NC0004685_Application_20180228

GLASS FOR FUTURE
Nippon Electric Glass
Renewal of NPDES Permit NC0004685
Electric Glass Fiber America, LLC, Shelby, N.C. Facility
February 28, 2018

940 Washburn Switch Rd
Shelby, North Carolina 28150 USA
T: 704-434-2261 x2124
r, i�c Cno Cl/T1IQC
C"i Nippon Electric Glass
Via Certified Mail
Return Receipt Requested
February 28, 2018
Wren Thedford
NC DEQ
Division of Water Resources
WQ Permitting Section — NPDES
1617 Mail Service Center
Raleigh, NC 27699-1617
Dear Ms. Thedford:
E: [e-mail]
Todd Douthlt
Plant Manager
Electric Glass Fibers America
Nippon Electric Glass
RFri=i\iM
MAR 0 2 2018
Subject: Renewal of NPDES Permit NC0004685
Electric Glass Fiber America, LLC, Shelby, N.C. Facility
CEC Project 122-243.0017
We are pleased to enclose an original, signed NPDES Permit Renewal Application package along
with the two required photocopies. This is for Electric Glass Fiber America, LLC. (EFGA) facility
in Shelby, NC. We are requesting the reissuance of NPDES Permit No. NC0004685. The primary
SIC Code for facility operations is 3229-Pressed and Blown Glass- not elsewhere classified.
Approximately one percent of the waste load is from the Hanwha sheet laminate facility (SIC
3083). The wastewater outfall, Outfall 001, is located at latitude 35 degrees, 20 minutes, 26
seconds, by longitude 81 degrees, 37 minutes, 0 seconds with the receiving water being Brushy
Creek.
There have not been any changes to the facility since the previous permit renewal. We request
that all NPDES permit issues be directed to Mr. Richard Young, Focus Factory Manager. The
facility Manufacturing Manager, Maintenance Manager, and Enterprise Excellence Manager are
authorized to sign all reports required by the permit.
As part of this permit renewal package, we have included:
1. Cover letter;
2. Introduction;
3. EPA Form 1;
4. EPA Form 2C;
5. Narrative description of the sludge management plan; and
6. Analytical data.

2
The data presented in Form 2C Section V is based on plant operating data for the period December
1, 2016 to November 2017 and special analysis conducted by Pace Analytical Services Inc. Copies
of the Pace reports on the special analysis have been provided in the package (Tab G). The plant
operating data is from monthly DMR submittals.
We are respectfully requesting NCDEQ consider the following changes to our NPDES permit:
1. Eliminate the fluoride monitoring only requirement: The fluoride utilizing processes have
been eliminated from operations at EGFA and formerly, PPG Industries Fiber Glass
Products, Inc. This past year three samples were below 0.5 mg/1, with one sample at 2.2
mg/l.
2. Reduce the oil and grease testing to once per month. Oil and grease has not been detected
above detection levels over the last 52 weekly samples.
3. Test for ammonia October through March only: Ammonia has only been detected during
winter operations because of possible nitrification inhibition during low basin
temperatures. To monitor for this possibility, we request reducing ammonia monitoring
during the winter months only, specifically during October through March.
4. The current permit requires quarterly sampling for copper, lead and zinc. None of these
metals has been detected over the last several years. For this reason, we respectfully
request reducing the metals testing to semi-annually.
5. The EGFA wastewater treatment plant is a biological treatment plant with chemical
addition as shown in the attached application. Chemical addition is commonly ancillary to
biological wastewater treatment, including addition of coagulants, flocculants and pH
adjustment comparable to the activities conducted at this treatment plant. For this reason,
we request a change in the clarification of the treatment plant to biological 3 only,
eliminating the additional PC2 classification. Please note that NCDENR rescinded the PC2
classification in 2015 for the PPG Industries Fiber Glass Products, Inc., Lexington, NC
wastewater treatment plant, which is comparable to this plant.
Please feel free to contact me if you need any additional information or if you have any questions
regarding this submittal.
Sincerely,
Todd Douthit
Plant Manager
Electric Glass Fiber America, LLC.
Attachment
cc: Richard Young
File

Electric Glass Fiber America, LLC
Shelby, North Carolina
NPDES Wastewater Permit Renewal Application for Permit Number NC0004685
TABLE OF CONTENTS
Introduction........................................................................................................................
SludgeManagement Plan..................................................................................................
EPAForm l.......................................................................................................................
EPAForm 2C —pages 1-4.................................................................................................
Attachments to Form 2C Sections IIA and IIB..................................................................
EPA Form 2C — Intake and Effluent Characteristics — Outfall 001...................................
EPA Form 2C — Intake and Effluent Characteristics — Outfal1 002...................................
Figures
Topographical Map
Laboratory Reports
Pace Analytical......
2
Tab A
.Tab B
.Tab C
Tab D
.Tab E
Tab F
.............Tab G

INTRODUCTION
Electric Glass Fiber America, LLC (EGFA) operates a Fiber Glass manufacturing facility in
Shelby, North Carolina. This facility operates under the existing NPDES Wastewater Permit
Number NC0004685 which expires on August 31, 2018. This permit allows the facility to
discharge treated wastewater at 1.3 million gallons/day to outfall 001 and to discharge non -
contact cooling water to outfall 002. In addition to EGFA's Fiber Glass Manufacturing
operation, a Hanwha sheet laminate manufacturing facility is located adjacent to the EGFA site
and discharges approximately 10,000 gallons per day to the EGFA Wastewater treatment plant
for treatment. Wastewater from EGFA and Hanwha operations are sent to EFGA's wastewater
plant for treatment and both operations are covered under the existing permit. Additional details
and clarification for several items relevant to this permit application are highlighted below.
1. SIC Codes and Outfall 001 Testing
The SIC code for the Hanwha (sheet laminate facility) is 3083. The Hanwha site
discharges 10,000 gallons wastewater per day to the EGFA wastewater treatment plant
for treatment. This discharge makes up approximately 1/1001" of EFGA's wastewater
flow. Therefore, as required for the 3083 SIC code, EGFA performed volatile compound
testing on Outfall 001. Results from this testing are incorporated into Form 2C of this
application.
2. Outfall (002) Testing
Outfall 002, the primary stormwater outfall, is currently permitted for the discharge of
non -contact cooling water. Therefore, EGFA conducted the testing as set forth in Form
2C. This testing also included the required volatile compounds for SIC codes 3083.
3. Wet Weather Only Outfalls
Outfalls 003, 004, 005, 006, 007 and 008 are covered under the General Stormwater
Permit #NCG070000, Certificate of Coverage #NCG070015. These outfalls are wet
weather outfalls only and would contain little, if any, drainage from industrial areas. For
this renewal, testing was not conducted on these wet -weather outfalls.
4. Sample Reporting and Averaging
Sample reporting and averaging was provided in Form 2C as per NCDEQ DWQ's
"Directions for Completing Monthly Monitoring Reports" dated March, 2014. These
instructions provide guidelines with respect to rules for reporting and averaging less than
detectable "<" values. (i.g., a sample result with a value of less than the detectable limit
is considered to equal "zero" when calculating monthly and long-term arithmetic
averages). Also per NC DEQ DMR reporting guidelines, fecal coliform monthly and
long-term averages were calculated using a geometric mean.
5. Signature Authority
There will be no change requested in signature authority for monthly monitoring report

requirements. Signature authority for monthly reports as a "Duly Authorized
Representative" per 15A NCAC 2B.0506(b)(2)(D), will remain unchanged and is
delegated to the people holding the titles of Manufacturing Manager, Maintenance
Manager and Enterprise Excellence Manager.

SLUDGE MANAGEMENT PLAN
The wastewater treatment plant (W WTP) sludge generated by the Shelby facility is a mixture of
both primary and secondary sludges. The primary sludge is the result of clarification using lime,
aluminum chloride, polymers and coagulants to achieve floc formation and settling. The
secondary sludge is waste activated sludge from the biological treatment system. The secondary
sludge also contains bentonite clay and a small amount of ferric chloride.
Both sludges are combined in a sludge thickener/storage tank prior to dewatering. Polymer
addition and mechanical mixing, along with dilution water, are required to prepare the sludge for
the belt press. The sludge is then pumped to the belt press for dewatering.
The belt press has both a gravity drain section and a pressure section where the water is removed.
Typically, the solids are increased from 4-5% as it leaves the storage tank, to 25-30% solids as
discharged from the belt press. The dewatered sludge is transported via screw conveyors to a
roll -off box. The water is routed back to the head of the W WTP.
Before the roll -off box is picked up for disposal, a paint filter test is conducted on the sludge to
ensure that free liquids are not present. The dewatered sludge is then taken to a permitted, lined
landfill for disposal.

TAB A
EPA FORM 1

fill-in areas are s aced for elite type, i.e.,
FORM
4YEPA
GENERAL
LABEL ITEMS
I. EPA I.D. NUMBER
III. FACILITY NAME
cferynch). For Approved. UMB No. ZU4U-UUdb. Approval
U.S. ENVIRONMENTAL PROTECTION AGENCY 1. EPA I.D. NUMBE
GENERAL INFORMATION F 110000349070
Consolidated Permits Program
V. FACILITY PLEASE PLACE LABEL IN THIS SPACE
MAILING LIST
A. FACILITY
LOCATION
the
in the
SPECIFIC QUESTIONS
YES
NO
FORI
ATrACf
A Is this facility a publicly owned treatment works
which results in a discharge to waters of the
❑
®
❑
U.S.? (FORM 2A)
18
17
1 18
C. s this feciliry which curendy results in
discharges to waters of Ne U.S. other Man
those described in A or B above? FORM 2C
®
❑
22
23
24
E. Does or will this facility treat. store, or dispose of
haa'ardous wastes? (FORM 3)
❑
M
❑
28
29
30
G. Do you or will you inject at this facility any
produced water other fluids which are brought to
the surface in connection with conventional oil or
El
®
❑
natural gas production, inject fluids used for
enhanced recovery of oil or natural gas, or inject
fluids for storage of liquid hydrocarbons?
34
35
39
RM4
.F
this facility a proposed stationary source
which is one of the 28 industrial categories listed
in the instructions and which will potentially emit
❑
®
❑
100 tons per year of any air pollutant regulated
under the Clean Air Act and may affect or be
located in an attainment area? FORM 51
40
41
42
III. NAME OF FACILITY
SKIP I Electric Glass Fiber America,
LLC.
Young, Richard, Focus Fact
to
ouTY MAILING ADDRESS
A.STREET
940 Washburn Switch Road
Shelby
VM1
s ace.
am
it an
nthesis following the question. Mark X' in the box in the third column if
I not submit any of these forms. You may answer "no" if your activity is
action D of the instructions for definitions of bold-faced terms.
MARK
"X°
SPECIFIC QUESTIONS
YES
NO
FORM
ATFACMED
Does or will this facility (either existing or
proposed) include a concentrated animal
feeding operation or aquatic animal
production facility which results in a discharge
to waters of the U.S.? (FORM 28)
❑
®
❑
19
1 20
1 21
s this proposal facility (other than those described
❑
®
❑
in A or a above) which will result in a discharge
25
28
1 27
to waters of the U.S.? lFORM 2D
Do you or will you inject at this facility industrial or
municipal effluent below the lowermost stratum
containing, within one quarter mile of the well
bore, underground sources of drinking water?
❑
®
❑
31
32
33
(FORM 4)
Do you or will you inject at this facility fluids for
special processes such as mining of sulfer by the
Frasch process. solution mining of minerals, in
situ combustion of fossil fuel, or recovery of
❑
®
❑
geothermal energy? (FORM 4)
37
38
39
s this facility a proposed stationary source
which is NOT one of the 28 industrial categones
listed in the instructions and which will potentially
❑
®
❑
emit 250 tons per year of any air pollutant
regulated under the Clean Air Act and may affect
NC 1 1 28150
434 1 1 2261
EPA FORM 3510-1 (8-90) CONTINUED ON REVERSE

FROM THE FRONT
VII. SIC CODES 4-di it, in order of priori
A. FIRST B. SECOND
c
3229
(sPecvy)
Stone, Glass 6 Clay
3083
(sPecfi)
Laminated Plastics (Hanwha, LLC)
1e
1s 17
1e 1s ,9
C. THIRD D. FOURTH
7 (specify) � (specify)
15 18 1] 15 18 i9
Vill. OPERATOR INFORMATION
' A. NAME B. Is the name listed in Item
c Electric Glass Fiber America, LLC. VIII-A also the owner? ❑❑
B YES NO
18 19 55
C. STATUS OF OPERATOR Enterthe appropriate lettermto the answerbox !f "Other"s ec'
D. PHONE area code & no.
F = FEDERAL M = PUBLIC (otherthan federal orstafe) P
(specify)
J04
434
2261
A
S = STATE O = OTHER (specify)
NA
18 18
19 21
Fn 25
P = PRIVATE 66
15
E. STREET OR PO BOX
940 Washburn Switch Road
26 55
F. CITY OR TOWN
G. STATE H. ZIP CODE IX. INDIAN LAND
c
Shelby
NC 28150 Is the facility located
on Indian lands?
B
❑ YES
42 42 47 51
® NO
15 1 16 40
X. EXISTING ENVIRONMENTAL PERMITS
A. NPDES (Discharges to Surface Water)
D. PSD Air Emissions from Proposed Sources
N NC0004685
9
15
18 17 ,8 30
15 1 16
1 17 1 18 30
B. UIC (Underground Injection of Fluids
E. OTHER (specify)
(Specify)
General Stormwater
Discharge Permit
a
U
I ' NA
1
s
°
NCG070015, NCGO70000
15 1
16
1 ] 1 18 30
15 1 16
1 17
1 10 30
C. RCRA Hazardous Wastes E. OTHER s ec (Specify)
s R ' NCD980559983 9 1 ° 01958R41 Air Permit
15 16 17 18 30 1 15 1 16 1 17 1 18 30
XI. MAP
Attach to this application a topographic map of the area extending to at least one mile beyond property boundaries. The map must
show the outline of the facility, the location of each of its existing and proposed intake and discharge structures, each of its
hazardous waste treatment, storage, or disposal facilities, and each well where it injects fluids underground. Include all springs,
rivers and other surface water bodies in the map area. See instructions for precise requirements.
XII. NATURE OF BUSINESS(provide a brief description)
Continuous strand fiber glass manufacturing. For NPDES purposes, the site wastewater treatment plant also
receives and treats sanitary effluent from Hanwha, LLC. Hanwha LLC manufactures sheet laminate; SIC Code
3083 as noted in item VII.B. The flow from Hanwha represents only 1 percent of the total slow to the WWTP.
XIII. CERTIFICATION see instructions
I certify under penalty of law that I have personally examined and am familiar with the information submitted in this application and
all attachments and that, based on my inquiry of those persons immediately responsible for obtaining the information contained in
the application, I believe that the information is true, accurate and complete. I am aware that there are significant penalties for
submitting false information including the Dossibili of fine and imprisonment
A. NAME R OFFICIAL TITLE (type orpdnt)
B. SIGNATURE
C. DATE SIGNED
Tdd Zok14.4
P�
z-2.8-IW
/ViCkA.'P ..
COMMENTS FOR OFFICIAL USE ONLY
c
C
15
16 55
EPA FORM 3510-1 (8-90)

TAB B
EPA FORM 2C
PAGES 1-4

EPA I.D. NUMBER (ropyjromllem I ojFonn 1) Form Approved.
OMB No. 2040-0086.
Please print or Noe in the unshaded areas only. 110000349070 Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
APPLIFOR PERMIT TO DISCHARGE WASTEWATER
.=oEPA EXISTING MANUFACTURING,JCOMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
I. OUTFALL LOCATION
For each ouffall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(hw)
B. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN.
3. SEC.
1. DEG.
2. MIN.
3. SEC.
001
35
20
26
81
37
0
Brushy Creek
002
35
19
23
81
38
12
Unnamed Tributary to Beaverdam Creek
003
35
19
36
81
38
7
Unnamed Tributary to Beaverdam Creek
004
35
19
48
81
37
44
Unnamed Tributary to Beaverdam Creek
005 35 19 42 81 37 38 Unnamed Tributary to Beaverdam Creek
11. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average lows between intakes, operations,
treatment units, and outfalls. If a water balance cannot be determined (0,9., for certain mining activities), provide a pictorial description of the nature and amount of any
Sources of water and any collection or treatment measures.
B. For each ouffall, provide a descripbon of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets if
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (G.si)
a. OPERATION (list)
b. AVERAGE FLOW
(mdvde urrm)
a. DESCRIPTION
It. LIST CODES FROM
TABLE 2C-1
001
See Attachment 2C.11.6. outfall DOI
002
Non -Contact Cooling water
115.000 GFD
None
utuarground Spring water
35,000 GPu
None
Stormwater - Peak Flow, l-/kr
]4.9 CPS
None
003
w Stormater - Peak Flow 1"/hr
12.9 CPS
N.—
004
St.rmwaier - Peak Flev ll/hr
2.3 CFS
None
005
Storawater - Peak Flow 1-/hi
1.3 CPS
None
Continued on Next Page...
OFFICIAL USE ON LY(,Dpuenl guidelines suh- legervs)
EPA Form 3510-2C (8-90) PAGE 1 of 4 CONTINUE ON REVERSE

EPA I.D. NUMBER (copyJro. he. l fFonn /) Form Approved.
110000349070 OMB No. 2040-0086.
Please print or type in the unshaded areas only. Approval expires 3-31-98.
FORM
2C
NPDES
U.S. ENVIRONMENTAL PROTECTION AGENCY
FOR PERMIT TO DISCHARGE WASTEWATER
8rEPA EXISTING MANUFACTURING,JCOMMERCIAL, MINING AND SILVICULTURE OPERATIONS
Consolidated Permits Program
I. OUTFALL LOCATION
For each outfall, list the latitude and longitude of its location to the nearest 15 seconds and the name of the receiving water.
A. OUTFALL NUMBER
(lrsr)
B. LATITUDE
C. LONGITUDE
D. RECEIVING WATER (name)
1. DEG.
2. MIN.
1 SEC.
1. DEG.
2. MIN.
3. SEC.
006
35
19
23
81
37
18
Unnamed Tributary to Beaverdam Creek
007
35
19
25
81
37
29
Unnamed Tributary to Beaverdam Creek
008
35
19
24
81
37
48
Unnamed Tributary to Beaverdam Creek
II. FLOWS, SOURCES OF POLLUTION, AND TREATMENT TECHNOLOGIES
A Attach a line drawing showing the water flow through the facility. Indicate sources of intake water, operations contributing wastewater to the effluent, and treatment units
labeled to correspond to the more detailed descriptions in Item B. Construct a water balance on the line drawing by showing average flows between intakes, operations,
treatment units, and oulfalls. If a water balance cannot be determined (e.g., for certain mining achvities), provide a pictorial description of the nature and amount of any
sources of water and any collection or treatment measures.
B. For each ouffall, provide a description of: (1) All operations contributing wastewater to the effluent, including process wastewater, sanitary wastewater, cooling water,
and storm water runoff; (2) The average flow Contributed by each operation; and (3) The treatment received by the wastewater. Continue on additional sheets If
necessary.
1. OUT-
2. OPERATION(S) CONTRIBUTING FLOW
3. TREATMENT
FALL
NO. (lin)
a. OPERATION (list)
IS. AVERAGE FLOW
fm l de un/ta)
a. DESCRIPTION
b. LIST CODES FROM
TABLE 2C-1
006
stormwater - Peak Flow 1^ sr
2.6 CPS
None
007
stonm+ater - Peak Flow 1^/hr
12.2 CPS
None
008
eto mwater - Peak Flaw 11/hr
12.9 CPS
None
OFFICIAL USE ONLY (efjluani guidelines sub-csteg...e.v)
EPA Form 3510-2C (840) PAGE 1 of 4 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
C. Except for storm runoff, leaks, or spills, are any of the discharges described in Items II -A or B intermittent or seasonal?
❑ YES (mmp(ete thefoBowing table) W) NO (ga m Section IIn
3. FREQUENCY
4. FLOW
a. DAYS PER
B. TOTAL VOLUME
2. OPERATION(S)
WEEK
b. MONTHS
a. FLOW RATE (w mRd)
(vpeeh vah untie)
1. LONGTERM
2. MAXIMUM
1. LONGTERM
2. MAXIMUM
C. DURATION
1. OUTFALL
CONTRIBUTING FLOW
Qom,,
PER YEAR
NUMBER (fisr)
Vw)
mange)
(X'i'uwmae)
AVERAGE
DAILY
AVERAGE
DAILY
III, PRODUCTION
A. Does an effluent guideline limitation promulgated by EPA under Section 304 of the Clean Water Act apply to your facility?
❑ YES (mmplcre it,. III-B) ® NO (gn to Seedon IV)
B. Are the limitations in the applicable effluent guideline expressed in terms of production (or other measure of operation)?
❑ YES (complete Item III-0 ® NO (ga m Section IV)
C. If you answered 'yes' to Item III-B, list the quantity which represents an actual measurement of your level of production, expressed in the terms and units used in the
applicable effluent guideline, and indicate the affected outfalls.
1. AVERAGE DAILY PRODUCTION
2, AFFECTED OUTFALLS
(list ouifall numbers)
a. QUANTITY PER DAY
b. UNITS OF MEASURE
c, OPERATION, PRODUCT, MATERIAL, ETC.
(sPecfJ')
IV. IMPROVEMENTS
A. Are you now required by any Federal, State or local authority to meet any implementation schedule for the construction, upgrading or operations of wastewater
treatment equipment or practices or any other environmental programs which may affect the discharges described in this application? This includes, but is not limited to,
permit conditions, administrative or enforcement orders. enforcement compliance schedule letters, stipulations, court orders, and grant or loan conditions.
❑ YES (complete die following table) ❑ NO (go ra Item 11'.B)
1. IDENTIFICATION OF CONDITION,
2. AFFECTED OUTFALLS
3. BRIEF DESCRIPTION OF PROJECT
4. FINAL COMPLIANCE DATE
AGREEMENT, ETC.
e. NO.
b. SOURCE OF DISCHARGE
a. REQUIRED
b. PROJECTED
B. OPTIONAL: You may attach additional sheets describing any additional water pollution control programs (or other environmental projects which may affect your
discharges) you now have underway or which you plan. Indicate whether each program is now underway or planned, and indicate your actual or planned schedules for
construction.
❑ MARK -X° IF DESCRIPTION OF ADDITIONAL CONTROL PROGRAMS IS ATTACHED
EPA Form 3510-2C (8-90) PAGE 2 of 4 CONTINUE ON PAGE 3

EPA I.D. NUMBER (carryjms Lem 1 y/Farm 1)
CONTINUED FROM PAGE 2 110000349070
V. INTAKE AND EFFLUENT CHARACTERISTICS
A, B, & C: See instructions before proceeding —Complete one set of tables for each outfall— Annotate the outfall number in the space provided.
NOTE: Tables V-A, V-B, and V-C are included on separate sheets numbered V-1 through V-9.
D. Use the space below to list any of the pollutants listed in Table 2c-3 of the instructions, which you know or have reason to believe is discharged or may be discharged
from any outfall. For every pollutant you list, briefly describe the reasons you believe d to be present and report any analytical data in your possession.
1. POLLUTANT
2. SOURCE
1. POLLUTANT
2. SOURCE
Acetaldehyde
The majority of the pollutants
Amyl Acetate
listed in V.D.1 have been
Ethylene diamine
detected in trace
Formaldehyde
concentrations in a small
Methyl mercaptan
fraction of EPGAs raw
Napthenic acid
materials (as per
Styrene
manufacturer's SDS). only
Ethylene diamine is found in
Vinyl acetate
the raw materials in excess of
Xylene
trace concentrations.
Therefore, the majority of
these pollutants may be
present in extremely trace
concentrations in the influent
to the WWTP prior to treatment
and in even lower
concentrations (if present at
a11) in the effluent to
outfall k001.
VI. POTENTIAL DISCHARGES NOT COVERED
BY ANALYSIS
Is any pollutant listed in Item WC a substance
or a component of a substance which you
currently use or manufacture as an intermediate
or final product or byproduct?
❑ YES (ltsr all such paUarann
helau) [Z
NO (go ra Iles VI-B)
EPA Form 3510-2C (5-90) PAGE 3 of 4 CONTINUE ON REVERSE

r.niNTIN11Fr1 FROU TFIF FRONT
VII. BIOLOGICAL TOXICITY TESTING DATA
Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made on any of your discharges or on a receiving water in
relation to your discharge within the last 3 years?
© YES (ul anh, the fear(,) and describe rheir purposes below) ❑ NO (go m ticnlon V![n
Chronic toxicity testing (Ceriodaphnia) is conducted quarterly per NPDES permit requirements.
Vill. CONTRACT ANALYSIS INFORMATION
Were any of the analyses reported in Item V Performed by a contract laboratory or consulting firm?
® YES (list the name, adJmss, and telephone nnmher qL o.dr,Wla hn, o.fv-'Jhv. ❑ NO Igo m Section LAJ
each mmh laboratory o fffmr below)
A. NAME
B. ADDRESS
C. TELEPHONE
D. POLLUTANTS ANALYZED
(arearode Ano.)
(list)
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
[phone]
All except pH,
(EPA Lab Code: NC00014) WW Cert.
Huntersville, NC 28078
temperature,low level
No. 12
chlorine, conductivity, WET
and (61BA9 a CTAS)
ENCO Laboratories, Inc. WW Cert.
102 Woodwinds Industrial Ct. Ste. A
[phone]
No. 591
Cary, NC 27511
Research and Analytical
106 Short St.
[phone]
Toxicity, Surfactants (MBAS
Laboratories, Inc. WW Cert. No.
PO Box 473
a CTAS)
34, Biological Cart. No. 14
Kerneraville, NC 27284
IX. CERTIFICATION
1 certify under penalty of law that this document and all attachments were prepared undermy direction or supervision in accordance with a system designed to assure that
qualthed personnel property gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons
directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belie( true, accurate, and complete. I am aware that there
are significant penalties for submitting false information, including the possibility of fine and imprisonment for knowing violations.
A. NAME & OFFICIAL TITLE (type orpnnr)
B. PHONE NO. (area code eF no.)
/� /
c(d �o"4.f P/ant Rant. ¢r
—70'4 434-z7-4/
C. SIGNATURE
D. DATE SIGNED
it
EPA Form 3510-2C (8-90) PAGE 4 of 4

TAB C
ATTACHMENTS TO FORM 2C
SECTIONS IIA AND IIB

EPA FORM 2C SECTION ILA
OUTFALL 001 SCHEMATIC
Electric Glass Fiber America, LLC.
City Water Supply
1,500,000 gpd
Research Misc.
Sanitary
Boiler
Misc Process
Filtration Forming
1,000 gpd 3,000
60,000
43,000
Water
15,000 850,000
gpd
gpd
gpd
75,000 gpd
gpd gpd
Stormwater Garage/ Pads
(185,000 gpd)
W WTP
1" rainfallrDewatering
(See W WTP Schematic)
HANWA SIC CODE H3083
=10,000 gpd
Recycle
OUTFACEMGD
up to 1.3 MGD
Evaporation
335,000 gpd
Product
1,300 gpd

EPA FORM 2C SECTION ILA
OUTFALL 002 SCHEMATIC
Electric Glass Fiber America, LLC.
City Water
Supply
Stormwater
98.6 acres
Non -Contact
peak flow =
Cooling up to
74.9 cfs
115,000 gpd
Underground
Spring est.
35,000 gpd
Outfall
#002
Up to 150,000 gpd
+ stormwater
Notes:
Outfall #002 is the primary stormwater outfall for the Industrial portions of the property.
Cooling water discharges from the outfall are permitted under #NC0004685.
Stormwater Discharges are covered under the General Stormwater Discharge Permit #NC070000,
CDC #NCG070015
Stormwater Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q= peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1= Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flow for stormwater was calculated using an intensity of 1"/hr.
The runoff coefficient (C) used was 0.76 based on the following estimate: 80% Industrial, (0.9).
10%wooded (0.1)

EPA FORM 2C SECTION ILA
OUTFALL 003, 004, 005, 006, 007 & 008 SCHEMATIC
Electric Glass Fiber America, LLC.
Stormwater
30.8 acres
Outfall
#003
Peak Flow
12.9 cfs
Stormwater
3.1 acres
Outfall
#004
Peak Flow
2.3 cfs
Stormwater
2.7 acres
Outfall
#005
Peak Flow
1.3 cfs
Stormwater
Stormwater
Stormwater
9.0 acres
33.8 acres
2.6 acres
iOutfall
#006
Peak Flow
2.8 cfs
4#007
l
Peak Flow
12.2 cfs
Outfall
#008
Peak Flow
0.9 cfs
Discharges from Outfalls #003, #004, #005, #006, #007 & #008 are covered under the General
Stormwater Discharge Permit #NC070000, CDC #: NCG070015.
These areas contain limited drainage from industrial areas of the property. Outfall 002 is the primary
stormwater discharge point of the Industrial portions of the property.
Peak Flows were calculated using the Rational Method (Q = CIA) where:
Q = peak flow (cfs)
C = Runoff Coefficient (where: 0.9 = Impermeable, 0.8 = Graveled, 0.3 = Grassed, 0.1= Wooded)
I = Intensity
A = Area (acres)
Note: The above peak flows were calculated using an intensity of 1"/hr. See below for runoff coefficient
calculations.
RUNOFF COEFFICIENT CALCULATIONS
OUTFALL
C
003
0.42
20% Industrial (.9), 80%grassed (.3)
004
0.75
90% paved parking lot (.9) and 10% grassed (.3)
005
0.48
30% paved parking lot (.9) and 70% grassed (.3)
006
0.31
95%lawn (.3), 2.5%wooded (A), 2.5%graveled (.8)
007
0.36
10% industrial (.9) and 90%grassed (.3)
008
0.36
10% Industrial (.9) and 90%grassed (.3)

EPA FORM 2C SECTION II.B
W WTP Treatment / OUTFALL 001 SCHEMATIC
Electric Glass Fiber America, U.C.
NPDES Permit NCO0O4685 Renewal Application
Process Water —(0.8 MGD)
Sanitary —(0.06 MGD) Bar
Screen
Stormwater—(0.12 MGD) 1-T
HANWA—(0.018MGD)
UTFALL #001 I
A -A
Recycle/
cooling Water
4-C
SLUDGE PROCESS SCHEMATIC
iw
"S�
ymer
tion
ter
Grinding
1-L
FeCla
Flow Load Flash Min Primary
equalization Equalization Tank Clarifers
1-0 2-D 1-011-G,2-C 1-U
me AICI, Anionic Polymer
Sludge to
Cationic Coagulant Thickener
Secondary Aeration
Clarifers l3) s Tank12)
2-C,1-U 1-1, 2-U
Polymer
Sludge to
Thickener
Lime
RAS to
Aeration
Bentonite
Clay
Treatment Codes Used From
Table 2C-1
1-G
Flocculation
1A
Grinding (Comminutors)
1-0
Muir
1-T
screening
1-u
sedimentation lsettlin
1-y
send Filtration
2{
Chemloal Precipitation
2-D
coagulation
34
Activated sludge
c-A
olsche eto surface water
4{
ReI / Rasycle of Effluent
s{
Bah Fihnlion
s-E
chemical conditiemng
si
Gravilynickening
5-0
Landfill

TAB D
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 001

PLEASE PRINT OR TYPE IN THE UNSHADED AREAS ONLY. You may report some Or all ofMls Informalion EPA I.D. NUMBER (-,j Men9/ 1Form 1)
on..parat. greets (use Me same ymm.) Instead of compleling these pages. 1100003990T0
SEE INSTRUCTIONS.
Ol1TFALL NO.
V. INTAKE AND EFFLUENT CHARACTERISTICS (c.n5nuetlfibm page J o/Form 2-O)
PART A -You most provide Me results of at bard are analysis fw every sollulam In this tube. Compirde one table for each ducall. See instructions Mr additional Pieces.
3. UNITS
4. INTAKE
2. EFFLUENT
G c?h Jelagk)
1. awmq
VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM DAILY VALUEa61Q
((fmroJoSb)
AVERAGE VALUE
d. NO. OF
a. CONCEN-
.NO. OF
01
1. POLLUTANT
(2)MA55
RIMASS
111CONCEMMTON
0; MASS
ANALYSES
TRATION
b. MASS
CONCEMRATON
(2)MASSa.mandtBOal
Oxygen31.29.95
1.71
T.22
52
mg/L
lbS
Dementl (BOO)b.
Chemkal Oxygen0
7COME�An�
1
mg/L
1bs
Demand(C OM
PCO�EWMPON
Tota OM.k Carbon24.4N/A
N/A
N/A
1
mg/L
1bs
a. Tmal Suspmbd21.T
1
52
mg/L
lbs
Send. (TS9
e. Amman. I.M
0
52
mg/L
lbs
VALUE
VALUE
VALUE
VALUE
I. Few
0.65
0.57
0.50
365
MGD
g. Temperature
VALUE
VALUE
VALUE
'C
VALUE
(wlnre�
25
23.3
19.6
258
h. Temperacm,
VALUE
VALUE
VALUE
•C
VALUE
wmer)
28
2T.5
29.1
258
MINIMUM
MAXIMUM
MINIMUM
MAXIMUM
1. PH
6.2
T.9
258
STANDARD UNITS
PART B- Me* W In column 2-a for each polluart you know Or have reason to belese ear present. Me* Win column 24b breech Pdub t you bellow to be absent. If you mark column 2a for any pollueM whish la limded either
directly, w indeactly but g,ph ssly, in an eSNent limitations guideline, you mug provide the results of st West one amebae for Ms, pollulant. For other Pollutants for which you mark coating 2a, you must provide
wmltativa data or an a .nation oftheir presence In Your discharge. Complete one cable for each ouHal. Sae the instructions foratltlltionel decide and require ...
2. MARK
-X•
3. EFFLUENT
4. UNITS
5. INTAKE
1. POLLIRANT
b. MAKIMUM 3O DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
b
a. MAXIMUM DAILY VALUE
Wuwdrable)
VALUE
CAS NO.
BELIEVED
BEUEVEO
d. NO. OF
a. CONCEN-
b. NO. OF
ItI
(11
p)
(11
(�/imnJuM1le)
PRESEM
ASSENT
CONcEN7M71ON
(21MASS
CONCE}ARATON
RI MASS
CONCENTRATION
121 MA5.
ANALYSES
TRATION
b.MASS
CONCENRUTON
(2)M415
ANALYSES
a. Sr.mie.
�/
x
(2x959bT-9)
to. Chlr,H, T.W
�/
Residual
c. Cd.r
X
d. Few"Norm
X
20.0
3.38
1.96
52
#/100 ml
a. Flume
V
2.2
11.9
2.2
10.5
0.85
3.5
4
mg/L
lee
ItBsaHe-sl
f'Nbale-Malt°
�/
17.4
94.3
17.4
82.7
14.63
61.0
4
mg/L
lbs
(a.A)
/�
EPA Form 351 LL= (S-Wh PAGE V-1 CONTINUE ON REVERSE

2. MARK'X'
3. EFFLUENT
4. UNITS
5. INTAKE(opmmm)
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
R. LONG TERM
AND
5
a. MAXIMUM DALY VALUE
('r—la6l.)
Wan ahuM.)
AVERAGE VALUE
CAS NO,
BELIEVED
SEUEVED
a. NO. OF
aCONCEN-
b. NO. OF
(L
O)_
(1)�
(tl
(i(uw,I.bk)
PRESENT
ABSENT
CONCENTRATION
(2)M
CONCENTRATION
121MAS5
CONCENTRATION
(2)MAW
ANALYSES
TRATION
b. MASS
cpncENIaATON
(21 MH33
ANALYSES
9.N Mini,
Tdtlmim, c(m
q
,�[`
h. ORa
n. OR and
X
<5
52
mg/L
lb.
Pinmomus
(m, P). TmN
2(
3.6
19.5
3.6
17.1
1.32
5.5
4
mg/L
lbs
pR}14-01
J. Rmiiomc"
(1)No. Total
X
(2)Beta, TOW
X
(3)Radium,
TWaI
(4)R aawm n1l.
X
ToW
Sub. b
( mvr.)
x32.1
179.0
1
mg/L
lbs
(ue5&]9a
L SuMM
�/
I. S)
3ulMe
d
ta28&a5.3)
n-da-d-
X
10.4
0
1
mg/L
lbs
..Aluminum.
Tatal
629-9 S
X
<0.1
a
1
mg/L
lbs
p. Barium, Trial
D449 3P3)
a. Boron, Tm.l
�/
x
0.360
1
mg/L
lbs
p44&aa)
1.9
..C.b.n.T.W
(744"84)
X
m
a. n. T to
..Iron,")
X
0
1
mg/L
lbs
<.D5
L mw..Nm,
TOW
X
2.38
12.9
1
mg/L
lbs
(2439A5i)
u.MoNDemum,
and
X
(74
043&9&
m
an..,
Indal
qaa
0.i&%5)
w. Tin. Total
(7 0.31s)
X
.,m.ni.m,
TOW
X
(]H0.Rfi)
EPA Form 351M12C (&90) PAGE V-2 CONTINUE ON PAGE V-3

EPA 1.0. NUMBER (amh from Lem l oho m 1)
OUTFALL NUMBER
110000349070
001
CONTINUED FROM PAGE 3 OF FORM 2-C
PART C - If you are a primary Industry and this oulfall contains process waeewgM, refer to Table 202 in the Instluc h nh to determine which of the GCIMS factors you must test for, Mark'%' in column 2-a for all such GCIMS
fractions that apply to your industry and for ALL toxic males, ryandhi.. and total phenol. If you are not required to mrtk column 2-a (serorrday IMush re, no bac cess wee ., oudalla, and Tmmequhed GUMS
ha4long, mark'%' b column 2-1, for each Pollutant you know or have reason to believe is pmeent. Mark'X- in column 2-C for each pollutant you believe Is absent. V you maw column 2a far any pollutant, you must
provde the ...he of M least one aneyes for that porutent. If you mask column 21, for any polutaM, you must provide the Others of at least one analysis for that pollutant if you know or have mason to believe it all as
discharged in cony Mbns of 10 ppb or greater. If you mark column 2b Nr acmMln, acryloniblb. 2A dinlbophenol, or 2-methyl-4, 6 Uindimphenol, you must provide the results of at ball one analysis for each of these
pellNeMs which you brow Or have reason to bebeve the you discharge In concentrations of 100 Pipe or granter. Olherade, for pollutants W which you mark colomn 21,, you must either submit at Mole One analysis or
belly, describe the marginal the Polluted is evened to be discharged. Note that them are T pages to this pad, please review, each carefully. COmPMte one table (ell T pages) far each orator, See IhMrvctlons for
additional details and requirements.
2. MARK'%'
3. EFFLUENT
4. UNITS
5. INTAKE (apnonaf)
I. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
b
r
w
a. MAXI3AUM OAILV VALUE
(q-1,61)
VALUE Q%✓wlluale)
AVERAGEVALUE
CAS NUMBER
BELIEVED
BEUEVEO
a. DONCEN-b.
NO.OF
O1
It)IIdNO.OF
flif.deAle)
PRESEM
ABSEM
CONCENTMTC. 121 MA53
CONCENTRATON O)MA63
CONCENTRATION 121MAa3
Af'LAlYSE$
TRATION b. MA35
CGNLENTMTION (21 MA%
ANPLYSE
METALS, CYANIDE, AND TOTAL PHENOLS
IM. Mdmmy, Teel
(344"SL)
2M. Afeedic, Tam
X
<0.01
0
1
mg/L
lbs
(T440.38-2)
3M. Beryllium, Tow
�/
x
p44041-T)
4M. C.Occom, Tme
H0139
9M. Chromium,
x
<.05
0
1
al
lbs
ew (7440-47-3)
M. Copper. TOM
�/
x
<0.005
0
4
mg/L
lb.
Tas"")
TM. Lead, Tow
�(
x
<0i005
0
4
mg/L
lbs
(7439-92-I)
By. Mercury, Taw
�/
x
(T4349Td)
sm. M4N, Tow
(7440-02-0)
X
IOM.SMenlum,
v
Tdel (TT82494t)
11 M. Suter, Tow
x
<0A05
0
1
mg/L
lbs
(7440-22-4)
12M. Trainor.
Total (7UD-28-0)
13M. Lost. Total
v
(T444S5 0)
14M. Cyanide,
v
TOM (57-124)
15M. changes
\/
Total
x
DIOXIN
2,3,7,CTetra
` /
DESCRIBE RESULTS
"odoanm-P-
I
I
DOdn (1T&-014)
/]�\
EPA Folm 3510-2C (8-90) PAGE V-3 CONTINUE ON REVERSE

2. MARK'X'
3. EFFLUENT
d. UNRS
5. INTAKE (o tlmaO
1. POLLUTANT
p. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
8. LONG TERM
AND
e
a. MAXIMUM DAILY VALUE
(q mnildileJ
VALUE (/mvllable)
AVERAGE VALUE
D. NO. OF
III
11
IT
Itl
CAS NUMBER
TESTNG BFLEVED
L
eEDEVED
dNO. OF
a. CONCFM
uwulWle
N )
REQUIRED PRESENT
ABSENT
CONOENIMTON Tp MA55
CONCENTRATION I IMA55
CONCENTRAT. (21 MA55
ANALYSES
TRATION b. MASS
CONCENTRATION (]I MASS
ANALYSES
GO/MS FRACTION— VOLATILE COMPOUNDS
N.Aevobq
x
e005
0
1
lb.
(t Bi-0be)
/�
2V'-13-1) ie
X
0
1
lbs
(tw-v-1)
<.05
3v.
x
002
0
1
lbs
9143E2)
/�
c,
fl�—/
(w4s-1)
5v.3
V
c.002
0
1
lbs
(7.B 2)oMm
)
/�
W. Cuban
TeDetltlotltle
X
c.002
0
1
lb.
(56235)
rv.cbnrapa�Mene
x
<.002
0
1
1g/L
lbs
(1n3-saT)
/�
ev. cWierors
bromomMme
X
<. 002
0
1
1g/L
lbs
f34i&t
x
<.002
0
1
ng/L
lbs
ITSaaJI
/�
iw.2-C
xbSheynvAl Eller
c.005
0
1
m9/L
lbs
x
002
0
1
m9/L
lbs
(6iE&J7$ 3)
/�melNm
<.
IW. Dk WI
wpmpmMene
5 74)
X
c.002
0
1
rtg/L
lbs
13VZNmo-
.E
X
<, 002
0
1
n /L
lbs
(dift" )e
]&i1-8)
MV. tt-oluJPro-
X
<.002
0
1
m9/L
lbs
Mena (i534J1
/�
15V. 1,2-0iN -
x
<.002
0
1
mg/L
lbs
18V.LI-gWNro-
�/
x
<. 002
0
1
mg/L
lbs
aNytena pS35 j
1T/.1.2-Ditl "
�/
x
<.002
0
1
mg/L
lbs
gopene P&ET-5)
Propylene
X
<. 002
0
1
mg/L
168
(Sd2-I�
1w. mymni°n°
X
<.002
0
1
m9/L
lb.
(10 14)
2W. WWyI
<. 002
0
1
m9/L
lbs
13.mi& (7"-0 I)
21V. WIA0
<. 002
0
1
tg/L
1bs
CWbp (Id-0T-S)
EPA FoBn 351&2C (&W) PAGE VA CONTINUE ON PAGE V-5

CONTINUED
2. MARK-%'
3. EFFLUENT
4. UNITS
S. INTAKE (opnonaq
1. POLLUTANT
b. MMM,UM 30 OAY VALUE
c. LONG TERM AVRG.
8. LONG TERM
AND
b.
<
aMA%IMUM DAILY VALUE
Qlmm/oDA
VALUE Q/uv"11A
AVERAGE VALUE
CAS NUMBER
TEs1lNG 0F11EVED
BELIEVED
C. NO. OF
a. CONCEN-
G. NO. OF
111
Ip
111
111
(I/wwlcAle)
REWIRED PRESENT
A63EN!
CONCEMMTCN R)MPb6
CONCENIRATIW 121 MA66
CONCENTRATION ]I MA55
ANALYSEfi
TRATNIN O. MA55
CONCENTRATION D)NAGS
Y$ES
GCIMS FRACTION- VOLATILE COMPOUNDS (rnnlnueq
M, Mamylene
�/
x
<, 002
0
I
mg/L
lbs
CFbn& (i5-0 2/
23V.1,122-
iebaddwoelhena
X
c.002
0
1
mg/L
lbs
8.34d
24V.
24v. TebacMMo-
x
c.002
0
1
mg/L
lb.
e(19-tb41
/�
VTo
x
002
0
1
mg/L
lbs
10"8mene (
/�
25V.13-Trans
pWoroempene
X
<. 002
0
1
mg/L
lbs
5 5
2T, 1,1,1-TneY
X
<. 002
0
1
mg/L
lbs
emana Tlld}al
28V. 1,12-T---1
c.002
0
1
mg/L
lbs
ewm D8d0a)
/�
28v Tndxwo-
V
<.002
0
1
mg/L
lbs
.mKenv De-mdl
/�
aoromam.ne
X
c, 002
0
1
mg/L
lbs
SSBd
TV. wnyl chime
X
c002
0
1
mg/L
lbs
TSdtd)
/�
3CBeS FRACTION -ACID COMPOUNDS
IA.x Narapbanel
�/
x
(8S5Td)
2A 2,4 DiM.w
o.ol(120-G4)
3A 24-DimamyF
�/
x
phenol(105474)
4A. 15-0ioilo-
v
Cresd(53452-1)
SA. 2 0-Dlnih
,_I(51-28-5)
5A.2-N4ophend
(80.IS5)
]A.FN&Whend
V
(10 M4)
8A.P WWa -
V
Cread(58-50-T)
BAPenMrmlmo-
\/
x
pnend (eTdea)
Id wand
IID8aS2)
/�
11A 3A,6-TlkNoro-
pnend l0e-o5-31
EPA Fmm 3510-2C (8-80) PAGE V-5 CONTINUE ON REVERSE

f.(1NTINIIFll FR(IN TNF MR W
2, MARX'X'
3. EFFLUENT
d. UNITS
5.INTAKE (apnMap
1. POLLUTANT
b. MAXIMUM ]O MY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
p
rZE..R.E.
a. MAXIMUM ONLY VALUE
11/mrv/ahle)
VALUE plawllohle)
-
AVERAGE VALUE
CAB NUMBER
TIOELEVFO
BEUEVEO
O. NO.OF
aCONCEN-
b. NO. OF
p)
IB
OI
Ip
(/favallMle)
O PRESENT
ABSEM
OONCENiNFTCN 2)A
CONCEMRATION RIMA55
CONCE.(l) .N RINA55
ANALYSES
TRATION b. MASS
CONCENiRAPON RI MA58
LYRE
GCMS FRACTION— SABEMEUTRAL COMPOUNDS
18.AcenapbMMe
x
I�
2B.AcenePbhiene
X
RO&95-8)
30.Mlbracme
�/
(120.12-7)
x
48. Bewtline
(92-Bi3)
x
se. Benin lol
AmNmme
�/
Is9-ssa)
/�
be. Beam b)
x
(so-32-e)
/�
73.3dRenz
W..a
wo mbmw
lzb}99z)
N].Bmm/sM
�/
x
PerMem(1B14.Z
M. B (a)
N)
V
(207
108. bB. Ba Csx/wa
1M91-1) ne
V
111-91-1)
/�
I B. Be (ICAUr
Elver
V
iH
28.& 12-
('Momuep PA
�/
x
EIFn1102-0 1)
13B.&aUlEAU-
OaT�PNMebte
—005
0
1
mg/L
lbs
plT-0Id
14B.4&omaP "o
PnmN E r
x014S
)
158. BuM&rMo
�/
x
FiM4-te (8 7)
165.}CNPro-
ee
X
(914&7)
5&T)
.1-Chao-
0
l2-3) EMe.
V
pb9}Tza)
(700
/�
(21&01-9)
t 9e. o9,errm lahl
MW1c3
x
(5}]0.])
I�
"S. 1,2-Cl -
v
berizMe(9SS0.1)
21
berrzme(511.T}I)
EPA Form Ml1 =(8-00) PAGE V-e CONTINUE ON PAGE V-0

2. MARK'X'
3. EFFLUENT
<. UNRS
5. INTA(E (opt-
1. POLLUTANT
0. MNUMUM 30 DAY VALUE
c. LONG TERM AVRG.
y. LONG TERM
AND
p,
e. MAXIMUM DALY VALUE
(I/mmlus/e)
VP1UE (UmvJnble)
AVERAGE V&UE
CASNUMBER
TESTING BELIEVED
BFLEV(D
G. NO.OF
e. C0NCE81
D. NO. OF
(t)
Itl
(11
(1j
flfv lvble)
REOUIREG PRESENT
AIBENT
rpryCENiRAT10N 12)1 4
CONCENTRATON U)M
CONCENTRATON
(])..
ANALYBEB
TRATION b. MA55
CONCENTRATION (2) A S
ANALYSE
GCIMSFRACTION—BASEMEUTRALCOMPOUNDS(.-I'e ,✓
me. 1,NNTMImo-
�/
ee.ne(18 7)
238.3.&Dhhlk ro-
�/
e dne(91-W)
US.. DktlM
�/
PMM1Yete(8 2)
x
25B.OImaNyl
PM1Ih-
1-11-
28B. Di-N- m
X
<.005
0
1
mg/L
lbs
PM1Mnleb (WTN 2)
2)8.2A- .
toluene (121-I42)
288.2,6-DmMo-
298. p 14-004
�/
x
PhMW.(117J 0)
38S 12-Ce(eny
me*
he (ea A -
bemm—) (I Rd
11 S. NoofenMN.
�/
2116d0.0)
RB. FW--
86 )1))
33B.*xod o-
�/
eevene(11874t)
lh l .ne (8788-3)
35B. Nee m—
rydo9enD8tlerw
(77474)
.8 HexaCiluo-
�/
x
.None (6)-T2-1)
ne. mmne
3%Nne
(19
l};y.9-55)
38B. Iaa9M1m .
8391)
398. MpWhalene
�/
x
(91-2o-3)
eo6. Nbob—
(8&9S3)
Nt B.
C lllmebMenYne
".h
(82-)}9)
NIB. NN .e
N-ProPNe
xnine �/
621-04n
EPAFoml35162C( W PAGEV-) CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
. MARK'X'
3. EFFLUENT
�. UNRS
S. INTAKE (opumP(]
1. POLLUTANT
b. MAXIMUM W DAY VALUE
c. LONG TERM AVRG.
e. LONO TERM
AND
b.
n,,UIE
c
a. MAXIMUM DAILY VALUE
Q(-1W
VALUE Ifmdleble)
AVERAGE VALUE
CAS NUMBER
BELIEVED
BELIEVED
E. NO. OF
B. CONCEN
b. NO. OF
II)
DI
(1)
(1)
ftf—'WO
PRESENT
ABSFNr
CONCEll' 11.N (2)MABB
CONGENTRATION (2)MASS
LONLENifWTION 121 MA55
ANALYSES
iRAT1ON b. MASS
LM'CENTRATION 121 MA55
LYSEB
G"S FRACTION —BASEMEUTRAL COMPOUNDS (emonue�
N.M¢u
43B.
UpbenybmaH
x
S&]O6
NB. PM1menNrene
(e5 01-0)
x
{SB. Ppene
v
(12&00-0)
N8. 12.FTrn
Wloroaeneene
�/
x
(1M 2-1)
GCRMS FRACTION —PESTICIDES
1P.AIOIR
x
2P.0 BHG
(]I9a2a)
X
3P. ryBHC
v
I]1B-05-T)
P.+BHL
15e-Beal
X
sv. a eHc
]1Befi-B)
/�
x
5Yue1
x
!P.{B-0DT
�/
x
(50.253)
W. 4,C-DDE
(724")
(7 54S)
10P, DjI
v
ISLLSAO
11P. e.Fll�7) W.b
x
12P, ryEnEawtlen
�/
(IIS29-T)
x
13RE dasulMn
3ullele
v
14P. E .m
�/
(T2.2")
x
m '.
A
X
Q421-9
21SH)
16P. IrclAor
v
ITBu e)
EPA Form 3510.2C (SM) PACE V-S CONTINUE ON PAGE V-9

EPA I.D. NUMBER(.-Pyyj Item l o/Fm 1) OUTFACE NUMBER
001
CONTINUED FROM PAGE V-B 1
110000349070
2. MARK-X
3. EFFLUENT
4. UNITS
$I INTAKE (aynw•0
1. POLLUTANT
0. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a LONG TERM
AMID
p
�FINLJ
e
e. MPXIMUM DA LY VALUE
(Wr—l-ble)
VALUE ("._, M1le)
AVERAGE VALUE
CAS NUMBER
rvSEL1WE0
Pc'UEYEO
E. ...OF
aCONCEN-
9. NO.OF
(p
(p,
(1)
j1I
(i(avoJM(e)
PRESENT
A6SE1?
CINKENIRA. (2I MA89
CONCENI' ON (2)AN5S
CONCENTRATON 121 MA55
ANALYSE$
TRATIGN E.MA$$
CONCENTRATION pM4SSALYSES
GCIMS FRACTION— PESTICIDES (oommned)
1TP.NIW•9heM1lm
(tl
45Td
X
1 SP. PCB-12Q
�/
(53e89-214)
19P. PCS-12U
�/
(I10973 1)
x
20P. PC61n1
�/
(Ifl01-2&2)
21 P, PCB-1232
�/
(111e1-IM)
22P. PCB-120
�/
(1MT2-2 )
x
3]P. PC61280
v
p 1095-02d)
24PgB-'216
(128TF11-2)
!9lP.To001-352);rene
v
.PA Form 3 11 n (&90) PAGE V-9

TAB E
EPA FORM 2C
INTAKE AND EFFLUENT CHARACTERISTICS
OUTFALL 002

PLEASE PRIM OR TYPE IN THE UNSHADED AREAS ONLY. You may hi some oral of this infonnnion EPA LD. NUMBER (e Aom Item) 7A'mm 1)
on separate sheatd (um Me same ydma0 instead of cdmpleting these prig®. 1100003490T 0
SEE INSTRUCTIONS.
OUTFALL NO,
V. INTAKE AND EFFLUENT CHARACTERISTICS (cmttnued from page 3 of Form 2-0)
PART A —You must posted the handle of M least one analyst for Sissy potdant In Ms uses. Compete one table far each oudall. See intlmtlions for addliomd detah.
3. UNITS
4. INTAKE
2. EFFLUENT
(.. n'F pblonAt
(.power)
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
a. MAXIMUM ONLY VAWE
01m.fiche)
gyovmleblel
AVERAGE VALUE
d. W. OF
a. CONCENH
b. NO. OF
1. POLLUTANT
CONCENTRATION
RI MASS
CONCNTRATON
(2)MASS
(1) CONCENTRATION
t21 MASS
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2) MASS
AN4YSE5
a. Diochambal Oxygen
c0. 02
0
1
mg/L
lea
Demand(80➢)
b. Chemical Oxygen
<25
0
1
mg/L
lbs
Daman If OD)
c. Tool Organic Carbon
2.1
0.53
1
mg/L
lea
(Tlwj
tl.TOW
(Suspentlatl
Sdi(ISs
c2 5
0
1
mg/L
lbs
e. Ammon I. At
0.27
0.07
1
mg/L
lbs
VALUE
VALUE
VALUE
I. Fla.VALUE
03
D3
,02
2
MGD
g. Temperature
VALUE
VALUE
VALUE
'O
VALUE
(wmree)
14
1
to. Temperabre
VALUE
VALUE
VALUE
°C
VALUE
yammer)
19
1
MINIMUM
MA7"Ll
MINIMUM
MAXIMUM
I pH
T
2
STANDARD UNITS
PARTS— McM'X' In column 2a foreach pollulamyou know orham reasonto balms is premnt.Mark'X- Incolumn 2-0for each polutintyou beteveto beabsent%you mark column 2aforartypolusmwhich Is lmftW SOW
di doW, or Indirect, but expemN, or an effluent limitations gulBable, you must proNde the results of at bast we analysis for that pollutant. For other polutn for whidf you mark column 2e, you must prdulde
uarsttNe data or an a anamn of their presence in your ducharde. Complete om table for each outfal. See the NaVudlons for additional details and requirement.
2. MARK'X'
3. EFFLUENT
4. UNITS
9. INTAKE (opnonu
1. POl1IRANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM AVERAGE
AND
a.a
a. M"MUM DNLY VALUE
(d mmlMle)
(W-1able)
VALUE
CAS NO,
9EUEVEO
SEUEVEO
dNO. OF
a. CONCEN-
b. NO. OF
U)
ry)
(tl
pl
((/m'wlWlef
PRESENT
ABSENT'
CONCENTMTION
(2)MASS
CONCENTRATION
t2)MASS
CONCENTRATION
(2)11
ANALYSES
TRATION
b. MASS
CONCENTRATION
(2)M444
ANALYSES
a. fCdriee
v
(N959bid)
b. Cleodoe. Tom
X
19.0
.0048
19.0
.0048
10.5
.0018
2
ug/L
lbs
Residual
/�
c Cder
J. Fecal Coal
`x
Y
,v`
e. Fluoride
(189µga-0)
hMbalB�llble
m M
X
EPA Form 35100.2C (8-90) PAGE V-I CONTINUE ON REVERSE

REM V-B CONTINUED FROM FRONT
2. MARK 9C
3. EFFLUENT
4. UNRS
$. INTAKE (o uwr
1. POLLUTANT
b. MNOMUM 30 DAY VALUE
c. LONG TERM AVRG. VALUE
a. LONG TERM
AND
a
a. MAAMUM DAILY VALUE
V.-Wb)
AVERAGE VALUE
CAS NO.
BEUEVEG
BEUEVED
5. W. OF
c CONCEN-
b. NO. OF
1TAA
Oj
Of—Wk)
PRESENT
AMSEM
CONC
(3 M455
NT
CONLENiRATION
❑ M143
S
CONCFMRATOH
(2j MASS
ANALYSES
TRATION
b. MA56
CANCENiRATON
(21 MA35
ANALYSES
TOW panic(ox
`,
1L
h.O0 end
Greu
I, PM1as
(u P). j,i T.1x
pi2alw)
y Re6oac9vn
(1)ftp.. TOW
(2)B., Total
`x
2[
,v`
(3) Re ium,
TOW
({) Radium 226.
Total
k. SUIMW
(-MIJ
(14808-)B-0)
/�
1. SUM&
�/
x
(uV
S aMN
.,j
X
14265�Sa1
a.Suft anm
X
p, M—.m,
T.,/�
v
<0.1
C
1
mg/L
lb.
R{29-903)
p.Bm m, TOW
R{ 39 n)
TOW)
(""2-8
X
33.7
8.4
1
mg/L
lbe
TOW
�/
(Cobak.
7""")
x
lmn.T W
1.3]
0.34
1
mg/L
lbe
(743"")
C mr.m.m,
TO l
6.68
1.67
1
mg/L
lb$
{39954)
u. ~ftnum.
Tall
V43p 98-i)
. MM.,...,
(743
R{3B %Sj
N.TaW
pU
x0d1-51 I�
A. TXmWm.
ee
(7MO 32E)
EPA Fann 3510.2C (8-90) PAGE V-2 CONRNUE ON PAGE V-3

EPA LD. NUMBER (held n.m h.m 1 o/FOrm q
OUTFML NUMBER
110000349070
002
CONTINUED FROM PAGE 3 OF FORM 2-O
PART O - If you area pmmary mdusiry and this DOWN cement preceN wastewMx Mier to Tape 2c-2'm me instmclWne to M.. wh,M .(Me GOIMS kW.ha you mug WM for. Muk'X- m cdumn 2-a for MI suds GCMS
hatllons teal appM la Your endustry and for ALL tom mdaW, ryanNee and Totalphenols. h ydu ere not required to mirk coumn 2-a (dew ifbudsros. nonprocess wadewMer oufMls. and fwmequaed GGs15
leoHMR), mark'%' m Wlumn 2.b bt each polutam you know or haN reason to Eeheve Is PMSem. Me& -X' In column 2-c far each pdlulYn you be gne Is edged. If you mast column 2a for any (gp m ydu must
proved the refuse of at used one analysis far mat possess. If you may column 21, for any poluMd. ydu must provide the reties of at heard one analysis for that polluted d you know or legs reason to Beal A"M
duhargd In com emrellons of 10 sob or greater. If you mark column 26 for acrotn. acrylonhnle. 2 a dndmphend. or 2.melhy". B dint/ phend, you dual provide the Might 00 Waal one analysis for each d these
pail which you under or have reason to believe mat you ddedrge in concentrations of 100 ppb Or gresier. Omenede, for pollutants for which you male column ID, you MUM either aubme at bap one analysis or
briefly dedcebe the reatons the plldent IE .,ad" t0 be discharged. Note that mere are T pagCs to This pan, please review each carefully . Complete One table (all l paged) for each cu fall See InMNellons for
addgling at anar wrements.
MARM'X-
0. EFFLUENT
a. UNITS
S. INTAKE (rwnada01.
POLLUTPNT
p, MAXMUM Mt DAY VALUE
c. LONG TERM AVRG.
a. LONG TERMA�
RUE
n2.
e
a
aMAXIMUM DNLY VALUE
(rmvewig
VALUE bTm'audle)
AVERAGE v
CAS NUMBER
BEUEVEO
BEUEVEO
O. NO. OF
a. CONCMi
111ftlpl
(1)b.NO.OF
(r(awrlaM<)
PRESENT
MMENT
CONCMrtRATK)N (2)M
CGNCENTMTIGN 121 MA99
<ONDENTRATIXI (21MA6$
ANALYSES
TRATION b. MASS
CCNCFl1TMTICN 121 NA56
Y
METALS. CYANIDE. AND TOTAL PHENOLS
1 M. MMmy. Tap1
�/
x
(1a1(-Ilia)
W. Ani Trial
X
<0. 01
0
1
al
lbb
Da10-a62)
IM. BaryYue, Trial
x
aM. Cadmium, TOW
x
SM. CNmnlum,
X
<.05
0
1
al
lb9
'blMN (1OiT-01
M. Copper Tonal
x
M. Les, Tot
x
pN4p2-1)
We. Mami TOW
�/
x
put&9T-0)
9M. New, Tat
x
(1aa11-02-0)
tOM. Belensm,
v
(TI-aF2)
Tole N
11 M. Silver, TOW
X
<0.005
0
1
mg/L
lbs
(1a102.)
12M. ThalWm.
TOW (14403Ba)
12M. 21nc. Tot
(1a10-06B)
x
Iasi. Cyandse.
�/
T" (57-124)
x
s6M. t..
�/
Total
x
DIOXIN
22,T.&TWr
` /
DESCRIBE RESULTS
daeredbtres-,
Teen(116a-01-0)
/J(\
EPA Form 3510.2C (6-90) PAGE V-9 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK'X'
S. EFFLUENT
<. UNITS
S. INTAKE umm�
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
c. LONG TERM AVRG.
a. LONG TERM
AND
b
c
a. MAXIMUM DAILY VALUE
(Vmm)dleJ
VALUE Q/�rvuNab/eJ
AVERAGE VALUE
CAS NUMBER
TESTING BEUEVEO
BEUEVFD
b. NO. OF
a. COWEN-
b.NI.OF
OI
(p
(I)
III
((/mv�lv6le)
REOUIREO PFESENT
ABSENT
CGNcE", - (3I.S.
CONLENTMTION (31 M°Ss
CGNCENtRPTIGN (II MA95
AF YSES
TRATl( b. MA55
CONCENTRATION (2) MA35
YBEB
GOIMS FRACTION- VOOIATILE COMPOUNDS
p10T�v2
X
<. 005
0
1
mg/L
lbs
)
37 °la
x
<-05
0
1
mg/L
lbs
po2-154-13-1)
)
/�
3V, kn 1)
(714
v
^
<.002
0
1
II
lbs
u
IM1er
0
1
mg/L
lbs
(542O
(saeo-tl
W. Bro
N 211-2) °
X
<. 002
0
1
mg/L
lbs
Bv. c.rom
v
Teo-afAbtlEe
/�
c. p02
0
1
BK]/L
lbs
Is&3}51
o. obalMma
x
c.002
0
1
mg/L
lbs
(
SV. CM1I"roR
broaameMpne
X
<.002
0
1
Bg/L
lb.
13H8-1
X
<. 002
0
1
mg/L
lbs
1
5V.2LNom
IM1MM"9I EIM1r
X
<.005
0
1
mg/L
lbs
no-rsa)
.IV. cmwo m
(67- )
v
^
<. 002
0
1
mg/L
lbs
12V. MOWb
N0"1p1"°NenO
<.002
0
1
mg/L
lbs
(T}]TJ)
13v.G r
dMwomegana
<.002
0
1
1Ig/L
lbs
(T5-it-ll)
11V.1]-DJOb
0
1
mg/L
lbs
em°ne 7s 1° s)
<.002
ISV.1RdICMom-
<.002
0
1
ag/L
lb.
etlI—(107 a2)
1Sv.1 I-DI.W.-
<. 002
0
1
mg/L
lbs
°m0°n°(753B )
Irv. Ia01°M1bra
<. 002
0
1
mg/L
lbs
propene(7M7-5)
ISVAL mmwo-
`,
wopyMne
X
<. 002
0
1
mg/L
lbs
(U2-7")
19V Emybevena
'.002
D
1
mg/L
=bs
U9wLq
M. Me9ry1
< 002
0
1
mg/L
_bs
&Omits O"F S)
211 Me ll
<. 002
0
1
mg/L
lbs
CMarM° (7"7.3)
EPA Form 851 (8 W) PAGE VA CONTINUE ON PAGE VS

2. MARK'X'
S. EFFLUENT
S. INTAKE (n umw)
1. POILIRANT
0. MAXIMUM 20 DAY Vr1LUE
C. LONG TERM AVRG.
a. LONG TERM
AND e.
.
P MAXMUM DAILV VALUE
(�/mmlydle)
VKUE rlmwla5k)
AVERAGE VALUE
AS NUMBER TESRNG EFIIEYEO
MUEVED
Q NO.OF
A CONCEIL
e. NO. OF
IFMRAi1W
IENfRATKKi
(i/m.,lo5/e) REOL9RF➢ PRESENT
ABSFNf
LONL 1]I MASS
CONCENTRATILX+ QI NA55
GCNCEj1N1RATCN QI Mr36
ANALYSES
IRATgN O. M/$5
CCNC 121MA55
YSE
GCMS FRACTION -VOLATILE COMF NOS k.w.uA
M. M.EAMR.
X
<. 002
0
1
mg/L
lb.
CMwI! 17"P21
2W 1.12.2-
TMnWabeNm.
X
<. 002
0
1
mg/L
lb.
P545
NV. ieb.d2mo-
�/
x
<. 002
0
1
mg/L
lb.
Mn5Nma 0z>-ts Nl
25V. TAum.
x
<. 002
0
1
Irg/L
lb.
(12 3)
2 ..12-T.
DkNmmrlgy
X
<.002
0
1
mg/L
lb.
t 56O0.5
1N.t]f-iNdipo-
X
0
1
mg/L
lb.
MNM (/1dN)
/�
c002
2N.1,1]-TXdiyo-
X
<. 002
0
1
mg/L
lb.
anm. (2w5d)
/�
T'OfO'
X
c.002
0
1
Rg/L
lb.
MM1„.m110.01d)
DW. TlkMoro-
Nnrbmenm.
X
<.002
0
1
mg/L
lbs
TsSw
-IV WOCN
x
c.002
0
1
mg/L
ibs
wtd)
NCMS FRACTK)N-ACID COMPOUNDS
.A.2-CNwaplw
x
s54Td1
u:,N-0vlido-
X
M.M 1125d12)
M 2,.-0Im.N
X
Fnma1155-st-01
NANO G-
X
sm-
Crnd(SM-Sb )
SA. 2,4-Din4o-
�/
x
Fbm.1151-25-51
SA.z-N,4.p al
( M)
)A N-NibCpMml
v
DNw$_n
MPLtJ w
V
C'.W(5& n
WPmbWwo-
X
prima tndedl
15A. m ma
x
N 04i5�
t1A 2A.birlWwo-
Fnma(5wS2)
EPA FoI 25MM (8d0) PAGE V-5 CONTINUE ON REVERSE

CONTINUED FROM THE FRONT
2. MARK 'X'
3. EFFLUENT
<. UNITS
5. INTAKE (ppuano]I
1. POLLUTANT
b. MAXIMUM 30 DAY VALUE
[. LONG TERM AVRG.
a. LONG TERM
AND
p,
[
a. MAXIMUM DAILY VALUE
VfmxplWle)
VALUE N. ,r )
AVERAGE VALUE
CASNUMBER
TESTING BELIEVED
BEIlEVEO
O. NO. OF
a. CONCEN-
b. NO. OF
111
(D
p1
(1)
(jwaJWle)
REOl11RE0 PRESENT
A0.4EM
CONOEN"),ION I01MA55
CONMA' TICN (2MA55
CONCENTRATION IL MASS
ANALYSES
TRATION b.MA35
CONCENTRATION 121MA55
LYSE
GUMS FRACTION —BASErNEUTRAL COMPOUNDS
1B324) lMma
x
2B.A neph4Ue
xpb&es-01
2B. AAMenme
x(12a12-7)
e8.B .tl a
�/
(92-0]-5)
x
SB.Bmzp(u)
ANft
(5"e3)
6B.BB.mm(a)
x
Pxen.(xiI22)
/�
iB. 2.4Rerlxo-
aoormmerre
X
20&99-2)
Bmezp(19leh1-25
PepleneB.
F2)
x
/�
9B.Ben
%wam-
(2074 9)
)
10B.ae. Bie
Yna9ne
V
111-91-1) 1-11
11B.9c(:flJuro-
M1 E
x
)
fl.ft(2
/�
12B.Bu1S-
CMnreMo
x
Elver 102-0&f
I
138. &a /-
-PM1flate
(11l-81-0)
14B, aaromophmyl
Phenyl EMer
�/
x
(M-6S 3)
15S. Uto Benzyl
x
PhMYM (85-06i1
mo-
n.pNhC
ep
x
(SLs&7)
W
I TB.4CMao-
Elher
V
QWe 724)
00&i2J
/�
x
216D1-9)
21 (1-9)
/�
19B. Dirmro fah)
MMrecme
x
s}io-3
I�
20B. 1.2Udilwo-
1)
xbenzene(9&
21B. 1.SDW Z
�/
x
bm:me(5U-T}1)
EPA Folm 351&2C (&90) PAGE V6 CONTINUE ON PAGE V4

PAGE VE
2 MARN'%'
3. EFFLUENT
4. UNITS
5. INTAKE a �orv�0
1. PoLLUTANT
b. MAXIMUM 30 DAY VALUE
b. LONG TERM AVRG.
a. LONG TERM
AND b.
a
e. MAXIMUM DAILY VALUE
Urmelmle)
VALUE plwudoa/e)
AVERAGE VALUE
CAS NUMBER TEBTINO BE4EVEO
9EUEVEO
dND. OF
e. CONCEN-
b. NO. OF
p(
PI
(tl
(11
(fmvilMl<) REOUMEO PRESEM
PBSEM
CONCEMRATON Dx MASS
CONCENTRATION (2) MASS
CONCENTRATION (21 MISS
ANALYSES
TRATION b. MASS
CONCENTpAtlpry (21 µeSS
ANALYSE
GCWS FRACTION-SAS"el.) AL COMPOUNDS (.nnnneen
228. 1,4 -We
xbeneene(188-1&7)
23B. 3.3-0IMlloro-
bewElne(81-9N)
PhNW. (84E&2)
x
258. DmMyl
Phb-1.
(131-11-3)
no. DFN-awtA
�/
x
P„NWM(W- 2)
27& 2,4-Dnlbo-
WW.-Dx1-14 )
Zee. x.5-DrNa
bluene (80&30.2)
x
x88. o.N-0nNl
vhnmere 111724-01
x
/�
3UB.1.2-Gpheny4
„ytlleane (es Aeo-
x
Oen[enel (1228J-
/�
Fo)anmene
2o5d4-
206 -b)
X
I2B. Nuo(ene
8&]}])
33B. Hexaalxo-
—(I1.741)
xben
34B. Hez 01.o
bule6ene(87-8&3)
35B. Hezm„lom-
Mdma
]d)
(77474)
38B He"awb
e (87-72-1)
x
3]B.Intlano
(133m) PPene
(19}39b)
US. lse,horone
�/
x
(1&5&1)
39B. N,hNNene
bmeene
(
x9&9S3)N.
41B.NNNo-
eoarmemyl.mine
x
(52-,
/�
428N-NNaa6
NFroppemine
v
EPA Form 3510.2C (&90) PAGE V-7 CONTINUE ON REVERSE

2. MARK W
3. EFFLUENT
4. UNITS
5. INTAKE (opennap
1. POLLUTANT
b. MAXIMUM 30 DAV VALUE
c. LONG TERM AVRG.
8. LONO TERM
AND
p
c
e. MAXIMUM DNLY VALUE
(�/mmluble)
VALUE (i/mmlubk
AVERAGE VALUE
CAS NUMBER
IESTNG BE4EYEO
BEUEYEO
J.NO. OF
&CONGER
b. NO.OF
(1)
Ol
111
O)
(I/mwlu5le)
FEQIIIHEP PRESENT
PBSEN!
LpNLENTBRTION 12)MA55
CONCEi") TICK R)N/55
CONCENTRATION
0)Me"
ANALYBES
TRATION b. M115B
LIXJCENIPATILN (21MASS
YSEB
GCNS FRACTION —BASEiNEUTRAL COMPOUNDS (mntiwedl
4W WNNu
mina
W30-6)i
X
IB&]oE)
H8. Pb.—retie
(8501a)
X
85B. Pyrene
(129a 0)
X
BBB. 1.24T6
"'o—ne
X
(12 8 _J)
OCIMS FMGTION—PESTICIDES
1P.A
�/
(309-00.2)
x
2P. a-SHC
pl8 )
X
3P. Q-BHC
\�
(319aiT1
x
'P. y He
�/
(584")
x
SP. F
319a )
X
W. CSbkene
57-7")
X
,P...f-DOT
(W6 3)
X
SP. s,e-DDE
�/
(]2S&9)
x
9P. A#' -DOD
�/
(123 8)
x
1 OP. Die Idnn
(565]-1)
X
11P.u-Enttullen
(115-2R])
X
12P. 0-EnewWln
(11&2&])
X
13P. EnBwuben
B I,
X
p9v-ma7
14P. Entrin
x
15P.
Nceh,di,
X
(74219z
]Qt lNl
18P. HePlecM1br
X
8� eI
EPA Farm 3510.2C (&OD) PAGE VA CONTINUE ON PAGE V-9

EPA I.D. NUMBER (.npv./mm lnm l PfFmmp OUTFALLNUMBER
PAGEVA 110000349070 002
2. MARK
3. EFFLUENT
!. UNITS
6. INTAKE (oprlarWj
1. POLLUTANT
0, MAXIMUM 3D DAY VPLUE
c. LONG TERM AVRO.
a. LONG TERM
APID a
r.E.W.E
c
a. MAXIMUM ONLY VPLUE
(�/m-1w)
VALUE (If. mr)
AVERAGE VA UE
CAS NUMBER STING BELEVED
BEUEVED
O, NO, OF
a. CONCEK
E. NO. OF
O)
(1I
(1)
j11
(lf ovoi(Mlr) 0 %iESENi
AB6EM
CONCENTRATON Ol MA66
CONCENI" nON (21MASS
CONCENTRATON (2)MASS
A YSES
TRATION 1. MASS
CONCEN nON (21MA66
ALYSE
GC/MS FRACTION -PESTICIDES (-1--)
I2P.IIeplaMbr
tl
(10 2
10245i-3)
X
18P. PC61212
OU6?21-9)
19P. PCB-1
x
20P. PCB-1221
�/
(111 426 )
x
21P. MB-12M
(111Q-16d1
x
22P. PCB-120
�/
(126i2-29 )
x
23P. PC61260
�/
(1109662b)
/�
NP. PCB-1016
(l Mi411.2)
ISP. TPra00900
�/
ml2)
x
EPA F. 3610-2C (690) PAGE V-6

TAB F
TOPOGRAPHIC MAP
FORM I
SECTION XI

s ax, / \� • Kingston
N I ))) am
WRT
OUTFALL 001 TO BRUSHY CREEK
• p� ui,, ,h LATITUDE. 35 20'25"
1`I LONGITUDE: 81.36'58" •O� �J
i 1
KI
CAI .\q.
'; \
n
Washburn
WT
q], I.. , 1 'ffl I ? . . I ?v
i i 1 yn 4i
am
�'�-'r*• OUTFALL 002 TO OVERFLOW BRANCH
LATITUDE 35 19'27
LONGITUDE: 81'37'50'
rf----
\
-J
REFERENCE SCALE IN FEET
1. U.S.G.S. 7.5' TOPOGRAPHIC MAP, BOILING SPRINGS NORTH
AND SHELBY QUADRANGLE, NORTH CAROLINA DATED: 2002. 0 2000 4000
AW IAV � ELECTRIC GLASS FIBER AMERICA, LLC
940 WASHBURN SWITCH ROAD
Civil & Environmental Consultants, Inc. SHELBY, NORTH CAROLINA
1900 Center Park Drive - Sufte A - Charlotte, NC 28217
Ph: 980.237.0373 • Fax! 980.237.0372 SITE LOCATION MAP
w .cecinc.com
DRAWN BY: JKS I CHECKED BY: GPT APPROVED BY: - FIGURE NO.:
20 DATE: JANUARY 2018 DWG SCALE: 1" = 00 PROJECT NO: 122-243.015

TAB G
LABORATORY REPORTS

2aceAnalyficala
w+wpacelabs, WM
November 14, 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: Permit Renewal 001
Pace Project No.: 92361385
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Sarah Graham for
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 23

2A17alytical
~Owwabl=
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
HuntemAlle, NC 28078
[phone]
CERTIFICATIONS
Project: Permit Renewal 001
Pace Project No.: 92361385
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Flodda/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification #: 84
North Carolina Field Services Certification #: 5342
Virginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Flodda/NELAP Certification M E87648
Massachusetts Certification M M-NC030
North Carolina Drinking Water Certification #: 3TT12
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginialVELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
witlwut the written consent of Pace Analytical Services, LLC. Page 2 of 23

/ PaceAnaly ical a
SAMPLE ANALYTE COUNT
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project:
Pace Project No.:
Permit Renewal 001
923613B5
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92361385001
001
EPA200.7
DS, SH1
7
PASI-A
EPA 625
Bpi
5
PASI-C
EPA 624
GAW
35
PASI-C
EPA 300.0
CDC
1
PASI-A
SM 5220D
SLB
1
PASI-A
SM 5310B
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 23

aceAnaVical e
~..PXWabaown
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
Sample: 001
Lab ID: 92361385001
Collected: 11/01/1708:00
Received: 11/01/1709:00 Matrix: Water
Parameters
Results
Units
Report Limit
OF
Prepared
Analyzed
CAS No. Qual
200.7 MET ICP
Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Aluminum
NO
ug/L
100
1
11/07/17 01:15
11/1311714:49
7429-90-5
Arsenic
NO
ug/L
10.0
1
11/07/17 01:15
11/14/1701:26
7440-38-2
Boron
367
ug/L
50.0
1
11/07/17 01:15
11/13/17 14,49
7440-42-8
Chromium
NO
ug/L
5.0
1
11/07/17 01:15
11/13/1714:49
7440-47-3 P8
Iron
NO
ug/L
60.0
1
11/07/17 01:15
11/13/17 14:49
7439-89-6 PB
Magnesium
2380
ug/L
100
1
11/07/17 01:15
11/1311714:49
7439-95-4
Silver
NO
ug/L
5.0
1
11/07/17 01:15
11113/1714:49
7440-22-4
625 MSSV
Analytical Method: EPA 625
Preparation Method: EPA 625
Di-n-butylphthalate
NO
ug/L
5.0
1
11/07/17 10:06
11/0811723:43
84-74-2
bis(2-Ethylhexyl)phthalate
NO
ug/L
5.0
1
11/07/17 10:06
11/0811723:43
117-81-7
Surrogates
Nitrobenzene-d5 (S)
53
%
10-120
1
11/07/17 10:06
11/08/17 23:43
4165-60-0
2-Fluorobiphenyl(S)
49
%
15-120
1
11/07/17 10:06
11/08/17 23:43
321-60-8
Terphenyl-dl4(S)
58
%
11-131
1
11/07/17 10:06
11/0811723:43
1718-51-0
624 Volatile Organics
Analytical Method:
EPA 624
acrolein
NO
ug/L
5.0
1
11/03/17 02:27
107-02-8
4crylonitrile
NO
ug/L
50.0
1
11/03/1702:27
107-13-1
3enzene
NO
ug/L
2.0
1
11/03/17 02:27
71-43-2
Bromodichloromethane
NO
ug/L
2.0
1
11/03/17 02:27
75-27-4
Bromoform
NO
ug/L
2.0
1
11/03/17 02:27
75-25-2
Bromomethane
NO
ug/L
2.0
1
11/03/17 02:27
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
11/03/17 02:27
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
11/0311702:27
108-90-7
Chloroethane
NO
ug/L
2.0
1
11/03/17 02:27
75-00-3
2-Chloroethylvinyl ether
NO
ug/L
5.0
1
11/03/17 02:27
110-75-8 c2
Chloroform
NO
ug/L
2.0
1
11/03/17 02:27
67-66-3
Chloromethane
NO
ug/L
2.0
1
11/03/17 02:27
74-87-3
Dibromochloromethane
NO
ug/L
2.0
1
11/03/1702,27
124-48-1
Dichlorodi0uoromethane
NO
ug/L
2.0
1
11/03/17 02:27
75-71-8
1,1-Dichloroethane
NO
ug/L
2.0
1
11/03/17 02:27
75-34-3
1,2-Dichloroethane
NO
ug/L
2.0
1
11/03/17 02:27
107-06-2
1,1-Dichloroethene
NO
ug/L
2.0
1
11/03/17 02:27
75-35-4
cis-1,2-Dichlomethene
NO
ug/L
2.0
1
11/03/17 02:27
156-59-2
trans-1,2-Dichloroethane
NO
ug/L
2.0
1
11/03/17 02:27
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
11/03/17 02:27
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:27
10061-01-5
trans-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:27
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
11/03/17 02:27
100-41-4
Methylene Chloride
NO
ug/L
2.0
1
11/03/17 02:27
75-09-2
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1
11/03/17 02:27
79-34-5
Tetrachloroethene
NO
ug/L
2.0
1
11/03/17 02:27
127-18-4
Toluene
ND
ug/L
2.0
1
11/03/17 02:27
108-88-3
1, 1, 1 -Trichloroethane
ND
ug/L
2.0
1
1110311702:27
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
11/0311702:27
79-00-5
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 23

25ceAnalyfical'
.pace bs.m
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
Sample: 001
Lab ID: 92361385001 Collected: 11/01/1708:00
Received: 11/01/1709:00 Matrix: Water
Parameters
Results Units
Report Limit
OF
Prepared Analyzed
CAS No. Qual
624 Volatile Organics
Analytical Method: EPA 624
Trichloroethene
ND ug/L
2.0
1
11103/1702:27
79-01-6
Trichlomfluoromethane
NO ug/L
2.0
1
11/0311702:27
75-69-4
Vinyl chloride
NO ug/L
2.0
1
11/0311702:27
75-01-4
Surrogates
4-Bromofluorobenzene (S)
98 %
70-130
1
11/03/17 02:27
460-00-4
Toluene-d8(S)
104 %
70-130
1
11/03/17 02:27
2037-26-5
1,2-Dichloroethane-d4 (S)
103 %
70-130
1
11/03/17 02:27
17060-07-0
300.0 IC Anions 28 Days
Analytical Method: EPA 300.0
Sulfate
32.1 mg/L
1.0
1
11/06/17 17:48
14808-79-8
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L
25.0
1
11/13/1719:02
L2
5310E TOC
Analytical Method: SM 5310E
Total Organic Carbon
4.5 mg/L
1.0
1
11/02/17 19:15
7440-44-0
Date: 11/14/2017 05:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 5 of 23

PaceAnalytical
' aww.pewlabs.com
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385479 Analysis Method: EPA200.7
QC Batch Method: EPA 200.7 Analysis Description: 200.7 MET
Associated Lab Samples: 923613B5001
METHOD BLANK: 2137810
Matrix:
Water
Associated Lab Samples: 92361385001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed Qualifiers
Aluminum
ug/L
NO
100
11/1311716:30
Arsenic
ug/L
NO
10.0
11/1411701:20
Boron
ug/L
NO
50.0
11/13/1716:30
Chromium
ug/L
200
5.0
11/13/1714:34
Iron
ug/L
188
50.0
11/13/1714:34
Magnesium
ug/L
NO
100
11/13/1716:30
Silver
ug/L
NO
5.0
11/13/1716:30
Pace Analytical Services, LLC
9800 Kincey Ave. Suke 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2137811
-
Spike
LCS
LCS
% Rae
Parameter
Units
Cone.
Result
%Rec
Limits Qualifiers
Aluminum
ug/L
5000
4640
93
85-115
Arsenic
ug/L
500
467
93
85-115
Boron
ug/L
500
456
91
85-115
Chromium
ug/L
500
446
89
85-115
Iron
ug/L
5000
4460
89
85-115
Magnesium
ug/L
5000
4470
89
85-115
Silver
ug/L
250
229
91
85-115
MATRIX SPIKE R MATRIX SPIKE
Parameter
DUPLICATE: 2137812
MS
92361368001 Spike
Units Result Cone.
MSD
Spike
Conc.
2137813
MS
Result
MSD
Result
MS
% Rae
MSD
% Rae
% Rae
Limits
RPD Qual
Aluminum
ug/L
NO
5000
5000
4760
4750
94
94
70-130
0
Arsenic
ug/L
NO
500
500
478
478
96
96
70-130
0
Boron
ug/L
0.090
500
500
557
560
93
94
70-130
1
mg/L
Chromium
ug/L
NO
500
500
444
442
88
88
70-130
1
Iron
ug/L
0.23
5000
5000
3450
3450
64
64
70-130
0 M1
mg/L
Magnesium
ug/L
1.6
5000
5000
6070
6090
90
90
70-130
0
mg/L
Silver
ug/L
NO
250
250
232
232
93
93
70-130
0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 6 of 23

/ .Pace Analytical e
wew-0soeYos.mm
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137814
2137815
MS
MSD
92361488001 Spike
Spike
MS
MSD MS
MSD % Rec
Parameter Units Result Conc.
Conc.
Result
Result % Rec
% Rec Limits RPD Qual
Aluminum ug/L
4650
4660
0
Arsenic ug/L
468
469
0
Boron ug/L
485
483
0
Chromium ug/L
626
625
0
Iron ug/L
4430
4490
1
Magnesium ug/L
4710
4750
1
Silver ug/L
229
229
0
Results presented on this page are in the units Indicated by the -Units- column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not 5e reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 7 of 23

/ !PaceMaVical
evmPli Mab+.wrm
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Hunlersville, NC 28078
[phone]
QC Batch: 385093
Analysis
Method:
EPA624
QC Batch Method: EPA624
Analysis
Description:
624 MSV
Associated Lab Samples: 92361385001
METHOD BLANK: 2134818
Associated Lab Samples: 92361385001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,12,2-Tetrachloroethane
ug/L
NO
2.0
11/02/17 17:58
1,1,2-Trichloroethane
ug/L
ND
2.0
11/02/17 17:58
1,1-Dichloroethane
ug/L
ND
2.0
11/02/17 17:58
1,1-Dichloroethene
ug/L
ND
2.0
11/02/17 17:58
1,2-Dichlorcethane
ug/L
NO
2.0
11/0211717:58
1,2-Dichloropropane
ug/L
NO
2.0
11/02/17 17:58
2-Chloroethylvinyl ether
ug/L
NO
5.0
11/02/17 17:58
Acrolein
ug/L
NO
5.0
11/02/17 17:58
Acrylonitrile
ug/L
NO
50.0
11/02/17 17:58
Benzene
ug/L
NO
2.0
11/02/17 17:58
Bromodichloromethane
ug/L
NO
2.0
11/02/17 17:58
Bromoform
ug/L
NO
2.0
11/02/17 17:58
Bromomethane
ug/L
NO
2.0
11/02/17 17:58
Carbon tetrachloride
ug/L
NO
2.0
11/02/17 17:58
Chlorobenzene
ug/L
NO
2.0
11/02/17 17:58
Chloroethane
ug/L
NO
2.0
11/02/17 17:58
Chloroform
ug/L
NO
2.0
11/02/17 17:58
Chloromethane
ug/L
NO
2.0
11/02/17 17:58
cis-1,2-Dichloroethene
ug/L
NO
2.0
11/02/17 17:58
cis-1,3-Dichloropropene
ug/L
NO
2.0
11102/1717:58
Dibromochloromethane
ug/L
NO
2.0
11/02/17 17:58
Dichlorodifluoromethane
ug/L
NO
2.0
11/02/17 17:58
Ethylbenzene
ug/L
NO
2.0
11/02/17 17:58
Methylene Chloride
ug/L
ND
2.0
11/02/17 17:58
Tetrachloroethene
ug/L
NO
2.0
11/02/17 17:58
Toluene
ug/L
NO
2.0
11/02/17 17:58
trans-1,2-Dichloroethene
ug/L
NO
2.0
1110211717:58
trans-1,3-Dichloropropene
ug/L
NO
2.0
11/0211717:58
Trichloroethene
ug/L
NO
2.0
11/02/17 17:58
Trichlorofluoromethane
ug/L
NO
2.0
11/02/17 17:58
Vinyl chloride
ug/L
NO
2.0
11/02/17 17:58
1,2-Dichloroethane-d4 (S)
%
97
70-130
11/02/17 17:58
4-Bromofluorobenzene (S)
%
100
70-130
11/02/17 17:58
Toluene-d6(S)
%
104
70-130
11/02/17 17:58
Qualifiers
LABORATORY CONTROL SAMPLE: 2134819
Spike LCS LCS % Rec
Parameter Units Conc. Result e/ Rec Limits Qualifiers
1,1,1-Trichloroethane ug/L 20 18.2 91 52-162
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 8 of 23

/ 2ceAnalytical
•rwPOCO lWa.=
QUALITY CONTROL DATA
Pace Analytical services, LLC
9800 Kincey Ave. Surte 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
LABORATORY CONTROL SAMPLE:
2134819
Spike
1-CS
LCS
% Rec
Parameter
Units
Conc.
Result
%Rec
Limits
Qualifiers
1,1,2,2-Tetrachloroethane
ug/L
20
17.1
86
46-157
1,12-Trichloroethane
ug/L
20
18.6
93
52-150
1,1-Dichloroethane
ug/L
20
17.5
87
59-155
1,1-Dichloroethene
ug/L
20
19.2
96
1-234
1,2-Dichloroethane
ug/L
20
18.2
91
49-155
1,2-Dichloropropane
ug/L
20
19.3
97
1-210
2-Chloraethylvinyl ether
ug/L
40
29.8
75
1-305
Acrolein
ug/L
100
130
130
15-152
Acrylonibile
ug/L
100
89.0
89
75-132
Benzene
ug/L
20
18.5
93
37-151
Bromodichloromethane
ug/L
20
18.4
92
35-155
Bromoform
ug/L
20
16.3
81
45-169
Bromomethane
ug/L
20
20.1
100
1-242
Carbon tetrachloride
ug/L
20
18.5
93
70-140
Chlorobenzene
ug/L
20
18.1
91
37-160
Chloroethane
ug/L
20
18.9
94
14-230
Chloroform
ug/L
20
17.8
89
51-138
Chloromethane
ug/L
20
17.3
87
1-273
cis-1,2-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
19.2
96
1-227
Dibromochloromethane
ug/L
20
16.8
84
63-149
Dichlorodifluoromethane
ug/L
20
16.2
81
70-130
Ethylbenzene
ug/L
20
17.5
88
37-162
Methylene Chloride
ug/L
20
21.6
108
1-221
Tetrachlormthene
ug/L
20
18.8
94
64-148
Toluene
ug/L
20
18.5
92
47-150
trans-1,2-Dichloroethene
ug/L
20
18.3
92
54-156
trans-1,3-Dichloropropene
ug/L
20
18.9
94
17-183
Trichloroethene
ug/L
20
19.6
98
71-157
Trichlorofluoromethane
ug/L
20
17.9
90
17-181
Vinyl chloride
ug/L
20
18.2
91
1-251
1,2-Dichloroethane-d4 (S)
%
103
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
104
70-130
MATRIX SPIKE SAMPLE:
2134821
92361205001
Spike
MS
MS
k Rec
Parameter
Units
Result
Conc.
Result
Y Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
20
20.9
105
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
18.2
91
73-159
1,1,2-Trichloroethane
ug/L
NO
20
20.0
100
64-152
1,1-Dichloroethane
ug/L
ND
20
20.1
100
43-172
1,1-Dichloroethene
ug/L
ND
20
22.1
111
48-189
1,2-Dichloroelhane
ug/L
NO
20
20.4
102
42.171
1,2-Dichloropropane
ug/L
ND
20
21.6
108
55-157
Results presented on this Page art In 0e unite Indicated by the -Units" column except where an alternate unit Is presented to the right or the result
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, L-C. Page 9 of 23

2aceAnalyticalo
wwwpscelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Project: Permit Renewal 001
Pace Project No.: 92361385
MATRIX SPIKE SAMPLE: 2134821
92361205001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Chloroethylvinyl ether
ug/L
ND
40
ND
0
70-130 M1,c2
Acrolein
ug/L
ND
100
138
138
70-130 M1
Acrylonitrile
ug/L
ND
100
101
101
70-130
Benzene
ug/L
ND
20
20.3
101
54-163
Bromodichloromethane
ug/L
ND
20
19.8
99
56-152
Bromoform
ug/L
ND
20
17.1
85
53-151
Bromomethane
ug/L
ND
20
16.8
84
10-200
Carbon tetrachloride
ug/L
ND
20
20.1
101
41-175
Chlorobenzene
ug/L
ND
20
20.7
103
67-152
Chloroethane
ug/L
ND
20
22.8
114
23-200
Chloroform
ug/L
ND
20
18.4
92
51-166
Chloromethane
ug/L
ND
20
17.0
85
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
21.2
106
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
19.9
100
38-146
Dibromochloromethane
ug/L
ND
20
18.8
94
65-144
Dichlorodifluoromethane
ug/L
ND
20
18.5
92
70-130
Ethylbenzene
ug/L
ND
20
19.8
99
57-152
Methylene Chloride
ug/L
ND
20
20.0
100
40-167
Tetrachloroethene
ug/L
ND
20
21.0
105
59-155
Toluene
ug/L
ND
20
20.6
103
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
21.1
106
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
19.4
97
39-148
Trichloroethene
ug/L
ND
20
21.7
109
60-153
Trichlorofluoromethane
ug/L
ND
20
21.3
107
42-199
Vinyl chloride
ug/L
ND
20
21.2
106
46-176
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8(S)
%
96
70-130
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichlorcethane
ug/L
ND
ND
1, 1,2,2-Tetrachloroethane
ug/L
ND
ND
1,1,2-Tdchloroethane
ug/L
ND
ND
1,1-Diohloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
2-Chloroethylvinyl ether
ug/L
ND
ND
Acrolein
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 10 of 23

/ ZacAnaVical e
snw.peMaE+.arn
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
uglL
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
102
4-Bromofluorobenzene(S)
%
100
97
Toluene-d8(S)
%
106
102
RPD Qualifiers
2
3
4
Pace Analytical Services, LLC
9800 Kincey Ave. SuHe 100
Huntersville, NC 28078
[phone]
Results presented on this page are in the units Indicated by the "Units" column eliCept where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 23

25ceAnalytical*
rnn Aweleba.corn
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385556
QC Batch Method: EPA 625
Associated Lab Samples: 92361385001
Analysis Method:
Analysis Description:
EPA 625
625 MSS
METHOD BLANK: 2138167
Matrix: Water
Associated Lab Samples: 92361385001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
bis(2-Ethylhexyl)phthalate
ug/L
ND
5.0
11/08/17 11:48
Di-n-butylphthalate
ug/L
ND
5.0
11/08/17 11:48
2,4,6-Tdbromophenol(S)
%
88
10-137
11/08/17 11:48
2-Fluorobiphenyl(S)
%
73
15-120
11/08/17 11:48
2-Fluorophenol(S)
%
38
10-120
11/08/17 11:48
Nitrobenzene-d5(S)
%
81
10-120
11/08/17 11:48
Phenol-d6 (S)
%
25
10-120
11/08/17 11:48
Terphenyl-dl4 (S)
%
74
11-131
11/08/17 11:48
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
2138168
Spike LCS LCS
% Rae
Parameter
Units
Cone. Result % Rae
Limits Qualifiers
bis(2-Ethylhexyl)phthalate
ug/L
50 41.6 83
8-158
Di-n-butylphthalate
ug/L
50 40.9 82
1-118
2,4,6-Tfibromophenol (S)
%
91
10-137
2-Fluorobiphenyl(S)
%
74
15-120
2-Fluorophenol(S)
%
39
10-120
Nitrobenzened5 (S)
%
78
10-120
Phenol-d6 (S)
%
29
10-120
Terphenyl-d14 (S)
%
70
11-131
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2138169
MS
Parameter
bis(2-Ethylhexyl)phthalate
Di-n-butylphthalate
2,4,6-Tdbromophenol (S)
2-Fluorobiphenyl(S)
2-Fluorophenol (S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyldl4 (S)
92361660001
Spike
Units Result
Cone.
ug/L ND
100
ug/L ND
100
o�
o�
2138170
MSD
Spike
MS
MSD
MS
MSD
% Rae
Cone.
Result
Result
% Rec
% Rae
Limits RPD
100
88.1
85.2
88
85
8-158 3
100
87.7
83.4
88
83
1-118 5
100
98
10-137
73
77
15-120
53
52
10-120
80
81
10-120
45
43
10-120
46
39
11-131
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, L-C.
Qual
Page 12 of 23

PaceAnalytical e
wwwpacelebs.avn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 385402
Analysis Method: EPA 300.0
QC Batch Method: EPA 300.0
Analysis Description: 300.0 IC Anions
Associated Lab Samples: 92361385001 -
METHOD BLANK: 2136998
Matrix: Water
Associated Lab Samples: 92361385001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Sulfate mg/L
NO 1.0
11/06/1713:48
LABORATORY CONTROL SAMPLE: 2136999
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits
Qualifiers
Sulfate mg/L
50
49.7
99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137000
2137001
MS
MSD
92361863002
Spike
Spike MS
MSD MS
MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result e/ Rec
% Rec
Limits
RPD Qual
Sulfate mg/L ND
50
50 52.4
52.9 104
105
90-110
1
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137002
2137003
MS
MSD
92361823001
Spike
Spike MS
MSD MS
MSD
%Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec
% Rec
Limits
RPD Qual
Sulfate mg/L NO
50
50 53.0
53.1 106
106
90-110
0
Results present" on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 23

i 2ace Analyticala
.pacelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 386547
Analysis Method: SM
52200
QC Batch Method: SM 5220D
Analysis Description: 5220D COD
Associated Lab Samples: 92361385001
METHOD BLANK: 2143913
Matrix: Water
Associated Lab Samples: 92361385001
Blank
Reporting
Parameter Units
Result
Limit
Analyzed Qualifiers
Chemical Oxygen Demand mg/L
NO 25.0
11/13/17 19:02
LABORATORY CONTROL SAMPLE: 2143914
Spike
LCS
LCS % Rec
Parameter Units
Conc.
Result
% Rec Limits Qualifiers
Chemical Oxygen Demand mg/L
1120
751
67 90-110 L2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143915
2143916
MS
MSD
92360409001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter Units Result
Conc.
Conc. Result
Result % Rec % Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 803
150
150 900
907 65 69
90-110
1 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143917
2143918
MS
MSD
92361431002
Spike
Spike MS
MSD MS MSO
%Rec
Parameter Units Result
Conc.
Conc. Result
Result %Rec %Rec
Limits
RPD Qual
Chemical Oxygen Demand mg/L 27.0
150
150 145
141 79 76
90-110
3 MO
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC.
Page 14 of 23

aceAnalytical a
www.pacelabs.con,
QUALITY CONTROL DATA
Project: Permit Renewal 001
Pace Project No.: 92361385
QC Batch: 384971 Analysis Method: SM 5310B
QC Batch Method: SM 5310B Analysis Description: 5310E TOC
Associated Lab Samples: 92361385001 -
METHOD BLANK: 2133960
Associated Lab Samples: 92361385001
Parameter Units
Total Organic Carbon mg/L
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifters
NO 1.0 11/02/1716:28
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2133961
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Total Organic Carbon mg/L 25 23.6 94 90-110
MATRIX SPIKE 8 MATRIX SPIKE DUPLICATE: 2133962 2133963
MS MSD
92361364001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conic. Conc. Result Result %Rec %Rec Limits RPD Qual
Total Organic Carbon mg/L 9.5 25 25 32.4 32.3 91 91 90-110 0
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
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Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, U.C.
Page 15 of 23

25ceAnalyticala
auwpacela0s.cwn
QUALIFIERS
Project: Permit Renewal 001
Pace Project No.: 92361385
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
Aseparate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analyzes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PAST-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
P8 Analyte was detected in the method blank. All associated samples had concentrations of at least ten times greater than
the blank or were below the reporting limit.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/14/2017 05:29 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 23

2aceAnalyfical'
wuwcacelabs.com
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project: Permit Renewal 001
Pace Project No.: 92361385
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92361385001
001
EPA 200.7
385479
EPA 200.7
385555
92361385001
001
EPA 625
385556
EPA625
385759
92361385001
001
EPA 624
385093
92361385001
001
EPA 300.0
385402
92361385001
001
SM 5220D
386547
92361385001
001
SM 53108
384971
Date: 11/14/2017 05:29 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 23

Document Name: Document Revised August 4, 2017
Sample Condition Upon Recei t(SCUR) ! Page 1 of 2
Document No.: Issuing Authority:
[ CBMBIj/lICBj
F-CAR-CS-033-Rev.04 Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑ Huntersville ❑l Ralelgh❑ Mechanicsville'
Client Name: py,- �_ projectit:I WO# 92361385
Greenwood
�bt, aF riMJllq
Courier: Fed Ex ❑UPS CUSPS ❑Client II
❑ Commercial [Pace ❑Other:'ll'IIIIIII'I1III'll
_ 91111 115
Custody Seal Present?
[]Yes aNcz
Seals Intact? []Yes LAND
�
DiPersian Examining Contems:,l/��
�44—
Packing Material:
❑Bubble Wrap
[Bubble Bags [—]None/ ❑ Other
Biological Tissue Fr zen?
Thermomet
IR Gun ID:
'� I R U I
wet ❑Blue
❑None ❑yes ❑No N/A
Ty 1 I[e:
Correction Factor:
Cooler Temp Corrected ('C):
Temp should be above freezing to 6Y
[]samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Sell (Q N/A, water sample)
Did samples on 1 afe in a quarantine zone within
the United States CA, NY, or SC (check maps)?
Did samples originate from a foreign source linternatlon illy,
mypc 11Nn
nalutlirw Hawa,i and Puerto atml? I,Yes MO
Comments/Discrepancy:
Chain or Custody Present?
es
ONO
N/A
s.
Samples Arrived within Hold Time?
Yes
No
N/A
2.
Short Hold Time Analysis 1e72 hr.)?
Elves
N
N/A
3
Rush Turn Around Time Requested?JYes
No
N/A
4.
Sufficient Volume?
eY
ONO
❑N/A
5
Correct Containers Used?
-Pace Containers Used?
i
Yes
ONO
No
❑N/A
N/A
6.
Containers Intact?
Yes
01.
N/A
7.
Dissolved analysis: Samples Field filtered)
Dyes
ONO
N/A
9.
Sample Labels Match COC?
Includes Date/Time/IO(Anal sis Matrix:
es
I
No
[]NO
❑N/A
9.
Heads ace in VOA Vials (a5 6mmi?
Yes
N
N/A
10,
Trip Blank Present?
Trip Blank Custody Seals Presenl2
❑Yes
Yes
o
No
❑N/
N/A
11.
CLIENT N076ICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of splitcontainers'
Project Manager SCURF Review:
Project Manager SRF Review:
Field Data Required? ❑Yes ❑No
Date/Time:
Date:
Date:
Note: Whenever there is a discrepancy affecting North Carolina compliance UMPles, A Copy of this form will oe sent to the North Carolina DENNR Certification Office fie
0u1 of hold, mccriect preservative, out of temp, incorrect containers)
Page 18 of 23

/,Pace Analytical
'Check mark top half of box if pH and/or dechlorination
Is verified and within the acceptance range for
preservation samples.
.*Bottom half of box is to list number of bottles
Name,
Document Revised August 0,
P.Receipt)SCUR)
Page 2 of 2
t No.
Issuing Authority.
t ReY.04
Parr n,uln„nffi—
Project p WO# : 92361385
PM: AMB Due Date: 11/15/17
CLIENT: 92—PPG
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pH Adjustment Log for Preserved Samples
Sample ID
Type of Preservative
pH upon receipt
Dote preservation adjusted
Time presveata.
adjusted
Amount of Preservative
added
Lot a
Page 19 of 23

PaceAnalytical
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CHAIN -OF -CUSTODY I Analytical Request Document
Tire Chain-of-Cuslocy Is a LEGAL DOCUMENT. All relevanl bobs mus; Iw mmplMod accurately
Section A Section B Section C P.O.: / of / m
RlWIroO Cirenl lnlarma4M Required Pr,gocl rnl"mrawn. d
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ADDITIONAL COMMENTS
REL.RIOUISHED BY IAFFILUITION
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TIME
ACCEPTED BY; AFFILIATION
DATE
TIME
SAMPLE CONDITIONS
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SAMPLER NAME AND SIGNATURE
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Analytical Results
Pace Analytical
9800 Kincey Suite 100
Huntersville, NC 28078
Receive Date: 11/02/2017
Reported: 11108/2017
For: 92361385
Comments:
Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst
171102-17-01 MBAS
Respectfully submitted,
'`r ,') io
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA #NC00909
001 <0.1 mg/L SM5s OC 2000 11/03/2017 MD
PO Box 228 • Statesville, NC 28687 • 704/872/g4697
Page 1 gage 21 V 23

Condition of Receipt
Sample Number 171102-17-01 Temp on Arrival: 3
Parameter Schedule: MBAS
Received on Ice
PO Box 228 • Statesville, NC 28687 • 704/872/4697
Page 2 gage 22 of 23

Chain of Custody
Workorder 92361385 Workorder Name- Permit Renewal 001
MaeA r1rholls To
Angela 8arom
Pace Analytical Charlotte
9800 Kmcev Ave S.-le 100
Hintemwille. INC MQ79
Phone [phone]
E,na.1 angela baion�,Ppacelabs con,
Slaty of Sample Or�gln INC
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aceAnalytical
. pacelabs corn
November 15, 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: Permit Renewal 002
Pace Project No.: 92361389
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 01, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
tea. m-
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
41 without the written consent of Pace Analytical Services, LLC.
Page 1 of 20

2eAnalytical'
ws ps bs.oan
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
CERTIFICATIONS
Project: Permit Renewal 002
Pace Project No.: 92361389
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
South Carolina Certification #: 99006001
Louisiana/NELAP Certification # LA170028
Flodda/NELAP Certification #: E87627
North Carolina Drinking Water Certification #: 37706
Kentucky UST Certification M 84
North Carolina Field Services Certification #: 5342
VirginiaNELAP Certification #: 460221
North Carolina Wastewater Certification #: 12
Asheville Certification IDs
2225 Riverside Drive, Asheville, NC 28804
Flodda/NELAP Certification M E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
North Carolina Wastewater Certification #: 40
South Carolina Certification #: 99030001
VirginiaNELAP CeNfication #: 460222
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 2 of 20

Pace Analytical Services, LLC
a 9800 Kinsey Ave. Suite 100
;ace Analytical Huntersville, NC 28078
~pmalads.cm [phone]
SAMPLE ANALYTE COUNT
Project:
Pace Project No.:
Permit Renewal 002
92361389
Analytes
Lab ID
Sample ID
Method
Analysts
Reported
Laboratory
92361389001
002
EPA 200.7
SH1
7
PASI-A
EPA624
GAW
35
PASI-C
SM 2540D
SLB
1
PASI-A
SM 521013
KMM
1
PASI-A
EPA 350.1 1993 Rev 2.0
BRJ
1
PASI-A
SM 5220D
SLB
1
PASI-A
SM 5310B
KDF1
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC. Page 3 of 20

' PaceAnalytical
~pacelabs.c
ANALYTICAL RESULTS
Project: Permit Renewal 002
Pace Project No.: 92361389
Pace Analytical services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: 002 Lab ID: 92361389001 Collected: 11/0111707:55 Received: 11/01/1709:00 Matrix: Water
Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual
200.7 MET ICP Analytical Method: EPA 200.7 Preparation Method: EPA 200.7
Aluminum
ND
ug/L
100
1
11/14/17 12:35
11/15/17 12:26
7429-90-5
Arsenic
ND
ug/L
10.0
1
11/14/17 12:35
11/15/17 12:26
7440-38-2
Boron
33700
ug/L
500
10
11/14/17 12:35
11/15/17 14:10
7440-42-8 M6
Chromium
ND
ug/L
5.0
1
11/14/17 12:35
11/15/17 12:26
7440-47-3
Iron
1370
ug/L
50.0
1
11/14/17 12:35
11/15/17 12:26
7439-89-6
Magnesium
6680
ug/L
100
1
11/14/17 12:35
11/15/17 12:26
7439-95-4
Silver
ND
ug/L
5.0
1
11/14/17 12:35
11/15/17 12:26
7440-22-4
624 Volatile Organics Analytical Method: EPA 624
Acrolein
ND
ug/L
5.0
1
11/03/17 02:45
107-02-8
Acrylonitdle
ND
ug/L
50.0
1
11/03/17 02:45
107-13-1
Benzene
NO
ug/L
2.0
1
11/03/17 02:45
71-43-2
Bromodichloromethane
ND
ug/L
2.0
1
11/03/17 02:45
75-27-4
Bromoform
NO
ug/L
2.0
1
11/03/17 02:45
75-25-2
Bromomethane
ND
ug/L
2.0
1
11/03/17 02:45
74-83-9
Carbon tetrachloride
NO
ug/L
2.0
1
11/03/17 02:45
56-23-5
Chlorobenzene
NO
ug/L
2.0
1
11/0311702:45
108-90-7
;hloroethane
NO
ug/L
2.0
1
11/03/17 02:46
75-00-3
2-Chloroethylvinyl ether
ND
ug/L
5.0
1
11/03/1702A5
110-75-8 c2
;hloroform
ND
ug/L
2.0
1
11/03/17 02:45
67-66-3
Chloromethane
ND
ug/L
2.0
1
11/0311702:45
74-87-3
Dibromochloromethane
ND
ug/L
2.0
1
11103/1702:45
124-48-1
Dichlorodifluoromethane
ND
ug/L
2.0
1
11/03/17 02:45
75-71-8
1,1-Dichloroethane
ND
ug/L
2.0
1
11/03/17 02:45
75-34-3
1,2-Dichlorcethane
ND
ug/L
2.0
1
11/03/17 02:45
107-06-2
1,1-Dichloroethene
ND
ug/L
2.0
1
11/03/17 02:45
75-35-4
cis-1,2-Dichloroethene
ND
ug/L
2.0
1
11/03/17 02:45
156-59-2
trans-1,2-Dichloroethene
ND
ug/L
2.0
1
11/03/17 02:45
156-60-5
1,2-Dichloropropane
NO
ug/L
2.0
1
11/03/17 02:45
78-87-5
cis-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:45
10061-01-5
Vans-1,3-Dichloropropene
NO
ug/L
2.0
1
11/03/17 02:45
10061-02-6
Ethylbenzene
NO
ug/L
2.0
1
11/03/17 02:45
100-41-4
Methylene Chloride
ND
ug/L
2.0
1
11/03/17 02:45
75-09-2
1,1,2,2-Tetrachloroethane
NO
ug/L
2.0
1
11/03/17 02:45
79-34-5
Tetrachloroethene
ND
ug/L
2.0
1
11/03/17 02:45
127-18-4
Toluene
NO
ug/L
2.0
1
11/03/17 02:45
108-88-3
1,1,1-Trichloroethane
ND
ug/L
2.0
1
11/03/17 02:45
71-55-6
1,1,2-Trichloroethane
ND
ug/L
2.0
1
11/03/17 02:45
79-00-5
Trichloroethene
NO
ug/L
2.0
1
11/0311702:45
79411-6
Trichlorofluoromethane
ND
ug/L
2.0
1
11/03/17 02:45
75-69-4
Vinyl chloride
ND
ug/L
2.0
1
11/03/17 02:45
75-01-4
Surrogates
4-Bromofluorobenzene (S)
94
%
70-130
1
11/03/17 02:45
460-00-4
Toluene-d8(S)
101
%
70-130
1
11/03/17 02:45
2037-26-5
1,2-Dichlorcethane-d4 (S)
101
%
70-130
1
11/03/17 02:45
17060-07-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 4 of 20

PaceAnalytical
w Pacelabs.com
ANALYTICAL RESULTS
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
Sample: 002
Lab ID: 92361389001 Collected: 11/0111707:55
Received: 11/01/1709:00 Matdx:Water
Parameters
Results Units
Report Limit
DF
Prepared Analyzed CAS No. Qual
2540D Total Suspended Solids
Analytical Method: SM 2540D
Total Suspended Solids
NO mg/L
2.5
1
11/02/17 08:29
5210E BOD, 5 day
Analytical Method: SM 5210B
BOD, 5day
NO mg/L
2.0
1
11/02/1702:41 11/06/1721:19 B2,1-2
350.1 Ammonia
Analytical Method: EPA 350.1 1993
Rev 2.0
Nitrogen, Ammonia
0.27 mg/L
0.10
1
11/09/1701:16 7664-41-7
5220D COD
Analytical Method: SM 5220D
Chemical Oxygen Demand
NO mg/L
25.0
1
11/13/1719:02 L2
5310B TOC
Analytical Method: SM 5310B
Total Organic Carbon
2.1 mg/L
1.0
1
11/02/17 19:25 7440-44-0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, U.C. Page 5 of 20

/ ZeAnayical'
wray-0BEMBbCpan
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 386674
Analysis Method: EPA 200.7
QC Batch Method: EPA 200.7
Analysis Description: 200.7 MET
Associated Lab Samples: 92361389001
METHOD BLANK: 2144442
Matrix: Water
Associated Lab Samples: 92361389001
Blank
Reporting
Parameter
Units
Result
Limit
Analyzed
Qualifiers
Aluminum
ug/L
ND 100
11/15/17 12:20
Arsenic
ug/L
NO 10.0
11/15/1712:20
Boron
ug/L
NO 50.0
11/15/17 14:04
Chromium
ug/L
NO 5.0
11/1511712:20
Iron
ug/L
NO 50.0
11/15/1712:20
Magnesium
ug/L
NO 100
11/15/17 12:20
Silver
ug/L
NO 5.0
11/15/17 12:20
LABORATORY CONTROL SAMPLE:
2144443
Spike
LCS
LCS % Rec
Parameter
Units
Conc.
Result
% Rec Limits Qualifiers
Aluminum
ug/L
5000
4830
97
85-115
Arsenic
ug/L
500
485
97
85-115
Boron
ug/L
500
486
97
85-115
Chromium
ug/L
500
480
96
115-115
Iron
ug/L
5000
4750
95
85-115
Magnesium
ug/L
5000
4790
96
85-115
Silver
ug/L
250
245
98
85-115
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2144444
2144445
MS
MSD
92361389001
Spike
Spike MS
MSD MS MSD
% Rec
Parameter
Units
Result
Conc.
Conc. Result
Result %Rec %Rec
Limits
RPD Qual
Aluminum
ug/L
NO
5000
5000 4920
4970
98 99
70-130
1
Arsenic
ug/L
NO
500
500 493
492
99 98
70-130
0
Boron
ug/L
33700
500
500 36700
36600
608 584
70-130
0 M6
Chromium
ug/L
ND
Soo
500 490
495
98 99
70-130
1
Iron
ug/L
1370
5000
5000 6240
6250
97 98
70-130
0
Magnesium
ug/L
6680
5000
5000 11800
11800
103 103
70-130
0
Silver
ug/L
ND
250
250 247
252
99 100
70-130
2
Results presented on this page are In the units indicated by the -UMW column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, I.I.C.
Page 6 of 20

11!;a1ceAnaVical"
IMw.peakW.am
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 385093 Analysis Method: EPA 624
QC Batch Method: EPA 624 Analysis Description: 624 MSV
Associated Lab Samples: 92361389001
METHOD BLANK: 2134818
Associated Lab Samples: 92361389001
Parameter
Units
Matrix:
Blank
Result
Water
Reporting
Limit
Analyzed
1,1,1-Trichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,1,2,2-Tetrachloroethane
ug/L
ND
2.0
11/02/17 17:58
1,1,2-Tdchloroethane
ug/L
NO
2.0
11102/1717:58
1,1-Dichloroethane
ug/L
ND
2.0
11/02/17 17:58
1,1-Dichloroethene
ug/L
ND
2.0
1110211717:58
1,2-Dichloroethane
ug/L
NO
2.0
11/02/17 17:58
1,2-Dichloropropane
ug/L
NO
2.0
11/02/17 17:58
2-Chloroethylvinyl ether
ug/L
ND
5.0
11/02/17 17:58
Acrolein
ug/L
ND
5.0
11/0211717:58
Acrylonitrile
ug/L
ND
50.0
11/02/17 17:58
Benzene
ug/L
ND
2.0
11/02/17 17:58
Bromodichloromethane
ug/L
ND
2.0
11/0211717:58
Bromoform
ug/L
ND
2.0
11/0211717:58
Bromomethane
ug/L
ND
2.0
11/0211717:58
Carbon tetrachloride
ug/L
ND
2.0
11/02/17 17:58
Chlorobenzene
ug/L
NO
2.0
1110211717:58
Chlorcethane
ug/L
NO
2.0
11/02/17 17:58
Chloroform
ug/L
NO
2.0
11102/1717:58
Chloromethane
ug/L
NO
2.0
1110211717:58
cis-1,2-Dichloroethene
ug/L
ND
2.0
11/02/17 17:58
cis-1,3-Dichloropropene
ug/L
ND
2.0
11/02/17 17:58
Dibromochloromethane
ug/L
ND
2.0
11/0211717:58
Dichlorodifluoromethane
ug/L
ND
2.0
11/0211717:58
Ethylbenzene
ug/L
ND
2.0
11/02/17 17:58
Methylene Chloride
ug/L
ND
2.0
11/02/17 17:58
Tetrachloroethene
ug/L
ND
2.0
11/02/17 17:58
Toluene
ug/L
ND
2.0
11/0211717:58
trans-1,2-Dichloroethene
ug/L
ND
2.0
11/02/17 17:58
trans-1,3-Dichloropropene
ug/L
ND
2.0
11/02/17 17:58
Trichloroethene
ug/L
ND
2.0
11/02/17 17:58
Trichlorofluoromethane
ug/L
ND
2.0
11/02/17 17:58
Vinyl chloride
ug/L
ND
2.0
11/02/17 17:58
1,2-Dichlorcethane-d4 (S)
%
97
70-130
11/02/17 17:58
4-Bromofluorobenzene (S)
%
100
70-130
11/02/17 17:58
Toluene-d8 (S)
%
104
70-130
11/02/17 17:58
Qualifiers
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2134819
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
1,1,1-Tdchloroethane ug/L 20 18.2 91 52-162
Results presented on this Page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result.
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, L-C. Page 7 of 20

aceAnalytical e
' arwpecelabs.com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
LABORATORY CONTROL SAMPLE:
2134819
Spike
LCS
LCS
% Rec
Parameter
Units
Conc.
Result
% Rec
Limits
Qualifiers
1,1,2,2-Tetrachloroethane
ug/L
20
17.1
86
46-157
1,1,2-Trichloroethane
ug/L
20
18.6
93
52-150
1,1-Dichloroethane
ug/L
20
17.5
87
59-155
11-Dichloroethene
ug/L
20
19.2
96
1-234
1,2-Dichloroethane
ug/L
20
18.2
91
49-155
1,2-Dichloropropane
ug/L
20
19.3
97
1-210
2-Chloroethylvinyl ether
ug/L
40
29.8
75
1-305
Acrolein
ug/L
100
130
130
15-152
Acrylonitrile
ug/L
100
89.0
89
75-132
Benzene
ug/L
20
18.5
93
37-151
Bromodichloromethane
ug/L
20
18.4
92
35-155
Bromoform
ug/L
20
16.3
81
45-169
Bromomethane
ug/L
20
20.1
100
1-242
Carbon tetrachloride
ug/L
20
18.5
93
70-140
Chlorobenzene
ug/L
20
18.1
91
37-160
Chloroethane
ug/L
20
18.9
94
14-230
Chloroform
ug/L
20
17.8
89
51-138
Chloromethane
ug/L
20
17.3
87
1-273
cis-1,2-Dichloroethene
ug/L
20
18.4
92
68-146
cis-1,3-Dichloropropene
ug/L
20
19.2
96
1-227
Dibromochloromethane
ug/L
20
16.8
84
53-149
Dichlorodifluoromethane
ug/L
20
16.2
81
70-130
Ethylbenzene
ug/L
20
17.5
88
37-162
Methylene Chloride
ug/L
20
21.6
108
1-221
Tetrachloroethene
ug/L
20
18.8
94
64-148
Toluene
ug/L
20
18.5
92
47-150
trans-1,2-Dichloroethene
ug/L
20
18.3
92
54-156
trans-1,3-Dichloropropene
ug/L
20
18.9
94
17-183
Trichloroethene
ug/L
20
19.6
98
71-167
Tdchlorofluoromethane
ug/L
20
17.9
90
17-181
Vinyl chloride
ug/L
20
18.2
91
1-251
1,2-Dichloroethane-d4(S)
%
103
70-130
4-Bromofluorobenzene(S)
%
96
70-130
Toluene-d8 (S)
%
104
70-130
MATRIX SPIKE SAMPLE:
2134821
92361205001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
1,1,1-Trichloroethane
ug/L
ND
20
20.9
105
46-171
1,1,2,2-Tetrachloroethane
ug/L
ND
20
18.2
91
73-159
1,12-Trichloroethane
ug/L
ND
20
20.0
100
64-152
1,1-Dichloroethane
ug/L
ND
20
20.1
100
43-172
1,1-Dichloroethene
ug/L
ND
20
22.1
'I'll
48-189
1,2-Dichloroethane
ug/L
ND
20
20.4
102
42-171
1,2-Dichloropropane
ug/L
ND
20
21.6
108
55-157
Results presented on this page are in the units indicated by Me "Units" column except where an alternate unit is presented to the right or the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, U.C. Page 8 of 20

PaceAnalylical
wwui pateldbs.CWn
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntemville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
MATRIX SPIKE SAMPLE:
2134821
92361205001
Spike
MS
MS
% Rec
Parameter
Units
Result
Conc.
Result
% Rec
Limits Qualifiers
2-Chloroethylvinyl ether
ug/L
ND
40
ND
0
70-130 M1,c2
Acrolein
ug/L
ND
100
138
138
70-130 Mill
Acrylonitrile
ug/L
ND
100
101
101
70-130
Benzene
ug/L
ND
20
20.3
101
54-163
Bromodichloromethane
ug/L
ND
20
19.8
99
56-152
Bromoform
ug/L
ND
20
17.1
85
53-151
Bromomethane
ug/L
ND
20
16.8
84
10-200
Carbon tetrachloride
ug/L
ND
20
20.1
101
41-175
Chlorobenzene
ug/L
ND
20
20.7
103
67-152
Chloroethane
ug/L
ND
20
22.8
114
23-200
Chloroform
ug/L
ND
20
18.4
92
51-166
Chloromethane
ug/L
ND
20
17.0
85
40-175
cis-1,2-Dichloroethene
ug/L
ND
20
21.2
106
45-174
cis-1,3-Dichloropropene
ug/L
ND
20
19.9
100
38-146
Dibromochloromethane
ug/L
ND
20
18.8
94
65-144
Dichlorodifluoromethane
ug/L
ND
20
18.5
92
70-130
Ethylbenzene
ug/L
ND
20
19.8
99
57-152
Methylene Chloride
ug/L
ND
20
20.0
100
40-167
Tetrachloroethene
ug/L
ND
20
21.0
105
59-155 .
Toluene
ug/L
ND
20
20.6
103
47-162
trans-1,2-Dichloroethene
ug/L
ND
20
21.1
106
47-178
trans-1,3-Dichloropropene
ug/L
ND
20
19.4
97
39-148
Trichloroethene
ug/L
ND
20
21.7
109
60-153
Trichlorofluoromethane
ug/L
ND
20
21.3
107
42-199
Vinyl chloride
ug/L
ND
20
21.2
106
46-176
1,2-Dichloroethane-d4 (S)
%
101
70-130
4-Bromofluorobenzene (S)
%
96
70-130
Toluene-d8 (S)
%
96
70-130
SAMPLE DUPLICATE: 2134820
92361204001
Dup
Parameter
Units
Result
Result
RPD
Qualifiers
1,1,1-Trichloroethane
ug/L
ND
ND
1,1,2,2-Tetmchloroethane
ug/L
ND
ND
1, 1, 2-Trichloroethane
ug/L
ND
ND
1,1-Dichloroethane
ug/L
ND
ND
1,1-Dichloroethene
ug/L
ND
ND
1,2-Dichloroethane
ug/L
ND
ND
1,2-Dichloropropane
ug/L
ND
ND
2-Chloroethylvinyl ether
ug/L
ND
ND
Acrolein
ug/L
ND
ND
Acrylonitrile
ug/L
ND
ND
Benzene
ug/L
ND
ND
Bromodichloromethane
ug/L
ND
ND
Bromoform
ug/L
ND
ND
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 20

PaceAnalytical e
wwwpaceiabs cry,
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
SAMPLE DUPLICATE: 2134820
Parameter
Units
92361204001
Result
Cup
Result
Bromomethane
ug/L
ND
ND
Carbon tetrachloride
ug/L
ND
ND
Chlorobenzene
ug/L
ND
ND
Chloroethane
ug/L
ND
ND
Chloroform
ug/L
ND
ND
Chloromethane
ug/L
ND
ND
cis-1,2-Dichloroethene
ug/L
ND
ND
cis-1,3-Dichloropropene
ug/L
ND
ND
Dibromochloromethane
ug/L
ND
ND
Dichlorodifluoromethane
ug/L
ND
ND
Ethylbenzene
ug/L
ND
ND
Methylene Chloride
ug/L
ND
ND
Tetrachloroethene
ug/L
ND
ND
Toluene
ug/L
ND
ND
trans-1,2-Dichloroethene
ug/L
ND
ND
trans-1,3-Dichloropropene
ug/L
ND
ND
Trichloroethene
ug/L
ND
ND
Trichlorofluoromethane
ug/L
ND
ND
Vinyl chloride
ug/L
ND
ND
1,2-Dichloroethane-d4 (S)
%
100
102
4-Bromofluorobenzene (S)
%
100
97
Toluene-d8(S)
%
106
102
RPD Qualifiers
2
3
4
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntereville, INC 28078
[phone]
Results presented on this page are In the units indicated by the "Unfits" column except where an alternate unit is presented to the right of the result
REPORT OF LABORATORY ANALYSIS
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Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, L-C. Page 10 of 20

PaceAnalytical s
avrwpecelabs,com
QUALITY CONTROL DATA
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 384949
Analysis Method:
SM 2540D
QC Batch Method: SM 2540D
Analysis Description:
2540D Total Suspended Solids
Associated Lab Samples: 92361389001
METHOD BLANK: 2133904
Matrix: Water
Associated Lab Samples: 92361389001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
Total Suspended Solids
mg/L
NO
2.5 11/02/17 08:25
LABORATORY CONTROL SAMPLE: 2133905
Spike LCS
LCS % Rec
Parameter
Units
Conc. Result
% Rao Limits Qualifiers
Total Suspended Solids
mg/L
250 228
91 90-110
SAMPLE DUPLICATE: 2133906
92361383001 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
NO
ND
SAMPLE DUPLICATE: 2133907
92361391003 Dup
Parameter
Units
Result Result
RPD Qualifiers
Total Suspended Solids
mg/L
ND
NO
Results presented on this page are in the units indicated by the "Onus" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 20

i PaceAnalytical a
www.pacelBhs.Cpm
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 384933 Analysis Method: SM 5210B
QC Batch Method: SM 5210B Analysis Description: 5210E BOD, 5 day
Associated Lab Samples: 92361389001
METHOD BLANK: 2133872 Matrix: Water
Associated Lab Samples: 92361389001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOD, 5 day mg/L NO 2.0 11/06/17 20:53
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2133873
Spike LCS LCS % Rec
Parameter Units Cone. Result % Rae Limits Qualifiers
BOD, 5 day mg/L 198 154 78 84.6-115.4 L2
SAMPLE DUPLICATE: 2133874
92361437001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day mg/L NO ND D6
Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11115/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 12 of 20

2aceAnalyficals
wwwpacelabs. Won
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 385507
QC Batch Method: EPA 350.1 1993 Rev 2.0
Associated Lab Samples: 92361389001
METHOD BLANK: 2137940
Associated Lab Samples: 92361389001
Parameter Units
Nitrogen, Ammonia mg/L
QUALITY CONTROL DATA
Analysis Method: EPA 350.1 1993 Rev 2.0
Analysis Description: 350.1 Ammonia
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.10 11/09/17 00:36
Pace Analytical services, LLC
9800 Kincey Ave. Suite
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2137941
Spike LCS LCS % Rec
Parameter Units Conc. Result e/ Rec Limits Qualifiers
Nitrogen, Ammonia mg/L 5 5.1 101 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137942 2137943
MS MSD
92361633002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L 4.8 5 5 9.6 9.6 97 97 90-110 0
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2137944 2137945
MS MSD
92362056001 Spike Spike MS MSD MS MSD %Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Nitrogen, Ammonia mg/L NO 5 5 4.9 4.9 98 98 90-110 0
Results presented on this page are In Me units Indicated by the -Units" column except where an altemate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC.
Page 13 of 20

2aceAnalyticala
rvapvpacelabs. com
QUALITY CONTROL DATA
Project: Permit Renewal 002
Pace Project No.: 92361389
QC Batch: 386547 Analysis Method: SM 5220D
QC Batch Method: SM 5220D Analysis Description: 5220D COD
Associated Lab Samples: 92361389001
METHOD BLANK: 2143913
Associated Lab Samples: 92361389001
Parameter Units
Chemical Oxygen Demand mg/L
LABORATORY CONTROL SAMPLE: 2143914
Parameter Units
Chemical Oxygen Demand mg/L
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 25.0 11/1311719:02
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
1120 751 67 90-110 L2
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143915 2143916
MS MSD
92360409001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 803 150 150 900 907 65 69 90-110 1 MO
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2143917 2143918
MS MSD
92361431002 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conic. Conc. Result Result % Rec % Rec Limits RPD Qual
Chemical Oxygen Demand mg/L 27.0 150 150 145 141 79 76 90-110 3 MO
Results presented on this page are in the units Indicated by the 'Units" column except where an alternate unit is presented to the right of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, U.C.
Page 14 of 20

-PaceAnalytical e
wwwpacipabs.com
Project: Permit Renewal 002
Pace Project No.: 92361389
OC Batch: 384971
QC Batch Method: SM 5310B
Associated Lab Samples: 92361389001
METHOD BLANK: 2133960
Associated Lab Samples: 92361389001
Parameter Units
Total Organic Carbon mg/L
QUALITY CONTROL DATA
Analysis Method: SM 5310B
Analysis Description: 5310B TOC
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
NO 1.0 11/0211716:28
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Hunlersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 2133961
Spike LCS LCS % Rec
Parameter Units Conc. Result %Rec Limits Qualifiers
Total Organic Carbon mg/L 25 23.6 94 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 2133962 2133963
MS MSD
92361364001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conic. Result Result % Rec % Rec Limits RPD Qual
Total Organic Carbon mg/L 9.5 25 25 32.4 32.3 91 91 90-110 0
Results presented on this page are in the units indicated by the "Units' column except where an alternate unit is presented to the tight of the result.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, L-C.
Page 15 of 20

Pace Analytical Services, LLC
% 9800 Kincey Ave. Suite 100
aceAnalylrcal Huntersville, INC 28078
w Pnelabs.= (704)875-W!32
QUALIFIERS
Project: Permit Renewal 002
Pace Project No.: 92361389
DEFINITIONS
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
NO - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PQL - Practical Quantitation Limit.
RL - Reporting Limit.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
B2 Oxygen usage is less than 2.0 for all dilutions set. The reported value is an estimated less than value and is calculated
for the dilution using the most amount of sample.
D6 The precision between the sample and sample duplicate exceeded laboratory control limits.
L2 Analyte recovery in the laboratory control sample (LCS) was below QC limits. Results for this analyte in associated
samples may be biased low.
Mo Matrix spike recovery and/or matrix spike duplicate recovery was outside laboratory control limits.
M7 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
c2 Acid preservation may not be appropriate for the analysis of 2-Chloroethylvinyl ether.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 11/15/2017 07:59 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 20

iPaceAnalytical
. pacelabs, Wr,
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Permit Renewal 002
92361389
Analytical
Lab ID
Sample ID
QC Batch Method
QC Batch
Analytical Method
Batch
92361389001
002
EPA 200.7
386674
EPA 200.7
386787
92361389001
002
EPA 624
385093
92361389001
002
SM 2540D
384949
92361389001
002
SM 5210B
384933
SM 5210B
384937
92361389001
002
EPA 350.1 1993 Rev 2.0
385507
92361389001
002
SM 5220D
386547
92361389001
002
SM 5310B
384971
Date: 11/15/2017 07:69 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 17 of 20

Document Name.
Document Revised: August 4, 2017
Sample Condition Upon lt"eipt(SCUR)
Page 1 of 2
Document No.: Issuing Authority:
BCBARalyllCdl
F-CAR-CS-033-Rev.04 - Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden❑ Greenwood ❑
Huntersville [� Raleigh❑ Mechanicsville❑
• Client Name:
WO# : 92361389
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[-:I �1''I��
Project h:
17c rYl !TIYtU1Lc.
ram-
Courier ax ❑UPS
Client II I III III II II' I II III
❑ Commercial pace ❑Other _
92361389
Custody Seal Present? ❑Yes No Seals Intact? ❑Yes
❑No'L
Dote/InItIB6 Person Examining Conlenfs: I)� j I /I
Packing Material: ❑Bubble Wrap ❑Bubble Bags ❑None
❑ Other Biological Tissue Fr n?
Thermomete �JnI
rylA Gun 10: we[
1-1 L Type
❑Yes ❑No 11
❑Blue ❑None
of
Correction Factor: Cooler Temp Corrected ('Cl: 2.
Temp should be above Freezing to 6'C
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil (❑ N/A, water samplel
Did samples originate in a quarantine zone within the United States CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
byes FIN.
Nxw and puartn AIrnIT Mr., f-IN.
Comments/Disc anq:
Chain of Custody Present?
YesR[31r.C]NIA
1.
Samples Arrived within Hold Time?
Yes2.
Short Hold Time Anal sis (<72 hr.)?
Yes3.
Rush turnAround Time Re uested?
Yes4.
Sufficient Volume?
s
S.
Correct Containers Used?
-Pace Containers Used?
Y
Yes
ONO
ONO
❑N/A
ONJA
6.
Containers Intact?
Yes
No
N
7.
Dissolved analysis: Samples Field Filtered?
r
[]No
ENIA
Is
Sample Labels Match COC?
-Includes Date/Time/ID/AnalYsis Matrix:
res
W 7
ONO
❑N/A
9.
Headsace In VOA Vials (s5'firri
❑Yes
NP
ONJA
10.
Trip Blank Present?
TripBlank Custody Seals Present?
Oyes
Yes
No
No
❑N/
N/A
11.
CUENT NOTIFf"TION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of split Containers
Date/Time:
Field Dana Required? ❑Yes []No
Project Manager SCURF Review: Date: II —I -I�-
Project Manager SRF Review: I� I hI. I U Date: I I r)s-It 1
Note: Whenever there Is a discrepancy affecting North Catalina Compliance Samples, a copy of this form will be sent to the North Carolina DDWR Certification Office like
Out of hold, mcurrect preservative, out or temp, incorrect containers)
Page 18 of 20

Document Name:
Sample Condition Upon Rec
. 2CBi1(lril jAfCB� Document No.
r
"Check mark top half of box If pH and/or dechlorination
is verified and within the acceptance range for
preservation samples.
"Bottom half of box is to list number of bottles
Document RevisedAugust 6,
Page 2 of 2
Issuing Authority:
Parn n,ulitu nffiry
Project# I WO# : 92361389
PM: AMB Due Date: 11/15/17
CLIENT: 92-PPG
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pH upon receipt
Date preservation adjusted
Time preserval,on
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Page 19 of 20

i
FaceAnalytical
CHAIN -OF -CUSTODY 1 Analytical Request Document
Tne Chamrol-Custody Pan LEGAL DOCUMENT All relevant fields must De ComPete0 a¢ur;rys::y
Page: / of /
Section A Section B Section C
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pre:¢ Inlwnulion'. Required Pucl<l Inlgmat— Inmo, Inlomlation
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PaceAnalytical
x ,pacelabs.co,
November 22, 2017
Mr. Guy O'Connor
Electric Glass Fibers of America, LLC
940 Washburn Switch Road
Shelby, NC 28150
RE: Project: CTAS Resample - Permit Renewal
Pace Project No.: 92362439
Dear Mr. O'Connor:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Enclosed are the analytical results for sample(s) received by the laboratory on November 08, 2017.
The results relate only to the samples included in this report. Results reported herein conform to the
most current, applicable TNI/NELAC standards and the laboratory's Quality Assurance Manual,
where applicable, unless otherwise noted in the body of the report.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
o,".
Angela Baioni
[e-mail]
[phone]
Project Manager
Enclosures
cc: John Littlejohn, Electric Glass Fibers of America, LLC
Mr. Richard Young, Electric Glass Fibers of America, LLC
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 1 of 6

Document Name:
Document Revised: August 4, 2017
,CeAnaVlaal
Sample Condltlon Upon R![Npt(SCUR)
Page 1 of 2
Document No.:
Issuing Authority:
F-CAR-CS�033•Rev.04
Pace Quality Office
Laboratory receiving samples:
Asheville ❑ Eden[] Greenwood ❑ Huntersville Fl? Rafeigh❑ Mechanicsville❑
Client Name: . Project g WO# : 92362439
5p5 ❑Client II'II'lll'IIIIIIIII fII
Courier: ❑Fed Es ❑UP$ UPS
❑ Commerciale []Other: 92362439
Custody Seal Present? []Yes JQ'vp Seals intact? []Yes -..-❑No
Date/Initials Person Examining Contents:
Packing Material: ❑Bubble Wrap ❑Bubble Bags �]fitine ❑ Other Biological Tissue Frozen?
Thermometer: I ❑Yes_2No ❑N/A
ElfitGun ID: 1 I l U 1 Type of ice: jawet ❑Blue ❑None
Correction Factor: Cooler Temp Corrected ('C): Temp should be above freezing to 6Y
❑Samples out of temp criteria. Samples on ice, cooling process
has begun
USDA Regulated Soil NIA, water sample)
Did samples origin to in a quarantine zone within the United States. CA, NY, or SC (check maps)? Did samples originate from a foreign source (internationally,
r lv.< nr. .m,am. N.-..it P.,.nn s irnU F-1yes r7Nu
CommentsJOisve anty:
Chain of Custody Present)
r3140
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1.
Samples Arrived within Hold Time?
B Yes
Clivo
N/A
2.
Short Hold Time Analysis 471 hr.l?
vef
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❑N/A
3.
Rush Turn Around Time Requested?
Yes
o
NIA
4.
Sufficient Volume?
W es
[]NO
N/A
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Pace Containers Used?
24,
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❑NO
No
❑N/A
N/A
S.
Containers Intact?
es
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N n
7.
Dissolved analysis: Samples Field Filtered?
Y
N A
B-
Sample Labels Match COC?
Includes Crate/Time/ID/Analysis Matrix:
Clryes
❑No
❑N/A
9.
Heads ace In VOA Vials 14.1imm ?
Yu
N�o
A
10.
Trip Blank Present?
Trip Blank Custody Seals Present?
Cites
yes
.Jt-��,"
13.
❑N/A
/A
It.
CUENT NOTIFICATION/RESOLUTION
Person Contacted:
Comments/Sample Discrepancy:
Lot ID of spin containers:
Project Manager SCURF Review:
Project Manager SRF Review:
Date/Time
Date:
Date:
Field Data Required? ❑Yes []NO
Note: Whenever there is a discrepancy affecting North Catalina compliance samples, a copy of this form v41 be sent to the North Carolina DENNR Certification Office (Le.
Out of hold,'mcorrect preservative, out of temp, incorrect containers}
Page 2 of 6

Document Name. i Document
i _ .r uw nnnry war I Document No.: I Issuing Authority.
F-CAR-CS-033-Rev.04
'Check mark top half of box If pH and/or dechlorination Project 1 W0 : 92362435
is verified and within the acceptance range for PM: AMB Due Dale: 11/22/17
preservation samples. CLIENT: 92-PPG
"Bottom half of box is to list number of bottles
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Page 3 of 6

y CHAIN -OF -CUSTODY I Analytical Request Document
PaeeAnalytical Tne Cham-al Custudy is a LEGAL DOCUMENT. All relevam helas must be complelea a¢umtely o
e.v.YrtxNEatom
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RESEARCh & ANALyTICAL
LAbORATOR1ESi INC.
For: Pace Analytical-Huntersville
9800 Kincey Avenue Suite 100
Huntersville, NC 28078
Attn: Angela Baioni
Report of Analysis
11/21/2017
AfW
Q�O ANC 3H4 e_o��
Utz;
= NC 1137701
��CFA O7RF�� �S�yJ`
Client Sample ID: Effluent Lab Sample ID: 42542-01
Site: Pace -Huntersville Collection Date: 11/8/2017 8:00
Parameter
CTAS
Method
Result Units
<0.4
Rep Limit Analyst Analysis Date/Time
I
0.4 DW 11/9/2017 1530
P.0 Box 473 106 Short Street Kemersville, North Carolina 27284 Tel: [phone] Fax'. 336-996.0326
NA = not Onalyzea
v randalabs com Page 1
Page 5 of 6

u
Cftatti of Custody
aceAnalytj
w pawlab
Workorder. 92362439 Workorder Name. rTAQ ao�—..r„ o...-..:.
- - ----"'r•- -•••^• ••.., •..••a,
Re orl / nvoice To
ISubcontract To
Angela Baioni
Pace Analytical Charlotte + w Labs P.O. I V9 Re)
9800 Kincey Ave. Suite 100 ` 1
Huntersville, NC 28078S\•y`,Q�-
mesulcs
Kequestea
Requested
t5y:
11/ZZ/ZU17
Anal
sis
Phone[phone]
Email: [e-mail]
1a-99LV- a
State of Sample Origin: NC 33�—I
Preserved Containers
U
Item
Sample ID
Collect
Date/Time
Lab ID
Matrix
3
g
LAB USE
1
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Effluent _
11/81201705:00
92362439001
Water
_
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Received By
Comments
Date/Time
1
�
-
-
2
3
Cooler Temperature on Recei t °C
Custod Seal Y r N
Received on Ice Y or N
Sam les Intact Y or N
�F 4AS Tv AeQwe
Wednesday. November 08, 2017 12:52:03 PM
rr:N
FMT-ALL/0021bv,0024March2009 P,-, r, I