NC0004243_Regional Office Physical File Scan Up To 12/13/2022

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cealshmencaum
I Sevier
Friday, June 5,1998
Don Link
Department of EHNR
Ground Water Section
Interchange Bld. 59 Woodfin Place
Asheville, NC 28801-2414
Coats American
PO Box 368 Phone: [phone]
Marion NC 28752 FAX [phone]
email:
Subject: Repair of our wastewater clarifier
Dear Mr Link:
This letter is to confirm our recent telephone conservation concerning the repairs
needed on the wastewater clarifier.
Our plans include:
1- Installattion of wells around the clarifier to lower the water table.
2- Draining the clarifier.
3- Repair the concrete and sludge raking mechanism.
It is our understanding that we do not need a permit to install wells around the clarifier,
or to pump groundwater into the stream.
Please call if you have any _questions.
hryckinney
Environmental Manager
cc Rex Stuckey
Jerry Sisk
�V t
JUN 1 1 1998
Groundwater Section
Asheville Re 'onal Office

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X
DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
March 3, 1993
MEMORANDUM
TO: Bob Cheek, Groundwater Section
Raleigh Central Office
THROUGH: Donald R. Link, Regional Groundwater Supervisor
Asheville Regional Office
FROM: Kay Dechant, Hydrogeologist
Asheville Regional Office
SUBJECT: Groundwater Monitoring Requirements
Renewal of Permit No. NC0004243
Coats American
McDowell County; North Carolina
The subject NPDES permit, which expires June 30, 1993 is currently up for
renewal. It is my recommendation that specific groundwater monitoring
requirements be incorporated in Permit No. NC0004243.
Coats American is currently conducting groundwater monitoring at the
subject site as the result of a permit modification (letter attached). Also,
groundwater monitoring is required at an adjacent site, coal ash settling
basin, per Non -discharge Permit No. WQ0005603 (monitoring requirements
attached).
I recommend that NPDES No. NC0004243 contain the same monitoring schedule
and parameters as Non -discharge Permit No. NC0005603. Having the groundwater
monitoring requirements compatible for the two adjacent sites will facilitate
the permittee's reporting and our review of compliance monitoring data.
I recommend reissuance of the subject permit with the following conditions:
All wells shall be sampled every April, August, and December for the
following parameters:
COD TDS
TOC pH
Selenium Chloride
Water Level Total Suspended Solids
SO4 Magnesium
Calcium
Volatile Organic Compounds -In December only
(by Method 1 or Method 2 below)

Memo/Bob Cheek/Renewal of Coats American Permit NC0004243/3-3-93 Page 2
i 9
Method 1: Method 6230D (Capillary - Column), "Standard Methods for the
Examination of Water and Wastewater", 17th edition, 1989
Method 2: Method 502.2 "Methods for the Determination of Organic
Compounds in Drinking Water", United States Environmental
Protection Agency - 600/4-88/039
The measurement of water level must be made prior to sampling for the
remaining parameters.
The measuring points (top of well -casing) of all monitoring wells shall be
surveyed to provide relative elevations of the measuring point for each of the
monitoring wells. The depth of water in each well shall be measured from the
surveyed point on the top of the casing.
If TOC concentrations greater than 10 mg/1 are detected in any
downgradient monitoring well, additional sampling and analysis must be
conducted to identify the individual constituents comprising this TOC
concentration. If the TOC concentration as measured'in the background monitor
well exceeds 10 mg/1; this concentration will be taken to represent the
naturally occurring TOC concentration. Any exceedances of this naturally
occurring TOC concentration in the downgradient wells shall be subject to'the
additional sampling and analysis as described above.
If any volatile organic compounds are detected by method 6230D, or the
equivalent method 502.2, then EPA methods 604 and 611 must also be run to
detect other organic compounds which may be present. The results of all
analysis specified in the monitoring requirements, including 604 and 611 if
required, must be submitted simultaneously.
The results of the sampling and analysis shall be sent to the N. C.
Division of Environmental Management on Form GW-59 (Compliance Monitoring
Report Form) every May, September, and January.
The Compliance Boundary for the disposal system is specified by
regulations in 15 NCAC 2L, Classifications and Water Quality Standards
applicable to the groundwater of North Carolina.. An exceedance of Groundwater
Quality Standards beyond the Compliance Boundary is subject to penalty
provisions applicable under General Statute 143-21.5.6A. The sale of property,
by the Permittee, which is within or contiguous to the disposal system site may
alter the location of the Compliance Boundary.
For facilities permitted on or after December 30, 1983, the Compliance
Boundary is established at the lesser of 250 feet from the waste disposal area,
or 50 feet within the property boundary.
If the title to any property which may affect the location of the
Compliance Boundary is changed, the permittee shall notify the Division
Director within 14 days. The Director shall then establish a modified
Compliance Boundary which will be done as a modification to the Permit.

State of North Carolina
Department of Natural Resources and Community Development
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor R. Paul Wilms
S. Thomas Rhodes, Secretary Director
GROUNDWATER SECTION
August 1,�1988
American Thread Co.
P.O. Box 880
Old Fort, North Carolina 28762
Attn: Mr. Jerry W. Sisk
SUBJECT: Permit Modification
NPDES Permit No. NC0004243
American Thread Co.
McDowell County
Dear Mr. Sisk:
In accordance with the policy of the Division of
Environmental Management to ensure the good quality of North
Carolina's groundwater, the referenced Permit requires
several activities related to groundwater monitoring. The.
following guidelines are presented to assist you in
complying with those requirements.
1. Condition No. 1: The North Carolina Well Construction
Standards 15 NCAC .0107(b) requires that a permit be issued
prior to construction of any monitor well, and thus permit
application forms are attached for your convenience. To
facilitate the permitting process and discuss the location
and construction requirements relevant to your specific
facility, you should contact:
Asheville Regional Office
159 Woodfin Street
Asheville, NC 28801
[phone]
Hyd. Reg. Supervisor: Don Link
Pollution Prevention Pays
I
limCF.,IVF
S�1P f9
P.O. Box 27687, Raleigh, North Carolina 27611-7687
Telephone [phone] Grounduvlater section
Asheville Regional Office
An Equal Opportunity Affirmative Action Employer

2. Condition No. 2: Sampling of the above referenced
wells on the schedule and for the constituents listed
below:
SCHEDULE: The monitor wells must be sampled initially
after construction (and prior to waste
disposal operations) and thereafter every
March, July and November.
CONSTITUENTS:
�TOX
�H.
.-O- Pho s
HOC
,,Water Level
✓COD
L-9'agnesium
"vCa.Icium
`SOa
Chloride
Selenium
The measurement of water levels must be made prior to
sampling for the remaining parameters.
In the event that a TOX concentration of 5.0 ppb or
greater is detected, any individual halogenated organic
compound(s) present at or above the method detection
limit (MDL) must be identified and quantified utilizing
EPA Method 601, 602, 604 and 611.
A supply of forms (GW-59) on which the analytical
results must be reported are attached. Instructions are
provided on the reverse of the white copy of each 3-part
form. The analytical results should be sent to the address
shown at the top of the form and are due in our office no
later than the last working day of the month following
sample collection.
Additional forms will be provided upon receipt of the
attached form GW-59 RO.
If you have any questions, please do not hesitate to
contact me at [phone].
Si cerely,
aid D�,�J
Robert B. Cheek
Supervisor
Permits and
Groundwater
Attachments
cc: Don Link
Nargis Toma
Compliance
Section

State of North Carolina
Department of Natural Resources and Community Development
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor R. Paul Wilms
S. Thomas Rhodes, Secretary July 25, 1988 Director
Mr. Jerry W. Sisk
American Thread Company
P. 0. Box 880
Old Fort, North Carolina 28762
Subject: Permit Modification
NPDES Permit No. NC0004243
American Thread Company
McDowell County, North Carolina
Dear Mr. Sisk:
The subject permit was issued June 9, 1988, without specific
groundwater monitoring requirements for the existing monitor wells
downgradient from the waste treatment lagoons. I am hereby modifying
the groundwater monitoring section of the permit to react as follows:
The downgradient cells shall be sampled three
times a year, during the months of March, July,
and November, for pH, total dissolved solids (TDS),
total organic carbon (TOC), chemical oxygen demand
(COD), orthophosphate', chloride, sulfate, calcium,
magnesium, and selenium. A measurement of water
level must be made prior to sampling. The wells
shall also be sampled once a year during the month
of November for total organic halides (TOX).
The analytical methods used for TOX must be capable
of detecting the total of all halogenated organic
compounds present at a concentration of 5.0 parts
per billion (ppb) or greater. Any individual
halogenated organic compound present at a con-
centration at or above the method detection limit
(MDL) must be identified, quantified, and reported
with the sampling results.
Pollution Prevention Pays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Mr. Jerry W. Sisk
Page 2
If the conditions of this modification are unacceptable to you, you
have the right to an adjudicatory hearing before a hearing officer. In
order to request such a hearing, you must send your request to the Director
within thirty days of receipt of this modification, identifying the
specific issues being contended. Unless such a request is made, this
modification shall be final and binding.
If you have any questions concerning this matter, please contact Mr.
Don Link at [phone], extension 301.
S}.zfc--e ely. "
i
R. Paul Wilms
cc: Bo Cheek
oy Davis
George Everett
REC-EIVE-OD
Water Quality Section
JUL 2 1 1988
,Asheville Regional Ci;•^e
Asheville, North Carolina

DIVISION OF ENVIRONMENTAL MANAGEMENT
ASHEVILLE REGIONAL OFFICE
GROUNDWATER SECTION
July 15, 1988
mRMdRANDUM
TO: R. Paul Wilms, Director
Division of Environmental Management
'THROUGH: Bob Cheek, Supervisor
Permits & Compliance Unit
Roy M. Davis, Regional Supervisor
Division of Environmental Management v�
FROM: Don Link, Hydrogeological Regional Supervisor / n�
Groundwater Section
SUBJECT: Modification of NPDES Permit No. NC0004243
American Thread Company
McDowell County
After reviewing NPDES Permit No. NCO004243 for American Thread Company
in McDowell County, it is my recommendation that groundwater monitoring be
included in the permit. American Thread Company had anticipated
groundwater monitoring and installed three wells downgradient from the
waste treatment lagoons in October, 1987.
Groundwater monitoring parameters should include pH, total dissolved
sol-ids, chlorides, COD, SO , orthophosphates, calcium, magnesium, selenium,
T& and static water levels at each of the existing downgradient wells.
The permit should be modified to read: "The downgradient wells shall
be sampled threestimes a year, during the months of March, July, and
November, for pH, total dissolved solids (TD'S), total organic carbon (/TOC),
chemical oxygen demand (Cd)), orthophosphate, chloride, sulkte, calcium,
magnesium, and selenium. A measurement of water level must be made prior
to sampling. The wells shall also be sampled once a year during the month
of November for total organic halides (TOX).
The analytical methods used for TOy must be capable of detecting the
total of all halogenated organic compounds present at a concentration of
5.0 parts per billion (ppb) or greater. Any individual halogenated organic
compound present at a concentration at or above the method detection limit
(MDL) must be identified, quantified, and reported with the sampling
results".
DL:ar
cc: Jim Reid

State of North Carolina
Department of Natural Resources and Community Development
Division of Environmental Management
512 North Salisbury Street • Raleigh, North Carolina 27611
James G. Martin, Governor R. Paul Wilms
S. Thomas Rhodes, Secretary Director
Mr. Jerry W. Sisk
American Thread Company
P. 0. Box 880
Old Fort, North Carolina 28762
Subject: Permit Modification
NPDES Permit No. NC0004243
American Thread Company
McDowell County, North Carolina
Dear Mr. Sisk:
The subject permit was issued June 9, 1988, without specific
groundwater monitoring requirements for the existing monitor wells
downgradient from the waste treatment lagoons: I am hereby modifying
the groundwater monitoring section of the permit to read as follows:
The downgradient wells shall be sampled three
times a year, during the months of March, July,
and November, for pH, total dissolved solids (TDS),
total organic carbon (TOC), chemical oxygen demand
(COD), orthophosphate, chloride, sulfate, calcium,
magnesium, and selenium. A measurement of water
level must be made prior to sampling. The wells
shall also be sampled once a year during the month
of November for total organic halides (TOX).
The analytical methods used for TOX must be capable
of detecting the total of all halogenated organic
compounds present at a concentration of 5.0 parts
per billion (ppb) or greater. Any individual
halogenated organic compound present at a con-
centration at or above the method detection limit
(MDL) must be identified, quantified, and reported
with the sampling results.
Pollution Prevention Pays
P.O. Box 27687, Raleigh, North Carolina 27611-7687 Telephone [phone]
An Equal Opportunity Affirmative Action Employer

Mr. Jerry W. Sisk
Page 2
If the conditions of this modification are unacceptable to you, you
have the right to an adjudicatory hearing before a hearing officer. In
order to request such a hearing, you must send your request to the Director
within thirty days of receipt of this modification, identifying the
specific issues being contended. Unless such a request is made, this
modification shall be final and binding.
If you have any questions concerning this matter, please contact Mr.
Don Link at [phone], extension 301.
Sincerely,
R. Paul Wilms
cc: Bob Cheek
Roy Davis
George Everett

SrA 4
D
North Carolina Department of Human Resources
Division of Health Services
P.O. Box 2091 • Raleigh, North Carolina 27602-2091
James G. Martin, Governor
David T. Flaherty, Secretary August 9, 1989
Ms. Dianne Eskenasy
Groundwater Section, DEM
59 Woodfin Place
Asheville, NC 28801
Courier 067816
Dear Dianne:
Subject: American Thread Company, Sevier Plant
NCD "003 157 377 .
Ronald H. Levine, M.D., M.P.H.
State Health Director
Please find enclosed a copy of the lab results for samples
collected by the Superfund Section at the subject site on March
29, 1989. I have also included a site sketch showing the
approximate location of the soil samples collected on site.
If you have any questions, please contact me at (919)
733-2801.
PD/acr
Attachments
cc: Charlotte Varlashkin
Sincerely,
Pat DeRosa, Environmental Chemist
Superfund Section
Division of Solid Waste Management
6'
'J ce'l'V
AUG I r) 1989
Groundwater Section
Asheville Regional Office

SAMPLE #
1
2
3
N
5
0
A
TABLE 1
AMERICAN THREAD COMPANY/SEVIER PLANT
NCD 003 157 377
SAMPLING LOCATIONS, MARCH 29, 1989
TYPE DESCRIPTION
Groundwater
Monitoring Well #9
(MW-9), K8019.
Approx. 25 ft. south
of aeration basin.
Groundwater
Monitoring Well #5
(MW-5), K80L5.
Approx. 100 ft. east
of extended aeration
basin
Groundwater
Monitoring Well #2
(MW-2), K80L2.
Background well,
Approx. 1100 ft.
south of plant building.
Soil
Background soil
sampled at 0-3"
depth across road
from burn area.
Soil
Burn area sampled
at 3-6" depth;
encountered charred
fragments.
Soil
Burn area sampled at 3"
depth at 2nd location in
burn area; encountered
charred fragments.
Soil
Sluice ash disposal
area sampled at 0-8"
U93U
1015
1100
1215
1230
1255
1305

Nlatef Q1181i17 Sp'ctiosl
r 0 a r,1
NOV ,
State of North Carolina Asheville Regional OtfiW
Department of Environment, Health and Natural ReAW14, Borth Caroft
Division of Environmental Management
512 North Salisbury Street. Raleigh, North Carolina 27604
James G. Martin, Governor George T. Everett,Ph.D.
William W. Cobey, Jr., Secretary Director
November 15, 1991
Mr. JERRY MCKINNEY
COATS AMERICAN
P. O. BOX 670
TOCCOA, GEORGIA 30577
Subject: Application No. NCO004243
COATS AMERICAN
SERIER PLANT
Mcdowell County
Dear Mr. MCKINNEY:
The Division's Permits and Engineering Unit acknowledges receipt of your permit application and
supporting materials received on November 14, 1991. This application has been assigned the number
shown above. Please refer to this number when making inquiries on this project.
Your project has been assigned to Mack Wiggins for a detailed engineering review. A technical
acknowledgement will be forthcoming. If this acknowledgement is not received within thirty (30)
days, please contact the engineer listed above.
Be aware that the Division's regional office, copied below, must provide recommendations from the
Regional Supervisor for this project prior to final action by the Division.
If you have any questions, please c t Mack Wiggins at [phone].
- A ,T
cc: Asheville Regional Office
Sincerely,
( 47t", D'&I�
M. Dale Overcash, P.E.
Supervisor, NPDES Permits Group
Pollution Prevention Pays
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone [phone]
An Equal Opportunity Aff=i ative Action Employer

ICAN �°
Cp�tr� AMER
November 51 1991
Mr- Don Safrit$ection
Water Quality
P. 0• Box 29535 27 626- 0535
N.C.
Raleigh'
Sevier Plant NC0004243
Reference• NPDES Permit Number
Sevier Plant s
Safrit: hanged on our Coats
Dear Mr• name be chanq The new name is
issue the
We request that t number NC0004243• Company)• please
enclosed a
ermi Thread name. We h
discharge P ormally American company
•
Mexican i t with °roces ing of this change
necessary permfor the p
check for $50 have any questions.
me a call if you
Please give
yours very truly,
COATS AMERICAN
W• R• 5tuckeEngineering
Director of
WRS/I'll
Enclosure er Cothran
CC: Mr. Ron Budnick
Mr Jerry Sisk
15/p3 SE'
Jerry McKinney
Sevier Plant
a.
��nx 670 .Toccoa,
Georgia 30577 4p4 1886-2141

Inorganics
Total (mg/1 or mg/kg)
Arsenic
Barium
Chromium
Lead
Mercury
Extractable (mg/1)
Barium
Organics (ug/1 or ug/kg)
Napthalene
Acenapthene
Fluorene
Phena*nthene
Anthracene
Fluoranthene
Pyrene
Benz (a) anthracene
Chrysene
Benzo (k) fluoranthene
Benzo (a) pyrene
Indeno (1,2,3-c,d) pyrene
Dibenzo (a,h) anthracene
Benzo (g,h,i) perylene
Dibenzofuran
2-Methyl Napthalene
Benzo (b) fluoranthene
1,1-Dichloroethane
Chloroform
TABLE 2
AMERICAN THREAD COMPANY/SEVIER PLANT
NCD003157377
Summary of Sampling Results
March 29, 1989
Sample Location/Number
MW-9
MW-5
MW-2
BKGD
BURN
BURN
SLUICE
SOIL
AREA
AREA
ASH
#1
#2
#3
#4
#5
#6
#7
<0.01
<0.01
<0.01
3.6
11
9
39
+�M_
0.9
0.2
89
144
124
769
0.1
0.04
<0.01
<40
<40
<40
<40
901"
0.05
<0.03
20
44
25
<20
0.0003
<0.0002
<0.0002
<0.10
0.18
0.12
<0.10
NA
NA
NA
<0.04
0.04
0.06
0.16
--
--
--
--
--
--
--
--
12,000
--
--
--
`-
--
-
17,667
--
--
--
330K
9,667
1881667
330K
--
--
--
--
26,833
206,333
330K
--
--
--
330K
32,667
330,000
433
--
--
--
330K
29,333
278,667
467
--
--
--
--
-
223,667
--
--
--
--
301000
194,000
330K
--
--
--
--
261333
127,000
--
--
--
--
--
24,333
92,333
--
--
--
--
--
34,667
183,000
--
--
--
--
--
-
67,000
--
--
--
--
16,667
161,333
--
--
--
--
-
4,333
--
--
--
-
3,333
--
--
--
--
--
--
1650K
--
4J
--
--
--
--
--
< = None detected, detection limit noted J = Estimated Value
-- = None detected K = Actual value is less than value
NA = Not Applicable given (detection limit)

Dirk T--,OaA
A me(-,\ c ct n -Tk (-- e a 4 p I
QC
I
I me I-e,,,
e-
m

Department of Human Resources SAMPLE ANALYSES REQUEST
ision of Health Services
State Labor.:'ory of Public Health
P. 0. Box 28047
:06 `l. Wilmington Street
Raleigh, 27611
Number Field Sample Number 3
re of Site Site.)_-ocarion 'i f 7')� )_/V-<
lected By o ' ID# 3 � Date Collected 3
X of Sample:
;nvironmental Concentrate ,,cc Comments
Groundwater (1) _ Solid (5) `/4Da
L' ;d (6)
_ Surface Water (2) tqui ------ --
Soil (3) Sludge (7)
Other (4) Other (8)
APB �, 7 1989
TTQnRCYANT(- (—RFI IISTRY
^! .'n e
Extractables
Total SUPERFUND BRANCII
Parameter Results mg/I
Parameter Results mg/I
Parameter Results mg/1
Arsenic
Barium < 0 •`� t{
Cadmium (9-� D 8
Chromium U • •2--D
Lead U
Mercury
Selenium
Silver �o� ')_0
`Arsenic 3, 6
—'-""'Barium /YCI
`Cadmium < h
Chloride
�_Z Chromium -
Copper
Fluoride
Iron
Aver y6
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
-i_Z Lead 6
Manganese
Mercury 0' to
_
_
—Nitrate. ��—T-
-,ZSelenium
_
rnn r e 71TTP r'T-TFMT.(;TRY
Parameter Results mg/I
Parameter Results mg/I
Parameter Results mg/1.
P&T:GC/MS
_ Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex) -
_
nyr1 y nv RADIOCHEMISTRY
Parameter1 ..
Parameter Results PCi/I
(\AF) Coliform Colonies/ 100m1s
__ (MPN) Coliform Colonies/ 100mis
--Gross Alpha — —
Gross Beta
ire Received
Date Reported
ire Extracted
Date Analyzed
:ported By Lab Number
U ti,'

State Laboratory of Public Health
Department of human Resources SAMPLE ANALYSES REQUEST P. °. n° zso47
ision of Health Services 306 :�. Wilmington Street
Raleigh, 27611
_ Number J �' � Q �� � 5 � � � � Field Sample Number b - Site Location %f a
me of Site ) _
ID# 3 Date Collected 3
Ilected By
pe of Sample:
Comments
Concentrate
environmental
Solid 5
Groundwater (1) ( )
Surface Water (2) Liquid (6) — --
Soil (3) Sludge (7)
Other (4) Other (8)
APR 2 7 09
INORGANIC CHEMISTRY
Extractables
Parameter
,,Arsenic
,,LBarium
i.,LCadmium
Chromium
Lead
-Z ?,,Mercury
c� ge!enium
ZSilvcr
Results mg/1 Parameter
n (_ ✓Arsenic
_Z Barium
_,zCadmium
Chloride
Chromiurr
Copper
Fl 'de
Parameter Results mg/ 1
— P&T:GC/MS
Acid,:B/N Ext.
TOX
_ uoL
Iron
Lead
Manganese D `�
Mercury
Nitrate
�.Zelenium ('
Total SDPERI"UND BRANCI-1
Results mg/1 Parameter Results mg/1
ORGANIC CHEMISTRY
Parameter Results mg/1
EDB
PCB's
Petroleum
Endrin
Lindane
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Parameter
Methoxychlor
Toxaphene
2,4-D
. 2,4,5-TP (silvex)
Results mg/ 1
MICROBIOLOGY RADIOCHEMISTRY
Parameter Parameter Results PCi/1
(1,4F) Coliform Colonics/100m1s —_ Gross Alpha
(1`4PN) Coliform Colonics/100m1s -- Gross Beta
)ate Received
)ate Extracted
Date F�eported
Date Analyzed
�cportcd By
)1.11; 1191 1 Revised 7/ 85)
Lab Number
�.. I:ri.t .JJ v

Z. Department of Human Resources SAMPLE ANALYSES REQUEST'
ision of Health Services
State Labor:.'ory of Public Health
P. O. Box 28047
306 t:,, Wilmington Street
Raleigh, 27611
Number J �G L Q 3 15 Field Sample Numbe//r��4 a
me of Site Site.)_.ocation Ilected By ---
0—� IDN 3 0 Date Collected 3 - y c( !-,me
-)e of Sample:
nvironmental
Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate Comments
ii
Solid (5) �A
Liquid (6) UN
Sludge (7)
Other (8) ,[1PP 2 7IQkL1
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
Arsenic O c>
��Arsenic
—`silver < yh
Barium 0• �%
y'Barium
Sulfates
Cadmium 6• 4 g
-.Cadmium 6
Zinc
Chromium <"Q.
— Chloride
Ph
Lead �� U
---'Chromium y
Conductivity
Mercury O- D _
Copper
TDS
Scl^nium 4 D • Oo-�5
Fluoride
TOC
12)
l Silver
Iron
—!5�1
Lead _
Manganese
✓ Mercury �' l
_
__
�itrate
_
Selenium l�
r-\ b t— n -KI T (` (-T-T P'K f T g r P V
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/ 1
— P&T:GC/MS
Acid:B/N Ext.
_ TOX
EDB
PCB's
Petroleum
Endrin
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silve\)
_
Lindane
1YLLVL\V LLV ✓vv .
Parameter
-
Parameter Results PCi/1
(MF) Coliform Colonies/1001111s
(M)N) Coliform Colonies/100nds
I —_ Gross Alpha
Gross Beta —
ate Received
ate Extracted
eported 13y
Date Reported
Date Analyzed
Lab Number

C. Deparrment of Human Resources
SAMPLE ANALYSES
State Labot..t
REQUEST
ry of Public Health
P. O. Bo\ 28047
,ision of Health Services
306 N.
Wilmington Street
Raleigh, 27611
Number J
7 3 7
Field Sample Number
me of Site
Site ) ocation _f / a r/ b� 1My
�?)--
�
a
ID9 3 �
Date Collected 3 - � � � � ( 7 i=
.e �5
Ilected By
0e of Sample:
environmental Concentrate
Comments
Groundwater (1)
Surface Water (2)
Solid (5)
Liquid (6)
Soil (3)
Sludge (7)�
v
Other (4)
Other (8)
AQ? J, 7 iORs'
TT.TrnRC:ANTC'
M4F.MTSTRY (N(MPIMP;Et Dona.trtl
Extractables
Total
Parameter
Results mg/ 1
Parameter
Resultsmg/ 1
Parameter Results mg/ 1
Arsenic
O - I
6.
��Arsenic
-� Barium
G
6 I
Silver < y6
Sulfates
L Barium
Cadmium
S
✓ Cadmium
—
Zinc
Chromium
{ 0-
Chloride
Ph
Lead
11 0
_Chromium
-
Conductivity
Mercury
Q- 0 a—
Copper
TDS
Selenium
4 O .0 C -1b
Fluoride
—
TOC
7 Silver
' ")-6
Iron
Lead
Manganese
v
_
�Z Mercury�4
_
Nitrate.
Selenium
nRC~ANTC'. t,HF.MTSTRY
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
— Acid:B/N Ext.
_ TOX
EDB
PCB's
Petroleum
Endrin
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silve\)
_
Lindane
1 .lT/_b (III TnT nnv RADIOCHEMISTRY
Parameter
Parameter Results PCi/ 1
(MF) Coliform Colonies/ I00mis
(MPN) C:oliform Colonies/ 100mis
—_ Gross Alpha
--Gross Beta
acc Reccived
Date Reported
,ice Extracted
Date Analyzed
-ported By Lab Number

N. C. Department of Human Resources SAMPLE ANALYSES REQUEST
Division of Health Services
State Laboratory of Public Health
P. O. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number J �D d
3 �5
Field Sample Number 3 a T
Name of Site
Site Location (j a Fm
a ID# 3 �
Date Collected 3 _`� � � � �
Time
Collected By
Type of Sample:
-_ :'.1 �.
Environmental
Concentrate
,"' `;c.y - Cohn Ats
✓ Groundwater (1)
Solid (5)/
Surface Water (2)
Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
TT.1nu n e T�77(� (-`HF.M
Extractables��a
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
Arsenic o ` O
ilver - S
Arsenic
__iZ
Barium 1 5-
-
Sulfates
Barium
Cadmium
✓ Cadmium l D, o S'
Zinc
Chromium
Chloride
✓ Chromium 0 '
Ph
Conductivity
Lead
Mercury
Copper
TDS
Selenium
Fluoride
TCC —
Silver
Iron
Lead Oil 3
Manganese
_ Mercury
Nitrate ,
Selenium < o 0 I
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX '.. �
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
r\T1T/1T !ll�li
i:6a1ritui":INei9tizW-MA
Parameter
Parameter Results PCi/1
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Gross Alpha
Gross Beta
Date Received
Date Extracted
Reported By
Date Reported�`�—�/U
Date Analyzed
Lab Number
DHS 3191 (Revised 7/85)

. C. Department of Human Resources State Laboratory of Public Health
ivision of Health Services SAMPLE ANALYSES REQUEST P. 0. Box 28047
306 N. Wi!mington Street
Raleigh, 27611
to Number J 5 Field Sample Number 302 .�
ame of Site Site.j,ocation . / (,-?Ia
c>
oZllected By 0ID# � Date Collected 3 V a � �� ( Time
1pe of Sample:
Environmental
Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
TTJnRC,ANTC' CHF.MTSTRY
` t4
Extractables
Tota �,
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
Arsenic C "
Arsenic
ny
� Barium O• ✓
Sulfates
Barium
— Cadmium
c/ Cadmium D. oo s
Zinc
_ Chromium
Chloride
-.ZChromium
Ph
Conductivity
_—_ Lead
Mercury
Copper
TDS
Selenium
Fluoride —
TOC
— Silver
Iron
✓ Lead
_
Manganese
Mercury
.�,c Nitrate .
`� Selenium O '
_
name NJTr' (-'TXPMTST12Y
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
XXT/-DnnTnT nr:v RADIOCHEMISTRY
Parameter
Parameter Results PCi/1
_ (MF) Coliform Colonies/ I00mis
— (MPN) Coliform Colonies/100mis
—_ Gross Alplia
Gross Beta —
)ate Received
Date Reported
)ate Extracted
.eported By
Date Analyzed
Lab Number

State Labor::ory� of Public Health
�. Department of Human Resources ision of Health Services SAMPLE ANALYSES REQUEST P. Q- Box 2S� 47
306'"11. Wilmington Street
Raleigh, 27611
Field Sample Number 3s
Number
lie of Site
Site j_-ocation /�n �� f� /y L—
)
Date Collected 3 - q - P L( -= ime
.zz
lected By
)e of Sample:
environmental
Concentrate
Comme;Kts ,t,,;,,
'�.
— — �,��:�:':'"�-�•:,.._. ,r
Groundwater (1)
Solid (5)
Surface Water (2)
Liquid (6)
y
Soil (3)
Sludge (7)
Other (4)
Other (8)
'3�fi'� �@,�•=
�-
A
Extractables
Parameter Results mg/1
Arsenic
Barium
_ Cadmium
Chromium
Lead
Mercury
_ Selenium
Silver
ell
INORGANIC CHEMISTRY
Parameter
Arsenic
Barium
Cadmium
Chloride
_L/— Chromium
Copper
Fluoride
Iron
Lead
Manganese
s, Mercury
Nitrate
Selenium
Total
Results mg/1
Parameter
-� O -
✓ Silver
O. oZ
Sulfates
O. D©sue
Zinc
Ph
<-- D • U 1
Conductivity
TDS
TOC
C-? •O-07 Ua—
_< o.av
r--% r-,.nT,,TT(' (`TXP),ATgTRY
` Iti
Results 'mg/ 1
z D -O S
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
_
Lindane
MICROBIOLOGY
Parameter
_-.—(MF) Coliform Colon ies/I00MIs
(MPN) C:oliform Colonies/ IOOmIs
atc Received
atr Extracted
:ported lay
Parameter
Gross Alpha
Gross Beta
Date Reported
Date Analyzed
Lab Number'
RAll1UUhLN11ti 1 R y
Results PCi / 1

DICISION OF iiE.-'? TE SEr 'ICES
SOLID ANTI t-- kkRDOU S WASTE YJ-N-AG:r �N T r
tC?
JcatiCU of Sa--pling
C:nain of Custod.- Record
EaZar6ous 'Waste Haterials
Generator
Storage Facility
Transpor
Disposal
Other:
r�.pany's Name � Telephone(
idress
)llec,or's Name
suture
Teleahone (y/ ) -7-3 3 -,2eO
ent Fac- i
ill
:te. Sampled �- a I -�Q q Time Sa pred
--Pe o= Process Generating Waste
:elc 11forMatiOD
_e1d Sample N3, - '3) f�%� , � ��% 30 -a 3-— 317?
(( —�
iain of Possession:
611
signature title
es`'..s reported
si gT,ature
sig„atUre
izIe-
intlus- ve dates
1n uS1V dates
inclusive. dates
Gate
T15LrUCi.lOI15: COiyDlete all 2ppliCaDle7.I1t0%.Gt10I1 111C1-UC1%7 S_g-naLUres) 2P.d
SU[):nj7 w-ith cna1vsls reaUes i iorm. s

State Laboratory of Public Health
N. C. Department of Human Resources
SAMPLE ANALYSES REQUESTP.
O. Box 28047
Division of Health Services
306 N. Wilmington Street
Raleigh, 27611
JO C� 3 1 �5
�7
T ��
l '
i� q. - `
Field Sample Nurn er' `'°:` ; r ° :'"i . , i
Site Number
Name of Site
ocaAIL
Site J._ r /y
o---�
ID# 3
c�
Date Collected 3 d g (
q
Time < n
Collected By
Type of Sample:
Environmental Concentrate
Comments
m `
.� Groundwater (1)
Solid (5)�
Surface Water (2)
Liquid (6)
Soil (3)
Sludge (7)
Other (4)
Other (8)
Total
Extractables
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Conductivity
Lead
Chromium
Mercury
Copper
TDS
Selenium
Fluoride
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Parameter Results mg/ 1
EDB
PCB's
Petroleum
Endrin
Lindane
Parameter
Gross Alpha
Gross Beta
Parameter Results mg/ 1
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
RADIOCHEMISTRY
Results PCi/ 1
Date Received 3- •'3 1- g Date Reported ~� eq
Date Extracted Date Analyzed :02'� -7uxJ
Reported By �L�---' Lab Number
DHS 3191 (RevisP7/85) C� &o
Solid and Hazardous Waste (Review 7/87)

N. C. Department of Human Resources State Laboratory of Public Health
Division of Health Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 N. Wilmington Street
Raleigh, 27611
Site Number J �D �/ 6 0 3 / S'7 3 Field Sample Number _T` 3 7� /1
Name of Site Site j_.ocation,%���/ Collected By 0' ID# Date Collected 3 - g L( Time � _ 2 36
Type of Sample: II
Environmental Concentrate a am _e?ts
Solid (5) �f-�
�! Groundwater (1) /
Surface Water (2) Liquid (6)
Soil (3) Sludge (7)
Other (4) Other (8)
TWTr VD r, e 701(- r`uF'KATC'TR V
SUPEREUND BRANCH
Extractables
Total
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chromium
— Lead
Mercury
— Selenium _
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
Silver
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene —
2,4-D
2,4,5-TP (silvex)
r l'1TlT/'lT r`r,�r K A I M It :M111ML1 I MI
1�11Vll�v ✓av ✓v v ..
Parameter
Parameter Results PCi/ 1
(MF) Coliform Colonies/100mis
(MPN) Coliform Colonies/100mis
Gross Alpha
Gross Beta
Date Received L 3 l - Rat CM Date Reported
Date Extracted LI-3-69 }i,$ a&"P0"Mk) Date Analyzed
Reported By
DHS 3191 (Revised 7/85)
r_i• _ _ c�____�_.._ wi__.., ID e..�.,... 7/R71
Lab Number C 9 () S T

N. C. Department of Human Resources State Laboratory of Public Health
Division of Department
Services SAMPLE ANALYSES REQUEST P. 0. Box 28047
306 N. Wilmington Street
_ Raleigh, 27611
Site Number J �G l� �) 3 1,5 7 377 Field Sample Number
Name of Site Site.J-ocation r ?�
L �
Collected By p,� ID# 39 Date Collected 3 g ~ l Time y% �
Type of Sample:
Environmental
Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
ATTrI r_1_7RA1fTC1rT2 V
0 W11 Jt
6n
V 1TI DR' 1��1
Extractables
Total
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium
Silver
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride —
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Ph
Conductivity
TDS —
TOC
—
—
__
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Methoxychlor
Toxaphene —
2,4-D
2,4,5-TP (silvex)
Lindane
1V11 L+L\V iJLV LVV i
Parameter
Parameter Results PCi/ 1
(MF) Coliform Colonies/100mis
(MPN) C:oliform Colonies/100mis
Gross Alpha
Gross Beta --
Date Received Date Reported
Date Extracted
Date Analyzed 14-,)4- 8'9
Reported By
DHS 3191 (Revised 7/85)
c.i:.i --.J \Y1--(Rwirw 7/87)
Lab Number P.Pi() 8 5

I. C. Department of Human Resources State Labor_tory of Public Health
livision of Health Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 N. Wilmington Street
Raleigh, 27611
ite Number J �G 1) Q L� 3 / 5 3 Field Sample Number
y� 7� (/e
lame of Site Site.Z.ocation � �
:ollected By ��� ID# -3 Date Collected 3 - ~� ( Time —Ie �
'ype of Sample:
Environmental Concentrate Come EI
Groundwater (1) Solid (5) AL (2- - ,ZZ I�V —
Surface Water (2)
Soil (3)
Other (4)
Liquid (6)
Sludge (7) �liRtC1Eain un�e,�.
„� irov l:t,lll
Other (8)
Ti.1rev ra e T.7Tr' r `T4PMTCTR V
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium —
Silver
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride —
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc I�
Ph
Conductivity
TDS
TOC
I
I
r-1 r- e 7-7Tr (`T 'PMT.qTR V
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
•.ter �r�r�r !1l�V
1.9 F-"b INMI a91LTJ101V1W4
Parameter, }
Parameter Results PCi/1
(MF) Coliform Colonies/ 100m1s
(MPN) Coliform Colonies/100mis
__ Gross Alpha
Gross Beta
--
I
I
Date Received 3- 31-59 K8 Date Reported
DateExtracted - �� ��{� Date Analyzed -
L957
Reported By Lab Number
DIMS 3191 (Revised 7/85)

C. Department of Human Resources State Labor:_::ory of Public Health
!men.vision of menti Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 t-:. Wilmington Street
Raleigh, 27611
ite Number J �C f� 3 5 13 Field Sample Number 7, /7
lame of Site Site J_ocation /n�� F �'1 1, y L
c
;ollected By �"1D#1 3 9 Date Collected 3 - T:me
'ype of Sample:
Environmental
Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
YT.TnR Cl- e 7177C' (_'"'PMTSTR V
Comments
EN��l�ll� nTAA 6f A.. -_
r . « At,19c11
Extractables
Total
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chromium
Lead
Mercury
Selenium —
Silver
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC --
nR r_' A NTC' C.T4FMTSTRY
Parameter Results mg/1
Parameter Results mg/ 1
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
rnt_1N'aTnr nrw RADIOCHEMISTRY
Parameter
Parameter Results PCi/1
(1.4F) Coliform Colonies/100mis
(1.4PN) C:oliform Colonies/ 100mis
Gross Alpha
Gross Beta
Dare Received 3 " l` Rai 'yW Date Reported
Date Extracted
Reported By
Date Analyzed L _,�Le`gG _fir
Lab Number �,9108S8
I)IIS3191 (RC%'iscd 7/85)

C. Department of 1-luman Resources State Labor..:ory of Public Health
iision of Health Services SAMPLE ANALYSES REQUEST P. U. Box 281047
306 1. Wilmington Street
Raleigh, 27611
c Number J �•� 5 '7 3 .7 '7Field Sample Number T 3 7y --
me of Site site.L ocation /oaT2-
c
,llected By ' ID#( � � Date Collected 3
pe of Sample:
Environmental
Groundwater (1)
_ Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
1r7\jr1R(--ANT(-` (-`-RT .MTSTRY
Comments
i CVI
SC° ER INID GRANICIH
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
_ Arsenic
Barium
— Cadmium
— Chromium
—_ Lead
Mercury
_—Selenium _
— Silver
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
Iron
Lead
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC —.
_
_
_
_
nTP ra A NTH rHF.MTSTRY
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
EDB
Methoxychlor
7—Acid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
Lindane
2,4,5-TP (silvex)
_
a,r,r-,pnurnT rnr`v RADIOCHEMISTRY
Parameter
Parameter Results PCi,'1
— (MF) Coliform Colonies/100mis
(MI'N) Coliform Colonies/100m1s
Gross Alpha
—_ Gross Beta
ate Reicived - I - r Date Reported
rt,
late Extracted 14-3-a9j:m8,ark, ` k),LMQ Date Analyzed � 13&
cloned By Lab Number

State Labor_.zory of Public Health
'. C. Department of Human Resources
SAMPLE ANALYSES BEQUEST
P. Box 2
Division of Health Services
306 �^d. Wilmi8047 ngton Street
Raleigh, 27611
T
J �C l� 3 5
Field Sample Number z/3 79-
---- —
ite Number
fame of Site
Site.)_.ocation,//)%(J-a fr?I � A
0--�
ID# 30
Date Collected 3 - c)
: ==me
:ollected By
'ype of Sample:
Environmental Concentrate
Comments
S`�-
`'3
Groundwater (1)
Solid (5)
T q1)aL0(':� "�
_—©
Surface Water (2)
Liquid (6)
'
Sludge
_
f^"tf
Soil (3)
(7)
i;
Other (4)
Other (8)
A 1.TT/" "LI T:IXTQ rD V
Total 15UP :lti' f'�D ru��`NC
Extractables
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
Mercury
Copper
TDS
Selenium _
Fluoride
TOC
Silver
Iron
Lead
Manganese
—
Mercury
Nitrate
Selenium
-
T\TT/- !"T- V K,(TCTR V
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1.
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin '
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
/tiT 111'lTllT V
110 offeloJwi-R 1b`NIM
1V11\�L\V L1V a.ivv i
Parameter
Parameter Results PCi/ 1
(MF) Coliform Colonies/ 100mis
(MPN) Coliform Colonies/100mis
—__ Gross Alpha
Gross Beta
Date Received 3 -3 1 Date Reported,
3-31 S_9 PLJ Date Analyzed 7-17�_ 66 j- ��N`2t4'S�I ytt�
Dare Extracted �-�
Reported By Lab Number Q008 0 --
DHS 3191 (Revised 7/85)

. C. Departent of Human Resources State Laboratory of Public Health
1.mvision of .eli Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 N. Wilmington Street
Raleigh, 27611
00
ice Number J © 0 3 I 5 3 77 Field Sample Number
lame of Site
Site.Location IeOar —
12 c
,ollected By
�� ID# � Date Collected 3 - Time
ype of Sample:
Environmental
Groundwater (1)
_ Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
A77n nT-TUI fTCTR V
Comments
Extractables
Total
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
Arsenic
Silver
Arsenic
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
Mercury
Copper
TDS
Selenium
Fluoride —
TOC
Silver
Iron
Lead
Manganese
.
_
Mercury
Nitrate
Selenium
�n t n A7T(1 0U'P_hATq'T'14 V
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
&T:GC/MS
EDB
Methoxychlor
_ACid:B/N Ext.
PCB's
Toxaphene
TOX
Petroleum
2,4-D
Endrin
Lindane
2,4,5-TP (silvex)
r ♦ rT�/lTYT1lT C'TTT �T
iVl l%_LX II Ij A.
Parameter
Parameter Results PCi/ 1
— (MF) Coliform Colonies/ 100mis
(MPN) C:oliform Colonies/ 100mis
—_ Gross Alpha
Gross Beta
Date Received 3 - 1 3� Date Reported
7 7—
Dace Extracted '5�q Date Analyzed ��"�-�� ��• �-°��`� n'i'`'y
'11� 21 0 IS SI
Reported By
Lab Number
1. HS 3191 (Revised 7/85)

State Labor::, ory of Public Health
C. Department of Human Resources SAMPLE ANALYSES REQUEST P. O. Box 28047
ivision of Health Services 306 1-3. Wilmington Street
Raleigh, 27611
ite Number J (9 3 15 3 7 Field Sample Number Y_3 (?
�amc of Site / A / —
Site j_ocation / )a fzSL`2a / �' J —
>
'.ollected By
P— ID# Date Collected 3 - c( T,me
ype of Sample:
Environmental Concentrate Comments
/I
Groundwater (1) Solid (5)
Surface Water (2) Liquid (6) 3 � "
Sludge 7 ' �°� �VE
F
_� Soil (3) g ( )
Other (4) Other (8) -
• ��Tr, riY L`A AT QT'DV 4�31fi"eP"d'�f't t51<*•, ?ti ?.S aen,.
Total
_..
Extractables
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chromium _
Lead
Mercury
Selenium
Silver
Parameter Results mg/ 1
Parameter Results mg/ 1
Arsenic
Barium
Cadmium
Chloride
Chromium
Copper
Fluoride
I �--
Iron
Lead -
Manganese
Mercury
Nitrate
Selenium
Silver
Sulfates
Zinc
Ph
Conductivity
TDS
TOC
,
_
r�ri r n i.�T r, t"TZ VAA7 QTR V
arameter Results mg/ 1
Parameter Results mg/ 1
Parameter Results mg/ 1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D —
2,4,5-TP (silvex)
--
MICROBIOLOGY
Parameter
(MF) Coliform Colonies/100mis
(MPN) C:oliform Colonies/100mis
Parameter
Gross Alpha
Gross Beta
KAL)1UUHtM1J l K Y
Results PCi/1
Dare Received 3' -g� S Date Reported R — _
$ `
Date Extracted �I' Date Analyzed
08fF", .
Number
Nu "
Reported By La -
1�1IS 3191 (Revised 7/85)

I. C. Department of Human Resources State Labor:it_-.ry of Public Health
)ivision of Health Services SAMPLE ANALYSES REQUEST P. O. Box 28047
306 IN. Wilmington Street
T Raleigh, 27611
itc Number J ©�� �5 Field Sample Number
L
lame of Site Site.J_ocation-
c
._
;ollected By a"`� ID#! `3 � Date Collected 3� q 1 Ti: e
ype of Sample:
Environmental
Groundwater (1)
Surface Water (2)
Soil (3)
Other (4)
Concentrate
Solid (5)
Liquid (6)
Sludge (7)
Other (8)
IT-7nR C-, A N T C' CHEMISTRY
Comments
Extractables
Total t3ip -it,,, f=.��.,�
idil-d 'r!d!! i e _
✓Results
Parameter Results mg/ 1
Parameter Results mg/ 1
Parameter mg/ 1
Arsenic
Arsenic
Silver
Barium
Barium
Sulfates
Cadmium
Cadmium
Zinc
Chromium
Chloride
Ph
Lead
Chromium
Conductivity
Mercury
Copper
TDS
Selenium
Fluoride
TOC
_— Silver
Iron
Lead
Manganese
_
Mercury
Nitrate
Selenium
�v n n T.TTf' r,"P'K _fq rP V
Parameter Results mg/1
Parameter Results mg/1
Parameter Results mg/1
P&T:GC/MS
Acid:B/N Ext.
TOX
EDB
PCB's
Petroleum
Endrin
Lindane
Methoxychlor
Toxaphene
2,4-D
2,4,5-TP (silvex)
LVL L V L\ II LJ L k_1A-vv i
Parameter
Parameter Results PCi/1
(MF) Coliform Colonies/100mis
(MPN) C:oliform Colonies/100mis
Gross Alpha
-- Gross Beta
Date Received -3 - Date Reported
Date Extracted ��'Z,l-Sc} Date Analyzed '!7-9 1_b �'4- �-R!9l a_
0,Ce086)3
Reported By Lab Number ` •'''
Il1-10 3 1 Q I r R,•.• s,•,1 7 /85 )

DIVISION OF HEALTH SERVICES SOLID AN` AN` b.7ARDOUS WASTE ? A2E -AGE*='T 'ICE
Chain of Custody- Record
Bazardous Waste 2-Saterials
C Y " Y Y�ar V11 �� � 1:�nt FYA�
,ocatien of Sampling: Generator TransDo. tee_ G ?� ti [, F �¢re ent Facil e
Storage Facility Disposal 7zcility Landfill
Other: 1 ;
ompan;-'s Name Z-42 lj�j} / ►`� � Telephone
Adress
ollector's Name
signature'
J
TeleDnoae (y/ ?
ate Sampled j - - <Q Time Sampled
ype of Process Generating Waste
V'
ielc 1 reformation
i. e1 d Sample N o . � 3 3 '3 7 Y
-32
pain of Possession:
Neste-zs reported
•--
inclusive dates
LS)UAJ-(Qcx C-R�n� . Q�� "�. . --- 3 ;3I - 9 9
signature title inclusive dates
signature
sl&7�aL_Ure
t i z 1 e
inclusive dates
Q a t e
1.n5-rUCtiOnS: Cooplete all applicable lniL
0ii.,ct1011 1nC1:JCil%` S:.gilaLUreS, and
subm-: L with '.analysis reauest forms.

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
1 ACID
EXTRACTABLES
/
1
ZMMW
♦
r
sWliW
N-nitrosodimethyl
•• ••
• •
■■��■__■_.■_
• • • • .
■■_�■__■�■_■S
hexachloroethane■■��
_■�■_■S
nitrobenzene
1,2,4-trichlorobenzene■■
�■
naphthalene
hexachlorobutadiend
,6-trichlorophenol
2,4acenaphthene
■■ice
acenaphthylene
dim6thyl phthalate
•
■■■
�■�®
• '
:
�■
�■■i■t
fluorene
diethyl plithalate
MOM
azobenzene
hexachlorobenzene 10
pentachlorophenol
•
/ o
_`■■__�dibutyl
anthracene
phthalate
fluoranthene��■�
m-D L
J - Estimated value. f'12.0/50/L-
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but .not detected. The number is the Minimum Detection Limit. MDL
NA - Not analyzed.
l/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
N.C. D.iviz i.Un a 6 Neat th S ehv.icu
DNS 3068-0 (4186 Labanatmy)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST.. RALEIGH, N.C. 21611
ORGANIC CHEMICAL ANALYSIS
BASE/NEUTRAL
COMPOUND
TYPE
pyrenebenzidine
butyl benzyl phthalate
• -
chrysene
�'�_�_�'®
o • •
• • .
• • • •
-____A�____
aniline
/ YI
benzoic aci•
• . • •
m�bI-
J - Estimated value. Ha01.1-0/L
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number
NA - Not analyzed.
l/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
is the Minimum Detection Limit.
N.C. Viui,ion o5 Heatth SeJviceb
DHS 3068-0 (4186 Laboka,tmy)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
11RrANTr MPMTrAI AMAI VCTC
BASE/NEUTRAL AND ACID
EXTRACTABLES
LAB NO
113
FIELD #
COMPOUND
TYPE
(•
(
( )
UNITS
/k
/1 /k
/1 /k
/1 /k
/l /k
/1 /k
N-nitrosodimeth lamine
p
Cal..
bis(2-chloroeth 1)ether
2-chlorophenol
phenol
1 3-dichlorobenzene
1 4-dichlorobenzene
1 2-dichlorobenzene
bis(2-chloroi 1)ether
hexachloroethane
-
b`a,r
ll
N-ni troso-di .-n 1 amine
, , ; -;.-•
nitrobenzene
isophorone
2-nitrophenol
MITI,!) i`(ANMI
i
2 4-dimeth 1 henol
F
bis 2-chloroethox methane
2 4-dichlo henol
1 2 4-trichlorobenzene
naphthalene
hexachlorobutadiene
4-chloro-m-cresol
hexachloroc cl ntadiene
2 4 6-trichlo henol
2-chloronaphthalene
acenaphthylene
dimeth 1 phthalate
2 6-dinitrotoluene
acenaphthene
2,4-dinitrophenol
SO 65'O
2 4-dini.trotoluene
0
4-nit henol
0 0
fluorene
101330
4-chlorophenylphenylether
diethyl phthalate
4 6-dinitro-o-cresolJ-0/96510
di hen lamine
azobenzene
111/
4-bromophenylphenylether
33 D
hexachlorobenzene
pentachlorophenol
Mho
henanthrene
1,01330
33 0 K.
anthracene
I
33 .
dibut 1 phthalate
U_
fluoranthene
3
m-D L
J - Estimated value. 9'0/s0/L
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number is the Minimum Detection Limit. M 2) L
NA - Not analyzed.
1/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
N.C.. Divizion ab HeaLth Senvicu
DHS 3068-0 (4186 Labanatany)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, H.C. DEPARTMENT OF HUMAN RESOURCES
P.O. 00X 28047 - 306 H. wliMINCTO*. D.. KxiElSH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
COMPOUND
TYRE
CA—
t>enzo(k)fluoranthene
Lk'
benzoic acid
t>enzyl alcohol
M'bL
J - Estimated value. Hw- 0/ SO���
K - Actual value is known to be less than valve given.
L - Actual valve is known to be greater than value given.
u - Material was analyzed for but not detected. The number
NA - Not analyzed.
l/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
is the w\o\nmm Detection Limit. ��77)U
N.C. Vio^&ioo 06 KeuZth SeAo�cU
OKS 3068-0 (4/86 La6mutm4)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C_ DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON, ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
PURCEABLE COMPOUNDS
LAB NO
q©O ."
FIELD #
43 -7
43
4,3s7o
Lfo •
COMPOUND
TYPE
( 1
t
l
(3
UNITS
/kj
/k
/1 /k
/1 /k
/1 /k
chloromethane
bromomethane
dichlorodif1uoromethane
f
pb
i
t
I
i
vinyl chloride
chloroethane
methylene chloride
trichlorofluoromethane
ethene 1 1-dichloroti�'(i
I
-
ethane 1 1-dichloro-
1 2-trans-dichloroethene
7
�%
chloroform
1
ethane 1 2-dichloro-
!
ni
--•-.••
-
i
ethane 1 1 1-trichloro-
"1 6i
F i
4.
carbontetrachloride
brarKAichlorcmethane
propane, 1,2--dichloro-
1,3-trans-dichlor,opropene
i
trichloroeth lene
chlorodibromomethane
benzene
ethane 1 1 2-trichloro-
1 3-cis-dichlo ne
!
'
2-chloroeth 1 vinyl ether
!
1
bromoform
�—
ethane, 1 1 2 2-tetrachloro-
ethene tetrachloro-
toluene
chlorobenzene
eth lbenzene
acetone
LA-�-
2-butanone
j
1
carbondisulfide
i
!
2-hexanone
4-methyl-2 ntanone
i
styrene
vinyl acetate
1
x lens
j - tstimated value.
K - Actual value is known to be less than value given.
L - Actual value is known to be greater than value given.
U - Material was analyzed for but not detected. The number is the Minimum Detection Limit.
NA - Not analyzed.
1/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
N.C. Division of Health Services
D1lS 3068-0 (4/86 Laboratory)

STATE LABORATORY OF PUBLIC HEALTH
DIVISION OF HEALTH SERVICES, N.C. DEPARTMENT OF HUMAN RESOURCES
P.O. BOX 28047 - 306 N. WILMINGTON. ST., RALEIGH, N.C. 27611
ORGANIC CHEMICAL ANALYSIS
PURGEABLE COMPOUNDS
LAB NO
a oo $(D3
FIELD a
4 3 r
COMPOUND
TYPE
( 3
UNITS
/1 /k
/1 Vglkg
V9/l /k
/1 /k
/1 /k
/1 /k
chloromethane
brcanTethane
dichlorodifluoromethane
vinyl chloride
chloroethane
methylene chloride
trichlorofluoromethane
ethene 1 l-dichloro
ethane 1 1-dichloro-
1 2-trans�ichlorcethene
_H�,�i7
*.a l
chloroform
ethane 1 2-dichloro-
ethane 1 1 1-trichlorc-
carbontetrachloride
.PF-R,
<<'.:! 1,
bromodi chl orcmethane
propane, 1,2-dichloro-
1,3-trans-dichloropropew
trichloroeth lene
chlorodibranomethane
benzene
ethane 1 1 2-trichloro-
1 3-cis-dichlo ne
2-chlorceth 1 vinyl ether
bronoform
ethane 1 1 2 2-tetrachloro--
ethene tetrachloro--
toluene
chlorobenzene
eth lbenzene
acetone
p b
2-butanone
carbondisulfide
2-hexanone
4-methyl -2ntanone
styrene
vinyl acetate
,
x l enes 64,+al
V — LJ 111$dLCU vdiue.
K - Actual value is known to be less than value given.
L - Actual value -is known to be greater than value given.
U - Material was analyzed for but not detected. The nuaber is the Minimun Detection Limit.
NA - Not analyzed.
l/ - Tentative identification.
2/ - On NRDC List of Priority Pollutants.
N.C. Division of Health Services
DHS 3068-0 (4/86 Laboratory)

ermit No. NC0004243
e
STATE OF NORTH CAROLINA
DEPARTMENT OF NATURAL RESOURCES & COMMUNITY DEVELOPMENT
DIVISION OF ENVIRONMENTAL MANAGEMENT
PERMIT
To Discharge Wastewater Under The NATIONAL
POLLUTANT DISCHARGE ELIMINATION SYSTEM
In compliance with the provisions of North Carolina General Statute
143-215.1, other lawful standards and regulations promulgated and adopted
by the North Carolina Environmental Management Commission,'and the Federal
Water Pollution Control Act, as amended, '
The American Thread Company, Inc.
is hereby authorized to discharge wastewater from a facility located at
American Thread Company
Sevier Finishing Plent'
McDowell County
to receiving waters
North Fork Catawba River in the Catawba River Basin,
in accordance with effluent limitations, monitoring requirements, and other
conditions set forth in Parts I, II,.and III hereof.
This permit shall become effective October 16, 1978.
This permit and the authorization to discharge shall expire at midnight
on March 31, 1981.
Signed this day of October 16, 1978.
by
A. F. McRorie, Director
Division of Environmental Management
By Authority of the Environmental
Management Commission
M 1 & I 1