WQ0034775_Monitoring - 11-2022_20221202

Monitoring Report Submittal
Permit Number #*
Name of Facility:*
Month: * November
Report Information
Type *
GW-59
WQ0034775
Bakelite Synthetics
Confirmation Email Address: *
Name of Submitter: *
Signature:
Date of submittal:
Initial Review
Year:* 2022
Upload Document*
CLRS Permit WQ0034775 1.21 MB
November 2022 Submittal.pdf
PDF Only
Please upload one PDF containing all applicable monitoring reports
(i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59).
[e-mail]
W. Ben Moore
�0
Reviewer: Gerald, Wanda
12/2/2022
This will be filled in automatically

Is the project number correct?* WQ0034775
Is the monitoring report accepted?* - Yes NO
Regional Office* Wilmington
Reviewer: _anonymous
Review Date: 12/19/2022

GW-59A COMPLIANCE REPORT FORM Pelrinit (# WQ0034775
(Submit tone each rnottitoring period ►vlth GII! 59 farms.)
1
Enter date monitoring results were due. ( 12 31 2Q22) Will this monitoring report (GW-59 and GW-59A)
Y1:S
NO
be submitted after the established due date?
2
Was any required information missing on the GW-59 report forms?
X1GS
NO
IF the answer to question I or 21s "YES", list In the space provided below the well Identification number(s) and
explalo the problems encountered In obtaining the required Information.
3
Are any of the monitor wells in need of repair or maintenance (damaged casing, imiocked or missing cap, missing
Y1CIS
NO
identification plate, area overgrown, etc.)? If the aw ver Is "Yes", contact the Regional Officeforguidance,
4
Are any monitored constituents equal to or above the established standards?
tS
NO
If the answer to question 4 Is NO ; skip. to section 8.
If the answer to question .4 Is "YES" list the affected wells individually with constituent(s) and concentration(s)
exceeding standards in the space provided below:
W WMW-1: Total Dissolved Solids (744 mg/L); Total Ammonia Nitrogen (540 mg1Q Sulfate (730 mg/L) W WMW-2: Total Dissolved Solids (713
mg/L) Total Ammonia Nitrogen (45.6 mg/L); Nitrate (55,(i mg/L); pH (M9 so)
5
For the constituents Identified In question 4 above, have standards been exceeded previously for the
YES
NO
same constituent(s) In the same well(s) In the last two years?
If the answer to question 5 Is "NO", skip to section B.
If the answer to question 5 Is "YES; list in the space provided below, each well with constituent(s) exceeding
standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years).
W WMW-1; Teta$Ammaaia Nitrogen 610 mg/L(n/24/201, 748 mg/L (3/17/21), 890 mg/L (7/08/11), 760 m9/1_411/10/21y, SOO m9/L(3/09/22), 396mg/L (7/13122); 1051380 mg/L (11/24/20), 1840
mg/L (3/17/21), 252omg/L (7/oa/21), 2410 MOIL (11/10/21),1260 mg&(3/09/22),1136mg/L(7/13/22);Suifate772 mg/L(11/24/201, 761 mg/L (3/17/211, 315 MOIL 0/08/211, 1590 m8/L (11/10/21)
807 me/L (3/09122), 442 mg/L I711112n22); W W M W-2: Talai Ammonla Nilronen 28.5 mg/L (11/24I20), 45.4 mg/L (3/17/211, 54.1 mg/L (7/08/21), 64.2 mg/L (11/10/21), 26.1 mg/L (3/09122), 78.3
mg/L(7I19/2022); �H 4.Sa su (11/24j20], 4.73 su i3/17f21), 5.58 su (7/OB/21}, S56 su {l3/10/21), 5.92 su (3/09/22), 6.21 su (7/13122); Nitrate 48.9 mg/L(11/24/10),72.6 nsg/L(1/17121), 5s.4mg/L
(7/08/21); 32.6 mg/L(3I09/24,19.5 mg/L (7/13/221
6
Are the monitoring wells listed In section 5 located at or beyond the review boundary?
Y1 S
NO
If the answer Is "YES", a groundwater quality problem may be occurring. CONTACT THE REGIONAL
OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO") monitoring wells may be Improperly
located, contact the Regional Office.
7
Is the permittee Implementing previously approved actions required by the Division involving this
Y1 S
NO
groundwater quality problem?
If the answer to question 71s "YES", describe those actions In the space provided below.
If the answer.to question 7 Is "NO", contact the Re—glonal Office: within 90 days, an evaluation may be
required to determine the Impact the waste dlsl2osal system Is having at the review and coml2flance
boundaries surroundina this faclllt . Failure to do so may sub'ect the 12ermlifee to a Notice of Violation
fines and/or penalties.
The Lined Pond has been permanently removed from closed -loop recycle service.
g
The person completing this. portion (GW 59A) of the monitoring report should sign ,below and submit this
form with GW 59 forms for required wellsto the address provided at the top of the current OW-59 form,
Sign ure of Permiltee (or u orized Agent) bate
GW-59A 12/8/2003

SUBMIT FORM ON YELLOW PAPER ONLY
DEPARTMENT OF'ENVIRONMENT &,NATURAL" RESOURCES
GROUNDWATER QUALITY MONITORING:
DIVISION OFWATERQUALrrY INFORNIATIOitii PROCESSWG UNIT "
COMPLIANCE REPORT FORM
15i7 MAIL SERVICE C@NTERjiRALEIGFI; NC 27699-I617 , F?hpne: (919] 733=3227
FACILITY INFORMATION
Please Print Clearly or Type
PERMIT Number: WQ0034775 Expiration Date: January31, 2028
Facility Name: Bakelite LLC
Non -Discharge UIC
Permit Name (if different): permit No. W00034775 Bakelite Synthetics— Riegelwood CLRS Closed -Loop Recycle System Columbus County
N PDES Other
Facility Address: 333 Neils Eddy Road
TYPE OF PERMITTED OPERATION BEING MONITORED
Riegelwood {street} NC
28456 County Columbus
El Lagoon ElRemediation: Infiltration Gallery
iciryj tS-arej
(41p)
❑ Spray Field ❑ Remediation:
Contact Person: Mr. Ronald Bazinet
Telephone#. [phone] ext 5257
❑ Rotary Distributor ❑ Land Application of Sludge
We[[ Location/Site Name: WWMW-1
No. of wells to be sampled: 2
❑ Water Source Heat Pump N Other: CLRS
(tram Permit)
SAMPLING INFORMATION
If WELL
WELL ID NUMBER (from Permit): WWMW-1
Date sample collected: November 02, 2022
FIELD ANALYSES:
WAS
Well Depth: 17.80 ft.
Well Diameter: 2 in.
pH 00400: 7.44 units Temp. ammo: 19.87 °C
DRY at
Depth to Water Level 82546: 10.70 ft. below measuring point Screened Interval: 7-8 ft. to
17.8 ft.
Spec_ Cond. 00094: 3536 p.Mhos
time of
sampling,
Measuring Point is 2.45 ft. above land surface
Relative M.P. Elevation: 23.29 ft.
Odor coon: odor
check
Volume of water pumped/bailed before sampling:
5.0
gallons
Appearance blacklcloudy
here:®
Samples for metals were collected unfiltered: [I YES
❑ NO and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
Date sample analyzed: Novembero3-15, 2022
Laboratory Name: Environmental Chemists,
Inc.
Certification No. 94
PARAMETERS NOTE: Values should reflect
dissolved
and colloidal concentrations.
COD oo3m
mg/L
Nitrite (NO,) as N o0615
mg/L
Pb - Lead o1051 ug/L
Coliform: MF Fecal 31s1s
/100mL
Nitrate (NO3) as N D0620 <0.02
mg/L
Zn -Zinc 01092 mg/L
Coliform: MF Total 315o4
/100mL
Phosphorus: Total as P oosss 2.46
mg/L
(Note: Use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 70300 744
mg/L
AI - A[uminum ol1o5
mg1L
Formaldehyde (8315A): 110 ug/L
pH (Lab) 00403
units
Ba - Barium o1 oo7
ug/L
1,2,4-Trichlorobenzene (8260): 0.62 ug/L
TOC ooeso 38.1
mg/L
Ca - Calcium 00g16
mg/L
1,3-Dichlorobenzene (8260): 0_67 ug/L
Chloride 00940
mg/L
Cd - Cadmium o1 o27
ug1L
n-Butylbenzene (6260): 0.98 ug/L
Arsenic 01002
ug1L
Chromium: Total of os4
ug1L
Grease and Oils 00552
mg/L
Cu - Copper o1 o42
mg/L
ORGANICS: (by GC, GC/MS, HPLC)
Phenol 32730
ug/L
Fe - Iron 01045
uglL
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 730
mg/L
Hg - Mercury 71900
ug1L
Lab Report Attached? ❑I< Yes (1) ❑ No (0)
Specific Conductance C0095
pMhos
K- Potassium 00937
mg/L
VOC(GWVOC) method # 6260 low concentration
Total Ammonia o17610 540
mg/L
Mg - Magnesium o0927
mg/L
method #
(Ammonia Nitrogen; NHos N; Ammonla Nitrogen, Total)
Mn - Manganese c1 o55
ug/L
method #
TKN as N 00625
mg/L
Ni - Nickel C1067
ug1L
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Ronald BaZnet - Bakelite Site Leader
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.2/2010
J
ttee (or A
l�?_/1l Z_
(pate)

SUBMIT FORM ON YELLOW PAPER ONLY
GROUNDWATER QUALITY MONITORING:
COMPLIANCE REPORT FORM
and 1 or
6
FACILITY INFORMATION Please Print Clearly or Type PI
Facility Name: Bakelite LLC
Ni
Permit Name (if different): Hermit No. WQ0034775 Bakelite Synthetics— Riegelwood CLRS Closed -Loop Recycle System Columbus County N1
Facility Address: 333 Neils Eddy Road
Riegelwood 611vv ° NC 28456
County Columbus
(Citvi (state) r710
Contact Person: Mr. Ronald Bazinet
Telephone#: [phone] ext 5257
Well Location/Site Name: WWMW-2
No. of wells to be sampled: 2
(from Permit)
SAMPLING INFORMATION
WELL ID NUMBER (from Permit): WWMW-2
Date sample collected: November 02, 2022
Well Depth: 13.21 ft.
Well Diameter: 2 in.
Depth to Water Level 82546: 8.35 ft. below measuring point
Screened Interval: 3.21 ft, to 13.21 ft_
Measuring Point is 1.56 ft. above land surface
Relative M.P. Elevation: 15.89 ft.
Volume of water pumped/bailed before sampling: 4.0 gallons
Samples for metals were collected unfiltered: ® YES ❑ NO
and field acidified: ® YES ❑ NO
LABORATORY INFORMATION
:RMIT Number: W00034775 Expiration Date: January 31, 2028
n-Discharge UIC
'DES Other
'PE OF PERMITTED OPERATION BEING MONITORED
❑ Lagoon ❑ Remediation: Infiltration Gallery
❑ Spray Field ❑ Remediation:
❑ Rotary Distributor ❑ Land Application of Sludge
❑ Water Source Heat Pump 0 Other: CLRS
FIELD ANALYSES:
PH 00400: 5.89 units
Spec. Cond. 00094: 1147
Odor ooc85: none
Appearance cloudy
Temp. 000lo: 20.91 °C
µMhos
Date sample analyzed: November 03-15, 2022
Laboratory Name: Environmental Chemists, Inc.
Certification No, 94
PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations.
COD oo335
mg/L
Nitrite (NO2) as N oo615
mg1L
Pb - Lead olc51 ug/L
Coliform: MF Fecal 31616
/100rnL
Nitrate (NO3) as N oos2o 55.6
mg/L
Zn - Zinc 01092 mg/L
Conform: MF Total 31504
/100ml-
Phosphorus: Total as P oo665 0.12
mg/L
(Note: use MPN method for highly turbid samples)
Orthophosphate 70507
mg/L
Other (Specify Compounds and Concentration Units):
issolved Solids:Total 703oc 713
mg1L
Al - Aluminum oilo5
mg/L
Formaldehyde (8315A): <50 ug/L
PH (Lab) 00403
units
Ba - Barium 01007
ug/L
TOC ooeec 6.8
mg/L
Ca - Calcium 00916
mg/L
Chloride 00940
mg1L
Cd - Cadmium 01027
ug/L
Arsenic 01002
uglL
Chromium: Total 01034
ug/L
Grease and Oils 00552
mg/L
Cu - Copper oio42
mg/L
ORGANICS: (by GC, GCIMS, HPLC)
Phenol 32730
ug/L
Fe - Iron olo45
ug/L
(Specify test and method #. ATTACH LAB REPORT.)
Sulfate 00945 210
mg/L
Hg - Mercury 71900
uglL
Lab Report Attached? ON Yes (1) ❑ No (0)
pecific Conductance o0oas
µMhos
K- Potassium 00937
mg/L
VOC (GWVOC) method # 8260low concentraton
Total Ammonia oo610 45.6
mg/L
Mg - Magnesium 00927
mglL
method #
(Ammonia Nitrogen; NH, as N; Ammonia Nitrogen, Total)
Mn - Manganese oloss
ug1L
,method #
TKN as N 00625
mg/L
Ni - Nickel 01067
uglL
method #
For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal%
Ronald Bazinet- Bakelite Site Leader
Permittee (or Authorized Agent) Name and Title - Please print or type
GW-59 Rev.212010
DRY at
time of
sampling,
check
here:

Einvironniental Chemists, .1,111C.
6602 Windiriffl Way, Wflryiiingtcni, 44 rN( ' 1 28405 m 91092 3921223 Lab * 91.0.3,24 Fa x
71.0 Bc)wsertown Road, Manteo, NC 27954 a, 252.473.5702 Lab/Fax
255-A Wilrningtcm I fighway, Jacksonville, 28540 , 910.347.5843 Lal..)/Fax
nnifi.)@c,-iivij'oininent,,ilcheiTiists.c(anm
Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-53379 Site: WWMW-01
11/2/2022 9:30AM
Water Client
Test
Method
Results Date Analyzed
Iron
EPA 200.7, Rev. 4.4,1994 (Dissolved)
0.648 mg/L
11/08/2022
Manganese
EPA 200.7, Rev. 4.4, 1994 (Dissolved)
0.186 mg/L
11/08/2022
Sulfate
EPA 300.0, Rev, 2.1, 1993
730 mg/L
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0, 1993
540 mg/L
11/04/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
744 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
2.46 mg/L
11/09/2022
Sulfide
SM 4500 S D-2011
12.4 mg/L
11/07/2022
Total Organic Carbon (TOC)
SM 5310 6-2014
38.1 mg/L
11/02/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
1, 1, 1 -Trichloroethane
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
1, 1,2,2-'Fetrachloroethane
SW 646 Method 8260D/503013
<0.5 pg/L
11/08/2022
1, 1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
1,1-Dichloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/5030B
<0.5pg/l-
11/08/2022
1,2,3-Trichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,4-Trichlorobenzene
SW 846 Method 826013/503013
0,62 pg/L
11/08/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
1,2-Dichlorobenzene
SW 846 Method 826OD15030B
<0.5 lig/L
11/0812022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0,5 pg/L
11/08/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/5030B
0.67 pg/L
11/08/2022
Report#:: 2022-21778 Pagel cat

Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
1,3-Dichloropropane
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/50305
<M pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<M jig/1-
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Benzene
SW 846 Method 826OD/50305
<M pg/L
11/08/2022
Bromobenzene
SW 846 Method 826OD/5030B
<M pg/L
11/08/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromoform
SW 846 Method 8260D15030B
<M pg/L
11/08/2022
Bromomethane
SW 846 Method 826OD15030B
<M pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 826OD/5030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroform
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 lig/L
11/08/2022
cis- 1,2-Dich loroethene
SW 846 Method 8260D/50309
<M pg/L
11/08/2022
cis- 1, 3-Dich loropropene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
Dibromomethane
SW 846 Method 8260D/50305
<M pg/L
11/08/2022
Dichlorodifluoromethane
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
Hexachlorobutadiene
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
1 sopropyl benzene
SW 846 Method 8260D/5030B
<0.5pg/L
11/08/2022
M+P Xylene
SW 846 Method 8260D/6030B
<1.0 pg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D15030B
<0.5 lig/L
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
0.98 pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
ortho-Xylene
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
Report#,� 2022-21778
Page 2 of 9

1"Aivironmerital. Chemists, Inc.
6602 ffindmill Way, Wihxdigtm, N(28405 a 9103910223 Lab @ 910.392.4424 Fax
710 Bowa sertowii Road, Mriteo, NC 2795* 252.473.5702 Lab/Fax
255 A Wflirnh%torw i fighway, Jacksmville, NCI 28540 n 910.34:7.5843 Lab/Fax
itifa)�'4i?enviionxii(,,ijtal(,,,Iic°inists,coxit
Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive , Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
p-isopropyltoluene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
sec -Butyl benzene
SW 846 Method 8260D150306
<0.5 pg/L
11/08/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11108/2022
tert-Butylbenzene
SW 846 Method 826OD15030B
<0.5 pg/L
11/0812022
Tetrachloroethene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Toluene
SW 846 Method 826OD15030B
<0.5pg/L
11/08/2022
Trans-1,2-Dichloroethene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trans- 1, 3-d ich loropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Trichloroethene
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
Trichlorofluoromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 846 Method 826013/503013
<M pg/L
11/08/2022
Formaldehyde
SW846 8315A
110 pg/L
11/04/2022
Nitrate Nitrogen (Calc)
Nitrite Nitrogen
EPA 353,2, Rev 2,0, 1993
0.06mg/L
11/03/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev. 2.0, 1993
< 0.02 mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
<0.02 mg/L
11/15/2022
Total Nitrogen (Calc)
Total Kieldahl Nitrogen (TKN)
EPA 351.2, Rev, 2.0, 1993
579 mg/L
11/09/2022
Total Nitrogen
Total Nitrogen
579 mg/L
11/15/2022
........... . ....... ................. . .............. ............................................. ................................
Repoirt#:2022-21778 Page 3 of 9

ental Chemists, ,In.c. I!,aivironm
6602 Winchnfli Way, Wiliningftm, lq('28405 9103910223 1 ab �, 910.392.4424 Fax
710 Bowsei-town Road, Manteo, NU(. . 27954 * 252.473.5702 Lab/[,ax
255-A Wily.nington. Ffighway, Jacksonville, NC.' 28540 o 91.0.347.5843 Lab/Fax
i4ifo(.,,,eri.vii'o4,iiTietalchefniisis.coni
Test
Method
Results
Date Analyzed
Iron
EPA 200.7, Rev. 4.4,1994 (Dissolved)
<0.06 mg/L
11/08/2022
Manganese
EPA 200.7, Rev. 4.4,1994 (Dissolved)
0.839mg/L
11/08/2022
Sulfate
EPA 300.0, Rev. 2.1, 1993
210 mg/L
11/07/2022
Ammonia Nitrogen
EPA 350.1, Rev, 2.0, 1993
45.6 mg/L
11/04/2022
Total Dissolved Solids (TDS)
SM 2540 C-2015
713 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
0.12 mg/L
11/09/2022
Sulfide
SM 4500 S D-2011
<0.05 mg/L
11/07/2022
Total Organic Carbon (TOC)
SM 5310 B-2014
6.8 mg/L
11/02/2022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1, 1, 1 -Trichloroethane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/08/2022
1, 1,2,2-Tetrachloroethane
SW 846 Method 826OD/50305
<0,5pg/l-
11/08/2022
1, 1,2-Trichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
M-Dichloroethane
SW 846 Method 826OD/50305
<0.5pg/l-
11/08/2022
1, 1 -Dichloroethene
SW 846 Method 826010/503013
<0.5 pg/L
11/08/2022
1,1-Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
1,2,3-Trichloropropane
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
1,2,4-Trichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
1,2,4-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,2-Dichloroethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
1,2-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,3,5-Trimethylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 8260D/50305
<0.5 pg/L
11/08/2022
Report # . 202Z21776 Page 4 of 9

1., s Inc
nVI''ron.m.ental Clteniiffb.' , 0
6602 Windrnffl Way, Wilmington, P2('28405 o 9103910223 Lab w 910,392.4424 Fax
71.0 Bowsertown Road, Manteo, NC 27954 * 252473.5702 Labjax
255 A Wflnihighm Ifighwa * Jacks�)nvflle, NC28540 91.0,347.5843 Lab/1'ax
Y,
Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive, Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #. 2022-21778
Project ID: Bakelite Acme CLRS
1,3-Diehloropropane
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 8260D/5030B
<M lig/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/l..
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<M pg/L
11/0812022
Benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromobenzene
SW 846 Method 826OD15030B
<0,5 pg/L
11/08/2022
Bromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromomethane
SW 846 Method 8260D15030B
<M pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroethane
SW 846 Method 8260D/5030B
<0.5 pgA.
11/08/2022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
ci5-1,2-Dichloroethene
SW 846 Method 826OD/5030B
<0.5 pg/L
11/08/2022
cis- 1, 3-Dich loropropene
SW 846 Method 8260015030E
<M pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromomethane
SW 646 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dichlorodifluoromethane
SW 046 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 8260D/5030B
<Mpg/L
11/08/2022
llexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 lig/L
11/08/2022
1 sopropyl benzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
MFP Xylene
SW 846 Method 8260D/5030B
<1.01.jg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D/5030B
<Mpg/l-
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 826OD/5030B
<Mpg/L
11/08/2022
ortho-Xylene
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
Report #:: 2022-21778
Page 5 of 9

Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive , Suite 110
Customer PO #a
Wilmington NC 28405
Customer ID: 1107001
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLR
p--Isopropyltoluene
SW 946 Method 8260D/5030B
<0.5 pg/L
11/08/2022
sec-Butylbenzene
SW 946 Method 9260M3/50305
<0.5 pg/L
11/08/2022
Styrene
SW 946 Method 6260D/5030B
<0.5 pg/L
11/08/2022
tert-B utyl benzene
SW 646 Method 926013/503013
<0.5 pg/L
11/08/2022
Tetrachloroethene
SW 646 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Toluene
SW 946 Method 8260D/5030B
<M pg/L
11/08/2022
Trans-1,2-Dichloroethene
SW 946 Method 8260D/5030B
<0.5 fag/L
11/08/2022
Trans- 1,3-dichloropropene
SW 946 Method 9260D/50305
<0.5 p /L
11/08/2022
Trichloroethene
SW 946 Method 926010/503013
<0.5 pg/L
11/08/2022
Trichlorofluoromethane
SW 946 Method 9260D/50305
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 946 Method 8260D15030B
<0.5 pg/L
11/08/2022
Formaldehyde
SW646 9315A
<50 lag/L
11 /04/2022
Nitrate Nitrogen (C lc)
Nitrite Nitrogen
EPA 353.2, Rev. 2.0,1993
0.23 rig/L
11/03/2022
Nitrate+Nitrite®Nitrogen
EPA 353.2, Rev. 2.0, 1993
55.6 mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
55.6rng/L
11/15/2022
Total Nitrogen (Clc)
Total Kjelahl Nitrogen (TN)
SPA 351.2, Rev. 2.0, 1993
19.2 rng/L
11/09/2022
Total Nitrogen
Total Nitrogen
75.0 mg/L
11/15/2022
IPelport M, 2022-21 "r'/'9 Page 6 of 9

Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive, Suite 110
Customer PC #.
Wilmington NO 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
Lab ID Sample ID:
Collect Date/Time Matrix Sampled by
22-53383 Site: WWMW-03
11/2/2022 10:00AM
Water Client
Test
Method
Results Date Analyzed
Iron
EPA 200.7, Rev. 4.4, 1994 (DissoWd)
0.106 mg/L
1110812022
Manganese
EPA 2003, Rev. 4,4,1994 (DissoWd)
0.079 mg/L
1110812022
Sulfate
EPA 300.0, Rev. 2.1, 1993
38 mg/L
1110712022
Ammonia Nitrogen
EPA 350.1, Rev. 2.0,1993
160 mg/L
1110412022
Total Dissolved Solids (TDS)
SM 2540 C-2015
400 mg/L
11/03/2022
Total Phosphorus
SM 4500 P (F-H)-2011
< 0.04 mg/L
1111112022
Sulfide
SM 4500 S D-2011
<0.05 mg/L
1110712022
Total Organic Carbon (TOC)
SM 5310 B-2014
19.9 mg/L
1110212022
1, 1, 1,2-Tetrachloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
1110812022
1, 1, 1 -Trichloroethane
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1, 1,2,2-Tetrachloroethane
SW 846 Method 826OD/50300
<0.5 pg/L
11/08/2022
1, 1,2-Trichloroethane
SW 046 Method 02BOD/5030B
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethane
SW 846 Method 826OD/50300
<0.5 pg/L
11/08/2022
1, 1 -Dichloroethene
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1, 1 -Dichloropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
1110812022
1,2,3-Trichlorobenzene
SW 846 Method 8260D/50300
<0.5 pg/L
1110812022
1,2,3-Trichloropropane
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1,2,4-Trichlorobenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
1110812022
1,2,4-Trimethylbenzene
SW 046 Method 02BOD/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromo-3-Chloropropane
SW 846 Method 826OD/5030B
<0.5 pg/L
11/08/2022
1,2-Dibromoethane
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1,2-Dichlorobenzene
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1,2-Dichloroethane
SW 846 Method 8260D/5030B
<0.5 pg/L
1110812022
1,2-Dichloropropane
SW 046 Method 026OD/5030B
<0.5 pg/L
1110812022
1, 3,5-Trimethylbenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
11/08/2022
1,3-Dichlorobenzene
SW 846 Method 82BOD/5030B
<0.5 pg/L
1110812022
Report # 2022-21770 Page 7 of 9

Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive, Suite 110
Customer
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLIP
1,3-Dichloropropane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
1,4-Dichlorobenzene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
2,2-Dichloropropane
SW 846 Method 82BOD/50305
<M pg/L
11/08/2022
2-Chlorotoluene
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
4-Chlorotoluene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Benzene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Bromobenzene
SW 846 Method 8260DI5030B
<0.5 pg/L
11/08/2022
Bromochloromethane
SW 646 Method 8260D15030B
<0.5 pg/L
11/08/2022
Bromodichloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromoform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Bromomethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Carbon tetrachloride
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
Chlorobenzene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloroethane
SW 846 Method 826OD/50305
<M pg/L
11/0812022
Chloroform
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Chloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
cis- 1, 2-Dich loroethene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
cis- 1, 3-Dich loropropene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromochloromethane
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Dibromomethane
SW 846 Method 826OD15030B
<0.5 pg/L
11/08/2022
Dichlorodifluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Ethylbenzene
SW 846 Method 8260D15030B
2.30 pg/L
11/08/2022
Hexachlorobutadiene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
lsopropylbenzene
SW 846 Method 8260D/6030B
<0.5 pg/L
11/08/2022
M+P Xylene
SW 846 Method 826OD15030B
<1.0pg/L
11/08/2022
Methylene chloride
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
Naphthalene
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
n-Butylbenzene
SW 846 Method 826OD/50305
<M pg/L
11/08/2022
n-Propylbenzene
SW 846 Method 826OD/50306
<0 .5 pg/L
11/08/2022
ortho-Xylene
SW 846 Method 826OD/50305
<0.5 pg/L
11/08/2022
Report #:: 2022-21778
Page 6 of 9

Wood - WSP USA E&I Inc
Date of Report: Nov 15, 2022
5710 Oleander Drive , Suite 110
Customer PO #:
Wilmington NC 28405
Customer ID: 11070019
Attention:
Report #: 2022-21778
Project ID: Bakelite Acme CLRS
p-isopropyltoluene
SW 846 Method 8260D/5030B
21.2 pg/L
11/08/2022
sec -Butyl benzene
SW 846 Method 826013/503013
<0.5 pg/L
11/08/2022
Styrene
SW 846 Method 8260D/5030B
<0.5 pg/L
11/08/2022
tert-B utyl benzene
SW 846 Method 8260D/5030B
<0,5 pg/L
11/08/2022
Tetrachloroethene
SW 846 Method 826013/5030B
<0.5 pg/L
11/08/2022
Toluene
SW 846 Method 8260D/5030B
1.52 pg/L
11/08/2022
Trans- 1, 2-D ich loroethene
SW 846 Method 8260D/503013
<0.5 pg/L
11/08/2022
Trans-1,3-dichloropropene
SW 846 Method 8260D15030B
<0.5 pg/L
11/0812022
Trichloroethene
SW 846 Method 8260D15030B
<M pg/L
11/08/2022
Trichlorofluoromethane
SW 846 Method 8260D15030B
<0.5 pg/L
11/08/2022
Vinyl chloride
SW 846 Method 8260D/5030B
<M pg/L
11/08/2022
Formaldehyde
SW846 8315A
<50 pg/L
11/04/2022
Nitrate Nitrogen (Cato)
Nitrite Nitrogen
EPA 353 2, Rev. 2 0, 1993
0.02 mg/L
11/03/2022
Nitrate+Nitrite-Nitrogen
EPA 353.2, Rev 2,0,1993
0. 14 mg/L
11/03/2022
Nitrate Nitrogen
Subtraction Method
0.12 mg/L
11/15/2022
Total Nitrogen (Cale)
Total Kieldahl Nitrogen (TKN)
EPA 351.2, Rev 2 O, 1993
148 mg/L
11/09/2022
Total Nitrogen
Total Nitrogen
148 mg/L
11/15/2022
Comment:
Reviewed by:
Relportkl 2022-21778 Page 2 of 0

.1 A.,.BORATORY CONTROL, SAMPIX #1
Reporl.92022 2 q 778 Page I of 3
Method
5pike
.................................. B..I.a..nk �Vpike
........ .... ...... ...
QC Limits
Spike (7ompounds
Blank
Added
Resuft Recoveq
(Mandatoq)
Result
%
1% Recovery Range
ID i ch.lorodi fluorom ethane
.
<0.5
.
10
. ......................................
L34 113
80 �120
..........................................................................................................................................................................
Chloromethane
<0.5
10
10.66 107
80-120
.......................................................
Vinyl chloride
..................................................................
<0.5
.
1.0
................ . . ................... --
u.7 117
80-120
Bror-nomethane
<0.5
10
11 � 4 M
80 ,120
. ..........
Chloroetharie
............... . .
<0.5
.
10
..................................................................
11,58 116
. .. . . ......
80-120
..........................................................................................................................................................................................................
Trichlorofluoromethane
�<0.5
10
.
0.98 110
. .................. . . .....
80-120
lj.-I)ichloroethene
<0.5
10
10.61 106
80-120
............................................................................................................................................................ I . .
Methylene chloride
.
<0.5
.
10
..................................................................
10.51 105
80 120
... . ..... . ...................... .... ........................................................................................................
trans 1,2 Dichloroethene
. ........ .
<OU.5
. . ........
10-
10.99 110
......................................
80-120
.. .
.............................................................. ............. . ... . ... . .. . .......................................................................................................................
1,L Dichloroethane
11-..-�---
<0. 5
1()
1031 107
...- I -.-
80-120
2,2...Dichloropropane
.5
10
10,48 105
80-120
cis- 1,2--Dichloroethene
<0.5
10
10.83 108
80 120
. .................................
Bromochloromethane
<0.5
10
M85 109
80 ,120
..................................................................................................................................................................................
Chloro.form
...... . ...................... . ........................
<0.5
.
10
.................................................................
1034 107
80-120
1, 1, 1 ...'Frichloroethane
.
<0.5
............................................................
10
-
0.75 108
80 ,120
..................................................................................................................................................................................................................
Carbon tetrachloride
-... . . .....
.5
'10 1
........ -.-I -
10,71 1 107
80-120
....... . ........................................
I, I -]DicMoropropene
...................................................................
<0.5
............................................................
10
..................................................................
103 107
. ........
80-1,20
Benzene
<0.5
10
0.83 1108
80 120
. .. . ........... . . . . . .
1,2 Dichloroethan
........................ . . .
0.5
10
10.66 107
80-120
.... .
Trichloroethen
.
0.5
. ....... .
10
M78 108
80-120
I
1,2-11.)ichloropropayae
.
< .5 1
.
. .
10
.
. ......... . . . ............. -
� 0,9 109
..................................................................
80 ,120
........................................................................................
Dibromomethane
........................................................................................................................................................................................................................
<0.5
.................................................................... ..............................
10 J.
.
10.81 1 108
..... ....... ....... ....
80-120

LABORATORY CONTRO1, SAMPLE #1
Repon#2022 21778 Page 2 of 3
Method
Spike
Blank.Ypike
QC Limits
Spike Compounth
Blank
Re.vult
Added
Resut
l
Recoveyy
(MandatoiY
)
%
% Recovery Range
Brornodid-floromethan
.. ­
.......................................................................................................................­.1-1.1 .....................................................
0.5
10
1035
.................... . . ........
108
80-120
cis....1,3 DicNoropropene
<0.5
10
10,,5
1105
80-120
.......................................................
'roluene
...........................
<0.5
10
10.86
109
1 80-120
trans.- 1,3-Nchloropropene
. .............. . ... .
<0.5
....
1.0
1 OJ2
105
.................
1,1,22-1richloroelhano
........................................................................................................................................................... .
<0*5
.
10
............................................................
11 koy 9 1
..........
109
80-120
'Fetrachloroethene
........................................................................
�<0.5
1 10
10,8
108
80420
1,1 D�cNoropropane
- — ­­-- ......-- -- -
;gyp'...........,.........
10
10. 81
W8
80 120
I)ibromochloroniethane
<0.5
10
10.92
09
0-1
820
rl, 2 -TNbrornoethane
<0.5
. ........................................................
10
...........................................................
10.8
.................................................................
IN
. . .
80 120
. . ..................................... . ..................................................
Chlorobenzene
<0.5
1
10.69
107
80-120
�Ethyl berizene
.............................................................................................
<0.5
.
10
...................... _ ........ .
1 O�92
. .......... . ........................
09
...........................................................................................
80,420
I �, 1, 1 ,2-,retrachl oroethane
.
<0.5
. .... . .... ............................................
10
10.92
109
80 �120
M �1' Xylene
I. ....................................................................................................................... . . ..... .
<
...................................................................
20
18
........ I ........21.................. .
111
. .........
80 120
G Xylene
.
<0.5
..... . ............
10
103
107
80-120
Styrene
<0.5
10
............................................................
O.93
..................................................................
109
80 120
..................................................................... —
Brornoform
< 9
10
1039
108
. .
80-120
. . . .......
Isopropylbenzene
<0.5
10
.
1 O�95
. ........ . ............................................
110
80-120
Bromoberizene
... .
<0.5
. ....... ___ ..............
10
1 LOI
................................
110
80-120
...­ . . ...... .
1, 1,2,2-Tetrachloroethane
......... .....................
<0.5
10
1 V75
108
...................................................................................
80-420
n •P ropy lbervene
<0.5
10
IL01
110
80-120
................................................................ . .................. . ..... . ........................ . ........ . . .............................................................................
1,2,3-Trichloropropane
<03
1.0
11.1
1
.................................................................
80-120
2-Chlorololuene
<0.5
10
11
1 0
80 120
........................................................................................................................................................................................................................
1,3,5•Trirn e thyl benzene
.........................................................
<0.5
.10
1 L 14
111
. . ..... __..
80-120
. .................

Method
Spike
I Blank
Spike
QC Limits
IV
pike Compounds
Blank
Result
Added
lt
overy
(Mandator
y)
%
% Recoveq Range
.............................................................................................................
4-Chlorotoluene
<0310
...................................................................................................................................
1 1 „03
.m...........................
1 W
.......................................................................................................................................................
- 20
.....................................................................................................I.........._....
_
.............
.................................. ..._...................................................................................................................................... _
....................................................................
to80-120
................................................
.................................... _..... _..................
see;,- u ty]benze e
.....................................................................
0.
to
11„11
111
........ -®-.._.................... .... ._............ _......
- 20
...........
... ...�........ ..................................__............................................_..
..... .....................................................................
......
...................................................................................................._.
.
.....................................................................................................................................................
...........................................................................................-.-..............................................................................................
1,4_Duchloroberuz sue
<0.5
............................................................
10
....
M2
..............................................................................................................................................................................................................................................
109
- 2
......................................................................................................................._...........
�..... uu1ylb n'z uu
0.
10
11„06
......................................................
111
..... ......
��.�.�..�.__��__�.............
.............................. ...............................
1,2....Dichlowbenz n
0.
.0
W.68
107
.........................
0-120
.............................................................................................................................._.�.,...............................................................................................__
1,2.-Dibro o......-ohloropropan e
0.5
10
10„64b
.............
106
0- 2
...............................................................................................................................
n ,2y4....°r richlorobe zee
.....
.
10
11 „ I 1
............
1 1 I
.......................................................................................................................................................
��,,,420
.........................................
1 lexacJhlorobu tadie e
<0.5
to
....
1 1.5.E
.............................................................................................................................................................................................................................................
115
80,,,,,120
Naphthalene e
0.5
10
11. 3
116
.. .... .�.............
0-420
1,,2,3,,,.Trichlorobenzettu .................... .....
..............1 ...................
10
I L 111
q....�............................
,,,, 120

LABORATORY CONTROL SAMPIX #2
.... ..... ..... ...T.. .... .....
.................................................................. ii. e 't #"20'22 2 � 778 Page I o . f . 3 .............. .... . ...................
Method
Spike
................... BlankSpike
. ......
QC Linifts
Blank
Spike Compounds
Result
Added
.Revult
over
Y
(Mandatoi�
y)
%
Recovery Range
........................................................................................................................................ .......... .
Dichlorodifluoroniethane
..................................................................
�<0.5
1.5
.............................................
IT34
.
116
......................................................................................................................................................
80-1.20
............... . . . . . . . ........................... . . ..... . ... . ..........
Chloromethane
...................................................
<0.5
15
15.67
.
104
......... ...........
1 80 120
. .... . .... . ...........
Vinyl chloride
<0.5
15
16.98
113
80-1.20
................................ ......................................................................................................................................................................................
Bromornethane
.......................................... .
<03
. .. .... . .................... . ..
15
....................................................... . ........
16.35
..... . ...................................................................................
M
80-4.20
........................................................................................................................................................................................................................
Chloroethane
.......... . ........ 111-
<0.5
..........
15
17.81
119
80-1.20
.................................................. . . . .. . .. . ...... . ............. . .......................................................................................................................
Trichlorofluoromethane
....................................................................
<0.5
............................ I ......................
15
16 727
80 �1.20
................................................... .... ..............................................................................................................................................................
lyl Dichloroethene
<0.5
.....................................
15
16.04
107
80-120
........................................................................................................................................................................................................................
Methylene chloride
. .........................
<0.5
....................
15
. .............
16.31
109
80 1.20
. ............
trans - 1 .2- Dichloroethene
<0.5
15
16.45
Ito
80-1,20
....................................................... . ...............................................................................................................................................................
1, 1 � Dichloroethane
...................................................................
I <0.5
...........................................................
i H
� 62
108
80 420
........................................................................................................................................................................................................................
2,,2--Dichloropropy ne
- . ............
<0.5
. . . . ......
15
........ .
17A
. .......................... -
116
80 120)
................................................................................................................. .
cis....1,2 Dichloroethene
. .. . ...... . ...... ...... . .......................
. .
<0.5
1.5
16,54
. .....
i
Ito
80 120
. ............ . ...... - ....... . ..........................................................................................................................
Brornochloromethanc
....................................................................
<0.5
..........................................................
15
..................................................................
16,33
...........................................................................................
109
..................................................................................................................
80 �120
............................................................................................................................................................................................ ..........................
Chloroform
........ . . . .
<0.5
. ...........................................
1.5
.........
163
109
80 120
1, 1 . 1-17richloroetliane
<0.5
1.5
6.08
107
80 120
Carbon tetrachloride
<0.5
1.5
16.04
107
......................................................................................................................... ..........................
80-4.20
................................................................................
1, 1 Dichloropropene
<0.5
15
. ..........................
5A4
106
80 120
......................
Berizene
<0.5
1.5
16.43
.... ............ .....
Ito
. ..................................................................................................
80 120
........................................................................................................................................................................................................................
1,2-Dichloroethane
...................................................................
<0.5
1.5
16
M
80 420
..........
"rrichloroethene
<0.5
15
. . . ... . ...............
16.15
108
80 120
. . . ...........................
1,,Z-Dichloropropane
........................................................................................................................................................................................................................
<0.5
...................................................................
1.5
-
6.78
112
80-420
. ... . ........................................ . . .... ... -
Dibromornethane �
....... . ... .... I ............. ..
<03
. .. . ....................
15
16.24
1108
80 420

Repor ..112022....21778 Page 2 of .3
Method
,, ik
k �Ypike
�..................................
C Laaaaaty
Blank
Spike ; poaand
���p�pm
u�114�0 � �
Added
Result
over
(Mandatory)
Recovery Range
.._......................................................................................
rom odichDoranmethann
_.................................. ....... ........... ............. ........ ............. ...... ....... ....._
_ ..
_......... ...... .............. ....................
15
_15,
16. 17
108
0-12
cn, ,,,. D 3-DichIoropropene
0 5
..
� 5, 7➢
..............-_..........
105
�-120
.......
16.22
....
15.48
.... .......
....................................................................................................................................................................... .........
� 6.
162
1,3-DJichlanroprop arms
0w
5,I.. ��
10
DD,,,,, 20
u .,9
1,2-Dibror noethairn
0.
1
107
�-120
�.�
,,.
q..3:3
M f-P Xylene
1
30
110
0,,,,, 20
.a. b
16.2 I
Styrene
<0.5
15
1.7
110
0-1 20
,. c
flan ro Db ffnznn
0.5
5
9 Gn„7 I
n n n
0,,, 120
�6.2
D., Y y2,,.'1etr achloroeth n
..................................................................................
0w
.15
.....m........mm...........................
1622
............................................................................................
108
0,,,,,120
.....................................
......, w
.........
.........................................................................�...............
.........�.......
.....................
.....................................................................................................................................................................................................................................................
.....
....
....
1,3, ,,,.,..D.' imethyDbnz ne
<0.5 1
15
16.75
u 12
0-1 20

LABORATORY CON'rizoj, SAMPLE #2
Report#2022 21778 Page 3 of 3
Method
'Spike
.. . .......... Blank
pike
QC Limits
�,V..ike C"ompounds
Result
Added
Resuft
Recovery
(Mandatory)
%
% Recovery.Range
..........
4-Chlorotoluene
<0 5
.15
16.53
110
80 120
............... . .................................................. -
tort- Butylbenzene
. . . ............... . ......................................
<0.5
............................................................
1.5
...................................................
16.64
111
.......... ...... . . ............................................................................................................................
80-120
1,2,4.-Trimethylbenzene
.
<0.5
.
15
....................................... —
1 6J5
110
..... .............
80420
.......................................................
sec-]Butylbenzene
....... . ............ ...........................................
<0.5
......... . .......... . ....................................
15
.........................................
16�67
111
80-120
.......................................................
1,3-Dichloroberizene
<0.5
15
1635
109
80-120
................................................. . . . . ................................................................
4-1sopropyholuene
<0.5
15
.................................... —
16�76
112
. ........................................................................................................................................
80-120
...........................
],,4-Dichloi-obenzene
i—..
<o,'5
15
1629
109
................................................................................ I..—
80-1.20
.
ri-Butylbenzerie
<0.5
15
I7009
114
— ......................................................................................................
80-120
.............................................
1,2 Dichlorobenzene
<0.5
15
15.95
106
80-120
....................
1,2-Dibromo-3-chloropropane
<0.5
15
15.02
100
. ........................................................... ........................................................................
80 120
. ............. ..................................................... . .......... ..................................................... . . .
1,2,4-Trichlorobenzene
................................. .
<03
.
15
. .........................................................
15.95
106
80-1.20
. . .................................. . . ..................................................................
flexachlorolwtadiene
<0.5
..................
U5
......................................................
dT]8
.
115
. .................................................................................................................................
80-1.20
. . . . ............................................................. .
Naphthalene
<0.5
15
5.86
106
80-120
........................................... --.-
123 1'richlorobenzene
.............. . ... . ..
.
<03
. ..... . ......................................................... ....
. ........ . .......
15
. . .. . ... . ..... ................ ....................................................................
15.78
-
105
.............................................................
80-120

ANALYTICAL & CONSUL:nING CHEMISTS
C heiniiiiisAls,
6602 Windinfll WaY, Wffir6n44hwi, NC 28405 a 910,3910223 Lab m 9103924424 Fax
710 Blowsertowni Road, Manteo, NC27954 * 2152,473,5702 lzb/Fax
255--A Wjbindrigton I fighway, Jacksonvifle, N(28540 e 9144.34T15843 1 ab/Fax
iiifo�'ia,,cri.vii-onnwntal(.heynisi�s,(,,orri
Wood QC .- 2022-21778
GCS
Parameter
True Vdlue
Result
%Recovery
Limits
mg/L
m9/1
?1101
Ammonia
5.O
5.2
104
90-110
Iron
2.00
1.95
98
90-110
Manganese
1.00
1.01
101
90-110
NO2
0.60
0.62
103
90-110
tNO3 & N-02
-1 M-
O.97
97
90-110
Sulfate
50.0
46.6
93
90-110
TDS
600
600
100
90-110
Sulfide
UO
0.46
92
90-110
TOC
I 0.0
103
103
90-110
TKN
4.0
3.9
98
90-110
TP
1.60
1.58
99
90-110
1.60
1.57
98
90-110
MS/MSD
True Value
Recovery
%
Limits %
Limits %
Parameter
Recovery
mg,,L
Difference
Recovery
Diff
erence
Ammonia
4.0
3.3/33
92/92
0
80-120
�5 20
.Iron
LOO
LOI'LOO
103/100
3
80420
� 20
Manganese
0.100
0. 100/0., 100
100/100
0
80-120
� 20
NO2
O.50
OA5/0.48
90/96
6
80-120
!<-5 2 0
NO3 & NO2
0.50
0.55/0.56
110/112
2
80-120
<20
Sulfate
MO
&8/8.8
88/88
0
80-120
<20
-N/A
N/A
N/A
N/A
80-120
<20
Sul de
0.50
0.40/039
80/78
2
70-130
<30
Toc
10.0
10.2
102 1
N/A
80-120
:5 20
TKN
5.0
4.7/5. 1
94/102
8
80-120
<20
4F
100
1.91/100
96/100
4
80420 1
5 20
.99/ �199
99.5�/995
-0
80 120
<20

DUPIACATE SA.MP
I..,ES
Result.v
Parameler
% D�.ff�rence
Limits %
mg,'L
Ammonia
N/A
... .
N/A
. ..... . ................................................. . ..
N/A
. ..... . ..................
<10
Iron
N/A
..............................
N/A
N/A
N/A
Manganese
. .............................. . ......
N/A
N/A
N/'A
N/A
NO2
N/A
N/A
.
N/A.
. ............... . ........................
<10
NO3 & NO2
N/A
N/A
. ............... . .........................
N/A
!S 20
............ .......... I .... . .............. . .... . ..............
S u I fire
....... . .. -
<5
<15
0
....................................................
10
,..ID
.................. . .
744
...................... .. . . . .........................
'766
3
10
.................................. Suffide
..........
0. 120
0. 12 8
6
<10
TOC
1.4
........................
1.3
7
. . ........
510
rKR
N/A
N/A
N/A
<10
. . ......... ....... . .
BLAN K
.........................
Results
.............................
Limit
Parameter
mg,,J,
Mg/L
Ani.monia
<0, I
OA
Iron
<U05
0.005
Manganese
-- - ------- --7 . . .. . .....................
-U5 -
<0.005
........................ . ..............
0.005
N
<0.0 I
-- - -- - -------------------
0.�Ol
NO3 & NO2
--0.0 1
0.01
.................... Sull'ate
<2.5
2,5
TDS
<15
.............................................
2.5
SUlfide
<U25
...... . ........................................ . ...
U25
TCSC"
�<0,25
0.25
................. TKN
........................ .
<0.25
025
. .. . .
TP
..........................................................
..................................... . .. . ......
<0.02
--- - --
0.02
Tp
<0.02
0.02
............................................................. . ..............

Analytical Environmental Services, Inc
IClieiiit. Env4unmenW Chemists, Inc. Client SainlAe IM 22-53379
Prme� oject Na2022-21778 Collection Date: 11/2/2022 9,30-00 AM
Lalb IM 2211360-001 Matrix- Aqueous
.. . ......... . ............................................ . .......... . ...... . ........ . .............................. —.1 ................................ . .. . .............. ................... . ...................................... . ..... ......................... . ........... .. . ............. . ... . .................. . ................................................. . ......................... ............... . . ..... . ......................... — ................. ................... ..... . ....................... . ......................... . ............................
I"
Analyses Result Reporfing Quial Units ffiatchlD Dilution DateAnWyzed Analyst ,
Limitctor . ........................... 1-1 . ................................................. —.1 . ................................. . ................................... .. . ........................... . ........................... . .................................. . . ............................ . ... . ........................................... . ... 1. .................................. I .. . . . ............................ . ......................... ........................... . . ........................... . ......................... I., . ............................. . ................. . I . ...............
Formaldehyde by SW8315A.
Formaldehyde HO WO ug/L 345847 l 11/0412022 1449 Cm
Qua hnem . Wue exceeds ormunum camunuArm Ilrvr6
BR L Bda. mpammg Imut
11 HoWging WTICS for IprrcmaUanon Or analyms emeded
N Anu�ye nw NELAC comified
B Anapye deected m dw amocmed mehod blhnk
Gfweir dian Resuh vahm
E Esau watma (vs ue abo,�e qpmnumnon range)
S SpAke Rmmvegy ouwde hmms due Ao mnwrAx
Mar, SV, CaSp tA,,Ay3JRVV,
F Anayud m ffir M hwh As a devRahon fhm, On mehod
". Less than Rmuk vahAe
J Bummed i alue. deArmled Wow RepoARRing Lima
Page 3 of 9

Analytical Envirowittiental Services, Inc
DateI I •-1' ov-22
Client: Environmental Chemists, Inc, Client Sam1fle J.D, 22-53382
Project Name.- 2022-21778 Coflection Date-, 11/2/2022 9:45: 00 AM
I..,ab ID. 2211360-002 Ma trix: A q u e o i i s
....................... . ... .... . . .... —
Analyses Remilt Reporting Qual thnits Batchf.D Dillution DafeAnsly,zed Ainalyst
LimitFactor ............... ............................... ....................... . ... . ........................... . . . ......
Formaldehyde by SW8315A
FormaWehyde BRI., 50 UFA, 345847 1 1 � /04/2022 � 4 59 CM
Qualfiflem Wee exce.r.6 mamnum cuimmAinnant level
BRI, BrIlow zeponmg hniAt
I d 19011dHIS "Imes fog prep malion ov anad)em exceeded
N Analyte wt NELAC cenffied
B Analyte detected m de wsmated gneflmd bl.nk
11 Geateir ffian Result value
E. Enawcd (vaiue above qumwmuon moge)
S Sphke Recomy ouwde hmLs due to gnairm
Nwr See msenwatwe
F AnzllyzW m lhe Ilab awrhich Rs a de,Rauan frum 6e method
< Lem dtan Result alue
3 f1stunited i,allue detected Wow Repumng l.oimq

Analytical Environmental Sex -vices, Inc
Date- I I -Nov-22
Client: Environmental Chemists, Inc, Chent Sample ID-. 22-.53383
Project Name: 2022-21778 Collection Date. 11/2./2022 10:00-OOA.M
Lab ID. 2211360-003 Matrix: Aqueous
............ I . . ....... .............. ...... ... ..................... . ..... . .............. . ................... . ............. . .................................................. - ............ . ......... ........................ . ............ . ..... . ... . ................. .. . . .......... ................................ . ................................... . .... .. . ................... . ............... . ............... . ........... ................ . .............. . ...................... . ................ - ....................... . .............................. . . ............
Anodyses Result Reporthng Qual Units BatchlD Dilution DateAnalyzed AnWyst
U11, it Factor
. ........... —.. .............................................. . .. . ............................ . ................................ .. . .................................. . ................................. . ..................................... . ................. 2 ..................... . . . .............................. . ............................. . ............................................................................ I .. . ................................... . ......................... . .... . ............................................ ... ..........
Formaldehyde by SW831.5A
Formzddehyde BRI., 50 ubdl.' 345847 p lga"0412022 B 5 21 CM
QuMffiem
Vahm excmds wmxnnum conummAiRR kvd
BRI.
BeNwrporunghmiRt
I d
floldmg Imes for prepaimuon ov aguflysu; exceeded
N
AgWyne not NELAC ceRufied
B
Analpe dewved uun fl,e assmuae,whediml Wank
Gawer Um Rmh wflue
E Estunaud (value abo"quamiumbon rainge)
S Sptke Recomy owsuk Ilunuts due w nuum
Nwr Seecasmwrnwe
F AgWymA m ffie tab whwh us a dmauOn front tM> rnegiud
IT Lem dmn RLsuh flue
J Estunated wflue dewocd k�ow Reporung Linut

Enviroinmei Ral Chernist, Inc., Wflmington, NC I a lb #94,
6602 WinJrnffl Way
Wilmington, NC 28405
91-0.392.0223
Sample IReceipt Checklist
— ................ . .............. Date-, ... ...... ..... ..... . ..... Report Nurnber. 2022
4 . . . ............. . ........
Rece�pt of sarne-
1"CHEM Pickup i Ckmt DeHvery F."r"
--- ---" -­­ 11 ..... . ... . .. . ..... . .. ... —, --
i"edfx i"..] Other El
-ere custody seais present on the cooleir'?
DJ I . .....................
YES -11-3
11
............................
NO ...............
............. —11 ............. . ..... . . ....................... . .......................... . . .................................... . . .................. .
N/A 2. ff custody seak weire present, were they intact/unbiroken?
OrigMM ternperature upon receipt Correctec.1 tenverature upon receipt
... .... . . . ............... . . . .. ......... ...............
—[�A­ —ai —1:B
How temperah.M`E�
. . ............................... . ..........
takem,
. ................
-- — ------- -- . . ......
[3 Temperature Blank g ns" o"t, ti e" s
. . . . .. ................ ---
M (3LU11 M.I hOMasTraceabie
.............. . . ................. ............ . . . ............ . .. ..........
S/N 1.925.1.1.657 M Gpun CorrecUon Factor T' 0.0
. ...............
YES
. .. ..
.........
E]
NO
. .....
. ................................ . .............. . . . ............. — ............ - .......... . . . . . ..........................
1 if temperature of cor.fler exceeded 6' C, was Pro ect Mgi-,/QA notified'?
..... - -- — - -------- - — — ----------- - J
YES ..-
........... .
E]
. ..........................
NO
. . .
. ... ................. . ........... -=-" ---` ...... ... ......... . . . .....
4. We re pro �pe r custody p� oced t,� res (re I � nq u ished/rece �ved) fo � �mved ?
........... . .. . .......... .
12 ,-
YES
-YES
—r—.."INO
n
NO
- —
................................. . .. ............................ . ... . . ................ ................ . .......... . ...................... ......... . ......... . . . . ........... . ........
5, Were sarnp�e M's listed on the COC?
—
...........
. ..........
----- 67"W"", e —re 's a —m p"Te" s i D s -H"s —te c'i o �'i" -s" a � —n 1) 1 e (`:"o-i i t a —ir i e s ? .... . ............. ---`,`—,---
. ......
r�—Y
........ ......
F S""
. .
T .
. ....................
i�-C') . ..........
7. —Were—coHe`—cflm'i-d` a t, e—a in 'd, t i'�T-ie —fist-e" t -h e C ( ............ ------- — — ----- - -----
. . C ?
Y,E...S ...............
1.71Were
. . .............. - .......... —) .............. ............ .. . .. ...... . ..........
tests to be perfurned HSUad on the COCR ......... .
YES
T-T-NO
- —
...........
. . ............ . ................................. .. ......... . .....
-- —96ici "s arnp—Res a"-r ri v-e" in 1,iroper containers for eac'.:h test'?
NO
. ........... -1 ......................... . ................ . ...... ..... ............... 1. ............ I . .......
D. Dki sarnples arrrve an good condffion for, each test'?
YR S
E.3
—sairripfe -sio-fi.-j;,-r-;e—ava,- u--1 a-- i-)i e T
(.2 YES ............ I ... . ........................ .. ,, rec6ved Mthhn proper hoid�ng dime fo�ll �'r eqUestecl tests , ?
— ........... . . ......... Were sarnpies
....
YES
.................. . . ... .
.... ..........
NO
.
-----------
13. Were acid preserved sa rnp�es receRved at a pl i of -2';)
.
C.".]
I., ........
YES
. ..... .......... --.-
11
��o
- . ...........
...... . - — --------- - - ----------- - ----------- ­­ "' .................... . ......... -.- . . ............. .
.1.4, Were cyanWe saimpies received at a pH >12'?
.......
YES
n
\i 0
. .. ............. . . ............... ............... . . . . .............. . ......... .
"'")' kq("`0 SUM& sairnp�es received at a pH >9?
IS
13
NO
6, Were M113/10/i3henoi received at a dhloii1ne residual of <0,5 rn/t.'?
..........
Y, S ............ ...
pp II''N
.. ......
C")
....... — --
. ........ . ........ . . . . . .......... . ....... ........... . . .
.7, Weire Suffide/Cyanlde received at a chk)idne resklual of: <0,13 rn/i..'?
— -------- - --------- - - - ------------- . .............. . .. ......... ... . . .............. . .
F1
YES
D
.... . ..
NO
. ......... ......
.......... ........................... . . . ....... .. . ....... .
1.8, Were oirthophosphate swnp�es filtered in the. field within 1.5 minutes?
. ............ ---- .............
iOC/Vc)ati�esar.epicR-recI�<edatt�,rrerat aria9ysRs and recordedon the benchsheet,
Bactleria sarnples are checked for Ciflorine at tirne, of anaRysis and recorded on the benchsheet.
--- ---------- . . . . . .. .. .. .. .. .. .. .. . . .. .. .. .. .. .. .. .. .. . . . . . . .. .. .. .. . . .. .. .. .. .. .. .. .. .. .. .. .. .. . . ..... . ..... .. .. --
SampIe Preservation: (Must be cornpieted for any sarnp�e(s) incorreclAy preserved or with headspace)
Sample(s) were received incm rectiy pireserved and were adjusted accor(fingly
by adding (cir-cie same)) 1-R2SO4 1--R iq03 110 Na(DH
rime of preservatmoin-
ff rnore than one preservative Rs needed, notate in corniments below
............... --.- ........ . ........... I ......... . .............. —.1
...... . . ......... . . . ................. . .................................. . .............
Note: Notffy customer service 'rmrriediateiy for incorrectly preserved sanipas, Obtain a 1 oew sarnpe ov
notlify the state Ub ff directed to imaiyzed lby the customer. Who was noflhed, da: te and flme:
. ....... . . . . . ............ ...... . . ................. .
olal,Hes Safflp6e(s)
CGIMMEATS,
were recelve(.] with headspace
[)OC',A,002 Rev I
a

!ENVIRONMENTAL CHEMISTS, 6642 Windmill Way it ins ton, 1C 2 406
- OFFICE: 919®392-9223 FAX 910-392=4424
Analytical & Consulting Chemist- CDE R; DWQ CERTIFICATION # 94 NCDHHS: DLS CERTIFICATION # 37729 [e-mail]
COLLECTION ECTI AND CHAIN F CUSTODY
Client: PROJECT 4_
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T
ADDRESS: C
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- SITE t
a 3. E72 -I y xREPORT TO-
E1
-COPY TO: ;
I email: s
_=
Sampled By: ----------------
SAMPLE TYPE: I Influent, F Effluent. = Well, ST = Stream,
Collection
SO a Soil, SL Sludge Other;
I °
PRESERVATION
Sample Identification
Date Time Tep
v� s �z IESTED
z�.
.. _ ' C PG re
C F
L
I I C F
I
[ 'J
-------------
1
} C Pa i I
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Transfer -1 Relinquished a ate/Time Received
Y Date/Time
I,L ;
.
Trrature when R��ived �C_ ��epted;_ ��-� �`e�ted°
RearpleReueted;
Ilvar d R R Iv d _ — f c .
C
Date; z__ Tie_ rt s T k6N
I
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4M-
ENVIRONMENAL IN C 6602 Windmill WayWilmington,N
CHEMISTS, OFFICE-
91-39M223 FAX [phone]
Analytical & Consuffina Chemists
NC ENR; DWQ CERTIFICATION # 94 NCDHHS° DLS CERTIFICATION # 37729
info enuironmentalche ist&coe
COLLECTION � CHAINP CUSTODY
'Client- e �
T `r
E T e
ADDRESS: %0
_
SITE:-
P ,
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PHONE/FAX:
COPYTO:
ailarQ
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A PLE TAPE; I = Infltter�t, o Efflc e e, Well,
ST = Stream, SO o Soil, ILL � Sludge, ether;
ile�ti17 t PPERVATION
ie eiltii�atttl I
c y c
Cn m 0 - "a
E a E 10 0
�
w ANALYSIS REQUESTED
Qt➢ i
Date
0 � soa � �
Time Temp`� z d z
2
p E
E [
_
I C
t
I
i C
] G
17
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C pi
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C F; P _
Transfer
.4Relinquis ed ; ate/Time eceivy:
Date/Time
2,
wale .Requested:
comments;T�,a
—Date:
TURNAROUND:

Client: `
ADDRESS: 4�n
V
65692 Windm2li Way Mmington, NC 28446
ENVIRONMENTAL CHEMISTS, INC OFFICE: 910®392-0223 FAX [phone]
NCDENR: DWQ CERTIFICATIC?gJ # 94 NCDHHS. DLS CERTIFICATION # 37729 [e-mail]
COLLECTION AND CHAIN OF CUSTODY
T INAIIII_ _ _ , ;REPORT
4 f
SITEe
n g. l
}
I -REPORT
TO:
=.
E/
ICOPY TO:
it° trv,. L U -
SA PLE TYP.- I = Influent, E Effluent, W Well, ST = Stream, SO _ Soil, SL = Sludge, Other;
C II c l n
CL
PRESERVATION
E �° .P, E_'
<
z
ANALYSIS REQUESTED
Date Time Temp
` �
s
2
z I
z
z
zfM
C P
V i
_
l
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I
1
' I
I
t,
_LPL,
I
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f_� _
-
r
- E
[p
-
y R
°
Tem er ture when Received 'C= accepted°
Delivered Received E
Comments-
ejected: Resample Requested:
Date: I Time:
TIN;