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NC Department of Environmental Quality | Division of Water Resources | Laboratory Certification Branch
4405 Reedy Creek Road | 1623 Mail Service Center | Raleigh, North Carolina 27699-1623
919-733-3908
June 10, 2022
5246
Mr. Roger Sullivan
Town of Stantonsburg WQ Lab
P.O. Box 10
Stantonsburg, NC 27883
Subject: North Carolina Wastewater/Groundwater Laboratory Certification Branch (NC
WW/GW LCB) Maintenance Inspection
Dear Mr. Sullivan:
Enclosed is a report for the inspection performed on May 3, 2022 by Jill Puff. Where Finding(s)
are cited in this report, a response is required. Within thirty days, please supply this office with a
written item for item description of how these Finding(s) were corrected. Please describe the steps
taken to prevent recurrence and include an implementation date for each corrective action. If the
Finding(s) cited in the enclosed report are not corrected, enforcement actions may be
recommended. For Certification maintenance, your laboratory must continue to carry out the
requirements set forth in 15A NCAC 02H .0800.
A copy of the laboratory’s Certified Parameter List at the time of the audit is attached. This list will
not reflect any changes made during the audit. Copies of the checklists completed during the
inspection may be requested from this office. Thank you for your cooperation during the
inspection. If you have questions or need additional information, please contact me at (919) 733-
3908 Ext. 251.
Sincerely,
Anna Ostendorff
Technical Assistance & Compliance Specialist
Division of Water Resources
Attachment
cc: Todd Crawford, Jill Puff, Master File #5246
On-Site Inspection Report
LABORATORY NAME: Town of Stantonsburg WQ Lab
NPDES PERMIT #: NC0057606
ADDRESS: 7655 Peacock Bridge Rd.
Stantonsburg, NC 27883
CERTIFICATE #: 5246
DATE OF INSPECTION: May 3, 2022
TYPE OF INSPECTION: Field Municipal Maintenance
AUDITOR(S): Jill Puff
LOCAL PERSON(S) CONTACTED:
Roger Sullivan
I. INTRODUCTION:
This laboratory was inspected by a representative of the North Carolina Wastewater/Groundwater Laboratory
Certification Branch (NC WW/GW LCB) to verify its compliance with the requirements of 15A NCAC 02H
.0800 for the analysis of compliance monitoring samples.
II. GENERAL COMMENTS:
The facility is neat and well organized and has all the equipment necessary to perform the analyses. The
lab supervisor assumed the role in 2020. Since then, he has written Standard Operating Procedures and
implemented a documented training program. He was forthcoming, responded well to suggestions from
the auditor and has already submitted preliminary corrective measures for review.
All required Proficiency Testing (PT) Samples for the 2022 PT Calendar Year have not yet been analyzed.
The laboratory is reminded that results must be received by this office directly from the vendor by September
30, 2022.
The laboratory is reminded that any time changes are made to laboratory procedures, QA/SOP
document(s) must be updated and relevant staff retrained. Staff must acknowledge that they have read
and understand the changes as part of the documented training program. The same requirements apply
when changes are made in response to Findings, Recommendations or Comments listed in this report, to
ensure the methods are being performed as stated, references to methods are accurate, and the QA
and/or SOP document(s) is in agreement with each approved practice, test, analysis, measurement,
monitoring procedure or regulatory requirement being used in the laboratory. In some instances, the
laboratory may need to create an SOP to document how new functions or policies will be implemented.
Revisions to the SOPs, based on the Findings, Comments and Recommendations within this
report must be submitted to this office by December 30, 2022.
The laboratory is also reminded that SOPs are required to be reviewed at least every two years and are
intended to describe procedures exactly as they are to be performed. Use of the word “should” is not
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appropriate when describing requirements (e.g., Quality Control (QC) frequency, acceptance criteria, etc.).
Evaluate all SOPs for the proper use of the word “should”.
Contracted analyses are performed by Environment 1, Inc. (Certification # 10).
Approved Procedure documents for the analysis of the facility’s currently certified Field Parameters were
provided at the time of the inspection.
III. FINDINGS, REQUIREMENTS, COMMENTS AND RECOMMENDATIONS:
Documentation
A. Finding: The laboratory benchsheet is lacking required documentation: meter calibration
time.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule. Ref:
15A NCAC 02H .0805 (g) (4).
Requirement: The following must be documented in indelible ink whenever sample analysis
is performed: Meter calibration and meter calibration time(s). Ref: NC WW/GW LCB Approved
Procedure for the Analysis of Dissolved Oxygen (DO).
B. Finding: The laboratory benchsheet is lacking required documentation: the method or
Standard Operating Procedure reference; the laboratory identification; the instrument
identification; the proper units of measure and all quality control assessments.
Requirement: All laboratories shall use printable laboratory benchsheets. Certified Data shall
be traceable to the associated sample analyses and shall consist of: the method or Standard
Operating Procedure; the laboratory identification; the instrument identification, the proper
units of measure; the quality control assessments. Each item shall be recorded each time
samples are analyzed. Analyses shall conform to methodologies found in Subparagraph (a)(1)
of this Rule. Ref: 15A NCAC 02H .0805 (g) (2) (A), (B), (C), (L) and (O).
Comment: The laboratory identification is documented on the calibration log but not on the
benchsheet.
Recommendation: It is recommended that the laboratory add the NC WW/GW LCB
Certification number (#5246) to the benchsheet to improve the legal defensibility of the data.
C. Finding: The laboratory is not documenting traceability information for purchased materials,
reagents and standards.
Requirement: 15A NCAC 02H .0805 (a)(7)(K) and (g)(7) requires laboratories to have a
documented system of traceability for the purchase, preparation, and use of all chemicals,
reagents, standards, and consumables. That system must include documentation of the
following information: Date received, Date Opened (in use), Vendor, Lot Number, and
Expiration Date (where specified). A system (e.g., traceable identifiers) must be in place
that links standard/reagent preparation information to analytical batches in which the
solutions are used. Documentation of solution preparation must include the analyst’s
initials, date of preparation, the volume or weight of standard(s) used, the solvent and final
volume of the solution. This information as well as the vendor and/or manufacturer, lot
number, and expiration date must be retained for primary standards, chemicals, reagents,
and materials used for a period of five years. Consumable materials such as pH buffers,
lots of pre-made standards and/or media, solids and bacteria filters, etc. are included in
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this requirement. Ref: NC WW/GW LCB Traceability Documentation Requirements for
Chemicals, Reagents, Standards and Consumables Policy.
Comment: The laboratory was provided with a traceability log at the time of inspection and
immediately placed it into service, entering information for Total Residual Chlorine (TRC)
reagents that had been received and opened on the previous day.
D. Finding: The laboratory is not documenting the temperature, barometric pressure and
salinity values used to calibrate the DO meter.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H .0805 (g) (4).
Requirement: The following must be documented in indelible ink whenever sample
analysis is performed: Calibration variables (temperature, elevation or barometric pressure
[in mmHg], and salinity). Ref: NC WW/GW LCB Approved Procedure for the Analysis of
Dissolved Oxygen (DO).
Comment: The calibration temperature and barometric pressure change daily and are
displayed on the screen of the DO meter. A salinity value of zero is programmed into the
meter and can be documented as a blanket statement on the benchsheet rather than
documenting each day.
E. Finding: Only one time for sample collection and analysis is documented without noting
samples are analyzed in situ.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H .0805 (g) (4).
Requirement: Date and time of sample analysis must be documented to verify the 15-
minute holding time is being met. Alternatively, one time may be documented for collection
and analysis with the notation that samples are measured in situ or immediately at the
sampling site. Ref: NC WW/GW LCB Approved Procedure for the Analysis of Dissolved
Oxygen and NC WW/GW LCB Approved Procedure for the Analysis of pH.
Requirement: The following must be documented in indelible ink whenever sample
analysis is performed: Date and time of sample collection; Date and time of sample analysis
- Alternatively, one time may be documented for collection and analysis with the notation
that samples are measured in situ or immediately at the sampling site (i.e., immediately
following collection at a location as near to the collection point as possible). When this ‘one
time’ option is used, state that the documented time is both collection and analysis time.
Ref: NC WW/GW LCB Approved Procedure for the Analysis of Temperature.
Comment: This Finding applies to DO, pH and Temperature.
Quality Control
F. Finding: Error corrections are not always properly performed.
Requirement: All documentation errors shall be corrected by drawing a single line through
the error so that the original entry remains legible. Entries shall not be obliterated by
erasures or markings. Wite-Out®, correction tape, or similar products designed to obliterate
documentation are not to be used; instead the correction shall be written adjacent to the
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error. The correction shall be initialed by the responsible individual and the date of change
documented. Ref: 15A NCAC 02H .0805 (g) (1).
Comment: On July 7, 2021, the pH, DO and Temperature reading corrections were not
dated. For the week of September 20 – 23, 2021, data were corrected but not initialed or
dated. On October 23, 2021, the pH value correction was not dated. On April 7, 2022, the
time of analysis was corrected but not initialed or dated.
G. Finding: An inconsistency was noted between the SOP and laboratory practice as follows:
The instructions for preparing the annual PT Sample specifies the use of volumetric
glassware.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
A copy of each analytical method or Approved Procedure and Standard Operating
Procedure shall be available to each analyst and available for review upon request by the
State Laboratory. Standard Operating Procedure documentation shall state the effective
date of the document and shall be reviewed every two years and updated if changes in
procedures are made. Each laboratory shall have a formal process to track and document
review dates and any revisions made in all Standard Operating Procedure documents.
Supporting Records shall be maintained as evidence that these practices are implemented.
Ref: 15A NCAC 02H .0805 (g) (4).
Comment: A 1000 mL beaker was used to dilute the Proficiency Testing Sample for TRC.
The laboratory is in possession of volumetric glassware and the analyst was instructed in
the proper use during the inspection.
H. Finding: The laboratory is not calibrating the mechanical volumetric liquid-dispensing
device used for critical measurements at least once every 12 months.
Requirement: Mechanical volumetric liquid-dispensing devices (e.g., fixed and adjustable
auto-pipettors and bottle-top dispensers) shall be calibrated at least once every twelve
months. Ref: 15A NCAC 02H .0805 (g) (10).
Comment: The pipettor is used for the preparation of the annual PT Sample for TRC.
Proficiency Testing
I. Finding: The laboratory is not documenting PT Sample analyses in the daily analysis records.
Requirement: All PT Sample analyses must be recorded in the daily analysis records as for
any Compliance Sample. This serves as the permanent laboratory record. Ref: Proficiency
Testing Requirements, February 19, 2020, Revision 5, Section 3.6.
Requirement: The laboratory shall retain all records necessary to facilitate historical
reconstruction of the analysis and reporting of analytical results for PT Samples. This means
the laboratory must have available and retain for five years [pursuant to 15A NCAC 02H .0805
(a) (7) (E) and (g) (1)] all of the raw data, including benchsheets, instrument printouts and
calibration data, for all PT Sample analyses and the associated QC analyses conducted by
all parameter methods. Ref: Proficiency Testing Requirements, February 19, 2020, Revision
5, Section 4.0.
Requirement: The analysis of Proficiency Testing (PT) Samples is designed to evaluate the
entire process used to routinely analyze and report Compliance Sample results. PT Samples
must be analyzed the same as Compliance Samples. Also, documentation must be made on
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the same benchsheets used for Compliance Samples. Ref: NC WW/GW LCB Proficiency
Testing Samples Analyzed and Documented Same as Compliance Samples Policy.
Comment: The results of PT testing were written on the instructions from the vendor packet.
The NC WW/GW LCB ‘Proficiency Testing Samples Analyzed and Documented Same as
Compliance Samples’ Policy was updated on March 9, 2022 to include the requirement that
PT Sample analysis be documented on the same benchsheet that is used for Compliance
Samples.
J. Finding: The laboratory is not documenting the preparation of PT Samples.
Requirement: PT Samples received as ampules are diluted according to the Accredited PT
Sample Provider’s instructions. It is important to remember to document the preparation of PT
Samples in a traceable log or other traceable format. The diluted PT Sample then becomes a
routine Compliance Sample and is added to a routine sample batch for analysis. No
documentation is needed for whole volume PT Samples which require no preparation,
however the instructions must be maintained. Ref: Proficiency Testing Requirements,
February 19, 2020, Revision 5, Section 3.6.
Comment: Dating and initialing the instruction sheet for each prepared PT Sample would
satisfy the documentation requirement.
Temperature – Standard Methods, 2550 B-2010 (Aqueous)
Comment: Temperature is being reported to 0.1°C on the Discharge Monitoring Report (DMR).
Recommendation: Unless greater precision is required by the permit or data receiving agency, it is
recommended that all temperatures reported for compliance monitoring, be reported in whole
numbers as recommended by the DWR’s Precision in Discharge Monitoring Reports document.
K. Finding for Immediate Response: The temperature sensors on the pH and DO meters
used to obtain reported temperature values have not been checked against a Reference
Temperature-Measuring Device every 12 months.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H 0805 (g) (4).
Requirement: All compliance temperature-measuring devices without a valid NIST
certificate must be checked initially and every 12 months against an NIST traceable
temperature-measuring device and the process documented. Verification documentation
must include the serial number of the device being checked. The serial number, stated
accuracy and expiration date of the Reference Temperature-Measuring Device used in the
comparison must also be documented. Verification data must be kept on file and be available
for inspection for 5 years. Note: International Organization for Standardization (ISO) 17025
compliant vendors or other Certified laboratories may provide assistance in meeting this
requirement. When an ISO compliant vendor provides this assistance, they must provide the
serial number, accuracy and calibration date for the Reference Temperature-Measuring
Device used for the verification. When a Certified laboratory provides this service, they must
provide a copy of the NIST traceable certificate of the Reference Temperature-Measuring
Device used for the verification. Ref: NC WW/GW LCB Approved Procedure for the Analysis
of Temperature. Please respond with the corrective actions taken to prevent further
recurrence of this Finding.
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Requirement: A Reference Temperature-Measuring Device is an NIST traceable
temperature-measuring device used only to verify the calibration of other temperature-
measuring devices. It must have a stated accuracy of ± 0.5 °C, be able to distinguish
temperature changes of 0.1 °C and equilibrate rapidly. Ref: NC WW/GW LCB Approved
Procedure for the Analysis of Temperature.
Requirement: To check a compliance temperature-measuring device, compare readings at
two temperatures that bracket the range of compliance samples routinely analyzed against a
Reference Temperature-Measuring Device and record all four readings. The readings from
both devices must agree within 0.5ºC. If they do not, the device may not be used for
temperature compliance monitoring. Ref: NC WW/GW LCB Approved Procedure for the
Analysis of Temperature.
Comment: A Notice of Finding for Immediate Response (NOFIR) was issued due to the
impact on reported data and so the laboratory would have the temperature sensor verified
more quickly than if waiting to first receive the inspection report to take corrective action. A
new NIST thermometer to be used as the Reference Temperature-Measuring Device was
ordered by the laboratory on April 19, 2022, with a targeted ship date of May 10, 2022. A
response due date of May 17, 2022 was negotiated, but this deadline was missed due to
supply chain issues. The laboratory made arrangements with Environment 1 to have the
verifications completed by May 20, 2022, and documentation demonstrating acceptable
verifications was submitted to the auditor on May 23, 2022.
L. Finding: Temperature sensor check readings for devices used for compliance monitoring
varied more than 0.5°C from the Reference Temperature-Measuring Device reading.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H .0805 (g) (4).
Requirement: To check a compliance temperature-measuring device, compare readings
at two temperatures that bracket the range of compliance samples routinely analyzed
against a Reference Temperature-Measuring Device and record all four readings. The
readings from both devices must agree within 0.5ºC. If they do not, the device may not
be used for temperature compliance monitoring. Ref: NC WW/GW LCB Approved
Procedure for the Analysis of Temperature.
Comment: In April 2021, four temperature sensors were checked and the readings varied
from 1.6 °C to 2.6°C from the Reference Temperature-Measuring Device. Upon
examination of the Reference Temperature-Measuring Device during the audit a separation
of the liquid in the column was discovered. The laboratory submitted documentation of
temperature verification by Environment 1 on May 23, 2022. Three sensors had acceptable
results, but a fourth did not and was taken out of service.
M. Finding: The compliance temperature-measuring device is not checked at two temperatures
that bracket the range of observed sample temperatures.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule. Ref:
15A NCAC 02H .0805 (g) (4).
Requirement: To check a compliance temperature-measuring device, compare readings at
two temperatures that bracket the range of compliance samples routinely analyzed against a
Reference Temperature-Measuring Device and record all four readings. The readings from
both devices must agree within 0.5 ºC. If they do not, the device may not be used for
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temperature compliance monitoring. Ref: NC WW/GW LCB Approved Procedure for the
Analysis of Temperature.
Comment: The probes used for compliance Temperature monitoring were only checked at a
single temperature.
pH – Standard Methods, 4500 H+ B-2011 (Aqueous)
N. Finding: Values were reported that exceed the method specified accuracy of 0.1 units.
Requirement: By careful use of a laboratory pH meter with good electrodes, a precision
of ±0.02 unit and an accuracy of ±0.05 unit can be achieved. However, ± 0.1 pH unit
represents the limit of accuracy under normal conditions, especially for measurement of
water and poorly buffered solutions. For this reason, report pH values to the nearest 0.1
pH unit. Ref: Standard Methods, 4500 H+ B-2011. (6).
Comment: The laboratory is reporting pH to two decimal places on the DMR.
Comment: Per PT Vendor instructions, the PT Sample results should be reported to two
decimal places, which is an exception to the requirement for Compliance Samples.
O. Finding: The laboratory is not analyzing a post-analysis check standard buffer when analyses
are performed at multiple sample sites in a single day.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H .0805 (g) (4).
Requirement: When performing analyses at multiple sample sites, a post-analysis
calibration verification using the check standard buffer must be analyzed at the end of the
run. It is recommended that a mid-day check standard buffer be analyzed when samples
are analyzed over an extended period of time. The post-analysis check standard buffer(s)
must read within ±0.1 S.U. or corrective actions must be taken. If recalibration is necessary,
all samples analyzed since the last acceptable calibration verification must be reanalyzed,
if possible. If samples cannot be reanalyzed, the data must be qualified. Ref: NC WW/GW
LCB Approved Procedure for the Analysis of pH.
Comment: The laboratory is not analyzing a post-analysis check standard buffer on dates
when analyses are performed at the upstream and downstream sites.
Total Residual Chlorine – Standard Methods, 4500 Cl G-2011 (Aqueous)
Comment: The facility utilizes UV disinfection and did not have compliance data available for
review. Proficiency Testing data was evaluated for this parameter.
P. Finding: The laboratory is not verifying the instrument’s Factory-set Calibration Curve
every 12 months.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule.
Ref: 15A NCAC 02H .0805 (g) (4).
Requirement: Annual Factory-set Calibration Curve Verification: This type of calibration
curve verification must be performed initially, at least every 12 months and any time the
instrument optics are serviced. Zero the instrument with a Calibration Blank and then
analyze a Method Blank and a series of five standards (do not use gel or sealed liquid
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standards for this purpose). The calibration standard values obtained must not vary by
more than ±10% from the known value for standard concentrations greater than or equal
to 50 μg/L and must not vary by more than ±25% from the known value for standard
concentrations less than 50 μg/L. Ref: NC WW/GW LCB Approved Procedure for the
Analysis of Total Residual Chlorine (DPD Colorimetric by SM 4500 Cl G-2011).
Comment: The factory-set calibration curve was last verified by Environment 1, Inc. on
June 10, 2020.
Q. Finding: The laboratory has not assigned the gel-type standard a true value.
Requirement: Laboratory procedures shall comply with Subparagraph (a)(1) of this Rule. Ref:
15A NCAC 02H .0805 (g) (4).
Requirement: Purchased “gel-type” or sealed liquid standards may be used only for daily
calibration curve verifications. These standards must have a true value assigned initially and
every 12 months thereafter. Ref: NC WW/GW LCB Approved Procedure for the Analysis of
Total Residual Chlorine (DPD Colorimetric by SM 4500 Cl G-2011). Please submit a copy
of the gel verification with the report reply.
Reporting
R. Finding: Data qualifiers from the contract laboratory reports are not being transferred to the
DMR.
Requirement: Each certified Field Laboratory shall be in accordance with Paragraph (e) of
this Rule. Ref: 15A NCAC 02H .0805 (g) (17).
Requirement: Reported data associated with quality control failures, improper sample
collection, holding time exceedances, or improper preservation shall be qualified as such. Ref:
15A NCAC 02H .0805 (e) (5).
Comment: The samples analyzed by Environment 1, Inc. on September 29, 2021, February
9, 2022, February 16, 2022 and February 22, 2022 were lacking the following qualifications
on the DMR: BOD – b. The Dilution water blank was >0.20 mg/L. The samples analyzed by
Environment 1, Inc on February 12, 2022, February 22, 2022 and February 23, 2022 were
lacking the following qualifications on the DMR: BOD – g. The GGA check standard was not
198 ± 30.5 mg/L.
IV. PAPER TRAIL INVESTIGATION:
The paper trail consisted of comparing original records (e.g., laboratory benchsheets, logbooks, etc.) and
contract laboratory reports to DMRs submitted to the North Carolina Division of Water Resources. Data
were reviewed for Stantonsburg WWTP (NPDES permit # NC0057606) for June 2021, September 2021
and December 2021. No transcription errors were observed. The facility appears to be doing a good job
of accurately transcribing data. However, as stated in Finding R, data qualifiers were not transferred from
the contract laboratory report.
To avoid questions of legality, it is recommended that you contact the appropriate Regional Office for
guidance as to whether an amended DMR(s) will be required. A copy of this report will be made available
to the Regional Office.
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V. CONCLUSIONS:
Correcting the above-cited Findings and implementing the Recommendations will help this laboratory to
produce quality data and meet Certification requirements. The inspector would like to thank the staff for
their assistance during the inspection and data review process. Please respond to all Findings and
include supporting documentation, implementation dates and steps taken to prevent recurrence
for each corrective action.
Report prepared by: Jill Puff Date: May 10, 2022
Report reviewed by: Jason Smith Date: May 11, 2022
Certificate Number:5246
Effective Date:1/1/2022
Expiration Date:12/31/2022
Lab Name:Town of Stantonsburg WQ Lab
Address:7655 Peacock Bridge Rd
Stantonsburg, NC 27883
North Carolina Wastewater/Groundwater Laboratory Certification
Certified Parameters Listing
Date of Last Amendment:7/17/2020
The above named laboratory, having duly met the requirements of 15A NCAC 2H.0800, is hereby certified for the measurement of the parameters listed below.
CERTIFIED PARAMETERS
INORGANIC
CHLORINE, TOTAL RESIDUAL
SM 4500 Cl G-2011 (Aqueous)
DISSOLVED OXYGEN
Hach 10360-2011, Rev. 1.2 (Aqueous)
pH
SM 4500 H+B-2011 (Aqueous)
TEMPERATURE
SM 2550 B-2010 (Aqueous)
This certification requires maintance of an acceptable quality assurance program, use of approved methodology, and satisfactory performance on evaluation samples. Laboratories are subject to civil penalties and/or decertification for infractions
as set forth in 15A NCAC 2H.0807.