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WQ0000798_Monitoring - 11-2022_20221221 (2)
Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * November Report Information WQ0000798 Shallotte WWTF Type * NDMR, NDAR-1, NDAR-2, NDMLR GW-59 Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Year:* 2022 Upload Document* Shallotte DMR November 1.05MB 2022.pdf PDF Only Shallotte MW November 1.81MB 2022.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). matthew.henry@brunswickcountync.gov Matthew Henry 17W 12/21 /2022 This will be filled in automatically Initial Review Reviewer: Gerald, Wanda Is the project number correct?* WQ0000798 Is the monitoring report accepted?* Yes No Regional Office* Wilmington Reviewer: _anonymous Review Date: 1/11/2023 GW-59A COMPLIANCE REPORT FORM P e r ni it #k'211M DM— (Submir one each monitoring period with GFV-.59fePr#nsJ . ....................................... . .............. . ...................................... ...... . ...... ,2 j.1l.I.I.:il.,.,.,.,.,.,.,.,.,.I ...................... ......................................................... . ........................................... . .......... — ...... Enter date monitoring results were due. ( ?f , /,, 2- Will this monitoring report (GW-59 and GW-59A) . ........... . YES . ............... NO be submitted after the established due date? 2 ......................................................... — .................................................. . ............. . - . .. .. .. .. .. .. .. . ........................................................................ Was any required information missing on the GW-59 report forms? . YES ................. NO ................... .... ........ . ....................................... . ............................................ I ............................................................................................................................. ............ .. .. .. .. .. .. .. . I.,.,.,.,.,.,., .. .. . ........................................ . ................ . .... . ............. e answer to question I or 2 is "YES, list in the space provided below the well identification number(s) and ..................... explain the problems encountered in obtaining the required information. 3 .. .. . . ............................................................................................................................................ ........................................................................................... . .... Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing Vis NO identification plate, area overgrown, etc.)? if the answer is "Yes ", coma(! the Regional Office for guidance. 4 ........................................................................................................................................... . ......... . .... . ......................... . .............................................................. Are any monitored constituents equal to or above the established standards? ...................... YES— NO ................... . . ....................................................................................................................................................... If the answer to question 4 is 'NO", skip to section & ..................... .................. If the answer to question 4 is "YES" list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below. 5ee ............................. ...................... .......... ....................................................................................................................................................................................... For the constituents identified in question 4 above, have standards been n . .. .. .. .. ..exceeded.. .I... .. .. .. .. previously for the YES NO same constituent(s) in the same well(s) In the last two years? .................... ........................................................................................................................................................................................................................................................... 11- ................................................................................... ............ If the answer to question 5 is "NO", skip to section B. ..................... ................. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). .................... 6 .... A ... . ..... ................. .. . .................................... .. ................................ . ..... .......................... . . . . . . ... . . . . . . . . ......... . ... ... . . . . . . ............................... . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. . .. . ...... . . re the monitoring wells listed In section 5 located at or beyond the review boundary? .. . ................. YES ................. NO .................... .................................................................................................................................................................................................................................................. ........................................................................... If the answer is "YES'; a groundwater quality problem may be occurring. CONTACT THE REGIONAL ..................... .................. OFFICE IMMEDIA TEL Y FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located, contact the Regional Office. 7 ......... . ..... I.,., ............I...... ......... ......... ......... ......... ......... ....... Is the permittee Implementing previously approved actions required by the Division involving this ..................... YES .................. NO groundwater quality problem? -.1.1.1.-.,.�-11.11.1.1.1.1.1.1.1.1.I ................. . . . ......... . . . .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. .. . . . .. . .. .. .. . .. . . . .. .. . .. . .................................................................................................................................................................... . ... If the answer to question 7 is 'YES", describe those actions in the space provided below. 17 . ............... if the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may sublect the Vermittee to a Notice of Violation, Fines, and/or penalties. ................... 8 ...... The person completing this portion (GW-59A) of the monitoring report should sign below an d submit ,this . ................... .................. form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above Information was evaluated and the, information submitted In this report (Gompliance Report %W-59A)js true and complete to the, best of, my IqjqW!pqge. 1,4zz 1 Is - .................... Signature of Permittee (or Authorized Agent) Date/ ............................................................................................................. . ........................... -1-111-1 .............. ......................................... .............. GW-59A 1218/2003 0 ER1 , a 0 - :110111-1111 FACILITI'li;FOR.LATIOR eiasse ol wean; or i1pe i iPERMIT Number: Expiration Date: 12131/2024 Facility Name: Shallotte WWTF —'iNon-Discharge WQ0000798 UIC '!Permit Name (if different): I!NPDES Other ',Facility Address: Forest Dr, -TYPE OF PERMITTED OPERATION BEING MONITORED Shallofte NC 28459 County Brunswick El Lagoon E] Remediation: Infiltration Gallery IN Spray Field El Remediation: iContact Persil Matthew Henry Telephone#: (910)231-8646 El Rotary Distributor El Land Application of Sludge Well Location/Site Name: MW #6 No. of wells to be sampled: 9 —Pennd) El Water Source Heat Pump EI Other: F�m !iSAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW #6 Date sample collected: 11121/2022 FIELD ANALYSES: 'iWAS 1 !Well Depth: 20 ft. Well Diameter: 2 in. pH 004l 5.8 units i Temp. 000lo: 16-7 Oc DRY at Depth to Water Level 82546- 2.5 ft. below measuring point Screened Interval: ft, to ft. Spec. Cond. 00094: pMhos litime of Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor =85: NONE Isa fin "Volume of water pumped/bailed before sampling: 5 gallons Appearance Orange ';Samples for metals were collected unfiltered: El YES IS NO and field acidified. El YES E NO Vate sample analyzed: 11/21/2022 Laboratory Name- Environmental Chemists aARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mi Nitrite (NO2,) as N oom 0.03 mg/L Coliform: MF Fecal 31616 <1 A.:! L Niate (li as N 00620 11 ni Coliform: MF Total 31504 11OOmL Phosphorus: Total as Poa6650.18 mg/L (Note; Use MPN mthod For highly turbid samples! Orthophosphate 70507 mg/L �,issolved Solilil 70300 216 A] - Aluminum ol ioti mg/L pH (Lab) 00403 units Ba - Barium 0 1007 ul TOC oo6so 4.5 mg/L Ca - Calcium 00916 mg/L Chloride ol 56 l Cd - Cadmium 01027 ul Arsenic 01002 ug/L Chromium: Total 01034 ul Grease and Oils 00552 mg/L Cu - Copper 0 1042 mg/L Phenol 32730 ug/L Fe - Iron l ul Sulfate 00945 Hg - Mercury 71900 ul 'Pacific Conductance 000gs pMhos K - Potassium 00937 mg/L Total Ammonia oo6jo <0.2 mg/L Mg - Magnesium 00927 mg/L (Ammonia Nitrogen; NH3 as Ill Ammonia Nitrogen, Total) Mn - Manganese 01055 ul TKN as N 00625 mg/L Ni - Nickel 01067 ul rm M-MITMEN-2016M Pb - Lead o1o5i ll Zn - Zinc olo92 mg/L Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? IN Yes (1) 0 No (0) VOC 7873 method# method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mi Effluent Total VOCs: mi VOC Remill I Donald Dixon; Deputy Director Permittee for Authorized Agent) Name and Title - Please print or tvpe Signature of Permittee (or Authollized Aqent) GW-59 Rev. 06-07-2018 I -U!WJQd JO sinjou5n lalea) UuatiV pezpoqlnV jo) I' rill'' ZHU= F �T M • 3MMMEMITNEW # 13041aw # PO4jaw # P041ow wwwo wnari stems # 130419W CLSL 3OA E] (0 SOA Fg-1 Lpatjoeuv podall qe-1 CINOd3ld SVJ HDVJ-LV '# P0418W Pue Ise; f4joads) (0-1i 'Svji 00 Aq) '931INV9110 -jjBw Z60 La oug - uz -115n t-low peal - qd U01492AM LUO Ull -115n Mill-0 18313IN - �N -116n �(jutlu asque6uevq I/BW LZ600 wnisauBeVy - BVI J�tw LC600 wnlssElOd -A -I/Bn 006tL funwaVy - 6H -jIBn 91,0to u0i - aj -116W zvow jaddoo - no -JIB" noto jejo_L:wmwojt4o -1/115n LzoLo wniujpeo - po I/Bw 9L600 wni3jeo - eo -1/Bn L0011,0 wnpeg - eq -J/BW got to wnuiwnIV - IV I/BW LOSOL ajzqdso4doL44jO I/BW Vo'o 99900 d se ITa)o.L:snJOl .1. iMZ-L0-90'AG8 69-ME) adAj jo 4UUd 93e8ld - OW-L Pue OWEN 0u8lJV P821JOIL11111V JO) 88911wiOd Jol Ajnd9(3!uoxi(] pleuo(] -Vo5w SZ900 N 98 NAI (le1G1'u6ftVN 9!—WV:N WHIM!U060MN Vill Z'O> 0 00 elill 1910-L SOqjNji 96000 Gouelonpluoo og!oad.. -116w Sv600 ejejInS IjBn ouze IOuaqd 116w zssoo S[l pue aseajE) -jjBn zooto 0julasiv I/Bw 9z onoo qp!jOIqo 1/6w Z* L L 09900 oOJ quin sovoo (qel) Hd IIBUJ 0 1 � 00M 1810_L:SP!IOS POAJOSSIq !sPiduies piqjnl All J01 1130ifl9w NdVY ssn -010N) ILUIDMI w9kc 181O.L =Ivq :wjOi I/6W W1 OZ900 N Su (SON) 91eJ1!N IWOOI/ gigitr jeoe=1 =IV4:wjoj!ioo I -jjbw I/BW MID 911,900 N se (zON) 8114A g8coo CIOO 'Su011eilueawo leplolloa pue POAJOSSIP 4*81;GJ pIl sanjeA .31ON Sa2.L3wvw_ _9w8N fuol SISIWO40 IeIUOWUOJIAU3 zzoz/t.zjtt:P9zAIeue aldwes alet R S3A Lj :POWPIDU P189 PIZ ON E S3,k [-] :pajejIll pa)a@IIo3 ejam slejew jol soldweS umoie,11 aouejeaddV SUOI186-9 luildwes ajo;aq paI!uq/padwnd jejem jo awnjol OUON -!mwoa JOPO :UO11eA8I3 -d-VY 8All eoepns puel eAoqe Sil Mod BuiinsgoIN SO4INTi P6000 , puoo oadS 14 01 u :Ie"9)uI pauaajoS juiod Buunseaw molaq -V 9't, :9VSZR 19AW1 j9jeM ol Ljjda(]. :oL000,dwaj qjun Cyq :001,00 Hd 1-6 Z Jajewel(] 119M u !;z :41da(] lie M :S3SAIVNV C1131:1 ZZOZI L ZI L I :pa)o9IIoo aldwes 9je(] L# MR *!uu9d Luoji) newnN C11 -1-13M :j9qjO E] dwnd Mi aoinoS jejuM a6pnIS jo uoi ol pue-1 E] :UO4u1P0W9U El plai AejdS FE1 /uqIIeE) U0118JI11jul :uO11e1pqwqN 0 U006el E] GM011NOW ON1313 N011VH3d0 (131iMilld :10 3dAJ Ja4j1? 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P P WiUs 10 11 L•1,1 M r ', West Brunswick Regional ., 235 Grey Water IF Supply, . 4 . 1 Please see the following exceedence's for parameters on the well's listed: -7 TOC TOC- 11.2 mg/L 11/21/22 TOC- 8.7mg/L 7/19/2022 TOC- 10.7 mg/L 3/4/2022 TOC- Below limit 11/17/21 TOC- 10.5 mg/L 7/12/21 TOC- Below Limit 3/15/21 TOG Below Limit 11/18/20 TOC- 13.1 mg/L 7/20/20 W-8A TOC TOC- 10.6mg/L 11 /21 /2022 TOC- 14.9 mg/L 7/19/2022 TOC- 19.2 mg/L 3/4/2022 TOC- 19.3 mg/L 11/17/21 TOC- 18.6 mg/L 7/12/21 TOC- 21.3mg/L 3/15/21 TOC- 21.3mg/L 11 / 18/20 TOC- 199mg/L 7/20/20 TOC- 15.1mg/L 3/19/20 TOC- 11.3 mg/L 11/19/19 TOC- 27.6 mg/L 7/25/19 TOC- 31.2mg/L 3/25/19 TOC- 25.1 mg/L 11/9/18 TOC- 21.7mg/L 07/19/18 TOC- 18.7 mg/L 03/14/18 TOC- 19.4mg/L 11/20/17 DRY 3/27/17 * * Well was replaced by MW8A on 1 A20 * * TOC- 30.9mg/L 11/14/16 DRY 7/8/ 16 TOC- 38.8mg/L 3/16/16 MW-9A TOC TOC- 12.4mg/L 11 /21 /2022 TOC- 9.4 mg/L 7/19/2022 TOC- 11.9mg/L 3/4/2022 TOC- Below Limit 11/17/21 TOC- 11.0 mg/L 7/12/21 TOC- 12.8mg/L 3/15/21 TOC- 17.0 mg/L 11/18/20 TOC- 12.7 mg/L 7/20/20 TOC- 12.2 mg/L 3/19/20 TOC- 11.3 mg/L 11/19/19 TOC- 14.5mg/L 7/25/19 TOC- 10.4mg/L 3/25/19 TOC- 14.1mg/L 11/9/18 TOC- 11.8mg/L 07-19-18 TOC- 18.5 mg/L 03/14/18 TOC- 12.8 mg/L 11/20/17 TOC- 13.3 mg/L 3/27/17 TOC- 18.6 mg/L 11/14/16 TOC- 22.7 mg/L 7/8/16 TOC -11.5 mg/L 3/ 16/ 16 TOC - 13.9mg/L 11/23/15 TOC - 20.6mg/L 7/13/15 TOC - 19.4mg/L 3/5/15 -11 TOC TOC- 4.8 mg/L 11 /21 /2022 TOC- 4.6 mg/L 7/19/2022 TOC- 3.9mg/L 3/4/2022 TOC- Below limit 11/17/21 TOC- Below Limit 7/12/21 TOC- 14.6mg/L 3/15/21 TOC- 22.1 mg/L 11/18/20 TOC- 29.2 mg/L 7/20/20 TOC- 16.2 mg/L 3/19/20 Sincerely, ** Well was replaced by MW9A on 4/23/15** Matthew Henry Wastewater Sunerintendent. Brunswick Coun Big EnvitronmentW Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab 0 910392,46A424 710 Bowsertown Road, Manteo, NC 27954 & 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 0 910.347.5843 Lab/Fax] Brunswick County Public Utilities Date of Report. Dec 12, 2022 Post Office Box 249 Customer Bolivia NC 28422 Customer ID: 08100011 Attention- Report #: 2022-23234 Project ID: Old Shallotte Monitoring Its Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-57143 Site: Well 6 11121/2022 10:27 AM Water Chris House Test Method Results Date Analyzed Color Color Orange 11/2V2022 Depth to water, ft. Depth to Water, Ft 2.5 feet 11/21/2022 Ammonia Nitrogen EPA 350.1. Rev, 2,0,1993 < 0.2 mg/L 12/01/2022 Gallons balled before sampling Gallons Balled before sampling 5.0 gallons 11/21/2022 Odor Qualitative None 11/2112022 Total Dissolved Solids (TDS) SM 2540 0-2015 216 mg/L 11/2212022 Temperature SM 2550 B-201 0 16.7 C 11/21/2022 pH SM 4500 H 8-2011 5.8 units 11/21/2022 Total Phosphorus SM 4500 P (F-H-201111 O. 18 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5310 8.2014 4.5 mg/L 11/21/2022 Fecal Coliform SM 9222 0-2015 MF <1 Colonies1100mL 11/21/2022 Chloride SM4500 Cl E-2011 56 mg/L 11/2312022 1 , 1 , 1 2-Tetrachloroethane SW 846 Method 82ooDi503oB <0.5 pg/L 11/29/2022 1, 1, 1 -Trichloroethane SW 846 Method 82410015030B. <0.5pg/L 11/29/2022 1 , 1,2,2-Tetrachloroethane SW 848 Method 626OD15030B <0.5 pg/L 11/29/2022 1, 1,2-Trichloroethane SW 848 Method 8260D15030B <05pg& 11/29/2022 1,1-Dichloroethane SW 846 Method 8260DIS0308 <0,5 pg/L 1112912022 1, 1 -Dichloroethene SW 846 Method 82BOD15030B <0,5 pg/L 11/29/2022 1, 1 -Dichloropropene SW 846 Method 82800/50308 <05 pg/L 11/29/2022 1, 2,3-Trichlorobenzene SW 1146 Method 0200DI50309 <0,5pg& 11/29/2022 1,2,3-Trichloropropane SW 846 Method 8280DI5030B <0.5 pg/L 11/29/2022 1, 2,4-Trio hlorobenzene SW 846 Method 82BOD15030B <0.5pg/L 11129/2022 1,2,4-Trimethylbenzene SW 848 Method 82GOD15030B <0.5pg/L 11/29/2022 1,2-Dibromo-3-Chloropropane SW 848 Me(hod 8260/5=8 <0.5pg/L 11/29/2022 1,2-Dibromoethane SW 848 Method 826oDi5o3oo <0.5 pg/L 11/29/2022 1,2-Dichlorobenzene SW 846 Method e2tioDi5owe <0.5 pg/L 11/29/2022 Report #:: 2022-23234 Page 1 of 27 t F iliPrpn �.. 9 �>X ANALYTICAL & CONSULTING CHEMISTS Environmentid Chemists, Inc. sl' Windmillt 1 t ;b 910.392,4424 Fax 255-A Wilmington Highway, Jacksonville, NC 1 I.347.5843 Lab Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dichloroethane SW e46 Method 826OD15030B <0.5 pg/L 11/29/2022 1,2-Dichloropropane SW 846 Method 82BOD15030B <0.5 pg/L 11/29/2022 1,3,5-Trimethylbenzene SW 846 Method 0200D150308 <0.5 pg/L 11/29/2022 1,3-Dichlorobenzene SW 846 Method 0260D150308 <0,5 pg/L 11/29/2022 1,3-Dichloropropane SW 848 Method 6260D150308 <0.5 pg/L 11/29/2022 1,4-Dichlorobenzene SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 2,2-Dichloropropane SW 846 Method 82BODr5030B <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 848 Method 626OD15030B <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 846 Method 82BOD15030B <0.5 pg/L 11/29/2022 Benzene SW 846 Method 82BOD15030B <0.5 pg/L 1 1/29/2022 Bromobenzene SW 846 Method 82SOD15030B <0.5 pg/L 11/29/2022 Bromochloromethane SW 846 Method 82BOD15030B <0.5 pg/L 11/29/2022 Bromodichloromethane SW 846 Method 02600150308 <Q,5 pg/L 11/29/2022 Bromoform SW 846 Method 8260015030E <0.5 pg/L 11/29/2022 Bromomethane SW 846 Method 8260D15030B <0.5pg/L 11/29/2022 Carbon tetrachloride SW 846 Method 82600/50308 <0.5 pg/L 11/29/2022 Chlorobenzene SW 046 Method 826OD15030B <0.5 pg/L 11/29/2022 Chloroethane SW 848 Method 626OD15030B <0.5 pg/L 11/29/2022 Chloroform SW 848 Method 02GOD15030B <0.5 pg/L 11/29/2022 Chloromethane SW 846 Method 826OD15030B <0.5 pg/L 11/29/2022 cis-1,2-Dichloroethene SW 845 Method 8260D15030B <0.5 pg/L 11/29/2022 cis-1,3-Dichloropropene SW 848 Method e260D150308 <0.5 pg1L 11/29/2022 Dibromochloromethane SW 846 Method 8260015030E <0.5 pg/L 11/29/2022 Dibromomethane SW 046 Method92600150308 <0.5 PA 11/29/2022 Dichlorodifluoromethane SW 846 Method e260D/5030B <0.5 pg/L 11/29/2022 Ethylbenzene SW 846 Method 6260015030E <0.5 pg/L 11/29/2022 Hexachlorobutadiene SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 lsopropylbenzene SW 846 Method 828OD15030B <0.5 pg/L 11/29/2022 M+P Xylene SW 846 Method 826OD15030B <1.0 pg/L 11/29/2022 Methylene chloride SW 846 Method 826OD150308 <0.5 pg/L 11/29/2022 Repod 8:: 2022-23234 Page 2 of 27 BrunswickllUtilities Dec 12, 2022 Post Office Box249 Customer Bolivia 422 Customer ID: 08100011 Attention.,2022-23234 Project ID: Old Shallatte Monitoring Wells NaphthaleneSW 846 Method 8260DIS0308 < .55 /L 11/2 / 22 n-Butylbenzene SW 848 Method a260DI50308 <05 U /L 11/2 2 n-Propylbenzene SW 845 Method 8 /5030 <0.5 u /L 11129/2022 ortho-Xylene SW a4e Method 820/5030B C u /L 1 1 /2 2 p-Isopropyltoluene SW 846 Method 82 r5030 < . /L 11/2912022 sec-Butylbenzene SW 848 Method 8260DIS030B < /L 11/29/2022 Styrene SW 848 Method 826OD150308 < /L 11/2912022 tert-Butyl benzene SW 84e Method 82 0D15030 < , 5 u IL 11 /2 2 Tetrachloroethene SW 846 Method 82600150B < ,5 I 11129/2022 Toluene SW 646 Method 82GOD15030B[ /L 11/29/2022 Trans-1,2-Dichloroethene SW 845 Method 82SOD1B <0.5 pg/L 1112912022 Trans-1,3-dichloropropene SW846 Method 620OD15030 E /L 111 2 Trichloroethene SW 848 Method 02 0Dr503o < /L 11 22 Trichlorofluoromethane SW 846 Method 626015030 < / 11/29/2022 Vinyl chloride SW 846 Method 6260015030E < /L 1112912022 Nitratei I Nitrite Nitrogen EPA 353.2. Rev, 2.0, 1993 0.03 mg/L 11122/2022 ftr t itrite-N itrogen EPA 353.2, Rev 2,0, 193 11. /L 11/2312022 Nitrate itr n Subtraction e 11. /L 12/0912022 r&epork M 2022.2323,1 Flage 3 of 27 Brunswick County Public Utilities Post Office BOX 249 Bolivia NC 28422 Attention: Environmental 6602 Windmillt i t vt .392.4424 t Bowsertown Road, Manteo, NC 27954 255-A Wilmington Highway, Jacksonville, NC 28540 P 910.347.5M3 Lab/Fax] info@environmentalchemists.com Date of Report: Dec 12, 2022 Customer PO #: Customer ID: 08100011 Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: 22-57150 Site: Well 7 Test Collect Date/Time 11/21/2022 11:44 AM Method Matrix Sampled by Water Chris House Results Date Analyzed Color color Lt. Brown 11121/2022 Depth to water, ft. Depth to water, Ft. 4.8 feet 11/21/2022 Ammonia Nitrogen EPA 350.1. Rev 2.0. 1993 < 0.2 mg/L 12101/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0gallons 11/21/2022 Odor Qualitative None 11/21/2022 Total Dissolved Solids (TDS) SM 2540 c-2016 110 mg/L 11/22/2022 Temperature SM 2550 B-2010 19.1 C 11/21/2022 pH SM 4500 H B-2D11 5.0 units 11/21/2022 Total Phosphorus SM 4500 P (F-*2011 0.04 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 53108.2014 11.2mgIL 11/21/2022 Fecal Coliform SM 9222 D-2a15 MF <1 Colonies1100ml- 11/21/2022 Chloride sM4500 Cl E-2011 28 mg/L 11 /23/2022 1,1,1,2-Tetrachloroethane SW 846 Method 8260DIS0308 <0.5 pg/L 11129/2022 1, 1, 1 -Trichloroethane SW 646 Method 82000150308 <0.5 pg/L 11/29/2022 1,1,2,2-Tetrachloroethane SW 646 Method 82000150308 <0,5 pg/L 11129/2022 1,1,2-Trichloroethane SW 646 Method 828DDIS0308 <0.5 pg/L 11/29/2022 1,1-Dichloroethane SW 846 Method 828a015030e <0.5 pg/L 11/29/2022 1, 1 -Dichloroethene SW 846 Method 82600/50308 <0.5 pg/L 11/29/2022 1, 1 -Dichloropropene SW 846 Method 8260D15030B <0.5 pg/L 11 /29/2022 1,2,3-Trichlorobenzene SW 846 Method 826OD15030B <0.5 pg/L 11/29/2022 1,2,3-Trichloropropane SW 846 Method 82601315030B <0.5 pg/L 11/29/2022 1,2,4-Trichlorobenzene SW 846 Method 0260D15030B <0.5 pg/L 11/29/2022 1,2,4-Trimethylbenzene SW 846 Method 82600150308 <0.5 pg/L 11/29/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 1,2-Dibromoethane SW 845 Method 8280D150308 <0.5 pg/L 11/29/2022 1,2-Dichlorobenzene SW 848 Method 626OD15030B <Q-5 pg/L 11/29/2022 Report C. 2022-23234 Page 4 0127 011 EnviLronmental Chemists, Inc. 6602 Windmill Way, Wilnri4igton, NC 28405 e 910.392.0223 Lab o 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info@environmentalchemist&com Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO M. Bolivia NC 28422 Customer ID: 08100011 Attention: Report 9, 2022-23234 Project ID: Old Shallotte Monitoring Its 1,2-Dich1oroethane SW 846 Method 82BOD150300 <0.5pg/L 11/29/2022 1,2-Dichlore propane SW 846 Method 82600160308 <05 pg/L 11/29/2022 1,3,5-Trimethylbenzene SW $46 Method 8260DI5O30B <0.5 pg/L 11/29/2022 1,3-Dichlorobenzene SW 846 Method 11260DI50306 <0,5 pg/L 11/29/2022 1,3-Dichloropropane SW 046 Method 8200DI50308 <0.5 Pg/L 11/29/2022 1.4-Dichlorobenzene SW 846 Method 82901)150308 <0,5pgll- 11/2912022 2,2-Dichloropropane SW B46 Method 8260DIS030B <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 0260DI5030B <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 846 Method 8260DIS0308 <0.5pg/L 11/29/2022 Benzene SW 046 Method 8280DI50308 <0.5 pg/L 11129/2022 Bromobenzene SW 646 Method 8280016030B <0. 5 pg/L 11/29/2022 Bromochfor omethane SW 848 Method 0260DIS0308 <0.5 pg/L 11/29/2022 Bromodichlore methane SIN 848 Method 8200DI50308 <0.5 pg/L 11/29/2022 Brornoform. SIN 846 Method 8260D/5030B < 0. 5 pg/L 11/2912022 Bromomethane SW 045 Method 0260DI50300 <0.5 pg/L 11129/2022 Carbon tetrachloride SW 540 Method 82600I50308 <0.5 pg/L 11/29/2022 Chlorobenzene SW a46 Method 8280U15030B <0.5 pg/L 11129/2022 Chloroethane SW 846 Method 82GOD/5030B <0.5 pg1L 11/29/2022 Chloroform SW 846 Method 02GOD15030B <0, 5 pg/L 11/29t2022 Chloromethane SW 846 Method 8260DI50300 <0.5 pg/L 11/29/2022 cis-1 2-Dichlord ethene SW 848 Method 8260D15030B <0.5 pg/L 11/29/2022 cis-1.3-Dichloropropene SW 846 Method 8260D16030B <0.5 pg/L 11/2912022 Dibromochlore methane SW 846 Method 8260DI5030B <0,6pg/L 11/29/2022 Dibromomethane SW 846 Method 026OD150308 <0,5pg/L 11129/2022 Dichlarodifluoromethane SW 846 Method 82BOD/5030B <0.5 pg/L 11129/2022 Ethylbenzene SIN 848 Method 82500150308 <0.5 pg/L 11129/2022 Hexachlorobutadiene SW 846 Method 8200DI5030B <0.5 lig/L 11/29/2022 lsopropylbenzene SW 846 Method 82600/50308 <0.5 pg/L 11/2912022 M+P Xylene SW 848 Method 8280DI5030B <1.0pg/L 11/29/2022 Methylene chloride SW 840 Method $260DIS030B <0.5 pg/L 11129/2022 Report #. 2022-23234 Page 5 of 27 t�`� t't�tFIi4Y9r,Ird sm;",., SM' ANALYTICAL & CONSULTING CHEMISTS Environmental s 661' Windmill Way, Wilmington,:41 " 1 I 910392.4424 #' Dowsertown Road, Manteo, NC 27954I Wilmington s I 0 910.347.5843 1 4 I Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO : Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Naphthalene SW 846 Method 826013/50308 <0.5 uglL 11 /29/2022 n-Butylbenzene SW 848 Method 8260DI5030B <0.5 pg/L 11/29/2022 n-Propylbenzene SW 046 Method 826ao150308 <0.5 pg/L 11/29/2022 ortho-Xylene SW 846 Method 8280D/90308 <0.5 pg/L 11/29/2022 p-Isopropyltoluene SW 848 Method 8260DIS030B <0.5 pg/L 11/29/2022 sec-Butyibenzene SW 848 Method 8280D/5030B <0.5 pg/L 11/29/2022 Styrene SW 848 Method 8250D15030B <0.5 IJg/L 11/29/2022 tert-Butyl benzene SW 846 Method 82600150308 <0.5 pg/L 11/29/2022 Tetrachloroethene SW 846 Method 82600150300 <0„ 5 }jg/L 11/29/2022 Toluene SW 848 Method 0280D15030B <0.5 pg/L 11/29/2022 Trans-1 ,2-Dichloroethene SW 848 Method 8200DI50308 <0, 5 pg/L 11/29/2022 Trans-1,3-dichloropropene SW 848 Method 828OD150308 <0.5 pg/L 11/29/2022 Trichloroethene SW 846 Method 8260D15030B <0.5 Ng/L 11/29/2022 Trichlorofluoromethane SW 846 Method 8200DIS030B <0.5 pg/L 11/29/2022 Vinyl chloride SW 848 Method 626OD15030B <0.5 pg/L 11/2M022 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353.2. Rev. 2.0, 1993 0.03 mg/L 11/22/2022 Nitrate+ N itrite-N itrogen EPA 353 2, Red, 2.0, 1903 1.94 mglL 11/23/2022 Nitrate Nitrogen subtraction Method 1.91 mg/L 12/09/2022 -------------------- Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO M Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 22-57151 Site: Well 8 11/2112022 11:25 AM Water Chris House Test Method Results Date Analyzed for Color Clear 11/21/2022 Depth to water, ft. Depth to Water, Ft. 5. 9 feet 11/2112022 Ammonia Nitrogen EPA 360, 1, Rev 2.0,190 < 0.2 mg/L 12/0112022 Gallons bailed before sampling Gallons Bailed before sampling 5.Ogallons 11/21/2022 Odor Qualitative None 11/2112022 Total Dissolved Solids (TDS) SM 2540 C-201 5 128 mg/L 11122/2022 Temperature SM 2550 B-2010 19.0 C 11/2112022 pH SM 4500 H 8-2011 5.4 units 11/21/2022 Total Phosphorus SM 4500 P (F-H).201i < 0.04 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5310 B-2014 10.6 mg/L 11/21/2022 Fecal Coliforrin SM 9222 D-201 5 MF < 1 Colonies/I 00m L 1112112022 Chloride SM4500 Cl E-2011 38 mg/L 11/2312022 1, 1, 1,2-Tatrachloroethane SW 845 Method 8260DIS0300 <0,5pg& 1112912022 1, 1. 1 -Trichloroethane SW 846 Method 82600160308 <0.5pg/L 11129/2022 1, 1,2,2-Tetrachloroethane SW 846 Method 0260D/50308 <0.5pg/L 11/29/2022 1 , 1,2-Trichloroethane SW 846 Method 8260D/5030B <0.5 pg/L 11/2912022 1, 1 -Dichlorcethane SW $46 Method 8260DI50308 <0.5 pg/L 11/29/2022 1,1-Dichloroethene SW 046 Method 0260DIS030B <0.5pg& 11/2912022 1,1-Dichloropropene SW U6 Method 8200DIS0308 <0.5pg/L 11/29/2022 1, 2,3-Trichlorobenzene SW 846 Method 8260DI5030B <0.5pg/L 11129/2022 1,2,3-Trichlaropropane SW 846 Method 826OD/50308 <0-5 pg/L 11129/2022 1,2,4-Trichlorobanzene SW 848 Method $20015009 <06pg& 11129/2022 1, 2,4-Trimethylbenzene SW 846 Method e2eODi503m <0.5pg/L 1112912022 1,2-Dibromo-3-Chlord propane SIN 846 Method 62801315030B <0.5pg/L 11/29/2022 1,2-Dibromoethane SW 846 Method 82BOD/5030B <0.5pg/L 11/29/2022 1, 2-Dichlore benzene SW 846 Method 8260015030B <0.5 pg/L 11/29/2022 Report#:: 2022-23234 Page 7 of 27 ANALYTICAL & CONSULTING CHEMISTS info(' ,environmenlalche ists.co Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO : Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dlchloroethane SW 846 Method 82GOD150308 <0.5 pg/L 11/29/2022 1,2-Dichloropropane SW 846 Method 8280D15030B <0.5 pg/L 11/29/2022 1, 3,5-Trimethyl benzene SW 846 Method 828OD150308 <0.5 pg/L 11/29/2022 1,3-Dichlorobenzene SW 646 Method 8260D150300 <0.5 pg/L 11/29/2022 1,3-Dichloropropane SW 846 Method 828OD150308 <0.5 pg/L 11/29/2022 1,4-Dichlorobenzene SW 846 Method 8260D/50308 <0.5 pg/L 11/29/2022 2,2-Dichloropropane SW 846 Method 828®D150308 <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 Benzene SW 848 Method 8260015030B <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method 8260015030B <0.5 pg/L 11/29/2022 Bromochloromethane SW 848 Method e260Drs030B <0.5 pg/L 11/29/2022 Bromodichloromethane SW 846 Method 826OD150308 <0.5 pg/L 11/29/2022 Bromoform SW 846 Method 8260DIS030D <0.5 pg/L 11/29/2022 Bromomethane SW 846 Method 8260D16030B <0.5 pg/L 11/29/2022 Carbon tetrachloride SW 646 Method 8260D150308 <0.5 pg/L 11/29/2022 Chlorobenzene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Chloroethane SW 846 Method 8260D/50308 <0.5 pg/L 11/29/2022 Chloroform SW 846 Method 8260D150300 <0.5 pg/L 11/29/2022 Chloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 cis-1,2-Dichloroethene SW 646 Method 8260015030E <0.5 pg/L 11/29/2022 cis-1,3-Dichloropropene SW 840 Method 826OD15030B <0.5 pg/L 11/29/2022 Dibromochloromethane SW 846 Method 6200D15030B <0.5 pg/L 11/29/2022 Dibromomethane SW 848 Method 826ODr5030B <0,5 pg/L 11/29/2022 Dichlorodifluoromethane SW 845 Method 82BOD150308 <0.5 pg/L 11/29/2022 Ethylbenzene SW 846 Method 8280DIS030D <0.5 pg/L 11/29/2022 Hexachlorobutadiene SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 Isopropyl benzene SW 846 Method 8260D/60308 <0.5 pg/L 11/29/2022 M+P Xylene SW 846 Method 8260D150308 <1,0 pg/L 11/29/2022 Methylene chloride SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Repot It2022-23234 Page 8 of 27 ANALYTICAL & CONSULTING CHEMISTS info(ken +ironmentalch ist&com ..... Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box Bolivia 2 1 0 11 Attention: 2022-23234 Project ID: Old Shallotte Monitoring Wells NaphthaleneSW 846 Method 82600150 c /L 11/2912022 n-Butylbenzene SW 846 Method 6260DIS030B < .5 /L 11/29/2022 n-Propylbenzene SW 846 Method 82a= 30B <0.5 u / 11/29/2022 ortho-Xylene Ew 846 Method 826OD15030B< N / 11/29/2022 p-isopropy[toluene SW 846 Method82800/5030 <0.5 u / 111 / 2 sec -Butyl n n sw ear Method 8280rs0300 <0, ♦j /L 11/29/2022 Styrene8w sae Method 8260DIS030B <0. lJ / 11129/2022 tert-Butylbenzene sw 846® 82600160308 <0.5 u /L 11/29/2022 Tetrachloroethene SW 846 Method826001 30B <0.5 lJ / 11/2912022 Toluene SW 848 Method 82e015030 <0.5 it 1L 11/29/2022 Tr -1,2- is loco t sw e46 Method 820DD/50309 < / 11129/2022 Trans-1,3-dichlorapropene sw 046 Method 825030 <0.5 u /L 1 1/22 Trichloroethene SW 846 Method8260D150308 <, W/ 11/29/2022 Trichlorofluoromethane sw 84a Method 8280015030E <0.5 p /L 11/29/2022 Vinyl chloride SW 646 Method 8260DIS030B <0. p /L 11/29/2022 Nitrite Nitrogen EPA 353.2, Rev. 2.0, 10®3 < 0.02 /L 11/22/2022 itr + itrit - itr n EPA 353.2. Rev 2,0.1093 0.28 mg/L11/23/2022 Nitrate Nitrogen ubtra n Method 0.28/L 12/0912022 Report d, 2022.23234 Page 9 of 27 21 ANALYTICAL & CONSULTING CHEMISTS Environmental Chemists, Inc. 710 Bowsertown Road,252.473.5702 Lab/Fax 910-347-5843 Lab/ Fax Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO 0: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-57152 Site: Well 9A 11/21/2022 11:58 AM Water Chris House Test Method Results Date Analyzed Color Color Brown 11/21/2022 Depth to water, ft. Depth to Water. Ft. 11.9 feet 11/21/2022 Ammonia Nitrogen EPA 360.1. Rev. 2.0. 1993 < 0.2 mg/L 12/01/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11121 /2022 Odor Qualitative None 11121 I2022 Total Dissolved Solids (TDS) SM 2540 C-2015 98 mg/L 11/22/2022 Temperature SM 2550 6.2010 20.1 C 11/21/2022 pH SM 4500 H 8.2011 5.1 units 11/21/2022 Total Phosphorus SM 4500 P (F-H)-2011 0.05 mg/L 12/02/2022 Total Organic Carbon (TOC) SM53108-2014 12.4mg/L 11/21/2022 Fecal Coliform SM 9222 0-2015 MF <1 Colonies1100mL 11/21/2022 Chloride SM4600 Cl E-2011 25 mg/L 11/23/2022 1,1,1,2-Tetrachloroethane SW 846 Method 826OD150308 <0.5 pg/L 11/29/2022 1,1,1-Trichlomethane SW 846 Method 8260DIS030B <0.5 pg/L 11/29/2022 1.1,2,2-Tetrachloroethane SW 846 Method 8260015030E <0.5 pg/L 11/29/2022 1,1,2-Trichloroethane SW 846 Method 8260Dr50309 <0.5 pg/L 11 /29t2022 1. 1 -Dichloroethane SW 846 Method 0260D15030B <0.5 pg/L 11/29/2022 1. 1 -Dichloroethene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 1,1-Dichloropropene SW 846 Method 8280DI50308 <0.5 pg/L 11/29/2022 1,2,3-Tdchlorobenzene sw 846 Method 8260DI5030B <0.5 pg/L 11/29/2022 1,2,3-Tdchloropropane SW 840 Method 82600150305 <0.5 pg/L 11/29/2022 1,2,4-Trichlorobenzene SW 846 Method 026OD150308 <0.5 pg/L 11/29/2022 1,2,4-Trimethylbenzene SW 948 Method 8260DI50308 <0.5 }tg/L 11/29/2022 1,2-Dibromo-3-Chloropropane SW $45 Method 82a0D15030B <0.5 pg/L 11/29/2022 1,2-Dibromoethane SW 846 Method 8260D/W308 <0.5 pg/L 11 /29/2022 1,2-Dichlorobenzene SW 846 Method 8260DI50308 <0.5 pg/L 11/29/2022 Report *:: 2022-23234 Page 10 of 27 Environmental Chemists, Inc. JUA 6602 Windmill Way, Wilmington, NC 28405 * 910,392,0223 Lab 0 910,392.4424 Fax 1 110 1110 i 710 Bood wsertwn Roa, Manteo, NC 27954 o 252.473.5702 Lab/Fax 41111, 255-A Wilmington Highway, Jacksonville, NC 28540 m 910347.5843Lab/Fax Brunswick County Public Utilities Date of Report: Dec 12, 2022 of Office Box 249 Customer PO #, Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID. Old Shallotte Monitoring Wells 1,2-Dichloroethane SW 846 Method 8260DI5030B <0.5 pg1L 11/2912022 1,2-Dichloropropane SW 845 MeMod 8260615030B <0.5pg/L 11/29/2022 1,3,5-Trimethylbenzene SW 846 Method a2t;=5=8 <0.5 lig/L 11/29/2022 1,3-Dichlorobenzene SW 846 Method 8260DI50308 <0.5pg/L 11/29/2022 1,3-Dichloropropane SW 646 Method 8260DI50308 <0.5 pg/L 11/29t2022 1,4-Dichlorobenzene SW 046 Method 8260DIS030B <0.5pg/L 11/29/2022 2,2-Dichloropropane SW 848 Method 8260015030B <0.51jg/L 11/29/2022 2-Chlorotoluene SW 846 Method 8260DIS030B <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 040 Method 82GOD15030B <0.5 pg/L 11129/2022 Benzene SIN 846 Method 8280D150308 <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method $26001503oB <0,5pg/L 11129/2022 Bromochloramethane SW 848 Method 8200DI6030B <0.5 pg/L 11/29/2022 Bromodichloromethane SW 848 Method 62GOD/5030B <0.5 pg/L 11/29/2022 Bromoform SW 846 Method B260DIS0308 <0Z pg/L 1112912022 Bromornethane SIN 046 Method 8260IN5030B <0.5 pg/L 11129/2022 Carbon tetrachloride SW 846 Method 8280DI50300 <0.5 pg/L 11/29/2022 Chlorobenzene SW B46 Method 8260DIS030B <0.5 pg/L 11/2912022 Chloroethane SW 846 Method 8260DI5030B <0.5 pg/L 11/29/2022 Chloroform SW 646 Method 02600150308 <0.5pg/L 11/2912022 Chlord methane SW 840 Method 8250DIS030B <0.5pg/L 11/29/2022 cis-1 2-Dichloroethene SW $45 Method 82NDI50308 <0.5 pg/L 11129/2022 cis-1,3-Dichlorapropene SW 846 Method 0260DIS0308 <0,5 pg/L 11129/2022 Dibromochloromeftne SW 846 MeMod 02600/50308 <0.5pg/L 11129/2022 Dibromomethan e SW 846 Method 8260DIS0306 <0.5 Pg/L 11/29/2022 Dichlorodifluoromethane SW 846 Method 8260DIS0308 <0,5pg/L 11129/2022 Ethylbenzene Sw 848 Method 6200DIS0308 <0.5pg/L 11129/2022 Hexachlorobutadiene SW 646 Method 8280DI5030B <0.5pg/L 11/29/2022 Isopropyl benzene SW 846 Method 0280DIS030B <0.5pg/L 11/29/2022 M+P Xylene SW 846 Method 82BOD/60308 <11.0 pg/L 11/29/2022 Methylene chloride SW 848 Method 0260DIS0308 <0, 5 pg/L 11/29/2022 RepoIrl #:: 2022-23234 Page 1 I of 27 Chemists,Environmental Inc. 6602 Windmill Way, Wilmington, NC 2W5 a 910.392.0223 Lab + 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 m 910.347.5843 Lab/Fax infb 4Pendirocmentalchcmismcorn Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Naphthalene SW 848 Method 8260D15a30B <0,5 pg/L 11/29/2022 n-Butylbenzene SW 848 Method 8280DIS030B <0.5 pg/L 11/29/2022 n-Propylbenzene SW 840 Method 82GOD15030B <0.5 pg1L 11/29/2022 ortho-Xylene SW 540 Method 828013150398 <0, 5 pg/L 11/29/2022 p-Isopropyltoluene SW B46 Method 82GOD150308 <0.5 pg/L 11/29/2022 sec-Butyibenzene SW 846 Method 826OD160308 <0.5 pg/L 11/29/2022 Styrene SW 846 Method 826015=8 <0.5 pg/L 11/29/2022 tent-Butylbenzene SW 846 Method 82BODr50308 <0.5 pg/L 11/29/2022 Tetrachloroethene SW 846 Method a260D/5030B <0.5 pg/L 11/29/2022 Toluene SW 848 Method 82eoD/5030B <0.5 pg/L 11/29/2022 Trans-1 ,2-Dichloroethene SW 646 Method 8260D150308 <0.5 pg/L 11/29/2022 Trans-1,3-dichloropropene SW 846 Method 82600150308 <0,5 pg/L 11/29/2022 Trichloroethene SW 848 Method B260DI5030B <0.5pg/L 11/29/2022 Trichlorofluoromethane SW 846 Method 8260DIS0306 <0.5 pg/L 11/29/2022 Vinyl chloride SW 848 Method 626pD150308 <0.5 pg/L 11/29/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2, Rev, 2.0, 1993 < 0.02 mg/L 11/22/2022 Nitrate+Nitrite-Nitrogen EPA 353.2. Rev, 20. 1993 0.13 mg/L 11/23/2022 Nitrate Nitrogen Subtraction Method 0.13 mg/L 12/09/2022 E-invirmunenta Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 -, 910392,0223 Lab w 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 279,54 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 * 910.347.SU3 Lab/Fax Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO 9, Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-57153 Site: Well 10 11/21/2022 10:41 AM Water Chris House Test Method Results Date Analyzed Color Color Clear 11/21/2022 Depth to water, ft. Depth to Water, Ft, 5.1 feet 11/21/2022 Ammonia Nitrogen EPA 350.1. Rev 2. D, 1903 < 0.2 mg/L 12/0112022 Gallons bailed before sampling Gallons Baited before sampling 5.0 gallons 11/21/2022 Odor Qualitative one 11/21/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 114 mg/L 11/22/2022 Temperature SM 2550 0-2010 119.0c 11/21/2022 pH SM 4500 H B-2011 5.0 units 11/21/2022 Total Phosphorus SM 4500 P (F-H)-2011 < 0.04 mg/L 12102/2022 Total Organic Carbon (TOC) sm 5310 B-2014 2.0 mg/L 11/22/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/1100ml- 11/21/2022 Chloride SM4500 Cl E-2011 33 mg/L 11/23/2022 1, 1, 1,2-Tetrachloroethane SW 846 MeOwd 8260N50308 <0.5pg/L 11/29/2022 1. 1, 1 -Trich loroethane SW 846 Method 8260DI50308 <0.5 wg/L 11/2912022 1,1,2,2-Tetrachloroethane SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 1, 1,2-Trichloroethane SW 046 Method 8260D15030B <0.5 pg/L 11129/2022 1, 1 -Dichloroethane SW 846 Method 5280DI5030B <0.5 pg/L 11/29/2022 1,1-Dichloroethane SW 848 Method 82BOD150308 <0.5 pg/L 11/29/2022 1,11-Dichloropropene SW 845 Method 8260015030121 <0.5 pg/L 11/29/2022 11,2.3-Trichfor obenzene SW 046 Method 82600150308 <0.5pg/L 11/2912022 1,2,3-Trichloropropane SW 846 Method 8260DI5030B <0pg/L 11/2912022 1,2,4-Tdchlorobenzene SW 846 MeUmd 8260DI5030B <0.5pg/L 11/2912022 1,2,4-THmethylbenzene SW $46 Method 8280DI50308 <0.5 pg/L 1 V2M022 1,2-Dibromo-3-Chloropropane SW 848 Nletlwd 820Dar S0308 <0.5 pg/L 11/29/2022 1,2-Dibromoethane SW 848 Method 112GOD150308 <0.5pg& 11/29f2022 1,2-Dichlorobenzene SW 846 Method 82BOD150300 <0.5 pg/L 11/29/2022 Report #:: 2022-23234 Page l3of27 , /� ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 w 910.347.5843 Lab/Fax info 4)cnvironmentalchemists.com Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dichloroethane SW 846 Method 82800150308 <0.5 pg/L 11/29/2022 1,2-Dichloropropane SW 846 Metfwd 8280016030B <0.5 pg/L 11/29/2022 1, 3, 5-Trimethylbenzene sw 846 Method 8280D16030B <0.5 pg/L 11/29/2022 1, 3-Dichlorobenzene SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 1, 3-Dichloropropane SW 846 Method 82WD150308 <0.5 pg/L 11/29/2022 1,4-Dichlorobenzene SW 846 Method 82600/50308 <0.5 pg/L 11/29/2022 2,2-Dichloropropane SW 646 Method 8260015030E <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 82601315030B <0,5 pg/L 11/29/2022 4-Chlorotoluene SW 846 Method 8260D15030B <0,5 pg/L 11/29/2022 Benzene SW 846 Method 8280D150308 <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method 628oar503o8 <0.5 pg1L 11/29/2022 Bromochloromethane SW a46 Method 026OD150306 <0.5 pg/L 11/29/2022 Bromodichloromethane SW 846 Method 82800/50300 <0.5 pg/L 11/29/2022 Bromoform SW 845 Method 8260015030B <0.5 pg/L 11/29/2022 Bromomethane SW 845 Method 8280D1503013 <0.5 pg/L 11/29/2022 Carbon tetrachloride SW 848 Method 826OD15030B <0.5 pg/L 11/29/2022 Chlorobenzene SW 846 Method8286D150308 <0.5 pg/L 11/29/2022 Chloroethane SW 846 Method 82801315030B <0.5 pg/L 11/29/2022 Chloroform sw 846 Method 826aD15030B <0.5 pg/L 11/29/2022 Chloromethane SW 846 Method 8260015030E <0, 5 pg/L 11/29/2022 cis-1,2-Dichloroethene SW 846 Method 826oD15030B <0,5 pg/L 11/2912022 cis-1,3-Dichloropropane SW 846 Method 6260DIS0308 <0.5 pg/L 11/29/2022 Dibromochloromethane SW 846 Method 82BODIS0308 <0,5 pg/L 11/29/2022 Dibromomethane SW 846 Method 826oD150308 <0.5 pg/L 11/29/2022 Dichlorodifluoromethane SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 Ethylbenzene SW 846 Method 8260015030E <0.5 pg/L 11/29/2022 Hexachlorobutadiene SW 846 Method 82000150308 <0.5 pg/L 11/29/2022 Isopropylbenzene SW 048 Method 82000160308 <0.5 pg/L 11/29/2022 M+P Xylene SW 846 Method 82WD/50308 <1,0 pg1L 11/29/2022 Methylene chloride SW 846 Method 826OD150308 <0.5pg/L 11/29/2022 Report N 2022.23234 Page 14 of 27 Envirormental Chemists,Inc. Wilmington,t Bowsertown Road,252.473.5702 Lab/Fax Jacksonville,255-A Wilmington Highway, i 0 0 910.347.5843Lab/Fax CONSULTINGANALYTICAL & - Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box Olivia NC 28422 Customerl: 08100011 Attention:2022-23234 Project : Old Shallotte Monitoring Wells Naphthalene 6 Method 8250D150308 <0.5 /L 111 / 0 2 n-Butylbenzene SW 848 Method 82GO 150300 .5 jJ /L 1 112 / 0 2 n-Propylbenzene SW 848 Method 8260DIS0306 <0.5 /L 11/29/2022 ortho-Xylene sw 848 Method 82600150308 <0. / 11/29/2022 p-isopropyltoluene SW 846 Method 828=50308< .51a IL 11/ / 2 sec-Butylbenzene SW 848 Method 820013160308 <0.5 /L 11/2912022 Styrenesw 845 Method 8260DI5030B 40.5iJ /L 11/29/2022 tert-Butylbenzene SW 846 Method8260DI5030B <0.5 u IL 11/ 2 Tetrachloroethene SW 846 Method 82BOD15030B <0.5 pg1L 1112912022 Toluene sw 846 Method 82GOD160300 <0. fJ /L 11 /2 022 Trans-1,2-Dichloroethene SW 848 Method 62GOD1 30B <0.5 u IL 11/2912022 Trans-1,3-dichloropropene SW 840 Method82GOD15030B <0, p /{ 11/2912022 Trichloroethene sw 646 Method 62000130B <0. u IL 11/29/2022 Trichlorofluoromethane sw 646 Methode OD15030B <0. u /L 11/29/2022 Vinyl chloride SIN 846 Method 82 0DIS0308 <0.5N /L 11/2912022 Nitrate i Icy Nitrite Nitrogen EPA 353.2, Rev. 20°, 1903 < 0.02 /L 11/22/2022 Nitrate+Nitrite-Nitrogen EPA 353 2, Rev 2 0, 1993 3.27 mg1L 111 2 Nitrate Nitrogen subtraction Method 3.27 /L 1 /0 /20 2 Report 0. 2022-23234 Page 15 of 27 Environmental Chemists, • 6602 Windmill Way, Wilmington, NC 28405 • 910.392.0223 Lab *, 910.392.4424 Fax i 710 Bowsertown Road, Manteo, NC 27954 0 252.473.5702 lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 • 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info*environmentalchemists com Brunswick County Public Utilities Post Office Sox 249 Bolivia NC 28422 Attention: Date of Report: Dec 12, 2022 Customer PO #: Customer ID: 08100011 Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-57164 Site: well 11 11/21/2022 10:55 AM Water Chris House Test Method Results Date Analyzed Color cow Tan 11/21/2022 Depth to water, ft. Depth to water. Ft, 7.8 feet 11/21/2022 Ammonia Nitrogen EPA 350.1. Rev, 2 0, 1993 < 0.2 mg/L 12101 /2022 Gallons bailed before sampling Gallons Balled before sampling 5.0 gallons 11/21/2022 Odor oualitauve None 11/21/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 199 mg/L 11/22/2022 Temperature sM2550B-2010 19.1 C 11/21/2022 pH SM 4500 H B-2011 5.0 units 11/21/2022 Total Phosphorus SM 4500 P (F40.2011 0.36 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5310 B-2014 4.8 mg/L 11/22/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11/21/2022 Chloride SM4500 Cl E-2011 < 5 mg/L 11/23/2022 1, 1, 1,2-Tetrachloroethane SW 848 Method 82eoDI50308 <0.5 pg/L 11/29/2022 1,1,1-Trichloroethane SW 846 Method 8280015030E <0, 5 pg/L 11/29/2022 1, 1,2,2-Tetrach loroethane SW 848 Method 6260015030B <0.5 pg/L 11/29/2022 1,1,2-Trichloroethane sw 848 Method 8200Df5030B <0.5 pg/L 11/29/2022 1,1-Dichloroethane SW 846 Method a2e0D15030B <0.5 pg/L 11/29/2022 1,1-Dichloroethene SW 848 Method 6260D=30B <0.5 pg/L 11/29/2022 1,1-Dichloropropene sw 848 Method 8280D15030B <0.5 Pg/L 11/29/2022 1,2,3-Trichlorobenzene SW 848 Method 82BOD150308 <0.5 pg/L 11/29/2022 1,2,3-Trichloropropane sw 848 Method e250015030B <0.5 pg/L 11/29/2022 1,2,4-Trichlorobenzene sw 840 Method 82GOD15030B <0.5 pg/L 11 /29/2022 1,2,4-Trimethylbenzene SW 848 Method 82a0D150308 <0.5 pg/L 11/29/2022 1,2-Dibromo-3-Chloropropane SW 848 Method 8260DIS030B <0.5 pg/L 11/29/2022 1,2-Dibromoethane sw 848 Method 8260D150308 <0.5 pg/L 11/29/2022 1,2-Dichlorobenzene SW 848 Method 8260D15030B <0.5 pg/L 11/29/2022 Report N 2022-23234 Page 16 of 27 ANALYTICAL & CONSULTING CHEMISTS infb*environmentalchrrnistsxom Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO X: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID. Old Shallotte Monitoring Wells 1,2-Dichloroethane SW 846 Method 826OD15030B <0.5pg1L 11/29/2022 1,2-Dichfor opropane SW 046 Method 826OD150308 <0.5pg/L 11/29=22 1,3,5-Trimethylbenzene SW 846 Method 8260DI5030B <0. 5 pg/L 11/2912022 1,3-Dichlorobenzene SW 848 Method 02600=30B <0.5pg/L 11/29/2022 1.3-Dichloropropane SW 846 Method 8260DIS030B <0.5pg/L 11129/2022 1.4-Dichfor obenzene SW 545 Method 82SOD15030B <0.5 pg/L 1112912022 2,2-Dichfor opropane SW 848 Method 8200DI5030B <0.5pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 8260DI5030B <0.15 vg1L 11/2912022 4-Chlorotoluene SW 045 Method 82ODD15030B <0.5pg/L 11/2912022 Benzene SW 846 Method e280D6=8 <0.5 pg/L 11/2912022 Bromobenzene SW 846 Method 8280DI5030B <0.5pgil- 11129/2022 Bromochfor omethane SW 846 Method 8260DI5030B <0.5 pg1L 11/29/2022 Bromodichfor omethane SW 846 Method 02GOD15030B <0.5pg/L 11/29/2022 Bromoform SW 848 Method 826OD150308 <0.5 pg/L 11/2912022 Bromomethane SW 846 Method 826=6030 <0.5 pg/L 11/29/2022 Carbon tetrachloride SW 846 Method 0280015030B <0.5 pg/L 1112912022 Chlorobenzene SW 846 Method 828=50308 <0. 5 pg/L 11/29n022 Chloroethane SW 848 Method 82600160308 <0.5 pg/L 11/2912022 Chloroform SW 846 Method $26=50308 <0,5 pg/L 11/2912022 Chlore methane SW 046 Method 8260DI50308 <0.5 pg/L 11/29/2022 cis-1,2-Dichloroethene SW 84s Method 6260DI50308 <0.5 pg/L 11/29Q022 cis-1,3-Dichloropropene SIN 846 Method 82=150309 <0. 5 pg/L 11/29/2022 Dibromochloromethane SW 846 Method 8200DI50308 <0.5 pg/L 11/29/2022 Dibromomethane SW 045 Method 62SOD1503013 <0.5pg/L 11129/2022 Dichfor odifluoromethane SW $46 Method 6260DI50308 <0.5 pg/L 11/29/2022 Ethylbenzene SW 846 Method 826=603011 <0.5pg/L 11129/2022 Hexachlorobutadiene SW 046 Method 6260DI50300 <0.5 pg/L 11/2912022 lsopropylbenzene SW 846 Method 8260DI50308 <0.5pg/L 11/29f2022 M+ylen SW 846 Method 82SOD150308 <1.0 pg/L 11/29/2022 Methylene chloride SW 848 Method 6260DI5030B <0.5 lig/L 11129/2022 Report k 2022-23234 Page 17 of 27 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Date of Report: Dec 12, 2022 Customer PO #: Customer ID: 08100011 Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Naphthalene SW 846 Method 82600150308 <0,5 pg/L 11/29/2022 n-Butylbenzene SW 846 Method 0260D/50308 <0.5 pg/L 11/29/2022 n-Propylbenzene SW 846 Method 828OD/50308 <0.5 pg/L 11/29/2022 ortho-Xylene SW 846 Method 8280D/5030B <0.5 pg/L 11 /29/2022 p-lsopropyltoluene SW 846 MethodBMD150309 <0.5 pg/L 11/29/2022 sec-Butylbenzene SW 846 Method 8250DI5030B <0.5 pg/L 11/29/2022 Styrene SW 846 Method 82SOD15030B <0, 5 pg/L 11/29/2022 tert-Butylbenzene SW 846 Method 826OD/50308 <0 5 pg/L 11/29/2022 Tetrachloroethene SW 846 Method 82600/50308 <0, 5 pg/L 11 /29/2022 Toluene SW 846 Method 528OD/5030B <0,5 pg/L 11/29/2022 Trans-1 ,2-Dichloroethene SW 846 Method 828OD15030B <0.5 pg/L 11/29/2022 Trans-1 ,3-dichloropropene SW 846 Method 8260D150309 <0.5 pg/L 11/29/2022 Trichlomethene SW 846 Method 82600150308 <0.5 pg/L 11/29/2022 Trichlorofluoromethane SW 846 Method8200D15030B <0.5 pg/L 11/29/2022 Vinyl chloride SW 846 Method 828OD15030B <0.5 pg/L 11/29/2022 Nitrate Nitrogen (Calc) Nitrite Nitrogen EPA 353.2. Rev. 2.0, 1993 0.02 mg/L 11/22/2022 Nitrate+Nitrite-Nitrogen EPA353.2, Rev. 2.0,1993 0.39 mg/L 11/28/2022 Nitrate Nitrogen Subtraction Method 0.37 mglL 12/09/2022 Rep 2022-23234 Pape 18 of 27 J mem ""nvironental Chists, Inc. 121 1 6602 Windmill Way, Wilmington, NC 28405 * 910.392.D223 Lab e 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 a 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 2854D - 910-347.5843 Lab/Fax F-11 k' V V1 I DO Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID-. Collect Date/Time Matrix Sampled by 22-57155 Site: Well 12 11/2112022 11:09 AM Water Chris House Test Method Results Date Analyzed for Color Clear 11/21/2022 Depth to water, ft. Depth to Water, Ft. 8. 9 feet 11121 22 Ammonia Nitrogen EPA 350.1, Rev. 2.0,1993 < 0.2 mgIL 12/01/2022 Gallons balled before sampling Gallons Balled before sampling 5.0 gallons 11/21/2022 Odor Qualitative one 11/21/2022 Total Dissolved Solids (TDS) SM 2540 C-2ai5 93 mg/L 11/22/2022 Temperature SM 2550 B-2010 201 C 11/21/2022 pH SM 4500 H B-2011 5.3 units 11/21/2022 Total Phosphorus SM 4600 P (F-H).2011 < 0. 04 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5310 B-2014 3.5 mg/L 11/22/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml- 11121/2022 Chloride SM4500 Cl E-2011 9 mg/L 11/23/2022 1. 1, 1.2-Tetrachloroethane SW 848 Method 8260DI5030H <0.5 pg/L 11/29/2022 1, 1. 1 -Trichloroethane SW 645 Mathocl 6260DI5030B <0.5pg/L 11/29/2022 1, 1,2,2-Tetrachloroethane SW W Method 8260DIS0308 <0.5 pg/L 11/29/2022 1, 1, 2-Trichlorot hane SW 846 Method 82600150308 <0.5 pg/L 11/29/2022 11-Dichfor oethane SW 846 Method 0260DI50308 <0.5 pg/L 11/29/2022 1,1-Dichloroethene SW 846 Method 02BODIS0309 <0.5ligil- 1 1/29f2022 1,1-Dichloropropene SW 84a Method 0260D/5=8 <0.5pg/L 1112912022 1,2,3-Tdchlorobenzene SW 045 Method 828OU5030B <0.5pg/L 11/29/2022 1,2,3-Trichloropropane SW 046 Method 82SOD/5030B <0.5 pg/L 11/29/2022 1,2,4-Trichlorobenzene SW 846 Method 8260DI5030B <0.5 Wg/L 11/29/2022 1, 2,4-Trimethylbenzene SW 046 Method 828OD15030B <0.5 pg/L 1112912022 1,2-Dibromo-3-Chloropropane SW 846 Method 8280DIS030B <05pg/l- 11/29/2022 1,2-Dibromoethane SW 846 Method 8260DI5030B <0.5 (a IL 11/29/2022 1,2-Dichlorobenzene SW B45 Method 0n0W50308 <0. 5 pg/L 11/29/2022 ReponV 2022.23234 Page 19 of 27 21 ANALYTICAL & CONSULTING CHEMISTS Chemists,Environmental 660: Windmill Way, Wilmington, NC 28405 - r t 910.392.4424 Road,�Manteo, NC 27954 , 252.473.5702 255-A Wilmington Highway, Jacksonville, NC t Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dichloroethane SW 646 Method 8260015030B <0.5 pg/L 11/29/2022 1,2-Dichloropropane SW 046 Method 8260D150308 <0.5 pg/L 11/29/2022 1,3,5-Trimethylbenzene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 1, 3-Dichicrobenzene SW 846 Method BMD150308 <0.5 Ng/L 11/29/2022 1, 3-Dichloropropane SW 846 Method 82000150308 <0.5 pg/L 11/29/2022 1,4-Dichlorobenzene SW 846 Method 8200DIS0306 <0.5 pg1L 11/29/2022 2,2-Dichloropropane SW 846 Method8280D15030B <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 826OD15030B <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 846 Method 8280D15030B <0.5 pg/L 11/29/2022 Benzene SW 846 Method 8260016030E <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Bromochloromethane SW 846 Method 8260D/5030B <0.5 pg/L 11 /29/2022 Bromodichloromethane SW 646 Method 8266D15030B <0.5 pg/L 11/29/2022 Bromoform SW 846 Method 826OD150308 <0.5 pg/L 11/2912022 Bromomethane SW 846 Method 6260D15030B <0.5 pg/L 11/29/2022 Carbon tetrachloride SW 846 Method8260D15030B <0.5 pg/L 11/29/2022 Chlorobenzene SW 648 Method 82e0o150308 <0.5 pg/L 11/29/2022 Chloroethane SW e46 Method 8260Dr5030B <0.5 pg/L 11/29/2022 Chloroform SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 Chloromethane SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 cis-1,2-Dichioroethene SW 646 Method 825OD150308 <0.5 pg/L 11/29/2022 cis-1,3-Dichloropropene SW $45 Method 6260D150308 <0.5 pg/L 11 /29/2022 Dibromochloromethane SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Dibromomethane SW 545 Method 326OD150308 <0.5 pg/L 11/29/2022 Dichlorodifluoromethane SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Ethylbenzene SW 848 Method 8260015030E <0.5 pg/L 11/29/2022 Hexachlorobutadiene SW 846 Method 82BOD15030B <0.5 pg/L 11/29/2022 Isopropylbenzene SW 846 Method 826OD150308 <0.5 pg/L 11/29/2022 M+P Xylene SW 646 Method 8280D1503DB <1.0 pg/L 11/29/2022 Methylene chloride SW 846 Method 82600150308 <0.5 pg/L 11/29/2022 Report M: 2022-23234 — Pepe 20 of 27 Environmental Chemists, 6602 3- 910.392.0223 , 910.392.4424 Fax Wilmingtono' t 1 .347.5843 Lab/Fax ini`o4environmentalchernists.com Brunswick lic Utilities Date of Report: Dec 1, 2022 Post Office Box 249 Customer PO #: Bolivia 28422 Customer i: 08100011 Attention:2022-23234 Project ID: Old Shallotte Monitoring Wells Naphthalene SW 846Meto 1126aD150308 <0. U /L 11/29/2022 n-Butylbenzene SW NO Method 826013150 <0.51t /L 11/ /2 2 n-Propylbenzene SW 840 Method 82e=50300 <0.5 u /L 11/ 02 oh-yl ne SIN 84e Method 628DD15o3o8 < .5 p IL 11/ /02 p-Isopropyltoluene SW 846 Method 82601150308 <0.5 IL 11/ / 2 sec-Butylbenzene SW 846 Method 8260DI60308 <0. /L 11/29/2022 Styrene SW 846 M01hod 826aD150306 <0.5 u /L 11/2912022 tert-Butyl benzene SW 846 Method 8280015030B<0. /L 11/2 22 Tetrachloroethene SW 846 Method 820DD/50308 <0.5 u /L 11 022 Toluene SW 048 Mettod 8260015030B <0.5 p /L 11/ 0 2 Trans-1,2-Dichloroethene SW 848 Method 820OD150308 <0. /L 11/29/2022 Trans-1,3-dichloropropene SW 846Me 260D15030B <0.5 pgIL 11/ 2 Trichloroethene SW 040 Method8260D15030B <0. N /L 11/2912022 Trichlorofluoromethane SW 846 Method 82 ❑1503013 <0. W /L 11/29/2022 Vinyl chloride NO Method 8260D15030 <0. N IL 11/2 02 Nitrate it Icy Nitrite Nitrogen EPA 353.2, Rev 2 0.1993 < 0,02 /L 11/22/2022 Itf te+ itrite- itr en EPA 353.2, Rev 2.0, 1 3 0.36 /L 11/28/2022 Nitrate itr Subtraction Method 0. /L 12/09/2022 Deport 0, 2022.23234 Page 21 of 27 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Date of Report: Dec 12, 2022 Customer PO #: Customer ID: 08100011 Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Lab ID Sample ID: Collect DatelTime Matrix Sampled by 22-57156 Site: Well 14A 11/21/2022 12:11 PM Water Chris }louse Test Method Results Date Analyzed Color color Lt. Brown 11/21/2022 Depth to water, ft. Depth to Water, Ft 6.2 feet 11/21/2022 Ammonia Nitrogen EPA 350.1, Rev 2 0.1993 < 0.2 mg/L 12/01 /2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2022 Odor aualita0ve None 11121 /2022 Total Dissolved Solids (TDS) SM 2540 C-2015 37 mg/L 11/22/2022 Temperature SM 2550 8.2010 17.0 C 11/21/2022 pH SM 4500 H B-2011 6.1 units 11/21/2022 Total Phosphorus SM 45M P (F-H)-2011 < 0.04 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5340 B-2014 3.2 mg/L 11/22/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/i 00ml- 11/21/2022 Chloride SM4500 Cl E-2011 8 mg/L 11/23/2022 1, 1, 1,2-Tetrachloroethane SW 648 Method 82600150305 <0.5 pg/L 11/29/2022 1, 1. 1 -Trichloroethane SW 846 Method 828oD150308 <0.5 pg/L 11/29/2022 1,1,2,2-Tetrachloroethane SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 1,1,2-Trichloroethane SW 848 Method 82BOD150308 <0.5 pg/L 11/29/2022 1,1-Dichloroethane SW 846 Method 6260D/5030B <0.5 pg/L 11 /29/2022 1,1-Dichloroethene SW 846 Method 6280D/50308 <0.5 pg/L 11/29/2022 1,1-Dichloropropene SW 846 Method 82NDIS0308 <0.5 pg/L 11/29/2022 1,2,3-Trichlorobenzene SW 80 Method 8260DIS0308 <0.5 pg/L 11/29/2022 1,2,3-Trichloropropane SW $45 Method 8260015030B <0.5 pg/L 11/29/2022 1,2,4-Trichlorobenzene SW 046 Method 826ao15030B <0.5 pg/L 11/29/2022 1,2,4-Trimethylbenzene SW 846 Method 8200DIS0308 <0.5 pg/L 11/29/2022 1,2-Dibromo-3-Chloropropane SW 846 Method 8260015030B <0, 5 pg/L 11/29/2022 1,2-Dibromoethane SW 846 Method 82800/5030B <0.5 pg/L 11/29/2022 1,2-Dichlorobenzene SW845Method 8280Dl5030B <0.5pg/L 11/29/2022 Report S: 2022.23234 Page 22 of 27 Brunswick County Public Utilities Date of Report, Dec 12, 2022 Post Office Box 249 Customer PO M Bolivia NC 28422 Customer 10: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dichloroethane SW 848 Method 82BODIS030B <0.5 lig/L 11/2912022 1,2-Dichloropropane SW 646 Method 8280015030E <0.6pg/L 11/2912022 1,3,6-Trimethylbenzene SW 846 Method 8260DIS030D <0.5 pg/L 11129r2022 1,3-Dichfor obenzene SW 848 Method B26OD15030B <0.5pg/L 11/29/2022 1,3-Dichloropropane SW 848 Method 8200DI5030B <0.5 pg/L 11/29/2022 1,4-Dichlorot) enzene SW 846 Method 826OD15030B <0.5pg/L 11/2912022 2,2-Dichloropropane SW 846 Method 0260DIS030B <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 846 Method 0260015030B <0.5WgIL 11/29/2022 4-Chlorotoluene SW $46 Method 8286D/5030B <0.5 pg/L 11/29/2022 Benzene SW 846 Method 11260015030S <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method 826OD/5030B <0.5pg/L 11/29/2022 Brornochloromethane SW 846 Methad 6260DIS030B <0.5 pg/L 1112912022 Bromodichloromethane SW 845 Method 8260015030E <0.5pg/L 11/29/2022 Bromoform SW a46 Method a26OD/503013 <0.5 pg/L 11/29/2022 Bromomethane SW 846 Method 8260015030B <0.5pg/L 11/29/2022 Carbon tetrachloride SW 946 Method 8200DI50308 <0.5pg/L 11/29/2022 CMoro benzene SW 846 Method 02600150308 <0.5pg/L 11/29/2022 Chloroethane SW 846 Method 0260DI50300 <0.5 pg/L 11/29/2022 Chloroform SW 846 Method 8280DIS030B <0.5 pg/L 11/29/2022 Chloromethane SW 646 Method 8280DIS030B <0.5 Vg/L 11129/2022 cis-1,2-Dichloroethene SW 846 MaUhod 8260DI50306 <0. 5 Vg/L 11/29/2022 cis-1,3-Dichloropropene SW 840 Method 8260DIS0308 <0.5pg/L 11/29/2022 Dibromochloromethane SW 848 Method 8260DIS030B <0.5 pg/L 11129/2022 Dibromometit ane SW W Method 826OD160308 <0Zpg/L 11/29/2022 Dichlorodifluoromethane SW 046 Method 6280DI50308 <0.5 lig/L 11/29/2022 Ethylbenzene SW 845 Method 82600/5030B <0.5pg/L 11/29/2022 Hexachfor obutadiene SW 848 Method 8280DI5030B <0.5 pg/L 11/29/2022 Isopropyl benzene SW 846 Method 82800150308 <0,5pg/L 11/29/2022 M+ylen SW 846 Method 8260DI50308 <1.0 pg/L 11/29/2022 Methylene chloride SW 846 Method 826015D308 <0.5pg/L 11/29/2022 Report #:: 2022-23234 Page 23 of 27 Brunswick County Public Utilities Post Office Box 249 Bolivia NC 28422 Attention: Date of Report: Dec 12, 2022 Customer PO #: Customer ID: 08100011 Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells Naphthalene Sw 846 method 82BOD150308 0.52 pg/L 11/29/2022 Naphthalene present in opening method blank at 0.27ppb and closing method blank and 0,26ppb n-Butylbenzene SW 846 Method 826DD15030B <0.5 pg/L 11/29/2022 n-Propylbenzene sw 846 Method 8280o/5030B <0.5 pgIL 11/29/2022 ortho-Xylene SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 p-Isopropyltoluene SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 sec-Butylbenzene sw 646 Method 6260DIS0308 <0.5 pg/L 11/29/2022 Styrene SW 046 Method 6260D15030B <0.5 pg/L 11/29/2022 tent-Butylbenzene SW 648 Method 82eo015030B <0,5 pg/L 11/29/2022 Tetrachloroethene SW 846 Method 8280D15030B <0.5 pg/L 11/29/2022 Toluene sw 846 Method 8260015080E <0.5 pg/L 11/29/2022 Trans-1,2-Dichloroethene SW 848 Method 6260Dr5030B <0.5 pg/L 11/29/2022 Trans- 1,3-dich loropropene SW 846 Method 826OD150308 <0.5pgIL 11/29/2022 Trichloroethene SW 840 Method 8250D150308 <0.5 pg/L 11/29/2022 Trichloroftuoromethane sw 846 Method 82600/5030B <0.5 pg/L 11 /29/2022 Vinyl chloride SW 00 Method 8250D150300 <0.5 pg/L 11/2912022 Nitrate Nitrogen (Cale) Nitrite Nitrogen EPA 353 2, Rev, 2 0.1993 < 0.02 mg/L 11/22/2022 Nitrate+Nitrite-Nitrogen EPA 3532„Rev 2 0. 1093 0.34mgIL 11/28/2022 Nitrate Nitrogen Subtraction Method 0.34 mg/L 12/09/2022 ANALYTICAL & CONSULTING CHEMISTS info(iienvironmentalchemists.com . .......... ........ .. - - ---- Brunswick County Public Utilities Date of Report. Dec 12, 2022 Post Office Box 249 Customer Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project 10: Old Shallotte Monitoring Wells Lob ID Sample ID: Collect Dateffirrie Matrix Sampled by 22-57157 Site: Well 15 11/2112022 12:44 PM Water Chris House Test Method Results Date Analyzed Color Color Brown 11/21/2022 Depth to water, ft. Depth to Water, Ft 7.8 feet 11/21/2022 Ammonia Nitrogen EPA 350.1, Rev 2 0,1003 < 0.2 mg/L 12/01/2022 Gallons bailed before sampling Gallons Bailed before sampling 5.0 gallons 11/21/2022 Odor Qualitative one 11121/2022 Total Dissolved Solids (TDS) SM 2540 C-2015 165 mg1L 11/22/2022 Temperature SM 2650 B-2010 17.5 C 11/21/2022 pH SM 4 500 H B-2011 4.5 units 11/21/2022 Total Phosphorus SM 450D P (F-H)-2011 0.04 mg/L 12/02/2022 Total Organic Carbon (TOC) SM 5310 0.2014 7.9 mg/L 11/22/2022 Fecal Coliform SM 9222 D-2015 MF <1 Colonies/100ml. 11/21/2022 Chloride SM4500 Cl E-2011 45 mg/L 11/23/2022 1, 1, 1,2-Tetrachloroethane SW 048 Method 8280D/5030B <0.5 pg/L 11/29/2022 1, 1, 1 -Trichloroethane SW 846 Method 626OD15030B <0.5pg/L 11/29/2022 1, 1,2,2-Tetrachloroethans SW 846 Method 8260015030B <0.5 pg/L 11129/2022 1, 1,2-Trichloroethane SW 846 Method 0260DI5030B <0.5pg/L 11/29r2O22 1, 1 -Dichloroethane SW 846 Method 82600150308 <0.5pg/L 11/29/2022 1,1-Dichloroethene SW 946 Method 0260DI5030D <0.5 pg/L 11/29/2022 1,11-Dichloropropene SW 846 Melhod 02600150308 <0,51jg/L 11/29/2022 1,2,3-Trichlorobenzene SW 846 Method SMD16030B <0.5 wg/L 11129/2022 1,2,3-Trichloroprop ane SW 846 Method 8260DI5030B <0.5pg/L 11/29/2022 1,2,4-Trichlorobenzene SW 846 Method 8260016030B <0.5 pg/L 11/29/2022 1,2,4-Trimethylbenzene SW NO Method 82GOD/5030B <0.5pg/L 11129/2022 1,2-Dibromo-3-Chloropropane SW 046 Method 8260DI5030B <0.5pg/L 11129/2022 1.2-Dibromoethane SW 046 Method 82BOD/50308 <0.5 pg/L 11/29/2022 1,2-Dichlorobenzene SW 846 Method 82ND15030B <0.5pg/L 11/29/2022 Report #. 2022-23234 Page 25 of 27 Brunswick County Public Utilities Date of Report: Dec 12, 2022 Post Office Box 249 Customer PO #: Bolivia NC 28422 Customer ID: 08100011 Attention: Report #: 2022-23234 Project ID: Old Shallotte Monitoring Wells 1,2-Dichloroethane SW e4e Method 8260D150306 <0.5 pg/L 11/29/2022 1,2-Dichloropropane SW 846 Method 8260015030B <0.5 pg/L 11/29/2022 1, 3, 5-Trimethyl benzene SW 848 Method 8260DI50308 <0.5 pg/L 1 1/2912022 1, 3-Dichlorobenzene SW 846 Method 826aD15030B <0.5 pg/L 11/29/2022 1, 3-Dichloropropane SW 846 Method 8280D15030B <0.5 pg/L 11/29/2022 1,4-Dichlorobenzene SW 846 Method 8250D150308 <0.5 pg/L 11/29/2022 2,2-Dichloropropane SW 846 Method 825OD15030B <0.5 pg/L 11/29/2022 2-Chlorotoluene SW 848 Method 826OD16030B <0.5 pg/L 11/29/2022 4-Chlorotoluene SW 845 Method 8280D15030B <0.5 pg/L 11/29/2022 Benzene SW 846 Method 8280015030E <0.5 pg/L 11/29/2022 Bromobenzene SW 846 Method 826OD16030B <0.5 pg/L 11/29/2022 Bromochloromethane SW 846 Method 8260D15030B <0.5 pg/L 11 /29/2022 Bromadichloromethane SW 846 Method 8260D150308 <0.5 pg/L 11/29/2022 Bromoform SW 846 Method 8260D15030B <0.5 pg/L 11/29/2022 Bromomethane SW 846 Method 826OD150308 <0.5 pg/L 11/29/2022 Carbon tetrachloride SW 846 Method e260D150308 <0.5 pg/L 11/29t2022 Chlorobenzene SW 846 Method 8260D150308 <0.5 pg/L 11 /29/2022 Chloroethane SW 846 Method 8260015030E <0.5 pg/L 11/29/2022 Chloroform SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 Chloromethans SW 846 Method 8280D150308 <0.5 pg/L 11/29/2022 cis-1,2-Dichloroethene SW 846 Method 8260DIS0308 <0.5 pg/L 11/29/2022 cis-1,3-Dichloropropene SW 846 Method 828OD150308 <0.5pg/L 11/29/2022 Dibromochloromethane SW 848 Method 8280D150308 <0.5 pg/L 11/29/2022 Dibromomethane SW 848 Method 82WD150308 <0.5 pg/L 11/29/2022 Dichlorodifluoromethane SW 8" Method 8260D15030B <0.5 pg/L 11/29/2022 Ethylbenzene SW 846 Method 8280D150306 <0.5 pg/L 11/29/2022 Hexachlorobutadiens SW 846 Method 82GOD150308 <0.5 pg/L 11/29/2022 Isopropyibenzene SW 648 Method 8260D15030B <0.5 pg/L 11/29/2022 M+P Xylene SW 646 Method 828ODMO30B <1.0 pg/L 11/29/2022 Methylene chloride SW 846 Method 8260015030B <0.5 pg/L 11/29/2022 Report 8:: 2022-23234 Page 20 0127 tr t . , 1711111 r r t ANALYTICAL & CONSULTING CHEMISTS info(Oenv'tronrnentalcherstistLcom Brunswick IiUtilities c 12, 2022 Post Office Boxr Bolivia 2 ID: 08100011 Attention: 0-22 Project ID. Oldhalls a Monitoring Wells Naphthalene SW 846 Method 8260DISMOD <0.5 p /L 11/29/2022 n-Butylbenzene SW e48 Method 82600/5030 <0.5 li/ 1 1/2 / 02 n-Propylbenzene SW 846 Method 8260 30 < W /L 11/ 2 ortho-Xylene SW 046 Mo0Vd 6 0D/5030 <0.5 U /L 11/ 02 P-1sopropyltoluene SW 846 Method 62a0D/ ® < . u /L 11/ 022 see-Butylbenzene Swe4e Method 8260DI50308 <0.51J /L 11/ /2 Styrene SW 846 Method 82BOD/3030B<0.5 N / 11/29/2022 tert-Butyl benzene SW 846 Mellhod 6260D15o30 <0.5 N /L 11 /2 22 Tetrachloroethene SW 846 Method 6260D/5030 <0. /L 11/29/2022 Toluene SW 048 Method 8280D/50308 <0, iJ /L 11/2 /2 22 Trans-1,2-Dichloroathene SW 046 Method 82000/5030 <0.5 tr /L 11/2 0 2 Trans-1 3-dichloropropene SW 846 Method 82a013150308<0.5 /L 11/ 2 Trichloroethene SW 845 MOM 0260D/5030 <0.5 W /L 11/ /2022 Trichlorofluoromethane SW NO Method 8260D1 0 <0, 5 p 11/29/2022 Vinyl chloride SW 846 Method 8260D15030 <0.5 u / 11/29r2022 NitrogenNitrate I) Nitrite Nitrogen EPA 353.2, Rev 2.0, 1993 /L 11/22/2022 itr t + !trite- itr n EPA 353 2,. 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N,ilwll U IFeu"mrnimume@ Noiier U,� '%API N II n:na" U,."kaN"h"a Environmental h1c., Wilmington, NC iLab ift, 94 6602 VViiflidrnilf Way W9Nming4,:m, NC 2840,5' 9.10 - 3 9 2.0 22 3 Sarnple IR ce 1 pt IC: h ie c ki �s t N x-1..�..!'..( "S'lij Da R,epa b le r �j t �A� ....... 2022......... ................. .................... . ... ... ........ .. . . ........ . ................... . ................ U1 1::. v ff, 11) X1, v 2 ir ........................... Z ............... . . . ....... ................. ........ . ........ ............ .. . . . .... .... ... . ......... . ...................................... RN:n . ............. r- � "- CU nify # eal!ui on the cook r? ............ ........ ........................... I.- .. . .............. - . . .......... . . .......... . . .... ................................... . . . ................. . .................... . ....... . ................. . 2� fl`c�,,��toijyseaj; ..................... ....................... 5 ori—` - :::R —1 -.., i, — ................... . ............................... . ............ . ............... '.nt, were �,hey intact/unbroken",1 g4,ia� L1PrvpF,.,.,rah.jre rrcii 1111.11� Ic .. ...... . . ......... . ... ................. ... I Corrected ternperatuire upion receipt ................ 11 ... ... . ..... !� .......... . ..... . ............................ —.1..".1 . . ...... ............................... ......... . . . ...... . ........... . ............. —Ta,; : P Elottles Hov, tengPirature ta�,,,ev EJ FemperatUre B[FnOz ,i, —a —Ir � , -i , - ]X ................ . ... . ............. . ........ . ................... ........ . .............. . — - — ------------- - ................. —, . . ... .... .. . .. .... �R Gtm ID� Thomas e-d: t4e::� VNI 192 51:.1657 M G�.,m Correction Factor'C° 0.0 .. .. ...... .... . ... - .. . . ... . ............... ........ . ........... . .................. . ......................................... . . ........ . ................. . .................. . .... .......... . ......... 'YES , [3 Pin:) 3, If temp�:!rxftme of ux.:Aer exceeded 6T ..................... ........... . . . ....... d? viias Pr�.:)ject Ri ... . .............................. .•...................... . . . . ........ .... ............... ...... ./QA nfQffieP . .......................... . .................. . . ............. ............ . .... YES :0 NO 4. Weu,:� proper ctis'NAy proceajtji,es,(relinqui�.�Niel /i-�eceivea1) foHowed? . ... . ... . ... . ........................... . . ................. 11 ......... . .......... . .. .... YE's El 11,1110 5, Were samp[e M's listed an'the COU .. . .._..................I..... ............................................................................ L . ....... . ........ -1 .. . ................... . ........... . . ....... . ...... YES P110 6, Were SWTIPIes ID'S listed on sarnple co ta4-wrs? ................ I ........... ....... . . ........ .......... I'll .................................. . ........... . ....... . ......................... n `v`ES C Were CoHection date and fiffle Hsted on'O,w COT-,: . . . . .................. . . .................. ................. ::h .............................. . .......... .. ..................................... --.1 . ..... . ..... —11 ............................. I . ......... . . ........... YE 5 N 0 �8, Were tests to be perfOrg"ned fisted on the CO("'? ........ .... ..... . ........ ...... .... . ........................ . .................................... YES P1110 9,, Uid samples arrive in propii,��r contai'�— . .. . .. ............ .. ..... .... . ............ ................ .................................... . .................................................................................. r each test? . . . ......... . .......... . ..... . .............. . ...................................... —_ ........................ . .................... ............. fj YE 10, Did s,amp�es arrivo,:-� in good condftiior� f. r each test? I . ......... . . . . . ..... ................... — - — - - - ---------- ------------ - -------- - — - — - ------------- - . ................. .. . P,10 1'' , L 'Was adequate SaMple vokirr-w aiitakiakAe?` —were-�"ia' m "No-. s r,rN:: e ive d M t h i n P O-P, e i-ii o" I 11,10 . . . .......brnf,:. for reit,:jijested �i�.mts? . .. ............ . . . ........ . . ....... . ...... .. . 'YES: 0 P�l C) �1.3, Were achi preserved samp�es received at a pH f�:)f Q? 14, We�re cyankie si:]mp �es received at >12? . ....... . . . ..... . .............. ...................................... . . _ .. . .... . ................................................... . . . . . . ........... YES . ...... . . . ......... . ....... :.- ................................. . . . .......... . . .. . ........................... . ..... . .... . ............................ ........... ............................... . —YES ................. 0 NO 115. Were suffide &3mples receii%,Ped at a pH >9? . . ................... . . . . .. . ....................... . .. . 'Y FS YE S n N 0 16. Were NH3/TKN/PhewA receuved at a —cMo6ne residufl of . ... . ..... ................. . . . ......... ..... . ................................. ....................................... . ............ —..- i- 0 — . ....... . ........... YES I I NJ 0 1 7 We rip sulFde/Cya nk:Je receivtM at a ciT�,,)rinu ... ............. ..... ......... ..... ................. ....... residuM of,<115 nrl/L? .... ....... . ........ ........................... . .... ..............•—.1 —.11 . ... ....... YES 0 f,wthophosphate sarnples (Aterecl in thiefield viith�n 15 .............. .. ............ . ..... —.- ................ . ........ --.. f,*� �,? ii PH checked a:: t Iave of i and rei:iord,d .th 0-,6ecki:.!id for Chkwima i time..� of �iri a �Ois 3 NJ rec(Yided on th'e be n chsheet. S,m0e Preservatiom orr P/lust be comr—fleteld for any . ........... sarnp�e(s) incectly preserved or mifth hii-�,"i-.Wspaci �ample(s) .......... _ . ................. 1,vere received incorrectiv, prespented aid vivre �IXJJUSited accor6ng by aid6n,- (circ le one) � ,�y P H, SO.- HNO., i U NaOH Time preseniatk:m ff more than onle pr;em:1YPje is commentsi be,40v, .................. ......... . ..... . ......... zz ................................................ .......................................... — .. . . ...................................................... ................................................... ................ ........... . ............................................. P--:1 11 " C ".2 : ,-a Z 1 1 IL :V 1/68t�iles sampk'!ts'l . ......... ................... . . .......................... r'erll,'..�j%i,rip Citj i t h h � COMMEN, "rsr DOC,, QA.002 Rev 1. I® w N C C M M A O a 3 ? a m cCIL _ C r O m 3 � N n � o A m w a 3 m G Sample Type Composite 00 G) 0 G) 0 G) n G) 0 G) 0 or Grab G) -0 0 -0 0 Container (P or G) a Chlorine mglL m LAB ID / NUMBER �( NONE �( HCL A HNO7 M NAOH a �[ THIO 0 z OTHER z -n z a a 2 O { lu w o �, z o n = V1 m 3 " o z v rn =z MC m z �o v 00 0 z M �rn 0z z z �a =r n 2 rN N �rn m ic � esem N n Q ♦A z �// 4 v 4f NZm 0 c a m C3 W N o M m a o o c _ to 0 3 n � c CL "� c z ,�- 0 m $ v I ITF � O rrrr tt, g 5 --1:11— m CIL m Sample Type Composite G)oM0G)C)G)nQn00 or Grab 0-v o m a m c m o H Gi Container —LL I I I EP or Or' d Chlorine � mpfL CD Lae Id NUMBER )( NONE )( HCL x H2304 10 m Iwap HNO] M NAOH a )C THIO Q 2 OTHER a C -n z z O 0a v w o O m N [7 w v 0 0 r r n z z v 0 a z C v m zZ n M x 00 " Zm M a m oZ z e..' �a zr 0 =n m m T N C? 0 ♦f) it y G _ Z 0 0 3 N0 0_ W O C ID � cr: 0Z d CL_ 7 — m OD =r -' CL 1 .r � A Q � v n � O 7 � z Q o Sample Type Composite G) C7 G) C) G) 0 G) 0 G) 0 0 (� or Grab Container (P or G) p Chlorine to m LAB ID � NUMBER �( NONE }( HCL ro �( H28Osi X pm N Ip HNO3 m NAOH W � x THIO p z OTHER a C (D Z W O H N w a { 0_ 0 = y m w p � Z m smn M rn VE !-1 a i mom�mmmmoom■ .■ ..:.gym U 2 v m z C �0 0 z K m z v r 0 m 3 CD z 0