,2-Dichloropropionic acid
Monomethyl amine
Table 2C-3

HAZARDOUS SUBSTANCES
1. Acetaldehyde
2. Acetic acid
3. Acetic anhydride
4. Acetone cyanohydnn
5. Acetyl bromide
6. Acetyl chloride
7. Acrolein
8. Acrylonitnle
9. Adipic acid
10. Aldrin
11. Ally[ alcohol
12. Ally[ chloride
13. Aluminum sulfate
14. Ammonia
15. Ammonium acetate
16. Ammonium benzoate
17. Ammonium bicarbonate
18. Ammonium bichromate
19. Ammonium bifluoride
20. Ammonium bisulfte
21. Ammonium carbamate
22. Ammonium carbonate
23. Ammonium chloride
24. Ammonium chromate
25. Ammonium citrate
26. Ammonium fluoroborate
27. Ammonium fluoride
28. Ammonium hydroxide
29. Ammonium oxalate
30. Ammonium silicofluoride
31. Ammonium sulfamate
32. Ammonium sulfide
33. Ammonium suKte
34. Ammonium tartrate
35. Ammonium thiocyanate
36. Ammonium thiosulfate
37. Amyl acetate
38. Aniline
39. Antimony pentachloricle
40. Antimony potassium tartrate
41. Antimony tribromide
42. Antimony tichloride
43. Antimony trifluoride
44. Antimony trioxide
45. Arsenic disulfide
46. Arsenic pentoxide
47. Arsenic trichlonde
48. Arsenic trioxide
49, Arsenic trisulfide
50. Barium cyanide
51. Benzene
52. Benzoic acid
53. Benzonitrile
54. Benzoyl chloride
55. Beryl chloride
56. Beryllium chloride
57. Beryllium fluoride
58. Beryllium nitrate
59. Butylacetate
60. n-Butylphthalate
61. Butylamine
62. Butyric add
63. Cadmium acetate
64. Cadmium bromide
65. Cadmium chloride
66. Calcium arsenate
67. Calcium arsenite
69. Calcium carbide
69. Calcium chromate
70. Calcium cyanide
71. Calcium dodecylberenesulfonate
72. Calcium hypochlorite
73. Caplan
74. Carbaryl
75. Carbofuran
76. Carbon disulfide
77. Carbon tetrachloride
78. Chlordane
79. Chlorine
80. Chlorobenzene
81. Chloroform
82. Chloropyrifos
83, Chlorosulfonic acid
84. Chromic acetate
85. Chromic acid
86. Chromic sulfate
87. Chromous chloride
88. Cobaltous bromide
89. Cobaltous formate
90. Cobaltous sulfamate
91. Coumaphos
92. Cresol
93. Crotonaldehyde
94. Cupric acetate
95. Cupric acetoarsenite
96. Cupric chloride
97. Cupric nitrate
98. Cupric oxalate
99. Cupric sulfate
100. Cupric sulfate ammoniated
101. Cupric tartrate
102. Cyanogen chloride
103. Cyclohexane
104. 2,4-D add (2,4- Dichlorophenoxyacetic
acid)
105. 2,4-D esters (2,4- Dichlorophenoxyacetic
acid esters)
106. DDT
107. Diazinon
108. Dicamba
109. Dichlobenil
110. Dichlone
111. Dichlorobenzene
112. Dichloropropane
113. Dichloropropene
114. Dichloropropene-dichloproropane mix
115. 2,2-Dichloropropionic acid
116. Dichlorvos
117. Dieldnn
118. Diethylamine
119. Dimethylamine
120. Dinitrobenzene
121. Dinitrophenol
122. Dinitrololuene
123. Diquat
124. Disulfoton
125. Diuron
126. Dodecylbenzesulfonic acid
127. Endosulfan
128. Endrin
129. Epichlorohydrin
130. Elhion
131. Elhylbenzene
132. Ethylenediamme
133. Ethylene dibromide
134. Ethylene dichloride
135. Ethylene diaminetetracetic acid (EDTA)
136. Ferric ammonium citrate
137. Ferric ammonium oxalate
138. Ferric chloride
139. Ferric fluoride
140. Ferric nitrate
141. Ferric sulfate
142. Ferrous ammonium sulfate
143. Ferrous chloride
144. Ferrous sulfate
145. Formaldehyde
146. Formic acid
147. Fumadc acid
148. Furfural
149. Guthion
150. Heptachlor
151. Hexachlorocyclopentadiene
152. Hydrochloric add
153. Hydrofluoric acid
154, Hydrogen cyanide
155. Hydrogen sulfide
156.Isoprene
157. Isopropanolam ine
dodecylbenzenesulfonate
158. Kelthane
159.Kepone
160. Lead acetate
161. Lead arsenate
162. Lead chloride
163. Lead fluoborate
164. Lead flourite
165. Lead iodide
166. Lead nitrate
167. Lead stearate
168. Lead sulfate
169. Lead sulfide
170. Lead thiocyanate
171. Lindane
172. Lithium chromate
173. Malalhion
174. Maleic acid
175. Maleic anhydride
176. Mercaplodimethur
177. Mercuric cyanide
178. Mercuric nitrate
179. Mercuric sulfate
180. Mercuric thiocyanate
181. Mercurous nitrate
182. Methoxychlor
183. Methyl mercaptan
184. Methyl methacrylate
185. Methyl parathion
186. Mevinphos
187. Mexacarbate
188. Monoethylamine
189. Monomethylamine
190. Naled
191. Naphthalene
192. Naphthenic acid
193. Nickel ammonium sulfate
194. Nickel chloride
195. Nickel hydroxide
196. Nickel nitrate
197. Nickel sulfate
198. Nitric acid
199. Nitrobenzene
200. Nitrogen dioxide
201. Nitrophenol
202. Nitrololuene
203. Paraformaldehyde
204. Parathion
205. Pentachlorophenol
206. Phenol
207. Phosgene
208. Phosphoric acid
209. Phosphorus
210. Phosphorus oxychlonde
211. Phosphorus pentasulfide
212. Phosphorus trichloride
213. Polychlorinated biphenyls (PCB)
214. Potassium arsenate
215. Potassium arsenite
216. Potassium bichromate
Table 2C-4

HAZARDOUS SUBSTANCES
217. Potassium chromate
247. Sodium selenite
270. Trimethylamine
218. Potassium cyanide
- 248. Strontium chromate
271. Uranyl acetate
219. Potassium hydroxide
249. Strychnine
272. Uranyl nitrate
220. Potassium permanganate
250. Styrene
273. Vanadium penoxide
221. Propargite
251. Sulfuric acid
274. Vanadyl sulfate
222. Propionic acid
252. Sulfur monochloride
275. Vinyl acetate
223. Propionic anhydride
253. 2,4,5-T acid (2,4,5-
276. Vinylidene chloride
224. Propylene oxide
Trichlorophenoxyacetic acid)
277. Xylene
225. Pyrethrins
254. 2,4,5-T amines (2,4,5-Trichlorophenoxy
278. Xylenol
226. Ouinoline
acetic acid amines)
279. Zinc acetate
227. Resorcinol
255. 2,4,5-T esters (2,4,5 Trichlorophenoxy
280. Zinc ammonium chloride
228. Selenium oxide
acetic acid esters)
281. Zinc borate
229. Silver nitrate
256. 2,4,5-T salts (2,4,5-Trichlorophenoxy
282. Zinc bromide
230. Sodium
acetic acid salts)
283. Zinc carbonate
231. Sodium arsenate
257. 2,4,5-TP acid (2,4,5-Trichlorophenoxy
284. Zinc chloride
232. Sodium arsenite
propanoic acid)
285. Zinc cyanide
233. Sodium bichromate
258. 2,4,5-TP acid esters (2,4,5-
286. Zinc fluoride
234. Sodium bifluoride
Trichlorophenoxy propanoic acid esters)
287. Zinc formate
235. Sodium bisulfte
259. TDE (Tetrachlorodiphenyl ethane)
288. Zinc hydrosulfte
236. Sodium chromate
260. Tetraethyl lead
289. Zinc nitrate
237. Sodium cyanide
261. Tetraethyl pyrophosphate
290. Zinc phenolsulfonate
238. Sodium dodecylbenzenesulfonale
262. Thallium sulfate
291. Zinc phosphide
239. Sodium fluoride
263. Toluene
292. Zinc silicofluoride
240. Sodium hydrosulfide
264. Toxaphene
293. Zinc sulfate
241. Sodium hydroxide
266. Trichlorofon
294. Zirconium nitrate
242. Sodium hypochlorite
266. Trichloroethylene
295. Zirconium potassium flouride
243. Sodium methylate
267. Trichlorophenol
296. Zirconium sulfate
244. Sodium nitrite
268. Triethanolamine
297. Zirconium tetrachloride
245. Sodium phosphate (dibasic)
dodecylbenzenesulfonale
246. Sodium phosphate (tribasic)
269. Triethylamine
Table 2C-4 (continued)

LINE DRAWING
Blue River
90,000 GPD
45,000 GPD 45.000 GPD
Raw Materials Fiber 15 000 20,0
10,000 GPD
Preparation GPD Dyeing GP
40,000 GPD 40,000 GPD
Solid Waste it Neutralization Loss
4,000 GPD Separator Tank 6,o0c
36.000 GPD 34,000 GPD
Waste
Stormwater Treatment 7U001
Max'. 20.000 GPD Plant *l
Municipal
Water Supply
Blue River
D
30,000
GPDter
Washing
10 000
GI
GP
Atma
40,000
t
ductGPD
GPDWasTreatm
Outfall
002
50.000 GPD
Schematic of Water Flow
Brown Mills, Inc.
City, County, State
Figure 2C-1

EPA I.D. NUMBER (copyjro.1fe. l of Form 1) Form Approved.
OMB No. 2040-0086.
Please onnt or Noe in the unshaded areas only. Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLICATIOFOR PERMIT TO DISCHARGE WASTEWATER
A&EPA EXISTING MANUFACTURING,4COMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consohdated Permits Program
L OUTFALL LOCATION
For each ouffall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(hsO
B. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN,
3. SEC.
1. DEG,
2. MIN. 1
3. SEC,
001
36
14
40
80
50
22
Yadkin River
11. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A. Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and oultalls. If a water balance cannot be determined (e.g., for certain mining activifies), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each outfall, provide a description of: (1) Al operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets 'd
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (llst)
a. OPERATION (list)
to AVERAGE FLOW
(include units)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
See Figure 1-4
see Figure 1-5
OFFICIAL USE ONLY (efluenrguidelmessub-categories)
EPA Form 3510-2C (8-90) PAGE I of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (complete lhejollowing mhlO m NO (w in Secton 111)
3. FREQUENCY
4. FLOW
a- DAYS PER
B. TOTAL VOLUME
2. OPERATION(s)
WEEK
b. MONTHS
a. FLOWRATE(mmxf)
(+petty w,A ww")
1. LONG TERM
2. MAXIMUM
1. LONG TERM
2. MAXIMUM
C. DURATION
1. OUTFALL
CONTRIBUTING FLOW
(xpe h
PER YEAR
NUMBER(/irt)
(lie)
mremge)
6w+'eib"Re)
AVERAGE
DAILY
AVERAGE
DAILY
li"d'y+)
III. PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Actapply to yourfacility?
® YES (romplete Gem 1!l-H) ❑ NO (go m Secnon 10
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or othermeasure of operation)?
© YES (complete Gem 111-0 ❑ NO (go to Section 1P)
C. If you answered "yes" to Item III-B, list the quantity which represents an actual measurement of your level of production, elpressed in the terms and units used in the
applicable effluent guideline, and indicate the affected ouffalls.
1. AVERAGE DAILY PRODUCTION
2. AFFECTED OUTFALLS
(fiat rim/ ll number.,)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
c. OPERATION, PRODUCT, MATERIAL, ETC.
ON110y)
752
LbB/day
Subpart C- Low Water Use Processing
001
14,687
Lbs/day
Subpart D- Woven Fabric Finishing
001
Details provided in Appendix A.
Production numbers represent the highest operating
level values from years 2015, 2016, and 2017
IV. IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This Includes, but is not limited to,
permit conditions, administrative or enforcement orders, enforcement compliance schedule letters. stipulations, court orders, and grant or can conditions.
❑ YES (complete the Jnlbwmg mble) NO (go mGem 1V-8)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
a. NO
b. SOURCE OF DISCHARGE
a. REQUIRED
b, PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental prgecfs which may aRecf your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK'X' IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D. NUMBER (copyfroml:em ! oJFarm I)
CONTINUED FROM PAGE 2
V. INTAKE AND EFFLUENT CHARACTERISTICS
A, B, & C. See instructions before proceeding - Complete one set of tables for each ouffall -Annotate the ouffall number in the space provided.
NOTE: Tables V-A, V-B, and V-C am included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2o-3 of the instructions, which you know or have reason to believe is discharged or may be discharged
from any outrall. For every pollutant you list, briefly describe the reasons you believe it to be present and report any analytical data in your possession.
1.POLLUTANT
2. SOURCE
1 POLLUTANT
2. SOURCE
Acetaldehyde
These pollutants are found at
Formaldehyde
trace levels in some process
Propylene oxide
chemicals used in the
Styrene
manufacturing of textiles at
Vinyl Acetate
Duvaltex (US), Inc.
VI. POTENTIAL DISCHARGES NOT COVERED BY ANALYSIS
Is any pollutant listed in Item V-C a substance or a component of a substance which you currently use or manufacture as an intermediate or final product or byproduct?
® YES (liar all ouch pollulanra below ) ❑ NO (Aro ro lrem VI-B)
The following detectable pollutants are components of the fibers, dyes, and auxillary chemicals currently used
at Duvaltex (US), Inc. to manufacture textiles:
METALS, CYANIDE, & TOTAL PHENOL- Total Antimony, Total Arsenic, Total Chromium, Total Zinc, Total Cyanide,
Total Phenols, and Total Copper
GC/MS FRACTION- VOLATILE COMPOUNDS- Acrylonitrile
The following detectable pesticide pollutants have not definitively been determined to be compcnenrs cf
materials used to manufacture textiles:
GC/MS FRACTION -PESTICIDES- 4,4-DDD, Dieldrin, Endrin, Endrin aldehyde
Though non -detect in the 2017 Priority Pollutant Analysis, the following pollutants are believed present as
components of the fibers, dyes, and auxilary chemicals currently used at Duvaltex (US), Inc. to manufacture
textiles:
METALS,CYANIDE, & TOTAL PHENOL- Total Cadmium, Total Lead, Total Mercury (Prop65 threshold only), Total Nickel.
Total Silver
GS/MS FRACTION- VOLATILE COMPOUNDS- 1,1-Dichloroethylene, Ethylbenzene, Vinyl Chloride
GC/MS FRACTION- EASE/NEUTRAL COMPOUNDS- 1,2-Dichlorobenzene, Di-N-Butyl Phthalate, Hexachlorobenzene
EPA Form 3510-2C (8-90) PAGE 3 of CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
VIL BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
mYES (rd,.,,h the tear(*1 and descobe than p;op.,ei beta ) ❑ NO (g. to Section VlfO
As a condition of NPDES Permit N0005312, Duvaltex (US), Inc. is required to perform quarterly monitoring of
toxicity using teat procedures outlined in the permit (Ceriodaphnia Effluent Bioassay). Effluent sampling fov
this testing is performed at the NPDES permitted final discharge. The permit specified effluent concentration
at which there may be no observable inhibition of reproduction or significant mortality is 1.9t.
A summary table of chronic toxicity testing and attached reports for the 2017 calendar year are included in
Appendix S.
VIII. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V performed by a contract laboratory or consulting firm?
®YES Ow oh, name,address,and,,kph.. number ofandpallmamranalyzedhy. ❑NO(go toSeatonIX)
each .ouch laboratory orfirm below)
A. NAME
S.ADDRESS
C. TELEPHONE
D. POLLUTANTS ANALYZED
(area code & rw )
(8at)
Pace Analytical
9800 Eincey Avenue, Suite 100
[phone]
1) Priority pollutant
Huntersville, NO 28078
analysis;
2)Other sampling for
renewal: TOC, Color,
Ammonia (as N),
Nitrate -Nitrite, Oil 8
Grease;
3)Permit requirements: BOO,
COD, TSS, Sulfide.,
Phenols, Chromium, Fecal
Coliform, Total Nitrogen,
Total Phosphorous, Chronic
Toxicity, Total Lead, Total
Arsenic, Benzene,
Ethylbenzene, Chloroform
(See Appendicies C s D)
IX. CERTIFICATION
1 cedily underpenalty of low mat this document and all attachments were prepared under my arm bon or supervision in accordance with a system designed to assure that
qualified personnel properly gamer and evaluate the information submitted. Based on my inquiry of the person or persons who manage me system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true, accurate, and complete. I am aware mat mere
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (Ope or prom)
B. PHONE NO. (arse code & no.)
Scott Taylor- Environmental Coordinator
[phone]
C. SIGNATURE
D. DATE SIGNED
EPA Form 3510-2C (8-90) P 4v= 4 0' 4

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some or all of this information EPA I.D. NUMBER (coMjrom Item / ofForor /)
on separate sheets (use the some forman instead of completing these pages.
SEE INSTRUCTIONS.
OUTFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (continued eom page 3 of Form 2-C)
PARTA—You must provide the results of at least one analysis forevery pollutant in this table. Complete one table for each outsell. See instructions for additional details.
3. UNITS
4. INTAKE
2. EFFLUENT
(e cl r Alank)
(o I.1)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
e. LONG TERM
a. MAXIMUM DAILY VALUE
(ijwailahle)
(jowiluhk)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
if)
(1)
(1)
1. POLLUTANT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
(1) CONCENTRATION
2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Biochemical Oxygen
SEE
ATTACHED
DATA
SHEET IN
Demand(BOD)
b. Chemical Oxygen
SECTION
2
&
APPENDIX C
Demand (('OD)
c. Total Organic Carbon
( rX')
d. Total Suspended
Solids(I\%)
e. Ammonia lay M
VALUE
VALUE
VALUE
VALUE
I. Flow
g. Temperature
VALUE
VALUE
VALUE
,C
VALUE
(mmrrr)
R Temperature
VALUE
VALUE
VALUE
,C
VALUE
(summer)
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
i. pH
STANDARD UNITS
PART B — Mark -X' in column 2-a for each pollutant you know or have reason to believe is present Mark'X' in column 2-b for each pollutant you believe to be absent. If you mark column 2a for any pollutant which is limited either
directly, or indirectly but expressly, in an effluent limitations guideline, you must provide the results of at least one analysis for that pollutant. For other pollutants for which you mark column 2a, you must provide
quantitative data or an explanation of their presence in your discharge. Complete one table for each outfall. See the instructions for additional details and requirements.
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (npumwQ
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a.
b.
a. MAXIMUM DAILY VALUE
(JovailahleJ
(Jovaila510)
VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
(t)
(1)
(1)
(11
(i/arniloAle)
PRESENT
ASSENT
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
a. Bromide
(24959-57-9)
b. Chlorine. Total
Residual
c. Cola
d. Fecal Coldmm
e. Fluonde
(189844&e)
I. Nitrale-Nitme
(as M
EPA Form 3510-2C (8-90) PAGE V-1 CONTINUE ON REVERSE

ITEM V-B CONTINUED FROM FRONT
2. MARK'X"
3. EFFLUENT
4. UNITS
5. INTAKE (opamwl)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
C. LONGTERM AVRG. VALUE
a. LONG TERM
AND
a.
b.
a. MAXIMUM DAILY VALUE
Wmyn/oh/0
(Javellah/e)
AVERAGE VALUE
CAS NO.
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
It)
(1)
(tJarwNnnle)
PRESENT
ABSENT
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MASS
ANALYSES
TRATION
b.MASS
CONCENTRATION
(2)MASS
ANALYSES
g. Nitrogen,
Total Organic (m
N)
h. Oil and
Greece
I. Phosphorus
(as P), Total
(7723-140)
j. Radioactivity
(1) Alpha, Total
(2) Bela. Total
(3) Radium,
Total
(4) Radium 226,
Tale)
k. Sulfate
(a ,Wj
(14808-79-8)
1. Sulfide
(ay.S)
m. Sulfite
(ar ,SO,)
(14265-45-3)
n. Sudadants
o. Aluminum,
Tots
(7429-90-5)
p. Barium, Total
(7440.39-3)
q. Boron, Total
(7440.42-8)
r. Cobalt, Total
(7440-4B-Q
a. Iron, Total
(7439-89-6)
t. Magnesium.
Total
(7439-954)
u. Molybdenum,
Total
(7439-98-7)
v. Manganese,
Total
(7439-96.5)
w. Tin, Total
(7"0-31.5)
s. Titanium.
Told
9"0.32-6)
EPA Form 3510-2C (8-90) PAGE V-2 CONTINUE ON PAGE V-3

CONTINUED FROM PAGE 3 OF FORM 2-C I
fryEPA I.D. NUMBER (c.Jm r1rrm y oJFnrm l) OUTFALL NUMBER
PART C - If you are a primary industry and this outfall contains process wastewater, refer to Table 2c-2 in the instructions to determine which of the GC/MS fractions you must test for. Mark'X" in column 2-a for all such GC/MS
fractions that apply to your industry and for ALL toxic metals, cyanides, and total phenols. If you are not required to mark column 2-a (secondary industries, nonprocess wastewater outlets, and nonrequired CCMIS
fractions). mark'X' in column 2-b for each pollutant you know or have reason to believe is present. Mark'X' in column 2-c for each pollutant you believe is absent. If you mark column 2a for any pollutant, you must
provide the results of at least one analysis for that pollutant. If you mark column 21h for any pollutant, you must provide the results of at least one analysis for that pollutant 8 you know or have reason to believe it will be
discharged in concentrations of 10 ppb or greater. If you mark column 2b for acmlein. acrylombile, 2,4 dinitrophenol, or 2-methy14, 6 dinitrophenol, you must provide the results of at least one analysis for each of these
pollutants which you know or have reason to believe that you discharge in concentrations of 100 ppb or greater. Otherwise, for pollutants for which you mark column 2b, you must either submit at least one analysis or
briefly describe the reasons the pollutant is expected to be discharged. Note that mere are 7 pages to this part; please review each carefully. Complete one table (all 7 pages) for each outfall. See instructions for
additional details and requirements.
2. MARK'X'
3. EFFLUENT
4. UNITS
S. INTAKE (.prim./)
1. POLLUTANT
b. MAXIMUM 30 DAV VALUE FF
c. LONG TERM AVRG.
a. LONG TERM
AND
a. MAXIMUM DAILY VALUE
I VALUE (J.�miloAle)
AVERAGE VALUE
CAS NUMBER
TESTING I
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
pJ.v.rl.Ale)
REQUIRED
PRESEN7
ABSENT
CONCENTRATION
(2 MASS
CONCENTRATION
(2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
ANALYSES
METALS, CYANIDE, AND TOTAL PHENOLS
1M. Antimony, Told
(7440-38-0)
2M. Arsenic, Total
(7440-38 2)
3M. Beryllium, Total
(744"1 7)
4M. Cadmium, Total
(7440-43-9)
5M. Chromium,
Told (744047-3)
6M. Copper. Total
(7440-50-8)
7M. Lead, Total
(7439-92-1)
8M. Mercury, Total
(7439-97-6)
9M. Nickel, Total
(7440-02-0)
tOM. Selenium,
Told (778249-2)
11 M. Silver, Total
(7440-224)
12M. Thallium,
Total (7440-28-0)
13M. Zinc, Total
(7440-66-6)
14M. Cyanide,
Total(57-12-5)
15M. Phenols,
Total
DIOXIN
2,3,7,8-TWm-
DESCRIBE RESULTS
chlorodlbenzo-P-
Dioxln (1764-01-6)
EPA Form 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK X'
3. EFFLUENT
4. UNITS
5. INTAKE (ophneal)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
c
a. MAXIMUM DAILY VALUE
(J'awiloAle)
VALUE (Jawilah/r)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
It)
(rJuwilah/e)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2) MASS
CONCENTRATION
2) MASS
CONCENTRATION
(2) MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(21 MASS
NALYSES
GC/MS FRACTION —VOLATILE COMPOUNDS
IV. Accrolein
(107-02-8)
2V. Acrybnibile
(107-13-1)
3V. Benzene
(7143-2)
4V. Bra
mnhy0 Ether
(542-86-1)
5V. Bromoform
(75-25-2)
BV. Carbon
Tetrachloride
(5&23.5)
7V. Chlorobenzene
(108-90-7)
8V. Chlorodi-
bromomethane
(124.48-1)
9V. Chlo thane
(75-0&3)
10V. 2-Chloro-
ethylyinyl Ether
(110-75-8)
11V. Chloroform
(67-66-3)
12V. Dichloro-
b ,rt methane
(75-274)
13V. Dlchloro-
diBuoromethane
(75-71.8)
14V. L1-Ditltloro-
ethane (75-34-3)
15V. 1,2-Dichloro-
ethane (107-06-2)
16V. 1,1-Dichloro-
ethylene (7&354)
17V. 1,2-Dichloro-
propane (78-87-5)
19V. 1,3Dirhloro-
propylene
(542-75-6)
19V. Ethylbenzene
(10041-4)
20V. Methyl
Bmmide (74-83-9)
21V. Methyl
Chloride (74-87-3)
EPA Form 351G-2C (8-90) PAGE V-4 CONTINUE ON PAGE V-5

CONTINUED FROM PAGE V-4
2. MARK"X"
3. EFFLUENT
4. UNITS
S. INTAKE (aprinnun
I.POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a
b
e
a. MAXIMUM DAILY VALUE
(rJuvallahle)
VALUE (rjuuai/nA/e)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
(1)
(1)
(1)
(juvnduAle)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MASS
ANALYSES
TRATION
b. MASS
CONCEMRATION
(2)MASS
NALYSES
GC/MS FRACTION — VOLATILE COMPOUNDS (cnnnnuerQ
22V. Methylene
Chlotltle (75.09-2)
23V. 1,1,2,2-
Telrachb thane
79-34-5
24V. Tetreclaoro-
ethylene(127-18.4)
25V. Tduane
(108-88-3)
26V. 1.2-Trens-
Dichloroelhylene
5650.5
27V. 1.1,1-Tanhloro-
ethane (71-55-6)
2BV. 1,1,2-Tnch ono
ethane (79-00-5)
29V Tnchloro-
ethylene (79-0")
30V. Tnchloro-
Bucromethane
755&4
31V. Vinyl Chlonae
(75-014)
GC/MS FRACTION — ACID COMPOUNDS
IA. 2-Chlarophend
(9557-8)
2A. 2,4-Dichlao-
phenol (120-83-2)
3A. 2,4-Dimetllyl-
phencl(105.67-9)
4A. 4,6-DinitroO-
Cresd(534-52-1)
5A. 2,LDinitro-
phend (51-28-5)
6A.2-Nitrophend
(88-75-5)
7A. 4Nltrophenol
(100-02-7)
BA. P-Chlo M-
Cresd(59-50-7)
9A. Panladllono-
phenol (8756.5)
10A. Phenol
(109-95-2)
11A. 2,4,6-Tnchloro-
phend (8,05.2)
EPA Fomn 3510-2C (8-90) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK'X'
3. EFFLUENT
4, UNITS
5. INTAKE („pn,.onl)
1 POLLUTANT
b. MAXIMUM 30 DAV VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
a.
b.
e.
a. MAXIMUM DAILY VALUE
(r{onnr/nhlr)
VALUE (Ijnrorluhle)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
pl
(U
111
(J erndohle)
REQUIRED
PRESENT
ABSENT
CONCENTRgT10N
(2)MA55
CONCENTRATION
121 MASS
CONCENTRATION
(2)MASS
ANALYSES
TRATION
b. MA55
CONCENTRATION 1
(2)MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS
18. Acenaphthene
(8332-9)
2B. Acenaphtylene
(208-96-8)
3B. Anthracene
(120-12 7)
48. Benzidine
(92-87-5)
SB. Banzo W)
Anthracene
(56-55 3)
6B. Benzo (a)
Pyrene(50-32-8)
7B.3A Benzo-
6uoranlhene
120599-2)
8B. Banzo (¢/u)
Perylene(191-24-2)
9B. Benzo (k)
Fluoranlhene
(207-08-9)
10B. Bis (1-<'Irinro-
erh,.s0 Methane
(111-91 1)
11 B- Bis (-'-('id.....
rrhr0 Ether
(111-44-4)
128. Bis (1-
rnn.rv,r.„P,,./,rq
Ellie, 002-80-1)
13B. Bis (2-Ehrl-
he.oi) Phthalate
(117-81-7)
14B. 4-Bromophenyl
Phenyl Ether
(101-55-3)
158. Butyl Ber l
Phthalate(85.68-7)
16B 2-Chloro-
naphthalene
(91-58-7)
17B. 4Chlcro-
phenyl Phenyl Ether
(7005 72-3)
18B. Chrysene
(218 01-9)
19B. Dibenzc (u.h)
Anthracene
(53 763)
208. 1,2-Dichloro-
benzene(95-50- 1)
21B. 1,3Di-chloro-
benzene (541-73-1)
EPA Form 3510-2C (8-90) PAGE V-6 CONTINUE ON PAGE V-7

CONTINUED FROM PAGE V-6
2. MARK'%'
3. EFFLUENT
4. UNITS
5. INTAKE( opuunol)
1. POLLUTANT
to MAXIMUM 30 DAY VALUE
C. LONG TERM AVRG
I
a. LONGTERM
AND
a
p
c
a. MAXIMUM DAILY VALUE
(il nvnduhle)
VALUE (/moduhlr)
I
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d.NO.OF
a-CONCEN-
b.NO. OF
(1)
ry)
(t7
ry)
(i/mm/oM1lr)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MASS
CONCENTRATION
(2)MAS6
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2)MASS
ANALYSES
GCIMS FRACTION— BASE/NEUTRAL COMPOUNDS (rnnnnumQ
22B. 1,4-Dichloro-
benzene(106-46-7)
23B. 33-Dichloro-
benzidine(91-94- 1)
24B. Diethyl
Phthalate (84-66-2)
25B. Dahelhyl
Phthalate
(131 -11-3)
26B. Di-N-Butyl
Phthalate (13474-2)
27B. 2.4-Dinitro-
toluene (121-14-2)
288. 2.6 Duutro-
toluene (606-20-2)
298, DI-N-Odyl
Phthalate (117-84-0)
30B. 1.2-Diphenyl-
hydrazine (as Azo-
benzene) (122-M 7)
31B. Fluoranthene
(206-44-0)
32B. Fluorene
(86-7g 7)
338. Hexachloro-
benzene(119-74-1)
34B. Hexachloro-
butadiene (87-68-3)
35B. Hexachloro-
cyclopentadiene
(77-47-4)
36B Hexachloro-
ethane(67-72-1)
37B.Indeno
(1,2,3-cd) Pyrene
(193-39-5)
38B. Isophorone
(78-59-1)
39B. Naphthalene
(91-2P3)
40B. NItrobenzene
(98-95-3)
41B. N-Nitro-
sodlmethylamine
(62 75-9)
42B. N-Nitrosodi-
N-Propylamine
(621-64-7)
EPA Form 3510-2C (8-90) PAGE V-7 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE (,,pnoval)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONGTERM
AND
a
b
a
a. MAXIMUM DAILY VALUE
Ql nvurlohlr)
VALUE (r/mvrJnhlr)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
b. NO. OF
(1)
ry)
(1)
(1)
(JuonduM1lr)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
(2)MA55
CONCENTRATION
(2)MA55
CONCENTRATION
(2)MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2)MASS
ANALYSES
GC/MS FRACTION — BASE/NEUTRAL COMPOUNDS (. .umnur.Q
438. NWVo-
sodiphenylamine
(96-30-6)
44B. Phenanthrene
(85-01-B)
458. Pyrene
(12f-00-0)
46B. 12,4-Tn-
chlurobeniene
(120-82-1)
GC/MS FRACTION — PESTICIDES
1P. Aldrin
(309-00-2)
2P a-BHC
(349-84-6)
3P. p BHC
(319-85-7)
4P y-BHC
(58-89-9)
5P b-BHC
(319-86-8)
6P. Chlordane
(57-749)
7P. 4.4'-DDT
(50-29-3)
BP. 4.4'-DDE
(72-55 9)
9P. 4,4'-DDD
(72-54-8)
10P. Dieldon
(60-57-1)
11P. a-Enosulfan
(11529-7)
12P. aEndosulfan
(115-29-7)
13P. Endosolfan
Sulfate
(1031-07-6)
14P. Endnn
(72-20-8)
15P. Endnn
Aldehyde
(7421-93-4)
16P Heptachlor
76-44-8)
EPA Form 3510-2C (8-90) PAGE V-8 CONTINUE ON PAGE V-9

CONTINUED FROM PAGE V-8 I
EPA I.D. NUMBER (enpyfrv+m/mm / ojFnrm /) OUTFACE NUMBER
2. MARK"X"
3. EFFLUENT
4. UNITS
S. INTAKE (oprionan
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
I
a. LONG TERM
AND
e
p
c
a. MAXIMUM DAILY VALUE
(/avadahle)
I VALUE (J'andaelr)
AVERAGE VALUE
CAS NUMBER
TESTING
BELIEVED
BELIEVED
d. NO. OF
a. CONCEN-
h. NO. OF
(1)
(1)
(1)
B)
(If v., aAle)
REQUIRED
PRESENT
ABSENT
CONCENTRATION
2) MASS
CONCENTRATION
2) MASS
CONCENTRATION
2) MAS$
ANALYSES
TRATION
b. MASS
CONCENTRATION
2) MASS
ANALYSES
GC/MS FRACTION — PESTICIDES (unmmued)
17P. Heptachlor
Epodde
(1024-57-3)
18P. PCB-1242
(5346&21-9)
19P. PCB-1254
(11097-WI)
20P. PCB-1221
(11104-28-2)
21P. PCB-1232
(11141-16-5)
22P. PCB-1248
(12672-29-6)
23P. PCB-1280
(1109&82-5)
24P. PCB-1016
(I2674T1-2)
25P. To�phene
(8001-3&2)
EPA Fotm 3510-2C (8-90) PAGE V-9

EPA 10 #NC0005312 OUTFALL # oot
PART
2. EFFLUENT
DAILY VALUE b. MAXIMUM 30 DAY VALUE savailabb c. LONG TERM AVERAGE VALUE Bavailable
tl. No, of
MASS b/da (m9Al MASS b/d CONCENTRATION(m9/L) MASS (lb/day) Are ses
3. UNITS
4. INTAKE(optional)
CONCENTRATION
MASS
a. LONGTERM AVERAGE
VALUE
MASS Ib/da
d. No. of
Ana ses
1. POLLUTANT
CONCENTRATION L
SOD
COD
T
T S
Ammon as N
Flaw
Tem eratura vAmer
Temperature summer
H
36.219
340.940
15.011
M243431.873
0
7535
2.5
283
7.02 Mnimum 7.59 Meamum
16.8 36.219
137 340.940
33.7 15.011
243 I31.873
N 0
047535
22.5
1 26.3
7.,A Minimum 1,59(Maximum)
6.368
4.303
249
m
Ibs
NA
NA
NA
101.5
68.704
49
m L
Ibs
NA
NA
NA
33,7
38.537
15.011
26041
1
249
m /L
L
lb.
NA
NA
NA
NA
Ibs
NA
NA
ND
0
1
m M1
Ibs
NA
NA
NA
0.080408476
365
NA
M 0
NA
NA
NA
168 122I
1 24.6 126
246
NA
NA
NA
'C1
1 Slartlard Units
NA
NA
NA
NA
NA
NA
ITEM V
PART B
2. MARK'X"
3, EFFLUENT
4. UNITS
5. INTAKE
tional
a. BELIEVED PRESENT
Is BELIEVED
ABSENT
a. MAXIMUM
DAILY VALUE
b. MAXIMUM 30 DAY
VALUE 9 avaitaNe
c. LONG TERM AVERAGE
VALUE 8 available
CONCENTRATION
MASS
a. LONGTERM AVERAGE
VALUE
MASS (III
d. No. or
Analyses
available)
(mg L)
MASS W
(m9A)
MASS b/
CONCENTRATION (mI
MASS (b/day)
d. Noof
Analyses
CONCENTRATION l-
Bromide 24959-67-9
X
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
CNorine. Total Residual
X
<25
0
Q5
0
QS
0
248
Ibs
NA
NA
NA
Color
X
NO ADMI Units
0
NO ADMI UNM
0
NO ADMI Units
0
1
ADMI Units
NC
NA
NA
NA
Fecal CaNarm
X
23 P/100mi-
NC
23 01100m1.
NC
125 Pn00mL
NC
24
a/ 100m1
NC
NA
NA
NA
Fkforkle 16984-48-6)
X
0.14
0.129
0.14
0.129
0.14
0.129
1
mgfL
Its
NA
NA
NA
Ndrate-NI le (as N)
X
092
0.849
0.92
0.849
0.92
0.849
1
m /L
Ibs
NA
NA
NA
Nor en. Total Or anc as N
X
3.2
6.746
3.2
6. 48
3.
2.43
15
m
Ibs
NA
NA
NA
01 arid Grease
X
NO
0
NO
0
NO
0
1
m
Its
NA
NA
NA
Pbos s as P 772314-0
X
2.8
8 095
2 8
8.095
28
2.153
12
MI
bs
NA
NA
NA
Radioact
. Total
X
NA
NA
NA
I NA
NA
NA
0
NA
NA
NA
NA
NA
Bela, Total
x
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
Radium, Total
z
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
Radium 226. Total
x
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
SuBate (as SO4) (14808-79-8)
X
27.1
25.022
28.8
26.592
28.8
26.592
1
m9ri
UPS
NA
NA
NA
Sulfide asS
X
0.11
0.254
0.11
0.254
OAB
0,170
24
mgk
bs
NA
NA
NA
Suite (as SO,) (14265-45-3)
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
Surfactems
X
0.18
0,081
0.18
0.081
0.18
0.081
1
NA
NA
NA
NA
NA
Aluminum, Total 7429-90-56
X
0.116
0.107
0.116
0.107
0.116
0.107
1
mgdL
Ibs
NA
I NA
Badum, Total 7440-39.3
X
0.0106
0.010
0.0106
0.010
0.0106
0.010
1
M91L
lb.
NA
NA
NA
Boma. Total 7440-42-8
NO
0
NO
0
ND
0
1
m
His
NA
NA
NA
Cobalt Total (74404")
NO
0
NO
0
NO
0
1
NA
NA
NA
NA
NA
Iran, Total 743989E
X
0. D904
0.083
0.45
1 0415
0.45
0415
1
mg/L.
Ibs
NA
NA
NA
Ma rles.. Total 7439-95-4
X
2,61
2410
2.23
1 2058
2.23
2.059
1
m A
NA
NA
NA
NA
Mo enum. TOW 7439-987
NA
NA
NA
NA
NA
NA
0
NA
NA
NA
NA
NA
Ma anese, Total 439955
X
0.0056
DI
00143
I Milli
0.0143
0.013
/
m
His
NA
NA
NA
Tin, Total 7440-31-5
NA
NA
NA
I NA
NA
NA
0
NA
NA
NA
NA
NA
TA.., Total 7440-32-6
X
NO
ND
0
NO
0
1
m 2
Ibs
NA
NA
NA
ITEM V
PART C
2. MARK'%'
3. EFFLUENT
4. UNITS
5 INTAKE(optional)
a. TESTING
REOUIRED
b. BELIEVED
PRESENT
c. BELIEVED
ABSENT
a, MAXIMUM DAILY VALUE
b. MAXIMUM 30 DAY VALUE isavailebb
c. LONGTERM AVERAGE VALUE If avalable
CONCENTRATION
MASS
a. LONG TERM AVERAGE VALUE
tl. No. of
Analyses
available)
(m0A) MASS (b/dayl
(m9l7MASS (b/ )
CONCENTRATION (m0/y MASS (b/day)
d. No. of
Analyses
CONCENTRATION ( L) MASS (Ib/dayl)
METALS. CYANIDE, AND TOTAL PHENOLS
Anturforry, Total 441 .3 O
X
X
0.496
0,224
0496
0,224
0,496
D.224
1
m
bs
NA
NA
NA
A afvc, Total 744038-2
X
X
NO
0
NO
0
NO
0
1
Its
NA
NA
NA
Beryllium, Total 7N0-41-7
X
NO
0
NO
0
NO
0
/
m A
Ibs
NA
NA
NA
Cadmiun, Total 7440-4 9
X
X
NO
0
NO
0
NO
0
1
m /L
Ibs
NA
NA
NA
Cbromsm, Total 440-47-3
X
X
0.026
0,089
0.026
0,009
0,0253
0.016
25
all
Ibs
NA
NA
NA
C er. Total 1440.598
X
X
0,014
0.013
0 014
0.013
0.014
0. 13
/
m /L
to.
NA
NA
NA
Lead, Total 743992-1
X
%
NO
0
NO
0
NO
0
1
m /L
lb.
NA
NA
NA
Mercury. Total 43997E
X
NO
NO
0
NO
0
1
m /L
Ibs
NA
NA
NA
Nickel, Total 740-02.0
%
X
NO
NO
NO
0
1
m
Ibs
NA
NA
NA
Selenium. Tot& 782-492
%
NO
a
NO
0
NO
0
1
m
Ibis
NA
NA
NA
Sher. Total 7H02&0
%
NO
0
ND
0
NO
0
1
m
Ibs
NA
NA
NA
TOaeium. Total 7440- A
%
X
ND
0
NO
0
ND
0
1
m
Ibs
NA
NA
NA
Zinc. Total 7440.6&8
%
X
NO
0
NO
0
NO
0
1
m 2
lb!
NA
NA
NA
C nide. Total 57-12-5
X
X
NO
0
ND
0
N
0
1
m
lbs
NA
NA
NA
PMnols, Total
%
X
0.02d
0.041
0.024
0.016
0.013
25
m A
Ibs
NA
NA
NA
DIOXIN
2.3 7e ra ro 1 Ko- - >on
(1764-01E)
NA
"
DESCRIBE RESULTS (lissfing Muirements waived)
GC/MS FRACTION - VOLATILE COMPOUNDS
Ataalein 107-02-8
X
NO
0
-
N
I 0
Ibs
NA
NA
NA
Mass 107-13-1
X
X
NO
0
NO
Ibs
I NA
NA
I NA
Bervnne 171J 2
X
I
NO
1 0
-
NO
0
P91L
I Ibs
I NA
NA
I NA
rs me
X
I
I
I NA
I NA
NA
NA
/L
I Ibs
I NA
NA
NA

Bmmoform 75-25-2)
X
X
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
Carbon TetracNor 5&215)
X
X
NO
0
NO
0
NO
0
1
L
Ibs
NA
NA
NA
Chlorobenzene 1015-90-7
X
ND
0
NO
0
ND
0
1
Ibs
NA
NA
NA
Chbrodbromomebane 12418.1
X
X
ND
0
NO
0
ND
0
1
/L
Ibs
NA
NA
NA
Chbroeltuw Ii0&J
X
NO
0
NO
0
NO
0
1
/L
—lb,
NA
NA
NA
2-Chbm-e1 v' Ether 110.75-8
X
ND
0
NO
0
ND
0
1
9/L
Ibs
NA
NA
NA
Chbroform 6766-3
X
%
ND
0
NO
0
ND
0
1
/L
bs
NA
NA
NA
DM robromomebaw 5-27-4
%
X
ND
0
ND
0
NO
0
1
WL
Ibs
NA
NA
NA
DicNom ftorometl i71b
x
X
NO
0
NO
0
ND
0
1
Pak
Ibs
NA
NA
NA
1. 1-Dkhbrcethane 7iJ43
x
X
NO
0
NO
0
NO
0
1
bs
NA
NA
NA
1.2-Dkhbrcelhace 1W-0&2
x
%
NO
0
N
0
ND
0
1
PQ&
bs
NA
NA
NA
1. 1-DiGWroP ew 7i35.4
%
X
NO
0
NO
0
NO
0
1
2
Ibs
NA
NA
NA
L 2-Dichbro ro ane 7&a7-5
%
X
NO
0
NO
0
NO
0
1
0.
Ibs
NA
NA
NA
.. 3-Dichbro ro we 542-75-6
X
X
NO
0
ND
0
NO
0
I
/L
Ibs
NA
NA
NA
E Demme 100-41-1
x
X
NO
0
ND
0
NO
0
PQIL
Ibs
NA
NA
NA
Meb Bromide 483-9
x
X
NO
0
ND
0
ND
0
1
Ibs
NA
NA
NA
Meth CNontle 7481-3
%
X
NO
0
0
ND
0
1
2
Ibs
NA
NA
NA
MmylemC nae 17S0 2
x
X
NO
0
NI
0
ND
0
1
pqIL
Ibs
NA
NA
NA
I L 2.2-TetraWoroethana 7&34-5
x
NO
0
NO
0
ND
0
1
Ibs
NA
NA
A
TetrwNbroeb ene 127-18-0
x
X
NO
0
ND
0
NO
0
1
p
Ibs
NA
NA
NA
To)uene 10&8&3)
x
X
N
0
NO
0
7
Ibs
NA
NA
NA
2 ^❑ichloroel ene I56-W5)
x
X
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
�niometharle 71-55-6
x
NO
4D
0
NO
0
1
Ibs
NA
NA
NA
-. hloroebare 79.00-5
X
X
NO
0
NO
NO
0
1
A
Ibs
NA
NA
NA
+"th bro 79-01-6
x
X
N
0
ND
0
NO
0
1
A
Ibs
I NA
I NA
NA
c,.oromeNare 71694
x
X
I NO
0
ND
1 0
NO
0
1 1
pg0.
I Ibs
I NA
I NA
NA
vm l Chlorde 75-014
X
%
I ND
0
NO
1 0
ND
0
I 1
PgA
I Ibs
I NA
I NA
i NA
GCIMS FRACTION - ACID COMPOUNDS
2-Chbm wl 95-5741
X
ND
0
NO
0
0
1
Ibs
NA
NA
NA
2.4Dk howl 12&83.2
x
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
2. 4Dimet hand 105-67-9
X
ND
0
NO
0
NO
0
1
/L
bs
NA
NA
NA
4, &Obem-O-Cresol 53452-1
x
NO
0
NO
0
NO
0
1
lb.
NA
NA
NA
2.4-Dkdm howl 51-28-5
x
NO
0
N':
0
NO
0
1
IL
Ibs
NA
NA
NA
2-Ni4 bawl 8&7&5
ix
NO
0
N
0
NO
0
1
Ibs
NA
NA
NA
4Nitr henol 10&02-7
ND
0
Nn
0
NO
0
i
lb.
NA
NA
NA
P-Chbro-M-Cresol 59-50-7
x
ND
0
ND
0
NO
0
1
Ibs
NA
NA
NA
Pe Woro henol 87-0&5
x
ND
0
NO
0
NO
0
1
Ibs
NA
NA
NA
Phenol (108-9i2
X
ND
0
NO
0
NO
0
1
bs
NA
NA
NA
2. 4,'-TrkMomphenol 88-05-2
e9t,U
%
NO
0
NO
0
ND
0
- 1
Ibs
NA
NA
NA
DCIMSFRACTION- I"RAL UUMPWNDS
Acena hb m 83-32-9
%
NO
0
NO
0
NO
0
1
bs
NA
NA
NA
Ape a h ne 20&9&8
X
NO
0
NO
0
NO
0
i
bs
NA
NA
NA
AntNace 120-12-7
X
NO
0
ND
0
NO
0
/
Ibs
NA
NA
NA
BeF74M 92A7-5
X
NO
0
ND
0
ND
0
/
Ibs
NA
NA
NA
emo a racene
X
NO
0
NO
0
NO
0
1
/L
lb.
NA
NA
NA
e 0 a ro
X
NX
NO
0
ND
0
NO
0
1
/L
Ibs
NA
NA
NA
3. 48eraoi ranbene 205-99-2
X
NO
0
ND
0
NO
0
1
Ibs
NA
NA
NA
emo 9 r e—
X
NO
0
NO
0
ND
0
1
/L
Ibs
NA
NA
NA
enzo ran ace
X
NO
0
ND
0
ND
0
1
Ibs
NA
NA
NA
Bia 2-Chbro-e1 Methane 111-91-1
X
ND
0
NO
0
NO
0
1
Ibs
is - om-e y er
X
NO
0
ND
0
ND
0
1
RGIL
bs
NA
NA
NA
s- omisopmpY m
x
x
ND
0
NO
0
ND
0
1
pQlL
Ibs
NA
NA
NA
R - y- exy a
x
%
NO
0
NO
0
ND
0
1
L
Ibs
NA
NA
NA
4Bremo hen Phenyl Elver 101-55-3
X
X
ND
0
ND
a
ND
0
1
pgk
bs
NA
NA
Nn
Butyl Benzyl Phthalate 85-68-7
%
%
NO
0
NO
0
ND
0
1
Ibs
NA
NA
NA
2-CNbrmne hthalene 91-5&7
X
X
NO
0
NO
0
1
Ibs
NA
NA
NA
4-CM Phen Ether lw0 12-3
X
NO
0
0
NO
0
1
bs
NA
NA
NA
ene 216-01-4
x
X
ND
0
NO
0
NO
0
t
Y9JL
Ibs
NA
NA
NA
OlimZoI- racewixw=
X
ND
0
NO
NO
0
1
PgA
Ibs
NA
NA
NA
1.2-DkNbmbemene 9i50-1
%
X
ND
0
NO
0
NO
0
1
PgA
Ibs
NA
NA
NA
1.3-Dichloroben " 541-]31
X
X
NO
0
NO
0
NO
0
f
bs
NA
NA
NA
1 40M71brobarizace 106-4&7
X
X
ND
0
NO
0
NO
0
1
Ibs
NA
NA
NA
3.3-DkMoroDenzidine 91-941
X
X
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
D Phlhalab 846&2
X
%
NO
0
NO
0
NO
0
1
IL
Ibs
NA
NA
NA
DMne Phtha2e, 1J1-11-3
%
X
NO
0
NO
0
NO
0
1
bs
NA
NA
NA
Di-N-Bu PMhelale 84742
X
NO
0
NO
0
NO
0
1
bs
NA
NA
NA
2.4Dinotmblwft 121-142
X
X
ND
0
NO
0
NO
0
1
2
Ibs
NA
NA
NA
2. &Dinamtobena 60&2&2
X
X
NO
0
N
0
NO
0
1
Ibs
NA
NA
NA
Di-N-Oct PhBaWe 117-840
%
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
p ro as
Ambenx )(122-6&7)
X
X
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
T06440
%
%
NO
0
ND
0
NO
0
1
Ibs
NA
NA
NA
Flwrece 8&73.7
X
NO
0
ND
0
ND
0
1
Ibs
NA
NA
NA
VFlwranlhane
H�,xachlorobemene 11&741
%
X
NO
0
ND
0
NO
0
1
Ibs
NA
NA
NA
xachlo,.Wtad.Em 8758-3
%
X
NO
0
NO
0
ND
0
1
Ibs
NA
NA
NA
!,W a ntatlieoe 11414
%
X
NO
0
ND
0
ND
0
1
Ibs
NA
NA
NA
exachbroetl we 67-72-1
%
I
I %
I ND
0
NO
0
I NO
0
1
1 P91L
bs
NA
NA
I NA

ergo
X
X
NO
0
NO
0
NO
0
1
IL
Ibs
NA
NA
NA
Is om(7&59-1)
X
X
NO
0
NO
0
ND
0
1
IL
Ibs
NA
NA
NA
Naph lene 91-20-3
%
X
NO
0
NO
0
ND
0
1
/L
Ibs
NA
NA
NA
Nlmbemem (9&9&3)
X
X
NO
0
NO
0
NO
0
1
PQ&
Ibs
NA
NA
NA
N-Ndms Ime mina 62-75-9
X
X
NO
0
NO
0
ND
0
1
PgA
Ibs
NA
NA
NA
N-N6msodLN-Pro miIv 621.84-7
X
NO
0
ND
0
ND
0
1
PWL
Ibs
NA
NA
NA
N-Nitmsadphe mine 86-30-6
X
X
NO
0
NO
0
NO
0
7
P91L
Ibs
NA
NA
NA
Phemnthrem 85-0141
%
%
NO
0
NO
0
ND
0
1
yg&
Ibs
NA
NA
NA
P m(129-MO)
%
X
NO
0
ND
0
NO
0
i
P91L
Ibs
NA
NA
NA
1, 2. 4-TriGdorobemaae 12 -82-1
X
X
NO
0
NO
0
NO
0
1
Ibs
NA
NA
NA
GC/MsFRACTION - PE TI IDE
Aldrin 309-00-2)x
NO
0
NO
ND
0
1
L
Ibs
NA
NA
NA
o-
X
NO
0
ND
0
ND
0
1
Ibs
NA
NA
NA
HC 379-85-7
X
NO
ND
0
NO
0
1
L
Ibs
NA
NA
NA
Y-
NO
ND
0
ND
0
i
Ibs
NA
NA
A
%
ND
0
NO
0
NO
0
1
/L
Ibs
NA
NA
NA
CtJordem 57-749
X
RX
NO
0
0
NO
0
1
/L
lb.
NA
NA
NA
x
NO
0
ND
0
NO
0
1
L
Ibs
NA
NA
NA
%
NO
0
N
0
NO
0
1
L
Ibs
NA
NA
NA
X
%
NO
0
0
NO
0
1
/L
Ibs
NA
NA
NA
Dieldnn(60-57-1)
%
X
NO
0
NO
0
ND
0
1
/L
Ibs
NA
NA
NA
o-Emsufen 115-29-7
%
NO
0
ND
0
NO
0
7
L
Ibs
NA
NA
NA
EM ndf.n 115-M7
x
I
X
NO
0
NO
0
NO
0
1
pglL
Ibs
NA
NA
NA
Endosudan Sulfate 1031-07-8
X
%
NO
0
NO
0
NO
0
1
/L
Ibs
NA
NA
NA
Enddn 72-20-8
x
X
NO
0
NO
0
ND
0
1
Ibs
NA
NA
NA
Ergdn Aldo a 7421-93-4
x
X
NO
0
NO
0
ND
0
1
ligiL
Ibs
NA
NA
He tachlor &448
x
%
NO
0
NO
0
ND
0
1
/L
Ibs
NA
NA
Ha ladIlor a odda 102457-3
X
X
NO
0
NO
0
NO
0
1
/L
Ibs
NA
NA
�NtA
Tama
hem 8001-35-2
X
X
NO
0
NO
0
NO
V91L
Ibs
NA
NA
NA
GC S FRACTION
- PCBs
PCB-1242 53469.21-9
X
I
X
NO
0
1 NO
1 0
1 NO
1 0
1 1
1 PgA
Ibs
NA
NA
NA
PCB-1254 11097-69-1
X
X
NO
0
N
0
NO
0
1
Ibs
NA
NA
NA
PCB-1221 1110428-2
X
X
NO
0
NO
0
NO
0
/
7L
Ibs
NA
NA
NA
PM1232 11141465
%
X
NO
0
ND
0
NO
0
1
/L
Ibs
NA
NA
NA
PC&1248 12672-2941
X
%
ND
0
NO
0
NO
0
1
Ibs
NA
NA
NA
PC&1260 11098-02-5
%
%
NO
0
No
0
NO
0
1
Ibs
NA
NA
NA
PCB-10/6 1267411-2
%
%
NO
0
NO
0
ND
0
1
Ibs
NA
NA
NA

Duvaltex (US), Inc. VWVTP Totals
2017
Average
Maximum
#of
BOD
Lb/Day
Flow MGD
m /L
Lb/Day
Flow (MGD)
m /L
Analysis
Jan
2.20049
0.07027
3.75500
15.98380
0.30421
6,30000
20
Feb
2.26583
0.06154
4.41500
14.86069
0.23141
7.70000
20
Mar
2.38188
0.06927
4.12273
19.64946
0,31414
7.50000
22
Apr
3.43093
0A0008
4.11053
20.56580
0.27707
8.90000
19
May
3.75157
0.10699
4.20455
27.75093
0.47535
7.00000
22
Jun
1.80802
0.05305
4.08636
7.57644
0.11798
7.70000
22
Jul
1.66079
0.06671
2.98500
7.12463
0.18176
4.70000
Aug
1.37323
0.08607
1.91304
10.61649
0.28288
4.50000
Sep
1.86472
0.09126
2.45000
13.27316
0.25262
6.30000
Oct
1.61111
0.09922
1.99545
14.93554
0.37309
4S0000
d22
Nov
3.00420
0.077384.65500
36,21895
0.25850
16.80000
Dec
4.30336
0.08102
6.36842
26.65881
0.21310
15.00000
MAX 4.30336
6.36842 36.21995
16.80000 249
2017
Average
Maximum
# of
COD
LbIDay
Flow (MGD)
m L
Lb/Day
Flow (MGD)
mg1L
Analysis
Jan
45.41630
0.07027
77.50000
253.71114
0.30421
100.00000
4
Feb
52.09090
0,06154
101.50000
264.40444
0.23141
137.00000
4
Mar
46.21957
0.06927
80.00000
238.41341
0.31414
91.00000
4
Apr
61.97425
0.10008
74.25000
205.65798
0.27707
99.00000
4
May
68.70448
0.10699
77.00000
340.94003
0.47535
86.00000
5
Jun
41.81161
0.05305
94.50000
124.96206
0.11798
127.00000
4
Jul
53.55134
0.06671
96.25000
168.26250
0.18176
111.D0000
4
Aug
60.15386
0.08607
83.80000
219.40739
0.28288
93.00000
5
Sep
57.65417
0.09126
75.75000
233.86044
0.25262
111.00000
4
Oct
55.27504
0.09922
66.80000
304.93392
0.37309
98.00000
5
Nov
50.66166
0.07738
78.50000
204.80955
0.255So
95.00000
4
Dec
0.06757
0.08102
0.10000
0.26659
0.21310
0.15000
2
MAX 68.70448
101.50000 340.94003
137.00000 49
2017
AveWe
Maximum
# of
TSS
LbfDay
Flow MGD
mg1L
LblDay
Flow (MGD)
mg/L
Analysis
Jan
15.45180
0.07027
26.36750
253.71124
0,30421
100.00000
20
Feb
10.79026
0.06154
21.02500
94.56801
0.23141
49.00000
20
Mar
7.75491
0.06927
13.42273
68.11812
0.31414
26.00000
22
Apr
10.06876
0.10008
12.06316
64.70139
0.27707
28.00000
19
May
15.18069
0.10699
17.01364
172.05578
0.47535
43AD000
22
Jun
4.96752
0.05305
11.22727
25.18920
0.11798
25.60000
22
Jul
4.84927
0.06671
8.71579
24.25405
0.18176
16.D0000
20
Aug
4.66275
0.08607
6.49565
30.19801
0.28288
12.80"
23
Sep
9.21325
0.09126
12.10500
84.27403
0.25262
40.00000
20
Oct
13.20192
0.09922
15.95455
133.79754
0,37309
43.00000
22
Nov
14.64670
0.07738
22.69500
134.74313
0.25850
62.50000
20
Dec
26.04064
0.08102
38.53684
431.87272
0.21310
243.00000
19
MAX 26.04064 38.53684 431.87272 243.00000 249

True Elkin, Inc. WWTP Totals
2017
Average
Maximum
#of
Sulfides
Lb/Day
Flow (MGD)
mg/L
LblDay
Flow (MGD)
m /L
Analysis
Jan
NA
0.07027
<0.100
NA
0.30421
<0.100
2
Feb
NA
0.06154
<0.300
NA
0.23141
<0.300
2
Mar
NA
0.06927
<0.100
NA
0.31414
<0.100
2
Apr
0.16981
0.10008
0.08000
0.25435
0.27707
0.11000
2
May
NA
0.10699
<0.1D0
NA
0.47535
<0.100
2
Jun
NA
0.05305
<0.1D0
NA
0.11798
<0.300
2
Jul
NA
0.06671
<0.100
NA
0.18176
<0.100
2
Aug
NA
0.08607
<0.1D0
NA
0.28288
<0.1D0
2
Sep
NA
0.09126
<0.100
NA
0.25262
<0.100
2
Oct
NA
0.09922
<0.300
NA
0.37309
<0.100
2
Nov
0.04843
0.07738
0.075D0
0.21573
0.25850
0.300D0
2
Dec
0.00642
0.08102
0.00950
0.02490
0.21310
1 0.01400
2
MAX 0.16981 0.08000 0.25435 0.11000 24
2017
Average
Maximum
# of
Phenols
LblDay
Flow (MGD)
m /L
Lb/Day
Flow (MGD)
mglL
Analysis
Jan
0,00762
0.07027
0.01300
0.03300
0.30421
0.01300
2
Feb
0.00385
0.06154
0,00750
0.01931
0.23141
0.01000
2
Mar
NA
0.06927
<0.0100
0,00000
0.31414
0.00000
2
Apr
0.01336
0.10008
0.01600
0.04393
0.27707
0.01900
2
May
0.00714
0.10699
0.00800
0.04364
0.47535
0.01100
2
Jun
0.00553
0.05305
0.01250
0.01378
0.11798
0.01400
2
Jul
0.00807
0.06671
0.01450
0.03640
0.18176
0.02400
2
Aug
0.00790
0.08607
0.01100
0.02597
0.28288
0.01100
2
Sep
NA
0.09126
<0.0100
0.00000
0.25262
0.00000
2
Oct
NA
0.09922
<0.0100
0.00000
0.37309
0.D0000
2
Nov
NA
0.077 88
<0.0100
0.00000
0.2585
00.00000
2
Dec
0.00646
0.08102
0.00955
0.02027
0.21310
0.01140
2
7/25/17 ppa
0.01016
0.11071
0.011
0.01016
0.11071
0.011
1
MAX 0.01336 0.01600 0.04393 0.02400 25
2017
Average
Mmdmum
# of
Chromium
Lb/Day
Flow(MGD)
mg/L
Lb/Day
Flow(1i
m /L
Analysis
Jan
0.00956
0.07027
0.01630
0.05433
0.30421
0.02140
2
Feb
0.00786
0.06154
0.01530
0.02955
0.23141
0.01530
2
Mar
0.00373
0.06927
0.0064S
0.01992
0.31414
0.00760
2
Apr
0.D0864
0.10008
0.01035
0.03145
0.27707
0.01360
2
May
0.01424
0.10699
0.01595
0.06863
0.47535
0.01730
2
Jun
0.00503
0.05305
0.01135
0.01526
0.11798
0.01550
2
Jul
0.00404
0.06671
0.00725
0.01138
0.18176
0.00750
2
Aug
0.00316
0.08607
0.00440
0.01487
0.28288
0.00630
2
0,00762
0.09126
0.01000
0.02446
0.25262
0.01160
2
0.00468
0,09922
0.00565
0.02740
0.37309
0.00880
2
E
0.01634
0.07738
0.02130
0.05609
0.25850
0.02600
2
0.00270
0.08102
0.00400
0.00889
0.21310
0.00500
2
0.DO508
0.11071
0.00550
0.00508
0.11071
0,00550
1
MAX 0.01634 0.02530 0.06863 0.02600 25

True Elkin, Inc. WWTP Totals
2017
Average
Maximum
•of
Fecal Coliform
col/100mL
Flow (MGD)
col/100mL
Flow (MGD)
Analysis
Jan
<2.5
0.07027
<3
0.30421
2
Feb
<1
0.06154
<1
0.23141
2
Mar
<1
0.06927
<1
0.31414
2
Apr
<1
0.10008
<1
0.27707
2
May
0.75
0.10699
1
0.47535
2
Jun
<1
0,05305
<1
0.11798
2
Jul
<1
0.06671
<1
0.18176
2
Aug
12.5
0.08607
23
0.28288
2
Sep
3.25
0.09126
6
0.25262
2
Oct
<1
0.09922
<1
0.37309
2
Nov
<3.5
0.07738
<2
0.25850
2
Dec
6.25
0.08102
12
0.21310
2
MAX 12.50000 23.00000 24
2017
Average
Maximum
s of
Chlorine Residual
pg/L
Flow (MGD)
Lbs
pglL
Flow (MGD)
Lbs
Analysis
Jan
<25
0.07027
<25
0.30421
20
Feb
<25
0.06154
<25
0.23141
20
Mar
<25
0.06927
<25
0.31414
21
Apr
<25
0.10008
<25
0.27707
19
May
<25
0.10699
<25
0.47535
22
Jun
<25
0.05305
<25
0.11798
22
Jul
<25
0.06671
<25
0.18176
20
Aug
<25
0.08607
<25
0.28288
23
Sep
<25
0.09126
<25
0.25262
20
Oct
<25
0.09922
<25
0.373D9
22
Nov
<25
0.07738
<25
0.25850
20
Dec
<25
0.08102
<25
0.21310
19
MAX <25 0,00000 <25 0.00000 248
2017
Average
Maximum
8 of
Total Nitrogen
Lb/Da
Flow (MGD)
mg/L
Lb/Day
Flow (MGD)
m IL
Analysis
Jan
0.32838
0.07027
0.56
1.42170
0.30421
0.56
1
Feb
0.58030
0.06154
1.13
2.18227
0.23141
1.13
1
Mar
0.41046
0.06927
0.71
1.86135
0.31414
0.71
1
Apr
0.43431
0.10008
0.52
1.20238
0.27707
0.52
1
May
0.60713
0.10699
0.68
2.69755
0.47535
0.68
1
Jun
1.07143
0,05305
2.42
2.38271
0.11798
2.42
1
Jul
0.50106
0.06671
0.9
1.36517
0.18176
0.9
1
Aug
1.27138
0.08607
1.77
4.17852
0.28298
1.77
1
Sep
2.43713
1.09121
3.2
6.74629
0,25262
3.2
1
Oct
0.94393
0.09922
1.14
3.54949
0.37309
1.14
1
Nov
0.55538
0.07738
0.86
1.85527
0.25850
0.86
1
Dec
0.43951
0.08102
0.65
1.15596
0.21310
0.65
4
MAX 2.43713 3.20000 6.74629 3.20000 is

True Elkin, Inc. WWTP Totals
2017
Average
Maximum
# of
Total
Phosphorous
Lb/Day
Flow (MGD)
mg/L
Lb/Day
Flow (MGD)
mg/L
Analysis
Jan
1.34871
0.07027
2.3
5.83914
0.30421
2.3
1
Feb
1.38657
0.06154
2.7
5.21427
0.23141
2.7
1
Mar
1.50311
0.06927
2.6
6.81623
0.31414
2.6
1
Apr
1.92098
0.10008
2.3
5.31820
0.27707
2.3
1
May
1.69640
0.10699
1.9
7.53728
0.47535
1.9
1
Jun
1.06257
0.05305
2.4
2.36302
0.11798
2.4
1
Jul
1.55887
0.06671
�; _. 2w6.
4.24721
0.18176
2.8
1
Aug
1.65207
0.08607
2.3
5.42972
0.28288
2.3
1
Sep
1.67553
0.09126
2.2
4.63808
0.25262
2.2
1
Oct
2.15282
0.09922
2.6
8.09533
0.37309
2.6
1
Nov
NA
0.07738
<0.010
NA
0.25850
<0.010
1
Dec
1.14949
0.08102
1.7
3.02329
0.21310
MAX 2.15282 2.80000 8.09533 2.80000 12
2017
Average
Maximum
# of
Temp
°C
Flow (MGD)
C
Flow (MGD)
Analysis
Jan
6.1
0.07027
10.2
0.30421
20
Feb
7.5
0.06154
11.3
0.23141
20
Mar
9.3
0.06927
14.6
0.31414
21
Apr
15.4
0ADDD8
17.7
0.27707
19
May
18.7
0.10699
21.5
0.47535
22
Jun
21.9
0.05305
24A
0.11798
22
Jul
24.6
0.06671
25.9
0.18176
20
Aug23.9
0.08607
26.5'..:
0.28288
23
Sep
20.4
0.09126
22.2
0.25262
20
Oct
16.6
0.09922
22.5
0.37309
22
Nov
9.7
0.07738
15.0
0.25850
20
Dec
4.9
0.08102
8.3
0.21310
19
MAX 16.6 22.5 122
(Jan-Mar/Oct-Dec)
MAX 24.6 26.3 126
(April -Sept.)
2017
Minimum
Maximum
ft of
PH
PH
Flow (MGD)
H
Flow (MGD)
Analysis
Jan
7.3
0.02964
7.4
0.30421
20
Feb
7.1
0.06752
7.4
0.23141
20
Mar
7.1
0.13732
7.3
0.31414
21
Apr
7.2
0.17579
7.6
0.27707
19
May
7.3
0.02766
7.5
0.47535
22
Jun
7.3
0.03991
7.6
0.11798
22
Jul
7.4
0.08023
7.5
0.18176
20
Aug
7.2
0,12271
7.4
0.28288
23
Sep
7.2
0.01407
7.4
0.25262
20
Oct
7.1
0.09969
7.3
0.37309
22
Nov
7.2
0.04375
7.3
0.25850
20
Dec
7.0
0.03459
7.2
0.21310
19
MAX 7.0 7.6 248
Notes:
Prior to calculating average values, non -detect values were changed to 1/2 of the laboratory reporting limit.
Highlighted cell = Maximum value for analyte.

DISTRIBUTION

DUVALTEX (US), INC. TRUE ELKIN, INC.
ELKIN FACILITY WATER USAGE (GPD)
BIG ELKIN CREEK PUMP
MAY 16,2018
152,000 A
NOTE:
i B4O00B
WEAVE 11 SETTLING POND
EVAPORATION VALUES ROUNDED TO NEAREST 100
133,200 C
2017 USAGE DATA
USAGE BASED ON 365 DAYS ANNUALLY
WATER FILTRATION PLANT
133,200 C
TOM OF ELKIN POTABLE WATER
CLEARWELL
8,200 E
8,200 E 200 F
FACILITY DOMESTIC WATER USAGE MUNICIPAL WWTP
133,200 C
0 FIRE PROTECTION ONLY USED IN EMERGENCY
1.000 D
LARGE RESERVOIR
EVAPORATION
ELKIN FACILITY NPDES WASTEWATER APPLICATION
132,200 C
8.000
37,000 G
15,100 H
STEAM PLANT OPERATIONS EVAPORATION
21,900
BLOW DOWN 2,9001
95,200
19.000
11.900
650 L 6501
FINISHINGOPERATIONS rFMTERs EXHAUST
NPDES WASTEWATER APPLICATION
95,200
WATER USE SCHEMATIC
113,550
DUVALTEX (US), INC. - ELKIN FACILITY
125,450
304 EAST MAIN STREET
45,200
ELKIN, NORTH CAROLINA
WASTEWATER TREATMENT PLANT EVAPORATION/LOSS
80.200K
hart: hickman 29215outh Tryon Streeti��
2a2l1
CharloUe, Nosh C.I. 2021 �1
7114586{MM17(p) 71145940373(f
YADKIN RIVER
SMABTFA ENVIRONMENTAL SOLUTIONS bonne # C-IM9 / #C-245 Gn d
DATE: 5-25-18 REVISION NO. 0
JOB NO. VCP-002 FIGURE NO. 1-4
201]
WATER SOURCE
SURFACE
AREA IFT'I
EVAPORATION
RATE IW,DAYI
LOCATION ON
DIAGRAM
FLOW
(GAIAMY)
COMMENT
ELKIN CREEK
A
151,851
20i]-ANNUAL WATER USE REPORT
WEAVE II RESERVOIR EVAPORATION
207RSB
0.1425
B
iB,410
WATER FILTRATION PLANT PRODUCTION
C
133,2d4
LARGE RESERVOIR EVAPORATION
11,310
0.1425
D
1005
�
CITY WATER
E
6,1�
AVERAGE AS INVOICED
CITY WATER
F
18]
AVERAGE AS INVOICED
FILTER WATER CONSUMED -BOILER
G
78.]80
FROM MONTHLY REPORT -ASSUME 50°A BOILER RETURN
CONDENSATE FLASH EVAPORATION
H
15,OB5
ASSUME 8%NORMAL FLASH LOSSES � 33%VENT FOR OVERSRD 80LIER
BOILER ROOM ANCILLPRY EQUIPMENT
I
2.Blq
ASSUME 2 GPM
BOILER TOTAL
54,TSB
W'MPEVAPORATION/LOSS
J
28,150
INFLUENT EFFLUENT METERING
DISCHARGE TO YADKIN RIVER
K
80,238
201]-ANNUAL WATER USE REPORT
ENTERING FABRIC MOISTURE (%BY WEIGHT)
60%
ENTERING FABRIC COATING (%BY WEIGHT)
23%
EXITING FABRIC MOISTURE (%BY WEIGHT)
3%
EXITING FABRIC COATING (Y.BY WEIGHT)
12%
ANNUAL FABRIC PRODUCTION (YAR0.S)-COATED
586,]90
21
ANNUAL FABRIC PRODUCTION(YARDS)-POLYBINDER
692,827
f30
ANNUAL FABRIC PRODUCTION (YARDS)-SCOI1Rfl DRY
26N,982
d9]
TOTAL ANNUAL PRODUCTION
3922,BOB
L
816

3-E
3-13
1-U
PROCESS
1-T
PRE -AERATION
AERATION
SETTLING
INFLUENT
SCREENING
(EO BASIN)
BASIN
(2 SECONDARY CLARIFIERS)
5-A
2-F
AERATION
DISINFECTION
DIGESTION
(CHLORINE)
5-H
DRYING
2 E
BEDS
DECHLORINATION
5-P
4-A
LAND
DISCHARGE TO
APPLICATION
SURFACE WATERS
OUTFALL 001
NPDES WASTEWATER APPLICATION
WASTEWATER TREATMENT PLANT SCHEMATIC
DUVALTEX (US), INC. - ELKIN FACILITY
304 EAST MAIN STREET
NORTH CAROLINA
_•ELKIN,
hart `_ hickman 29'235ou North Tryon
28203N
704586-0W7(p) 7U458G0373(Q
SMARTER ENVIRONMENTAL SOLO MS Licrose # C-1269 / #C-245 Geology
DATE: 5-23-18 REVISION NO. 0
JOB NO. VCP-002 FIGURE NO. 1-5
TREATMENT UNIT CODE
SIZE
RETENTION TIME
FLOW (MGD)
1-T SCREENING
8 SCREENS RATED CAPACITY=3.1
MGD EACH
�
0.0804
3-E PRE -AERATION
2.9 MG
38 DAVS
0.0804
3-B AERATION BASIN
2.1 MG
72 HR
0.07034
1-U BETTING/AEROBIC
DIGESTION
0.376 MG EACH
13 HR
0.7034
5-A AEROBIC DIGESTION
0.040 MG
10 DAYS
0.004
5-H DRYING BEDS
6 BEDS 35' X 82' X 2' EACH
12-38 WKS
0.003
5-P LAND APPLICATION
80.6 ACRES
NA
0
2-F DISINFECTION
0.088 MG
28 HR
O.OB04
2-E DECHLORINATION
4.0 MG
NA
0.0804
4-A DISCHARGE TO SURFACE
WATERS
20 INCH BANK OUTFACE PIPE
NA
0.0804

Duvaltex (US), Inc.
EPA ID# NCO005312
Appendix A
Production Data

Production Data for NPDES Effluent Permit Calculations
Subpart C - Low Water Use Processing
Subcategory
Total
Operating Level
Year
Average ounds/ day
Max. ounds/da
Pounds/day
2015
1,037
3,399
752
2016
1,123
3,843
612
2017
1,251
3,739
735
Subpart D -Woven Fabric Finish in
Subcategory
Total
Operating Level
Year
Average pounds/day
Max. pounds/day
Pounds /day
2015
22,846
37,057
14,687
2016
22,670
36,100
13,664
2017
21,798
37,052
13,594
Average pounds / day is the annual average for actual production days.
Max. pounds / day is the actual maximum production day for the year.
Operating Level pounds / day is the calendar year average.

Duvaltex (US), Inc.
EPA ID# NC0005312
Appendix B
Wet Tests

North Carolina Ceriodaphnia
Chronic Pass/Fail Reproduction Toxicity Test
LC50/Acute Toxicity Test
Effluent Concentration: 1.9%
Date
Passed
Failed
% Reduction
2/15/2017
X
3.0
5/17/2017
X
1.8
8/9/2017
X
2.6
11/15/2017
X
8.3

P0. Box 16414, Creenv Ne SC 296M
(664) 8776942 . fN1 (864) 8T76908
4 Craftsman CmfL Gram, SC 29550
Ceriodaphnia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: TRUE TEXTILES
Facility: ELKIN
NPDES #: NC0005312
Test Date: 15-Feb•17
Laboratory ID #: T48617
Teat Revkwed sod Approved By:
Robert W. KdLy, Ph.D.
QA/QC OfBca
CereBeotlon SFA7819
TW i mlb pmated in this o:pat coat w aE of
NEIAC, codmtd wda NEIAC CMI&ation Nwnbo E87819
Florida DepL of HcOffi IneMded remb pe=n ody w provldcd aevarla.
Page I of 6
Fuhad Rostaapos
Laboratory Directs
SCDHEC ceraBp6on#21ta
NCDENR CeiVOcation g 422

Effluent Toxicity Report Form - Chronic Pass/Fall and Acute LC50
x
EnWommnlN Sctences Branch
Div. W water Quality
N.C. DENR
1621 Mall SerWw Center
Raleigh, Noah Carolina 27699-1621
Calculated t=
Critical Value=
CONTROL ORGaW6M5 , 2 2 a 5 a 7 a 9 10 11 12 % Reduction=
R You Pmoua.. 19 tp 19 19 to is 11 A 22 21 21 to Wn.11y N
AEua ILYW (D)Sad L L L L L L L L L L L L 0%
Conan
Effluent % 1.9°6 0%
T TWNT 20RG4uNrSMS
RY Pwe1a4
naWt fL7'w ID"
pH ,.t.a .
Control 7.5 79 7.7 7.6 7.7 7.9
Treatment 2 6.9 7.9 1 7.7 7.7
D.O. eW1 etl .WI tAo son eq
and
Control 7.6 7.5 7A 8.4 8.9 7.9
Treatment 7.7 7.9 L7.7 8.4 81 7.9
LCSolAcute Toxicity Test
(Mo71.luY salwawa s. %. mmdrun9
L
1 13Fe 17
S.mge l 7( 2
SWOO2 1 X 2
H.rde..InelL)
Cnianiw (rrya)
12
-0.801
19.2
:.n.p
19.8
%W I PASS FM
100% FX
TW SW Dom
1&1. 17
1.1 2M
Tar I.
044 Se . Sam .
184 1 1871 181
frozen
ub a .w a we
LC50 • % Method of Determination C.W
6%conaomw um.a npAwep. Prohit O 1pgn Corc.
% % sp..elm 1(Bar Other pH D.O.
Page 2 of 6

STATISTICAL ANALYSIS RESULTS
Eple
: TRUE TE%TILES wnass NC0005312Date:
1D: WWTp ErnTYan 15-Feb-17
to Cenillcatinn 0: NCO22 I Fa . Data I UIr2017
Survival Data
7 Day Survival Test Uscd: FISHERS TEST
Caroni 100% Test Statistic: Pa 1.000
Effluent 100% Critical Value: P- 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data
Tarfor NOM400
Mean young/female
Std. Dev.
Tat Used: Shapiro-WOb Tat:
Control
19.2 1.53
Effluent
19.8 2.01
W:
0.953
Critical Value:
0.884
mlyslr for D/garenea in Rq-&cden
Test fir Houogeneity of Variance
Tat Used: Egaal Variance t Test
Test Used: F Tat
Calculated[-
-0.80
Fa
1.72
Critical Value
2.51
Critical Value-
5.32
The data are barsegenecas In variance
PASS: The effluent is not chronically toxic.
Page 3 of 6

=M
VW
2, SSF 2-9-17C
5. SSF 2-12-17
MA-Lasl w wt �ss0
Page 4 of

Er;
Po a.a I*. I.. ageawv��..q pE 3+RDO->e11
1+641 P7>-e+4a, loom a+�-saes rY:1aeM 047 ee30
BwMVga APPgvR: 4 Ew.�aw.. EL aR[[R, Yo a+eso
W WM.[TfRMWRPNwC�nY.CPY
CHAIN OF CUSTODY RECORD
Page __of_
Client:
Facility: _
6
3-a
Progrem
s�
y
ti
S
z:
c
a
Coetalaen
a
E
b
C
>
Preservaeht
2-RCL
Parameters
we.kEmamtTax ty
E=
Bt
9
p
f
(///
i i.�
�� ��
I ChemicalAnalysis & Other
p
m
o
$Lail: NPDES a• j ,
Ank
Chrvnk
Teat Oraeebm
SAMPLE ID
u
(CPmpmhe MY)
°.�ksl.go+. Time
(one«Clmporik)
sP�r.cw.w.R ram.
cn«two
=
a
U
s
N
a$�
t`i
y
G
Li
e
c
P
rti
E
;
y
'
.04
(`i
vn
r _
+
"U4
I/c
t/i �rJ�lcN
�1
tl� s
Special hstructums:
Sample Custody Transfer Record
Due Time Ebelivou y/Ortanization
Received B / O
®lion
Secure
Arne
Receipt
Tem °C
Sample
Preserved?
9-1Na
o
L
«_
�,
.1-1
Z,
t
-2- 14: 1-7
;7
o.o
COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: 1 sample each hour for 24 hours, Equal vole
or at minimum 1 sample every 4 hours over 24 hours.
Flow al: As per instructions m NPDES permit
TEMPERATURE MONITORING PROCEDURES
Sample temperasae during collection and transport must be between
0.0 and 6.0 C. Samples most not be frown. Use water ice in sealed bags.
HOLD T/ME PROCEDURES
For toxicity testing the sample must first be used within 26 hows
of sample collection (completion of composite sample).
Sample may trot be used after 72 hours from sample collection.

0
ETT
bwl 07".42. IWM..baane.gM .."••s•
«rw/s ww� i c•.rrru. m. o®t ee ssy
CHAIN OF CUSTODY RECORD
ac
4!Sl�1SIfr7!^e!7�i7j�i�.]Cyci1�
Q'�
�7
I
!■■■■!■■■■�0�
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a■mrai�i�■■■i��■r
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om
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ll
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it

f
PO Box 16414. Creenvle SC 29606
(664) 8776942 .17AX [phone]
4 Craflumn Court, Giver, SC 28/00
Ceriodaphnia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: True Textiles
Facility: ELKIN
NPDES #: NC0005312
Test Date: 17-May-17
Laboratory ID #: T49328
Test Reviewed and Approved By:
Robert W. Kelley, Ph.D.
QA/QC Officer
Certification #E67819
Tm mutts prcmad to this report conaxm to all requYemnxs of
NELAC, ca.dicwd u A. NELAC Cem".. Nmnbcr U7919
Fbnda Dept of H..16 Included milts pennn oNy to V.*d sample.
Page 1 of 6
Farhad Rostarnpotsr
Laboratory Director
SCDHEC certitation#23m
NCDENR Certification# 022

Effluent Toxicity Report Form - Chronic Pass/Fall and Acute LC60
F'.ril
Test:
MAIL ORIGINAL TO Envlronmanal Seances Branch
DIY. of water Quality
N.C. DENR
1621 bail Service Center
Raloth, North Carolina 27699-1621
forth Carolina CeriorLaohnia Chronic Pas/Fall Reoroductiion Toxicity Toot Chronic Test Results
Calculated t= 0.4674
dtical Value= 2.508
CONTROL ORGANISMS 1 2 3 4 5 6 7 a a 10 11 12 %Reduction= 1.8%
layo^iprveaat 1 24 1 21 1 20 1 21 1 26 1 26 1 25 26 24 27 24 Ed
A pr
Reo9
Asa n L L L L L L L L L L L 0% 23.4
Cwara Comma
Effluent % 1.B% 0% 23.0
raelmmt2 Tie N2
Cv
TREATMENT 2 ORGANISMS 1 2 3 4 5 8 7 8 9 10 11 12 10.0%
/Y pmaued 1 25 26 I 22 1 19 1 21 1 22 1 24 1 21 1 21 1 24 1 24 F11
%3m Bnxd PASS FML
A" (LaelnN.a L L L L L L L L L L L 100%ro X
mWeb TMearElth•rT•M Test Stan Cale
pH tsta a to a 2n0 tngb 1 ISMay-17 SamWe2 1AMaP17
Control 7.5 7.7 7.4 7.6 7.6 7.6 7s:,:M1.2
a4Treatment 2 7.5 7.7 7.7 Z5 7.6 7.4 ffX2�
m Im
To. To.
01I . Sample Sarno.
aW efE eat anc man end
�•O• in ImemnWe 2N samole Hmm (m94) 48.0
Control 7.6 8.5 8.1 8.4 8.3 8.0 slac core. tMaasl 1 a4 178 182
Treatment2 7.B 7.8 8,2 8.9 8.7 8.2 Cr/pna("Wo
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(uataMy•pesos as%. Dona nppcate.)
traaon
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LC50 • % Method of Determination ® caws
x CmtlOerxw limo Avera9s oat w9n care.
% % SoeanMn Kaoar r pH D.O.
Page 2 of 6

STATISTICAL ANALYSIS RESULTS
E
. True Textiles NeDW NC0005312
LD: WWFP ern Tents Date. 17-May-17
Certificalion M.- NCO22 I Exp Date. 111112017
Survival Data
7 Day Survival Test Used FISHERS TEST
Control 100% Test Statistic: P= 1.000
Effluent 100% Critical Value: P- 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data
Twfor Normal!!,
Mean youngifamak
Std. Dev
Test Used. Shapirv-Wala Test:
Control
23.4 2.35
Effluent
23.0 2.00
W
0.937
Critical Value.
0.894
rtalysis for DlBerencea in 8eprodwcdon
Teu for Homogeneity of Variance
Test Used: Equal Vadnsce t Tnt
Test Used: F Test
Calculated t-
047
F
1.38
Critical Value-
2.51
Critical Value—
5.32
The data are ham0 eseoas is variance
PASS: nee Muent is not chronically topic.
Page 3 of 6

Page 4 of 6

CHAIN (ff CUSTODY RECORD
wan a09-4942, laool of 1-aaaa r.:wael n77 6938
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TEMPERATURE MONITORING PROCEDURES
Sample temperatuse during collection and transport must he bel een
0.0 and 6.0 *C. Samples must not be Dozen. Use water ke in sealed bags.
HOLD TIME PROCEDURES
For tOxicity tesriag the sample must first be used within 36 hours
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Sample may not be used after 72 hours from sample coliectia.

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must fuss be need within 36 hours
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: I Sample escb hour for 24 hours. EtRW w
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of sempie collxtme (complafon of composite sample).
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x�
RO. Box 16414. Creetnplk. GC 20606
[phone] . FAX (6B4) aT78908
4 CrebrmM Coat, 6lrsar, BC 2YBL0
Ceriodaphnia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: True Textiles
Facility: Elkin
NPDES #: NC0005312
Test Date: 09-Au`-17
Laboratory ID N: T49798
Test Reviewed and Approved By:
Roben W Kelley, Ph.D.
QA/QC Officer
-Cerafteation NES7819
Tm results presented in this report conform to an requiemms of
NELAC, mmk. d,rider NELAC Cauffcation Nuober E37819
Florida Oepe of Health Included resits pertain only to providtd sampies
Page 1 of 6
Fathad Rostampour
Laboratory Director
SCDHEC Certincatiooa2 m
NCDENR Certiftulioe8 022

Test:
Cammmo
Environmantal geleneaa Branch
Div. of WatarDualhy
N.C. DENR
1621 mail Service cones
Raleigh, North CaroUno 27699-1621
CCWROLORGAMSMS 1 2 3 a 5 6 f 6 9 10 11 12 %Reds
# Yowig Produced 1 23 1 23 1 15 1 24 1 21 1 20 1 24 1 23 1 24 1 23 1 25 21 %Merest
Haut (L)i a (0)oad t. L L L L L L L L L L L 0%
Cone!
Effluent % 1.9% 0%
led t= -0.467
Value= 2.508
22.2
:nT
22.8
TREATMEIPT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 12.1%
N yixog Produced 1 26 1 19 1 19 1 19 1 16 1 27 1 23 1 23 1 25 1 23 2J 2a %3N&ood PASS FAIL
MWI (LNve (Diesel L L L I L I L L I L L L L L L 100% X
TMa for EMMrTaat Test Sun OMe
�kaolioh (SUM Die, O9Au -17
pH 1M sample lsrsarrola hid sarvie Save 07'Au9-17 Semp82 09Aug-17
Control 121
7.5 7.5 7.8 7.7 7.7
Treatment 2 7.5 7.5 7.6 1 7.6 7.6 1M 2mrabffaroh
X2M.
Sami. 1 To. To
Srrgle2
NIINm San" Semple
alert end elan erW Nan and
D.O. 1st fet as Harmees(myL) 46.0
Control 8.0 8.1 7.6 8.2 8.4 8.6 Spec. Corte. W,*o) 185 145 19;
Treatment 2 7.9 7.9 7.7 8.4 8.7 8.5 chlonm (-A) <.05 <.05
w Tam a mxi,w rY.1 n S m C
LC80/Acute Toxicity Teat
(MonahN ugmaaed as W. conWNng tephoales)
Monellly aww.m staNend
LC50 = % Method of Determination Cawa
15%Cmfio)"Limlla MoHm Average fObit High Com
% % rman r(arear Other PH 0.0.
DEM Form AT-1
Page 2 of 6

STATISTICAL ANALYSIS RESULTS
acdt : True Textiles uroesa NC0005312
ample ID: WWTP eTrr TOM Date: 09-Aug-17
I l,orato Certification g: NCO22 Exp. Date: 1111/2017
Survival Data
7 Day Survival
Test Used:
FISHERS TEST
Control
100%
Test Statistic:
P= 1.000
Effluent
100%
Critical Value:
P. 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data
Testfor Normality
Mean young/female
Std. Dev
Test Used: Shapiro -Willis Test:
Control 22.2
2.69
Effluent 22,8
3.39
W:
0.962
Critical Value:
0.884
nalysis for Differences, in Reproduction
Testjor Homogeneity of Variance
Test Used: Equal Variance t Teat
Test Used: FTest
Calculated t=
•0.47
F=
1,58
Critical Value=
2.51
Critical Value=
5.32
The data are homogeneous in variance
PASS: The effluent is not chronically toxic.
Page 3 of 6

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COMPOSITE SAMPLING PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: I sample each hour for 24 hours. Fqual volu
or at minimum 1 sample every 4 hours over 24 hours.
Flow P 'onsi: As Per instructions in NPDES pernit.
TEMPERATURE MONITORING PROCEDURES
Sample temperature during collection and transport must be between
0.0 and 6.0'C. Samples most not be (roan. Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample most first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hours from sample collection.

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Time Proportional: 1 sample each hour for 24 hours. Equal "hu
or at minimum 1 sample every 4 hours over 24 hours.
FlowProportional: AS per mAroctions in NPDES Permit.
TEMPERATURE MONITORING PROCEDURES
Sample Iempenu a during collection and transport must be between
0.0 and 6.0'C. Samples must not be frozen. Use water ice in sealed hags.
HO ME PROCEBOURES
For toxicity testing the sample must first be used within 36 hours
of sample collection (completion of composite sample).
Sample may not be used after 72 hows from sample coilecitm,

am ,Ina [phone]. rAX (NN) 8778938
r`.O. Box 16414, Oreenvlie SC 29606 4 Cratianan Court, Grew, SC 28890
Ceriodaphnia dubia Survival and Reproduction Test
EPA-821-R-02-013 Method 1002
Client: TRUE TEXTILES
Facility: Elkin
NPDES #: NC0005312
Test Date: 15-Nov-17
Laboratory ID #: T50430
Test Reviewed and Approved By:
.�1ar
Robert W. Kelley, Ph.D.
QAlQC Officer
CeraBcation #E87819
Tat resubs presented m ads report coNormto all requie. of
NEIAC, conducted ardor NEIAC Cadikation Nm ber E87819
Florida Dept ofawlth bochded remwln perum only to provided samples.
Page 1 of 8
Farhad Rosfampour
Laboratory Director
SCDHEC Cere&ado. 023104
NCDENR Certlacad"It 022

Effluent Toxicity Report Form - Chronic PesNFall and Acute LC50
Date 27-No*17
Facility: True Te lies WWTP NPDESN NC0005312 Pipe N 001 Couffly SUITY
Laboratory Performing Teal;
x
Comhenr
Signature of Operator' s l0 a
50
Signature o1 Laboratory SuPerymor
MAIL ORIGINAL TO EnYtronnmmw sciences Branch
DIV. W W8W Quality
N.C. DENR
1621 NO s0r14e6 Center
Raleigh, Norm Carolina 27699-IM
led t= 1
Value=
CONT CRG"SrS 1 2 3 1 S 6 7 a 9 10 11 12 Reduction= S.:
lwyoxvVmexeE I 2a 21 26 1 20 1 22 1 16 1 20 1 22 1 la 1 21 1 :11
22 mxxtalty Mg RWmd.
Aaun (L I.e6 I L L L I L L L I L I L I L I L I L L 0% 21.1
canna Cax"
Effluent % 1.9% 0% 19.3
Treelrrant2 Treer4wM12
eeh c
TREATwEM 2 ORGAWSr3 1 2 3 2 3 a 7 a 9 10 11 12 12.7%
N Ya. RoauoO I 17 to 1 2e 1 21 1 20 1 11 1 11 22 21 1 18 1 23 20 %U09rooe PASS FAIL
Auer (L)Le 1oya6 L L L L L L L L L L L L 100% X
l T111e br 6N.r T.et Tell Srn Gee
�r,l S 17
pH 1w lei 2" eenW SrW.l 13lbv-1) Senol.2 1SrbviT
Control 7.7 8.0 7.6 7.9 7.6 &0
Treatment 2 7.8 7.9 7.6 7.9 7.6 8.0 mP wa lw, lei 2na
Senor1 X 20... Toe Tax
S.0.2 X 24,,e. DWW sw" swoo
D.O. wan err .w .nor ,rent .nor NNr6rrx (m9M1) 46.0
Control 7A 8.0 1 7.9 8.3 7-9 8.2 sP.a. core. lwMa.1 183 182 11
Treatment 2 7.7 8.2 7-9 8.3 7.7 8.3 C"Im (rho) <.05 <.05
0.2
trozen
LCSO/Acute ToxICIty Test
(Mwleety norm" n %, omrnNe.core)
AIawI3y erNem el.w.nd
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IS%Conlaeno Llmir --, Alwa(Ie '^^�-'molt O Illeh fahc
% % Kano. ' toner pN D.O.
-1
Page 2 of 6

STATISTICAL ANALYSIS RESULTS
:
True Textiles
[reaese NC0005312
Iacili
ample ID:
I -
WWTP
ens isesse
Date: 15-Nov-17
Certification M: NCO22
I Esp. Date: I UU2018
Survival Data
7 Day Survival Test Used: FISHERS TEST
Control 100% Test Sutistic: P- 1.000
Effluent 100% Critical Value: P- 0.01
PASS: The effluent does not reduce survival of the test organisms.
Reproduction Data
Raw Data
rastforNormaHty
Meao youngifetaale
Sid. Dev.
Test Used: Shapire-Willa Test.
Control 21.1
2.68
Effluent 19.3
3.47
W.
0.949
Critical Value:
0.884
natyt8 for Di,(fmnces in Reproduction
TestforHomogeneity of Varian -
Test Used: Equal Variance i Test.
Test Used: F Test
Calculatedt-
1.38
F-
1.68
Critical Value
2.51
Critical Value,
5.32
The data are boom anus in variance
PASS: The effluent is not chronically toxic.
Page 3 of 6

C W MW%Sft d. R.pmtl. by T.n D.y
1 2 3 4 5 6 1 8
.W1
.3.7
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2
4
.8.9
21
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254
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IA
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Sample Custody Transfer Record
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Receipt
Sample
Date Time AcliduishedAv Racnived B / Otamigation
Area
Temp °C
Preserved?
0
kbvir [WIL1,11
COMPOSITE SAMPLING PROCEDURES
TEAOD£RATURE MONITORING PROCEDURES
HOLD TIME PROCEDURES
Composite samples must be collated over a 24 how period.
Sample temperature during collection and transport must be between
For toxicity acting the sample man first be used within 36 hours
Time Proportional: i sample each how for 24 haws. Equal vol
0.0 and 6.0 T. Samples most nm be fi=n. Use tester ice in sealed bags.
of sample collection (completion of composite sample).
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Sample may not be used after 72 hours from sample collection.
Flow 'onal: As per instructions in NPDE$ p2mit.

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CHAIN Or, CUSTODY RECORD
-4-
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Sample Custody Transfer Record
Date Time kofiraquishc4by ! Ontatization A By) Oriummasion
Secure
Area
Receipt
Temp ¢C
Sample
Prtserved7
11- !o-1
077,01f�
r
0830
d
Ear
COMPOSITE VMPIJNG PROCEDURES
Composite samples must be collected over a 24 hour period.
Time Proportional: I sample each hour for 24 {mars. Equal volu
or at minimum 1 sample every 4 hours over 24 hours.
Flow Proportionat As per instructiorm in NPDES permit.
TEMPERATURE MONITORING PROCEDURES
Sample tempenwe during collection and transport must be between
0.0 and 6.0 [C. Samples must not be fma Use water ice in sealed bags.
HOLD TIME PROCEDURES
For toxicity testing the sample must first be used w4thin 36 hours
of sample collection (completion of composite sample).
Sample may ram be used after 72 hours from sample collation.

Duvaltex (US), Inc.
EPA ID# NCO005312
Appendix C
Priority Pollutant
Analysis Results

aceAnalytical e
/ mvwpace/abscam
August 04, 2017
Mr. Glen Gary
TRUE, Inc.
304 E. Main St.
Elkin, NC 28621
RE: Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Pace Ana"cal Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Dear Mr. Gary:
Enclosed are the analytical results for sample(s) received by the laboratory on July 25, 2017. The
results relate only to the samples included in this report. Results reported herein conform to the most
current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual, where
applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Matthew Brainard
[e-mail]
[phone]
Project Manager
Enclosures
cc: Scoff Taylor, True Textiles
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 1 of 41

aceAnalytical
e parelabsx=
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Pace Analytical services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Charlotte Certification IDs
9800 KinceyAve. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Eden Certification We
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
CERTIFICATIONS
South Carolina Certification #: 99006001
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP Certification #: 460222
North Carolina Wastewater Certification #: 633
Virginia/VELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report shall not he reproduced, except in full,
without the written consent of Pace Analyfical Services, L.I.C. Page 2 of 41

aceAnalytkal
eww.parofabs.wm
SAMPLE ANALYTE COUNT
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID
Sample ID
Method
Analysts
Analysts
Reported
Laboratory
92348913001
Effluent Comp
EPA 6010
SH1
20
PASI-A
EPA 7470
KAL
1
PASI-A
EPA300.0
CDC
2
PASI-A
EPA 350.1 1993 Rev 2.0
AES2
1
PASI-A
EPA353.2
CJH1
1
PASI-A
SM 5310B
KDF1
1
PASI-A
EPA 7196
CJH1
1
PASI-A
92348913002
Effluent Grab
SM 2120E Color ADMI
CTB
4
PASI-E
EPA 1664B
JMS
1
PASI-C
EPA8081
PKS
22
PASI-C
EPA 8082
HSK
8
PASI-C
EPA 8270
BPJ
74
PASI-C
EPA 8260
2D0
34
PASI-C
SM 4500-S20
NAL
1
PASI-A
EPA420.4
DMN
1
PASI-A
SM 4500-CN-E
BRJ
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproeuceo. except in full,
without the written consent of Pace Analytical Services, LLC.
Page 3 of 41

Pace Analytical Services, LLC
aceAnalytical ® 9800 ncey Ave. Suite 100
Hunteraville, NC 28078078
w Pacela0s. can [phone]
ANALYTICAL RESULTS
Project: Annual Sampling 07125/17
Pace Project No.: 92348913
Sample: Effluent Comp Lab ID: 92348913001 Collected: 07/25/17 07:15 Received: 07/25/17 07:55 Matrix: Water
Parameters
6010 MET ICP
Aluminum
Antimony
Arsenic
Barium
Beryllium
Boron
Cadmium
Chromium
Cobalt
Copper
Iron
Lead
Magnesium
Manganese
Nickel
Selenium
Silver
Thallium
Titanium
Zinc
7470 Mercury
Mercury
300.0 IC Anions 28 Days
Fluoride
Sulfate
350.1 Ammonia
Nitrogen, Ammonia
353.2 Nitrogen, NOLNO3 pries.
Nitrogen, NO2 plus NO3
5310E TOC
Total Organic Carbon
7196 Chromium, Hexavalent
Chromium, Hexavalent
Date: 08/04/2017 05:20 PM
Results Units Report Limit DF Prepared Analyzed CAS No. Qual
Analytical Method: EPA 6010 Preparation Method: EPA 3010A
116
ug/L
100
1
07/31/17 15:40
08/02117 05:12
7429-90-5
L
ug/L
5.0
1
07/31/17 15:40
08/02117 05:12
7440-36-0
ND
ug/L
10.0
1
07/31/17 15:40
08/02/17 05:12
7440-38-2
��
ug/L
5.0
1
07/31/17 15:40
08/02117 05:12
7440-39-3
ND
ug/L
1.0
1
07/31/17 15.40
08102/17 0512
7440-41-7
ND
ug/L
50.0
1
07/31/17 15.40
08/03/17 18:21
7440-42-8
ND
ug/L
1.0
1
07/31/17 15:40
08/02/17 05:12
744043-9
5.6
ug/L
5.0
1
07131/17 15:40
08/02/17 05:12
7440-47-3
ND
ug/L
5.0
1
07/31/17 15:40
08102/17 D512
7440-48-4
14.0
ug/L
5.0
1
07/31/1715:40
08/02117 05:12
7440-50-8
90.4
ug/L
50.0
1
07/31/17 15:40
08/02117 05:12
7439-89-6
ND
ug/L
5.0
1
07/31/17 15:40
08102117 05:12
7439-92-1
2610
ug/L
100
1
07/31/17 15:40
08/02117 D512
7439-95-4
5.6
ug/L
5.0
1
07/31/17 15:40
08102/17 05:12
7439-96-5
NO
ug/L
5.0
1
07/31/17 15:40
08/02/17 05:12
7440-02-0
ND
ug/L
10.0
1
07/31/17 15:40
08/02/17 05:12
7782-49-2
ND
ug/L
5.0
1
07/31/17 15:40
08/02/17 05:12
7440-22-4
ND
ug/L
10.0
1
07/31117 15:40
08/02/17 05:12
7440-28-0
NO
ug/L
5.0
1
07/31/17 15:40
08/02/17 05:12
7440-32-6
ND
ug/L
10.0
1
07/31/17 15:40
08/02/17 05:12
7440-66-6
Analytical Method: EPA 7470 Preparation Method: EPA 7470
NO ug/L 0.20 1 07/26117 11:18 07/27/17 D0:24 7439-97-6
Analytical Method: EPA 300.0
0.14 mg/L 0.10 1
27.1 mg/L 1.0 1
Analytical Method: EPA 350.1 1993 Rev 2.0
NO mg/L 0.10 1
Analytical Method: EPA 353.2
0.92 mg/L 0.020 1
Analytical Method: SM 53108
33.7 mg/L 1.0 1
Analytical Method: EPA 7196
ND mg/L 0.010 1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
07/30/17 20:20 16984-48-8
07130/17 20:20 W08-79-8
08/01117 15:08 7664-41-7
08/01117 04:18
OI?Ly7,tf[jiitrSiP_i ��SSr]
07/26/17 05:41 18540-29-9
Page 4 of 41

lCeAnalyticale
www.pxroleesam
1
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvllle, NC 28078
(7o4)e75-9092
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Sample: Effluent Grab lab ID: 92348913002 Collected: 07125/17 07:40 Received: 07125/17 07:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
2120E ColorADMI Analytical Method: SM 2120E Color ADMI
Color, ADMI
NO
units
25.0
1
07/2611713:08
Adjusted Color, ADM I
NO
units
25.0
1
072611713:08
PH
7.4
units
1.0
1
0726/1713:08
Adjusted pH, ADMI
7.6
units
1.0
1
07126/17 13:08
HEM, Oil and Grease
Analytical Method: EPA 1664E
Oil and Grease
NO
mg/L
5.0
1
08102/17 06:28
8081 Organochlorine Pesticides
Analytical Method: EPA 8081 Preparation Method: EPA 3510
Norm
NO
ug/L
0.060
1
07126/17 15:30 072611719:18
309-00-2
alpha-BHC
NO
ug/L
0.050
1
07126/17 15:30 07/26/17 19:18
319-84-6
beta-BHC
NO
ug/L
0.060
1
07/26/17 15:30 07/26/17 19:18
319-85-7
delta-BHC
NO
ug/L
0.050
1
07/26/17 15:30 072611719:18
319-86-8
gamma-BHC (Lindane)
NO
ug/L
0.050
1
0726/17 16:30 0726117 19:18
58-89-9
Chlordane (Technical)
NO
ug/L
0.20
1
0726/17 15:30 0726/17 19:18
57-74-9
4,4'-DDD
NO
ug/L
0.050
1
0726/1715:30 072611719:18
72-54-8
4,4'-DDE
NO
ug/L
0.050
1
0728/1715:30 07/2611719:18
72-55-9
4,4'-DDT
NO
ug/L
0.050
1
07/26/17 15:30 07126/17 19:18
50-29-3
Dielddn
NO
ug/L
0.050
1
07/26/17 15:30 07/26/17 19:18
60-57-1
Endosulfan I
NO
ug/L
0.050
1
07/26/17 15:30 0726117 19:18
959-98-8
Endosulfan II
ND
ug/L
0.050
1
07/26/17 15:30 0726/17 19:18
33213-65-9
Endosulfan sulfate
NO
ug/L
0.050
1
07126/17 15:30 0726117 19:18
1031-07-8
Endrin
NO
ug/L
0.050
1
07/26/17 15:30 07/26/1719:18
72-20-8
Endrin aldehyde
ND
ug/L
0.050
1
07/26/17 15:30 07/26/17 19:18
7421-93-4
Endrin ketone
NO
ug/L
U)50
1
0726/17 15:30 07/26/17 19:18
53494-70-5
Heptachlor
NO
ug/L
0.050
1
07/26/17 15:30 07/26/17 19:18
76-44-8
Heptachlor epoxide
NO
ug/L
0.050
1
07/26/17 15:30 0726/17 19:18
1024-57-3
Methoxychlor
NO
ug/L
0.15
1
072511715:30 07/26/17 19:18
72-43-5
Toxaphene
NO
ug/L
0.20
1
07/26/17 15:30 07/26/17 19:18
8001-35-2
Surrogates
Tetrachloro-m-xylem (S)
55
%
20-130
1
0726/17 15:30 0726/17 19:18
877-09-8
Decachlorobiphenyl (S)
31
%
20-130
1
0726/17 15:30 07/26/17 19:18
2051-24-3
8082 GCS PCB
Analytical Method: EPA 8082 Preparation Method: EPA 3510
PCB-1016 (Aroclor 1016)
NO
ug/L
0.50
1
0726117 09:01 0726117 20:10
12674-11-2
PCB-1221 (Aroclor 1221)
NO
ug/L
0.60
1
07/26117 09:01 07/26/17 20:10
11104-28-2
PCB-1232 (Aroclor 1232)
NO
ug/L
0.50
1
07/26/17 09:01 0726/17 20:10
11141-16-5
PCB-1242 (Aroclor 1242)
ND
ug/L
0.50
1
07/26/17 09:01 0726117 20:10
53469-21-9
PCB-1248 (Aroclor 1248)
NO
ug/L
0.50
1
07/26/17 09:01 07/26/17 20:10
12672-2941
PCB-1254 (Aroclor 1254)
ND
ug/L
0.50
1
07/26/17 09:01 0726/17 20:10
11097-69-1
PCB-1260 (Amdor 1260)
NO
ug/L
0.50
1
07/26/17 09:01 0726/17 20:10
11096-82-5
Surrogates
Decachlorobiphenyl (S)
37
%
10-132
1
0726117 09:01 07/26/17 20:10
2051-24-3
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthene
NO
ug/L
10.0
1
0727/1714:30 07/28/1712:22
83-32-9
REPORT
OF LABORATORY
ANALYSIS
This report shall not be reproduced, except
in full,
Date: 08/042017 05:20 PM
without the written consent of Pace Analytical Services. LLC.
Page 5 of 41

Pace Analytical Services, LLC
• 9800 Kincey Ave. Surte 100
;alce
"Iytical Hurltemvdle, NC 28078
www.pcsh omi [phone]
I
ANALYTICAL RESULTS
Project. Annual Sampling 07/25/17
Pace Project No.: 92348913
Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received: 07/25M7 07:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Oual
8270 MSSV Semivolatile Organic Analytical Method: EPA 8270 Preparation Method: EPA 3510
Acenaphthylene
NO
ug/L
10.0
1
07/2711714:30
07/2811712:22
208-96-8
Aniline
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
62-53-3
Anthracene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
120-12-7
Benzo(a)anthracene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
56-55-3
Benzo(a)pyrene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
50-32-8
Benzo(b)8uoranthene
NO
ug/L
10.0
1
07/27/171430
0712811712:22
205-99-2
Benzo(g,h,i)perylene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
191-24-2
Senzo(k)Buoranthene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 1222
207-08-9
Benzoic Acid
NO
ug/L
50.0
1
07/27/17 14:30
07/28/1712:22
65-85-0
Benzyl alcohol
NO
ug/L
20.0
1
07/27/17 14:30
07/28/17 1222
100-51-6
4-Bromophenylphenyl ether
NO
ug/L
10.0
1
07127/1714:30
07/2811712:22
101-55-3
Butylbenzylphthalate
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
85-68-7
4-Chloro-3-methylphenol
NO
ug/L
20.0
1
07/27/17 14:30
071281171222
59-50-7
4-Chloroaniline
NO
ug/L
20.0
1
07/2711714:30
07/28/1712:22
10647-8
bis(2-Chloroethoxy)methane
NO
ug/L
10.0
1
07127/171430
07/2811712:22
111-91-1
bis(2-Chlorcethyl) ether
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
111444
2-Chloronaphthalene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
91-58-7
2-Chlorophenol
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
95-57-8
4-Chlorophenylphenyl ether
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
7005-72-3
Chrysene
NO
ug/L
10.0
1
07127/1714:30
07/28/171222
218-01-9
Dibenz(a,h)anthracene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 1222
53-70-3
Dibenzofuran
NO
ug/L
10.0
1
07/27/17 14:30
07/28117 12:22
132-64-9
1,2-Dichlorobenzene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
95-50-1
1.3-Dichlorobenzene
NO
ug/L
10.0
1
07127/1714:30
07/28/1712:22
541-73-1
1,4-Dichlorobenzene
NO
ug/L
10.0
1
07/27/17 14:30
0712811712:22
10646-7
3,3'-Dichlorobenzidine
NO
ug/L
20.0
1
07/27/17 14:30
07/2811712:22
91-94-1
24-Dichlorophenol
NO
ug/L
10.0
1
07127/1714:30
07128/1712:22
120-83-2
Diethylphthalate
NO
ug/L
10.0
1
07127/1714:30
0712811712:22
84-66-2
2,4-Dimethylphenol
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
105-67-9
Dimelhylphthalate
ND
ug/L
10.0
1
07/27/17 14:30
07/281171222
131-11-3
Di-n-burylphthalate
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
84-74-2
4,6-Dinitro-2-methylphenol
ND
ug/L
20.0
1
07/27/17 14:30
07/28/17 12:22
534-52-1
2,4-Dinitrophenol
NO
ug/L
50.0
1
07/27/1714.30
07/28/171222
51-28-5
2,4-Dinitrotoluene
NO
ug/L
10.0
1
07/27/17 1430
07/28/17 1222
121-14-2
2,&Dinitrotoluene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
606-20-2
Di-n-octylphthalate
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 1222
117-84-0
bis(2-Ethylhexyl)phthalate
NO
ug/L
6.0
1
07/27/17 14:30
07/28/17 12:22
117-81-7
Fluoranthene
NO
ug/L
10.0
1
07127/1714:30
07128/1712.22
206-44-0
Fluorene
NO
ug/L
10.0
1
0712711714:30
07/28/17 12:22
86-73-7
Hexachloro-1,3-butadiene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
87-68-3
Hexachlorobenzene
NO
ug/L
10.0
1
07127/1714:30
07/2811712:22
118-74-1
Hexachlorocyclopentadiene
NO
ug/L
10.0
1
07/27/17 14:30
07/2811712.22
77-474
Hexachloroethane
NO
ug/L
10.0
1
07/27/17 14:30
07/28/1712:22
67-72-1
Indeno(1,2,3-cd)pyrene
NO
uglL
10.0
1
07/27/17 14:30
07/28/17 12:22
193-39-5
Isophorone
NO
ug/L
10.0
1
07/27/17 14:30
07/28/1712:22
78-59-1
1-Methylnaphthalene
NO
ug/L
10.0
1
07/27/171430
07/28/171222
90-12-0
2-Methylnaphthalene
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
91-57-6
REPORT OF LABORATORY ANALYSIS
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Date: 08/04/2017 05:20 PM without the written consent of Paw Analytical Services. LLC. Page 6 of 41

//IceAnalytical e
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ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suxe 100
Huntersv0le, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Sample: Effluent Grab
Lab ID: 92348913002 Collected: 07/25/17 07:40
Received: 07/25/17 0755 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Oual
8270 MSSV Semivolatile Organic
Analytical Method: EPA 8270 Preparation Method: EPA 3510
2-Methylphenol(o-Cresol)
NO
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
95-48-7
384-Methylphenol(m&p Cresol)
NO
ug/L
10.0
1
0712711714:30
0712811712:22
lWl-10-4
Naphthalene
NO
ug/L
10.0
1
07127/1714:30
07128/1712:22
91-20-3
2-Nitroaniline
NO
ug/L
50.0
1
07/27/17 14:30
07/28/17 12:22
88-74-4
3-Nitroaniline
NO
ug/L
50.0
1
07/27/17 14:30
07/28/17 12:22
99-09-2
4-Nitroaniline
NO
ug/L
20.0
1
07127/1714:30
0712811712:22
100-01-6
Nitrobenzene
NO
ug/L
10.0
1
0712711714:30
0712811712:22
98-95-3
2-Nitrophenol
NO
ug/L
10.0
1
07/27/17 14:30
0712811712:22
88-75-5
4-Nitrophenol
NO
ug/L
50.0
1
07127/1714:30
07/2811712:22
100-02-7
N-Nitrosodimethylamine
NO
ug/L
10.0
1
07/27/17 14:30
07/2811712:22
62-75-9
N-Nitroso-di-n-propylamine
NO
ug/L
10.0
1
07127/1714:30
0712811712:22
621-64-7
N-Nitrosodiphenylamine
NO
ug/L
10.0
1
0712711714:30
0712811712:22
86-30-6
2,2'-Oxybis(1-chloropropane)
ND
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
108-60-1
Pentachlorophenol
ND
ug/L
25.0
1
07/27/17 14:30
07/28117 12:22
87-86-5
Phenanthrene
ND
ug/L
10.0
1
07/27/17 14:30
0712811712:22
85-01-8
Phenol
ND
ug/L
10.0
1
07/2711714:30
07/2811712:22
108-95-2
Pyrene
ND
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
129-00-0
1,24-Trichlorobenzene
ND
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
120-82-1
2,4,5-Trichlorophenol
ND
ug/L
10.0
1
07/27/17 14:30
07/28/17 12.22
95-95-4
2,4,6-Trichlorophenol
ND
ug/L
10.0
1
07/27/17 14:30
07/28/17 12:22
88-06-2
Surrogates
Nitrobenzene-d5 (S)
33
%
21-110
1
07/27/17 1430
07/28/17 12:22
416550-0
2-Fluorobiphenyl (S)
41
%
27-110
1
07/27/17 1430
07/28/17 12:22
321-60-8
Terphenyl-d14(S)
54
%
31-107
1
07/27/17 14:30
07/2811712:22
1718-51-0
Phenol-d6 (S)
13
%
10-110
1
07/27/17 14:30
07/28/17 12:22
13127-88-3
2-Fluorophenol(S)
17
%
12-110
1
07/27/17 14:30
07/28/17 12:22
367-124
2,4,6-Tribromophenol(S)
57
%
27-110
1
07/27/17 14:30
07/28/17 12:22
118-79-6
8260 MSV
Analytical Method: EPA 8260
Acrolein
NO
ug/L
100
1
07/30/17 01:48
107-02-8
Acrylonitrile
NO
ug/L
100
1
07/30/17 01:48
107-13-1
Benzene
NO
ug/L
5.0
1
07/30/17 01:48
71-43-2
Bromodichloromethane
NO
ug/L
5.0
1
07/30/17 01:48
75-27-4
Bromoform
NO
ug/L
5.0
1
07/30/17 01 48
75-25-2
Bromomethane
NO
ug/L
10.0
1
07/30/17 01:48
74-83-9
Carbon tetrachloride
NO
uglL
5.0
1
07/30/17 01:48
56-23-5
Chlorobenzene
NO
ug/L
5.0
1
07/30/17 01:48
108-90-7
Chloroethane
NO
ug/L
10.0
1
07130/1701:48
75-00-3
2-Chloroethylvinyl ether
NO
ug/L
10.0
1
07/30/17 01:48
110-75-8 c2
Chloroform
NO
ug/L
5.0
1
07/30/17 01:48
67-66.3
Chloromethane
NO
ug/L
5.0
1
07/30/17 01:48
74-87-3
2-Chlorotoluene
NO
ug/L
5.0
1
07/30/17 01:48
95-49-8
4-Chlorotoluene
NO
ug/L
5.0
1
07/30/17 01:48
106-434
Dibromochloromethane
NO
ug/L
5.0
1
07/30/17 01:48
124-48-1
1,1-Dichloroethane
NO
ug/L
5.0
1
07130/1701:48
75-34-3
12-Dichloroethane
NO
ug/L
5.0
1
07/30117 01:48
107-06-2
1,1-Dichloroelhene
NO
ug/L
5.0
1
0713011701:48
75-35-4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analyecel Services, LLC. Page 7 of 41

aceAnalytical e
~pacelaexcan
ANALYTICAL RESULTS
Project: Annual Sampling 07125/17
Pace Project No.: 92348913
Pace Analytical Services, LLC
9800 Kincey Ave. Sune 100
MunteravNle, NC 28078
[phone]
Sample: Effluent Grab Lab ID: 92348913002 Collected: 07/25/17 07:40 Received. 07/25/17 07:55 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Thal
8260 MSV Analytical Method: EPA 8260
trans-1,2-Dichloroethene
ND
ug/L
5.0
1
07/30/17 01:48
156-60-5
1,2-Dichloropropane
ND
ug/L
5.0
1
07/30/17 01:48
78-87-5
cis-1,3-Dichloropropene
ND
ug/L
5.0
1
07130/1701:48
10061-01-5
trans-1.3-Dichloropropene
ND
ug/L
5.0
1
07/3011701:48
10061-02-6
Ethylbenzene
ND
ug/L
5.0
1
07130/1701:48
100.414
Methylene Chloride
ND
ug/L
5.0
1
07/30/17 01:48
75-09-2
1,1.2,2-Tetrachloroethane
ND
ug/L
5.0
1
07/30/17 01:48
79-34-5
Tetrachloroethene
ND
ug/L
5.0
1
07/30/17 01:48
127-184
Toluene
ND
ug/L
5.0
1
07/30/17 01:48
108-88-3
1,1,1-Trichloroethane
ND
ug/L
5.0
1
07/30/1701:48
71-55-6
1,1.2-Trichloroethane
ND
ug/L
5.0
1
07/30/17 01:48
79-00-5
Trichloroethene
ND
ug/L
5.0
1
07/30/17 01:48
79.01-6
Vinyl chloride
NO
ug/L
5,0
1
07/30/17 01:48
75-014
Surrogates
4-Bromofiuorobenzene (S)
99
%
70-130
1
07/30/17 01:48
460-004
1.2-Dichloroethane-d4 (S)
94
%
70-130
1
07/30/17 01:48
17060-07-0
Toluene-d8 (S)
100
%
70-130
1
07/30/17 01:48
2037-26-5
4500S2D Sulfide Water
Analytical Method:
SM 4500-520
Sulfide
NO
mg/L
0A0
1
07/31/1717:42
18496-25-8
420.4 Phenolics, Total
Analytical Method:
EPA 420.4
Phenol
0.011
mg/L
0,010
1
07/31/1714:33
108-95-2
4500CNE Cyanide, Total
Analytical Method: SM 4500-CN-E
Cyanide
ND
mg/L
0,0080
1
08/02/1705:40
57-12-5
Date: 08/04/2017 05:20 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 8 of 41

aceAnalytical
wwwpacelaba,.ih
QUALITY CONTROL DATA
Pace Analocal Services, LLC
9800 Kinc Ave. Suite 100
Hunlersville. NC 28078
[phone]
Project:
Annual Sampling 07/25117
Pace Project No.:
92348913
QC Batch:
370563 Analysis Method: SM 2120E Cola ADMI
QC Batch Method:
SM 2120E Color ADMI Analysis Description: 2120E Color ADMI
Associated Lab Samples:
92348913002
METHOD BLANK: 2053311
Associated Lab Samples: 92348913002
Parameter Units
Color. ADMI units
LABORATORY CONTROL SAMPLE: 2053312
Parameter Unds
Color. ADMI units
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 07/26/1712:56
Spike LCS LCS % Rec
Conic. Result %Rec Limits Qualifiers
125 122 98 90-110
SAMPLE DUPLICATE: 2053313
92348816001 Dup
Parameter Units Result Result
Color, ADMI units NO ND
RPD Qualifiers
Results presmrtee on this page are in the units indicated by Me "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date: 08/04/2017 0520 PM without the written consent of Pace Analytical Services, -I-C. Page 9 of 41

1eAnalytical"
www.paceleAs.avn
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371460
QC Batch Method: EPA 1664B
Associated Lab Samples: 92348913002
METHOD BLANK: 2058032
Associated Lab Samples: 92348913002
Parameter Units
Oil and Grease mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 1664E
Analysis Description: 1664 HEM. Oil and Grease
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 5.0 08/02/1706:26
Pace Analytical services, LLC
9800 Kincey Ave. Sude 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2058033
Spike LCS
LCS
% Rae
Parameter
Units
Cone. Result
% Rae
Limits
Qualifiers
Oil and Grease
mg/L
40 37.8
94
78-114
MATRIX SPIKE SAMPLE:
2058034
92348970002 Spike
MS
MS
% Rec
Parameter
Units
Result Cone.
Result
% Rae
Limits Qualifiers
Oil and Grease
mg/L
NO 40
40.0
97
78-114
Resuhs presented on this page are in the ands Indicated by the "Urns" column except where an ahemate unit is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full.
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services. LLC Page 10 of 41

aceAnalytical o
/ wwwparela0s.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 370574 Analysis Method: EPA 7470
QC Batch Method: EPA7470 Analysis Description: 7470 Mercury
Associated Lab Samples: 92348913001
METHOD BLANK: 2053343 Matrix: Water
Associated Lab Samples: 92348913001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Mercury ug/L NO 0.20 07/26/1722:17
LABORATORY CONTROL SAMPLE: 2053344
Spike LCS LCS %Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Mercury ug/L 2.5 2.7 108 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2053345 2053346
MS MSD
92348930001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Mercury ug/L NO 2.5 2.5 2.3 2.3 90 90 76-125 0
Results presented on this page are in the units indicated by the "Units" column except where an a8ernate unit is presented to the right ofthe result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 11 of 41

ace Analytical
www.pscdeDscpm
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371135 Analysis Method: EPA 6010
QC Batch Method: EPA 3010A Analysis Description: 6010 MET
Associated Lab Samples: 92348913001
METHOD BLANK: 2056354
Associated Lab Samples: 92348913001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
Aluminum
ug/L
NO
100
08/01117 14:28
Antimony
ug/L
NO
5.0
08/01/17 14:28
Arsenic
ug/L
NO
10.0
08101/1714:28
Barium
ug/L
NO
5.0
08/01/17 14:28
Beryllium
ug/L
NO
1.0
08/01/17 14:28
Boron
ug/L
NO
50.0
08/01117 16:14
Cadmium
ug/L
NO
1.0
0810111714:28
Chromium
ug/L
NO
5.0
08/01117 14:28
Cobalt
ug/L
NO
5.0
08/01/17 14:28
Copper
ug/L
NO
5.0
08/01/17 14:28
Iron
ug/L
NO
50.0
08/01/17 14:28
Lead
ug/L
NO
5.0
08/01117 14:28
Magnesium
ug/L
NO
100
08/01117 14:28
Manganese
ug/L
NO
5.0
08/01/17 14:28
Nickel
ug/L
NO
5.0
08/01117 14:28
Selenium
ug/L
NO
10.0
08101/1716:14
Silver
ug/L
NO
5.0
08/01/17 14:28
Thallium
ug/L
NO
10.0
08/01/1716:14
Titanium
ug/L
NO
5.0
08/01/1716:14
Zinc
ug/L
NO
10.0
08/01/17 14:28
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
2056355
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Aluminum
ug/L
5000
4710
94
80-120
Antimony
ug/L
500
489
98
80-120
Arsenic
ug/L
500
542
108
80-120
Barium
ug/L
500
550
110
80-120
Beryllium
ug/L
500
544
109
80-120
Boron
ug/L
500
491
98
80-120
Cadmium
ug/L
500
547
109
80-120
Chromium
ug/L
500
542
108
80-120
Cobalt
ug/L
500
558
112
80-120
Copper
ug/L
500
558
112
80-120
Iron
ug/L
5000
4630
93
80-120
Lead
ug/L
500
550
110
80-120
Magnesium
ug/L
5000
4530
91
80-120
Manganese
ug/L
500
543
109
80-120
Nickel
ug/L
500
539
108
80-120
Selenium
ug/L
500
579
116
80-120
Pace Ans"cal services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Results presented on this page are in the units indicated by the "Units' column except where an a8emate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the wntten consent of Pace Analytical Services, LLC. Page 12 of 41

/JeAna1j6ca1e
I trarrpawltlzcan
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Pace Analocal Services, U-C
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2056355
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits Qualifiers
Silver
ug/L
250
242
97
80-120
Thallium
ug/L
500
555
111
80-120
Titanium
ug/L
500
492
98
80-120
Zinc
ug/L
500
552
110
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2056356
MS
92349027001
Spike
Parameter
Units
Result
Conc.
Aluminum
ug/L
NO
5000
Antimony
ug/L
NO
500
Arsenic
ug/L
NO
500
Barium
ug/L
NO
500
Beryllium
ug/L
NO
500
Boron
ug/L
NO
500
Cadmium
ug/L
NO
500
Chromium
ug/L
NO
500
Cobalt
ug/L
NO
500
Capper
ug/L
NO
500
Iron
ug/L
52.5
5000
Lead
ug/L
NO
Soo
Magnesium
ug/L
1700
5000
Manganese
ug/L
NO
500
Nickel
ug/L
NO
500
Selenium
ug/L
NO
500
Silver
ug/L
NO
250
Thallium
ug/L
NO
500
Titanium
ug/L
NO
500
Zinc
ug/L
NO
500
MSD
Spike
Conc.
2056357
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
5000
4750
4870
94
96
75-125
2
500
483
499
97
100
75-125
3
500
542
564
108
113
75-125
4
500
546
559
109
112
75-125
2
500
547
560
109
112
75-125
2
500
495
507
95
98
75-125
2
Soo
538
555
108
111
75-125
3
500
536
549
107
110
75-125
2
500
539
557
108
111
75-125
3
500
558
572
111
114
75-125
2
5000
4620
4740
91
94
75-125
2
500
527
545
105
109
75-125
3
5000
6130
6270
89
91
75-125
2
500
535
549
107
109
75-125
3
500
523
540
104
108
75-125
3
Soo
549
577
109
115
75-126
5
250
240
245
96
98
75-125
2
500
586
495
117
99
75-125
17
500
483
610
96
122
75-125
23 R1
500
546
562
108
111
75-125
3
Results presentee on this page are in the units Indicated by the "units" column except where an alternate unit a presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 41

lcmnalXicale
R pocobbs.m
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371101 Analysis Method: EPA 8260
QC Batch Method: EPA 8260 Analysis Description: 8260 MSV
Associated Lab Samples: 92348913002
METHOD BLANK: 2056233
Associated Lab Samples: 92348913002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
NO
5.0
07/30/17 00:11
1,1,2,2-Tetrachloroethane
ug/L
ND
5.0
07130117 00:11
1,1,2-Tdchloroethane
ug/L
ND
5.0
07/30/17 00:11
1,1-Dichloroethane
ug/L
NO
5.0
07130/17 00:11
1,1-Dichloroethene
ug/L
ND
5.0
07130/17 00:11
1,2-Dichloroethane
ug/L
ND
5.0
07/30117 00:11
1,2-Dichloropropane
ug/L
NO
5.0
07/30/17 00:11
2-Chloroethylvinyl ether
ug/L
NO
10.0
07/30117 00:11
2-Chlorotoluene
ug/L
ND
5.0
07/30117 00:11
4-Chlorotoluene
ug/L
NO
5.0
07130/17 00:11
Acrolein
ug/L
NO
100
07/30/17 00:11
Acrylonitrile
ug/L
NO
100
07/30117 00:11
Benzene
ug/L
NO
5.0
07/30117 00:11
Bromodichloromethane
ug/L
NO
5.0
07130117 00:11
Bromoform
ug/L
NO
5.0
07/30/17 00:11
Bromomethane
ug/L
NO
10.0
07/30/17 00:11
Carbon tetrachloride
ug/L
NO
5.0
07130117 00:11
Chlorobenzene
ug/L
NO
5.0
07130117 00:11
Chloroethane
ug/L
NO
10.0
07/30/17 00:11
Chloroform
ug/L
ND
5.0
07/30117 00:11
Chloromethane
ug/L
NO
5.0
07/30117 00:11
cis-1,3-Dichloropropene
ug/L
ND
5.0
07/30/17 00:11
Dibromochloromethane
ug/L
ND
5.0
07130/17 00:11
Ethylbenzene
ug/L
NO
5.0
07/30/17 00:11
Methylene Chloride
ug/L
ND
5.0
07130/17 00:11
Tetrachloroethene
ug/L
NO
5.0
07/30117 00:11
Toluene
ug/L
NO
5.0
07130/17 00:11
trans-1,2-Dichloroethene
ug/L
NO
5.0
07130117 00:11
trans-1,3-Dichloropropene
ug/L
NO
5.0
07/30/17 00:11
Trichloroethene
ug/L
NO
5.0
07/30/17 00:11
Vinyl chloride
ug/L
NO
5.0
07130/17 00:11
1,2-Dichloroetharle-d4 (S)
%
89
70-130
07/30/17 00:11
4-Bromofluorobenzene(S)
%
101
70-130
07130117 00:11
Toluene-d8(S)
%
97
70-130
07/30/17 00:11
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 26078
[phone]
LABORATORY CONTROL SAMPLE: 2056234
Spike LCS LCS % Rao
Parameter Units Conc. Result %Rec Limits Qualifiers
1,1,1-Tdchloroethane ug/L 50 47.2 94 71-129
1,1,2,2-Tetrachloroethane ug/L 50 44 1 88 70-124
Results preserved on Nis page are in the units indicated by Ne'9rnits" column except where an alternate unit is preserved to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 14 of 41

aceAnalytical e
wwwpace180s.corn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Sute 100
Huntersville. NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
LABORATORY CONTROL SAMPLE:
2056234
Spike
LCS
LCS
°h Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2-Tnchloroethane
ug/L
50
43.4
87
85-125
1,1-Dichloroethane
ug/L
50
44.4
89
73-126
1,1-Dichloroethene
ug/L
50
50.0
100
66-135
1,2-Dichloroethane
ug/L
50
43.9
88
67-128
1.2-Dichloropropane
ug/L
50
46.7
93
75-132
2-Chloroethylvinyl ether
ug/L
100
96.6
97
40-160
2-Chlorotoluene
ug/L
50
45.9
92
74-132
4-Chlorotolcene
ug/L
50
45A
90
76-133
Acrolein
ug/L
250
325
130
24-160
Acrylonitrile
ug/L
250
232
93
40-160
Benzene
ug/L
50
49.0
98
80-125
Bromodichloromethane
ug/L
50
46.9
94
78-124
Bromoform
ug/L
50
40.9
82
71-128
Bromomethane
ug/L
50
34.7
69
40-160
Carbon tetrachloride
ug/L
50
48.6
97
69-131
Chlorobenzene
ug/L
50
46.9
94
81-122
Chloroethane
ug/L
50
46.2
92
39-148
Chloroform
ug/L
50
44.4
89
73-127
Chloromethane
ug/L
50
51.7
103
44-146
cis-1,3-Dichloropropene
ug/L
50
45.6
91
72-132
Dibromochloromethane
ug/L
50
44.1
88
78-125
Ethylbenzene
ug/L
50
46.6
93
70-121
Methylene Chloride
ug/L
50
53.4
107
64-133
Tetrachlorcethene
ug/L
50
43.5
87
78-122
Toluene
ug/L
50
48.4
97
80-121
trans-1,2-Dichloroethene
ug/L
50
48.7
97
71-127
trans-1,3-Dichloropropene
ug/L
50
44.2
88
69-141
Trichloroethene
ug/L
50
45.3
91
78-122
Vinyl chloride
ug/L
50
51.2
102
58-137
1,2-Dichloroethane-04 (S)
%
92
70-130
4-Bromofiuorobenzene(S)
%
101
70-130
Toluene-d8(S)
%
100
70-130
MATRIX SPIKE SAMPLE:
2056235
92348343003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Tnchloroethane
ug/L
NO
400
415
104
70-130
1,1,2,2-Tetrachloroethane
ug/L
ND
400
395
99
70-130
1,1,2-Tnchloroethane
ug/L
NO
400
402
101
70-130
1. 1 -Dichloroethane
ug/L
ND
400
423
106
70-130
1,1-Dichloroethene
ug/L
ND
400
451
113
65-160
1,2-Dichloroethane
ug/L
ND
400
406
101
70-130
1,2-Dichloropropane
ug/L
NO
400
441
110
70-130
2-Chloroethylvinyl ether
ug/L
NO
800
NO
0
70-130 P5
2-Chlorotoluene
ug/L
NO
400
403
101
70-130
Results presented on Mb page are in tM arks indicated by Me 'Units' column except where an alternate unR la presented M the right of this emu t.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full.
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 41

/ ZeAnalyficale
l - ivww.PawleEs.wm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hurtersvitle, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
MATRIX SPIKE SAMPLE:
2056235
92348343003
Spike
MS
MS
% Rec
Parameter
Units
Result
Conic.
Result
%Rec
Limits Qualifiers
4-Chlorotoluene
ug/L
NO
400
398
100
70-130
Acrolein
ug/L
ND
2000
3520
176
70-130 M7
Acrylonitrile
ug/L
NO
2000
2180
109
70-130
Benzene
ug/L
NO
400
431
108
58-162
Bromodichloromethane
ug/L
NO
400
431
108
70-130
Bromoform
ug/L
ND
400
355
89
70-130
Bromomethane
ug/L
NO
400
307
77
70-130
Carbon tetrachloride
ug/L
NO
400
453
113
70-130
Chlorobenzene
ug/L
ND
400
417
104
70-138
Chloroethane
ug/L
NO
400
432
108
70-130
Chloroform
ug/L
NO
400
443
111
70-130
Chloromethane
ug/L
NO
400
440
110
70-130
cis-1,3-Dichloropropene
ug/L
NO
400
418
105
70-130
Dibromochloromethane
ug/L
NO
400
390
97
70-130
Ethylbenzene
ug/L
ND
400
409
102
22-189
Methylene Chloride
ug/L
NO
400
495
124
70-130
Tetrachloroethene
ug/L
NO
400
385
96
70-130
Toluene
ug/L
ND
400
491
110
65-152
trans-1,2-Dichloroethene
ug/L
NO
400
450
112
70-130
trans-1,3-Dichloropropene
ug/L
NO
400
383
96
70-130
Trichloroethene
ug/L
NO
400
386
96
70-142
Vinyl chloride
ug/L
NO
400
437
109
70-130
12-Dichloroethane-d4 (S)
%
98
70-130
4-Bromofiuorobenzene(S)
%
101
70-130
Toluene-d8 (S)
%
100
70-130
SAMPLE DUPLICATE' 2056236
92348343002
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichloroethane
ug/L
NO
NO
1,1.2,2-Tetrachloroethane
ug/L
NO
NO
1,1,2-Trichloroethane
ug/L
NO
NO
1.1-Dichloroethane
ug/L
NO
ND
1,1-Dichloroethene
ug/L
NO
ND
1,2-Dichloroethane
ug/L
NO
NO
1,2-Dichloropropane
ug/L
NO
ND
2-Chloroethylvinyl ether
ug/L
NO
NO
2-Chlorotoluene
ug/L
NO
NO
4-Chlorotoluene
ug/L
NO
NO
Acrolein
ug/L
NO
NO
Acrylonitrile
ug/L
NO
NO
Benzene
ug/L
NO
NO
Bromodichloromethane
ug/L
NO
NO
Bromoform
ug/L
NO
NO
Bromomethane
ug/L
NO
NO
Results presented on this page are In the units Indicated by Me "Unto" column except where an ahemate unit is presented to Me right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC, Page 16 of 41

IceAnaliticale
www.pacelabs.cam
i
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
SAMPLE DUPLICATE: 2056236
Parameter
Units
92348343002
Result
Dup
Result
Carbon tetrachloride
ug/L
NO
ND
Chlorobenzene
ug/L
NO
NO
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
NO
NO
Chloromethane
ug/L
NO
ND
cis-1,3-Dichloropropene
ug/L
ND
NO
Dibromochloromethane
ug/L
NO
ND
Ethylbenzene
ug/L
NO
ND
Methylene Chloride
ug/L
NO
NO
Tetrachloroethene
ug/L
NO
NO
Toluene
ug/L
3590
3670
trans-1,2-Dichloroethene
ug/L
ND
NO
trans-1,3-Dichloropropene
ug/L
ND
NO
Trichloroethene
ug/L
NO
ND
Vinyl chloride
ug/L
ND
NO
1,2-Dichloroethane-d4 (S)
%
99
101
4-Bromofluorobenzene (S)
%
106
99
Toluene-d8 (S)
e/
98
99
RPD Qualifiers
2
2
7
1
Pace Anatytical Services, LLC
9800 KinceyAve. Suite 100
Huntersville, NC 28078
[phone]
Resuits presented on this page are in the unite Indicated by the "Units" column except where an attemate unit b presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC, Page 17 of 41

-PaceAnalytical
/ euavpacelabsco.
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 700
Huntersville, NC 28078
[phone]
Project: Annual Sampling 07125/17
Pace Project No.: 92348913
QC Batch: 370645
Analysis Method:
EPA 8081
QC Batch Method: EPA3510
Analysis Description.
8081AGCS Pesticides
Associated Lab Samples: 92348913002
METHOD BLANK: 2053818
Matrix:
Water
Associated Lab Samples: 92348913002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
4,4'-DDD
ug/L
NO
0.050
07126/17 20:12
4,4'-DDE
ug/L
ND
0.050
07126/17 20:12
4,4'-DDT
ug/L
ND
0.050
07/26/17 20:12
Aldrin
ug/L
ND
0.050
07/26/17 20:12
alpha-BHC
ug/L
ND
0.050
07/26/17 20:12
beta-BHC
ug/L
ND
0.050
07/26/17 20:12
Chlordane (Technical)
ug/L
NO
0.20
07/26117 20:12
delta-BHC
ug/L
ND
0,050
07/26/17 20:12
Dieldrin
ug/L
ND
0.050
07/26/17 20:12
EndosulfanI
ug/L
NO
0,050
07126/17 20:12
Endosulfan It
ug/L
NO
0.050
07126/17 20:12
Endosulfan sulfate
ug/L
ND
0.050
07126/17 20:12
Endrin
ug/L
NO
0.050
07/26/17 20:12
Endrin aldehyde
ug/L
NO
0.050
07/2611720:12
Endrin ketone
ug/L
ND
0.050
07126/17 20:12
gamma-BHC (Lindane)
ug/L
ND
0.050
07/26/17 20:12
Heptachlor
ug/L
ND
0.050
07126117 20:12
Heptachlor epoxide
ug/L
ND
0.050
07/26/17 20:12
Methoxychlor
ug/L
ND
0.15
07/26/17 20:12
Toxaphene
ug/L
ND
0.20
07/26/17 20:12
Decachlorobiphenyl (S)
%
64
20-130
07/26117 20:12
Tetrachloro-m-xylene (S)
%
84
20-130
07/26/17 20:12
LABORATORY CONTROL SAMPLE 8 LCSD:
2053819
2053820
Spike
LCS
LCSD
LCS LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec % Rec
Limits RPD
RPD Qualifiers
4,4'-DDD
ug/L
.25
0.20
0.23
80 92
20-150
13
30
4,4'-DDE
uWL
.25
0.19
0.22
75 87
20-150
15
30
4,4'-DDT
ug/L
.25
0.19
0.23
78 94
20-150
19
30
Aldrin
ug/L
.25
0.15
0.17
61 69
20-150
13
30
alpha-BHC
ug/L
.25
0.17
0.20
70 82
20-150
16
30
beta-BHC
ug/L
.25
0.16
0.18
64 74
20-160
16
30
delta-BHC
ug/L
.25
0.17
0.21
70 84
20-150
18
30
Dieldrin
ug/L
.25
0.19
0.21
78 85
20-150
9
30
Endosulfan I
ug/L
.25
0.19
0.22
78 87
20-150
12
30
Endosulfan II
ug/L
.25
0.20
0.22
80 89
20-150
11
30
Endosulfan sulfate
ug/L
.25
0.20
0.23
80 91
20-150
13
30
Endrin
ug/L
.25
0.20
0.23
82 92
20-150
11
30
Endrin aldehyde
ug/L
.25
0.18
0.21
71 83
20-150
15
30
Endrin ketone
ug/L
.25
0.19
0.21
78 87
20-150
11
30
Results presented on this page are in the units Indicated by the-UnW column exceptwhere an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Date08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 18 of 41

aceAna1j6ca1a
/ wwwysp6Atcpn
QUALITY CONTROL DATA
Pace Ana"cal Services, LLC
9800 Kincey Ave. Suite 100
Hunlersvile, NC 26078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
LABORATORY CONTROL SAMPLE 8 LCSD:
2053819
2053820
Spike
LCS
LCSD
LCS
LCSD
% Rec
Max
Parameter
Units
Conc.
Result
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
gamma-BHC (Lindane)
ug/L
.25
0.18
0.21
72
84
20-150
16
30
Heptachlor
ug/L
.25
0.15
0.19
62
76
20-150
20
30
Heptachlor epoxide
ug/L
.25
0.17
0.21
70
84
20-150
19
30
Methoxychlor
ug/L
.74
0.64
0.70
86
94
20-150
9
30
Decachlorobiphenyl(S)
%
69
80
20-130
Tetrachloro-m-xytene (S)
%
85
96
20-130
Results presented on this page are in the units indicated by Me "Unxs"column except where an ahemate unit Is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall Trot be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 19 of 41

aceAnalytical'
QUALITY CONTROL DATA
Pace Analytical Services. LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Annual Sampling 07126/17
Pace Project No.: 92348913
QC Batch: 370359
Analysis Method: EPA 8082
QC Batch Method: EPA 3510
Analysis Description: 8082 GCS PCB
Associated Lab Samples: 92348913002
METHOD BLANK: 2052153
Matrix: Water
Associated Lab Samples: 92348913002
Blank Reporting
Parameter
Units
Result Limit
Analyzed
Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
NO 0.50
07/26/17 20:30
PCB-1221 (Aroclor 1221)
ug/L
ND 0.50
07/26/17 20:30
PCB-1232 (Aroclor 1232)
ug/L
ND 0.50
07/26/17 20:30
PCB-1242 (Aroclor 1242)
ug/L
ND 0.50
07/26/17 20:30
PCB-1248 (Aroclor 1248)
ug/L
ND 0.50
07/26/17 20:30
PCB-1254 (Aroclor 1254)
ug/L
NO 0.50
07/26/17 20:30
PCB-1260 (Aroclor 1260)
ug/L
ND 0.50
07/26/17 20:30
Decachlorobiphenyl (S)
%
72 10-132
07/26/17 20:30
LABORATORY CONTROL SAMPLE & LCSD:
2052154
2052155
Spike LCS LCSD
LCS LCSD
% Rec Max
Parameter
Units
Cone. Result Result
% Rec % Rec
Limits RPD RPD Qualifiers
PCB-1016 (Aroclor 1016)
ug/L
5 4.1 4.5
81 90
50-150 10 30
PCB-1260 (Aroclor 1260)
ug/L
5 3.2 3.3
65 67
50-150 3 30
Decachlorobiphenyl (S)
%
83 84
10-132
Results presented on this page are in the units indicated by the 'Units" column except where an ahemate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 20 of 41

aceAnalytical e
eneepacslabscom
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 370788 Analysis Method: EPA 8270
QC Batch Method: EPA 3510 Analysis Description: 8270 Water MSSV
Associated Lab Samples: 92348913002
METHOD BLANK: 2054651
Associated Lab Samples: 92348913002
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,2,4-Tdchlorobenzene
ug/L
NO
10.0
07/28/17 11:01
1,2-Dichlorobenzene
ug/L
NO
10.0
07/28/1711:01
1,3-Dichlorobenzene
ug/L
NO
10.0
07128/1711:01
1,4-Dichlorobenzene
ug/L
NO
10.0
07/2811711:01
1-Methylnaphthalene
ug/L
NO
10.0
07/28/17 11:01
2,2'-Oxybis(1-chloropropane)
ug/L
NO
10.0
07/28/17 11:01
2,4,5-Tdchlorophenol
ug/L
NO
10.0
07/28/17 11:01
2,4,6-Tdchlorophenol
ug/L
NO
10.0
07128/1711:01
2,4-Dichlorophenol
ug/L
NO
10.0
07/28/17 11:01
2,4-Dimethylphenol
ug/L
NO
10.0
0712811711:01
2,4-Dinitrophenol
ug/L
NO
50.0
07/28/17 11:01
2,4-Dinitrotoluene
ug/L
NO
10.0
07/28/17 11:01
2,6-Dinitrotoluene
ug/L
NO
10.0
07/28/17 11:01
2-Chloronaphthalene
ug/L
NO
10.0
07/28/17 11:01
2-Chlorophenol
ug/L
NO
10.0
07/28/17 11:01
2-Methylnaphthalene
ug/L
NO
10.0
07/28/17 11:01
2-Methylphenol(o-Cresol)
ug/L
NO
10.0
07/2811711:01
2-Nitroaniline
ug/L
NO
50.0
07/28/17 11:01
2-Nitrophenol
ug/L
NO
10.0
07/28/17 11:01
3&4-Methylphenol(m&p Cresol)
ug/L
NO
10.0
07/28/17 11:01
3,3'-Dichlorobenzidine
ug/L
NO
20.0
07/2811711:01
3-Nitroaniline
ug/L
NO
50.0
07/28/17 11:01
4,6-Dinitrc-2-methylphenol
ug/L
NO
20.0
07/28/17 11:01
4-Bromophenylphenyl ether
ug/L
NO
10.0
07/28/17 11:01
4-Chloro-3-methylphenol
ug/L
NO
20.0
0712811711:01
4-Chloroaniline
ug/L
NO
20.0
07/28/17 11:01
4-Chlorophenylphenyl ether
ug/L
NO
10.0
07/2W17 11:01
4-Nitroaniline
ug/L
NO
20.0
07/28/17 11:01
4-Nitrophenol
ug/L
NO
50.0
07/28/17 11:01
Acenaphlhene
ug/L
NO
10.0
07/28/17 11:01
Acenaphthylene
ug/L
NO
10.0
07/28/17 11:01
Aniline
ug/L
NO
10.0
07/28/17 11:01
Amhracene
ug/L
NO
10.0
07128/1711:01
Benzo(a)anthracene
ug/L
NO
10.0
07/28/17 11:01
Benzo(a)pyrene
ug/L
NO
10.0
07/28/17 11:01
Benzo(b)fluoranlhene
ug/L
NO
10.0
07128/1711:01
Benzo(g.h,i)perylene
ug/L
NO
10.0
07/28/17 11:01
Benzo(k)fluoranthene
ug/L
NO
10.0
07/2811711:01
Benzoic Acid
ug/L
NO
50.0
07/28/17 11:01
Benzyl alcohol
ug/L
NO
20.0
07/28/17 11:01
bis(2-Chloroethoxy)methane
ug/L
NO
10.0
07/28/17 11:01
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Results presented as this page am In the was Indicated by ate "Unks" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/042017 0520 PM without the written consent of PaceAnalytical Services, LLC Page 21 of 41

aceAnalytical e
www.pacela6.ccam
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
METHOD BLANK: 2054651
Matrix:
Water
Associated Lab Samples: 92348913002
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
bis(2-Chlormthyl) ether
ug/L
ND
10.0
07/28/17 11:01
bis(2-Ethylhexyl)phthalate
ug/L
ND
6.0
07/28/1711:01
Bulyibenzylphthalate
ug/L
ND
10.0
07/2a11711:01
Chrysene
ug/L
ND
10.0
07/28/17 11:01
Di-n-butylphthalate
ug/L
ND
10.0
07/28/17 11:01
Di-n-oWphthalate
ug/L
ND
10.0
07/28/1711:01
Dibenz(a,h)anthracene
ug/L
ND
10.0
07/28/17 11:01
Dibenzofuran
ug/L
ND
10.0
07/28/17 11:01
Diethylphthalate
ug/L
NO
10.0
07/28/17 11:01
Dimethylphthalate
ug/L
NO
10.0
07128/1711:01
Fluoranlhene
uglL
NO
10.0
07/28/17 11:01
Fluorene
ug/L
NO
10.0
07/28/17 11:01
Hexachloro-1,3-butadiene
ug/L
ND
10.0
0712811711:01
Hexachlorobenzene
ug/L
NO
10.0
07128/1711:01
Hexachlorocyclopentadiene
ug/L
NO
10.0
07/28/17 11:01
Hexachloroethane
ug/L
NO
10.0
07/28117 11:01
Indeno(1,2,3-cd)pyrene
ug/L
NO
10.0
07/28117 11:01
Isophorone
ug/L
ND
10.0
07/28/17 11:01
N-Nitroso-di-n-propylamine
ug/L
ND
10.0
07128/17 11:01
N-Nitrosodimethylamine
ug/L
ND
10.0
07128/1711:01
N-Nitrosodiphenylamine
ug/L
ND
10.0
07/28/17 11:01
Naphthalene
ug/L
ND
10.0
07/28/17 11:01
Nitrobenzene
ug/L
ND
10.0
07/28/17 11:01
Pentachlorophenol
ug/L
ND
25.0
07/28/17 11:01
Phenanthrene
ug/L
ND
10.0
07/28/1711:01
Phenol
ug/L
ND
10.0
07/28117 11:01
Pyrene
ug/L
ND
10.0
07/28/17 11:01
2,4,6-Tribromophenol(S)
%
41
27-110
07/28/17 11:01
2-Fluorobiphenyl(S)
%
90
27-110
07/28/17 11:01
2-Fluorophenol(S)
%
44
12-110
07/28/17 11:01
Nitrobenzene-d5(S)
%
83
21-110
07/28N7 11:01
Phenol-d6 (S)
%
33
10-110
07/28/17 11:01
Terphenyld14 (S)
%
99
31-107
07/28/17 11:01
Qualifiers
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE &LCSD:
2054652
2054653
Spike
LCS
LCSD
LCS
LCSD
%Rec
Max
Parameter
Units
Cone.
Result
Result
% Rec
% Rae
Limits
RPD
RPD
1,2,4-Trichlorobenzene
ug/L
50
33.1
31.3
66
63
31-120
6
30
1,2-Dichlombenzene
ug/L
50
30.4
32.9
61
66
38-120
8
30
1,3-Dichlorobenzene
ug/L
50
28.1
28.2
56
56
30-122
0
30
1,4-Dichlorobenzene
ug/L
50
30.9
30.6
62
61
37-120
1
30
1-Methylnaphthalene
ug/L
50
42.6
39.2
85
78
34-113
8
30
2,2'-Oxybis(1-chloropropane)
ug/L
50
30.5
32.1
61
64
18-120
5
30
2,4,5-Trichlorophenol
ug/L
50
45A
41.2
90
82
43-113
9
30
Results presented on this page are In the units indicated by the "Units" column except where an aitemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
Qualifiers
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC, Page 22 of 41

aceAnalytical e
wwwpacebbs.com
QUALITY CONTROL DATA
Pace Andt"cal Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
LABORATORY CONTROL SAMPLE & LCSD:
2054652
2054653
Spike
LCS
LCSD
1-CS
LCSD
% Rec
Max
Parameter
Units
Conc.
Resuh
Result
% Rec
% Rec
Limits
RPD
RPD Qualifiers
2,4,6-Thchlorophenol
ug/L
50
49.0
46.7
98
93
42-120
5
30
2,4-Dichlorophenol
ug/L
50
41.9
39.8
84
80
30-120
5
30
2,4-Dimethylphenol
ug/L
50
42.4
43.3
85
87
29-111
2
30
2,4-Dinitrophenol
ug/L
250
234
227
94
91
19-132
3
30
2,4-Dinbrotoluene
ug/L
50
49.1
49.1
98
98
58-128
0
30
2,6-Dinitrotoluene
ug/L
50
51.1
50.6
102
101
54-129
1
30
2-Chloronaphthalene
ug/L
50
47.3
47.7
95
95
43-117
1
30
2-Chlorophenol
ug/L
50
37.0
40.7
74
81
37-120
9
30
2-Melhylnaphthalene
ug/L
50
41.3
38.7
83
77
33-120
6
30
2-Methylphenol(o-Cresol)
ug/L
50
31.2
35.9
62
72
31-120
14
30
2-Nitroaniline
ug/L
100
80.9
77.0
81
77
48-121
5
30
2-Nitrophenol
ug/L
50
40.9
41.1
82
82
25-116
0
30
3&4-Methylphenol(m&p Cresol)
ug/L
50
52.9
59.9
106
120
23-120
12
30
3,3'-Dichlorobenzidine
ug/L
100
77.2
75.3
77
75
10.154
3
30
3-Nitroaniline
ug/L
100
88.8
85.8
89
86
43-115
3
30
4,6-Dinitro-2-methylphenol
ug/L
100
92.6
92.2
93
92
44-124
0
30
4-Bromophenylphenyl ether
ug/L
50
38.1
37.2
76
74
34-113
2
30
4-Chloro-3-methylphenol
ug/L
100
84.1
83.4
84
83
31-110
1
30
4-Chloroaniline
ug/L
100
61.8
60.2
62
60
20-120
3
30
4-Chtorophenylphenyl ether
ug/L
50
42.8
41.4
86
83
34-116
3
30
4-Nitroaniline
ug/L
100
96.5
97.7
96
98
46-128
1
30
4-Nitrophenol
ug/L
250
111
102
44
41
11-120
8
30
Acenaphthene
ug/L
50
46.3
45.2
93
90
48-114
2
30
Acenaphthylene
ug/L
50
43.8
42.7
88
85
48-112
2
30
Aniline
ug/L
50
21.4
20.6
43
41
26-120
4
30
Anthracene
ug/L
50
42.9
42.7
86
85
57-118
1
30
Senzo(a)anthracene
ug/L
50
41.8
41.8
84
84
56-121
0
30
Benzo(a)pyrene
ug/L
50
42.9
42.8
86
86
55-127
0
30
Benzo(b)fluoranthene
ug/L
50
44.7
43.5
89
87
53-128
3
30
Benzo(g,h,i)perylene
ug/L
50
43.9
52.5
88
105
54-125
18
30
Benzo(k)fluoranthene
ug/L
50
42.4
42.2
85
84
51-123
0
30
Benzoic Acid
ug/L
250
95.4
84.7
38
34
10-120
12
30
Benzyl alcohol
ug/L
100
64.4
72.4
64
72
27-120
12
30
bis(2-Chloroethoxy)methane
uglL
50
37.7
35.1
75
70
32-120
7
30
bis(2-Chloroethyl) ether
ug/L
50
38.1
41.2
76
82
33-111
8
30
bis(2-Ethylhexyl)phthalate
ug/L
50
45.1
44.2
90
88
50-145
2
30
Butylbenzylphthalate
ug/L
50
45.5
44.0
91
88
54-138
3
30
Chryserre
ug/L
50
42.3
41.8
85
84
68-127
1
30
Di-n-butylphthalate
ug/L
50
46.6
46.5
93
93
56-125
0
30
Di-n-octylphthalate
ug/L
50
45.7
44.6
91
89
50-134
2
30
Dibenz(a,h)anthracene
ug/L
50
45.0
52.3
90
105
53-129
15
30
Dibenzofuran
ug/L
50
45.8
45.1
92
90
45-120
2
30
Diethylphthalate
ug/L
50
48.7
48.1
97
96
53-120
1
30
Dimethylphlhalate
uglL
50
49.7
49.0
99
98
55-116
1
30
Fluoranthene
ug/L
50
45.1
45.4
90
91
57-125
1
30
Fluorene
ug/L
50
46.2
44.9
92
90
53-118
3
30
Hezachloro-13-butadiene
ug/L
50
29.3
28.9
59
58
23-120
1
30
Results presented on this page are In the units indicated by the "Units"
column
except where an aitemate
unit Is
presented to the debt or the
result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the writlen consent of Pace Analytical Services, LLC. Page 23 of 41

ceAnalytical
_ etswpapa'aDs.mm
I
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE & LCSD:
Parameter
2054652
Units
Spike
Conc.
2054653
LCS LCSD
Result Result
LCS LCSD
% Rec % Rec
% Rec
Limits
RPD
Max
RPD Qualifiers
Hexachlorobenzene
ug/L
50
44.4
43.4
89
87
49-116
2
30
Hexachlorocyclopentadiene
ug/L
50
34.5
31.4
69
63
26-158
9
30
Hexachloroethane
ug/L
50
27.5
28.8
55
58
30-114
5
30
Indeno(1,2,3-cd)pyrene
ug/L
50
47.4
54.7
95
109
55-128
14
30
Isophorone
ug/L
50
40.9
39.2
82
78
31-118
4
30
N-Nitros"i-n-propylamine
ug/L
50
42.5
46.2
85
92
32-119
8
30
N-Nitrosodimethylamine
ug/L
50
26.8
28.0
54
56
13-120
4
30
N-Nitrosodiphenylamine
ug/L
50
42.3
41.4
85
83
43-120
2
30
Naphthalene
ug/L
50
37.8
37.0
76
74
32-120
2
30
Nitrobenzene
ug/L
50
40.0
36.9
80
74
33-110
8
30
Pentachlorophenol
ug/L
100
91.7
92.0
92
92
10-137
0
30
Phenanthrene
ug/L
50
42.2
42.0
84
84
57-117
0
30
Phenol
ug/L
50
20.8
23.0
42
46
10-120
10
30
Pyrene
ug/L
50
39.2
39.7
78
79
55-122
1
30
2,4,6-Tdbromophenol(S)
%
96
90
27-110
2-Fluorobiphenyl(S)
%
91
86
27-110
2-Fluorophenol(S)
%
50
49
12-110
Nitrobenzene-d5(S)
%
85
77
21-110
Phenol-d6 (S)
%
33
36
10-110
Terpher l-d14(S)
%
97
91
31-107
Results presented on this page are In the units indicated by Me "Units" column except where an alternate unit is presented to the right of Me result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 41

aceAnalytical e
.pacelabs. com
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 370915
QC Batch Method: SM 4500-S2D
Associated Lab Samples: 92348913002
METHOD BLANK: 2055361
Associated Lab Samples: 92348913002
Parameter Units
Sulfide nlg/L
LABORATORY CONTROL SAMPLE: 2055362
Parameter Units
Sulfide mg/L
QUALITY CONTROL DATA
Analysis Method:
Analysis Desrxiption.
Matrix: Water
SM 4500-S2D
4500S2D Sulfide Water
Pace Analytical services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Blank Reporting
Result Limit Analyzed Qualifiers
NO 0.10 07/3111717:42
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.5 0.53 105 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2055363 2055364
MS MSD
92348902005 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L ND .5 .5 0.44 0.44 80 80 80-120 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2055365 2055366
MS MSD
92349104001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Sulfide mg/L NO .5 .5 0.48 0.48 96 96 80-120 0
Results presented on this page are In the units Indicated by Me "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Dale: 08/04/2017 05:20 PM without the written consent of Pace Analytcal Services. LLC.
Page 25 of 41

ace Analytical e
wvmpace/abscdm
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 370558 Analysis Method: EPA300.0
QC Batch Method: EPA 300.0 Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92348913001
METHOD BLANK: 2053285 Matrix: Water
Associated Lab Samples: 92348913001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Fluoride mg/L NO 0.10 07/30/17 13:26
Sulfate mg/L NO 1.0 07/3011713:26
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2053286
Spike LCS LCS % Rae
Parameter Units Cone. Result % Rec Limits Qualifiers
Fluoride mg/L 2.5 2.7 108 90-110
Sulfate ni 50 54.4 109 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2053287
2053288
MS
MSD
92348833001 Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter Units Result Cone.
Cone.
Result
Result
% Rae % Rae
Limits RPD Qual
Fluoride ng/L 10.9 2.5
2.5
14.5
13.9
146 120
90-110 5 M6
Sulfate mg/L 5760 50
50
5770
5740
33 -32
90-110 1 M6
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
2053289
2053290
MS
MSD
92348730008 Spike
Spike
MS
MSD
MS MSD
%Rec
Parameter Units
Result Cone.
Cone.
Result
Result
% Rae % Rae
Limits RPD Qual
Fluoride mg/L
NO 2.5
2.5
3.4
3.4
134 135
90-110 0 Mt
Sulfate rng/L
5.2 50
50
75.1
75.1
140 140
90-110 0 Mt
Results presented on this page are In the units indicated by the "Units" column except where an ahemate unit Is presented to the rightof the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/042017 05:20 PM without the written consent of Pace Analytical Services. LLC.
Page 26 of 41

aceAnalytical e
www_pacelabs. rom
QUALITY CONTROL DATA
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371344 Analysis Method: EPA 350.1 1993 Rev 2.0
QC Batch Method: EPA 350.1 1993 Rev 2.0 Analysis Description: 350.1 Ammonia
Associated Lab Samples: 92348913001
METHOD BLANK: 2057310
Associated Lab Samples: 92348913001
Parameter Units
Nitrogen, Ammonia mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 08/01/1714:42
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2057311
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 4.9 98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057312 2057313
MS MSD
92348842027 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conic. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 1.7 5 5 6.4 6.4 94 94 9D-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2067314 2057315
MS MSD
92348913001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L ND 5 5 4.9 4.9 98 98 90-110 0
Results presented on this page are In the units Indicated by Me "Units" column except where an Where ate unit is presented to the night of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not t e reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pare Analytical Services, LLC.
Page 27 of 41

aceAnalytical
' awwpacelabscom
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371277
Analysis Method: EPA 353.2
QC Batch Method: EPA 353.2
Analysis Description: 353.2 Nitrate + Nitrite, preserved
Associated Lab Samples: 92348913001
METHOD BLANK: 2057068
Matrix: Water
Associated Lab Samples: 92348913001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Nitrogen, NO2 plus NO3 mg/L
ND 0.020
08/01/17 03:54
LABORATORY CONTROL SAMPLE: 2057069
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
%Rec Limits Qualifiers
Nitrogen, NO2 plus NO3 mg/L
2.5
2.5
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057070
2057071
MS
MSD
92349334008
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Nitrogen, NO2 plus NO3 mg/L NO
2.5
2.5 2.6
2.6 103 102
75-125
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057072
2067073
MS
MSD
92349326001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Nitrogen, NO2 plus NO3 mg/L 8.3
2.5
2.5 10.9
11.0 104 109
75-125
1
Results presented on this page are in the units indicated by Me "Units' column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced. except in full,
Dale: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 28 of 41

e
aceAnalytical
wwx PacelabSCem
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersvdle, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
OC Batch: 370723
Analysis Method: EPA 420A
QC Batch Method: EPA420.4
Analysis Description: 420.4 Phenolics
Associated Lab Samples: 92348913002
METHOD BLANK: 2054277
Matrix: Water
Associated Lab Samples: 92348913002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Phenol mg/L
NO 0.010
07/31/1713:32
LABORATORY CONTROL SAMPLE: 2054278
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
%Rec Limits
Qualifiers
Phenol mg/L
.05
0,049
98 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2054279
2054280
MS
MSD
92347765002
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Phenol mg/L 43.7
.05
.05 0.16
0.16 235
240
90-110
2 M1
ug/L
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2054281
2054282
MS
MSD
92348521002
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Phenol rig/L 1.5
.05
.05 1.5
1.5 2
-44
90-110
2 M6
Res ohs presented on this page are In the units indicated by the "Units' column except where an ahemate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/042017 05:20 PM without the written consent of Pace Analytical Services, LLC.
Page 29 of 41

IceAnalytical"
www.pace/abll
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suee 100
Huntersville, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
QC Batch: 371302
Analysis Method: SM 4500-CN-E
OC Batch Method: SM 4500-CN-E
Analysis Description: 450OCNE Cyanide, Total
Associated Lab Samples: 92348913002
METHOD BLANK: 2057187
Matrix: Water
Associated Lab Samples: 92348913002
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Cyanide mg/L
ND 0.0080
08102/1705:26
LABORATORY CONTROL SAMPLE: 2057188
Spike
LCS
LCS % Rec
Parameter Units
Cone.
Result
% Rec Limits Qualifiers
Cyanide mg/L
.1
0,099
99 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057189
2057190
MS
MSD
92349156001
Spike
Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec % Rec
Limits
RPD Qual
Cyanide mg/L ND
.1
.1 0.099
0.096 94 90
80-120
3
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057191
2057192
MS
MSD
92348937001
Spike
Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Cone.
Cone. Result
Result % Rec % Rec
Limits
RPO Qual
Cyanide mg/L ND
.1
.1 0.11
0.10 104 94
80-120
10
Results presented on this page are In the units indicated by Me "Units' column except where an aitemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services. LLC.
Page 30 of 41

aceAnalytical
sww.patz6W.cdm
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvile, NC 28078
[phone]
Project: Annual Sampling 07/25/17
Pace Project No: 92348913
QC Batch: 371309
Analysis Method: SM 5310B
QC Batch Method: SM 5310B
Analysis Description: 5310E TOC
Associated Lab Samples: 92348913001
METHOD BLANK: 2057215
Matrix: Water
Associated Lab Samples: 92348913001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Total Organic Carbon mg/L
NO 1.0
08/02/17 18:51
LABORATORY CONTROL SAMPLE: 2057216
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Total Organic Carbon mg/L
25
23.4
94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057217
2057218
MS
MSD
92349334008
Spike
Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Quai
Total Organic Carbon mg/L 4.0
25
25 26.4
26.1 90 88
90-110
1 M1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2057219
2057220
MS
MSD
92348968003
Spike
Spike MS
MSD MS MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Total Organic Carbon mg/L 1.4
25
25 23.6
23.7 89 89
90-110
0 M1
Results presented on this page are in the units indicated by Me "Units" column except where an aaemate end is presented to Me fight of the result
REPORT OF LABORATORY ANALYSIS
This report shell not be reproduced, except in full,
Date: 08/04/2017 05,20 PM without the written consent of Paco Analytical Services, LLC.
Page 31 of 41

aceAnalytical e
waw.parolaDs.wm
Project: Annual Sampling 07125117
Pace Project No.: 92348913
QC Batch: 370541
QC Batch Method: EPA 7196
Associated Lab Samples: 92348913001
METHOD BLANK: 2053247
Associated Lab Samples: 92348913001
Parameter
Chromium, Hexavalent
QUALITY CONTROL DATA
Analysis Method: EPA 7196
Analysis Description: 7196 Chromium, Hexavalent
Matrix: Water
Blank Reporting
Units Result Limit Analyzed Qualifiers
mg/L ND 0.010 07/26/1705:41
Pace Analytical services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2053248
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Chromium, Hexavalent mg/L .25 0.27 107 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2053249 2053250
MS MSD
92348913001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chromium, Hexavalent mg/L NO .25 .25 0.20 0.20 79 80 75-125 1
Results presented on this page are In the units indicated by Me 'Units" column except where an ahemate unit is presented to Me right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date. 08/04/2017 05:20 PM without the written consent of Pace Analytical Services. LLC.
Page 32 of 41

Pace Analytical services, LLC
2ceAnalyticala 9800 noey Ave. Suke
Huntersville, NC 28078078
.Pacelabs co, [phone]
QUALIFIERS
Project: Annual Sampling 07/25/17
Pace Project No.: 92348913
DEFINITIONS
DF - Dilution Factor. if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL-Adjusted Method Detection Limit.
PQL- Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitmsodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PAST -A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI-E Pace Analytical Services - Eden
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
PS The EPA or method required sample preservation degrades this compound, therefore acceptable recoveries may not be
achieved in sample matrix spikes.
R1 RPD value was outside control limits.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the wnaen consent of Pace Analytical Services, LLC, Page 33 of 41

aceAnalytical e
s+rw:PsoekGs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Annual Sampling 07/25/17
92348913
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92348913002
Effluent Grab
SM 2120E Color ADM[
370563
92348913002
Effluent Grab
EPA 1664E
371460
92348913002
Effluent Grab
EPA 3510
370645
EPA 8081
370726
92348913002
Effluent Grab
EPA 3510
370359
EPA 8082
370550
92348913001
Effluent Comp
EPA 3010A
371135
EPA6010
371329
92348913001
Effluent Comp
EPA 7470
370574
EPA 7470
370636
92348913002
Effluent Grab
EPA 3510
370788
EPA 8270
370919
92348913002
Effluent Grab
EPA 8260
371101
92348913002
Effluent Grab
SM 4500-S213
370915
92348913001
Effluent Comp
EPA 300.0
370558
92348913001
Effluent Comp
EPA 350.1 1993 Rev 2.0
371344
92348913001
Effluent Comp
EPA 353.2
371277
92348913002
Effluent Grab
EPA 420.4
370723
92348913002
Effluent Grab
SM 4500-CN-E
371302
92348913001
Effluent Comp
SM 5310B
371309
92348913001
Effluent Comp
EPA 7196
370541
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 08/04/2017 05:20 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 41

vocen, Name:
.r Sample ConditionumUpon Rec
/- aceAnarytical• nnnimant Nn-
Laboratory receiving samples:
Asheville ❑ EdenO Greenwood ❑
Document Nevisea: Sept. 21, lUlb
eipt(SCUR) Page 1 of 2
Issuing Authority:
)1 Pace Quality Office
Huntersville b Raleigh❑ Mechanicsville❑
I Client Name:
_-1 n Project p
Courier: ❑rd Ex UPS ❑USPS — ❑Client
❑ Commercial ( ace ❑Other:
Custod Seal Present? s�Y' o (� �.
Y ❑Ves � o Seals Intact. ❑Yes No
Date/Initials Person Examining C.4-._2 2S �
Packing Material: ❑Bubble Wrap []Bubble Bags c[allone ❑Other:_
Thermometer•
--�-•�L"C�� •%Jet ❑Blue
_�✓R Gun ID:-+--�->� Type of Ice:
Correction Factor: Cooler Temp Corrected ('C): • ?
Temp should be above f eefing to 6'C
USDA Regulated Soil (RN/A, water sample)
❑DidYes (�b sample -orriginate In a quarantine zone within the United States: CA, NY, or SC (check maps)?
WO#:92348913
II' III'llll III
92348913
❑None �Pamples on ice, cooling p ocess has begun
Biological Tissue Frozen? []Yes o ❑N/A
Did samples originate from a foreign source (in ter ationally,
including Hawaii and Puerto Rico)? ❑Yes No
Comments/Discrepancy:
Chain of Custody Present?
Y6s
No
N/A
1.
Sam les Arrived within Hold Time?
_ s
ONO
N/A
2.
Short Hold Time Analysis (<72 hr.)?
No
N/A
3.
Rush Turn Around Time Requested?
❑Yes
I. IQo
N/A
4.
Sufficient Volume?
t yes
ONO
❑N/A
S.
Correct Containers Used?
-Pace Containers Used?
.F7
es
ONO
ONO
❑N/A
❑N/A
6.
Containers Intact?
es
ONO
N A
7.
Samples Field Filtered?
Oyes
ONO
/A
B. Note Ifsediment is visible in the dissolved container
Sample Labels Match COC?
-Includes Date/rime/ID/Analysis Matrix:
11 _ 'Cles
❑No
❑N/A
9. t`t'YlcC od � (v cmo `�
1` \
Headspace in VOAVials (>5-6mm)?
QYeS
ONO
/A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
❑Yes
❑Yes
Q o
❑No
❑N/A
N/A
11.
CLIENT NOTIFICATION/RESOLUTION
Person Contacted:
Commen',:•/Sample
Discrepancy:
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes ❑No
Date/Tme:
Date: , j 1, J0
Date: 41 L. U0 }
Note: Whenever there is a discrepancy affecting North Carolina compliance samples, a copy of this farm will be sent to the North Carolina DEHNR Certification Office (i.e.
Out of hold, incorrect preservative, out of temp, incorrect containers)
Page 35 of 41

Document Name:
Document Revised: Sept. 21, 2016
Sample Condition Upon ReceiptlSCURI
Page 2 of 2
Document No.:
Issuing Authority:
AnalXical'
P�a
F-CAR-CS-033-Rev.01
Pace Quality Office
'Check mark top half of box if pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles
Project k 1
WO#:92348913
PM: MWB Due Date: 08/08/17
CLIENT: 92-Interface
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Sample ID
Type of preservative
pH upon receipt
Date preservation adjusted
Time preservation
adjusted
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added
lot p
Page 36 of 41

4 CHAIN -OF -CUSTODY I Analytical Request Document
PaeeAnalytieal The Cram -of -Custody is a LEGAL DOCUMENT. All relevant Gelds must be completed accurately
sone'scelaas<om
Section A Section IS Section C
P. / of
Required C6en1 Information : Required Protect Information. Invoice Information.
Company Retad To Auomion.
Address.
brli_
Copy To:
Company Name:
'
REGULATORY AGENCY
N �..-.-�...h'L
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NPDES GROUND WATER DRINKING WATER
Email To purcnass
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Name:
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VIAFFILWTION
DATE
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DATE
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SAMPLER NAME AND SIGNATURE
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p CHAIN -OF -CUSTODY / Analytical Request Document
PaeeAnalytieal The Chanwf-Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately
we.weelaev.wm
Pa9e: 2 of
Section A Section B Section C
Rianim U Chem InfovoaUnn: Repuimd Prolocl Information'. Immue rilmmalion
Company - Relaon
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Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 07/26/2017
Reported: 07/27/2017
For: 92348913
Comments:
Sample Number Parameter
170726-10-01 MBAS
Respectfully submitted,
hi)A,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
Sample ID Result
Eff 018
Unit Method
mg/L SM5s OC-moo
Analyzed Analyst
07/27/2017 CL
PO Box 228 a Statesville, NC 28687 • 704/872/4697
Page 1 Kfag39e 39 of 41

Condition of Receipt
Sample Number 170726-10-01 Temp on Arrival 2
Parameter Schedule: MBAS
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 Wage 40 of 41

Chain of Custody
n'1MC/19
aceAnalytical •
/- xvweetal•CJwm
i
Rasults Reauested Bv: 818/2017
Matttl Brainard
•
,.1�
••, •,
:
�.
HInterSville, NC 28078
Phone 0 909
State of Sample Origin: N C
Mill
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Duvaltex (US), Inc.
EPA ID# NCO005312
Appendix D
DMRs

NPDES PERMIT NO.: NCDO05312
FACILITYNAME: 304 Ent Main Str plant
OWNER NAME: True Textiles Inc
GRADE: WW-4.
cDMR PERIOD: 01.2017 (January 2017)
PERMIT VERSION: 4.0
CLASS: WW 4.
ORC: Glen Edword Guy
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sony
ORC CERT NUMBER: 939696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NC00053 t 2
FACILITY NAME: 304 East Main Stmet tint
OWNER NAME: Ttnc Tcatilcs Inc
GRADE: WW-4.
cDMR PERIOD: 01.2017 (January, 2017)
PERMIT VERSION: 4.0
CLASS: W WA.
ORC: Glut Edward Guy
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sally
ORC CERT NUMBER: 989696
STATUS: Pwmscd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: True Textiles Inc
GRADE: W W-4.
eDMR PERIOD: 01.2017 (January 2017)
COMPLIANCE STATUS: Complinot
PERMIT VERSION. 4,0
CLASS: WW4.
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE 9: 3368351083
PERMIT STATUS: Active
COUNTY: Su�rr
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 00/162017
rtifier Signature: GICX E Gary E-Mail:[e-mail] Phone #:[phone] Date
By this signature, 1 certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or die appropriate Regional Office any noncompliance that potentially threatens public health or die environment.
Any information shall be provided orally within 24 hours from the time die perminee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the petminee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part ILE.6 of
the NPDES_nermit.
O.-- CT- 0
Permittee/Submitter Signature:--/ Scott Taylor E-Mail:scott.taylor@truetextiles,com Phone #:[phone] x6418 Date
Permittee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: 12131/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision is accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based an my inquiry of the person or persons who managed the
system, or dime persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete, 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: Tax Textiles, Inc.
CERTIFIED LAB 4: 5010
PERSON(.) COLLECTING SAMPLES: Glen Gary, Billy Stone
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://poml.nedew.ors/wcbAvq/sv4vWnpdcsffomis.
FOOTNOTES
Use only units of measurement designated in the reporting fteility's NPDES permit for reporting data.
• No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there arc no data to be entered for all of the parameters on the DMR
for entire monitoring period.
•• ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
•'• Signature of Permittee: If signed by otter than the perminee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Sueet plant
OWNER NAME: Ttuc TatOea Inc
GRADE: W WA
cDMR PERIOD: 01-2017 (January 20M
Outfall 001 - Effluent Comments:
Conaact Labamtory Qualified Lab Data:
PERMIT VERSION: 4.0
CLASS; W W-4.
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
In observance of the statu holidays no samples wve taken on January 2 and 16
WjAE January 03, EMwnt TSS
Tlsc dissolved oxygen depiction of the dilution water blank exceeded 01 mg0
AOAJAI January 09. Effluent DOD
PERMIT STATUS: AeliVC
COUNTY: Seery
ORC CERT N00fEER: 98%96
STATUS: Pmcessed
Aualyla recovery in the laboratory central sample (LCS) was below QC limits Eeaulm far this gulyte In u ' t d sarmples smay be biasccl I

NPDES PERMIT NO i NCOMS312
FACILITY NAME: 304 Ent Main Street plant
OWNER NAME: TmTexNe[ Inc
GRADE: WW4.
eDMR PERIOD- 02-2017 (Febntary 2017)
PERMIT VERSION: 4.0
CLASS: W W-0.
ORC: Glen Edward Guy
ORC RAS CHANGED: N4
VERSION: 1.0
PERMIT STATUS: Aciive
COON V: Scary
ORC CERT NUMBER 9996%
STATUS: Pmcmed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE': NO
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NPDES PERMIT NO.: NCONS312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: Tmv Textiles Inc
GRADE: W W-4.
eDMR PERIOD: 02-2017 (Febnwy 2017)
PERMIT VERSION: 4-0
CLASS: W WA.
ORC: Glen EdwaN Gary
ORC HAS CHANGED: No
VERSION: to
PERMIT STAWS: Active
COUNTY:Smy
ORC CERT NUMBER: 989696
STATUS: P oanutd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 00I NO DISCHARGE*: NO (Continue)
I
l4lil
"`•No Repening Rex+en�ENFRIAE•Fb Now•ReudRecyck; EVVWM-Ne Vmiwioe-Adw Wmtw,, NOFLOW-No Fbw, HOLMAY-No ViaWb.-Hofifty

NPDES PERMIT NO.: NCM5312
PERMIT VERSION: 4.0
FACILITY NAME: 304 Fist Main Street plant
CLASS: W W4.
OWNER NAME: True Textiles Inc
ORC: Glen Edward Gary
GRADE: W W4.
ORC HAS CHANGED: No
eDMR PERIOD: 02-2017(February 2017)
VERSION: 1.0
COMPLIANCE STATUS: Compliant
CONTACT PHONE #: [phone]
ORC/Certifier Signa((--tuurrre: Gt E Gary E-Mail: glen.gary@truetexti
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
PERMIT STATUS: Active
COUNTY: Sorry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 031152017
com Phone #:[phone] Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time Ore permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by pan ILE.6 of
the NPDES permit, _
Permitter/Submitter Signature:•'• abcott Taylor E-Mail: [e-mail] Phone #:[phone] x6418 Date
Permittee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
.accurate, and complete. I am aware that there arc significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Textiles, Inc.
CERTIFIED LAB #: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Billy Stone
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Cade assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://porW.nedem.org/web/wq/swplps/npdeslfbr .
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
• No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
" ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
`•e Signature of Permitter: If signed by other than the petrittee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 Cut Main Street plant
OWNER NAME: True Textile Inc
GRADE: WWA.
eDMR PERIOD: 02-2017 (Febnmry 2017)
O utfall COI - Elflimat Commears:
PERMIT VERSION: CO
CLASS: W W-9.
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: IA
PERMIT STATUS: Active
COUNTY:Suny
ORC CERT NUMBER "9696
STATUS: Processed
Contract 1.abOmt"y Qualified Lab Data:
ko February 02, 07, 13 and 27 EfBunt ROD
Anadyle co cry in the labomtory control samplc (LCS) was below QC limjt Results fa this analyte in associated samples maybe biased low.
Si.t February 24. EfRumt TSS
The dissolved oxygen depkrion of the dilution water blank exceeded 0.2 mad.

NPDES PERMIT NO.: NC➢D05312
FACILITY NAME: 3D4 End Main Sheet plat
OWNER NAME: Tme Teaila Inc
CRADE: W W-4.
eDMR PERIOD: 03-2017 (Mach 2017)
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Gim Edwud Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: LUEX
ORC CERT NUMBER: 9896%
STATUS: Pmceescd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
•••. No R4poning Re ENFRUSE-No FIaw.ReuuAexydo. C•NVWTOt•No VlsiWion-Advert Weagi ,, NOFLOW-No Platy. ROLIDAY-No Visitadon-Rolldey

NPDES PERMIT NO.: NOD005312
FACILITY NAME: 304 Emt [.tin Shw plant
OWNER NAME: T= Tut9cs Im
GRADE: %V4.
eDMR PERIOD: 03.2017 (Mazc6 201n
PERMIT VERSION: 4.0
CLASS: W W4.
ORC• Gim Edward Guy
ORC HAS CHANGED: No
VERSION: 1.0 '
PERIRIT STATUS: Active
COUNTY: Sully --
ORCCERT NUMBER: 9596%
STATUS: Pm cd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: NC00DS312
FACILITY NAME: 304 East Mein Stan plan(
OWNER NAME: True Textiles Inc
GRADE: WW4
eDMR PERIOD: 03-2017 (March 2017)
COMPLIANCE STATUS: Compliant
ORC/Certifier Signature: Wien E
PERMIT VERSION: 4.0
CLASS: WW-4.
ORC: Gtm Edward Gary
ORC HAS CHANGED: No
VERSION: I_0
CONTACT PHONE p: 3369351083
( J.Z— � —i
ry E-mail: g len.gary@tr
By this signature,( certify that (his report is accurate and complete to the best of my knowledge.
PERMIT STATUS: Active
COUNTY:
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 04/18/2017
04/18/20
iles.com Phone R:[phone] Date
The permince shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the euvronment.
Arty information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part HE 6 of
the NPD�it.
�V
i%- ozol7
Perm ittectSubmitter Signature:--' fott Taylor E-Mail:[e-mail] Phone 0:207.876-3331 x6418 Date
Permittee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible far gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for
}mowing violations.
CERTIFIED LABORATORIES
LAB NAME: True ImWe; IM
CERTIFIED LAB p: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Billy Stone
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting httpJ/portal.ncdew .orgtweblwq/sn/pstnpdes/fortes.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
• No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are m data to be entered for all of the parameters on the DMR
for entire monitoring period
'" ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204,
"• Signature of Permittee: If signed by other than the penninee, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(b)(2)(D).

NPOES PERMIT NO: NC0005312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: Tnre TmWen Inc
GRADE: W Wes.
eDMR PERIOD: 03-2017 (March 2017)
Outran 001 - Effluent Gmmenuc
PERMIT VERSION: 4.0
CLASS: W W4.
ORC: Olen Edwwd Gary
ORC HAS CHANGED: No
VERSION: 1.0
A transforrmc bkw an Mweb 1, 2017 power omage to site from 16:00 3/1 aid 12:00 3/4 m Bow during Ibis lime
Contract Labomtory Qualified Lab Data:
49 Mamb 7, Effluent Pbosphosus
Matno spike rmovery exceeded QC limits. Bamb accepted baud on kborstory control sompk (LCS) recovery.
dxt Much 14, Efflueu BOD
The precision between the sample and sample duplic exceeded laboratory =Vol limits.
M d Marcb 15. Effluent TSS
PERMIT STATUS: Active
COUNTY: Suny —
ORC CERT NUMBER: 989696
STATUS: Processed
The precision betwem the sample and sampte duplicate exceeded laboratory central limits.
49 Much 20, Effluent BOD
The dissolved oxygen depklion of the dihdion wmar blank exceeded 0.2 mgA.
$Lt Mamb 29,30 vM 31 Effluent BOO
Analyze recovery in the laboratory control sample (LCS) was blow QC limits. Resuhs for this analyse in associated sampks may be biased low.

NPDES PERMIT NO.: NCOODS312
FACILITY NAME: 304 East Main Streot plant
OWNER NAME- True TettOea Inc
GRADE- WW4.
eDMR PERIOD: 04-2017 (Apn'12017)
PERMIT VERSION: 4.0
CLASS: WW-4.
ORC: Olm Edwmd Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Acdw
COUNTY: Su —
ORC CERT NUMBER: 999696
STATUS: Pro xd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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••"NA Reposing Rtawn: ENFRt1SE Nwflow.ReweRecyc3r ENVWPHR-No Ywikdm-Adverse Wmlbc, NOFLOW-No Fbw, HOLMAY-No VaiIalim-Holiday

NPDES PERMIT NO.: NCOODS312
FACILITY NAME: 306 Earl Mein Sven plant
OWNER NAME: T1v6 Textile Inc
GRADE: W W d.
eDMR PERIOD: 04-2017 (April 2017)
PERMIT VERSION: 4.0
CLASS: W W4.
ORC; Olm Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Actlae
COUNTY. Swq
ORC CERT NUMBER 98%%
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: N00005312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: True Textiles Inc
GRADE: W W-4.
eDMR PERIOD: 04-2017 (April 20M
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Glyn Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY: Su ry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 0511 W2017
ORC/Certifier Signature: Glen Gary E-Mail:[e-mail] Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the Appropriate Regional Office any noncompliance that potentially threatens public health or the environment
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made As required by part II.E.6 of
the NPIJES-otr nit. /)
OS/1012017
Perm ittee/S u bmitter Signature:"'* Pott Taylor E-Mail: [e-mail] Phone #:[phone] x6419 Date
Perminec Address: 304 E Main St Elkin NC 28621 Permit Expiration Datc: 123112018
I certify, under penalty of low, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those protons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I Am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Textiles, Inc,
CERTIFIED LAB 6: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Billy Stone
CERTIFIED LABORATORIES
PARAMETER CODES
parameter Cade assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.ncd=,orgiweblwglswp/pslnpdes/fo=.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
• No FlowfDischarge From Site: Check this box if no discharge occurs and, As a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
•' ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
*** Signature of Permittee: If signed by other than the permittee, then delegation of the signatory authority must be on file with the state per 1 SA NCAC 2S
.0506(b)(2)(D).

NPDES PERMIT NO.; NC0005312
FACILITY NAME: 304 Em Main Strut plem
OWNER NAME: True Twit= Inc
GRADE: W W4.
eDMR PERIOD: 04.2017 (Apnl 2017)
Outfoll 001- EMwat Commmu:
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Glen Edv d Gary
ORC HAS CHANGED: No
VERSION: 1.0
No samples On 04-14. 2017 in abscmM" Of The state hold y
Contract Laboratory Qoali6cd Lab Data:
!dE Apnl 17, 21, 24 and 20 Emu=t BOD
PERMIT STATUS: Agive
COUNTY: Smty —
ORC CERT NUMBER: 939696
STATUS: Pmc d
Analyte me EX in the Iabmtwy control sample (LCS) was —blill OC limits, RMIM for this ")Ic in aasocix d pl<s may be b ued low

NPDES PERMIT NO.: NCOODS312
FACILITY NAME: 304 East Main St%aA plant
OWNER NAME: T7oeTetSikS Inc
GRADE: WWA.
tOMR PERIOD: 05-2017 (May 20M
PERNUT VERSION: 4.0
CLASS: W WA.
ORC: Glen Edward Corry
ORC RAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Aadw
COUNTY:
ORC CMNUMBER: 98%96
STATUS: FMaeuM
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: OOI NO DISCHARGE*: NO
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NFDES PERMIT NO.: NCM5312
FACILITY NAME: 304 Ent Main Seat phut
OWNER NAME: hue Textile Inc
GRADE: W W-4.
*DMR PERIOD: 05-2017 (May 2017)
PERMTT VERSION: 4.0
CLASS: W W.4.
ORC: Glen Edwmd Gary
ORCnASCHANGED:No
VERSION: 1.0
PERMIT STATUS: Actin
COUNTY: Sm" —
ORC CERT NUMBER: 9996%
STATUS; Pmoeaed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
.... Nakepmtin'Rneon:F}1FRUSE. No flaw-ka=WRmyek; EKVWIRR-No Vifiptm-Adr Welber. NOFLOW a No Flow: HOLIDAY a 4o Vki"m-Ro6dry

NPDES PERMIT NO, NC0005312
FACILITY NAME: 304 East Main Strew plam
OWNER NAME: True Texliiu Inc
GRADE: W WA.
0MR PERIOD: 05.2017 (May 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Glen Edward Gary
ORC HAS CH.A:NGED: No
VERSION: 1.0
CONTACT PHONE#: [phone]
PERMIT STATUS: Active
COUNTY: Surry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 005/2017
U & —/ — 06/15/2017
ORC/Certifier Signature: len E Gary E-Mail:glen.gary®truetex(iles.com Phone fl:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also he
provided within 5 days of the time the permitter becomes aware of the circumstances.
if the facility is noncompliant, please attach a list of comctivc actions being taken and a time-tabic for improvements to be made as required by part II.E.6 of
the NPDES permit
c)b-1b-Z017
Permittec/Submittcr Signature:'- Scott Taylor E-Mail:scott.taylorQtruetextiles.com Phone 0:207-876-3331 x6418 Date
Fermin" Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: I2l31/2018
1 certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submincd. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the beat of my knowledge and belief, true,
accurate, and complete. I am awwo that there arc significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: True Texul", Inc.
CERTIFIED LAB #: 5D10
PERSON(,) COLLECTING SAMPLES: Glen Gay, Billy Stone
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http://portal.nedem.oreweb/wq/swp/p3lnpdcs/fom&
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
• No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
♦r ORC on Site?: ORC must visit facility and document visitation of facility as required per ISA NCAC 8G .0204.
`•• Signature of Permittec: If signed byother than the permittee, than delegation of the signatory authority must be on file with the state per ISA NCAC 2B
.0506(b)(2)(D).

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Ssren plant
OWNER NAME: True Textiles Inc
GRADE: W W.4.
eDMR PERIOD: 05-2017 (May 2017)
PERMIT VERSION: 4.0
CLASS: W WA.
ORC: Glen Edward Croy
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: suny —
ORC CERT NUMER: 989696
STATUS: Proemxd
Outfou 001- Ef lueat Cmmenu:
No Sampks On 05-29- 2017 in observance of the state holiday,
Contract Labormory Qualified Lab Data:
aj,O May 4, 11 and 22 EMum HOD
Armlyto teeovtq in the laboratory eannol sampk (LCS) was below QC limits. Results for this analyze in nasociakd Sam lea my be biaud low.
ILt May I and 25 Effluent ROD
The dissolved oxygen depletion ofthc wesr blank ceeded0' g/l

NPDES PERMIT NO.: NCOODS312
FACILITY NAME: 304 East Main Strom pbw
OWNER NAME: True Tcdles Inc
GRADE: W WA.
eDMR PERIOD: 06.2017 (Jm1e 2017)
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Gkn Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sully
ORC CERT NUMBER: 9E9696
STATUS: Prolxued
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NCOODS312
FACILITY NAME: 304 East Main Strap 91M
OWNER NAME: hue TalDes Ina
GRADE: W W4.
eDMR PERIOD: W2017 (June 2017)
PERMIT VERSION: 4.0
CLASS: W W4.
ORC: Glen Edavd Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Aedw
COUNTY: S
ORC CERT NUMBER: 959696
STATUS: Procemd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 Eau Main Street plant
OWNER NAME: True Textiles Inc
GRADE: WW4_
eDMR PERIOD: 06-2017 (June 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW4.
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE N: 3369351093
PERMIT STATUS: Active
COUNTY: Simy
ORC CERT NUMBER: 90696
STATUS: Processed
SUBMISSION DATE: 0711 &2017
07/18/2017
ORC/Certifier Signature: Glen Gary E-Mail: [e-mail] Phone #:[phone] Date
By this signature,) certify that this report is accurate and complete to the best of my knowledge.
The permince shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the perminee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permittce becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by pan 11,E.6 of
the NPDE-Spermit. n
rY / / 07/18l2017
Permittee/Submitter Signature:• "Scott Taylor E-Mailscott.taylorQtruetextiles.com Phone #:[phone] z6418 Date
Perminee Address: 304 E Main St Elkin NC 29621 Permit Expiration Date: 12/312018
1 ccrify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best ofmy knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Textiles, Inc.
CERTIFIED LAB #: 5010
PERSON(.) COLLECTING SAMPLES: Glen Gary, Billy Slone
CERTIFIED LABORATORIES
PARAM=R CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http.,I/portal.ncdenr.org(mbfwqtswp/pslnpdesifems.
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for rcponing data.
No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 80 .0204.
"•• Signature of Permittec: If signed by other than the petmittce, then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
A506(b)(2)(D).

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Street pWtt
OWNER NAME: True Textiles Inc
GRADE: WWA.
eDMR PERIOD: 0(-2017 (lone 2017)
OutrAll 001-Em mat Comments:
PERMIT VERSION: 4.D
CLASS: WWA.
ORC: GIen Edw" Gary
ORC HAS CHANGED: No
VERSION: LO
PERMIT STATUS: Active
COUNTY: Suny
ORC CERT NUMBER: "9696
STATUS: Processed
Contract Laboratory Qualified Lab Data:
SCC June 6 and 7 Efllueot BOD
The dissolved oxygen depkum of the waw blank exceeded 0.2 mg/I.
bit June 9 and 9 Effluent BOD
Acolyte recovery in the laboratory canaml sanplc (LCS) was below QC luni�s P sWls for this acolyte in easoeiated samples June be biased low.

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 Ess1 Main Socef Plan
OWNER NAME: True Tatilm Im
GRADE: W W4.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4.0
CLASS: W W4.
ORG Olen Ed..d Cy
ORC HAS CHANGED: No
VERSION: LO
PERMIT STATUS: Active
COUNTY:�= -
ORC CERT NUMBER: 96%%
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Streit plant
OWNER NAME: Tsw Twilea Inc
GRADE: WW4.
eDMR PERIOD: 07-2017 (July 2017)
PERMIT VERSION: 4A
CLASS:%VA.
ORC: Gkn Edwafd Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Amive
COUNTY: Sun
ORC CERT NUMBER: 959696
STATUS: Piwessed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Sheet plant
OWNER NAME: True Textiles Ix
GRADE: WW-4.
eDMR PERIOD: 07.2017 (July 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4,0
CLASS: W W 4.
ORC: Gin Edward Cary
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE #: [phone]
PERMIT STATUS: Active
COUNTY:Surry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 08212017
08/16/2017
ORC/Certifier Signature: Glen E ary E-Mail: glen. gary Ctruetexti les.com Phone #:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The perriamcc shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware oFthe circumstances. A written submission shall also be
provided within 5 days of the time the permince becomes aware of the circumrtancu.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part iLE.6 of
the NPDES permit.
Permittcc/Submitter Signature:'"' Sfott Taylor E-MaiLscott.tay]orQtruet<ztiles.com Phone #r207-876-3331 x6418 Date
Permittee Address, 304 E Main St Elkin NC 28621 Permit Expiration Date: 12/31/2018
1 certify. under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person orprsons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Textiles, IM.
CERTIFIED LAB #: 5010
PERSON(,) COLLECTING SAMPLES: Glen Gary, Billy Stone
CERTIFIED LABORATORIES
PARAMETER CODES
Pammeter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http7/portal.nedenr.org/web/wq/swp/ps/npdes/forms.
FOOTNOTES
Use only units of measurement designated in the reporting facility�s NPDES permit for reporting data.
"No Flow/Discharge From Site: Check this box if no discharge occurs and, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
"• ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
'a" Signature of Permittee: If signed by other than the perminee, then delegation of the signatory authority must be on file with the state per 15A NCAC 213
.0506(b)(2xD).

NPDES PERMIT NO.: NCOOOS312
FACILITY NAME: 304 Eat Main Sheet poet
OWNER NAME: hue Textiles Inc
GRADE: WW4.
eDMR PERIOD: 07.2017 (July 20M
OutfxU 001- EfRueet Comtneau:
PERMIT VERSION: 4.0
CLASS: W W.4.
ORC: Glen Edward Gary
ORC HAS CHANCED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: §Lin
ORC CERT NUMBER: 999696
STATUS: Processed
Cnnlraxl laboratory Qualified Lob Data:
No samplcs on July 4 in absmance of the state holiday.
Gyp July 3 Effl cot TSS
The precision by w the samp)c and sample duplicme exceeded laboratory control limn:.
ddd)Wy 6.11,13, 14, 21 uW 24 Effluent ROD -
The dineolved oxygen dopkfim of the waw bunk exceeded 0.2 vV.
ij July 10 and IS Effluent ROD
Analytr recovery in the hbomwy control sampk (LCS) wu below QC limils. R"ts for this aratyte in auoeiafad samples JWy be biamd low.

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Street pbm
OWNER NAME: Tm4 Texliks Inc
GRADE: WWA.
cDMR PERIOD: 08-2017 (Augat 20M
PERMIT VERSION: 4.0
CLASS: W W-4.
ORC: Glen Edwad Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
ORC CERT NUMBER: 989696
STATUS: Procamd
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NCOWS312
FACILITY NAME: 304 Ent Main SReet plmR
OWNER NAME: True Twilk Inc
GRADE: WW4.
eDMR PERIOD:09.2017 (Anpa 20M
PERMIT VERSION: 4.0
CLASS: W W4.
ONG: GIn Edward Owy
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUN7Y:Stm —
ORC CERT NUMBER: 989696
STATUS: Procedaed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
.... Ne Ra9anin4Renec:ENFRUSEallo Flew.Remv%"k; ENWFIM-No ViSiMi a-Adv W"6w. NOFLOW-No Fkw HOLIDAY -No KWaBoa-Ra&y

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 Fitt Main Street
OWNER NAME: Tmc Textiles Ix
GRADE: WW4.
eDMR PERIOD: 08.2017 (August 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: WW4.
ORC Glen Edward Crary
ORC HAS CHANGED: N.
VERSION: 1.0
CONTACT PHONE A: 3368351083
PERMIT STATUS: Active
COUNTY: Scary
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 091182017
/ 0911512UII
ORC/Certifier Signature: Gle E Gary E- Mail: glen. gary@tructexti les. corn Phone p:[phone] Date
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
The pc minee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the permince becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part 11.E.6 of
the NPDES- ermit.
09/18/2017
Permittee/Submitter Signature:•' Scott Taylor E-Mail:[e-mail] Phone 4:207.876-3331 x6418 Date
Pennittee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date. IZ(31/2015
I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME: True Texldes, Inc.
CERTIFIED LAB 9: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Billy Stone
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit (919) 807-63DO or by visiting http://portal.ncdcu,orWwebtwgf5wplpslnpdWfo=s.
FOOTNOTES..
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
. No Flow/Discharge From Site: Check this box if no discharge occursand, as a result, there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
11 ORC on Site?: ORC must visit facility and document visitation of facility as required per ISA NCAC 80.0204.
... Signature of Permitter: If signed by other than the permirtee, then delegation of the signatory authority most be on file with the state per 15A NCAC 2B
0506(b)(2)(D).

NPDES PERMITNO.t NCDO05312
PERMIT VERSION: 4.0
PERMIT STATUS: Activc
FACILITY NAME: 344 Eau Main Street plant
CLASS: W W-4.
COUNTY: SwTy
OWNER NAME: Tme Teaziles Inc
ORC: Glen Edward Gary
ORC CERT NUMBER: 989696
GRADE: W W4.
ORC HAS CHANGED: No
eDMR PERIOD: W2017(AVal 2017J
VERSION: I.D
STATUS: Processed
outfall 001 - Emumt Commmu:
Contras Gbonstary Oushfied I.Ab DAW
4rj August 3 E8lpent TSS
7be ptecision behmen the sample and sample duplicate exceeded lebomory conol limits
40 August 7 Ettlumt BOD
The seed blast was onside umpwce criteria. Results wets accepted based on rmuining quality control indicators
140 August 19 ElBumt TSS
The pmeisim between the sample and sample duplicate exceeded laboratory ventral limits
i j Augum 11, 17, 18, 24 and 31 Efllumt BOD
The dissolved oxygen depletion of the water blank exceeded 0.2 mgA
i40 August 21 EDLxpt DOD
O ypm unge is lass Wm 2.0 fw all dilutions set The repoged value is an estimated less than value and is talculawd foe the dilution using the moat amount of sample.
140 August 29 Eflluml BOD
Analyze ruovery in the laboratory control sample (LCS) waabeluw OC limits. Results far this malyle is associated samples August be biased low.

NPDES PERMIT NO.: N00005312
FACILITY NAME: 304 Ensl Main Sincel plain
OVANER NAME: TSm Textiles Inc
GRADE: W W-4
eDMR PERIOD: 09-201715eptelnbm 2017)
PERMIT VERSION: 40
CLASS: WW4.
ORC2 Glen Ed% wd Gary
ORCHASCHANGED:No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: surry
ORC CERT NUMBER: 99%%
STATUS: Prore d
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE": NO
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NPDES PERMIT NO.: NCOOW312
FACILITY NAME: 30413 a Main Sucd oknl
OWNER NAME: Tnw Textiles Im
GRADE W W-3_
eDMR PERIOD: 09-2017 (Sepember 2017)
PERMIT VERSION: 4.0
CLASS: WW.4.
ORC: Glen F-d%wd Gary
ORC HAS CHANGED: No
VERSION: I.0
PERMm STATUS: Acllve
COUNTY: Sw'y —
ORC CERT NUMBER: 999696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDF.S PERMIT NO.: NC0005312
FACILITV NAME 3D4 East Main St" plant
OWNER NAME: Trw'fextites Inc
GRADED W W-4
eDMR PERIOD: 09-2017 (September 20171
COMPLIANCE STATUS: Compliant
PERMIT VERSION:4.0
CLASS: W W-4.
ORC: Glen Eduard Gary
ORC HAS CHANCED: No
VERSION: 1.0
CONTACT PHONE A: 3358351093
PERMIT STATUS: Active
COUNTY! Surry —
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 10/182017
—/ 10/ 18/2017
ORC/Certifier Signature: Gle E Gary E-Msil:glen.garyrii.duvallex.com Phone p:[phone] Dale
By This signature. I certify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the cm,honnrenL
Any information shall be provided orally within 24 hours from the time the permittoo became aware of the circumstances. A written submission shall also be
provided within $ days of the lime the permittee becomes aware of die cimumsmnces.
If the facility is noncompliant please attach a list of corrective actions being taken and a time -table for improvements to be made as required by pan H.E6 of
the NPDESRermit. _
1011812017
Perm ittee/S ubm itler. Signature:••' ycoti Taylor E-Mail:scotl.laylon?vuetextiles.com Phone 9:207.876-3331 x6418 Datt
Permittee Address: 304 E Main St Elkin NC 28621 Pemtit Expiration Date: 12131,2018
1 certify. under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system. or those persons directly responsible for gathering the information, the information submitted is to the best of my knowiedge and belief true.
accurate. and complete. I am aware that there arc significant penalties for submitting false information, including the possibility of finesand imprisonment for
knowing violations.
CERTIFIED LABORATORIES
LAB NAME -
CERTIFIED LAB a: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary. BillyStone
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDFS Unit (9I9) 807.6300 or by visiting http:/Iportal.ncdenrzrg/ueb/wghwptps/npdeslror .
FOOTNOTES
Use only units of measurement designated in the reporting facility's NPDES permit for reporting data.
• No FlowtDischarge From Site: Check this box if no discharge occurs and. as a result, there arc no data to be entered t'pr all of the parameters on the DMR
for enfuc monitoring period.
'e ORC on Site?: ORC muss visit facility and document visitation of facility as required per 15A NCAC 90.0204.
•ee Signature of Pemtittee: If signed by other than die perminee. then delegation of rim signatory authority must be on rite with the state per 15A NCAC 2B
.0506(bK2)(D).

NPDES PERMIT NO.; NC0005312
FACILITY NAME: 304 East Main Such Plan
O%VNER NAME: True Texli)es 1w
GRADE: WWJ.
eDAIR PERIOD: 09.2017(Septemba 2017)
Oalfall001 - Elnaem Commeals:
PERMIT VERSION: 4,0
CLASS: W W-a
ORC: Glen Edward Gary
ORC 141E CHANGED: No
VERSION: 1.0
No samples taken on Scplembv 4 in obsrrvance of theSa4c holiday
Contract Laboratory Qualirwd Lab Data
&F Suptembcr 1. 7. 12. 13. 18. L-1.27 and 28 L' wni BOD
The diswlved oxygen degctipn oft
he "Wr blank exeecded 0 2 m,n
k-,d September 11, 12, 19. 21. 22. 27 and 29 Effimm SOD
PERMIT STATUS: Actin
COUNTY: swy —
ORC CERT NUMBER: 989696
STATUS: ftemd
Amlylen=wry in the laboWory eoatrolaemde(LCSI Wes WOW QC limits Results l'm this anlyie in aSSacinld Samples SIPIC ber be biased Io

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Street plan)
O%VNER NAME: True Twiles Im
GRADE: WWA
eDMR PERIOD: 10-201710cb6er 2017)
PERMIT VERSION: 4 0
CLASS: W W4.
ORC: Gkn Edward Gmy
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Surry
ORC CERT NUMBER: 989696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDFS PERMIT NO.: NCOODS312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: True Textiles Inc
GRADE: WW-4.
eDMR PERIOD: 1"017 (October 2017)
PERMIT VERSION: 40
CLASS: WW-4
ORC: Glen Edmwd Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sure
ORC CERT NUMBER: 9E9696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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NPDES PERMIT NO.: NCO305312
FACII.ffY NAME: 304 East Main Street plam
OWNER NAME: True Textiles Inc
GRADE: WW4
eDMR PERIOD: 10-2017 (Oc(ober 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: W W4
ORC Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
336835f083
PERMIT STATUS: Active
COUNTY: Surry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 11/1712017
1 `%
0RC/Certifier Signature: Glen Gary E-M a i l: g l en.gary:ii duv a It ex.com vPhone #:[phone]
By this signature, I certify (hat this report is accurate and complete to the best of my knowledge.
12017
Date
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of (he circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
)f the facility is noacompliam. please attach a list of corrective actions being taken and a time -table for improvements to be made as required by pan II.E.6 of
the NPDES permit.
06 r I�,t,c�x�� (I— zo— wry 17 1yl7nD17
Perm iftee, Submit(er SignaturA'.• Scott Taylor E- Mail: scot(. tayl or.-ti4ructexiiles.com Phone #:[phone] x6418 Date
Permittee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: 12,3 V2018
I eerily, under penalty of law. that this document and all attachments were prepared under my direction or supervision in accordance svidi a system designed
to assure that qualified personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information. the m1brination submitted is. to the best army knowledge and belief. true.
accurate. and complete. I am aware that there are significant penalties for submitting false infomation. including the possibility of Imes and imprisonment for
knowing violations.
LAB NAME: True Textiles. Inc
CER'I-IF1ED LAB #: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary. Billy Stone
CERTIFIED LABORATORIES
PARAMETER CODES
Parumcier Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting hnp:/lportal.ncdenr.orgheeblwrysapipslnpdcs/fumts,
1-00INOTES
Use only units of measurement designated in the reporting facility's NPDES permit for epon ing data.
• No Flow/Discharge From Site: Check this box if no discharge occurs and. as a result. there are no data to be entered for all of the parameters on (he DMR
for entire monitoring period.
"• ORC on Site?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
te' Signature of Permittee: If signed by other than the permittee. then delegation of the signatory authority must be on file osith the state per I SA NC AC 2B
.0506(b)(2)(D).

NPOES PERMIT NO.: NC0005312
FACILITY NAME 30a Fast Main Strcct plant
OWNER NAME: True Textiles Inc
GRADE: WWA
eDMR PERIOD: 10-2017 (October 2017)
OutAll OBI . EBluwl Comments:
PERMIT VERSION:4.0
CLASS: W W4
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 10
PERMIT STATUS: Aeuve
COUNTY: Surry
ORC CERT NUMBER: 989696
STATUS: Processed
Contract Laboratory Ounbfied lab Data:
&0 October 2. 3, 5, 6, and 13 Effluent BOD
The dissolved oxygen depletion oflhewaterblank exceeded02m I
d4p October 2, 3, 5.10. 16,17.20.23,24 wd 25 Effluent BOD
Amlyte recovery in the McCain control sample (LCS) was below OC limits Rewlts for this walyle in associated samples October be biased I

NPDES PERMIT NO.: NC0005312
FACILM' NAME: 304 Ei sl Main Suee1 plain
OWNER NAME: True Tmilcs Inc
GRADE: W W4
eDMR PERIOD: 10-2017 (Oc(ober 2017)
PERMIT VERSION: 40
CLASS: W W4.
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sully
ORC CERT NUMBER: 989696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 Ent Main Strect plant
OWNER NAME: True Tcxtilca Inc
GRADE: WWA.
eDMR PERIOD: IO-200(October 2017)
PERMIT VERSION: d 0
CLASS: W W4
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Actim
COUNTY: Surry
ORC CERT NUMBER: 999696
STATUS Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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a<aa No Reponing Reason: ENFRUSE - No FIm-RemswRerycW ENVIVTHR • No Visitation-Adsoso Wculia. NOFIAW • No Flow. HOLIDAY `No Visitation - Holiday

NPDES PERMIT NO.: NCUS312
FACILITY NAME: 304 Easi Main Street plant
OWNER NAMEt True Textiles Inc
GRADE: WW4.
eDMR PERIODr 10-2017(October 2017)
COMPLIANCE STATUS: Compliant
PERMIT VERSION: 4.0
CLASS: W W4
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION:1.0
Y: 3368351083
PERMIT STATUS: Active
COUNTY: Sorry
ORC CERT NUMBER: 989696
STATUS: Processed
SUBMISSION DATE: 11/17R017
n
ORC/Certifier Signature: Glen
i
Gary B-M ail:glen.gary iie:duvaltes.com Phone 9:[phone]
By this signature, I certify that this report is accurate and complete to the best of my knowledge.
'20 17
Dalc
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permittee became aware of rho circumstances. A written submission shall also be
provided within 5 days of the time the permittee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time-taW a for improvements to be made as required by part II.E.6 of
the NPDES permit.
—&�r (I— 20— Zoi 7 I Ir17(2017
Perm i lteelSubmi tier SignaturA•" Scott Taylor E-Mail:scott.laylor.it.truetextiles.com Phone 9:207-876-3331 x6418 Dale
Perminee Address: 304 E Main St Elkin NC 28621 Permit Expiration Date: 12;3 V2018
1 certify. under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure dial qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system, or those persons directly responsible for gathering the information. the information submitted is to the best of my knowledge and belief. true.
accurate. and complete. I am ervare that there are significant penalties for submining false information, including die possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Textiles, Inc.
CERTIFIED LAB Y: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Billy Stone
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] or by visiting http:0portal.ncdenr.org/web/wq/swap/pslnpdcstfomis.
FOOTNOTES
Use only units ofineawreatent designated in the reporting facility's NPDES permit for reponing data.
• No Plow/Discharge From Site: Check this box if no discharge occurs and, as a result. there are no data to be entered for all of the parameters on the DMR
for entire monitoring period.
"• ORC on Si(e?: ORC must visit facility and document visitation of facility as required per 15A NCAC 8G .0204.
•"" Signature of Perminee: If signed by other than the permince. then delegation of the signatory authority must be on file with me state per 15A NCAC 2B
.0506(b)(2x D).

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East 14w Sacci plant
ONNER NAME: True Textiles Inc
GRADE: W W4
eDMR PERIOD: 10.2017 (October 2017)
Outrall001 - Elllaml Comments:
PERMIT VERSION: 4.0
CLASS: W W-4
ORC. Glen Edtwd Gay
ORC HAS CHANGED: No
VERSION•10
PERMIT STATUS: Active
COUNTY:
ORC CERT NUMBER: 989696
STATUS: Processed
Contract Laboratory Qomlirmd Lab Data:
iLO October 2. 3, 5. 6, and 13 Effluent SOD
The dissolved oxygen depleilm of the water blank exceeded 02 m&4
649 Owoba 2, 3, 5.10, 16 ,17. 20. 23 24 and 25 Effluent Boo
Analyze raovuy in the laboratory control sample (LCS) was below QC hints Results for this analyte in associated samples October be biased to v

NPDES PF.RI 11T NO,: NC0005312
FACILITY NAME: 304 EJ131 Main Sucel plant
OWNER NAME: True Te%lilcs II1c
GRADE: WW-4"
eDMR PERIOD: 11-2017 4Novemba 2017)
PERMIT VERSION: 4,0
CLASS: W W 4.
ORC: Glen Ed%wd Gary
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS Amine
COUNTY•Swry —
ORC CERT NUMBER: 999696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO
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NPDES PERMIT NO.: NC000531-1
FACILFTV NAM@ 303 East Main Stted plan
OWNER NAME: True Tutilm Inc
GRADE: W Wd.
eDMR PERIOD: I -2017(November 2017)
PERMIT VERSION: 4.0
CLASS: W WA
ORC: Glen Edswrd Gay
ORC HAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Aenve
COUNTY: Susry
ORC CERT NUMRER: 999696
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
04—No Reponirg Ream tTFRUSE, No Flow.ReuwReryek: ENVWTHR a No Visitation-Ad%-r R'egba.. NOFLOW-No Flow:HOLIDAY - No Visilutlw - 14441,

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Street plant
OWNER NAME: True Textiles Inc
GRADE: WW4.
eDMR PERIOD: 11-2017 (November 2017)
COMPLIANCE STATUS: C liant
PERMIT VERSION: 4.0
CLASS: W W4
ORC: Glen Edward Gary
ORC HAS CHANGED: No
VERSION: 1.0
CONTACT PHONE C 33683$1083
PERMITSfATUS: Active
COUNTY: SUM
ORC CERT NUMBER: 989696
STATUS: Prwmcd
SUBMISSION DATE: 12/10017
12/39/2017
ORC/Certifier Signature: Glen E a r y E-Mall:glen.garyfiJduvallex.com Phone R:[phone] Date
By this signature, ) certify that this report is accunte and complete to the best of my knowledge.
The penninec shall mpon to the Director or the appropriate Regional Once any noncompliance that potentially threatens public health or the environment.
Any information shall be provided orally within 24 hours from the time the permince became aware of the circumstances. A written submission shall also be
provided within 5 days of the time the pemminee becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements to be made as required by part II.E.6 of
3 1 7- ao f % 12/ L B/2617
Perm Itice/Submi tier Signature:*** Slott Taylor E-Mail:scott.taylor&dtruetextiles.com Phone R:207-876-3331 x6418 Date
Perminee Address: 304 E Main St Elkin NC 29621 Permit Expiration Date: 12/31/2019
1 certify, trader penalty of law. that this document and all anachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system. or those persons directly responsible for gathering the in(ommatior4 the information submitted is. to the best of my knowledge and belief. true,
accurate, and complete. 1 am aware that there are significant penalties for submitting false information. Including the possibility of fines and imprisonment for
knowing violations.
LAB NAME: True Texdies, Inc.
CERTIFIED LAB R: 5010
PERSON(s) COLLECTING SAMPLES: Glen Gary, Bdb Stone
CERTIFIED LABORATORIES
PARAMETER CODES
Parameter Code assistance may be ob(ained by calling the NPDES Unit [phone] or by visiting Mtp•Jfportal.nodear.orgAwbArq/swp/p*pdeslforms.
FOOTNOTES
Use only units of measurement designated in the reponing facility's NPDES permit for reporting data.
* No Flow/Discharge From Site: Check this box if no discharge occurs and as a result. there are no data to be entered for all of the parameters on the DMR
for catim monitoring period. -
•" ORC on Site?: ORC must visit facility and document visitation of facility as required per ISA NCAC 8G .0204.
*"" Signature of Permittee: If signed by other than the perminee. then delegation of the signatory authority must be on file with the state per 15A NCAC 2B
.0506(bX2XD).

NPDES PERMIT NO,: NC M312
FACILITY NAME: 304 Eat Man Stmel plunl
ONNER NAME; Troe Twits Inc
GRADE; WW4.
eDMR PERIOD: 11.2017(Novenbe12017)
PERMIT V FRS10:V: 4.0
CLASS: WW4.
ORC: Glen Edwrd Gary
ORC HAS CHANGED: No
VERSION: I.0
Out011 Ool • EDlo"I Comments:
No samples taken on Nmember23wd24inohwmaneeoftheSweloliday
PERMITSTATUS: AUrve
COUNTY: So"
ORC CERT NUMBER: 989696
STATUS: Procrsmd
Conpaet LaboratoryQuauried Lab Dam
8yO November 1, 6 and 8 Effluent ROD
Analyle ceoovery in the laboraim eanool sample (LCS) was below OC hm ts Results fb, ghts anOlYlcn ass - t d samples No bee be h1ased i
AO November 2 and 7 Elllueot ROD
The Precision M%"n the sample and I=pk duel' ate crceedcd laboratory control I'm is
4.O November 3, 9 I0snd 13 EOluent ROD
The dissolved oxygen depletion of the water blank exceeded 0 2 mg/I

NPDES PERMIT NO.: NC0005312
FACILITY NAME 304 Fill Man Soto plant
OWNER NAME: True Teaiks Inc
GRADE: W W-4
eDMR PERIOD: 12.2017 (December 2017)
PERMIT VERSION: 4.0
CUSS: W WA.
ORC: Glen Ed%wd Gary
ORC IIAS CHANGED: No
VERSION: 1.0
PERMIT STATUS: Active
COUNTY: Sony
ORC CERT NUMBER: 9896%
S3'ATUk Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE": NO
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•••• N9 RepntOn; R0a0n, ENFR05E - NO Flo,, Reu5altecJOk: ENVRTNR - HO Viti100a- Adtene Wtadc NOFLOW • No Floe: HOLIDAY - X. VllnuOan Holidry

NPDES PERMIT NO.: NC0005312
FACILITY NAME: 304 East Main Sum plain
OWNER NAME: True Tcaiks Inc
GRADE: W W<.
eDMR PERIOD: 12.201 T (December 2017)
PERMIT VERSION: 4.0
cuss: Wwa.
ORC: Glen Educed Gay
ORC HAS CRANGED: No
VERSION: 1.0
PERAIIT STATUS: Active
COUNTY: Swy
ORC CERT NUMBER: 9996%
STATUS: Processed
SAMPLING LOCATION: EFFLUENT DISCHARGE NO.: 001 NO DISCHARGE*: NO (Continue)
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.... No Reporting Remm: F-NFRUSE No Fl.-Reuso'Rocyc2e: ENVWTHR No Vtwaoon Adceue WwNoe NOFLOW No Flm. HOLIDAY No VimaOm- Hohday

NPDES PERMIT NO- NCO005312
FACILITV NAME: 304 Eset Main Street plant
OWNER NAME: True Testiks use
CRADC WWl.
eDMR PERIOD-. 12-2017 (Daenber 2017)
COMPLIANCE STATUS Compliox
—% /i
PERMIT VERSION: 4.0
CLASS: WWI.
ORC-- GIN Ed%ard Gary
ORC HAS CHANCED: No
VERSIONt 1_0
CONTACT PHONE a: 3369351083
PERMITSfATUS: Active
COUNTY: SuTy
ORC CERT NUMBER: 999696
STATUS:- Processed
SU&MLSSION DATE: 0112212018
ORC/Certifier Signature: 6en E Gary E-Mail:glen.gsryrrduvaltex.cors Phone 0:[phone] Date
By this signature. I anify that this report is accurate and complete to the best of my knowledge.
The permittee shall report to the Director or the appropriate Regional Office any noncompliance that potentially threatens public health or the cnvirenment.
Any information shall be provided orally within 24 hours from the time the perminee became aware of the circumstances A ,sriiten submission shall also be
provided within 5 days of the time lire permiba becomes aware of the circumstances.
If the facility is noncompliant, please attach a list of corrective actions being taken and a time -table for improvements In be made as required by part ILE.6 of
the NPj3Tt$ permit. _
/—Or-J — c-,2o I O
Permittee/Submilter Signature:*** Pit Taylor E•Mail:[e-mail] Phone 0:207.976.3331 x6418 Dale
Permince Address: 304 E Main St Elkin NC29621 Permit Expiration Date: 12131/2018
1 certify. under penalty of Inv. that this document and all attachments were prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathm and evaluate the information submitted. Based on my inquiry of the person or persons who managed the
system. or those persons directly responsible fm gathering the information the information submitted is. to the best of my knowledge and belief, true.
accurate. and complete. I am aware that there are significant penalties for submining false information, including the possibility of fines and imprisonmenl for
knowing violations
CERTIFIED LABORATORIES
LAB NAME: True Textiks, he.
CERTIFIED LAB a: 5010
PERSON(s) COLLECTING SAAIPLPS: Glen Cry. Billy Saint
PARAMETERCODES
Parameter Code assistance may be obtained by calling the NPDES Unit [phone] m by visiting hnpJ/portal.rxdem.org/weNwghwry/psfnpde.Vfmms.
FOOTNOTES
Use only units of mansurement designated in the reporting facility's NPDES permit for reporting data.
• No Flow/Discharge From Site: Check this box if ma discharge occurs and, as a result, there arc no data to be entered for all of the parameters on the DMR
for entire monitoring period.
•• ORC on Site7: ORC must visit facility and document visitation of facility, as required per 15A NCAC 8G .0204.
'•v Signature of Permince: Ifsigned by other than the permittee, then delegation of the signatory authority must be on rile with the state per I SA NCAC 2B
.0506(b)(2)(D).

NPDES IERMITNO: NC00053:2
PERMIT VERSION: 40
PERMIT STATUS: Active
FACILITV NAME: 304 Ent Main Sven plant
CLASS: W Wd
COUNTY:
OWNER NAME: True Textiles lm
ORC: Glen Edwmd Gary
ORCCERTNUMBER:9996%
GRADE: W W-e,
ORC HASCHANGED: No
eDMR PERIOD: 12-2017(Deamba 2017)
VERSION: 1_0
STATUS Processed
DaBaR 601 - EFDt I Ce wmf :
No sampks liken an De=mba 25 and 26 in obsava ofdm Sute holiday
CarenLob"my Qualified Lab DNa
49 Daattba 4, 5, 6, 11, 12, 20, 21.22.23EMI i SOD
Amyw a avay in dK labmatay carol magic (LCS) ion below QC I' im Resdu rm this walyw in moctmed sempl Dannbm be biped low
ho Deamba 4 EHltmtt11S5
The peaisnn between the ample a id ample duplicatexceeded labotsy
_ comeol limiu
Aa Decemba 7, I I.12, 15. 19,20 EfHueta BOD
The d¢ lved oxygen depiction of the was blank mceeded 0.2 mg&