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HomeMy WebLinkAboutNC0025496_Renewal 2015_20150130 CITY OF LINCOLNTON WASTEWATER TREATMENT PLANT Naj9aai�tuaaaa 1111 1 'c- FFP J�_ JSyti t C f tttttttttttt RECEIVED/DENRIDWR January 28,2015 JAN' Mr.Jon Risgaard NCDENR-DWR Water Quality Water Quality Permitting Section/Wastewater Branch Permitting Section 1617 Mail Service Center Raleigh,NC 27699-1617 Dear Mr. Risgaard, Enclosed is the City of Lincolnton Wastewater Treatment Plant NPDES permit renewal application for NPDES Permit NCOO25496.The following items are included in this package: Completed and signed original+2 copies of the NPDES Form 2A Application and Exhibits A and B. If you have any questions or need any additional information about this permit application or exhibits, please do not hesitate to contact me at 704-736-8960 or by e-mail at:donaldburkey(aci.lincolnton.nc.us. Sincerely, g Donald A. Burkey,Jr. WWTP Superintendent City of Lincolnton (704)736-8960 608 WEST Hwy. 150 BY-PASS • P.O. Box 617 • LINCOLNTON, NORTH CAROLINA 28093-0617 PHONE (704) 736-8960 • FAX (704) 732-6137 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVTP, NC0025496 Renewal Catawba FORM - 2A NPDES FORM 2A APPLICATION OVERVIE NPDES APPLICATION OVERVIEW Form 2A has been developed in a modular format and consists of a "Basic Application Information" packet and a "Supplemental Application Information" packet. The Basic Application Information packet is divided into two parts. All applicants must complete Parts A and C. Applicants with a design flow greater than or equal to 0.1 mgd must also complete Part B. Some applicants must also complete the Supplemental Application Information packet. The following items explain which parts of Form 2A you must complete. BASIC APPLICATION INFORMATION: A. Basic Application Information for all Applicants. All applicants must complete questions A.1 through A.8. A treatment works that discharges effluent to surface waters of the United States must also answer questions A.9 through A.12. B. Additional Application Information for Applicants with a Design Flow>_0.1 mgd. AI r a mens wo DENRIDWRign flows greater than or equal to 0.1 million gallons per day must complete questions B.1 through Kt C. Certification. All applicants must complete Part C(Certification). JAN 3 0 2015 SUPPLEMENTAL APPLICATION INFORMATION: Water Quality Permitting Section D. Expanded Effluent Testing Data. A treatment works that discharges effluent to surface waters of the United States and meets one or more of the following criteria must complete Part D(Expanded Effluent Testing Data): 1. Has a design flow rate greater than or equal to 1mgd, 2. Is required to have a pretreatment program(or has one in place), or 3. Is otherwise required by the permitting authority to provide the information. E. Toxicity Testing Data. A treatment works that meets one or more of the following criteria must complete Part E(Toxicity Testing Data): 1. Has a design flow rate greater than or equal to 1 mgd, 2. Is required to have a pretreatment program(or has one in place), or 3. Is otherwise required by the permitting authority to submit results of toxicity testing. F. Industrial User Discharges and RCRA/CERCLA Wastes. A treatment works that accepts process wastewater from any significant industrial users(SIUs)or receives RCRA or CERCLA wastes must complete Part F(Industrial User Discharges and RCRA/CERCLA Wastes). SIUs are defined as: 1. All industrial users subject to Categorical Pretreatment Standards under 40 Code of Federal Regulations(CFR)403.6 and 40 CFR Chapter I, Subchapter N (see instructions); and 2. Any other industrial user that: a. Discharges an average of 25,000 gallons per day or more of process wastewater to the treatment works(with certain exclusions);or b. Contributes a process wastestream that makes up 5 percent or more of the average dry weather hydraulic or organic capacity of the treatment plant;or c. Is designated as an SIU by the control authority. G. Combined Sewer Systems. A treatment works that has a combined sewer system must complete Part G(Combined Sewer Systems). ALL APPLICANTS MUST COMPLETE PART C (CERTIFICATION) EPA Form 3510-2A(Rev. 1-99). Replaces EPA forms 7550-6&7550-22. Page 1 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton V VVTP, NC0025496 Renewal Catawba BASIC APPLICATION INFORMATION PART A.BASIC APPUCATION INFORMATION FOR ALL APPUCANTS: All treatment works must complete questions A.1 through A.8 of this Basic Application Information Packet. A.1. Facility Information. Facility Name City of Lincolnton Wastewater Treatment Plant Mailing Address Post Office Box 617 Lincolnton,North Carolina 28093.0617 Contact Person Mr.Donald Burkev Jr. _ _ RECEIVEDIDENRIDWR Title Operator In Responsible Charge(ORC).WWTP Superintendent JAN 30 2015 Telephone Number (704)7364960 Facility Address 550 Hwy 150 Bypass West Water Quality Permitting section (not P.O.Box) Lincolnton,North Carolina 28092 A.2. Applicant Information. If the applicant is different from the above,provide the following: Applicant Name City of Lincolnton Wastewater Treatment Plant Mailing Address Post Office Box 617 Lincolnton.North Carolina 28093-0617 Contact Person Stephen H.Peeler Title Director of Public Works&Utilities Telephone Number (704)736-8940 Is the applicant the owner or operator(or both)of the treatment works? ® owner U operator Indicate whether correspondence regarding this permit should be directed to the facility or the applicant. 0 facility U applicant A.3. Existing Environmental Permits. Provide the permit number of any existing environmental permits that have been issued to the treatment works (include state-issued permits). NPDES NC0025496 PSD UIC Other RCRA Other A.4. Collection System Information. Provide information on municipalities and areas served by the facility. Provide the name and population of each entity and,if known,provide information on the type of collection system(combined vs.separate)and its ownership(municipal,private,etc.). Name Population Served Type of Collection System Ownership Lincolnton 10.743 Separate Municipal Total population served 10.743 EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 2 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincointon WWTP, NC0025496 Renewal Catawba A.5. Indian Country. a. Is the treatment works located in Indian Country? ❑ Yes ® No b. Does the treatment works discharge to a receiving water that is either in Indian Country or that is upstream from(and eventually flows through)Indian Country? ❑ Yes ® No A.B. Flow. Indicate the design flow rate of the treatment plant(i.e.,the wastewater flow rate that the plant was built to handle). Also provide the average daily flow rate and maximum daily flow rate for each of the last three years. Each year's data must be based on a 12-month time period with the 12th month of"this year"occurring no more than three months prior to this application submittal. a. Design flow rate 6.0 _ mgd Two Years Mw 2012 Last Year 2013 This Year 2014 b. Annual average daily flow rate 2.39 mad (366 Java) 2.55 mad(365 days) 2.40 mgd(365 days) c. Maximum daily flow rate 5.20 mad 12.80 mad 7.40 mad A.7. Collection System. Indicate the type(s)of collection system(s)used by the treatment plant. Check all that apply. Also estimate the percent contribution(by miles)of each. ® Separate sanitary sewer 100 O Combined storm and sanitary sewer % A.8. Discharges and Other Disposal Methods. a. Does the treatment works discharge effluent to waters of the U.S.? ® Yes 0 No If yes,list how many of each of the following types of discharge points the treatment works uses: i. Discharges of treated effluent 1 ii. Discharges of untreated or partially treated effluent 0 iii. Combined sewer overflow points 0 iv. Constructed emergency overflows(prior to the headworks) 0 v. Other 0 b. Does the treatment works discharge effluent to basins,ponds,or other surface impoundments that do not have outlets for discharge to waters of the U.S.? 0 Yes ® No If yes,provide the following for each surface impoundment: Location: Annual average daily volume discharge to surface impoundment(s) mgd Is discharge 0 continuous or 0 intermittent? c. Does the treatment works land-apply treated wastewater? 0 Yes ® No If yes,provide the following for each land application site: Location: Number of acres: Annual average daily volume applied to site: mgd Is land application 0 continuous or 0 intermittent? d. Does the treatment works discharge or transport treated or untreated wastewater to another treatment works? 0 Yes ® No EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6 8,7550-22. Page 3 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVVVTP, NC0025496 Renewal Catawba If yes,describe the mean(s)by which the wastewater from the treatment works is discharged or transported to the other treatment works (e.g.,tank truck,pipe). If transport is by a party other than the applicant,provide: Transporter Name Mailing Address Contact Person Title Telephone Number ( ) For each treatment works that receives this dischame,provide the following: Name Mailing Address Contact Person The Telephone Number ( ) If known,provide the NPDES permit number of the treatment works that receives this discharge Provide the average daily flow rate from the treatment works into the receiving facility. _ mgd e. Does the treatment works discharge or dispose of its wastewater in a manner not induded in A.8.through A.8.d above(e.g.,underground percolation,well injection): 0 Yes ® No If yes,provide the following for each disposal method: Description of method(including location and size of site(s)if applicable): Annual daily volume disposed by this method: Is disposal through this method 0 continuous or 0 intermittent? EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 4 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WVVfP, NC0025496 Renewal Catawba WASTEWATER DISCHARGES: If you answered"Yes"to question A.8.a,complete questions A.9 through A.12 once for each outfall(Including bypass points)through which effluent Is discharged. Do not include information on combined sewer overflows In this section. If you answered"No"to question A.B.ago to Part B,"Additional Application Information for Applicants with a Design Flow Greater than or Equal to 0.1 mgd." A.9. Description of Outfall. a. Outfall number 001 b. Location City of Lincolnton 28093 (City or town,If applicable) (Zip Code) Lincoln North Carolina (County) (State) N35026'26" W81016'44" (Latitude) (Longitude) C. Distance from shore(if applicable) ft. d. Depth below surface(if applicable) ft. e. Average daily flow rate 2.40 mad (2014) mgd f. Does this outfall have either an intermittent or a periodic discharge? 0 Yes ® No (go to A.9.g.) If yes,provide the following information: Number f times per year discharge occurs: Average duration of each discharge: Average flow per discharge: mgd Months in which discharge occurs: g. Is outfall equipped with a diffuser? 0 Yes ® No A.10. Description of Receiving Waters. a. Name of receiving water South Fork Catawba River b. Name of watershed(if known) Catawba United States Soil Conservation Service 14-digit watershed code(if known): c. Name of State Management/River Basin(if known):Catawba United States Geological Survey 8-digit hydrologic cataloging unit code(if known): 03050102 d. Critical low flow of receiving stream(if applicable) acute cfs chronic cfs e. Total hardness of receiving stream at critical low flow(if applicable): _ mg/of CaCO3 EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 5 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WVVfP, NC0025496 Renewal Catawba A.11. Description of Treatment a. What level of treatment are provided? Check all that apply. 0 Primary ® Secondary 0 Advanced 0 Other. Describe: b. Indicate the following removal rates(as applicable): Design BOD5 removal or Design CBOD5 removal 95 % Design SS removal 93 Design P removal 25 Design N removal 78 Other % c. What type of disinfection is used for the effluent from this outfall? If disinfection varies by season,please describe: Sodium Hvpochlorite If disinfection is by chlorination is dechlorination used for this outfall? 0 Yes 0 No Does the treatment plant have post aeration? 0 Yes 0 No A.12. Effluent Testing Information. All Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the Indicated effluent testing required by the permitting authority for each outfall through which effluent Is discharged. Do not include information on combined sewer overflows In this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition,this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 138. At a minimum,effluent testing data must be based on at least three samples and must be no more than four and one-half years apart. Outfall number. 001 _ _ MAXIMUM DAILY VALUE AVERAGE DAILY VALUE PARAMETER Value Units Value Units Number of Samples pH(Minimum) 6.1 s.u. pH(Maximum) 7.4 s.u. Flow Rate 12.8 MGD 2.46 MGD 1065 Temperature(Winter) 25.7 °C 18.8 °C 277 Temperature(Summer) 32.7 °C 26.5 °C 427 *For pH please report a minimum and a maximum daily value MAXIMUM DAILY AVERAGE DAILY DISCHARGE DISCHARGE ANALYTICAL POLLUTANT METHOD ML/MDL Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS BIOCHEMICAL OXYGEN BOD5 54.9 mg/L 6.85 mg/L 727 SM 5210B-2001 2 mg/L DEMAND(Report one) CBOD5 FECAL COLIFORM 81 CFU/100 25.2 CFU/100 36 SM 9222D-1997 Colonies/100mL TOTAL SUSPENDED SOLIDS(TSS) 104 mg/L 9.81 mg/L 726 SM 2540D-1997 2.5 mg/L END OF PART A. REFER TO THE APPLICATION OVERVIEW(PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 8 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVV TP, NC0025496 Renewal Catawba BASIC APPLICATION INFORMATION PART B. ADDITIONAL APPLICATION INFORMATION FOR APPLICANTS WITH A DESIGN FLOW GREATER THAN OR EQUAL TO 0.1 MGD(100,000 gallons per day). All applicants with a design flow rate 2 0.1 mgd must answer questions B.1 through B.S. All others go to Pad C(Certification). B.1. Inflow and Infiltration. Estimate the average number of gallons per day that flow into the treatment works from inflow and/or infiltration. 700,000 gpd Briefly explain any steps underway or planned to minimize inflow and infiltration. B.2. Topographic Map. Attach to this application a topographic map of the area extending at least one mile beyond facility property boundaries. This map must show the outline of the facility and the following information. (You may submit more than one map if one map does not show the entire area.) a. The area surrounding the treatment plant,including all unit processes. b. The major pipes or other structures through which wastewater enters the treatment works and the pipes or other structures through which treated wastewater is discharged from the treatment plant. Include outfalls from bypass piping,if applicable. c. Each well where wastewater from the treatment plant is injected underground. d. Wells,springs,other surface water bodies,and drinking water wells that are: 1)within%mile of the property boundaries of the treatment works,and 2)listed in public record or otherwise known to the applicant. e. Any areas where the sewage sludge produced by the treatment works is stored,treated,or disposed. f. If the treatment works receives waste that is classified as hazardous under the Resource Conservation and Recovery Act(RCRA)by truck,rail, or special pipe,show on the map where the hazardous waste enters the treatment works and where it is treated,stored,and/or disposed. B.3. Process Flow Diagram or Schematic. Provide a diagram showing the processes of the treatment plant,including all bypass piping and all backup power sources or redunancy in the system. Also provide a water balance showing all treatment units,including disinfection(e.g., chlorination and dechlorination). The water balance must show daily average flow rates at influent and discharge points and approximate daily flow rates between treatment units. Include a brief narrative description of the diagram. B.4. Operation/Maintenance Performed by Contractor(s). Are any operational or maintenance aspects(related to wastewater treatment and effluent quality)of the treatment works the responsibility of a contractor? 0 Yes ® No If yes,list the name,address,telephone number,and status of each contractor and describe the contractor's responsibilities(attach additional pages if necessary). Name: Mailing Address: Telephone Number: j ) Responsibilities of Contractor. B.5. Scheduled Improvements and Schedules of Implementation. Provide information on any uncompleted implementation schedule or uncompleted plans for improvements that will affect the wastewater treatment,effluent quality,or design capacity of the treatment works. If the treatment works has several different implementation schedules or is planning several improvements,submit separate responses to question B.5 for each. (If none,go to question B.6.) a. List the outfall number(assigned in question A.9)for each outfall that is covered by this implementation schedule. b. Indicate whether the planned improvements or implementation schedule are required by local,State,or Federal agencies. ❑ Yes ❑ No EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 7 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton INV TP, NC0025496 Renewal Catawba c. If the answer to B.5.b is"Yes,"briefly describe,including new maximum daily inflow rate(if applicable). d. Provide dates imposed by any compliance schedule or any actual dates of completion for the implementation steps listed below,as applicable. For improvements planned independently of local,State,or Federal agencies,indicate planned or actual completion dates,as applicable. Indicate dates as accurately as possible. Schedule Actual Completion Implementation Stage MM/DD/YYYY MM/DD/YYYY -Begin Construction I l / / -End Construction I I / / -Begin Discharge / / / / -Attain Operational Level / / / / e. Have appropriate permits/clearances concerning other Federal/State requirements been obtained? 0 Yes 0 No Describe briefly: B.B. EFFLUENT TESTING DATA(GREATER THAN 0.1 MGD ONLY). Applicants that discharge to waters of the US must provide effluent testing data for the following parameters. Provide the indicated effluent testing required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combine sewer overflows in this section. Ail information reported must be based on data collected through analysis conducted using 40 CFR Part 138 methods. In addition,this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. At a minimum effluent testing data must be based on at least three pollutant scans and must be no more than four and on-half years old. Outfall Number: 001 MAXIMUM DAILY AVERAGE DAILY DISCHARGE ANALYTICAL ML/MDL DISCHARGE METHOD POLLUTANT Conc. Units Conc. Units Number of Samples CONVENTIONAL AND NON CONVENTIONAL COMPOUNDS AMMONIA(as N) 13.7 mg/L 2.13 mg/L 455 SM 4500NH3-1997 0.1 CHLORINE(TOTAL 49 ug/L 15.2 ug/L 727 SM 4500CLG-2000 20 RESIDUAL,TRC) DISSOLVED OXYGEN 7.26 mg/I 7.04 mg/I 3 SM 4500-H B 0.1 TOTAL KJELDAHL 34 mg/L 6.4 mg/L 34 EPA 351.2 0.5 NITROGEN(TKN) NITRATE PLUS NITRITE 5.3 mg/L 2.4 mg/L 34 SM 4500-NO3F 0.1 NITROGEN OIL and GREASE 5.8 mg/I 5.3 mg/ 3 EPA 1664A 5 PHOSPHORUS(Total) 5 mg/L 1.75 mg/L 35 SM 4500-P F 0.100 TOTAL DISSOLVED SOLIDS 380 mg/I 346.7 mg/ 3 SM 2540C 50 (TDS) OTHER Chloride 38 mg/I 36.3 mg/I 3 EPA 300 0.15 END OF PART B. REFER TO THE APPLICATION OVERVIEW(PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 8 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVfP, NC0025496 Renewal Catawba BASIC APPLICATION INFORMATION PART C. CERTIFICATION All applicants must complete the Certification Section. Refer to instructions to determine who is an officer for the purposes of this certification. All applicants must complete all applicable sections of Form 2A,as explained in the Application Overview. Indicate below which parts of Form 2A you have completed and are submitting. By signing this certification statement,applicants confirm that they have reviewed Form 2A and have completed all sections that apply to the facility for which this application is submitted. Indicate which parts of Form 2A you have completed and are submitting: ® Basic Application Information packet Supplemental Application Information packet: El Part D(Expanded Effluent Testing Data) El Part E(Toxicity Testing: Biomonitoring Data) El Part F(Industrial User Discharges and RCRA/CERCLA Wastes) 0 Part G(Combined Sewer Systems) ALL APPUCANTS MUST COMPLETE THE FOLLOWING CERTIFICATION. I certify under penalty of law that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system or those persons directly responsible for gathering the information,the information is,to the best of my knowledge and belief,true, accurate,and complete. I am aware that there are significant nalties for submitting false information,including the possibility of fine and imprisonment for knowing violations. Name and official title Mr.Sten n Haii0141111f, Di : Aligat",•tilitles_ Signature •//-4....e Telephone number (704) 36-8 Date signed Upon request of the permitting authority,you must submit any other information necessary to assure wastewater treatment practices at the treatment works or identify appropriate permitting requirements. SEND COMPLETED FORMS TO: NCDENR/DWQ Attn: NPDES Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 9 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVVVfP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART D. EXPANDED EFFLUENT TESTING DATA Refer to the directions on the cover page to determine whether this section applies to the treatment works. Effluent Testing: 1.0 mgd and Pretreatment Works. If the treatment works has a design flow greater than or equal to 1.0 mgd or it has(or is required to have)a pretreatment program,or is otherwise required by the permitting authority to provide the data,then provide effluent testing data for the following pollutants. Provide the indicated effluent testing information and any other information required by the permitting authority for each outfall through which effluent is discharged. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analyses conducted using 40 CFR Part 136 methods. In addition,these data must comply with QA/QC requirements of 40 CFR Part 138 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. Indicate in the blank rows provided below any data you may have on pollutants not specifically listed in this form. At a minimum,effluent testing data must be based on at least three pollutant scans and must be no more than four and one-half years old. Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT Number ANALYTICAL MUMDL Conc. Units Mass Units Conc. Units Mass Units of METHOD Samples METALS(TOTAL RECOVERABLE),CYANIDE,PHENOLS,AND HARDNESS. ANTIMONY 0.075 mg/L 0.037 mg/L 36 EPA 200.7 0.010 _ ARSENIC 0.0026 mg/L 0.0002 mg/L 35 EPA 200.8 0.001 BERYLLIUM <0.001 mg/L <0.001 mg/L 3 EPA 200.8 0.001 CADMIUM 0.0077 mg/L 0.00029 mg/L 36 EPA 200.8 0.001 CHROMIUM 0.053 mg/L 0.00593 mg/L 35 EPA 200.8 0.005 COPPER 0.030 mg/L 0.00929 mg/L 39 EPA 200.8 0.005 LEAD 0.060 mg/L 0.00289 mg/L 35 EPA 200.8 0.005 MERCURY 0.0000121 mg/L 0.00000466 mg/L 35 EPA 1631E 1 ng/I NICKEL 0.0092 mg/L 0.0014 mg/L 35 EPA 200.8 0.002 SELENIUM 0.010 mg/L 0.00106 mg/L 35 EPA 200.8 0.001 SILVER 0.005 mg/L 0.00025 mg/L 35 EPA 200.8 0.001 THALLIUM <0.001 mg/L <0.001 mg/L 3 EPA 200.8 0.001 ZINC 0.097 mg/L 0.042 mg/L 39 EPA 200.8 0.005 CYANIDE 0.017 mg/L 0.004 mg/L 48 SM 194500 0.006 TOTAL PHENOLIC 0.017 mg/L 0.005 mg/L 48 EPA 420.1 0.006 COMPOUNDS HARDNESS(as 31 mg/L 30 mg/L 3 EPA 200.7 0.61 CaCO3) Use this space(or a separate sheet)to provide information on other metals requested by the permit writer EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 10 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE Number ANALYTICAL POLLUTANT Conc. Units Mass Units Conc. Units Mass Units of METHOD ML/MDL Samples VOLATILE ORGANIC COMPOUNDS ACROLEIN <0.100 mg/L <0.100 mg/L 3 EPA 624 0.1 ACRYLONITRILE <0.100 mg/L <0.100 mg/L 3 EPA 624 0.1 BENZENE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.006 BROMOFORM <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 CARBON <0.005 mg/L <0.006 mg/L 3 EPA 624 0.005 TETRACHLORIDE CHLOROBENZENE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 CHLORODIBROMO- <0.006 mg/L <0.005 mg/L 3 EPA 624 0.005 METHANE CHLOROETHANE <0.010 mg/L <0.010 mg/L 3 EPA 624 0.010 2-CHLOROETHYLVINYL <0.010 mg/L <0.010 mg/L 3 EPA 624 0.010 ETHER CHLOROFORM <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 DICHLOROBROMO- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 METHANE 1,1-DICHLOROETHANE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 1,2-DICHLOROETHANE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 TRANS-I,2-DICHLORO- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 ETHYLENE 1,1-DICHLORO- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 ETHYLENE 1,2- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 DICHLOROPROPANE 1,3-DICHLORO- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 PROPYLENE ETHYLBENZENE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 METHYL BROMIDE <0.010 mg/L <0.010 mg/L 3 EPA 624 0.010 METHYL CHLORIDE <0.010 mg/L <0.010 mg/L 3 EPA 624 0.010 METHYLENE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 CHLORIDE 1,1,2,2-TETRA <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 CHLOROETHANE TETRACHLORO- <0.005 mg/L <0.006 mg/L 3 EPA 624 0.005 ETHYLENE TOLUENE <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 11 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANT Unit Number ANALYTICAL Conc. Units Mass Units Conc. s Mass Units of METHOD MLANDL Samples 1,1,1- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 TRICHLOROETHANE 1'1'2- <0.005 mg/L <0.005 mg/L 3 EPA 624 0.005 TRICHLOROETHANE TRICHLOROETHYLENE <0.006 mg/L <0.005 mg/L 3 EPA 624 0.006 VINYL CHLORIDE <0.010 mg/L <0.010 mg/L 3 EPA 624 0.010 Use this space(or a separate sheet)to provide information on other volatile organic compounds requested by the permit writer ACID-EXTRACTABLE COMPOUNDS P-CHLOROMA-CRESOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2-CHLOROPHENOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2,4-DICHLOROPHENOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2,4-DIMETHYLPHENOL <0.010 mg/L <0.010 mg/L 3 EPA 825 0.010 4,6-DINITRO-O- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 CRESOL 2,4-DINITROPHENOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2-NITROPHENOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 4-NITROPHENOL <0.050 mg/L <0.050 mg/L 3 EPA 625 0.050 PENTACHLOROPHENOL <0.010 mg/L <0.010 mg/I 3 EPA 625 0.010 PHENOL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2,4,8- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 TRICHLOROPHENOL Use this space(or a separate sheet)to provide information on other acid-extractable compounds requested by the permit writer BASE-NEUTRAL COMPOUNDS ACENAPHTHENE <0.010 mg/L <0.010 mg/I 3 EPA 625 0.010 ACENAPHTHYLENE <0.010 mg/L <0.010 mgA 3 EPA 625 0.010 ANTHRACENE <0.010 mg/L <0.010 mg/I 3 EPA 625 0.010 BENZIDINE <0.100 mg/L <0.100 mg/I 3 EPA 625 0.100 BENZO(A)ANTHRACEN <0.010 mg/L <0.010 mg/I 3 EPA 625 0.010 E I BENZO(A)PYRENE <0.010 mg/L <0.010 mg/I 3 EPA 625 0.010 EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 12 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVTP, NC0025496 Renewal Catawba Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) ANALYTICAL MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE MLJMDL METHOD POLLUTANT Number Conc. Units Mass Units Conc. Units Mass Units of Samples 3,4 BENZO- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 FLUORANTHENE BENZO(GHI)PERYLENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 BENZO(K) <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 FLUORANTHENE BIS(2- CHLOROETHOXY) <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 METHANE BIS(2-CHLOROETHYL)- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 ETHER BIS(2-CHLOROISO- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PROPYL)ETHER BIS(2-ETHYLHEXYL) 0.059 mg/L 0.036 mg/L 3 EPA 625 0.010 PHTHALATE 4-BROMOPHENYL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHENYL ETHER BUTYL BENZYL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHTHALATE 2-CHLORO- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 NAPHTHALENE 4-CHLORPHENYL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHENYL ETHER CHRYSENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 DI-N-BUTYL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHTHALATE DI-N-OCTYL <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHTHALATE DIBENZO(A,H) <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 ANTHRACENE 1,2 <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 DICHLOROBENZENE 1,3- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 DICHLOROBENZENE 1,4- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 DICHLOROBENZENE 3,3-DICHLORO- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 BENZIDINE DIETHYL PHTHALATE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 DIMETHYL PHTHALATE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 2,4-DINITROTOLUENE <0.010 mg/L <0.010 mg/L 3 EPA 626 0.010 2,6-DINITROTOLUENE <0.010 mg/L <0.010 mg/L 3 EPA 626 0.010 1,2-DIPHENYL- <0.010 mg/L <0.010 mg/L 3 EPA 626 0.010 HYDRAZINE EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 13 of 22 FACILITY NAME AND PERMIT NUMBER: 1 PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVV TP, NC0025496 Renewal Catawba Outfall number. 001 (Complete once for each outfall discharging effluent to waters of the United States.) MAXIMUM DAILY DISCHARGE AVERAGE DAILY DISCHARGE POLLUTANTNumber ANALYTICAL ML/MDL Conc. Units Mass Units Conc. Usrt Mass Units of METHOD Samples FLUORANTHENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 FLUORENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 HEXACHLOROBENZEN <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 E HEXADIENE - <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 BUTADIENE HEXACHLOROCYCLO- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PENTADIENE HEXACHLOROETHANE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 INDENO(1,2,3-CD) <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PYRENE ISOPHORONE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 NAPHTHALENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 NITROBENZENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 N-NITROSODI-N- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PROPYLAMINE N-NITROSODI- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 METHYLAMINE N-NITROSODI- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PHENYLAMINE PHENANTHRENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 PYRENE <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 1,2,4- <0.010 mg/L <0.010 mg/L 3 EPA 625 0.010 TRICHLOROBENZENE Use this space(or a separate sheet)to provide information on other base-neutral compounds requested by the permit writer Use this space(or a separate sheet)to provide information on other pollutants(e.g.,pesticides)requested by the permit writer END OF PART D. REFER TO THE APPLICATION OVERVIEW(PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 14 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVfP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART E. TOXICITY TESTING DATA POTWs meeting one or more of the following criteria must provide the results of whole effluent toxicity tests for acute or chronic toxicity for each of the facility's discharge points: 1)POTWs with a design flow rate greater than or equal to 1.0 mgd;2)POTWs with a pretreatment program(or those that are required to have one under 40 CFR Part 403);or 3)POTWs required by the permitting authority to submit data for these parameters. • At a minimum,these results must indude quarterly testing for a 12-month period within the past 1 year using multiple species(minimum of two species),or the results from four tests performed at least annually in the four and one-half years prior to the application,provided the results show no appreciable toxicity,and testing for acute and/or chronic toxicity,depending on the range of receiving water dilution. Do not include information on combined sewer overflows in this section. All information reported must be based on data collected through analysis conducted using 40 CFR Part 136 methods. In addition,this data must comply with QA/QC requirements of 40 CFR Part 136 and other appropriate QA/QC requirements for standard methods for analytes not addressed by 40 CFR Part 136. • In addition,submit the results of any other whole effluent toxicity tests from the past four and one-half years. If a whole effluent toxicity test conducted during the past four and one-half years revealed toxicity,provide any information on the cause of the toxicity or any results of a toxicity reduction evaluation,if one was conducted. • If you have already submitted any of the information requested in Part E,you need not submit it again. Rather,provide the information requested in question E.4 for previously submitted information. If EPA methods were not used,report the reasons for using alternate methods. If test summaries are available that contain all of the information requested below,they may be submitted in place of Part E. If no biomonitoring data is required,do not complete Part E. Refer to the Application Overview for directions on which other sections of the form to complete. E.1. Required Tests. Indicate the number of whole effluent toxicity tests conducted in the past four and one-half years. ®chronic 0 acute [ See Attached Toxicity Data ] E.2. Individual Test Data. Complete the following chart forg#Qh whole effluent toxicity test conducted in the last four and one-half years. Allow one column per test(where each species constitutes a test). Copy this page if more than three tests are being reported. Test number. Test number. Test number. a. Test information. Test Species&test method number Age at initiation of test Outfall number Dates sample collected Date test started Duration b. Give toxicity test methods followed. Manual title Edition number and year of publication Page number(s) c. Give the sample collection method(s)used. For multiple grab samples,indicate the number of grab samples used. 24-Hour composite Grab d. Indicate where the sample was taken in relation to disinfection. (Check all that apply for each. Before disinfection After disinfection After dechlorination EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 15 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba Test number Test number. Test number e. Describe the point in the treatment process at which the sample was collected. Sample was collected: f. For each test,include whether the test was intended to assess chronic toxicity,acute toxicity,or both Chronic toxicity Acute toxicity g. Provide the type of test performed. Static Static-renewal Flow-through h. Source of dilution water. If laboratory water,specify type;if receiving water,specify source. Laboratory water Receiving water i. Type of dilution water. If salt water,specify"natural'or type of artificial sea salts or brine used. Fresh water Salt water j. Give the percentage effluent used for all concentrations in the test series. k. Parameters measured during the test. (State whether parameter meets test method specifications) pH Salinity Temperature Ammonia Dissolved oxygen I. Test Results. Acute: Percent survival in 100% effluent LCro 95%C.I. X X X Control percent survival X X X Other(describe) EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 18 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WVVfP, NC0025496 Renewal Catawba Chronic: NOEC IC25 Control percent survival Other(describe) m. Quality Control/Quality Assurance. Is reference toxicant data available? Was reference toxicant test within acceptable bounds? What date was reference toxicant test run(MM/DD/YYYY)? Other(describe) E.3. Toxicity Reduction Evaluation. Is the treatment works involved in a Toxicity Reduction Evaluation? ❑ Yes ® No If yes,describe: E.4. Summary of Submitted Blomonitoring Test Information. If you have submitted biomonitoring test information,or information regarding the cause of toxicity,within the past four and one-half years,provide the dates the information was submitted to the permitting authority and a summary of the results. Date submitted: / / (MMIDD/YYYY) Summary of results: (see instructions) December 2012 DMR and January 2013 DMR(Heavy Rain-8"+) END OF PART E. REFER TO THE APPLICATION OVERVIEW(PAGE 1)TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 17 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject to,an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. a. Number of non-categorical Sills. 4 b. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: VT LeeBoy Mailing Address: 500 Lincoln County Parkway Ext. Lincolnton,NC 28092 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Manufacture Paving Equipment F.S. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Raw material(s): Raw steel parts,phosphate chemical solutions,sodium hydroxide F.6. Flow Rate. a. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 1500 gpd ( continuous or X intermittent) b. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 1000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards,which category and subcategory? Category 433 EPA Form 3510-2A(Rev. 1-99). Replaces EPA forms 7550-6&7550-22. Page 18 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVVVfP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? ❑ Yes ® No If yes,describe each episode. RCRA HAZARDOUS WASTE RECEIVED BY TRUCK, RAIL,OR DEDICATED PIPELINE: F.9. RCRA Waste. Does the treatment works receive or has it in the past three years received RCRA hazardous waste by truck,rail or dedicated pipe? ❑ Yes ® No(go to F.12) F.10. Waste transport. Method by which RCRA waste is received(check all that apply): ❑ Truck 0 Rail 0 Dedicated Pipe F.11. Waste Description. Give EPA hazardous waste number and amount(volume or mass,specify units). EPA Hazardous Waste Number Amount Units CERCLA(SUPERFUND)WASTEWATER, RCRA REMEDIATION/CORRECTIVE ACTION WASTEWATER,AND OTHER REMEDIAL ACTIVITY WASTEWATER: F.12. Remediation Waste. Does the treatment works currently(or has it been notified that it will)receive waste from remedial activities? O Yes(complete F.13 through F.15.) ® No F.13. Waste Origin. Describe the site and type of facility at which the CERCLA/RCRA/or other remedial waste originates(or is excepted to origniate in the next five years). F.14. Pollutants. List the hazardous constituents that are received(or are expected to be received). Include data on volume and concentration,if known. (Attach additional sheets if necessary.) F.15. Waste Treatment a. Is this waste treated(or will be treated)prior to entering the treatment works? ❑ Yes ❑ No If yes,describe the treatment(provide information about the removal efficiency): b. Is the discharge(or will the discharge be)continuous or intermittent? ❑ Continuous 0 Intermittent If intermittent,describe discharge schedule. END OF PART F. REFER TO THE APPLICATION OVERVIEW(PAGE 1) TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-6&7550-22. Page 19 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVVVTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART G. COMBINED SEWER SYSTEMS If the treatment works has a combined sewer system,complete Part G. G.1. System Map. Provide a map indicating the following: (may be included with Basic Application Information) a. All CSO discharge points. b. Sensitive use areas potentially affected by CSOs(e.g.,beaches,drinking water supplies,shellfish beds,sensitive aquatic ecosystems,and outstanding natural resource waters). c. Waters that support threatened and endangered species potentially affected by CSOs. G.2. System Diagram. Provide a diagram,either in the map provided in G.1 or on a separate drawing,of the combined sewer collection system that includes the following information. a. Location of major sewer trunk lines,both combined and separate sanitary. b. Locations of points where separate sanitary sewers feed into the combined sewer system. c. Locations of in-line and off-line storage structures. d. Locations of flow-regulating devices. e. Locations of pump stations. CSO OUTFALLS: Complete questions G.3 through G.6 once for each CSO discharge point. G.3. Description of Outfall. a. Outfall number b. Location (City or town,if applicable) (Zip Code) (County) (State) (Latitude) (Longitude) c. Distance from shore(if applicable) ft. d. Depth below surface(if applicable) ft. e. Which of the following were monitored during the last year for this CSO? ❑ Rainfall ❑ CSO pollutant concentrations ❑ CSO frequency 0 CSO flow volume ❑ Receiving water quality f. How many storm events were monitored during the last year? G.4. CSO Events. a. Give the number of CSO events in the last year. events (❑actual or❑approx.) b. Give the average duration per CSO event. hours (❑actual or❑approx.) EPA Form 3510-2A(Rev. 1-99). Replaces EPA forms 7550-6&7550-22. Page 20 of 22 FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVfP, NC0025496 Renewal Catawba c. Give the average volume per CSO event. million gallons(0 actual or 0 approx.) d. Give the minimum rainfall that caused a CSO event in the last year Inches of rainfall G.5. Description of Receiving Waters. a. Name of receiving water. b. Name of watershed/river/stream system: United State Soil Conservation Service 14-digit watershed code(if known): c. Name of State Management/River Basin: United States Geological Survey 8-digit hydrologic cataloging unit code(if known): G.6. CSO Operations. Describe any known water quality impacts on the receiving water caused by this CSO(e.g.,permanent or intermittent beach dosings,permanent or intermittent shell fish bed closings,fish kills,fish advisories,other recreational loss,or violation of any applicable State water quality standard). END OF PART G. REFER TO THE APPLICATION OVERVIEW(PAGE 1)TO DETERMINE WHICH OTHER PARTS OF FORM 2A YOU MUST COMPLETE. a EPA Form 3510-2A(Rev.1-99). Replaces EPA forms 7550-8&7550-22. Page 21 of 22 Additional information,if provided,will appear on the following pages. NPDES FORM 2A Additional information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WVVTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users(Sills)and Categorical Industrial Users(CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. c. Number of non-categorical Sills. 4 d. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Kaco USA,Inc Mailing Address: 1101 Lincoln County Parkway Lincolnton, NC 28092 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s). Automotive Seals Raw material(s): Steel alloys,synthetic rubber,bonding agents,chemical agents F.6. Flow Rate. c. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 1,600 gpd ( continuous or X intermittent) d. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 1000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes D No If subject to categorical pretreatment standards,which category and subcategory? Category 433 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Wast*Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? ❑ Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. e. Number of non-categorical SlUs. 4 f. Number of CIOs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Cataler North America Mailing Address: 2002 Cataler Drive Lincolnton,NC 28092 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Catalytic Converters Raw material(s): Precious metals,rare earth oxides,barium sulfate F.6. Flow Rate. e. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 20.000 gpd ( continuous or X intermittent) f. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 5900 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits EI Yes ❑ No b. Categorical pretreatment standards ❑ Yes ® No If subject to categorical pretreatment standards,which category and subcategory? NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVV TP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVWTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION ART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? ❑ Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIOs). Provide the number of each of the following types of industrial users that discharge to the treatment works. g. Number of non-categorical SIUs. 4 h. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: McMurray Fabrics Mailing Address: 1140 N.Flint Street Lincolnton,NC 28092 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Manufacture and finish fabric F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Fabrics Raw material(s): Fabric Dyes F.S. Flow Rate. g. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 304,000 gpd ( continuous or X intermittent) h. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 5000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards EI Yes ❑ No If subject to categorical pretreatment standards,which category and subcategory? 410 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton V V TP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WVVTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRAICERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? EI Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIOs). Provide the number of each of the following types of industrial users that discharge to the treatment works. i. Number of non-categorical SIUs. 4 j. Number of CIUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: South Fork Industries Mailing Address: PO Box 1220 Lincolnton,NC 28093 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Fabric Finishing and Dyeing F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Fabric Finishing and Dyeing Raw material(s): Fabric Dyes F.6. Flow Rate. i. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 322,000 gpd ( continuous or X intermittent) j. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 2000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits EI Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards,which category and subcategory? 410 NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VVVVfP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRAJCERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? ❑ Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. k. Number of non-categorical SIUs. 4 I. Number of ClUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: Mohican Mills Mailing Address: PO Box 190 Lincolnton, NC 28093 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. Manufacture of fabrics and lace,and dyeing fabric and lace F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Fabric and Lace Raw material(s): Fabric and Lace dyes F.6. Flow Rate. k. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 668,000 gpd ( continuous or X intermittent) I. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 5000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards ® Yes ❑ No If subject to categorical pretreatment standards,which category and subcategory? 410 NPDES FORM 2A Additional Information FACIUTY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton WWTP, NC0025496 Renewal Catawba SUPPLEMENTAL APPLICATION INFORMATION PART F.INDUSTRIAL USER DISCHARGES AND RCRA/CERCLA WASTES All treatment works receiving discharges from significant industrial users or which receive RCRA,CERCLA,or other remedial wastes must complete part F. GENERAL INFORMATION: F.1. Pretreatment program. Does the treatment works have,or is subject ot,an approved pretreatment program? ® Yes ❑ No F.2. Number of Significant Industrial Users(SIUs)and Categorical Industrial Users(CIUs). Provide the number of each of the following types of industrial users that discharge to the treatment works. m. Number of non-categorical SIUs. 4 n. Number of ClUs. 3 SIGNIFICANT INDUSTRIAL USER INFORMATION: 1111111.11.11.11M1111.0 Supply the following information for each SIU. If more than one SIU discharges to the treatment works,copy questions F.3 through F.8 and provide the information requested for each SIU. F.3. Significant Industrial User Information. Provide the name and address of each SIU discharging to the treatment works. Submit additional pages as necessary. Name: G&W NC Laboratories LLC Mailing Address: 1877 Kawai Road Lincolnton. NC 28092 F.4. Industrial Processes. Describe all the industrial processes that affect or contribute to the SIU's discharge. F.5. Principal Product(s)and Raw Material(s). Describe all of the principal processes and raw materials that affect or contribute to the SIU's discharge. Principal product(s): Compounding/Formulating Medications Raw material(s): Pharmaceutical Ingredients F.6. Flow Rate. m. Process wastewater flow rate. Indicate the average daily volume of process wastewater discharge into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 16.000 gpd ( continuous or X intermittent) n. Non-process wastewater flow rate. Indicate the average daily volume of non-process wastewater flow discharged into the collection system in gallons per day(gpd)and whether the discharge is continuous or intermittent. 3000 gpd ( continuous or X intermittent) F.7. Pretreatment Standards. Indicate whether the SIU is subject to the following: a. Local limits ® Yes ❑ No b. Categorical pretreatment standards El Yes ❑ No If subject to categorical pretreatment standards,which category and subcategory? Category 439,Subpart D NPDES FORM 2A Additional Information FACILITY NAME AND PERMIT NUMBER: PERMIT ACTION REQUESTED: RIVER BASIN: Lincolnton VWVfP, NC0025496 Renewal Catawba F.8. Problems at the Treatment Works Attributed to Waste Discharge by the SIU. Has the SIU caused or contributed to any problems(e.g., upsets,interference)at the treatment works in the past three years? 0 Yes ® No If yes,describe each episode. NPDES FORM 2A Additional Information NPDES Renewal Exhibit A Lincolnton WWTP,NC0025496 EPA FORM 2A—PART B Catawba Maps and Figures Facility Information Latitude: 35 deg 26 min 34 sec Longitude: 81 deg 15 min 39 sec Quad No.: F13NE Receiving Stream: South Fork Catawba Sub -Basin: 03-08-35 Stream Class: WS-Iv 0 100200 400 600 800 Feet City of Uncolnton 2010 NPDES Permit Pease Associates 2009027 MAIN LIFT STATION )STORAGE RINE CONTACT TANK /;� ^ /"''�' • ~—. ANAEROBIC DIGESTERS INFLUENT FLOW METER CHEMICAACILITIES y ' •' / INFLUENT FILTERSCREEN T EFFLUENT FLOW METER` /;' • /� - • = / VORTEX GRIT REMOVAL SYSTEM Gz DISSOLVED AIR FLOTATION THICKENER FINAL CLARIFIERS '/� _ , /• OXIDATION DITCH 6.4 M H 104 // _. ,+ _ � ' �: essrx.:.-• •moo RETURN SLUDGE PUMPING STATION looe dA 100 YEAR FLOOD BOUNDARY E;s LAB/OFFICE BUILDING AERATION BASINS" `►� `'� o- pm*WvWl e [ ( / E. K-m i' 140 O Wrl' M-c ON m5ii ` J V rt o 0 CD o r 0 n o cn o 0 rn Z cD n 3 w rn m 3 CD w Not"MmoiHma ONV N0LLtlNItl0l"3 I— --_ — — _—_ --_ 7---- _--- --_ >� — —_ —_—'_l . NPDES Renewal Exhibit B Lincolnton WWTP,NC0025496 EPA FORM 2A—PART E Catawba Toxicity Scan Reports Pace Analytical Services, Inc. Pace Analytical Services, Inc. 9800 Kincey Avenue, Suite 100 2225 Riverside Drive Huntersville, NC 28078 Asheville, NC 28804 'aceAnalytical® Phone:704.875.9092 Fax 704.875.9091 Phone:828.254.7176 Fax:828.252.4618 www.pacelabs.com Effluent Toxicity Report AT-1 Form Chronic Pass/Fail and Acute LC50 Date: 9/29/2010 • Facility: LincolntonWWTP NPDES#NC 0025496 Pipe# 001 County Lincoln Laboratory P rforming Test PACE Analytical Services, Inc. Comments Signature of erator in Responsible Charg • xsianature of Laboratory Supervisor Samples Not Aerated Unless Otherwise Noted , Environmental Sciences BranchMITSIME, t MAIL ORIGINAL TO: Div.of N C.D NatRer Quality Calculated t -2.122 1621 Mail Service Center Tabular t 2.508 Raleigh,North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test %Reduction 0 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 %Mortalit Av.Re.rod. #Young Produced 29 27 26 26 18 20 26 20 25 22 28 29 Control Control Adult (L)ive(D)ead L LLLLLLLLLL L 0.00 24.70 • Treatment 2 Treatment 2 Effluent% 11 0.0 27.90 Control CV TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 15.2 PASS FAIL #Young Produced 20 30 34 28 28 27 30 24 27 30 32 25 %control organisms X . producing 3rd brood Adult (L)ive(D)ead LLLLLLLLLLL L 100.0 Check One 1st 1st 2nd Complete This For Either Test Test Start Date: pH Control 7.5 7.5 7.1 8.5 7.4 7.4 Collection Start Date Treatment 7.3 7.4 7.3 7.7 7.7 7.8 Sample 1 9/20/10 Sample 2 9/23/10 S E S E S E t n t n t Sample Type/Duration ro n � v� ! a d a d a d Grab Comp. Duration ' 2. -1 w -i r r r Sample 1 x X s t t t o X 24.08 hr o 3 0 3 1st 1st 2nd Sample 2 ..R- . a X 24.07 hrm D.O. Control 7.5 7.9 7.4 8.0 7.5 7.7 Hardness(mg/l) .... Treatment 7.5 7.8 7.5 8.0 8.1 8.0 Spec.Cond.(umhos/cm) MEI ... 809 Chlorine(mg/1) LC50/Acute Toxicity Test Sample temp.at receipt(C) 1B1® (Mortality exoressed as%.combining reolicatesl % % % % % % % % % Concentration Note: Please % % % % % % % % % Complete This Mortality Section also ; LC50= % Method of Determination start/end start/end. 95% Confidence Moving Avg. Probit Control % - % Spearman Other High Fp 151-1 Conc. U Organism Tested: Ceriodaphnia dubia Test Duration(Hours): . Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs NC Wastewater 40 This report shall not be reproduced,except in full, NC Wastewater 12 NC Drinking Water 37712 NC Drinking Water 37706 SC 99030 without the written consent of Pace Analytical Services, Inc. SC 99006 FL NELAP E87648 'M ."�" FL NELAP E87627 M1 O p'N `neh ,C Pace Analytical Services, Inc. Pace Analytical Services,Inc. 9800 Kincey Avenue,Suite 100 2225 Riverside Drive Huntersville, NC 28078 Asheville,NC 28804 ace Analytical® Phone:704.875.9092 Fax:704.875.9091 Phone:828.254.7176 Fax:828.252.4618 www.pacelabs.com Effluent Toxicity Report AT-1 Form Chronic Pass/Fail and Acute LC50 •• Date: 12/16/10 Facility: LincolntonWWTP NPDES#NC 0025496 Pipe# 001 County Lincoln La -tory Perforrr'ng Test PACE Analytical Services, Inc. 1 ,JF�fI• Comments Sig/ture of Operator in Respo le Charge • _.../ , /VA ,Sionatra of Laboratory Supervisor Samples Not Aerated Unless Otherwise Noted Environmental Sciences Branch Chronic Test Results MAI L ORIGINAL TO. Dv.of WNIC.DENR Quality Rank Sum 159 1621 Mail Service Center 1-Tailed Critical 109 Raleigh,North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test %Reduction 0 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 1 %Mortality h Ayg.Reprod I • #Young Produced 24 27 31 25 33 24 20 6 21 33 33 31 Control Control Adult (L)ive(D)ead L LLLLLLLLLL L 0.00 25.70 Treatment 2 Treatment 2 Effluent% 11 8.3 26.60 Cnntml CV TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 30.3 PASS FAIL i #Young Produced 31 0 23 25 31 31 20 24 34 36 35 29 %controlorganbrre x F:; Adult (L)ive(D)ead L d L L L L L L LLL L prodicing Check One Complete This For Either Test Test Start Date:I 1st 1st 2nd ( I 12/8/10 pH Control 7.5 7.9 7.3 7.4 7.3 7.5 Collection Start Date Treatment 7.5 7.6 7.4 8.1 7.4 _ 7.7 sample 1 12/6/10 Sample 2 12/9/10 S E S E S E 1 n t n t Sample Type/Duration ro n !� vig a d a d a d Grab Comp. Duration -- ga' -I r r r Sample 1 ■© v X X t t 1 24.23 M 1) 6 1st 1st 2nd Sample 2 ©® m . m D.O. Control 7.9 7.9 8.1 8.2 7.3 8.5 Hardness(mg/1) Treatment 7.9 8.3 8.0 8.5 8.3 8.4 Spec.Cond.(umhos/cm) 130el 720 Chlorine(mg/1) ::: <0.1 <0.1 LC50/Acute Toxicity Test Sample temp.at receipt(C) :• !. In® (Mortality expressed as%.combining reolicatesl % . % % % % % % % % 4 Concentration Note: Please % % % % % % % % % Complete This Mortality Section also LC50= % Method of Determination start/end startiend 95% Confidence Moving Avg. Probit Control ■■ % - % Spearman Other High MilConc. p 1.•. Organism Tested: Ceriodaphnia dubia Test Duration(Hours): . Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs NC Wastewater 40 NC Wastewater 12 NC Drinking Water 37712 This report shall not be reproduced,except in full, NC Drinking Water 37706 without the written consent of Pace Analytical Services, Inc. SC 99030 SC 99006 FL NELAP E87648 4o M ACCC90*`C FL NELAP E87627 • Melac Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/24/11 Facility: CITY OF LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labor tory Performing Test: TRITEST, INC. Comments: S mature of Oper , n Respon ' le Charge X /' m..d+,v -`.0 Signature of Labo/- ory Supe sor * PASSED: 5.32% Reduction * Work Order: 1103-01081 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 0.543 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 5.32 % Mortality Avg.Reprod. # Young Produced 26 20 28 24 20 19 25 19 22 16 26 18 - 0.00 21.92 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L - 0.00 20.75 Treatment 2 Treatment 2 Effluent %: 11% , TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 17.343% PASS FAIL # Young Produced 12 28 15 17 33 29 20 22 21 20 14 18 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 1005 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 03/16/11 Control 7.67 7.72 7.92 8.06 7.87 7.71 Collection (Start) Date Sample 1: 03/14/11 Sample 2: 03/16/11 Treatment 2 7.65 7.85 7.96 8.00 7.85 7.87 Sample Type/Duration 2nd 1st P/F s s • s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A r d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 42 Control 6.99 7.22 7.51 6.78 7.05 6.59 Spec. Cond. (µmhos) 220 590.0 628.0 Treatment 2 7.42 7.14 6.67 6.92 7.06 6.90 Chlorine(mg/1) <0.1 0.15 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.8 0.3 (Mortality expressed as %, combining replicates) I Note: Please % * % % % % % % % % Concentration Complete This Section Also I I I I I I I I I % Mortality start/end start/end LC50 = I Method of Determination Control 95% Confidence Limits Moving Average Probit I -- ISpearman Karber __ Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) 17141r Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/23/11 Facility: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labor tory Performing Test: TRITEST, INC. e / Comments: X S' ature o .�•e in R:syonsible Charge PO i G129 62.09 X :F Signature of L. •. -atory S -rvisor * PASSED: -16.04% Reduction * Work Order: 1106-00970 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -2.526 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -16.04 % Mortality Avg.Reprod. # Young Produced 20 28 25 18 20 28 22 23 20 17 23 24 0.00 22.33 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 25.92 Treatment 2 Treatment 2 Effluent Is: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 15.898% PASS FAIL # Young Produced 21 27 24 23 30 23 28 22 30 31 25 27 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 06/15/11 Control 7.87 7.76 7.77 7.71 7.81 7.71 Collection (Start) Date Sample 1: 06/13/11 Sample 2: 06/15/11 Treatment 2 7.82 7.79 7.90 7.87 7.91 7.87 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S. S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 43 Control 7.25 6.91 6.98 6.84 7.39 6.79 Spec. Cond. (µmhos) 176 659 737 Treatment 2 7.68 7.22 7.17 7.22 7.17 6.62 Chlorine(mg/1) <0.1 0.11 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.6 2.0 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This Section Also t % % ' % Is t * % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit -- Spearman Karber -- Other High - __ Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/22/11 Facility: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labo t• ory Performing Test: TRITEST, INC. X ;, Comments: FLA_ k Ac 16 1$`� 4- s- . at - o Oper or in Responsible Charge r X eliql Signature o aboratory Supervisor * PASSED: -3.29% Reduction * Work Order: 1109-00847 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699,:1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -0.663 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -3.29 % Mortality Avg.Reprod. # Young Produced 22 25 30 31 22 28 23 23 26 22 26 26 0.00 25.33 Control Control Adult (L) ive (D)ead L L L L L L L L L L L L 0.00 26.17 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 12.292% PASS FAIL # Young Produced 23 30 30 23 26 27 28 24 23 29 29 22 % control orgs X - producing 3rd brood Check One Adult (L) ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 09/14/11 Control 7.58 7.69 7.80 7.95 7.61 7.15 Collection (Start) Date Sample 1: 09/12/11 Sample 2: 09/14/11 Treatment 2 7.49 7.54 7.85 7.83 7.86 7.40 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 40 Control 7.28 6.97 7.23 7.08 7.57 7.02 Spec. Cond. (µmhos) 151 754.0 825.0 Treatment 2 7.53 7.29 7.38 7.09 7.76 7.21 Chlorine(mg/1) 0.14 0.24 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 2.0 3 .8 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This . _ _ . Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average _ Probit _ % -- % Spearman Karber _ Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) rsw...4 ,41,...„ , . _ __ ___ __________ 11( Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/21/11 Facility: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labo tory Perfo ri • est: TRITEST, INC. Comments: 8c g21�$3�C� Comments: fre X ,/ _:I Si ature o ;:•e a o, in Response.• e C arge X 7°. ,v -� Signature o a•oratory Supervisor * PASSED: -27.78% Reduction * Work Order: 1112-00821 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699/1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -4.564 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -27.78 % Mortality Avg.Reprod. # Young Produced 19 22 24 24 19 16 22 21 20 21 24 20 • - 0.00 21.00 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 26.83 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 11.486% PASS FAIL # Young Produced 18 30 30 31 25 24 24 27 26 28 30 29 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L ; 91.7% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 12/14/11 Control 7.69 8.06 7.75 8.11 8.03 7.77 Collection (Start) Date Sample 1: 12/12/11 Sample 2: 12/14/11 Treatment 2 7.80 8.10 7.76 8.18 7.80 7.94 Sample Type/Duration 2nd - 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 - X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 39 Control 7.67 7.59 7.78 7.61 7.68 7.36 Spec. Cond. (µmhos) 108 614.0 936.0 Treatment 2 7.90 7.71 7.81 7.25 7.61 7.26 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 2.0 1.8 (Mortality expressed as %, combining replicates) Note: Please % % % % % % % % % % Concentration Complete This - Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control' 95% Confidence Limits Moving Average Probit -- - * -- % Spearman Karber -- Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Vflueut Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/29/12 lity: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labo -tory Performing Test: TRITEST, INC. _�C�CSG �C j!'I , Comments: Srz "gnature . Oper/or in Responsible Charge Or X aKr 1 -- Signature of L oratory Supervisor * PASSED: -8.28% Reduction * Work Order: 1203-01272 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -1.741 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -8.28 % Mortality Avg.Reprod. # Young Produced 27 30 26 26 26 26 21 27 23 28 25 29 0.00 26.17 Control Control Adult (L) ive (D)ead L L L L L L L L L L L L - 0.00 28.33 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 9.337% PASS FAIL # Young Produced 26 26 26 29 32 27 31 32 26 32 32 21 % control orgs X producing 3rd brood Check One Adult (L) ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample ' Complete This For Either Test pH Test Start Date: 03/21/12 Control 8 .08 7.78 7.85 7.73 7.74 7.83 Collection (Start) Date Sample 1: 03/19/12 Sample 2: 03/21/12 Treatment 2 7.88 7.83 7.87 7.81 7.81 7.90 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 42 Control 7.56 7.28 7.47 7.24 7.20 7.18 - Spec. Cond. (µmhos) 221 761 686 Treatment 2 7.57 7.15 7.42 7.21 7.13 7.03 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 2.0 1.5 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit _ % -- % Spearman Karber _ Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/22/12 Facility: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labor-tory Performing Test: PACE ANALYTICAL Comments: 0).4411 a�Gy?, S o ••era l-r in Responsible Charge lip X kit Signature o aboratory Supervisor * PASSED: 2.39% Reduction * Work Order: 1206-00825 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 0.560 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 2.39 % Mortality Avg.Reprod. # Young Produced 27 30 26 32 30 23 29 26 30 22 29 31 0.00 27.92 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 27.25 Treatment 2 Treatment 2 Effluent %: 11%TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 11.272% PASS FAIL # Young Produced 24 27 30 28 26 21 27 28 27 30 30 29 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 06/13/12 Control 7.58 7.76 7.43 7.90 7.76 7.86 Collection (Start) Date Sample 1: 06/11/12 Sample 2: 06/13/12 Treatment 2 7.67 7.89 7.78 7.79 7.79 7.97 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 43 Control 8.19 7.97 8.00 7.71 7.43 7.31 Spec. Cond. (µmhos) 327 666 836 Treatment 2 7.59 7.69 7.76 7.54 7.62 7.16 - Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 1.6 1.0 (Mortality expressed as %, combining replicates) I Note: Please % t % % % % 9' % % % Concentration Complete This Section Also % % % % % % t 9' % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit _ t -- 9' Spearman Karber _ Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Kfluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/20/12 Facility: CITY OF LINCOLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labor tory Perforjnin T st: PACE ANALYTICAL f/�J Comments: X Sil* re of Operator n Responsible Charge X ' ' AI CAS-- Signature of Laboratory Supervisor * PASSED: -16.071 Reduction * Work Order: 92130976 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia ronic Test Results Chronic Pass/Fail Reproduction Toxicity Test CCChroiced t = -2.429 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 1 Reduction = -16.07 I Mortality Avg.Reprod. # Young Produced 18 22 17 18 19 16 15 18 22 21 16 22 0.00 18.67 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 21.67 Treatment 2 Treatment 2 Effluent 1: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV13. PASS FAIL # Young Produced 19 18 2124 20 24 17 24 19 20 26 28 1 control s X producing 3rd brood Check One , Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 09/12/12 Control 7.57 7.46 7.44 7.51 7.28 7.43 CollecSample 1: Dateion (Start) 1: 09/10/12 Sample 2: 09/12/12 Treatment 2 7.73 7.75 7.68 7.73 7.64 7.73 Sample Type/Duration 2nd , 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. - Hardness(mg/1) 48 Control 9.09 7.80 8.88 8.38 8.61 8.08 Spec. Cond. (pmhos) 274 723 791 Treatment 2 8.55 7.97 8.13 7.32 8.14 8.00 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 4.1 2.5 (Mortality expressed as 1, combining replicates) I Note: Please % % I I I I I I I I Concentration Complete This Section Also I I I % % 1 1 1 % I Mortality start/end start/end LC50 = I Method of Determination Control 95% Confidence Limits Moving Average Probit % -- I Spearman Karber - Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/20/12 Fac' 'ty: CITY OF LI COLNTON NPDES#: NC0025496 Pipe#: 001 County: LINCOLN L- • • - ory ir • iri. T= -t: PACE ANALYTICAL Comments: X , !, !� S . ' -;--rat•' 'n Responsible Charge X 1 1 I: ill Signature o aboratory Supervisor Work Order: 9214-1428 Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 7.394 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 32.30 % Mortality Avg.Reprod. # Young Produced 29 30 27 25 25 26 20 29 27 29 29 26 0.00 26.83 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 18.17 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV - 10.278% PASS FAIL # Young Produced 22 19 17 16 21 18 22 17 16 12 17 21 % control orgs X producing 3rd brood Check One Adult (L) ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 12/12/12 Control 8.05 8.11 7.95 8.03 8.11 8.27 Collection (Start) Date Sample 1: 12/10/12 Sample 2: 12/12/12 Treatment 2 8.06 8.01 7.96 8.13 8.04 8.27 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 47 Control 7.50 7.45 7.61 7.46 7.49 7.21 Spec. Cond. (pmhos) 151 771 883 Treatment 2 7.95 7.55 7.54 7.22 7.37 7.06 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 1.5 2.8 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = is Method of Determination Control 95% Confidence Limits Moving Average Probit Is -- Spearman Karber - Other __ High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) r . Effluent Aquatic Toxicity Report Form/Phase II Chronic Ceriodaphnia Facility City of Lincolnton NPDES#: NC 0025496 Pipe#001 County Lincoln L story Performin Tes Pace Analyti ervices,Inc-Raleigh Comments M#9214495470‘' X 0.,1ax qi.vi 6 ., Signature of O. .0 Signature of Lab Supervisor Test Start Date End Date Start Time End Time Sample Information Sample 1 Sample 2 Control Information* 01/16/13 01/23/13 11:28 11:00 Collection Start Date 01/14/13 01/16/13 i ; . I Start Renew/Renew2 Start Renew1Renew2 Grab `wx x a Treatment 22 22 22 Control Control Control Composite ^ . *'''' pH Initial 8.11 8.01 8.13 8.05 8.03 8.13 (Duration) 24 24 ., . - . Hardness(mg/l y' ? ?4c43 pH Final 8.03 8.19 8.14 7.91 8.16 8.01 Spec.Cond.(i+mhos/cml 637.0 676.0 246.7 D.O. Initial 7.63 7.48 7.42 8.10 7.48 7.09 �,.,y„ ;. ... D.O. Final 7.10 7.37 7.50 7.04 7.26 7.52 Chlorine(mg/I <0.1 <0.1 "�. �. ;,;r- Z- Temp. Initial 25.7 25.5 25.2 25.3 25.1 25.2 Sample temp.at receipt 0.5 °e 0.5 ;'? Temp. Final 25.4 25.2 25.1 25.0 24.7 25.0 Organism# Chronic Test Results 1 2 3 4 5 6 7 8 9 10 11 12 Mean Final Control Mortality% 0 Control #Young 23 28 28 26 28 30 31 27 25 23 26.9 %Control 3rd Brooc 100 .^. Control Repro CV 9.983 Adult LL L L LLLLLL y �. Mortality � (L)ive (D)ead ..Y-" Control Hour rol IWC 1 2 3 4 5 6 7 8 9 10 11 12 Mean 0 of 10 0 of 10 Effluent% #Young 25 22 27 23 19 23 21 26 25 26 23.7 Significant?QY ONE: Adult %Redt Final Mortality Significant @ 5.5 (L)ive (D)ead L L L L L L L L L L ii.90 1 2 3 4 5 6 7 8 9 10 Mean % or(No Conc. Effluent% #Young 16 24 17 22 13 23 23 17 21 23 el Reproduction Analysis: Repro.LOEC= 8.25 %; NOEC= 5.5 % Adult %Red Method:DunnettsTest 8.25 (L)iye (D)ead LLLLLLLL LL leg Normal Distrib? Yes Method: Kolmogorov 1 2 3 4 5 6 7 8 9 10 Mean Statistic: 0.88173 Critical: 1.035 Equal Variances? Yes Method: Bartlett's Effluent% #Young 18 13 23 16 21 21 21 24 21 23 20.1. Statistic: 3.89806 Critical: 15.0863 11 (L)ive (D)ead L L L L LLLLLL %25.28 Non-Parametric Analysis(if applicable): Adult Red Method: 1 2 3 4 5 6 7 8 9 10 Mean Effluent% Rank Sum Critical Sum Effluent% #Young 29 18 14 21 21 17 24 23 15 20 20.2 :DuAdult (L)ive (D)ead LLLL LL LLLL 2` 1 2 3 4 5 6 7 8 9 10 Mean Effluent% #Young 19 19 25 19 16 13 18 22 18 22 19.1 ResultOverall Analysis: or 22Adult (L)ive (D)ead L L L L L L L L L L 9Roo TChronIcc Value=25 6.73610EC= 5.5 'Should use highest test concentration or MAIL AU: Environmental Sciences Branch highest concentration with D.O.>5.0 mgfl Div, of Water Quality "r0: N.C. DENR t%Reduction from Control Reproduction Mean 1621 Mail Service Center Raleigh, N.C. 27699-1621 DWQ form AT-3 (8/91)Rev. 11/95 J r o yr�3'' Effluent Aquatic Toxicity Report Form/ Phase II Chronic Ceriodaphnia y Facility: Lincolnton WWTP NPDES:# NCO() 25496 Pipe#: 001 County: Lincoln Laboratory Performing Test: Meritech, Inc. Comments: x c)ervii419A G 1 X 727,1/,-&-e Q - Signatufa of O. Signature of Laboratory Supervisor Sample Information Sample 1 Sample 2 ControlTest Start Date End Date Start Time End Time 2/4/13 2/6/13 5 '4 Information• 2/6/13 2/13/13 10:30 AM 9:40 AM Collection Start Date Start Renew 1 Renew 2 Start Renew 1 Renew 2 Grab ' < Treatment 22 % 22 % 22 % Control Control Control Composite r 4 (Duration) 24.1 24.1 g4 , ,; pH Initial 7.94 8.14 7.95 8.12 8.15 8.06 r ° t` ''s �, W 8.20 8.17 8.25 8.07 8.08 8.14 �� � �,,,�����rt�i pH Final Hardness(mg/I) . '�: `Watti wL 42 42 D.O.Initial 8.10 7.55 7.67 7.94 7.71 7.83 Spec.Cond.(pmhos/cm) 691 834 155 166 D.O.Final 7.30 7.28 7.15 7.42 7.60 7.36 Chlorine(mg/I) 0.1 0 1 li.�r ' ( g ) < < _: Temp.lnitial 25.3 25.2 24.9 25.5 25.4 24.9 0 »'t 4 Sample temp.at receipt 2.1 °C 0.8 C },i a' Temp.Final 25.2 25.0 24.9 25.2 25.0 24.9 Organism# Chronic Test Results 1 2 3 4 5 6 7 8 9 10 11 12 Mean Final Control Mortality% 0 Control #Young 21 23 21 24 18 20 21 26 21 17 21.2 %Control 3rd brood 100 Adult ..,- Control Repro CV 12.5 (L)ive(D)ead LL LLLLLLLL to 48 Hour Mortality Control IWC 1 2 3 4 5 6 7 8 9 10 11 12 Mean 0 of 10 0 of 10 Effluent% #Young 18 17 20 19 19 19 18 19 21 19 18.9 Significant? Y O Adult '%Rear Final Mortality Significant @ 5.5 (L)ive(D)ead LL LLLLLLLL 10.8 % or Nnc No Co 1 2 3 4 5 6 7 8 9 10 Mean Reproduction Analysis: Effluent% #Young 20 20 16 16 20 18 21 22 17 16 18.6 Repro.LOEC= 11 %; NOEC= 8.25 Adult %Red Method: 8.25 (L)ive(D)ead LLL L L L L L L L 12 3 Normal Distrib? NO Method: Koimogorov 1 2 3 4 5 6 7 8 9 10 Mean Statistic: 1.0542 Critical: 1.035 Equal Variances? YES Method: Bartlett Effluent% #Young 17 16 21 18 18 15 17 20 14 17 17.3 Statistic: 14.225- Critical: 15.09 Adult %Red 11 (L)ive(D)ead L L L L L L L L L L 1 e a Non-Parametric Analysis(if applicable): Method:Steel's Many One Rank Test 1 2 3 4 5 6 7 8 9 10 Mean Effluent% Rank Sum Critical Sum 5.5 76.0 75.0 Effluent% #Young 16 18 18 17 15 14 11 16 17 16 15.8 8.25 76.5 75.0 Adult %Red 11 67.0 75.0 16.5 (L)ive(D)ead LLL L LL LL L L 25.5 16.5 59.0 75.0 1 2 3 4 5 6 7 8 9 10 Mean 22 62.0 75.0 Overall Analysis: Effluent% #Young 18 19 5 15 15 15 15 14 19 18 15.3 Result=PASS/FAIL or Adult %Red Test LOEC= 16.5 %; NOEC= 11 % 22 (L)ive(D)ead ' L L D L L L L L L L 27.8 13.5 70 Chronic Value= ATT: Environmental Sciences Branch * Should use highest test concentration or highest MAIL Div.of Water Quality concentration with D.O.>5.0 mg/I N.C.DENR t Reduction from Control Reproduction Mean TO: 1621 Mail Service Center Raleigh,NC 27699-1621 DWQ form AT-3 (8/91)Rev. 11/95 , Effluent Aquatic Toxicity Report Form / Phase II Chronic Ceriodaphnia Facility: Lincolnton NPDES: # NCOO 25496 Pipe#: 001 County: Lincoln Lab ratory Performing T st: Meritech, Inc. Comments: X ,,Z.9 x 7/72.....1,4_ _, Signature of . . Signature of Laboratory Supervisor Sample Information Sample 1 Sample 2 Control rest Start Date End Date Start Time End Time Collection Start Date 2/18/13 2/20/13 s. Information- 2/20/13 2/27/13 10:02 AM 9:15 AM Start Renew 1 Renew 2 Start Renew 1 Renew 2 Grab Treatment 22 % 22 % 22 % Control Control Control Composite (Duration) 24.0 23 9 j.,t pH Initial 7.94 7.87 7.96 8.05 7.87 7.88 pH Final 8.24 8.14 8.14 8.05 7.93 7.86 Hardness(mg/I) 42 48 D.O.Initial 7.86 7.81 7.81 7.79 7.65 7.84 Spec.Cond.(pmhos/cm) 813 833 159 171 7.35 7.50 7.17 7.38 7.57 7.21 D.O.Final Chlorine(mg/I) <0.1 <0.1 Temp.Initial 25.1 24.9 25.0 25.2 24.9 25.3 Sample temp.at receipt 1.1 00 1.1 00 Temp.Final 24.9 25.0 24.8 24.9 25.0 24.8 Organism# Chronic Test Results 1 2 3 4 5 6 7 8 9 10 11 12 Mean Final Control Mortality% 0 Control #Young 24 21 25 23 26 26 27 21 24 22 23.9 %Control 3rd brood 100 Adult L L L L L L L I.. L L Control Repro CV 8.9 (L)ive(D)ead48 Hour Mortality Control IWC 1 2 3 4 5 6 7 8 9 10 11 12 Mean 0 of 10 0 of 10 Effluent% #Young 26 22 26 23 22 20 25 26 23 29 24.2 Significant? Y 0 Adult L L L L L L L L L L %Redt Final Mortality Significant @ 5.5 (L)ive(D)ead -1.3 % or CNo Conc) 1 2 3 4 5 6 7 8 9 10 Mean Reproduction Analysis: Effluent% #Young 24 24 25 25 26 23 26 21 24 26 24.4 Repro.LOEC= >22 %; NOEC= 22 °i° Adult 8,25 (Wive(D)ead L L L L L L L L L D %Rea Method: Dunnett'sTest 2.1 Normal Distrib? YES Method: Kolmogorov 1 2 3 4 5 6 7 8 9 10 Mean Statistic: 0.6528 Critical: 1.035 Effluent% #Young Equal Variances? YES Method: Bartlett 26 28 27 28 27 23 28 26 24 17 25.4 Statistic: 5.5537-- Critical: 15.09 Adult %Red 11 (L)ive(D)ead LLLLLLLLLL 6 3 Non-Parametric Analysis(if applicable): Method: 1 2 3 4 5 6 7 8 9 10 Mean Effluent% Rank Sum Critical Sum Effluent% #Young 26 26 26 23 28 25 24 22 21 27 24.8 Adult %Red 16.5 (L)ive(D)ead LLLLLLLLLL -3.8 1 2 3 4 5 6 7 8 9 10 Mean - Overall Analysis: Effluent% #Young 24 28 25 28 24 25 27 23 19 23 24.6 Result=PASS/FAIL or Adult L L L L L L L L L L %Red Test LOEC= >22 %; NOEC= 22 % 22 (L)ive(D)ead -2.9 >22 Chronic Value= ATT:. Environmental Scierioes Branch. * Should use highest test concentration or highest MAIL Div.of Water Quality - concentration with D.O.>5.0 mg/I N.C.DENR t Reduction from Control Reproduction Mean TO: 1621 Mail Service Center Raleigh,NC 27699-1621 DWQ form AT-3 (8/91)Rev. 11/95 Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/21/13 Facility: LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN ;1 4 Laboratory Perfor ligf-�ie'stJ' ITECH LABS, INC. r ` [ j Comments: dilution water batch 21 � X signature t�(operator in tp ponsi e C ar also used:hard-42, cond-168 X r igna ure o L oratory upervisor * PASSED: -5.38% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR • 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -1.503 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -5.38 . i 1 I Mortality Avg.Reprod. # Young Produced 22 23 25 27 21 21 23 26 25 19 25 221 - - 0.00 23.25 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 24.50 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 10.232% PASS FAIL # Young Produced 26 25 22 24 24 24 25 28 23 23 26 24 % control orgs X - - - producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 03/13/13 Control 8.13 8.02 8.05 8.00 8.05 7.99 Collection (Start) Date Sample 1: 03/11/13 Sample 2: 03/13/13 Treatment 2 8.03 8.09 8.09 8.09 8.07 8.06 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24.0 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 23.9 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 42 Control 7.80 7.63 7.99 7.37 7.78 7.57 Spec. Cond. (pmhos) 162 573 707 Treatment 2 7.95 7.52 8.07 7.39 7.82 7.61 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.7 0.7 (Mortality expressed as %, combining replicates) I Note: Please " % I % % % I % % % Concentration Complete This . Section Also % % I % % I % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit % -- I Spearman Karber - Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/26/13 Facility: LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Lab• tor . y oerf. 0 -st: MERITECH LABS, INC. Comments: second dilution water X � Si- . ure o: --rate Res nsible Charge batch: hard-46, cond-164 Signature of -�aboratory Supervisor PASSED: 9.24% Reduction Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 1.545 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 9.24 % Mortality Avg.Reprod. # Young Produced 26 30 21 28 24 25 23 28 25 21 28 24 - . - 0.00 25.25 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L - 0.00 22.92 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 11.344% PASS FAIL # Young Produced 18 30 27 22 16 26 26 17 20 25 25 23 `k control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 06/19/13 Control 8.16 8.05 8.12 8.09 8.05 8.10 Collection (Start) Date Sample 1: 06/17/13 Sample 2: 06/17/13 Treatment 2 8.15 8.08 8.12 8.18 8.06 8.12 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23.7 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 48 Control 7.87 7.69 7.86 7.72 7.93 7.65 Spec. Cond. (pmhos) 167 587 563 Treatment 2 7.73 7.68 7.97 7.76 7.89 7.62 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.4 1.1 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality - start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit % -- % Spearman Karber Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : _ Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 09/19/13 Facility: LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Lab r tf Ner in Te : MERITECH LABS, INC. Comments: X Signature o to Responsible Charge X ��� * PASSED: -11.11% Reduction S'gnature of L oratory Supervisor Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality . N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia ronic Test Results Chronic Pass/Fail Reproduction Toxicity Test CCChroaced t = Tabular t = CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -11.11 ' Mortality Avg.Reprod. # Young Produced 23 25 28 24 29 29 19 29 28 11 22 30 0.00 24.75 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 27.50 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Contro22.33l CV PASS FAIL # Young Produced 26 25 28 30 28 28 32 24 30 29 26 24 % control orgs X • producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 91.7% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 09/11/13 Control 7.89 7.76 7.82 7.87 7.84 7.76 Sample Date Collection Sample 2: 09/11/13 Treatment 2 7.83 7.78 7.74 7.92 7.82 7.86 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L M M ✓ d r d r d t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 44 ...,...... Control 7.78 7.52 7.65 7.47 7.68 7.43 Spec. Cond. (pmhos) 148 875 977 Treatment 2 7.80 7.54 7.65 7.55 7.72 7.44 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.7 0.9 (Mortality expressed as %, combining replicates) I Note: Please % % % % % % % % % % Concentration ColetCommppleteAThis g Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving AverageProbit High % -- % Spearman Karber Other g Conc. pH D.O. r Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) ' Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/24/13 iFacil'ty: INCOLNTO, WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN - ' Labo , 2127, . =t: MERITECH LABS, INC. Comments: X Si. a7w-op- - En Responsible Charge Signature of aboratory Supervisor * PASSED: -15.46 Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -2.118 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -15.46 % Mortality Avg.Reprod. # Young Produced 15 9 22 17 22 19 15 19 18 15 15 21 - 0.00 17.25 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 19.92 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV • 21.708% PASS FAIL # Young Produced 18 23 19 16 20 18 18 20 22 20 22 23 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 91.7% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 12/11/13 Control 8.14 8.09 8.08 8.12 8.07 8.06 Collection (Start) Date Treatment 2 8.04 8.11 8.07 8.21 8.10 8.09 Sample 1: 12/09/13 Sample 2: 12/11/13 ample Type/Duration 2nd 1st P/F. s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23.9 hrs L A A r d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 47 Control 8.20 7.81 6.93 7.88 7.77 7.31 Spec. Cond. (pmhos) 163 482 499 Treatment 2 8.04 7.93 8.20 8.08 7.95 7.42 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 1.7 0.4 (Mortality expressed as %, combining replicates) I Note: Please % * % % % % % % % % Concentration Complete This * V % % % % % % % % Mortality Section Also start/end start/end LC50 = t Method of Determination Control 95% Confidence Limits Moving Average Probit * -- % Spearman Karber = Other -- High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 03/12/14 Facility: LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Lab a oryfo ipg T st: RITECH LABS, INC. X I )�1 4 Comments: �� S . azure •• - ator i ponsible Charge X delli Signa ure of Labornr6Ty-Supervisor * PASSED: -5.53% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -1.113 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -5.53 % Mortality Avg.Reprod. # Young Produced 21 20 21 22 23 19 22 21 23 19 23 19 0.00 21.08 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 22.25 Treatment 2 Treatment 2 Effluent %: ilk TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 7.420% PASS FAIL # Young Produced 25 20 24 21 27 24 25 17 23 16 22 23 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 03/05/14 Control 8.08 7.96 7.90 7.89 8.00 7.82 Collection (Start) Date Sample 1: 03/03/14 Sample 2: 03/05/14 Treatment 2 8.13 7.96 7.83 7.93 7.87 7.89 Sample Type/Duration 2nd lst P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23.9 hrs L A A r d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample lst sample 2nd sample D.O. Hardness(mg/1) 42 Control 8.09 7.58 7.68 7.43 7.65 7.63 Spec. Cond. (pmhos) 189 478 637 Treatment 2 7.74 7.70 7.58 7.45 7.68 7.64 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.6 0.3 (Mortality expressed as %, combining replicates) I Note: Please I I I I I I I I I I Concentration Complete This - Section Also % % % % I I I I % I Mortality - start/end start/end • LC50 = I Method of Determination Control 95% Confidence Limits Moving Average Probit I -- I Spearman Karber = Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 06/16/14 Facil,}ty: LINCOLNTO0 P NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labora o ,ri .er i At: MERITECH LABS, INC. A ,Comments: X : Signature q Operato ' i Responsible Charge Signature of Laboratory Supervisor * PASSED: 4.56% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR • 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = 0.777 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = 4.56 % Mortality Avg.Reprod. # Young Produced 15 25 23 28 23 23 28 27 23 21 27 22 0.00 23.75 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 22.67 Treatment 2 Treatment 2 Effluent %: 111 TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 15.457% PASS FAIL # Young Produced 24 22 19 27 24 25 24 23 25. 15 22 22 % control orgs X . producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L ,L L L L L k 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH -- Test Start Date: 06/04/14 Control 8.02 8.15 7.94 6.67 7.06 7.93 Collection (Start) Date Sample 1: 06/02/14 Sample 2: 06/04/14 Treatment 2 8.07 8.17 8.22 6.73 6.75 7.95 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 24 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 46 Control 7.42 7.43 7.95 7.37 7.02 7.17 Spec. Cond. (pmhos) 201 574 713 Treatment 2 7.74 7.54 7.66 7.37 7.58 7.12 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.4 0.7 (Mortality expressed as %, combining replicates) I Note: Please t % % % % % % % % % Concentration Complete This . _ Section Also % % % % % % % % % % Mortality start/end start/end • LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit % -- % Spearman Karber _ Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 10/22/14 Facility: LINCOLNTON + P NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Labo•- •ry = .fo ' ,g :zt: RITECH LABS, INC. - Comments: O -� 0 (` _ X , Jr + Signature o !•era . esponsible Charge x,�:-tee, Signatu a of ratory Supervisor * PASSED: -36.12% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -5.205 Tabular t = 2.518 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -36.12 % Mortality Avg.Reprod. # Young Produced 24 18 18 21 19 14 17 22 18 19 19 13 0.00 18.50 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 9.09 25.18 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 16.541% PASS FAIL # Young Produced 26 26 28 22 29 25 0 25 24 28 18 26 W control orgs X producing 3rd brood Check One Adult (Wive (D)ead L L L D L L * L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 09/10/14 Control 8.10 8.00 8.02 7.97 8.18 8.19 Collection (Start) Date Sample 1: 09/08/14 Sample 2: 09/10/14 Treatment 2 7.98 8.09 8.01 8.10 8.06 8.14 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23.8 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24.0 hrs T P P 1st sample 1st sample 2nd sample D.O. Hardness(mg/1) 48 Control 7.70 7.47 7.84 7.76 7.92 7.89 Spec. Cond:(pmhos) 154 730 629 Treatment 2 7.47 7.42 7.99 7.86 7.90 7.85 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.4 0.6 (Mortality expressed as lc, combining replicates) I Note: Please % % % % % % % % % % Concentration Complete This - - Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit * -- % Spearman Barber = Other - High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) 1/ Effluent Toxicity Report Form - Chronic Pass/Fail and Acute LC50 Date: 12/18/14 Facility: LINCOLNTON WWTP NPDES#: NC0025496 Pipe#: 001 County: LINCOLN Laboratory Performing Test: MERITECH LABS, INC. Comments: X Si5rtu of rator in Responsible Charge 'gnat re o oratory Supervisor * PASSED: -7.45% Reduction * Work Order: Environmental Sciences Branch MAIL ORIGINAL TO: Div. of Water Quality N.C. DENR 1621 Mail Service Center Raleigh, North Carolina 27699-1621 North Carolina Ceriodaphnia Chronic Pass/Fail Reproduction Toxicity Test Chronic Test Results Calculated t = -2.158 Tabular t = 2.508 CONTROL ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 % Reduction = -7.45 % Mortality Avg.Reprod. # Young Produced 28 25 27 29 30 26 31 25 24 27 27 23 0.00 26.83 Control Control Adult (L)ive (D)ead L L L L L L L L L L L L 0.00 28.83 Treatment 2 Treatment 2 Effluent %: 11% TREATMENT 2 ORGANISMS 1 2 3 4 5 6 7 8 9 10 11 12 Control CV 8.966% PASS FAIL # Young Produced 29 28 29 27 30 26 28 26 33 28 31 31 % control orgs X producing 3rd brood Check One Adult (L)ive (D)ead L L L L L L L L L L L L 100% 1st sample 1st sample 2nd sample Complete This For Either Test pH Test Start Date: 12/10/14 Control 8.12 8.17 8.06 8.02 8.07 8.08 Collection (Start) Date • Sample 1: 12/08/14 Sample 2: 12/10/14 Treatment 2 8.18, 8.57 8.03 8.04 8.11, 7.91 Sample Type/Duration 2nd 1st P/F s s s Grab Comp. Duration D t e t e t e I S S a n a n a n Sample 1 X 23.9 hrs L A A ✓ d r d r d U M M t t t Sample 2 X 24 hrs T P P 1st sample 1st sample 2nd sample D.O. - Hardness(mg/1) 44 Control 8.00 7.82 8.05 7.84 7.63 8.51 . Spec. Cond. (pmhos) 165 839 800 Treatment 2 7.76 7.96 8.10 7.85 7.90 8.53 Chlorine(mg/1) <0.1 <0.1 LC50/Acute Toxicity Test Sample temp. at receipt(°C) 0.1 0.3 (Mortality expressed as %, combining replicates) Note: Please % % % % % % % % % % Concentration Complete This Section Also % % % % % % % % % % Mortality start/end start/end LC50 = % Method of Determination Control 95% Confidence Limits Moving Average Probit % -- % Spearman Karber _ Other High Conc. pH D.O. Organism Tested: Ceriodaphnia dubia Duration(hrs) : Copied from DWQ form AT-1 (3/87) rev. 11/95 (DUBIA ver. 4.41) VStart Date: 1/16/2013 Ceriodaphnia Survival and Reproduction Test-Reproduction Test ID: 25496 Sample ID: City of Lincolnton End Date: 1/23/2013 Lab ID: PACE-Pace-Raleigh#016 Sample Type: effluent Sample Date: Protocol: EPAF 91-EPA Freshwater Test Species: CD-Ceriodaphnia dubia Comments: Conc-% 1 2 3 4 5 6 7 8 9 10 Control 23.000 28.000 28.000 26.000 28.000 30.000 31.000 27.000 25.000 23.000 5.5 25.000 22.000 27.000 23.000 19.000 23.000 21.000 26.000 25.000 26.000 8.25 16.000 24.000 17.000 22.000 13.000 23.000 23.000 17.000 21.000 23.000 11 . 18.000 13.000 23.000 16.000 21.000 21.000 21.000 24.000 21.000 23.000 16.5 29.000 18.000 14.000 21.000 21.000 17.000 24.000 23.000 15.000 20.000 22 19.000 19.000 25.000 19.000 16.000 13.000 18.000 22.000 18.000 22.000 Transform: Untransformed 1-Tailed Conc-% Mean N-Mean Mean Min Max CV% N t-Stat Critical MSD Control 26.900 1.0000 26.900 23.000 .31.000 9.983 10 5.5 23.700 0.8810 23.700 19.000 27.000 10.721 10 2.073 2.287 3.530 *8.25 1.9.900 0.7398 19.900 13.000 24.000 19.164 10 4.535 2.287 3.530 *11 20.100 0.7472 20.100 13.000 24.000 17.146 10 4.405 2.287 3.530 *16.5 20.200 0.7509 20.200 14.000 29.000 22.237 10 4.341 2.287 3.530 *22 19.100 0.7100 19.100 13.000 25.000 17.530 10 5.053 2.287 3.530 Auxiliary Tests Statistic Critical Skew Kurt Kolmogorov D Test indicates normal distribution(p>0.01) 0.88173 1.035 -0.17 -0.0869 Bartlett's Test indicates equal variances(p=0.56) 3.89806 15.0863 Hypothesis Test(1-tail,0.05) NOEC LOEC ChV TU MSDu MSDp MSB MSE F-Prob df Dunnett's Test 5.5 8.25 6.7361 18.1818 3.52962 0.13121 91.67 11.913 1.6E-05 5,54 Dose-Response Plot 35 30- • 25- - 1-tail,0.05 level of significance t20 • •-....______♦ vs o> a15 10 0 • O to I4 N + N • 0 • t U Page 1 ToxCalc v5.0.23 Reviewed by`k L NCDENR North Carolina Department of Environment and Natural Resources Pat McCrory Donald R. van der Vaart Governor Secretary January 30,2015 Stephen H.Peeler,Dir. City of Lincolnton WTP PO Box 617 Lincolnton,NC 2893-0617 Subject: Acknowledgement of Permit Renewal Permit NC0025496 Lincoln County Dear Mr. Peeler: The NPDES Unit received your permit renewal application on January 30, 2015. A member of the NPDES Unit will review your application. They will contact you if additional information is required to complete your permit renewal. You should expect to receive a draft permit approximately 30-45 days before your existing permit expires. If you have any additional questions concerning renewal of the subject permit, please contact Teresa Rodriguez(919) 807-6387. Sincerely, Wire A,T D oro' Wren Thedford Wastewater Branch cc: Central Files Mooresville Regional Office NPDES Unit 1617 Mail Service Center,Raleigh,North Carolina 27699-1617 Location:512 N.Salisbury St Raleigh,North Carolina 27604 Phone:919-807-63001 Fax:919-807-6492/Customer Service:1-877-623-6748 Internet::www.ncwater.orq An Equal OpportunitylAffirmative Action Employer