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HomeMy WebLinkAboutWQ0002857_Monitoring - 10-2022_20221208Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * October Report Information WQ0002857 Piedmont Custom Meats WWTP Type * NDMR, NDAR-1, NDAR-2, NDMLR Confirmation Email Address:* Name of Submitter: * Signature: Date of submittal: Initial Review Year:* 2022 Upload Document* Piedmont Custom_Oct.pdf 3.07MB PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Jessica.Mize@pacelabs.com Jessica Mize jwd rA lip Reviewer: Gerald, Wanda 12/8/2022 This will be filled in automatically Is the project number correct?* WQ0002857 Is the monitoring report accepted?* Yes No Regional Office* Winston-Salem Reviewer: _anonymous Review Date: 12/20/2022 Page 1 of 3 NON -DISCHARGE WASTE NVATER MONITORING REPORT PERIMITNUNIBER: W 00102857 NIONTH: October YEAR: 2022 FACILITY NAME: Piedmont Custom Nleats WWTF COUNTY: Caswell now Mon�t.,iq Point: Effluent: D influent: !,Para,nieter M,oniterini PoinL EffluenL ED Influent: D Surface Water �SW): SW Code�Name� 'No 11 ...... ... .. . . . . . .. .. . ......... . ....... ... . . ......... Operator in Respo"sible Charge (ORC): (Aen" Price Grade: SI Phone: 336-996-2841 Check Box if ORC Has Changed: F-1 ORC Certif teation Ntj rnber: 987931/2f1771 Certified Laboratories (1): Pace Analvtical Services (2): Perso"(s) Collecting Samples: Glenn Price Mail ORIGINAL and Two COPIES to: ATI'N: Non4)ischnrge Compliance Unlit DE'NR (SI(r ;NATURE OFOPER,k FOR IN RESPONSIBLEC1111 Divkio"ofWater-Ouality By this signatorv, I vertify that this repwt is amirate and 1617 Maill Se -vice Center Complete to, the hest of lily k1lowledge. RAIAAGII, NC 27699-1617 DENR Form NDAR-1 (5/2003) NON DISCHARGE WASTEWATER MONITORING REPORT FACILITY STATUS: Please answer the following question: Compliant ,N) 1. Does all monitoring data and sampling frequencies meet permit requirements? If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (Signature of Permitee)V Date Baron Neal McDufiie (Authorized Agent) (Petmittee-Please print or type) 9683 Kerr's Chapel Road Gibsonville NC (Permittee Address) 01002 Arsenic 01022 Boron 00310 BOD5 01027 Cadmium 00916 Calcium 00940 Chloride 50060 Chlorine, Total Residual 01034 Chromium 00340 COD Baron Neal McDuffie (Name of Signing Official -Please print or type) Field Services Director (Pace Analytical Services) PARAMETER CODES 31504 _ Coliform, Total 00094 Conductivity 01042 Copper 00300 Dissolved Oxygen 31616 Fecal Coliform 01051 Lead 00927 Magnesium 71900 Mercury 00610 NH3 as N 01067 Nickel (Position or Title) 336-582-8247 (Phone Number) 00600 Nitrogen, Total 00630 NO2 & NO3 00620 NO3 00556 Oil & Grease W 09 PAN Plant Available 00400 pH 32730 Phenols 00665 Phosphorus, Total 00937 Potassium 00545 Settleable Matter 03/31/21 (Permit Exp. Date) 00929 Sodium 00931 SAR 00745 Sulfide 00515 TDS 00010 Temperature 00625 TKN 00680 TOC 00530 TSS/TSR 00076 idity 01092 Zinc Parameter Code assistance may be obtained by calling the Water -Quality Compliance/Enforcement Unit at (919) 733-5083, extension 529. The monthly average for Fecal Coliform is to be reported as a GEOMETRIC mean. Use only units designated in the reporting facility's permit for reporting data. * If signed by other than the Permittee, delegation of signatory authority must be on rile with the state per 15A NCAC 2B.0506 (b) (2) (D). Page 2 of — 3 NON -DISCHARGE APPUCAnON REpowr SPRAY IRRIGATION srn(S) THERE ARE TWO APPLICATION FIELDS PER PAGE. USE ADDIDTIONAL PAGES AS NEEDED PERMITNUMBER: XVQ0002857NION'ru: October YEAR: 2022 FACILITY NAME: Piedmont CustomMeatsWIWI 1, COUNTY: Caswell Formulas: Daily Loading (indies) NolurnL Apphed (gaVlonsl x O1336 (cubic fecrdpRon) x 12 (1ir)chG5Jficoj)j I [Area Sprayed (acresg x 43,560 (square feet/acqe6 or Nolurne Apphed 4ga0ons) / [Ama Sprayed (acresx 27,152 Maximum Hourly Loadmig (inches) = DaNy Loading (Inches) / ('Tirre rrigaled (Trinkiles) ? 60, (nUnUleslhour�l Montbiy Loading Iinches) 12 Month Fici Total Q6nches„ = Surn of this month's MorlitNy Loading p,nches) and pevio"s 11 nnointh's Monthly Loadings (inches) Average Weekly Loading �jrohws �= [M=Mly Loading (inchesmonth) i Number 0 days in the month 1V x 7 (days/week) "ANtaffier Codm C-clear, PU-partly cloudy, Cklmuhr, R-r a in, Sn-sno., Skl,eiir Sprayti,i-i(,-,,ttioit0l)erat(iriijilesi)omisit)IvCharge (OR(,'): (""IC111011-ice Phone: 336-996,-2841 ORC Certification Nuniber: 987931/20771 Check Box if ORC Has Changed: Mail ORIGINAL anal Two COPIES to: AIA'N; Non -Discharge ("orripliance Uiiit X_ — — ----- 1) 11, IN 11 (Sff',NA'1'URE OFOPERXMIZ IN RESPONSIBLE CILARGE) Division of NVater Qualit3 By this signature, I certify that this report is accurate and 1617 Mail Service Center complete to the best of m3 knowledge. RALEIGH, NC 27699-1617 DENR Form NDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. V 4. All buffer zones as specified in the permit were maintained during each application. L� S. The freeboard in the treatment and/or storage lagoon(s) was not less than the limit(s) specified in the permit. If the facility is non -compliant , please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." --'"l,_ /y- '�- )--�, Baron Neal McDuffie (Signature of Permitee)* Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Merit (Permittee-Please print or type) 9683 Kerr's Chanel Road Gibsonville. NC (Permittee Address) Field Services Director ( Pace Analytical Services) (Position or Title) 336-582-8247 (Phone Number) 03/31/21 (Permit Exp. Date) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per I SA NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) Page 3____ 0 f _. 3—.- NON-DISCIIARGE APPLICATION REPORT SPRAY IRRIGATION SITE(S) THERE ARE TWO APPLICATON FIELDS PER PAGE. USE ADDOTtONAL PAGES AS NEEDED PERMITNUMBEW INrQ00028-57 MONTH: October YEAR: 2022 FACILITY NAME: I"iedniont Custom Meats XVNN7'I'F COUNTY: Caswell ForMLJIaS: Daily Loading (inches) [VOUrne AppIked (plIong) x 0. 1 33G, (conic feel)gallon} x 12 (inchps)foot)]j i IArea SpiaryLd (,Ljciesp x u2l,MG0 (square feovacre) or (Volurne Appijed (gaiion5) (I/vei Sprayixl (acres)x 27,15� i9allons/a re c wch) Maximum Hourly Loading (inches) = Da0y Loading (inches)/ [Time it6gaTed tniinutesp 16D )rninwesihcurfl Morithly Loading (inches) -Surn of Daity Leading (inches) 12 Mondv Floafin g Total (inches) mm Sum of tHs rnonth's Monthly Loidnq {inches) and previous 11 monto's Monthly Loadwgs (rrlches) Average Weekly Loading (inches) = [Monthly Looding, (incheshnonth: / Number of days in the Month idoySInnonth )l x 7 d(Jayslwoek) -NN earlier Codes: C.-char, PC-paril) cloud), Chdoudy, Wraln, Sn-"io., Sksleet ORC Certification Number Mail 01ZIC1NA1. and *1')Ao COMES to: Al"I'N: Non-Discliar�e Compliance Unit DE NR Division of Water QuAty 1617 Mail Service Center RAI,EIGII, NC 27699-1617 Glenn price Phone: 987931/20771 CheckBox ifORCII-as C (SIGNA11RE, 01, OPE ' RVFOR IN RESPONSIB14' C'11, By this sigoalure, I certif�N that Ilds report is accurate and complete to Me best of any knovtedge. DENR Form NIDAR-1 (5/2003) FACILITY STATUS: Please indicate( by inserting Y(es) or N (o) in the appropriate box) whether the facility has been compliant with the following permit requirements: (Note: If a requirement does not apply to your facility put (NA) in the compliant box.) Compliant (Y,N) 1. The application rate(s) did not exceed the limit(s) specified in the permit. 'p 2. Adequate measures were taken to prevent wastewater runoff from the site(s). 3. A suitable vegetative cover was maintained on the site(s) in accordance with the permit. 4. All buffer zones as specified in the permit were maintained during each application. 5. The freeboard in the treatment and/or storage lagoon(s) was not less than the E2V limit(s) specified in the permit. If the facility is non -compliant, please explain in the space below the reason(s) the facility was not in compliance with its permit. Provide in your explanation the date(s) of the non-compliance and describe the corrective action(s) taken. Attach additional sheets if necessary. "I certify, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that a qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted is, to the best of my knowledge and belief true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 4 Y, 2- 3 Baron Neal McDuffie (Signa't6e of Permite * Date (Name of Signing Official -Please print or type) Baron Neal McDuffie (Authorized Agent) Field Services Director (Pace Analytical Services (Permittee-Please print or type) (Position or Title) 9683 Keres Chapel Road 336-582-8247 03/31/21 Gibsonville. NC (Phone Number) (Permit Exp. Date) (Permittee Address) * If signed by other than the Permittee, delegation of signatory authority must be on file with the state per 15A NCAC 2B.0506 (b) (2) (D). DENR Form NDAR-1 (5/2003) '01,07 9 1,,,.,*eAna1Xica1 wwwpacelabs.com November 14, 2022 Larry Moore Piedmont Custom Meats 430 NC Highway 49 South Asheboro, NC 27205 RE: Project: Piedmont Custom Meats Pace Project No.: 92633735 EMMMEM Pace Analytical Services, LLC 1377 South Park Drive Kernersvilie, NC 27284 (704)977-0981 Enclosed are the analytical results for sample(s) received by the Iaboratory on October 31, 2022. The results relate only to the samples included in tNs report. Results reported herein conform to 0-le applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted In the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical[ Services - Charlotte • Pace Analytical[ Services - Eden If you have any questuons concerning this report, please feel free to contact me. Sincerely, <71 4" Stephanie Knott stephanie.knott@pacelabs.com 704-977-0981 Project Manager Enclosures ,p TNs repotl shall riot be reproduced, except in full, wilhout the written consent of Pace Arialyfical Services, LLC. Pagel of37 1�5a'neAnalytical' www.pacelabs com I Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification M 12 South Carolina Laboratory ID: 99006 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 FloridaiNELAP Certification M E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification M 40 Pace Analytical Services Eden 205 East Meadow Road Suite A, Eden, NC 27288 North Carolina Drinking Water Certification M 37738 CERTIFICATIONS South Carolina Certification M 99006001 South Carolina Drinking Water Cert. M 99006003 Florida/NELAP Certification M E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 VirginiaNEL.AP Certification #: 460221 South Carolina Laboratory ID: 99030 South Carolina Certification M 99030001 VirginiaNELAP Certification M 460222 North Carolina Wastewater Certification M 633 YrginiaNELAP Certification M 460025 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 2 of 37 aceAnalytical e www.pacelaba.cam SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID Method Analysts Analytes Reported Laboratory 92633735001 MW-1 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 SRS 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 8260D CL 63 PASI-C EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92633735002 MW-4 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.01993 SRS 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 8260D CL 63 PASI-C EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 531OB-2014 MJP 1 PASI-A 92633735003 MW-5 SM 254OC-2015 DAW 1 PASI-E EPA 350.1 Rev 2.0 1993 SRS 1 PASI-E EPA 353.2 Rev 2.0 1993 SRS 1 PASI-E SM 9222D-2015 AED 1 PASI-E EPA 8260D CL 63 PASI-C EPA 120.1-1982 SMS 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 2 PASI-A SM 53108-2014 MJP 1 PASI-A 92633735004 Effluent SM 254OC-2015 DAW 1 PASI-E SM 254OD-2015 VLG 1 PASI-E EPA 353.2 Rev 2.01993 SRS 1 PASI-E SM 521OB-2016 SRS 1 PASI-E Colilert-18 SRS 1 PASI-E TKN+NO3+NO2 Calculation MDW 1 PASI-A EPA 300.0 Rev 2.1 1993 CDC 1 PASI-A EPA 350.1 Rev 2.01993 ARJ 1 PASI-A EPA 351.2 Rev 2.0 1993 MFO 1 PASI-A EPA 353.2 Rev 2.01993 KDF1 1 PASI-A EPA 365.1 Rev 2.0 1993 MDW 1 PASI-A PAS I -A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not to reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 3 of 37 1�5aaaceAnalytical J www.pacelabu m I SAMPLE ANALYTE COUNT Project: Piedmont Custom Meats Pace Project No.: 92633735 Lab ID Sample ID Method PAS I-E = Pace Analytical Services - Eden REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Analytes Analysts Reported Laboratory Page 4 of 37 ar �IaceAnalXical www.pacelabsxom ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-1 Lab lD: 92633735001 Collected: 10/31/22 11:13 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 338 mg/L 25.0 1 11/07/22 16:19 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia ND mg/L 0.10 1 11/03/2210:59 766441-7 363.2 NO2/NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 24.5 mg/L 0.40 10 11/01/22 11:28 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms ND CFU/100 mL 1.0 1 10/31/22 15:46 11/01/22 15:33 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone ND ug/L 25.0 1 11/10/22 08:06 67-64-1 Benzene ND ug/L 1.0 1 11/10/22 08:06 71-43-2 Bromobenzene ND ug/L 1.0 1 11/10/22 08:06 108-86-1 Bromochloromethane ND ug/L 1.0 1 11/10/22 08:06 74-97-5 Bromodichloromethane ND ug/L 1.0 1 11/10/22 08:06 75-27-4 Bromoform ND ug/L 1.0 1 11110/22 08:06 75-25-2 Bromomethane ND ug/L 2.0 1 11/10/22 08:06 74-83-9 2-Butanone (MEK) ND ug/L 5.0 1 11/10/22 08:06 78-93-3 Carbon tetrachloride ND ug/L 1.0 1 11/10/22 08:06 56-23-5 Chlorobenzene ND ug/L 1.0 1 11/10122 08:06 108-90-7 Chloroethane ND ug/L 1.0 1 11/10/22 08:06 75-00-3 IK,IL,v2 Chloroform ND ug/L 1.0 1 11/10122 08:06 67-66-3 Chloromethane ND ug/L 1.0 1 11110122 08:06 74-87-3 2-Chlorotoluene ND ug/L 1.0 1 11/10122 08:06 95-49-8 4-Chlorotoluene ND ug/L 1.0 1 11/10/22 08:06 10643-4 1,2-Dibromo-3-chloropropane ND ug/L 2.0 1 11/10122 08:06 96-12-8 Dibromochloromethane ND ug/L 1.0 1 11/10/22 08:06 12448-1 1,2-Dibromoethane(EDB) ND ug/L 1.0 1 11/10122 08:06 106-93.4 Dibromomethane ND ug/L 1.0 1 11/10/22 08:06 74-95-3 1,2-Dichlorobenzene ND ug/L 1.0 1 11/10/22 08:06 95-50-1 1,3-Dichlorobenzene ND ug/L 1.0 1 11/10/22 08:06 541-73-1 1,4-Dichlorobenzene ND ug/L 1.0 1 11/10122 08:06 10646-7 Dichlorodittuoromethane ND ug/L 1.0 1 11/10122 08:06 75-71-8 v2 1, 1 -Dichloroethane ND ug/L 1.0 1 11/10122 08:06 75-34-3 1,2-Dichloroethane ND ug/L 1.0 1 11/10/22 08:06 107-06-2 1,1-Dichloroethene ND ug/L 1.0 1 11/10/22 08:06 75-354 cis-1,2-Dichloroethene ND ug/L 1.0 1 11/10122 08:06 156-59-2 trans-1,2-Dichloroethene ND ug/L 1.0 1 11/10122 08:06 156-60-5 1,2-Dichloropropane ND ug/L 1.0 1 11/10/22 08:06 78-87-5 Date: 11/14/2022 02.43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, L-C. Page 5 of 37 aceAnalj6cal ( WWW.pacelatimin i ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-1 Parameters Lab ID: 92633735001 Collected: 10/31/22 11:13 Results Units Report Limit DF Received: 10/31/22 11:55 Matrix: Water Prepared Analyzed CAS No. Qual 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,3-Dichloropropane ND ug/L 1.0 1 11/10122 08:06 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/10/22 08:06 594-20-7 1,1-Dichloropropene ND ug/L 1.0 1 11/10/22 08:06 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/10122 08:06 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/10/22 08:06 10061-02-6 Ditsopropyl ether ND ug/L 1.0 1 11/10/22 08:06 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/10/22 08:06 100-414 Hexachloro-1,3-butadiene ND ug/L 2.0 1 11/10122 08:06 87-68-3 2-Hexanone ND ug/L 5.0 1 11/10/22 08:06 591-78-6 p-Isopropyttotuene ND ug/L 1.0 1 11/10122 08:06 99-87-6 Methylene Chloride ND ug/L 5.0 1 11/10/22 08:06 75-09-2 4-Methyl-2-pentanone(MIBK) ND ug/L 5.0 1 11/10/22 08:06 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/10/22 08:06 1634-04-4 Naphthalene ND ug/L 1.0 1 11/10/22 08:06 91-20-3 Styrene ND ug/L 1.0 1 11/10/22 08:06 100-42-5 1,1,1,2-Tetrachloroethane ND ug/L 1.0 1 11/10/22 08:06 630-20-6 1,1,2,2-Tetrachlorcethane ND ug/L 1.0 1 11/10/22 08:06 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/10/22 08:06 127-18-4 Toluene ND ug/L 1.0 1 11/10/22 08:06 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/10/22 08:06 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/10/22 08:06 120-82-1 1,1,1-Trichloroethane ND ug/L 1.0 1 11/10/22 08:06 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/10/22 08:06 79-00-5 Trichloroethene ND ug/L 1.0 1 11/10/22 08:06 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/10/22 08:06 75-69-4 1,2,3-Tdchloropropane ND ug/L 1.0 1 11/10/22 08:06 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/10/22 08:06 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/10/22 08:06 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/10/22 08:06 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/10/22 08:06 179601-23-1 o-Xylene ND ug/L 1.0 1 11/10/22 08:06 95-47-6 Surrogates 4-Bromofluorobenzene (S) 95 % 70-130 1 11/10/22 08:06 460-00-4 1,2-Dichloroethane-d4 (S) 91 % 70-130 1 11/10/22 08:06 17060-07-0 Toluene-d8 (S) 99 % 70-130 1 11/10/22 08:06 2037-26-5 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 527 umhos/cm 10.0 1 11/02/22 10:48 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 57.2 mg/L 1.0 1 11/02/2213:48 16887-00-6 Sulfate 1.1 mg/L 1.0 1 11/02/2213.48 14808-79-8 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 6 of 37 1�l5aceAnalOcal" www.pacelabs.com I ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilte, NC 27284 (704)977-0981 Sample: MWA Lab ID: 92633735001 Collected: 10/31/22 11:13 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310B TOC Analytical Method: SM 531 OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 1.9 mg/L 1.0 1 11/03/22 21:29 7440-44-0 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, without the written consent of Pace Analytical Services, I.I.C. Page 7 of 37 aceAnalytical www.pacelabs.com F i ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 t704)977-0981 Sample: MW-4 Parameters Lab ID: 92633735002 Collected: 10/31/22 10:27 Received: 10/31/22 11:55 Matrix: Water Results Units Report Limit OF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 540 mg/L 125 1 11/07122 16:23 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia 0.16 mg1L 0.10 1 11/03/22 10:45 7664-41-7 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 2.4 mg/L 0.040 1 11/01/22 11:06 14797-55-8 MBIO 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms NO CFU/100 mL 1.0 1 10/31/22 15:46 11/01/22 15:33 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone NO ug/L 25.0 1 11/10/22 08:25 67-64-1 Benzene NO ug/L 1.0 1 11/10/22 08:25 7143-2 Bromobenzene NO ug/L 1.0 1 11/10/22 08:25 108-86-1 Bromochloromethane NO ug/L 1.0 1 11/10/22 08:25 74-97-5 Bromodichloromethane NO ug/L 1.0 1 11/10/22 08:25 75-27-4 Bromoform NO ug/L 1.0 1 11/10/22 08:25 75-25-2 Bromomethane NO ug/L 2.0 1 11/10/22 08:25 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 11/10/22 08.25 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 11/10/22 08:25 56-23-5 Chlorobenzene NO ug/L 1.0 1 11/10/22 08:25 108-90-7 Chloroethane NO ug/L 1.0 1 11/10/22 08:25 75-00-3 IK,IL,v2 Chloroform NO ug/L 1.0 1 11/10/22 08:25 67-66-3 Chloromethane NO ug/L 1.0 1 11/10/22 08:25 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 11110/22 08:25 9549-8 4-Chlorotoluene NO ug/L 1.0 1 11110122 08:25 106434 1,2-Dibromo-3-chloropropane NO ug/L 2.0 1 11/10122 08:25 96-12-8 Dibromochloromethane NO ug/L 1.0 1 11/10122 08:25 12448-1 1,2-Dibromoethane (EDB) NO ug/L 1.0 1 11/10/22 08:25 106-93-4 Dibromomethane NO ug/L 1.0 1 11/10/22 08:25 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 1111012208:25 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 11/10/22 08:25 541-73-1 1,4-Dichlombenzene NO ug/L 1.0 1 11/1012208:25 10646-7 Dichlorodifluoromethane NO ug/L 1.0 1 11/10/22 08:25 75-71-8 v2 1, 1 -Dichloroethane NO ug/L 1.0 1 11/10/22 08:25 75-34-3 12-Dichloroethane NO ug/L 1.0 1 11/10/22 08:25 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 11/10/22 08:25 75-354 cis-1,2-Dichloroethene NO ugiL 1.0 1 11/10/22 08:25 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 11/10/22 08:25 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 11/10/22 08:25 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 8 of 37 aceAnalytical r wormpacelabaximi ANALYTICAL RESULTS Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Project: Piedmont Custom Meats Pace Project No.: 92633735 Sample: MW-4 Lab ID: 92633735002 Collected: 10/31122 10:27 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte 1,3-Dichloropropane ND ug/L 1.0 1 11/10/22 08:25 142-28-9 2,2-Dichloropropane ND ug/L 1.0 1 11/10/22 08:25 594-20-7 1, 1 -Dichloropropene ND ug/L 1.0 1 11/10/22 08:25 563-58-6 cis-1,3-Dichloropropene ND ug/L 1.0 1 11/10/22 08:25 10061-01-5 trans-1,3-Dichloropropene ND ug/L 1.0 1 11/10/22 08:25 10061-02-6 Diisopropyl ether ND ug/L 1.0 1 11/10/22 08:25 108-20-3 Ethylbenzene ND ug/L 1.0 1 11/10/22 08:25 100-414 Hexachloro-1,3-butadiene ND ug/L 2.0 1 11/10/22 08:25 87-68-3 2-Hexanone ND ug/L 5.0 1 11/10/22 08:25 591-78-6 p-Isopropyltoluene ND ug/L 1.0 1 11/10/22 08:25 99417-6 Methylene Chloride ND ug/L 5.0 1 11/10/22 08:25 75-09-2 4-Methyl-2-pentanone (MIBK) ND ug/L 5.0 1 11/10/22 08:25 108-10-1 Methyl-tert-butyl ether ND ug/L 1.0 1 11/10/22 08:25 1634-04-4 Naphthalene ND ug/L 1.0 1 11/10/22 08:25 91-20-3 Styrene ND ug/L 1.0 1 11/10/22 08:25 100-42-5 1,1,1,2 Tetrachloroethane ND ug/L 1.0 1 11/10/22 08.25 630-20-6 1,1,2,2-Tetrachloroethane ND ug/L 1.0 1 11/10/22 08:25 79-34-5 Tetrachloroethene ND ug/L 1.0 1 11/10/22 08:25 127-18-4 Toluene ND ug/L 1.0 1 11/10/22 08:25 108-88-3 1,2,3-Trichlorobenzene ND ug/L 1.0 1 11/10/22 08:25 87-61-6 1,2,4-Trichlorobenzene ND ug/L 1.0 1 11/10/22 08:25 120-82-1 1, 1. 1 -Trichloroethane ND ug/L 1.0 1 11/10/22 08:25 71-55-6 1,1,2-Trichloroethane ND ug/L 1.0 1 11/10/22 08:25 79-00-5 Trichloroethene ND ug/L 1.0 1 11/10/22 08:25 79-01-6 Trichlorofluoromethane ND ug/L 1.0 1 11/10/22 08:25 75-69-4 1,2,3-Trichloropropane ND ug/L 1.0 1 11/10/22 08:25 96-18-4 Vinyl acetate ND ug/L 2.0 1 11/10/22 08:25 108-05-4 Vinyl chloride ND ug/L 1.0 1 11/10/22 08.25 75-01-4 Xylene (Total) ND ug/L 1.0 1 11/10/22 08:25 1330-20-7 m&p-Xylene ND ug/L 2.0 1 11/10/22 08:25 179601-23-1 o-Xylene ND ug/L 1.0 1 11/10/22 08:25 95-47-6 Surrogates 4-Bromofluorobenzene (S) 94 % 70-130 1 11/10/22 08:25 460-00-4 1,2-Dichloroethane-d4 (S) 89 % 70-130 1 11/10/22 08:25 17060-07-0 Toluene-d8 (S) 100 % 70-130 1 11/10/22 08:25 2037-26-5 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 1010 umhos/cm 10.0 1 11/02/22 10:50 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 241 mg/L 5.0 5 11/03/22 04:17 16887-00-6 Sulfate 2.1 mg/L 1.0 1 11/02/2214:04 14808-79-8 REPORT OF LABORATORY ANALYSIS This report shalt not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 9 of 37 aceAnalytical e www.paealaEs.eam 1 I ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-4 Lab ID: 92633735002 Collected: 10/31/22 10:27 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 5310E TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon ND mg/L 1.0 1 11/03/22 21:50 7440-44-0 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 10 of 37 1�;a'cieAnaljftal" wuwa.pscelabLcom / t ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (704)977-0981 Sample: MW-5 Parameters Lab ID: 92633735003 Collected: 10/31/22 10:46 Results Units Report Limit OF Received: 10/31/22 11:55 Matrix: Water Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 254OC-2015 Pace Analytical Services - Eden Total Dissolved Solids 268 mg/L 50.0 1 11107/22 16:24 350.1 Ammonia EDN Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Ammonia NO mg/L 0.10 1 11/03122 10:51 7664-41-7 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2,0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 1.4 mg/L 0.040 1 11/01/22 11:07 14797-55-8 MB10 9222D Fecal Coliform EDN Analytical Method: SM 9222D-2015 Preparation Method: SM 9222D-2015 Pace Analytical Services - Eden Fecal Coliforms NO CFU/100 mL 1.0 1 10/31/22 15:46 11/01/22 15:33 8260D MSV Low Level Analytical Method: EPA 8260D Pace Analytical Services - Charlotte Acetone NO ug/L 25.0 1 11/10/22 08:43 67-64-1 Benzene NO ug/L 1.0 1 11/10/22 08:43 71-43-2 Bromobenzene NO ug/L 1.0 1 11/10/22 08:43 108-86-1 Bromochloromethane NO ug/L 1.0 1 11/10/22 08:43 74-97-5 Bromodichloromethane NO ug/L 1.0 1 11/10/22 08:43 75-27-4 Bromoform NO ug/L 1.0 1 11/10/22 08:43 75-25-2 Bromomethane NO ug/L 2.0 1 11/10/22 08:43 74-83-9 2-Butanone (MEK) NO ug/L 5.0 1 11/10/22 08:43 78-93-3 Carbon tetrachloride NO ug/L 1.0 1 11/10/22 08:43 56-23-5 Chlorobenzene NO ug/L 1.0 1 11/10/22 68:43 108-90-7 Chloroethane NO ug/L 1.0 1 11/10/22 08:43 75-00-3 IK,IL,v2 Chloroform NO ug/L 1.0 1 11/10/22 08:43 67-66-3 Chloromethane NO ug/L 1.0 1 11/10/22 08.43 74-87-3 2-Chlorotoluene NO ug/L 1.0 1 11/10/22 08:43 95-49-8 4-Chlorotoluene NO ug/L 1.0 1 11/10/22 08:43 106-43-4 1,2-Dibromo-3-chloropropane NO ug/L 2.0 1 11/10/22 08:43 96-12-8 Dibromochloromethane NO ug/L 1.0 / 11/10/22 08:43 124-48-1 1,2-Dibromoethane (EDB) NO ug/L 1.0 1 11/10/22 08:43 106-93-4 Dibromomethane NO ug/L 1.0 1 11/10/22 08:43 74-95-3 1,2-Dichlorobenzene NO ug/L 1.0 1 11/10/22 08:43 95-50-1 1,3-Dichlorobenzene NO ug/L 1.0 1 11/10/22 08:43 541-73-1 1,4-Dichlorobenzene NO ug/L 1.0 1 11/10/22 08:43 106-46-7 Dichlorodifluoromethane NO ug/L 1.0 1 11/10/22 08:43 75-71-8 v2 1,1-Dichloroethane NO ug/L 1.0 1 11/10/22 08:43 75-34-3 1,2-Dichloroethane NO ug/L 1.0 1 11/1012208.43 107-06-2 1,1-Dichloroethene NO ug/L 1.0 1 11/10/22 08:43 75-35-4 cis-1,2-Dichloroethene NO ug/L 1.0 1 11/10/22 08:43 156-59-2 trans-1,2-Dichloroethene NO ug/L 1.0 1 11/10/22 08:43 156-60-5 1,2-Dichloropropane NO ug/L 1.0 1 11/10/22 08:43 78-87-5 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 11 of 37 /5a'ceAna1j&ca10 j www.pacetabs.eem ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: MW-5 Lab ID: 92633735003 Collected: 10/31/22 10:46 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8260D MSV Low Level 1,3-Dichloropropane 2,2-Dichioropropane 1, 1 -Dichloropropene cis-1,3-Dichloropropene trans-1,3-Dichloropropene Diisopropyl ether Ethylbenzene Hexachloro-1,3-butadiene 2-Hexanone p-Isopropyltoluene Methylene Chloride 4-Methyl-2-pentanone (MIRK) Methyl-tert-butyl ether Naphthalene Styrene 1,1,1,2 Tetrachloroethane 1,1,2,2-Tetrachloroethane Tetrachloroethene Toluene 1,2,3-Trichlorobenzene 1,2,4-Trichlorobenzene 1, 1, 1 -Trichloroethane 1,1,2-Trichloroethane Trichloroethene Trichlorofluoromethane 1,2,3-Trichloropropane Vinyl acetate Vinyl chloride Xylene (Total) m&p-Xylene o-Xylene Surrogates 4-Bromofluorobenzene (S) 1,2-Dichloroethane-d4 (S) Toluene-d8 (S) Analytical Method: EPA 8260D Pace Analytical Services - Charlotte NO ug/L NO ug/L NO ug1L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug1L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L NO ug/L 93 % 94 % 99 % 1.0 1 11110/22 08:43 142-28-9 1.0 1 11110122 08:43 594-20-7 1.0 1 11/10122 08:43 563-58-6 1.0 1 11110/22 08:43 10061-01-5 1.0 1 11/10122 08:43 10061-02-6 1.0 1 11/10122 08:43 108-20-3 1.0 1 11/10122 08:43 100-41-4 2.0 1 11/10/22 08:43 87-68-3 5.0 1 11/10122 08:43 591-78-6 1.0 1 11/10/22 08:43 99-87-6 5.0 1 11/10/22 08:43 75-09-2 5.0 1 11/10/22 08:43 108-10-1 1.0 1 11/10/22 08:43 1634-04-4 1.0 1 11/10/22 08:43 91-20-3 1.0 1 11/10/22 08:43 100-42-5 1.0 1 11/10/22 08.43 630-20-6 1.0 1 11/10/22 08:43 79-34-5 1.0 1 11/10/22 08:43 127-18-4 1.0 1 11/10/22 08:43 108-88-3 1.0 1 11/10/22 08.43 87-61-6 1.0 1 11/10/22 08A3 120-82-1 1.0 1 11/10/22 08A3 71-55-6 1.0 1 11/10/22 08A3 79-00-5 1.0 1 11/10/22 08A3 79-01-6 1.0 1 11/10/22 08A3 75-69-4 1.0 1 11/10/22 08A3 96-18-4 2.0 1 11/10/22 08A3 108-05-4 1.0 1 11/10/22 08A3 75-01-4 1.0 1 11/10/22 08:43 1330-20-7 2.0 1 11/10/22 08.43 179601-23-1 1.0 1 11/10/22 08A3 95-47-6 70-130 1 70-130 1 70-130 1 120.1 Specific Conductance Analytical Method: EPA 120.1-1982 Pace Analytical Services -Asheville Specific Conductance 585 umhos/cm 10.0 1 300.0 IC Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 139 mg/L 3.0 3 Sulfate NO mg/L 1.0 1 REPORT OF LABORATORY ANALYSIS 11/10/22 08:43 460-00-4 11/10/22 08.43 17060-07-0 11/10/22 08A3 2037-26-5 11 /02/22 10:52 11 /03/22 04:32 16887-00-6 11 /02/22 14:19 14808-79-8 This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 12 of 37 1�5a'cmnalyfical" www.pacelabs.com f I ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 Sample: MW-5 Lab ID: 92633735003 Collected: 10/31122 10:46 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 53108 TOC Analytical Method: SM 531OB-2014 Pace Analytical Services -Asheville Total Organic Carbon 4.7 mg/L 1.0 1 11/03/22 22:38 7440-44-0 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.L.C. Page 13 of 37 2aaeAnalXical www.pacelabs.com i ANALYTICAL RESULTS Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Sample: Effluent Lab ID: 92633735004 Collected: 10/31/22 10:54 Received: 10/31/22 11:55 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 2540C Total Dissolved Solids Analytical Method: SM 2540C-2015 Pace Analytical Services - Eden Total Dissolved Solids 454 mg/L 50.0 1 11/07/22 16:27 25400 Total Suspended Solids Analytical Method: SM 2540D-2015 Pace Analytical Services - Eden Total Suspended Solids 80.0 mg/L 26.3 1 11/01/22 15:23 353.2 N021NO3 unpres EDN Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Eden Nitrogen, Nitrate 11.2 mg/L 0.20 5 11/01/22 11:29 14797-55-8 5210B BOD, 5 day EDN Analytical Method: SM 5210B-2016 Preparation Method: SM 521OB-2016 Pace Analytical Services - Eden BOD, 5 day 74.0 mg/L 2.0 1 11101/22 10:22 11/06122 10:12 R6 Colilert-18 Fecal Coliform EDN Analytical Method: Colilert-18 Preparation Method: Colilert-18 Pace Analytical Services - Eden Fecal Coliforms 2420 MPN/100mL 1.0 1 10/31/22 16:45 11/01122 11:17 El Total Nitrogen Calculation Analytical Method: TKN+NO3+NO2 Calculation Pace Analytical Services -Asheville Total Nitrogen 23.2 mg/L 0.040 1 11/10/22 15:18 300.01C Anions 28 Days Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services -Asheville Chloride 104 mg/L 2.0 2 11103122 04:48 16887-00-6 350.1 Ammonia Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville Nitrogen, Ammonia 0.10 mg/L 0.10 1 11/07/2215:13 7664-41-7 351.2 Total Kjeldahl Nitrogen Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, Kjeldahl, Total 11.5 mg/L 0.50 1 11104/22 16:15 11/10122 05:23 7727-37-9 353.2 Nitrogen, NO2/NO3 pres. Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services -Asheville Nitrogen, NO2 plus NO3 11.7 mg/L 0.40 10 11110122 09:52 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Rev 2.0 1993 Preparation Method: EPA 365.1 Rev 2.0 1993 Pace Analytical Services -Asheville Phosphorus 1.7 mg/L 0.050 1 11/03/2213:00 11/0312218:49 7723-14-0 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 14 of 37 00007" 0 aceAnalXical www.pacalabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 735295 Analysis Method: SM 254OC-2015 QC Batch Method: SM 254OC-2015 Analysis Description: 2540C Total Dissolved Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 METHOD BLANK: 3826833 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Dissolved Solids mg/L ND 25.0 11/07/22 16:14 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3826834 Spike LCS LCS % Rec Parameter Units Cone. Result % Rae Limits Qualifiers Total Dissolved Solids mg/L 250 252 101 90-110 SAMPLE DUPLICATE: 3826835 92633735001 Dup Parameter Units Result Result RPD Qualifiers Total Dissolved Solids mg/L 338 333 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 15 of 37 1eAnalyficalo www.pacelabs.ccm Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734070 Analysis Method: SM 254OD-2015 QC Batch Method: SM 2WD-2015 Analysis Description: 2540D Total Suspended Solids Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735004 METHOD BLANK: 3820650 Associated Lab Samples: 92633735004 Parameter Units Total Suspended Solids mg/L LABORATORY CONTROL SAMPLE: 3820651 Parameter Units Total Suspended Solids mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.5 11/01/2215:17 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 250 246 98 90-110 SAMPLE DUPLICATE: 3820652 92633792003 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 581 554 5 SAMPLE DUPLICATE: 3820653 92633904001 Dup Parameter Units Result Result RPD Qualifiers Total Suspended Solids mg/L 2240 2600 15 Results presented an this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except In full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 16 of 37 I�VaceAnaljilicalm t twtww.pacclabs.com r QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734588 Analysis Method: EPA 350.1 Rev 2.0 1993 QC Batch Method: EPA 350.1 Rev 2.01993 Analysis Description: 350.1 Ammonia, EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735001, 92633735002, 92633735003 METHOD BLANK: 3823174 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Ammonia mg/L ND 0.10 11/03/22 10:33 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3823175 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.0 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823176 3823177 MS MSD 92633850001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Quai Nitrogen, Ammonia mg/L 0.17 5 5 5.3 5.3 102 102 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823178 3823179 MS MSD 92633907007 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.1 5.1 103 103 90-110 0 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 17 of 37 1�5a'ne Analytical WWW.paeelabs.eem / QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 733976 Analysis Method: EPA 353.2 Rev 2.01993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, Unpres. EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 METHOD BLANK: 3820141 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Nitrate mg/L ND 0.040 11/01/22 10:52 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3820142 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Nitrogen, Nitrate mg/L 1.5 1.5 101 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3820143 MS 92633759001 Spike Parameter Units Result Conc. Nitrogen, Nitrate mg/L 2.6 1.5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3820145 MS 92633759002 Spike Parameter Units Result Conc. Nitrogen, Nitrate mg/L ND 1.5 3820144 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 1.5 4.1 4.1 99 99 90-110 0 3820146 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec ale Rec Limits RPD 1.5 1.5 1.5 102 102 90-110 0 Results presented an this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Quaff I0 Page 18 of 37 aceAnalytical e www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 733970 Analysis Method: SM 521OB-2016 QC Batch Method: SM 521OB-2016 Analysis Description: 5210E BOD, 5 day Final EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735004 METHOD BLANK: 3820105 Associated Lab Samples: 92633735004 Parameter Units BOD, 5 day mg/L Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 11/06/22 09:55 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3820106 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers BOD, 5 day mg/L 198 205 104 84.6-115 SAMPLE DUPLICATE: 3820108 92633712001 Dup Parameter Units Result Result RPD Qualifiers BOD, 5 day mg/L 2290 2220 3 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 19 of 37 aceAna1j6ca1" www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 OC Batch: 733947 Analysis Method: SM 9222D-2015 QC Batch Method: SM 9222D-2015 Analysis Description: 9222D Fecal Coliform(MF)-EDN Laboratory: Pace Analytical Services - Eden Associated Lab Samples: 92633735001, 92633735002, 92633735003 METHOD BLANK: 3820043 Matrix: Water Associated Lab Samples: 92633735001, 92633735002.92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 11/01122 15:33 METHOD BLANK: 3820046 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 11/01/22 15:33 METHOD BLANK: 3820047 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU/100 mL ND 1.0 11/01/22 15:33 METHOD BLANK: 3820048 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Fecal Coliforms CFU1100 mL 1.0 1.0 11/01/22 15:33 C8 SAMPLE DUPLICATE: 3820044 92633759001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 56.0 45.0 22 SAMPLE DUPLICATE: 3820045 92633759002 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms CFU/100 mL 28.0 49.0 55 D6 Results presented on this page are In the units indicated by the 'Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 20 of 37 5aiCceAnalytical j WWW.paceiabs.ecm i Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 733894 QC Batch Method: Colilert-18 Associated Lab Samples: 92633735004 QUALITY CONTROL DATA Analysis Method: Colilert-18 Analysis Description: Colilert-18 Fecal Coliform EDN Laboratory: Pace Analytical Services - Eden SAMPLE DUPLICATE: 3819923 92633754001 Dup Parameter Units Result Result RPD Qualifiers Fecal Coliforms MPN/100mL 1.0 3.1 102 D6 Pace Analytical Services, LLC 1377 South Park Drive Kemersvifle, NC 27284 (704)977-0981 Results presented on this page are In the units Indicated by the "Units' column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 21 of 37 acmnalyticalm www.patelabs.com 1 Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 735976 QUALITY CONTROL DATA Analysis Method: EPA8260D QC Batch Method: EPA 8260D Analysis Description: 8260D MSV Low Level Laboratory: Pace Analytical Services - Charlotte Associated Lab Samples: 92633735001, 92633735002, 92633735003 METHOD BLANK: 3830383 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Parameter Units Blank Result Reporting Limit Analyzed 1,1,1,2-Tetrachloroethane ug/L NO 1.0 11/10/22 07:48 1,1,1-Trichloroethane ug/L NO 1.0 11/10/22 07:48 1,1,2,2-Tetrachloroethane ug/L NO 1.0 11/10/22 07:48 1,1,2-Trichloroethane ug/L NO 1.0 11/10/22 07:48 1,1-Dichlomethane ug/L NO 1.0 11/10/22 07:48 1,1-Dichloroethene ug/L NO 1.0 11/10/22 07:48 1,1-Dichloropropene ug/L NO 1.0 11/10/22 07:48 1,2,3-Trichlorobenzene ug/L NO 1.0 11/10/22 07:48 1,2,3-Trichloropropane ug/L NO 1.0 11/10/22 07:48 1,2,4-Trichlorobenzene ug/L NO 1.0 11/10/22 07:48 1,2-Dibromo-3-chloropropane ug/L NO 2.0 11/10/22 07:48 1,2-Dibromoethane (EDB) ug/L NO 1.0 11/10/22 07:48 1,2-Dichlorobenzene ug/L NO 1.0 11/10/22 07:48 1,2-Dichloroethane ug/L NO 1.0 11/10/22 07:48 1,2-Dichloropropane ug/L NO 1.0 11/10/22 07:48 1,3-Dichlorobenzene ug/L NO 1.0 11/10/22 07:48 1,3-Dichloropropane ug/L NO 1.0 11/10/22 07:48 1,4-Dichlorobenzene ug/L NO 1.0 11/10/22 07:48 2,2-Dichloropropane ug/L NO 1.0 11/10/22 07:48 2-Butanone (MEK) ug/L NO 5.0 11/10/22 07:48 2-Chlorotoluene ug/L NO 1.0 11/10/22 07:48 2-Hexanone ug/L NO 5.0 11/10/22 07:48 4-Chlorotoluene ug/L NO 1.0 11/10/22 07:48 4-Methyl-2-pentanone (MIBK) ug/L NO 5.0 11/10/22 07:48 Acetone ug/L NO 25.0 11/10/22 07:48 Benzene ug/L NO 1.0 11/10/22 07:48 Bromobenzene ug/L NO 1.0 11/10/22 07:48 Bromochloromethane ug/L NO 1.0 11/10/22 07:48 Bromodichloromethane ug/L NO 1.0 11/10/22 07:48 Bromoform ug/L NO 1.0 11/10/22 07:48 Bromomethane ug/L NO 2.0 11/10/22 07:48 Carbon tetrachloride ug/L NO 1.0 11/10/22 07:48 Chlorobenzene ug/L NO 1.0 11/10/22 07:48 Chloroethane ug/L NO 1.0 11/10/22 07:48 Chloroform ug/L NO 1.0 11/10/22 07:48 Chloromethane ug/L NO 1.0 11/10/22 07:48 cis-1,2-Dichloroethene ug/L NO 1.0 11/10/22 07:48 cis-1,3-Dichloropropene ug/L NO 1.0 11/10/22 07:48 Dibromochloromethane ug/L NO 1.0 11/10/22 07:48 Dibromomethane ug/L NO 1.0 11/10/22 07:48 Qualifiers IK, IL,v2 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977.0981 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the fight of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 22 of 37 1�55'cieAnalyticalo www.pacelabs.com j , QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 METHOD BLANK: 3830383 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Dichlorodifluoromethane ug/L NO 1.0 11/10/22 07:48 v2 Diisopropyl ether ug/L NO 1.0 11/10/22 07:48 Ethylbenzene ug/L NO 1.0 11/10/22 07:48 Hexachloro-1,3-butadiene ug/L NO 2.0 11/10/22 07:48 m&p-Xylene ug/L NO 2.0 11/10/22 07:48 Methyl-tert-butyl ether ug/L NO 1.0 11/10/22 07:48 Methylene Chloride ug/L 5.4 5.0 11/10/22 07:48 Naphthalene ug/L NO 1.0 11/10/22 07:48 o-Xylene ug/L NO 1.0 11/10/22 07:48 p-Isopropyltoluene ug/L NO 1.0 11/10/22 07:48 Styrene ug/L NO 1.0 11/10/22 07:48 Tetrachloroethene ug/L NO 1.0 11/10/22 07:48 Toluene ug/L NO 1.0 11/10/22 07:48 trans-1,2-Dichloroethene ug/L NO 1.0 11/10/22 07:48 trans-1,3-Dichloropropene ug/L NO 1.0 11/10/22 07:48 Trichloroethene ug/L NO 1.0 11/10/22 07:48 Trichlorofluoromethane ug/L NO 1.0 11/10/22 07:48 Vinyl acetate ug/L NO 2.0 11/10/22 07:48 Vinyl chloride ug/L NO 1.0 11/10/22 07:48 Xylene (Total) ug/L NO 1.0 11/10/22 07:48 1,2-Dichloroethane-d4 (S) % 95 70-130 11/10/22 07:48 4-Bromofluorobenzene (S) % 96 70-130 11/10/22 07:48 Toluene-d8 (S) % 99 70-130 11/10/22 07:48 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 3830384 Units Spike Conc. LCS Result LCS % Rec % Rec Limits 1,1,1,2-Tetrachloroethane ug/L 50 47.7 95 70-130 1,1,1-Tdchloroethane ug/L 50 43.9 88 70-130 1,1,2,2-Tetrachloroethane ug/L 50 49.2 98 70-130 1,1,2-Tdchloroethane ug/L 50 46.0 92 70-130 1,1-Dichloroethane ug/L 50 44.9 90 70-130 1,1-Dichloroethene ug/L 50 46.4 93 70-130 1,1-Dichloropropene ug/L 50 45.6 91 70-130 1,2,3-Tdchlorobenzene ug/L 50 49.7 99 70-130 1,2,3-Tdchloropropane ug/L 50 51.4 103 70-130 1,2,4-Tdchlorobenzene ug/L 50 48.2 96 70-130 1,2-Dibromo-3-chloropropane ug/L 50 44.1 88 70-131 1,2-Dibromoethane (EDB) ug/L 50 46.3 93 70-130 1,2-Dichlorobenzene ug/L 50 48.4 97 70-130 1,2-Dichloroethane ug/L 50 47.0 94 70-130 1,2-Dichloropropane ug/L 50 49.7 99 70-130 1,3-Dichlorobenzene ug/L 50 48.5 97 70-130 1,3-Dichloropropane ug/L 50 47.8 96 70-130 Pace Analytical Services, LLC 1377 South Park Drive Kernersville, NC 27284 (704)977-0981 Qualifiers Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 23 of 37 5acemalXical www.pacelabs.com Project: Piedmont Custom Meats Pace Project No.: 92633735 QUALITY CONTROL DATA Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3830384 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers 1,4-Dichlorobenzene ug/L 50 49.4 99 70-130 2,2-Dichloropropane ug/L 50 41.5 83 68-135 2-Butanone (MEK) ug/L 100 92.9 93 70-134 2-Chlorotoluene ug/L 50 47.7 95 70-130 2-Hexanone ug/L 100 102 102 70-131 4-Chlorotoluene ug/L 50 49.8 100 70-130 4-Methyl-2-pentanone (MIBK) ug/L 100 100 100 70-130 Acetone ug/L 100 89.3 89 70-133 Benzene ug/L 50 45.1 90 70-130 Bromobenzene ug/L 50 46.3 93 70-130 Bromochloromethane ug/L 50 44.0 88 70-130 Bromodichloromethane ug/L 50 47.4 95 70-130 Bromoform ug/L 50 45.6 91 70-130 Bromomethane ug/L 50 59.9 120 45-151 Carbon tetrachloride ug/L 50 45.2 90 70-130 Chlorobenzene ug/L 50 48.5 97 70-130 Chlorcethane ug/L 50 36.0 72 39-1521K,IL,v3 Chloroform ug/L 50 45.3 91 70-130 Chloromethane ug/L 50 43.7 87 58-130 cis-1,2-Dichloroethene ug/L 50 45.8 92 70-130 cis-1,3-Dichloropropene ug/L 50 46.8 94 70-130 Dibromochloromethane ug/L 50 45.6 91 70-130 Dibromomethane ug/L 50 46.1 92 70-130 Dichlorodifluoromethane ug/L 50 37.7 75 54-133 v3 Diisopropyl ether ug/L 50 46.3 93 70-130 Ethylbenzene ug/L 50 49.7 99 70-130 Hexachloro-1,3-butadiene ug/L 50 47.3 95 70-135 m&p-Xylene ug/L 100 101 101 70-130 Methyl-tert-butyl ether ug/L 50 45.4 91 70-130 Methylene Chloride ug/L 50 48.7 97 66-130 Naphthalene ug/L 50 49.9 100 70-130 o-Xylene ug/L 50 48.2 96 70-130 p-Isopropyttoluene ug/L 50 49.5 99 70-130 Styrene ug/L 50 49.8 100 70-130 Tetrachloroethene ug/L 50 44.8 90 70-130 Toluene ug/L 50 47.2 94 70-130 trans-1,2-Dichloroethene ug/L 50 43.3 87 70-130 trans-1,3-Dichloropropene ug/L 50 47.7 95 70-130 Trichloroethene ug/L 50 47.1 94 70-130 Trichlorofluoromethane ug/L 50 52.3 105 62-130 Vinyl acetate ug/L 100 103 103 70-144 Vinyl chloride ug/L 50 44.4 89 62-130 Xylene (Total) ug/L 150 149 99 70-130 1,2-Dichloroethane-d4 (S) % 100 70-130 4-Bromofluorobenzene (S) % 100 70-130 Toluene-d8 (S) % 102 70-130 Results presented an this page are In the units Indicated by the "Units* column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 24 of 37 a0Analytical wttnvpacelabs.cdm QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersviile, NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830385 MS 92633735001 Spike Parameter Units Result Cone. MSD Spike Cone. 3830386 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual 1,1,1,2-Tetrachloroethane ug/L NO 20 20 22.4 18.2 112 91 70-141 21 1, 1. 1 -Trich loroethane ug/L ND 20 20 23.3 19.2 116 96 70-150 19 1,1,2,2-Tetrachloroethane ug/L ND 20 20 22.2 18.5 111 92 69-142 18 1,1,2-Trichloroethane ug/L NO 20 20 22.3 18.4 112 92 70-138 19 1,1-Dichloroethane ug/L NO 20 20 22.7 18.6 113 93 70-150 20 1,1-Dichloroethene ug/L ND 20 20 24.3 20.4 121 102 70-156 18 1,1-Dichloropropene ug/L ND 20 20 24.7 20.3 123 102 70-150 19 1,2,3-Trichlorobenzene ug/L ND 20 20 23.1 19.1 115 95 70-148 19 1,2,3-Trichloropropane ug/L ND 20 20 22.4 18.0 112 90 70-140 22 1,2,4-Trichlorobenzene ug/L ND 20 20 22.8 18.8 114 94 70-146 19 1,2-Dibromo-3-chloropropane ug/L ND 20 20 22.6 18.9 113 95 68-146 17 1,2-Dibromoethane (EDB) ug/L ND 20 20 23.1 18.4 115 92 70-138 22 1,2-Dichlorobenzene ug/L NO 20 20 23.3 19.4 117 97 70-141 18 1,2-Dichloroethane ug/L NO 20 20 22.8 19.3 114 97 69-143 17 1,2-Dichloropropane ug/L NO 20 20 23.4 18.7 117 94 68-156 22 1,3-Dichlorobenzene ug/L NO 20 20 23.1 19.0 115 95 70-143 20 1,3-Dichloropropane ug/L NO 20 20 22.9 18.5 115 92 70-138 22 1,4-Dichlorobenzene ug/L NO 20 20 22.7 18.9 114 94 70-142 18 2,2-Dichloropropane ug/L NO 20 20 24.2 19.6 121 98 52-170 21 2-Butanone (MEK) ug/L NO 40 40 43.3 35.2 108 88 60-157 21 2-Chlorototuene ug/L NO 20 20 23.3 19.1 117 96 70-147 20 2-Hexanone ug/L NO 40 40 46.3 36.7 116 92 68-146 23 4-Chlorotoluene ug/L NO 20 20 24.0 19.4 120 97 70-142 21 4-Methyl-2-pentanone (MIBK) ug/L NO 40 40 44.0 35.7 110 89 70-141 21 Acetone ug/L NO 40 40 42.3 35.1 106 88 58-157 19 Benzene ug/L NO 20 20 21.6 18.1 108 91 70-142 18 Bromobenzene ug1L NO 20 20 22.5 18.7 113 94 70-143 18 Bromochloromethane ug/L NO 20 20 23.0 19.0 115 95 70-146 19 Bromodichloromethane ug1L NO 20 20 22.6 18.6 113 93 70-139 19 Bromoform ug/L NO 20 20 22.0 18.3 110 92 64-140 18 Bromomethane ug1L NO 20 20 23.6 19.8 118 99 28-192 18 Carbon tetrachloride ug1L NO 20 20 23.1 19.5 116 97 70-148 17 Chiorobenzene uglL NO 20 20 23.5 19.3 117 97 70-141 20 Chioroethane ug/L NO 20 20 25.5 22.7 127 113 58-191 12 Chloroform ug/L NO 20 20 21.7 18.8 108 94 70-148 14 Chloromethane ug/L NO 20 20 23.9 20.8 119 104 43-162 14 cis-1,2-Dichloroetene ugiL NO 20 20 22.9 19.2 115 96 68-151 18 cis-1,3-Dichloropropene ug/L NO 20 20 22.1 18.3 110 92 70-139 18 Dibromochloromethane ug/L NO 20 20 22.5 18.6 113 93 70-144 19 Dibromomethane ug1L NO 20 20 21.9 18.0 109 90 70-139 20 Dichlorodifluoromethane ug/L NO 20 20 24.1 20.3 121 102 39-171 17 Diisopropyl ether ug/L NO 20 20 22.6 18.4 113 92 67-142 20 Ethylbenzene ug/L NO 20 20 23.3 19.0 116 95 70-143 20 Hexachloro-1.3-butadiene ug/L NO 20 20 24.9 20.1 125 100 64-163 21 m&p-Xylene ug/L NO 40 40 47.6 38.6 119 97 70-144 21 Methyl-tert-butyl ether ug/L NO 20 20 22.6 18.3 113 92 65-143 21 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 25 of 37 aceAnalytical s www.pacelab.ccm t I QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3830385 MS 92633735001 Spike Parameter Units Result Conc. MSD Spike Conc. 3830386 MS Result MSD Result MS % Rec MSD % Rec % Rec Limits RPD Qual Methylene Chloride ugiL ND 20 20 22.6 18.7 113 93 62-149 19 Naphthalene ugiL ND 20 20 23.6 19.4 118 97 67-147 19 o-Xylene ugiL ND 20 20 23.6 19.0 118 95 70-145 22 p-Isopropyltoluene ugiL ND 20 20 24.8 20.5 124 102 70-147 19 Styrene ugiL ND 20 20 23.6 19.2 118 96 70-143 21 Tetrachloroethene ugiL ND 20 20 22.6 18.9 113 94 70-145 18 Toluene ugiL ND 20 20 22.3 18.5 111 92 70-142 19 trans-1,2-Dichloroethene ugiL ND 20 20 23.2 19.5 116 98 70-151 17 trans-1,3-Dichloropropene ugiL ND 20 20 22.7 19.0 114 95 70-139 18 Trichloroethene ugiL ND 20 20 22.8 19.0 114 95 62-146 18 Trichlorofluoromethane ugiL ND 20 20 23.2 19.2 116 96 63-153 19 Vinyl acetate ugiL ND 40 40 47.3 38.9 118 97 61-162 20 Vinyl chloride ugiL ND 20 20 25.7 21.3 129 107 61-163 19 Xylene (Total) ugiL ND 60 60 71.1 57.6 119 96 70-143 21 1,2-Dichloroethane-d4 (S) % 99 98 70-130 4-Bromofluorobenzene (S) % 102 101 70-130 Toluene-d8IS) % 99 99 70-130 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 26 of 37 1�5a'cmnalyfical" ( www.pacelabs.com i QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734288 Analysis Method: EPA 120.1-1982 QC Batch Method: EPA 120.1-1982 Analysis Description: 120.1 Specific Conductance Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92633735001, 92633735002, 92633735003 METHOD BLANK: 3821518 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Specific Conductance umhos/cm ND 10.0 11/02/22 10:36 Pace Analytical Services, PLC 1377 South Park Drive Kemersville. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3821519 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Specific Conductance umhos/cm 1410 1410 100 90-110 SAMPLE DUPLICATE: 3821520 92633735003 Dup Parameter Units Result Result RPD Qualifiers Specific Conductance umhos/cm 585 585 0 Results presented on this page are in the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 27 of 37 aceAnaiytical o www.pacelabs.com I QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734281 Analysis Method: EPA 300.0 Rev 2.1 1993 QC Batch Method: EPA 300.0 Rev 2.1 1993 Analysis Description: 300.0 IC Anions Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 METHOD BLANK: 3821472 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003, 92633735004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Chloride mg/L ND 1.0 11/02/2212:12 Sulfate mg/L ND 1.0 11102/2212:12 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3821473 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Chloride mg1L 50 50.3 101 90-110 Sulfate mg1L 50 50.8 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3821474 3821475 MS MSD 92633982002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chloride mg1L 65.2 50 50 111 114 92 98 90-110 3 Sulfate mg1L 166 50 50 214 218 95 103 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3821476 3821477 MS MSD 92633965002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Chloride mgiL 1.6 50 50 51.5 52.0 100 101 90-110 1 Sulfate mg1L 9.5 50 50 59.9 60.4 101 102 90-110 1 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 28 of 37 aceAnalytical watwt.pacelabs.com Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 735249 QC Batch Method: EPA 350.1 Rev 2.0 1993 Associated Lab Samples: 92633735004 METHOD BLANK: 3826651 Associated Lab Samples: 92633735004 Parameter Units Nitrogen, Ammonia mg1L QUALITY CONTROL DATA Analysis Method: EPA 350.1 Rev 2.0 1993 Analysis Description: 350.1 Ammonia Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.10 11107/2214:05 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3826652 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Ammonia mg/L 5 5.2 105 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826653 3826654 MS MSD 92634343002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L ND 5 5 5.4 5.4 108 108 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3826655 3826656 MS MSD 92634343004 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Ammonia mg/L 0.79 5 5 6.3 6.3 110 110 90-110 0 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /14/2022 02:43 PM without the written consent of Pace Analytical Services, LLC. Page 29 of 37 acmnalXical wsna.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 QC Batch: 734770 Analysis Method: EPA 351.2 Rev 2.0 1993 QC Batch Method: EPA 351.2 Rev 2.0 1993 Analysis Description: 351.2 TKN Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92633735004 METHOD BLANK: 3824286 Matrix: Water Associated Lab Samples: 92633735004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, Kjeldahl, Total mg/L ND 0.50 11110122 04:59 LABORATORY CONTROL SAMPLE: 3824287 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, Kjeldahl, Total mg/L 10 10.2 102 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824288 3824289 MS MSD 92634325001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 1.6 10 10 11.2 11.5 96 99 90-110 2 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824290 3824291 MS MSD 92634325002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, Kjeldahl, Total mg/L 0.86 10 10 11.2 10.7 103 98 90-110 5 Results presented on this page are In the units Indicated by the "Units" column except where an alternate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full. Date: 11/1412022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 30 of 37 1�5a'ciemalxical www.pacelabuom QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 735784 Analysis Method: EPA 353.2 Rev 2.0 1993 QC Batch Method: EPA 353.2 Rev 2.0 1993 Analysis Description: 353.2 Nitrate + Nitrite, preserved Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92633735004 METHOD BLANK: 3829334 Matrix: Water Associated Lab Samples: 92633735004 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Nitrogen, NO2 plus NO3 mg1L ND 0.040 11110122 09:20 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie, NC 27284 (744)977-0981 LABORATORY CONTROL SAMPLE: 3829335 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Nitrogen, NO2 plus NO3 mg/L 2.5 2.5 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3829336 3829337 MS MSD 92634891002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg/L 0.074 2.5 2.5 1.6 1.6 62 62 90-110 0 M1 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3829338 3829339 MS MSD 92634891003 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual Nitrogen, NO2 plus NO3 mg1L 0.028J 2.5 2.5 2.3 2.3 92 92 90-110 0 Results presented on this page are In the units Indicated by the "Units- column except where an alternate unit is presented to the right of the result. Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, I.I.C. Page 31 of 37 acemalXical www.pacelabs.com Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734547 QC Batch Method: EPA 365.1 Rev 2.0 1993 Associated Lab Samples: 92633735004 METHOD BLANK: 3823041 Associated Lab Samples: 92633735004 Parameter Units Phosphorus mg/L QUALITY CONTROL DATA Analysis Method: EPA 365.1 Rev 2.0 1993 Analysis Description: 365.1 Phosphorus, Total Laboratory: Pace Analytical Services -Asheville Matrix: Water Blank Reporting Result Limit Analyzed Qualifiers ND 0.050 11/03/2218:48 LABORATORY CONTROL SAMPLE: 3823042 Spike Parameter Units Conc. Phosphorus mg/L 2.5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823043 MS 92633735004 Spike Parameter Units Result Conc. Phosphorus mg/L 1.7 2.5 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3823045 MS 92634154001 Spike Parameter Units Result Conc. Phosphorus mg/L 3.2 2.5 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 LCS LCS % Rec Result % Rec Limits Qualifiers 2.5 101 90-110 3823044 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD Qual 2.5 4.3 4.3 103 104 90-110 0 3823046 MSD Spike MS MSD MS MSD % Rec Conc. Result Result % Rec % Rec Limits RPD 2.5 5.8 5.8 103 103 90-110 0 Results presented on this page are In the units indicated by the "Units" column except where an attemate unit Is presented to the right of the resuh. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11 /1412022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 32 of 37 aceMaocal www.pacelabs.com QUALITY CONTROL DATA Project: Piedmont Custom Meats Pace Project No.: 92633735 QC Batch: 734737 Analysis Method: SM 531OB-2014 QC Batch Method: SM 5310B-2014 Analysis Description: 5310B TOC Laboratory: Pace Analytical Services -Asheville Associated Lab Samples: 92633735001, 92633735002, 92633735003 METHOD BLANK: 3824084 Matrix: Water Associated Lab Samples: 92633735001, 92633735002, 92633735003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Total Organic Carbon mg/L ND 1.0 11/03/22 17:06 Pace Analytical Services, LLC 1377 South Park Drive Kemersvilie. NC 27284 (704)977-0981 LABORATORY CONTROL SAMPLE: 3824085 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Total Organic Carbon mg/L 25 24.7 99 90-110 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824086 3824087 MS MSD 92634383001 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L 3.9 25 25 28.1 28.2 97 97 90-110 0 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 3824088 3824089 MS MSD 92633735002 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Total Organic Carbon mg/L ND 25 25 26.7 26.6 106 105 90-110 0 Results presented on this page are in the units Indicated by the "Units" column except where an ahernate unit Is presented to the right of the result. REPORT OF LABORATORY ANALYSIS This retort shall not be reproduced, except in full, Date: 11/14/2022 02:43 PM without the written consent of Pace Analytical Services, I.I.C. Page 33 of 37 Pace Analytical Services, LLC aceAnalj6cal a 1377 South Park Drive Kemersville, NC 272$4 wanv.pacelab ucm (704)977.0981 QUALIFIERS Project: Piedmont Custom Meats Pace Project No.: 92633735 DEFINITIONS OF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenyihydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as `Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes. TN -The NELAC Institute. ANALYTE QUALIFIERS C8 Result may be biased high due to carryover from previously analyzed sample. 06 The precision between the sample and sample duplicate exceeded laboratory control limits. El Reported value should be considered a minimum estimate since it is the maximum reportable number for this method based on the sample volume used. The true value is likely greater than the value reported. IK The recalculated concentration of the calibration standard(s) did not meet method acceptance criteria; this result should be considered an estimated value. IL This analyte exceeded secondary source verification criteria low for the initial calibration. The reported results should be considered an estimated value. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. R6 The RPD between valid sample dilutions exceeded 30%. v2 The continuing calibration verification was below the method acceptance limit. The analyte was not detected in the associated samples and the sensitivity of the instrument was verified with a reporting limit check standard. v3 The continuing calibration verification was below the method acceptance limit. Any detection for the analyte in the associated samples may have low bias. REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 11/14/2022 02.43 PM without the written consent of Pace Analytical Services, LLC. Page 34 of 37 5aceAnalj&caI m www.patelabs.com QUALITY CONTROL DATA CROSS REFERENCE TABLE Project: Piedmont Custom Meats Pace Project No.: 92633735 Pace Analytical Services, LLC 1377 South Park Drive Kemersville, NC 27284 (704)977-0981 Lab ID Sample ID QC Batch Method QC Batch Analytical Analytical Method Batch 92633735001 MW4 SM 254OC-2015 735295 92633735002 MW-4 SM 254OC-2015 735295 92633735003 MW-5 SM 254OC-2015 735295 92633735004 Effluent SM 254OC-2015 735295 92633735004 Effluent SM 254OD-2015 734070 92633735001 MW4 EPA 350.1 Rev 2.0 1993 734588 92633735002 MW-4 EPA 350.1 Rev 2.0 1993 734588 92633735003 MW-5 EPA 350.1 Rev 2.0 1993 734588 92633735001 MW4 EPA 353.2 Rev 2.0 1993 733976 92633735002 MW-4 EPA 353.2 Rev 2.0 1993 733976 92633735003 MW-5 EPA 353.2 Rev 2.0 1993 733976 92633735004 Effluent EPA 353.2 Rev 2.01993 733976 92633735004 Effluent SM 521OB-2016 733970 SM 52108-2016 734318 92633735001 MW4 SM 9222D-2015 733947 SM 92220-2015 733949 92633735002 MW-4 SM 9222D-2015 733947 SM 922213-2015 733949 92633735003 MW-5 SM 9222D-2015 733947 SM 9222D-2015 733949 92633735004 Effluent Colilert-18 733894 Colilert-18 733895 92633735001 MW4 EPA 8260D 735976 92633735002 MW-4 EPA 8260D 735976 92633735003 MW-5 EPA 8260D 735976 92633735001 MW4 EPA 120.1-1982 734288 92633735002 MWA EPA 120.1-1982 734288 92633735003 MW-5 EPA 120.1-1982 734288 92633735004 Effluent TKN+NO3+NO2 736282 Calculation 92633735001 MW-1 EPA 300.0 Rev 2.1 1993 734281 92633735002 MW-4 EPA 300.0 Rev 2.1 1993 734281 92633735003 MW-5 EPA 300.0 Rev 2.1 1993 734281 92633735004 Effluent EPA 300.0 Rev 2.1 1993 734281 92633735004 Effluent EPA 350.1 Rev 2.0 1993 735249 92633735004 Effluent EPA 351.2 Rev 2.0 1993 734770 EPA 351.2 Rev 2.0 1993 736074 92633736004 Effluent EPA 353.2 Rev 2,0 1993 735784 92633735004 Effluent EPA 365.1 Rev 2.0 1993 734547 EPA 365.1 Rev 2.0 1993 734719 92633735001 MW-1 SM 531OB-2014 734737 92633735002 MW-4 SM 531OB-2014 734737 92633735003 MW-5 SM 531OB-2014 734737 Date: 11/14/2022 02:43 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Page 35 of 37 'S 'S .w o rn 3= E m a;a aG) qQ ," CG' 3 d x n o 3 — ro _ 0o<•8 aMI 3 N LYI �. 3 c a s c m m 3c A 0 CL co 3 in rooOw0 t8dnl ron cv, Oc CD p = Oc3 CL x m a r uCr O� .mow. roo d_ Q p a Ci W. y� a 0U3 NrO onN it] to to m x d I(a^^= cra mW Iwom MM a mGla o nl CL O a m m m 0 r d 33 n f 0 3 o c��r v o% i; ca GR O m W -a N m o_ �K �_ e�� ro Q d d u< m C 4) a w C S m C m °�'' < • z :. a. G1 n .e �, m n III} m m 70 " D ^ '_' 3 O t7 "' 0 m m 0 0 N < a ID m H 3 ro o IT a a n G ^ m a d rn 7 m .� c < 0 m a_ m€ 0 0 0 „ ro -i m m ?: —T— m �' a ^� o -o 3 3 3 o°, o o@ o= R c —rD is d tm L' to — G yB O. > M > d M.z m C C z a 1 i m 00 ci0 co rF F.Coli - T 3 m m f Ax Chloride, NO3, SO4, TDS, Cond o az ,n 3ICU O N To y'j25 TOC .. w< a S m a d s O < aN' 0 VOG {8264) f n y m o tn a ,a°mn NH3-N` a fl 3� [ -.• m m y N BOD, TSS, TDS, Chloride, NO3 t A R rt 3 NH3-N, Total N., Total P. R a "__ � o N 0 a s -R n W +'S m n flt G 3 1 7 00 9 ' i r• w O_ N�� �n v F Z m —_ , rvr,y 0Coroto0wV)Gemm mn �y rc G W '� 1 b'�t roc2P.1�aC Vlam cUO D M K n r Lt W l7 m iLi V3 y M M R F+ R n � 3 �' �i 'n N O. M :. toC i+RrRC�' ,.N-nI -00 V+- o _O Pv, Rba.n 4 wG'.Da-Danon" Pm 3 m n m w P m 6 ^" C- R ➢I R 'C O '4 m 'D *J• 'O r tC m S 0--'O r D R ,q a C C e+• c P X+ a d r+ +R m rfi .+ �' ag D " 3, "' c , a� Z °' mo W 3'�.m 3aa r,0. :3 0 Ro- RPh o - eD�S"n OO ro n'c Drnt4Pm \ 4J ".7 R N D• n G F+ n R 7 R n - ° z we s ro � R �S R R i� ,+ n. 0 0 W P G Kf nl d a 3 a �.a m ',i, n�R-~ia�mi o s m ro �- .�.. '" cy OS+a rmn c n R A o r + ZOO 2 cno m ro 3 3 rk�_ etr. m m 4 a W CD a7 0 3 fi. n h m +, iL � 7'Ln °^ 0 G d 2 toD- QID i7 G n ,... Gi 0. 5 R � �SR N c¢r a is }(,��,� K (t 7J q 7>7 T 99 77 It Z > D n+� CC X� _ ld-lmtinca:icn Foci (?:F) i C.`,......a'1: (ice • F-CA;-CS-C�3•r�ay.C_ c, r;-- -; r, 'C.-:_ r~; ,cr hs c,atic(; ' - - 5cm^i25. ^0`rill 0 xl i 1i cf bcx is to list nunj1 e( of bottles Sample:D I �I\\ I I I \I I I NNI LII\I I\I I� I I HIE 11 pH Adjustment Loa for Preserved Samples T7pe of Praserrative pH upcn rec-.ipt I Cate preservation adjusted Time pre;ervation Anxeunt of Preservative Lat a 1 adjusted added "cote: vtnenever thare is a di;: epanc/ a'=:ec-.ing Ml rh Caroi'na Cornpilanca samples, a cop., of this fcrrn wi!l to sent to the Ncrh CamNr,3 CEjMB Car;'iC I :cn Dr-",cz (;.a. Out cf hclJ, incorrac prasarlrvive, out of temp, inccrre^, caltainers. Page 37 of 37