WQ0019960_Application_20070416

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APPLICATION FOR PERMIT MODIFICATION
AND RENEWAL
CITY OF MARION
PERMIT NO. WQ0019960
Prepared For:
City of Marion
Post Office Drawer 700
Marion, North Carolina 28752
Prepared By:
Branch Residuals & Soils, LLC
311 B South Westgate Drive
Greensboro, North Carolina 27407
March 2007

BRANCH RESIDUALS & SOILS, LLC
311 B South Westgate Drive • Greensboro, NC 27407
PHONE [phone] • FAX [phone]
March 29, 2007
NCDENR -Division of Water Quality
Aquifer Protection Section
Non -Discharge Permits
2728 Capital Boulevard
Raleigh, North Carolina 27604
Attention: Mr. Ed Hardee
Reference: MODIFICATION OF PERMIT NO. WQ0019660
City of Marion
Residual Solids Management Program
BR&S Job No. 2006-51
Dear Mr. Hardee:
Branch Residuals & Soils, LLC is under contract with the City of Marion to provide assistance in
the preparation of a permit renewal and modification to the above referenced permit. The city of
Marion request modifications on the following areas:
1. increase acreage of two previously permitted fields,
2. decrease TCLP monitoring from annually to once per permit cycle, and
3. remove the lime tower from the current wastewater treatment plant.
The purpose of the lime tower was as a back up in case volatile solids reduction requirements were
not met. Currently, the City of Marion has an air permit for this structure, but it no longer has any
lime in the tower. If there are 'notifications that should be made to' other agencies other than air
quality, please let me know. Your attention in the review of this application would be greatly
appreciated. Please contact me immediately if you require additional information or have questions
in the review of the permit application.
Sincerely,
rr ,
Robert T. Branch, L. S. S.
Project Manager
cc: Mr. Robert Boyette — City Manager City of Marion, North Carolina

Va.MOR
CITY OF NARION WATER AND SEWER FUND 10274 -
Aquifer Protection Divisi
Mm
03/26/z o07
CHECN NUMBFA
304015
NVOICE NUMBER
NVOICE MTE
INVOICE MOUNT
DISCOUNT
FMOUw RAU
032107
3/26/2007
325.00
325.OD
10274 Aquifer Protection Division N
Invoice # Inv Date PO Number Description
032107 3/26/2007
Check Total 325.00
03/26/2007
Check Total
304015
Amount
325.00
325.00

TABLE OF CONTENTS
Section No. Title
I NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM
II RESIDUALS SOURCE CERTIFICATION ATTACHMENT
Ha Facility vicinity map
Hb Process flow diagram and map
He Justification for residuals production rate
Ild Residuals sampling plan
III LAND APPLICATION SITE CERTIFICATION ATTACHMENT
IIIb County Manager Notification Attachment
IV JAMES C. FISHER
Landowner Agreement Attachment
Buffer Waiver Agreement Attachment
Vicinity and Buffer Maps
Soils Evaluation for Modified Site
Cumulative pollutant loading rates and analysis of soil samples to
include heavy metals
V MARIO DELUCA
Landowner Agreement Attachment
Buffer Waiver Agreement Attachment
Vicinity and Buffer Maps
Cumulative pollutant loading rates and analysis of soil samples to
include heavy metals
VI NANCY ROSS
Landowner Agreement Attachment
Vicinity and Buffer Maps
Soils Evaluation for Modified Site
Cumulative pollutant loading rates and analysis of soil samples to
include heavy metals

NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAM
(FORM: NDRLAP 10-06)
-- The Division of Water Quality will not accept this application unless all the instructions are followed. Failure to
submit all of the required items will lead to additional processing and review time.
For more information, visit our weh site at. http://h2o.enr.state.nc.us/7aulmain.hhnl
A. Application Form: (All Application Packages):
✓ Submit one original and two copies of the completed application package. Any changes made to this form will result in the
application being returned. The Division of Water Quality will only accept application packages that have been fully
completed and all applicable items are addressed.
✓ Non -dedicated residuals land application programs are ones in which all land application sites do not meet the criteria in 15A
NCAC 2T .1102(12). Specifically, a residuals land application program cannot be designated as non -dedicated if any of the
following is applicable:
♦ Any land application site certified for ,the residuals land application program that receives residuals at rates or
frequencies greater than agronomic rates.
♦ Any land application site certified for the residuals land application program that is used primarily for residuals
disposal, and agricultural crop production is of secondary importance.
♦ Any land application site certified for the residuals land application program that receives residuals through fixed
irrigation facilities or irrigation facilities fed through a fixed supply system.
✓ The signing official must meet the criteria stipulated in 15A NCAC 2T .0106(b). An alternate person may be designated as
the signing official, provided that a delegation letter from a person who meets the referenced criteria is submitted. The
delegation letter does not have to be resubmitted if the signing official has not changed since the last permitting action
associated with this residuals land application program.
✓ If this project involves a modification of an existing permit, submit one copy of the existing permit.
✓ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units.
B. Application Fee (New and Major Modification Application Packages):
✓ For new permits submit a check in the amount of $1,090 if over or equal to 300 acres of land required or $675 if less than
300 acres of land required, made payable to: North Carolina Department of Environment and Natural Resources (NCDENR).
Major modification fee are $325 and $205, respectively
C. Cover Letter (All Application Packages)
Submit a cover letter, which lists all items and attachments included in the application package as well as a brief project
description.
✓ If necessary for clarity, include attachments to the application form. Such attachments will be considered part of the
application package and should be numbered to correspond to the section to which they refer.
D. Environmental Assessments (May be Required — See 15A NCAC 1 C .0300):
✓ Submit one copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the
residuals treatment and storage facilities. An EA may also be required for private systems if any .public funds and/or lands
are used for the construction of the subject facilities.
E. Submission of Application Packages:
✓ To determine which attachment forms and supplemental attachments are required to make a complete application package,
read the instructions of each attachment form carefully. Application packages should be organized and bound (i.e., stapled,
placed in three-ring binder, etc.) in the following order prior to submission:
♦ Cover letter and application fee.
♦ Attachment Order 1: Non -Dedicated Residuals Land Application Programs (FORM: NDRLAP 10-06).
Attachment Order 1-a: Signing official delegation letter.
♦ Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA 10-06).
♦ Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA 10-06).
✓ The application package should be sent to the address at the end of this application form. Do not submit this application
package to any Division regional office.
FORM: NDRLAP 10-06 Page 1 of 6 Attachment Order 1

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
NON -DEDICATED RESIDUALS LAND APPLICATION PROGRAMS
(THIS FORMMAYBE PHOTOCOPIED FOR USE ASANORIGINAL)
! Application Number: (to be completed by DWQ)
AQUIx�A fl � �� NR /DIIV
I. OWNERSHIP INFORMATION: MAR �� 'FCT/QN
1. Specify whether the process facility is owned by: 0 2007
❑ County: ❑ Federal: ❑ Municipal; ❑ State: ❑ Non -Government
2. Owners name (please specify the name of the municipality, corporation, individual, etc).
Mr. J. Robert Boyette, City Manager
Mailing address: P.O. Drawer 700
City: Marion State: NC Zip: 28752
Physical address: 194 N. Main Street
City: Marion State: NC Zip: 28752
Telephone number. ( 828 ) 652-3551 Facsimile number. (828 ) 652-1983
E-mail address: [e-mail]
3. Signing official's name and title: (See Instruction A)
Mr. J. Robert Boyette, City Manager
Mailing address: P.O. Drawer 700
City: Marion State: NC Zip: 28752
Physical address: 194 N. Main Street
City: Marion State: NC Zip: 28752
Telephone number. ( 828 ) 652-3551 Facsimile number: ( 828 ) 652-1983
E-mail address: [e-mail]
H. PERMIT INFORMATION:
i. Application is for ❑ new, ® modified, ® renewed permit (check all that apply).
2. Fee Submitted: $ 325.00 (See Instruction B)
3. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number WQ0019960 ,
Most recent issuance date April 24, 2002 , and the expiration date June 30, 2006
Date of most -recently certified Attachment A: April 24„ 2002
Date of most -recently certified Attachment B: July 12, 2005
FORM: NDRLAP 10-06 Page 2 of 6 Attachment Order 1

4. Check all that apply to the requested permit modification:
the maximum permitted annual dry tonnage for existing residuals
❑ INCREASE ❑ DECREASE source -generating facility(ies) certified for this residuals land
application program.
❑ ADD ❑ DELETE residuals source -generating facility(ies) to/from those certified for
this residuals land application program.
® INCREASE ❑ DECREASE the net acreage associated with land applications site(s) currently
certified for this residuals land application program.
❑ ADD ® DELETE land application site(s) to/from those certified for this residuals land
application program.
N OTHER. Explain: Renewal, Remove Lime Tower from WWTP, Reduce TCLP 115 yrs.
M. RESIDUALS LAND APPLICATION PROGRAM INFORMATION:
1. County where residuals land application program is headquartered: McDowell
2. Count(ies) where residuals source -generating facilities are located McDowell
3. Count(ies) where land application sites are located: McDowell
4. Program Contact person and/or consulting firm who prepared application:
Branch Residuals & Soils, LLC
Mailing address: 311 B South Westgate Drive
City: Greensboro State: NC Zip: 27407
Physical address: 311 B South Westgate Drive
City: Greensboro State: NC Zip: 27407
Telephone number: ( 336 ) 510-0340 Facsimile number: ( 336 ) 510-0341
E-mail address: bbranchObranchrs.com
5. Who will be responsible for the day-to-day management of the residuals land application program:
❑ Permittee or ® residuals management firm. If a residuals management firm, complete the following:
Firm contact person and title: Mr. Dennis Key- President- Southern Soil Builders, Inc.
Firm name: Southern Soil Builders, Inc.
Mailing address: 958 Hoots Road
City: Roaring River State: NC
Physical address: 958 Hoots Road
Zip: 28669
City: Roaring River State: NC Zip: 28669
Telephone number: ( 336 ) 957-8909 Facsimile number: (_336 ) 957-8940
E-mail address: [e-mail]
FORM: NDRLAP 10-06 Page 3 of 6 Attachment Order I

6. List the Operator In Responsible Charge (ORC) and all Back -Up ORCs for the residuals land application prog
ram,
their certification numbers, and their affiliations in the following table:
Designation
Name
Affiliation
Certification
Number
ORC
Dennis Key
Southern Soil Builders, Inc.
13532
Back -Up ORC
David Key
Southern Soil Builders, Inc.
23629
Additional Back -Up ORCs
(if applicable)
If an ORC and at least one Back -Up ORC are not currently designated for this residuals land application
program, provide the candidates' names, affiliations, and an estimated time schedule for each candidate's
completion of the required training school and certification test:
7. Complete the following tables regarding management of the residuals land application program:
a. Plant Available Nitrogen Summary. Determine the maximum plant available nitrogen (PAN) generated
by all residuals source -generating facilities as currently certified and proposed for certification with this
application and list the results in the following table:
Maximum amount of residuals to be certified: 290 dry tons ner vear_
PAN
First - Year
Pounds of PAN per Dry Ton
(Weighted Average)
Pounds of PAN per Year
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
1 35.57
36.17
10,314.72
10,488.72
Five Year Maximum Adjusted
1 56.47
57.07
16,376.53
16,550.53
b. Land Application Site Use Summary: Summarize information regarding the land application sites as
currently certified and proposed for certification with this application:
Category
Use
Acres
Comments
Crops
Forest or Plantation
0.00
Row Crops
0.00
Hay
35.60
Pasture
96.10
Total.
131.70
Methods
Surface
131.70
Incorporation or Injection
0.00
Total.-
131.70
Restrictions
Year -Round
131.70
Seasonal
0.00
Total:
131.70
FORM: NDRLAP 10-06 Page 4 of 6 Attachment Order 1

C. Residuals Land Application Summary: Determine the minimum acreage required to land apply the
residuals as currently certified and proposed for certification assuming the scenarios listed in the
following table:
Assumed
Application Rate
abs PAN/ac yr)
Acres Required Using
First -Year PAN Concentration
Acres Required Using
Five -Year Maximum Adjust PAN
Concentrations
Surface
Incorporation or
Injection
Surface
Incorporation or
Injection
70
147.35
149.84
233.95
236.44
150
68.76
1 69.92
109.18
110.34
250 1
41.26 1
41.95
65.51
66.20
8. Identify and provide a plan as well as a schedule to resolve any issues that would prevent land application
of the proposed residuals due to the violation of North Carolina Administrative Code (e.g. not enough storage,
not enough land, vector reduction practices not in place, etc.)
FORM: NDRLAP 10-06 Page 5 of 6 Attachment Order 1

Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned' .a wastewater
facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or
abandoned, are compliant with active compliance schedule, and do not have any overdue annual fees under Rule 2T
.0105.
❑ Yes ® No, Explain:
I, Mr. L Robert Boyette, City Manager , attest that this application for City of Marion
Land Application Permit Renewal and Modification I has been reviewed by me and is accurate
and complete to the best of my knowledge. I understand that the Division of Water Quality may not conduct a technical
review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in
the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement
action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against
the Division of Water Quality should a condition of this permit be violated. I also understand that if all required parts
of this application are not completed and that if all required supporting information and attachments are not included,
this application package will be returned to me as incomplete. I further certify that the applicant or any affiliate has not
been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not
have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active
compliance schedule, and do not have any overdue annual fees under Rule 2T .0105. Note: In accordance with North
Carolina General Statutes § 143-215.6A and §143-215.6B, any person who knowingly makes any false statement,
representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not
to exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: - V Date:
RECEIVED / DENR / DWQ
AQUIFFR :oRnTFCTrnN cf:CTIQN
NAR 0 2007
THE COMPLETED APPLICATION PACKAGE,
INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS,
SHOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
AQUIFIER PROTECTION SECTION
LAND APPLICATION UNIT
By U.S. Postal Service:
1636 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1636
3202007 5:37 PM.
By Courier/Special Delivery:
2727CAPITAL BOULEVARD
RALEIGH, NORTH CAROLINA 27604
TELEPHONE NUMBER: [phone]
FORM: NDRLAP 10-06 Page 6 of 6 Attachment Order 1

RESIDUALS SOURCE CERTIFICATION ATTACHMENT

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(MS FORMMA Y BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
The Division of Water Quality (Division) will not accept this attachment unless all the instructions are
followed. Failure to submit all required items will lead to additional processing and review time.
For more information, visit our web site at: hQ.-Ilh2o.enr.state.nc.us/7au/main.html
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
_ _� ✓ Do not submit this attachment form for review without a corresponding residuals program application
form (FORM: NDRLAP 10-06, FORM: DRS 10-06, or FORM: SDRS 10-06).
✓ Any changes to this attachment form will result in the application package being returned.
✓ For new residuals programs or renewed residuals programs, submit a separate attachment form for each residuals
source -generating facility to be certified for this residuals program.
✓ For modified residuals programs in which any modification to the certified residuals -source generating facilities is
proposed, submit a separate attachment form for only those residuals source -generating facilities that are affected
by the proposed modification.
✓ The attachment should be organized prior to submission in the following order (i.e., by facility):
♦ Attachment Order 2: Residuals Source Certification Attachment (FORM: RSCA 10-06).
➢ Attachment .Order 2-a: Vicinity map.
➢ Attachment Order 2-b: Process flow diagram and/or narrative.
➢ Attachment Order 2-c: Quantitative justification for residuals production rate.
➢ Attachment Order 2-d: Sampling plan.
➢ Attachment Order 2-e: Laboratory analytical reports and operational data.
B. Residuals Source -Generating Facility Information:
✓ Attach a vicinity map that shows the location of the facility and meets all of the criteria in the latest version of the
document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals Permitting
Programs."
✓ Attach a detailed narrative and/or process flow diagram that describes how the residuals are to be generated,
treated, processed, and stored at the facility.
✓ Attach a quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is
the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that
this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any
chemicals, amendments, or other additives that are added to the residuals during processing.
C. Residuals Quality Information:
- ✓ Attach a detailed sampling plan for the residuals. source -generating facility. Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In
addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable
pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be
completed on the residuals as they are to be land applied, distributed, and/or disposed.
✓ Attach reports for all laboratory analyses used to complete this attachment form Attach documentation that the
facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction
reduction requirements.
✓ Item II. 3. does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100%
non -municipal, domestic wastewater only.
FORM: RSCA 10-06 Page 1 of 8 Attachment Order 2

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(THIS FORMMAYBE PHOTOCOPIED FOR USE ASAN ORIGINAL)
Applicant's name: City of Marion
Check all that apply: ❑ NEW RESIDUALS PROGRAM ® RENEWED RESIDUALS PROGRAM
❑ INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals
source -generating facility certified for this residuals program.
Current: 290 Dry Tons/yr. and proposed: 290
❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for
this residuals program.
® OTHER Explain: Reduce TCLP from annually to once per permit cycle
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Name of facility: Corpening Creek WWTP
2. Facility permit holder: City of Marion
Facility permit holder is (check one): ❑ federal, ❑ state, 0 local government, or ❑ private.
Facility permit number: NCO019660
Facility permit issued by (check one): ® Div. of Water Quality, ❑ Div. of Environmental Health, or
❑ other (explain: ).
3. If the facility permit is not issued by the Div. of Water Quality, complete the following:
a. Facility contact person and title:
Facility complete mailing address:
H
a
City: State: Zip:
Telephone number: ( ) Facsimile number: ( )
E-Mail address:
b. Facility complete location address:
City: State: Zip:
County:
Latitude: and longitude:
County where facility is located: McDowell
Purpose of the facility (check one):
® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater, or
(approximate percentages: % industrial and % domestic)
❑ other (explain:
FORM: RSCA 10-06 Page 2 of 8 Attachment Order 2

State of North Carolina
f Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(THIS FORMMAYBEPHOTOCOPIED FOR USEASANORIGINAL)
1 6. Is the facility required to have an approved pretreatment program: ® yes ❑ no.
7. Facility permitted/design flow: 3.0 MGD and facility average daily flow: 0.8 MGD.
8. Average amount of residuals to be .certified for this facility: 290 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment:
Type and volume of residuals storage (i.e., outside of residuals treatment units): None
H. RESIDUALS QUALITY INFORMATION (See Instruction C.):
I. Specify if residuals are regulated under (check one): ® 40 CFR Part 503 or ❑ 40 CFR Part 257.
2. Specify if residuals are intended for (check one):
❑ Land Application/Distribution (Class A or Equivalent).
Complete all items EXCEPT Items II. 4b., 7b., and 7c.
® Land Application (Class B or Equivalent).
Complete all items EXCEPT Items II. 4b., 7a., and 7c.
❑ Surface Disposal.
Complete all items EXCEPT Items II. 4a., 5., 7a., 7b., and 8.
***FORM: RSCA 10-06 CONTINUES ON NEXT PAGE***
FORM: RSCA 10-06 Page 3 of 8 Attachment Order 2

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(THIS FORMMAYBE PHOTOCOPIED FOR USE ASANORIGINAL)
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-
hazardous under RCRA:
a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-§261.24:
❑ yes ® no. Fill in the following tables with the results of the latest toxicity
characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and
reactivity: laboratory. PAR Laboratories and date of analysis: 4/28/04
Passed corrosivity test: ® yes ❑ no. pH: 6.3 s.u. (2 < pH < 12.5).
Passed ignitability test: N yes Elno. Flashpoint: >200 °F (> 140°F). -
Passed reactivity test: ® yes ❑ no. HCN: N' mg/kg (<250) & HZS: Non mg/kg (<500)
TCLP Parameter
Limit
mg/L)
Result
(mg/L)
TCLP Parameter
Limit
mg/L
Result
m97L)
Arsenic
5.0
<0.5
Hexachlorobenzene
0.13
<0.013
Barium
100..0
<10.0
Hexachloro-1,3-Butadiene
0.5
<0.05
Benzene
0.5
<0.05
Hexachloroethane
3.0
<0.3
Cadmium
1.0
<0.1
Lead
5.0
<0.5
Carbon Tetrachloride
0.5
<0.05
Lindane
0.4
<0.04
Chlordane
0.03
<0.003
Mercury
0.2
<0.02
Chlorobenzene
100.0
<10.0
Methoxychlor
10.0
<1.0
Chloroform
6.0
<0.6
Methyl Ethyl Ketone
200.0
<20.0
Chromium
5.0
<0.5
Nitrobenzene
2.0
<0.2
m-Cresol
200.0
<20.0
Pentachlorophenol
100.0
<10.0
o-Cresol
200.0
<20.0
Pyridine
5.0
<0.5
p-Cresol
200.0
<20.0
Selenium
1.0
<0.1
Cresol
200.0
<60.0
Silver
5.0
<0.5
2,4-D
10.0
<1.0
Tetrachloroethylene
0.7
<0.07
1,4-Dichlorobenzene
7.5
<0.75
Toxaphene
0.5
<0.05
1,2-Dichloroethane
0.5
<0.05
Trichloroethylene -
0.5
<0.05
1,1-Dichloroethylene
0.7
<0.07
2,4,5-Trichlorophenol
400.0
<40.0
2,4-Dinitrotoluene
0.13
<0.013
2,4,6-Trichlorophenol
2.0
<0.2
Endrin
0.02
<0.002
2,4,5-TP (Silvex)
1.0
<0.1
Heptachlor and its Hydroxide
0.008
<0.0008
Vinyl Chloride
0.2
<0.02
FORM: RSCA 10-06 Page 4 of 8 Attachment Order 2

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 10-06)
(TIHSFORMMAYBE PHOTOCOPIED FOR USEASANORIGINAL)
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the
residuals do not violate the ceiling concentrations for metals regulated under'40 CFR Part 503 or 40 CFR Part
257:
a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a
dry weight basis) for the following metal parameters:
Laboratory A&L Eastern Agricultural Labs and date of analysis: 1/19/05
Parameter
Ceiling
Concentration Limits
(Class A & Class B)
(mg1kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg1kg)
Result
(mg1kg)
Arsenic
75
41
1.94
Cadmium
85
39
3.60
Copper
4,300
1,500
506.00
Lead
840
300
22.00
Mercury
57
14
2.04
Molybdenum
75
n/a
67.00
Nickel
420
420
22.00
Selenium
100 1
100
5.10
Zinc
7,500 1
2,800
1,092.00
C. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory
and date of analysis:
Closest Distance to
Property Lines
(meters)
Arsenic
(mg/kg)
Chromium
(mg/k�
Nickel
(mg/kg)
> 0 but < 25
30
200
210
> 25 but < 50
34
220
240
> 50 but < 75
39
260
270
> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125 but < 150
62
450
420
> 150 1
73 1
600
420
FORM: RSCA 10-06 Page 5 of 8 Attachment Order 2

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 3.21 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the
following nutrient and micronutrient parameters: laboratory. A & L Agricultural Labs
and date of analysis: January 19, 2005
Parameter
Result
(mg/kg, dry weight)
Aluminum
24,053.00
Ammonia -Nitrogen
600.00
Calcium
1.61
Magnesium
0.47
Nitrate Nitrite Nitrogen
84.00
pH
6.50
Phosphorus
23,000.00
Potassium
4,700.00
Sodium
0.17
Total Kjeldahl Nitrogen
58,600.00
c. Using the results listed in Item H. 5b. above, calculate the sodium adsorption ration (SAR): 0.005
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the
residuals: 30 %. This rate is a 0 default value or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or
provide technical justification as to why the selected default value is appropriate to be applied to these
residuals: Default value for aerobic digestion.
Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table:
Application Method
First Year
Fire -Year
PAN
Maaumum Adjusted
PAN
(mg/kg)
(mg/kg)
Surface
17,784
28,235
Injection/Incorporation
18,084
28,535
e. Are the residuals are a registered fertilizer with the NC Department of Agriculture and Consumer
Services: ❑ yes g no. If yes, provide date of registration approval: ,
the current registration number:
and the fertilizer equivalent: %, %, and %.
FORM: RSCA 10-06 Page 6 of 8 Attachment Order 2

6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the
residuals and list the results of the latest analyses:
7. Pathogen Reduction Determination: Specify which alternative(s) will be used to meet the pathogen
reduction requirements:
a. For Class A or Equivalent:
❑ A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids.
OR
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed):
❑ Alternative 1 [40 CFR §503.32 (a)(3)] - Time/Temperature Compliance.
❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment.
❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric Virus/Viable Hehninth Ova.
❑ Alternative 4 [40 CFR §503.32 (a)(6)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 5 [40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation.
❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process.
Explain:
b. For Class B or Equivalent:
® Alternative 1 [40 CFR §503.32 (b)(2)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [40 CFR §503.32 (b)(3)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process.
Explain:
❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
c. For Surface Disposal:
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item H. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II.7b. above.
❑ Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
FORM: RSCA 10-06 Page 7 of 8 Attachment Order 2

8. Vector Attraction Reduction Determination: Specify which alternative(s) will be used to meet the vector
attraction reduction requirements:
® Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization.
❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [40 CFR §503.33 (b)(9)] - Injection.
❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Alternatives for Animal Processing Residuals Only:
Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10.
❑ Not Applicable - Non -Animal Processing Residuals Regulated under 40 CFR Part 257 with NO Domestic
Wastewater Contribution.
3/15/2007 3:28 PM
I
o � du ,
:39
lin
FORM: RSCA 10-06 Page 8 of 8 Attachment Order 2

Facility vicinity map

Process flown diagram and map

WASTEWATER TREATMENT PLANT PROCESS
The City of Marion operates a 3.0 million gallon capacity aerobic wastewater treatment plant. After
grit collection, the influent is pumped to one of two 400,000 gallon primary clarifiers. Liquids are
pumped to a 780,000 gallon aeration basin and continues to one of two 400,000 gallon secondary
clarifiers. Return activated sludge (RAS) is sent back to the aeration basin. Solids are sent to one of
two 65,000 gallon sludge thickening tanks. After thickening, solids are sent to a 780,000 aerated
sludge holding lagoon. Decant from the secondary clarifiers are sent to tertiary sand filters and on
to a chlorine contact chamber, re -aerated and dechlorinated before discharge. Liquids generated
from the thickening are sent to the head of the plant. Total storage for the facility is 780,000
gallons. Once storage is approached, a land application event is performed.

City of Marion Wastewater Treatment Plant Solids Plow Path

City of Marion Wastewater Treatment Plant Effluent Flow Path
RM

Justification for residuals production rate

JUSTIFICATION FOR RESIDUALS PRODUCTION RATE
Over the past several years the dry ton production has been below 290 dry tons. A review of past
applications indicate that this is a reasonable dry ton value. I have seen no reason to think this
facility will exceed the dry tons stated.

Residuals sampling plan

SAMPLING PLAN
Prior to application, a multiple samples are collected from the sludge holding lagoon. These
samples as grabs are analyzed for fecal coliform. Grab fecal samples are collected over a two week
period prior to an application event. Multiple samples are collected, composited from the sludge
holding lagoon. These samples are submitted for analyses for: nutrient, metal, volatile solids and
TCLP. Inflow volatile solids samples are collected prior to entering the aeration basin. Exit
volatile solids samples are collected from the sludge holding lagoon. Volatile solids reduction is
calculated from these values.
Annually, a composite residual solid sample from each of these sources will be analyzed for:
Cadmium, Copper, Lead, Nickel, Zinc, Aluminum, Ammonia — Nitrogen, Calcium, Nitrate -Nitrite,
Nitrogen, Magnesium, % Total Solids, pH, Phosphorus, Potassium, T .N, and Sodium. From this
information, the Plant Available Nitrogen (PAN) will be calculated. Currently Marion collects a
TCLP analysis annually but, has requested that this be reduced to once every permit cycle. A full
TCLP inccludes:
Arsenic
Hexachlorobenzene
pH for Corrosivity
Barium
Hexachloro-1,3-Butadiene
Benzene
Hexachloroethane
Flash point for ignitability
Cadmium
Lead
Carbon Tetrachloride
Lindane
Sulfides and Cyanides for reactivity
Chlordane
Mercury
1,2-Dichloroethane
Chlorobenzene
Methoxychlor
1,1-Dichloroethylene
Chloroform
Methyl Ethyl Ketone
2,4-Dinitrotoluene
Chromium
Nitrobenzene
Endrin
m-Cresol
Pentachlorophenol
Heptachlor and its Hydroxide
o-Cresol
Pyridine
Trichloroethylene
p-Cresol
Selenium
2,4,5-Trichlorophenol
Cresol
Silver
2,4,6-Trichlorophenol
2,4-D
Tetrachloroethylene
2,4,5-TP (Silvex)
1,4-Dichlorobenzene
Toxaphene
Vinyl Chloride

LAND APPLICATION SITE CERTIFICATION ATTACHMENT

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
LAND APPLICATION SITE CERTIFICATION ATTACHMENT
(FORM: LASCA 10-06)
(THIS FORMMAYBE PHOTOCOPIED FOR USEASAN ORIGINAL)
The Division of Water Quality (Division) will not accept this attachment unless all the instructions are followed.
Failure to submit all required items will lead to additional processing and review time.
For more information, visit our web site at: hgp.Ilh2o.enr.state.nc.us/7aulmain.html
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application form (FORM:
NDRLAP 10-06).
✓ Any changes to this attachment form will result in the application package being returned.
✓ For new residuals land application programs or renewed residuals land application programs, submit the requested
information for all land application sites to be certified for this residuals land application program.
✓ For modified residuals land application programs in which any new/transferred land application sites or modification to the
certified land application sites are proposed, submit the requested information for only those land application sites that are
new/transferred or affected by the proposed modification.
B. Land Application Site Information:
✓ Additional copies of Page 2 of 2 of this attachment form may be used if necessary.
✓ The status of the land application site with respect to this residuals land application program must be provided in the table in
Item I. 1. The status categories and their corresponding codes are as follows:
♦ New (N) ♦ Renewed (R) ♦ Modified (M) ♦ Transferred (T)
✓ If this is the first time that an application package is being submitted using Form NDRLAP, then a Watershed Classification
Attachment (FORM: WSCA 10-06) must be completed for all existing land application sites.
✓ For each land application site with a status code of N attach the following in the order specified:
♦ Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA 10-06).
➢ Attachment Order 3-a: Watershed Classification Attachment (FORM: WSCA 10-06).
➢ Attachment Order 3-b: County Manager Notification Attachment (FORM: CMNA 09-06).
➢ By Land Application Site:
■ Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA 09-06).
■ Attachment Order 3-d: Setback Waiver Agreement Attachment (FORM: SWAA 10-06).
■ Attachment Order 3-e: An updated vicinity/buffer map that meets all of the criteria in the latest version of the
document entitled "Guidance for the Preparation of Vicinity/Buffer Maps for North Carolina Residuals
Permitting Programs."
■ Attachment Order 3-f. A soils and agronomic evaluation that meets all of the criteria in the latest version of
the document entitled "Guidance for the Preparation of Soils and Agronomic Evaluations for North Carolina
Residuals Permitting Programs."
✓ For each land application site with a status code of Pil attach the following in the order specified:
♦ Attachment Order 3: Land Application Site Certification Attachment (FORM: LASCA 10-06).
➢ By Land Application Site:
■ Attachment Order 3-c: Landowner Agreement Attachment (FORM: LOAA 09-06).
■ Attachment Order 3-d: Buffer Waiver Agreement Attachment (FORM: SWAA 10-06).
■ Attachment Order 3-e: An updated vicinity/buffer map (i.e., see above for criteria guidance).
■ Attachment Order 3-g: An updated accounting of the land application site's cumulative pollutant loading rates
(CPLRs) that are required by the permit of the residuals land application program from which the site is being
transferred.
✓ For each land application site with a status code of M, contact the appropriate Division's regional office to determine
attachment requirements.
✓ For each land application site with a status code of T attach the following in the order specified:
♦ Attachment Order 3 through 3-f Everything required for land application sites with a status code of N.
➢ Attachment Order 3-g: An updated accounting of the CPLRs (i.e., see above for criteria guidance).
FORM: LASCA 10-06 Page 1 of 2 Attachment Order 3

Applicant's name: City of Marion
Check all that apply: ❑ NEW RESIDUALS LAND APPLICATION PROGRAM ® RENEW RESIDUALS LAND APPLICATION PROGRAM
❑ ADD ® DELETE this/these land application site(s) to/from those certified for this residuals land application program.
® INCREASE ❑ DECREASE the net acreage associated with this/these land application site(s) currently certified for this
residuals land application program.
❑ OTHER Explain:
Land application sites currently certified: 344.8 net acres and Total to be certified: 131.7 net acres.
I. LAND APPLICATION SITE INFORMATION (See Instruction B.):
1. Complete the following table with the requested information:
Status
Codea
Site/Field ID
Landowner(s)
Leasee(s) or Operators
County
Net Acres
Predominant
Soil Series
Soil
CEC
D
C-01
Curtis Causby
Curtis Causby
McDowell
9.5
D
Q-01
Frank Queen
Frank Queen
Burke
22
D
Q-02
Frank Queen
Frank Queen
Burke
18
D
Q-10
Frank Queen
Frank Queen
McDowell
9.8
-7
D
Q-13A
Frank Queen
Frank Queen
McDowell
28
D
Q-13B
Frank Queen
Frank Queen
McDowell
13.7
D
Q-15
Frank Queen
Frank Queen
McDowell
32.3
D
Q-16
Frank Queen
Frank Queen
McDowell
41.8
D
Q-20
Frank Queen
Frank Queen
McDowell
18.7
D
Q-21
Frank Queen
Frank Queen
McDowell
17.6
D
Q-23
Frank Queen
Frank Queen
McDowell
13.4
D
Y-01
Voua Yang
Voua Yang
McDowell
12
FORM: LASCA 09-06 Page 2 of 3 Attachment Order 3

I. LANK APPLICATION SITE INFORMATION (See Instruction B.):
2. Complete the following table with the requested information: (continued from previous page)
Status
Codea
Site/Field ID
Landowner(s)
Leasee(s) or Operators
County
Net Acres
Predominant
Soil Series
Soil
CEC
R
K-01
Anna Sindoni Deebold
Mario DeLuca
McDowell
16
Hayesville
11.8
R
K-02
Anna Sindoni Deebold
Mario DeLuca
McDowell
3% 35.8
Hayesville
13.4
R
F-1
James C. Fisher
James C. Fisher
McDowell
13.7
Braddock Var
8.4
R
F-2
James C. Fisher
James C. Fisher
McDowell
4.3
Braddock Var
6.3
M
F-3
James C. Fisher
James C. Fisher
McDowell
11.4 /, .; A
Hayesville
7.8
R
F-4
James C. Fisher
James C. Fisher
McDowell
8.2
Hayesville
8.4
M
R-01
Nancy Hice Ross
Nancy Hice Ross
McDowell
19.4 .,/
Hayesville
8.7
R
R-02
Nancy Hice Ross
Nancy Hice Ross
McDowell
o;- 22.9
Hayesville
12.6
� pis
3.q
'Status Code for land application sites are: ♦ N (New) ♦ R (Renew) ♦ M (Modified) ♦ T (Transferred)
*** END OF FORM LASCA 09-06 ***
FORM: LASCA 09-06 Page 3 of 3 Attachment Order 3

County Manager Notification Attachment

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
COUNTY MANAGER NOTIFICATION ATTACHMENT
(THIS FORMMAYBE PHOTOCOPIED FOR USE ASANORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to submit all of the required items will lead
to additional application processing and review time.
For more information or for an electronic version of this form, visit our web site at:
http://`h2o.enr.state.nc.uslaulapplications.html
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without a corresponding residuals program application
form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each county in which the land application sites for which the
applicant is seeking certification are located.
C. Mail the attachment form to the .appropriate county manager by certified mail with a return receipt
requested.
✓ The most current publication of the Directory of State and County Officials may be downloaded from the web
site at: http://www.secretary.state.nc.us/pubsweb/direct.asp.
✓ A list of the Division's regional offices, their county coverage, and their contact information may be
downloaded from the web site at: http://www.enr.state.nc.us/htmVregionaloffices.html
D. Attach an 8.5-inch by 11-inch copy of the return receipt to the back of this attachment form prior to
submission of the application to the Division for review.
To: County where land application sites are located:
Name and complete address of county manager:
60 East Court Street
City:
Marion
McDowell
Mr. Charles R Abernathy
State: NC
Zip: 28752
This is to notify you that the applicant listed in Item I(1) of this attachment form will be submitting an
application for the land application of residual solids to land in your county to the Division for review.
During this review, the Division will ensure that all federal and state regulations are enforced. Maps of the
land application sites included in this application will be available at the following location no later than the
listed expected application date:
Name and complete address of appropriate regional office: NCDENR-DWQ Asheville Regional Office
2096 US Highway 70
City:
Swannanoa
State: NC Zip: 28778
Telephone number. ( 828 ) 2964500 Facsimile number: ( 828 ) 299-7043
Expected date of application submission: April 1, 2007
Actual date of application submission (to be completed by DWQ):
Deadline for county manager response (to be completed by DWQ):
Should you desire to comment on this application as it related to your interests, please do so no later than
30 calendar days following the expected application submission date. If you have any questions or comments
about this notification or if you would like more information, please contact the Aquifer Protection
Supervisor of the appropriate regional office at the telephone number provided above. Thank you in advance
for your attention to this matter.
FORM: CMNA 09-06 Page 1 of 2 Attachment Order 3-b

I. GENERAL INFORMATION:
1. Applicant's name: City of Marion
2. Signing official's name and title: Mr. J. Robert Boyette
3. Complete mailing address of applicant: Post Office Drawer 700
0
City: Marion State: NC Zip: 28752
Telephone number: ( 828 ) 652-3551 Facsimile number: ( 828 ) 652-1983
E-mail address: [e-mail]
Name and complete mailing address of contact person and consulting firm who prepared application:
Bob Branch — Branch Residuals & Soils, LLC — 311 B South Westgate Drive
City: Greensboro State: NC Zip: 27407
Telephone number: ( 336 ) 510-0340 Facsimile number. ( 336 ) 510-0341
E-mail address: [e-mail]
IL PERMIT INFORMATION:
1. Application is for (check all that apply): ❑ new, ® modified, and/or ® renewed permit.
2. If this application is being submitted to renew or modify an existing permit, provide:
the permit number WQ0019960 ,
the most recent issuance date April 24, 2002 and the expiration date June 30, 2006
Date of most -recently certified Attachment A: April 24, 2002
Date of most -recently certified Attachment B: July 12, 2005
III. RESIDUALS LAND APPLICATION PROGRAM INFORMATION
1. County(ies) where residuals source -generating facilities are located: McDowell
2. Purpose of the residual source -generating facilities (check all that apply):
® treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
❑ treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial mixed with domestic wastewater, and/or
(approximate percentages: % industrial and % domestic)
❑ other (explain:
3. Are land application sites currently certified for this residuals land application program in this county:
® yes ❑ no. If yes, provide the total number of acres (i.e., excluding buffers that are certified
304.8 acres (approximate percentages: 0 % forested, 100 % agricultural, and 0
% reclamation sites). Addition of acres to currently permitted sites.
4. This application, if approved by the Division, will certify 10 additional acres (i.e., excluding buffers)
in this county for this residuals land application program (approximate percentages:
100 % agricultural, and 0 % reclamation sites).
*** END OF FORM CMNA 09-06 ***
0 % forested,
FORM: CMNA 09-06 Page 2 of 2 Attachment Order 3-b

BRANCH RESIDUALS & SOILS, LLC
311 B South Westgate Drive • Greensboro, NC 27407
PHONE [phone] • FAx [phone]
March 21, 2007
Mr. Charles R. Abernathy
60 East Court Street
Marion, NC 28752
REFERENCE: County Manager Notification Form for City of Marion
Dear Mr. Abernathy,
Please find attached the County Manager Notification Attachment for the City of Marion Land
Application Permit. Additional land is proposed to existing sites that are permitted in McDowell
County in the Dysartsville area. This notification is required by the North Carolina Department
of Environment and Natural Resources — Division of Water Quality and will allow the continued
operation of this permit. I am under contract with the City of Marion modify this permit.
If you have any questions regarding this please call Robert Boyette with the City of Marion at
[phone] or myself at [phone].
Sincerely,
Robert T. Branch, L.L.S
Project Manager/ Soil Scientist

Ur o uLLUMUL 01UPIMIg. JluputCui JWCUIpt
Page 1 of 1
Shipment Receipt
Transaction Date 21 Mar 2007
Address Information
Ship To:
MCDOWELL COUNTY MANAGER
CHARLES ABERNATHY
8286527121
60 EAST COURT STREET
MARION NC 28752-404i
Shipment Information
Service:
(Keep this for your records.)
Shipper:
BRANCH RESIDUALS & SOILS
BOB BRANCH
3365100340
311 B SOUTH WESTGATE DR.
GREENSBORO NC 27407
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3365100340
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GREENSBORO NC 27407
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John Fisher Farm

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
LANDOWNER AGREEMENT ATTACHMENT
(THIS FORMMAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to follow the instructions or to submit all of the
required items will lead to additional processing and review time for the application.
For more information orfor an electronic version of this form, visit our web site at. htip://h2o.enr state.nc.us/ndpu/
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being retumed.
B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner
and operated by a lesseeloperator (i.e., if applicable) other than the applicant.
✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and
the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS
TO PRIVATELY -OWNED LAND APPLICATION SITES
The undersigned landowner or his representative hereby permits:
Applicant's name: Mr. J. Robert Boyette, City Manager
Complete mailing address of applicant: City of Marion
P. O. Drawer 700
City: Marion State: NC Zip: 28752
Telephone number. [phone] Facsimile Number: [phone]
E-mail address: [e-mail]
hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -
generating facility(ies) onto the following land application site(s) (i.e., see attached buffer maps) in
accordance with the stipulations and restrictions as given in this AarE.amant•
Site/Field ID
Land Use or Cropping
Patterns
Intended Use or Disposition o�
Crops
Residuals Source -Generating
Facilities
See
Row Crops
Animal Feed
Marion WWTP
Attached
Hay/Pasture
The landowner or lus representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land application site(s) described above
for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for
the residuals land application program and shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.
FORM: LOAA 02/02 Pagel of 3 Attachment Order 3-c

L STIPULATIONS:
1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement.
The land application of any additional residuals or waste, other than that generated by the residuals source -generating
facilities specified by the Division's residuals land application program permit, is prohibited.
2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply
with all provisions of this Agreement.
3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third
party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions
of this Agreement.
4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the
subject matter of this Agreement.
S. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18
months from the date of the most recent residuals land application event.
6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge
Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application
site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a notice shall be
given by the current landowner to the new landowner that gives full details of the residuals applied or incorporated at the
land application site(s).
8. The Permittee has provided the landowner or his representative with information and data concerning the residuals land
application program, including an analysis of constituents of the residuals, residuals application methods, schedules for
typical cropping patterns, and a description of the equipment used by the Permittee.
9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program
permit that has been most -recently issued by the Division prior to commencement of any residuals land application event.
This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws and
regulations.
10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The
only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided that
a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least 6.0.
11. The Permittee will famish the landowner or his representative with a copy of the results of each soil analysis.
12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and the
Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil samples.
13. The landowner or his representative will furnish the Permittee with information regarding the amount and analysis of
other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application
site(s).
14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and
cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this
Agreement and schedule residuals land application events at appropriate periods.
15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee
and/or the landowner or his representative prior to and during a residuals land application event.
16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access
to the land application site(s) during active use and for the 12-month period following a residuals land application event.
Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s).
17. Animals shall not be grazed on the land application site(s) for a 30-dav period following a residuals land application
event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during
these periods after such residuals land application events.
18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals land
application program permit.
19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their
representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and to
established monitoring facilities on or near the land application site(s) as required by the residuals land application
program permit.
20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and
inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose
of determining compliance with the Division's residuals land application program permit; may inspect or copy any
records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater, surface
water, or leachate.
21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives to
take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination of,
this Agreement.

II. RESTRICTIONS:
Landowner's Certification:
® I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to
make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I
am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the
use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land
application site(s) are not included in any waste disposal contract or agreement with another municipality,
contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the
stipulations and restrictions, and do hereby grant permission to the Permittee to land apply residuals to the land
application site(s) as specified herein.
c
Landowner name: I --� o 6 C-. o-
Signature: ��, /V�.-=� Date: I n � b
NORTH CAROL A, ClafCOUNTY
I, the undersigned Notary Public do hereby certify that �es rS
personally appeared before me this day and acknowledged the due execution of the forgoing instrument.
WITNTSS my hand and official seal this the
' day of
Signature aril seal:
_My,conirnission expires:
Les e's/Operator's Certification:
I certify that I have read this A
specified herein.
Lessee/operator name: To
Signature:
Permittee's
4 ' 20 0 0
I
do hereby agree to abide by the stipulations and restrictions as
's
Date: glolo�
® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Signing offickal name: Mr. J. Robert Boyette, City Manager
Signature: Date:
** OF FORM LOAA 02/02 ***

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
BUFFER WAIVER AGREEMENT ATTACHMENT
(THISFORMMAYBEPHOTOCOPIED FOR USEASANORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to follow the instructions or to submit all of the
required items will lead to additional processing and review time for the application.
For more information or for an electronic version of thisform, visit our web site at: http.11h2o.enr.state.nc.us/ndpu/
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each property from which a waiver from 15A NCAC 2H .0219
(j)(5)(A)(ii) or (iii) is being sought.
✓ Any other buffers required by 15A NCAC 2H .0219 6)(5), other than those referenced above, cannot be
waived through execution of this attachment form.
✓ A copy of the completed and appropriately executed attachment form must be provided to the property owner.
AGREEMENT TO WAIVE THE BUFFER REQUIRED BY 15A NCAC 2H .0219 (j)(5)(A)(ii) and (iii)
The undersigned property owner hereby permits:
Applicant's name: City of Marion
Complete mailing address of applicant: P. O. Drawer 700
City: Marion
NC
Zip
28752
Telephone number: ( 828 ) 652-3551 Facsimile number: ( 828 ) 652-1983
E-mail address: bboyette(awnclink.com
hereinafter referred to as the Permittee, to land apply residuals within 100 feet (i.e., cannot be less
than 100 feet) of the residence or place of public assembly located at the following:
Location address of property: 3 c, 7 & ,
City: State: %%1 C, Zip: 2
This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for
the residuals land application program and shall be renewed each time this permit is renewed. In addition,
this Agreement shall only remain in effect for as long as the undersigned property owner owns the property
described herein.
The undersigned property owner agrees to abide by this Agreement until such time as written notification,
given 30 calendar days in advance, modifies or cancels this Agreement.
® I certify that I am a deeded property owner of above -referenced property and am authorized to make decisions
regarding this property on behalf of other deeded property owners Furthermore, I certify that I have read and
understand this Agreement and do hereby grant permission to the Permittee to land apply residuals to land
application site(s) as specifieltherein.
Property c
Signature:
s
L :. _
*** END OF FORM BWAA 02/02***
Date:
—as ( -" 71; :,�_ e_,—
FORM: BWAA 02/02 Page 1 of 1 Attachment Order 3-d

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SCALE: 1rr = 2 miles City of Marion Site
CHECKED BY: Land Application Program Vicinity
DRAWN BY: RTB BRANCH John Fisher Farm Map
REsmuALs
DATE: Dec-04 & SOI LS, LLC moil:« No. 2004-41

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SCALE: V 2000 City of Marion Soil
CHECKED BY: Land Application Program Survey
DRAWN BY: RTB BRANCH John Fisher Farm Map
RESIDUALS
DATE: Dec-04 & SOILS, LLC Project No. 200441

JOHN FISHER FARM
TRACT F
SOILS AND AGRONOMY REPORT
Field 3 has been modified to add 1.8 acres to this field. This field has been buffered to
exclude areas of slope, property lines, houses, creeks, drainage, wells, and roads.
Field investigations performed by a BR&S soil scientist concurred for the most part with the
mapping published in the McDowell County Soil Survey. The added area to the east of Field
3, has soils consistent with the majority of Field 3 which is the Hayesville soil series. A
detailed soil profile description from the investigation has been attached.
Soil samples from North Carolina Department of Agriculture NCDA are attached. These
fields should receive nitrogen applications in accordance with the predominant soil series
indicated and the corresponding realistic yield estimation (RYE) as available from
http://www.soil.ncsu.edu/mn /ncnmwgZyields/.
t%Ss'"NOMI

I
SOIL EVALUATION FORM
I
I
I
J,
I
I
I
BRANCH RESIDUALS & SOILS, LLC
311 B South Westgate Drive - Greensboro, NC 27407
PHONE [phone] — FAX [phone]
Project Name City of Marion
Owner John Fisher
Operator John Fisher
Slope 4-10 Sample No. 3
Project Number
Tract/Site
Field
Crop
2004-41
Added to Field 3
Fescue
'D
Wil
!!r
......
Ap
0-5
Lt. CL
5 YR 4/4
wk med gr
fr
n/a
Btl
5-21
CL
2.5 YR 4/8
mo med sbk
fr
n/a
Bt2
21-32
C
2.5 YR 5/8
mo med sbk
fr
n/a
BC
32-40+
CL
2.5 YR 5/8
wk med sbk
fr
7.5 YR 5/6
some miceous saprolite
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in. >40+
Depth to Restrictive Horizon (in.) n/a Type of Restrictive Horizon n/a
Boring needed prior to application: no Attached map with boring location no
Most Closely Related Soil Series Hayesville
Discussion of Site
Good year round site

- ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A"
IN A BLANK OR BOX WHEN NOT APPLICABLE.
?acility Name:
City of Marion
Permit #: WQ0019960 Annual Dry Tons Applied: 30.184128
1wner:
James Fisher Operator:
James Fisher Cation Exchange Capacity (non 503):
to #: F-01 Field #: F-01
Acres Utilized: 13.7 Acres Permitted:
13.7
#
l
S ci
per
Acre
o
/o
Solids
Dry Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
WA'st
Inches
Precip.
past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
all-
zation
Rate
TICT�1
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p 2
Gal.Totals
Cu.Yd.
Report
- Totals
Gal
Crop 1
Crop 2
m
of
2006
208,000
15182
3.48
2.203221022
WWTP
dry
0
s
0.5
30%
48300
3700
1
67.1145
#######
Fescue
0
0
0
0
0
0
0
0
0
0
1
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
OTALS:
15182
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
muallbs/acre
0.0083714
0.00881
0.18946
2.18097
0.25555
0.01718
0.10574
0.13659
0.0163
4.97878
121.606
67.11451
0
Date
lbs/ac
urrent Cumulative lbs/ac
0.0083714
0.00881
0.18946
2.18097
0.25555
0.01718
0.10574
0.13659
0.0163
4.97878
zor Years Cumulative lbs/ac
0
1 0
0 1
0
0
0
0
0
0
0
;rmitted C. P. L. R.***
36
34
NA
1338
267
15
1 NA
374
89
2498
`
;unit PAN Limit l st/2nd Crop
250
certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
,signed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
gnificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
t 2-," Z - 2-07 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of fiand Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
'acility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 6.602778
caner: James Fisher Operator: James Fisher Cation Exchange Capacity (non 503):
to #: F-02 Field #: F-02 Acres Utilized: 4.3 Acres Permitted: 4.3
o
S ec'
Totals
Per
Acre
o
/o
Solids
Dry
D Tons Per
Acre
Residual
Sources
(Summarize)
Site
Cond.
Dry,
Wet,
Moist
Inches
Preci p
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
•
cu.Yd.
Report
'>_ Totals
in Gal.
Crop 1
Crop 2
2006
45,500
10581
3.48
1.535529767
WWTP
dry
0
s
0.5
30%
48300
3700
1
46.7753
#######
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
3TALS:
10581
<>
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
mual lbs/acre
0.005833
0.00614
0.13201
1.51965
0.17806
0.01197
0.07368
0.09517
0.011361
3.4691
84.732
146.7753
0
Date
lbs/ac
><
irrent Cumulative lbs/ac
0.005 33 5 8 0.00614 0.13201 1.5196 0.17806 0.01197 0.07 368 0.09517 0.0 3 3 4
11 6 691 >'
0 0 0 0 0 0 1 0 0 0 0
36 34 NA 1 1338 267 15 NA 1 374 89 2498
::. 250
for Years Cumulative lbs/ac
.rmitted C. P. L. R.***
rmit PAN Limit l st/2nd Crop
certity, under penalty of law, that tins document was prepared under my direction or supervision in accordance with a system
.signed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
;nificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of LanZI Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
** The RSSF Data and the Dry Tons per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

Grower: Fisher, John
... 113 Linville St
Morganton, NC 28655
oil Te., Report
Farm:
i2/5/2006 SERVING N.C. RESIDENTS FOR OVER 60 YEARS McDowell County
Agronomist Comments
The heavy metal report is found on a separate page. Using Mehlich 3 as a soil test extractant, background levels of
these metals typically seen In NC soils when analyzed are as follows: arsenic (As)- 5.0 ppm, cadmium (Cd)- 0.2
ppm, chromium (Cr)- 0.3 ppm, lead (Pb)- 4.0 ppm, nickel (Ni)- 0.7 ppm, & selenium (Se)- 0.2 ppm
(FY2003-2005). Although the above metals here are not believed to pose a concern for plant growth, continue to
monitor these and note where elevated above background levels:
Copies To: Branch. Residuals & Soils
C - 12
Sample No.
Last Crop
Mo
Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B
Mn
See Note
F-1
1st Crop: Fes/OG/1'im,M
0
120-200
60-80
10-30
0
0
0
0
.0
0
12
2nd Crop: Fes/OG/fim;M
0
120-200
60-80
10-30
0
0
0
0
•0
0
12
Test Results
Soil Class
HM'0 W/V
CBC
BS•rb
Ae pH P-I K-1
Ca% Mgr6
Mn-1
Mn-AI(1) Mn-AI(2) Zn-1
Zn-Al
Cu-I
S-I
SS -I
NO3-N NH4-N
Na
MIN
0.56 0 97
9.2
89.0
1.0 6.3 30 68
55.0 30.0
323
206
206 114
114
127
48
0.1
Irleld In%rmation W
elpplied Lime....
Recorawendation a
Sample No.
Last Crop
Mo
Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B'
Mn
See Note
F-2
1st Crop: Fes/OG/Tim,M
0
120-200
30-50
60-80
0
0
0
0
.0
pH$
12
2nd Crop: Fes/OG/fim,M
0
120-200
30-50
60-80
0.
0
0
0
•0
pH$
12
Test Results
Soil Class
HM% W/V
1.11
CEC
BS%
Ac pH P-1 K 1
Ca% Mr,b
Mn-I
Mn-AI(1) Mn-AI(2) Zn-1
Zn-AI
Cu-1
S-I
SS -I
NO3-N NH4-N
N_ a
MIN
0.56
8.9
910
0.8 6.7 41 36
56.0 33.0
282
176
176 98
98
185
42
0.1
Field In%rmatiun
j Apg)lied Lime
,Recommendations
Sample No.
Last Crop
Mo
Yr T/A
Crop or Year
Lime
N
P205
K20
M
g
S
Cu
Zn
B
Mn
See Note
3
1st Crop. Fes/OG/I'Im,M
0
120-200
0
40-60
0
0
0
0
.0
pH$
12
2nd Crop: Fes/OG/Pim,M
0
120-200
0
40-60
0
0
0
0
•0
pH$
12
Test Results
Soil Class
HAP16 W/V
CBC
BS%
Ae pH P-I K.I
Ca% Mg',S
Mn-1
Mn-AI(1) Mn-AI(2) Zn-I
Zn AI
Cu-I
S-I
SS -I
NO3-N AWN
Na
MIN
0.66 1.07
10.8
93.0
0.8 6.7 96 42
58.0 - 33.0
235
147
147 182
182
219
45
0.1

Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime N
P205 K20 Mg S
Cis Zn B
Mn
See Note
F-4
1st Crop: Fes/OG/rim,M
0 120-200
20-40 30-50 0 0
0 0 .0
pH$
12
2nd Crop: Fes/OG/rfm,M
0 120-200
20-40 30-50 0 0
0 0 .0
pH$
12
Test Results
Soil Class HM% W/V
CEC BS•.6 Ac pH P-I K-I
Ca% Mg% Mn-I
Mn-AI(1) Mn-AI(2) Zn-1 Zn-AI
Cu-I S-I
SS -I
NO3-N NH4-N Na
MIN 0.86 1.07
9.6 90.0 1.0 6.5 49 54
55.0 32.0 420
261 261 107 107
158 42
0.1

Heavy Metal Soil Test Re on fisher, John Report #: 03375
113 Linville St
MEHLICH-3 EXTRAC'TION
McDowell County
Questians oancernine these analvses should be referred to the Agronomic Division, Soil Testing
Sample Cadmium
Arw*ef Lead Selenium Ckyomium Arsenic Aluminum
num iron
--------- --------- —------ ----------- -------------------rnq/cirr�3 f�D 1----------------------------------------------------on
1<-1
F-2
0.10
0.40
1.60
0.00
0.20
F-4
0.10
0.40
1.00
0.00
0.20
F-3
0.10
0.50
0.00
0.00
0.20
{1.10
0.50
0.00
0.00
0.20
2.90
761.30
195.40
320
886.70
165.40
4.30
1,307.00
104.70
3.80
1,101.00
133.70

Report Number:
R06263-0069 A&L EASTERN LABORATORIES, INC.
Acount Number: 7621 Whitepine Road ® Richmond, Virginia 23237 • [phone]
46368 Fax No. [phone] ° Email: [e-mail]
TO: BRANCH RESIDUALS & SOILS LLC RE: JOHN FISHER 2006-51 BOB BRANCH
311 B S WESTGATE DR
GREENSBORO, NC 27407
ATTN: BOB BRANCH
Date Received: 9/19/06 Date Reported: 09/22/2006
NC CERT #257
REPORT OF ANALYSIS
18060 F-1 Mercury - Mehlich-3 < 0.2 mg/kg SW 846-7471A
Molybdenum (Mo)- Mehlich 3 0.4 ppm NCR-13 No. 221, 1998
Page: 1
18061 F-2 Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
Molybdenum (Mo)- Mehlich-3
0.3
ppm
_NCR-13 No. 221, 1998
18062 F-3 Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
Molybdenum (Mo)- Mehlich-3
0.3
ppm
NCR13 No. 221, 1998
18063 F-4 Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
Molybdenum (Mo)- Mehlich-3
0.3
ppm
NCR-13 No. 221, 1998
ALE- ISC
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part nor may any reference be made ,)ajd
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Paul Chu, Ph.D.

Mario DeLuca Farm

State of North Carolina
Department of Environment and Natural Resources
IDivision of Water Quality
LANDOWNER AGREEMENT ATTACHMENT
(THIS FORM AM Y BE PHOTOCOPIED FOR USE ASAN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete unless
' all the instructions are followed. Failure to follow the instructions or to submit all of the required
items will lead to additionalprocessing and review time for the application.
' For more information or for an electronic version of thisform, visit our web site at:
h ttp: //h2o. enr. state. nc. us/ndpu/
INSTRUCTIONS TO THE APPLICANT:
' A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (Form,NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner
and operated by a lessee/operator (Le., if applicable) other than the applicant.
✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and
the lessee/operator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS
TO PRIVATELY -OWNED LAND APPLICATION SITES
The undersigned landowner or his representative hereby permits:
Applicant's name: City of Marion
Complete mailing address of applicant: PO Box 700
City: Marion State: NC Zip: 28752
Telephone number: ( 828 ) 652-8843 Facsimile number: ( 828 ) 659-1943
E-mail address:
hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -
generating facility(ies) onto the following land application site(s) (Le., see attached buffer maps) in
accordance with the stipulations and restrictions as given in this Agreement:
Site/Field ID
Land Use or
Cropping Patterns
Intended Use or
Disposition of Crops
Residuals Source -Generating
Facilities
Kl
Fescue
Hay
Marion WWTP
K2
Fescue
Hay
Marion WWTP
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land application site(s) described
above for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit
for the residuals land application program and shall be renewed each time this permit is renewed.
FORM: LOAA 02/02 Page 1 of 3 Attachment Order 3-c

The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days in advance,
modifies or cancels this Agreement.
L STIPIILATIONS:
1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement.
The land application of any additional residuals or waste, other than that generated by the residuals source -generating
facilities specified by the Division's residuals land application program permit, is prohibited.
2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply
with all provisions of this Agreement.
3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third
party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and
conditions of this Agreement.
4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference. to the
subject matter of this Agreement.
5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18
months from the date of the most recent residuals land application event.
6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR DWQ, Non -Discharge
Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land
application site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a
notice shall be given by the current landowner to the new landowner that gives full details of the residuals applied or
incorporated at the land application site(s).
8. The Permittee has provided the landowner or his representative with information and data conceming the residuals land
application program, including an analysis of constituents of the residuals, residuals application methods, schedules for
typical cropping patterns, and a description of the equipment used by the Permittee.
9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program
permit that has been most -recently issued by the Division prior to commencement of any residuals land application
event. This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws
and regulations.
10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The
only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided
that a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least
6.0.
11. The Permittee will finish the landowner or his representative with a copy of the results of each soil analysis.
12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and
the Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil
samples.
13. The landowner or his representative will finish the Permittee with information regarding the amount and analysis of
other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application
site(s).
14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and
cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this
Agreement and schedule residuals land application events at appropriate periods.
15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the
Permittee and/or the landowneror his representative prior to and during a residuals land application event.
16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public
access to the land application site(s) during active use and for the 12month period following a residuals land
application event. Such controls may include the posting of signs that indicate the activities being conducted at the land
application site(s).
17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application
event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access
during these periods after such residuals land application events.
18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals
land application program permit.
19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their
representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and
to established monitoring facilities on or near the land application site(s) as required by the residuals land application
program permit.
FORM: LOAA 02/02 Page 2 of.3 Attachment Order 3-c

20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter
and inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the
purpose of determining compliance with the Division's residuals land application program permit; may inspect or copy
any records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater,
surface water, or leachate.
21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives
to take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination
of, this Agreement.
FORM: LOAA 02/02 Page 3 of 3 Attachment Order 3-c

K RESTRICTIONS:
;Icerdo ner's Certification:
tify
that I am a deeded landowner of the above -referenced land application site(s) and am authorized to
make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that
I am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding
the use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced
land application site(s) are not included in any waste disposal contract or agreement with another
municipality, contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement,
understand the stipulations and restrictions, and do hereby grant permission to the Permittee to land apply
residuals to the land application site(s) as specified herein.
Landowner
Signature:
NORTH CAROLINA, /'YIC=D01JE LA- COUNTY
I, the undersigned Notary Public do hereby certify that , /} Ito A010 C /3
personally appeared before me this day and acknowledged the due execution of the forgoing ;instrument:._
WITNESS my hand and official seal this the
day of . tQ 2006 ?
Signature and seal: / LeA
'7 My commission expires: hoU0 �r
Lessee's/Operator's Certification:
❑ I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions 'as
specified herein.
Lesseetoperator rime: nj Oak / o V
Signature:
Date:
Perini" eels Certification:
certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Signing offi ' e: r
Signature: Date:
FORM: LOAA 02/02 Page 4 of 3 Attachment Order 3-c

State of North Carolina �F
Department of Environment and Natural Resources
Division of Water Quality
BUFFER WAIVER AGREEMENT ATTACHMENT
(THIS FORMMAYBE PHOTOCOPIED FOR USEASAN ORIGINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete unless
all the instructions are followed. Failure to follow the instructions or to submit all of the required
items will lead to additional processing and review time for the application.
For more information or for an electronic version of this form, visit our web site at.•
http: //h2o. enr. state. nc. usln dpu/
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each property from which a waiver from 15A NCAC 211.0219
(j)(5)(A)(ii) or (iii) is being sought.
✓ Any other buffers required by 15A NCAC 211 .0219 6)(5), other than those referenced above, cannot be
waived through execution of this attachment form.
✓ A copy of the completed and appropriately executed attachment form must be provided to the property
owner.
AGREEMENT TO WAIVE THE BUFFER REQUIRED BY 15A NCAC 211.0219 (j)(5)(A)(ii) and (iii)
The undersigned property owner hereby permits:
Applicant's name: C 1 % tj VP )T A ICI O JJ
Complete mailing address of applicant: {� �% Z+ x -7 O O
City: f)9A9l 0-Ai
State:
0 G zip:
-aP 7 5—
Telephone number: (F,),5P )
&,:� S W Zl -3
Facsimile number: ( 8a
29) (3
E-mail address:
hereinafter referred to as the Permittee, to land apply residuals within J60 feet (Le., cannot be less
than 100 feet) of the residence or place of public assembly located at thefollowing:
Location address of property: 1,2
9 �i �RCC
City: 60 /AF,812' State: zip: 02 27(o I
This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit
for the residuals land application program and shall be renewed each time this permit is renewed. In
addition, this Agreement shall only remain in effect for as long as the undersigned property owner owns the.
property described herein.
The undersigned property owner agrees to abide by this Agreement until such time as written notification,
giiven30 calendar days in advance, modifies or cancels this Agreement.
El n3I certify that I am a deeded property owner of above -referenced property and am authorized to make decisions
regarding this property on behalf of other deeded property owners Furthermore, I certify that I have read and
understand this Agreement and do hereby grant permission to the Permittee to land apply residuals to land
application site(s) as specified herein- „ n A --\ 0
Property owner name:
FORM: BWAA 02/02 Page 1 of 1 Attachment Order 3-d

Signature: 1.4x . v, c c
*** END OF FORM LOAA 02/02 ***
i
FORM: LOAA 02/02 Page 2 of 3 Attachment Order 3-c

N
n.
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d u74A (. (te to F unuaa ao T a0 MOfE (S� Pp {� 1 6
SCALE: V = 2.4 miles City of Marion Site
CHECKED BY: Land. Application Program Vicinity
DRAWN BY: RTB BRANCH Mario DeLuca Farm Map
RESIDUAI.,S
DATE: Feb-07 I & SOILS, LLC Projea No. 2006-51

N
EwG d '
�oLil%1 GoA 0 BrC2 N
loq HCC2 IoX
� Y
y a a r HeD r
s' 226 HCC2; 1769 _ a
� HcC2 t' DysartvrlleBrC2 loA ` '.� � Y�
`_ HcC2 BrC2 x
t"-
i 10 1
C2
r BIC2 w HcC2 1777 HCC2
H612 s IoA HCC2 a c) r
a Ss
BrB 2
-HeD
v s r HeDfe
7 n
1773
A Apb "
a s s Q HcC2 HeD 1cC2
x o
iR,
Hccz 4 , = Feld K 1 '�eD 3 F
1777
� e
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a ECF
i Field K 2 P ~x EwE
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a� 00
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}
SCALE: 1 ^ = 2000' City of Marion Soil
CHECKED BY: Land Application Program Survey
DRAWN BY: RTB BRANCH Mario DeLuca Farm Map
RESIDUALS
DATE: Feb-07 & SOILS, LLC Project No. 2006-51

r=== m m m� s_ m
■ Dwelling
A
Structure (Barn)
Pond
Well
Buffer Area
W
Wet Area
Legend
AMA
Wooded Area
- • - -►
Drainageway
=
Access Road
— — —
Property Line
x-x-x
Fence
®
Hand Auger B

M M' M m m m M - lllllllll>e -_ __
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE
MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name:
City of Marion Permit #: WQ0019960 Annual Dry Tons Applied:
92.96
Owner:
Toua & Tong Khang Operator: Toua & Tong Khang Cation Exchange Capacity (non 503):
;ite #:
Kl
Field #: K1 Acres Utilized: 16 Acres Permitted:
16
F-1 specify
1
Inches
Appli-
Voli-
Miner-
Ammo-
Ni-
Must Select
Totals
�3' Tons Per
Residual
Cond.Crop
Precip.
cation
tila-
ala-
TKN
nia-
trate
PAN 1
PAN 2
1 or Crop
2
Gal.
cr292,500
d.
Per
Solids
Acrels
Sources
(Summarize)
Dry,
Wet,
Past 24
Meth-
zati **
zation
Ni-
and
ort
A
Acre
His.
od
Rate
Rate
trogen
Nitrite
Crop 1
Crop 2
al.3-05
18281
3.21
2.447073281
WWTP
Moist
dry
0
s
0.5
30%58600
600
84
87.0375
/{######
Fescue10-OS0
25188
3.21
3.371523188
WWTP
dry
0
s
0.5
30%
58600
600
84
119.918
#######
Fescue
2
.5
0
0
0
0
0
0
0
0
0
43469
Current Cumulative lbs/ac
Prior Years Cumulative lbs/ac
0
0
0
3
0
0
0
4
0
0
0
5
0
0
0
E
0
0
0
i
0
0
0
f
0
0
0
S
0
0
0
1
0
0
0
1
0
0
0
1
As
Cd
Cr
Cu
Pb
HR
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
0.0225428
0.04183
0
5.87972
0.255641
0.0237
0.77854
0.25564
0.05926
12.689
267.26
1206.956
0
Date
lbs/ac
0.0694694
0.07654
0
9.11732
1.20438
0.06218
2.2682
0.56278
0.13769
24.1697
0.0469266
0.03471
0
3.2376
0.94874
0.03848
1.48966
0.30714
0.07843
.11.4807
Permitted C. P. L. R*** 36 34 NA 2338 267 15 NA 1 374 89 2498
xwa­
Permit PAN Limit 1 st/2nd Crop
:...: :.. 250
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature f Land Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incoruoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loadine Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
Into the some numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Pi .ArF A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960
)wner: Toua & Tong Khang Operator: Toua & Tong Khang
U. VI) Field #: K2 Acres Utilized: 38
Annual Dry Tons Applied: 124.37
Cation Exchange Capacity (non 503):
Acres Permitted:
38
11lC tt:
1
Inches
Appli-
Voli-
Miner-
Ammo-
Ni-
Must Select
i:s S eci
o �sEN
Totals
o
��
Dry Tons Per
Residual
Cond.
Preci p
cation
tila-
ala-
TKN
nia-
trace
PAN 1
PAN 2
Crop 1 or Crop
2
�•
0 c
Cu.Yd.
Per
Solids
Acre
Sources
(Summarize)
Dry,
Wet,Past
24
Meth-
zation
zation
Ni-
and
`: Report
a
'< Totals
AcreMoist
Hrs.
od*
Rate**
Rate
trogen
Nitrite
1
Eip
Crop 2
in Gal.
0.251862513
WW'f?
dry
0
s
0.5
30%
58600
600
84
9.95825
#######
Fescue
1
71,500
1881.61
3.21
-27-05
1.648554632
WWTP
dry
0
s
0.5
30%
58600
600
84
58.6358
#######
Fescue
2
3-05
469000
12316
3.21
1.373795526
WWTP
dry
0
s
0.5
30%
58600
600
84
48.8632
#######
Fescue
3
10-05
390000
10263
3.21
0
0
0
0
0
0
0
0
0
0
0
4
5
6
7
0
0
0
0
0
0
0
0
0
0
0
0
0
8
9
0
0
10
0
0
0
0
11
0
0
0
0
12
0
TOTALS: 24461 ;
0
As
Cd Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
X
Annual lbs/acre
0.012687E
0.02354 0
3.30924
0.14388
0.01334
0.43818
0.14388
0.03335
7.14168
150.42
116.457,
0
Date
lbs/ac
Current Cumulative lbs/ac
0.033137E 0.04501 0 6.73484 0.73548 0.03961 1.18968 0.31814 0.0724 14.3453 >
0.02045 0.02147 0 3.425E 0.5916 0.02627 0.7515 0.17426 0.03905 7.2036
36 34 NA 1338 267 15 NA 374 89 2498
1
.. . :. 250
,.'.
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit l st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a systehl
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Lan' Applier
-24-v--
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. Ile. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)

www.nc com/h mi
:NCDAC&'A '5 .Web' 7 3,206: a Re , rt No ;O337G
gr gr. no -
Grower: Deluca, Mario Copies TO: Branch Residuals & soils
460 Wilson Valley Dr
Marion, NC 28752
3 oil Test Report
,R
Farm:
12/5/2006 SERVING N.C. RESIDENTS FOR OVER 60 YEARS McDowell County
Agronomist Comments
The heavy metal report is found on a separate page. Using Melillch 3 as a soil test extractant, background levels of
these metals typically seen In NC soils when analyzed are as follows: arsenic (As)- 5.0 ppm, cadmium (cd)- 0.2
ppm, chromium (Cr)- 0.3 ppm, lead (Pb)- 4.0 ppm, nickel (Ni)- 0.7 ppm, & selenium (Se)- 0.2 ppm
(FY2003-2005). Although the above metals here are not believed to pose a concern for plant growth, continue to
monitor these and note where elevated above background levels.
C -- 12
Sample No.
Last Crop
Mo Yr
TIA
Crop or Year
Lime
IV
P205 K20
Mg
S
Cu
Zu
B
Mn
See Note
K-1
1st Crop: Fes/OG/rim,M
0
120-200
60-80 10-30
0
0
0
0
.0
0
12
2nd Crop: Fes/OG/Tim,M
0
120-200
60-80 10-30
0
0
0
0
.0
0
12
Test Results
Soil Class
Im WIV
CEC
BS916
Ac PH P-I K-I
Ca% Mg%
Mn-I
Mn-AI(1) Mn-AI(2) Zn-I
Zn-Al
Cu-I
S-I
SS -I
NO3-N NH4-N
Na
MIN
o.6 1.02
11.8
90.0
1.2 6.3 30 62
66.0 21.0
374
237 237 116
116
85
32
0.0
Tie
PP
vtecpmmen ati
R"
Sample No.
Last Crop
MO Yr
TIA
Crop or Year
Lime
N
P205 K20
Mg
S
Cie
Zn
B
Mn
See Note
K-2
1st Crop: Fes/OG/rim,M
0
120-200
0 10-30
0
0
0
0
.0
0
12
2nd Crop: Fes/OG/rim,M
0
120-200
0 10-30
0
0
0
0
.0
0
12
Test Results
Soil Class
ZW% W/V
CEC
BS%
Ae PH P-1 K-I
Ca% Mgl".1
Mn-1
Mn-AI(1) Mn-AI(2) Zn-1
Zn-Al
Cu-1
S-I
SS -I
NO3-N NH4-N
Na
MIN
0.86 1.04
13.4
87.0
1.8 6.2 223 66
70.0 14.0
174
118 118 542
542
294
59
0.1

`'$K3€ si'''_k3{:l.>L'+Tt€T•?•7lFai*_rnrsR.r�,-T. c��-_�sm+�aeee*�. - -- - - - - -
.� ;., cr,3 o -r. Is.= `.3 ii.'..:r_�}kr_u.l-, ,�-- 1E>�.._r -w. •,cr c-€n' \e?;?o�a4F i.. :�Th sIl i-1..-,-:kl,�l.#`-k
' � Eli. �..�" �' .•�� :���. II., € €1
�p;i-:P L.... 4J,1•:i�` € C.�..- .-ti�kl �.,,,.._ 4,. .r,_ r ��� k..i :.' r r;li5� ill...:,. . .: e.€! ,ti, �.#...i- ,-4r..i ,�..,+� .��i�� 1 - -`I�. s,i. �{
Y1ta...l a'�, �_�_�.1 �,.�4I'�V-y lu<r.��i.. r .,,?s.�.�l�:::uex�€ -.:5: .�. I.F•�iit.��.. ,-il-. �a _ _._€z. ,i.L �„,�I l"' i r�l .„ [.I, ,.I.I�`Lb.�_.,,1. SI . rF1€..::.al...Its..•=....�..4:_`:-f�;.r��;�;i
Heavy Metal Soil Test Repo Report#: 03376
Deluca, Mario
460 Wilson Valley Dr
MEHLICH-3 EXTRACT ION 3mon,
McDowell County
Questions concerning these analyses should be referred to the Agronomic Divisions, Soil Testing
Cd Ni P h Se Gr As At Fe
Sampk Cadmium Nickel Lead Selenium Chromium Arsenk Aluminum Iron
ID------------------------------ ------- -------- --------------------meq/drn3(ppm)--------------------------------_------_----------
K-1 0.10 0.50 1.00 0.10 0.20 3.10 833.70 82.00
K-2 0.10 0.40 7.20 0.00 0.10 3.90 1,045.00 137.20

Report Number:
R06263-0067 A&L EASTERN LABORATORIES, INC.
Acount Number: 7621 Whitepine Road • Richmond, Virginia 23237 , [phone]
46368 Fax No. [phone] - Email: [e-mail]
TO: BRANCH RESIDUALS & SOILS LLC RE: MARIO DELUCCA 2006-51 BOB BRANCH
311 B S WESTGATE DR NC CERT #257
GREENSBORO, NC 27407
ATTN: BOB BRANCH
Date Received: 9/19/06 Date Reported: 09/22/2006 REPORT OF A N A LYS I S
18056 K-1 Mercury - Mehlich-3 < 0.2 mg/kg SW 846-7471A
Molybdenum (Mo)- Mehlich-3 0.4 ppm NCR-13 No. 221 1998
___...._..._._. ____-..._..._._.. _._..._.___.........._
18057 K-2 Mercury - Mehlich-3 < 0.2 mg/kg SW 846-7471A
Molybdenum (Mo)- Mehlich-3 0.4 ppm NCR-13 No. 221, 1998
GI F_lA1—
Page: 1
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made ,)� eL—
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. V
Paul Chu, Ph.D.

Nancy Ross Farm

State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
LANDOWNER AGREEMENT ATTACHMENT
(HRS FORMMA YBE PHOTOCOPIED FOR USEASANORMINAL)
The Division of Water Quality (Division) will not consider this attachment form to be complete
unless all the instructions are followed. Failure to follow the instructions or to submit all of the
required items will lead to additional processing and review time for the application.
For more information or for an electronic version of thisform, visit our web site at: http://li2o.enr.state.nc.uslndpul
INSTRUCTIONS TO THE APPLICANT:
A. Attachment Form:
✓ Do not submit this attachment form for review without its corresponding residuals program
application form (Form NDRLAP).
✓ Any changes to this attachment form will result in the application package being returned.
B. Prepare a separate attachment form for each set of land application sites that are owned by a landowner
and operated by a lessee/operator (i.e.; if applicable) other than the applicant.
✓ A copy of the completed and appropriately executed attachment form must be provided to the landowner and
the lesseeoeperator.
AGREEMENT FOR THE LAND APPLICATION OF RESIDUALS
TO PRIVATELY -OWNED LAND APPLICATION SITES
The undersigned landowner or his representative hereby permits:
Applicant's name: Mr. J. Robert Boyette, City Manager
Complete mailing address of applicant: City of Marion
City: Marion
P. O. Drawer 700
State: NC Zip: 28752
Telephone number: [phone] Facsimile Number: [phone]
E-mail address: [e-mail]
hereinafter referred to as the Permittee, to land apply residuals from the following residuals source -
generating facility(ies) onto the following land application site(s) (Le., see attached buffer maps) in
accordance with the stipulations and restrictions as given in this Agreement-,
Site/Field ID
Land Use or Cropping
Patterns
Intended Use or Disposition of
Crops
Residuals Source -Generating
Facilities
See
Row Crops
Animal Feed
Marion WWTP
Attached
Hay/Pasture
The landowner or his representative receives, in consideration, full use of the nutrient value of the applied
residuals while the Permittee receives, in consideration, the use of the land application site(s) described above
for the disposal of the residuals.
This Agreement shall remain in effect for the length of the Division of Water Quality's (Division) permit for
the residuals land application program and shall be renewed each time this permit is renewed.
The undersigned landowner or his representative and the Permittee agree to abide with the following
restrictions and stipulations until such time as written notification, given 30 calendar days. in advance,
modifies or cancels this Agreement.
FORM: LOAA 02/02 Page 1 of 3 Attachment Order 3-c

I. STIPULATIONS:
1. The landowner or his representative shall not enter into any additional waste disposal contracts or agreements with
another municipality, contractor, or other permitted entity for the land application site(s) specified by this Agreement.
The land application of any additional residuals or waste, other than that generated by the residuals source -generating
facilities specified by the Division's residuals land application program permit, is prohibited.
2. The existing lessee or operator, if any, of the land application site(s) agrees, by execution of this Agreement, to comply
with all provisions of this Agreement.
3. Should the landowner or his representative lease or otherwise permit the use of the land application site(s) by a third
party, the landowner shall be responsible to ensure that the third party agrees and complies with the terms and conditions
of this Agreement.
4. This Agreement shall be binding on the grantees, the successors, and assigns of the parties hereto with reference to the
subject matter of this Agreement.
5. The landowner or his representative or successors shall adhere to the provisions of this Agreement for a period of 18
months from the date of the most recent residuals land application event.
6. Notification of cancellation of this Agreement shall be immediately forwarded to NCDENR-DWQ, Non -Discharge
Permitting Unit, 1617 Mail Service Center, Raleigh, NC 27699-1617.
7. The Permittee must request and obtain a permit modification from the Division prior to a transfer of the land application
site(s) to a new landowner. The request shall contain the appropriate forms and agreements. In addition, a notice shall be
given by the current landowner to the new landowner that gives full details of the residuals applied or incorporated at the
land application site(s).
8. The Permittee has provided the landowner or his representative with information and data concerning the residuals land
application program, including an analysis of constituents of the residuals, residuals application methods, schedules for
typical cropping patterns, and a description of the equipment used by the Permittee.
9. The Permittee will provide the landowner or his representative with a copy of the residuals land application program
permit that has been most -recently issued by the Division prior to commencement of any residuals land application event.
This permit will specify maximum application rates, limitations, and other restrictions prescribed by the laws and
regulations.
10. The land application site(s) shall be adequately limed to a soil pH of at least 6.0 prior to residuals land application. The
only exception is that residuals may be land applied when the land application site has a pH of less than 6.0, provided that
a sufficient amount of lime is also applied to achieve a final pH of the lime, residuals, and soil mixture of at least 6.0.
11. The Permittee will furnish the landowner or his representative with a copy of the results of each soil analysis.
12. Within the limits of the Division's residuals land application program permit, the landowner or his representative and the
Permittee will determine residuals application rates and schedules based on crop patterns and the results of soil samples.
13. The landowner or his representative will furnish the Permittee with information regarding the amount and analysis of
other sources of nutrients (e.g., fertilizer, unregulated animal waste, etc.) that have been applied to the land application
site(s).
14. The landowner or his representative will inform the Permittee of any revisions or modifications to the intended use and
cropping patterns for the land application site(s) prior to each planting season to enable the Permittee to amend this
Agreement and schedule residuals land application events at appropriate periods.
15. Specific residuals land application area boundaries shall be clearly marked on the land application site(s) by the Permittee
and/or the landowner or his representative prior to and during a residuals land application event.
16. Appropriate measures must be taken by the Permittee and/or the landowner or his representative to control public access
to the land application site(s) during active use and for the 12-month period following a residuals land application event.
Such controls may include the posting of signs that indicate the activities being conducted at the land application site(s).
17. Animals shall not be grazed on the land application site(s) for a 30-day period following a residuals land application
event. Land application sites that are to be used for grazing shall have fencing that will be used to prevent access during
these periods after such residuals land application events.
18. Crops for direct human consumption shall be harvested in accordance with the conditions of the Division's residuals land
application program permit.
19. The landowner or his representative hereby authorizes the Permittee, local officials, and State officials or their
representatives to inspect the land application site(s) prior to, during, and after any residuals land application event and to
established monitoring facilities on or near the land application site(s) as required by the residuals land application
program permit.
20. Any duly authorized officer, employee, or representative of the Division may, upon presentation of credentials, enter and
inspect any property, premises, or place on or related to the land application site(s) at any reasonable time for the purpose
of determining compliance with the Division's residuals land application program permit; may inspect or copy any
records that must be kept under the terms and conditions of this permit; or may obtain samples of groundwater, surface
water, or leachate.
21. The landowner or his representative authorizes the Permittee, local officials, and State officials or their representatives to
take necessary soil, surface water, and groundwater samples during the term of, and for 12 months after termination of,
this Agreement.

II. RESTRICTIONS:
Landowner's Certification:
® I certify that I am a deeded landowner of the above -referenced land application site(s) and am authorized to
make decisions regarding the use of the land application site(s) on behalf of other deeded landowners OR that I
am otherwise authorized, through a power of attorney or other legal delegation, to make decisions regarding the
use of the land application site(s) on behalf of the deeded landowners. I certify that the above -referenced land
application site(s) are not included in any waste disposal contract or agreement with another municipality,
contractor, or other permitted entity. Furthermore, I certify that I have read this Agreement, understand the
stipulations and restrictions, and do hereby grant permission to the Permittee to land apply residuals to the land
application site(s) as specified herein.
Landowner name: Man(iv H Pci-P Q S S
Signature: Date:
NORTH CAROLIN4 C e COUNTY
I, the undersigned Not Public do hereby certify thatAlAlVCQ . PO S5
personally appeared before me this day and acknowledged the due executi of the forgoing instrument.
WITNESS my hand and official seal this the
day
Signature an&seal:
My commission expires:
Lessee's/Operator's Certification:
❑ I certify that I have read this
specified herein.
Lessee/operator name:
Signature:
Permittee's Certification:
-A-- , 20 06
and do hereby agree to abide by the stipulations and restrictions as
Date:
® I certify that I have read this Agreement and do hereby agree to abide by the stipulations and restrictions as
specified herein.
Signing official name: Mr. J. Robert Boyette, City Manager
Signature: Date:
**� OF FORM LOAA 02/02 ***

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SCALE: 1'1= 2.4 miles City of Marion Site
CHECKED BY: Land Application Program Vicinity
DRAWN BY: RTB BRANCH Nancy Ross Farm Farm Map
RESIDUALS
DATE: Feb-07 & SOILS, LLC Project No. 2006-51

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�z � �z �n �O i`x' s S. j Fd �i'!.•;��• � S S.�wE �` � � K/ F K,Y x �•3��
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�tt� "3. t�Ci :�. ` � * *-t " d � :� x r`� - r+ � NV '� ��• °�,'+l�v \''Ji � '9 x.,
� **- � ra �� a .7 � m sa }� -s• e '� ,x� a..' '' !,r°`i z '`� ; � ?�,� cr z,i�r � ��
?'1>� HCC� i p }Yn. xY 6 ty`i r•-i ka t -.. es �..y N,t "-.y, �a
_.. �,�sa'��"t...-. rt.�•�'.,. •.emu-c+1 "'„�;. EWE �'t t c� �c^�?t"._.� } . .
SCALE: 1"=2000' City of Marion Soil
CHECKED BY: Land Application Program Survey
DRAWN BY: R'1'g BRANCH Nancy Ross Farm Map
]RESIDUALS
DATE: Feb-07 Sl SOILS, LLC Fmject No. 2006-51

NANCY ROSS FARM
TRACT R
SOILS AND AGRONOMY REPORT
Field 1 has been modified to add 3.4 acres to this field. This field has been buffered to
exclude areas of slope and property lines.
Field investigations performed by a BR&S soil scientist concurred for the most part with the
mapping published in the McDowell County Soil Survey. The added area to the north of
Field 1, has soils consistent with the majority of Field 1 which is the Hayesville soil series. A
detailed soil profile description from the investigation has been attached.
Soil samples from North Carolina Department of Agriculture NCDA are attached. These
fields should receive nitrogen applications in accordance with the predominant soil series
indicated and the corresponding realistic yield estimation (RYE) as available from
http://www.soil.ncsu.edg Limp/ncnmwg/yields/.

SOIL EVALUATION FORM
Project Name
Owner
Operator
Slope
BRANCH RESIDUALS & SOILS, LLC
'311 B South Westgate Drive - Greensboro, NC 27407
PHONE [phone] —FAX [phone]
City of Marion
Nancy Ross
Nancy Ross
10-Jun Sample No. 1
Project Number
Tract/Site
Field
'Crop
2004-41
Added to. Field I
Fescue
NX, Ni!
N'M--0
Ap
0-4SCL
5 YR 4/4
wk med gr
fr
n/a
Btl
4-18
CL
25 YR 4/8
mo med sbk
fr
n/a
W
18-30
C
2.5 YR 5/8
mo med sbk
fr
n/a
B/C
30-40+
CL
2.5 YR 5/8
wk med sbk
fr
7.5 YR 5/6
Grading to saprolite with veins of parent
material.
Additional Comments
Depth to Apparent Water Table (in.) >40+ Depth to Seasonal Water Table (in. >40+
Depth to Restrictive Horizon (in.) n/a Type of Restrictive Horizon n/a
Boring needed prior to application: no , Attached map with boring location no
Most Closely Related Soil Series Hayesville
Discussion of Site
Good year round site

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 41.503176
3wner: Wayne Ross Operator: Wayne Ross Cation Exchange Capacity (non 503):
Re #: Rl Field #: RI Acres Utilized: 16 Acres Permitted: 16
Specify site Inches Appli- Vola- Miner- Ammo- Must Select
o Gal. Totals Residual Cond. Ni-trate Crop 1 or Crop
D Tons Per Precip. cation tili- ali= nia-
N oRe
Per Dry Sources Dry, TKN and PAN 1 PAN 2 2
Solids Acre Past 24 Meth- nation nation Ni-
Ca Acre (Summarize) Wet, Hrs*** Rate trogen Nitrite Crop 1 Crop 2
in Gal.
I
2.5939485
WWTP
Moist
dry
0
s
0.5
30%
48300
3700
1
79.0169
#######
Fescue
6-206
286,000
17875
3.48
0
0
0
0
0-
0
0
0
0
00
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
L
0
0
0
0
1
0 0
TOTALS: 17875 < >><>
As
Cd Cr
Cu
Pb
H
Mo
Ni
Se Zn P PAN 1 PAN 2
Lime Applied
Annual lbs/acre
0.0098572
0.01038 0.22308
2.56806
0.3009
10.02023
0.12451
0.16083
0.0192 5.86244 143.189 79 0169 0
Date lbs/ac
Current Cumulative lbs/ac
0.0346572
0.02929 0.22308
5.6879
0.85263
0.03871
1.14636
0.33764
0.0718 12.321
0.0526 6.45904
89 2498
250
Prior Years Cumulative lbs/ac
0.0248
0.01891
0
3.11984
0.55173
0.01848
1.02185
0.17681
Permitted C. P. L. R.***
36
34
NA
1338
267
15
NA
374
Permit PAN Limit 1 st/2nd Crop
_
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
-0 '� *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of tirnd Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 27.354366
Dwner: Wayne Ross Operator: Wayne Ross Cation Exchange Capacity (non 503):
Re #: R2 Field #: R2 Acres Utilized: 12 Acres Permitted: 12
Specify
site
Inches
Appli-
Vola-
Miner-
Ammo-
Ni-trate
Must Select
*
o
Gal.
Totals
o
/o
Dry Tons Per
Residual
Cond.
Preci .
p
cation
tili-
ali-
TKN
ma-
and
PAN 1
PAN 2
Crop 1 or Crop
oE:in
Yd.
ort
Per
Solids
Acre
Sources
(Summarize)
Dry,
Past 24
Meth-
nation
nation
Ni-
Nitrite
2
A
als
Acre
Wet
Hrs.
od*
Rate**
Rate
trogen
Crop 1
Crop 2
-2006
al.
188,500
15708
3.48
2.2795305
WWTP.
Moist
dry
0
s
0.5
30%
48300
3700
1
69.4391
#######
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
E
0
0
0
0
7
0
0
0
0
F
0
0
0
0
S
0
0
0
0
1
0
0
0
0
1
0
0
0
0
1.
TOTALS:
15708
<«
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.0086602
0.00912
0.19599
2.25621
0.26436
0.01778
0.10939
0.1413
0.01.686
5.15054
125.801
69.4391
0
Date
lbs/ac
Current Cumulative lbs/ac
0.0293841
0.03354
0.19599
5.72237
0.69837
0.32423
0.70069
0.31196
0.05016
12.5973
Prior Years Cumulative lbs/ac
0.0207239
10.02442
0 13.46616
0.43401
0.30645
0.5913
0.17066
0.0333
7.44676
Permitted C. P. L. R.***
36
34
NA
1338
267
15
NA
374
89
2498
Permit PAN Limit 1 st/2nd Crop
250
>:
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
P14, --0 2�2 - %-11 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

NCDA&CS-A `ono�lic'-Division Phot a .g19 733..2655 W,eb Site www.ticacoma onoRe o'rt No. -03374 .
';'
Grower Ross, David Copies To: Branch Residuals & Soils
2545 Pax Hill Rd
Morganton, NC 28655
3 oil Test Report
Farm:
12/5/2006 SERVING N.C. RESIDENTS FOR OVER 60 YEARS McDowell County
Agronomist Comments
The heavy metal report Is found on a separate page. Using Mehlich 3 as a soil test extractant, background levels of
these metals typically seen In NC soils when analyzed are as follows: arsenic (As)- 5.0 ppm, cadmium (Cd)- 0.2
ppm, chromium (Cr)- 0.3 ppm, lead (Pb)- 4.0 ppm, nickel (Ni)- 0.7 ppm, & selenium (Se)- 0.2 ppm
(FY2003-2005). Although the above metals here are not believed to pose a concern for plant growth, continue to
monitor these and note where elevated above background levels.
C -- 12
Sample No.
Last Crop
Mo Yr
T/A
Crop or Year
Lime
N
P205
K20
Mg S
Cu
Zn
B
Mn
See Note
R-1
1st Crop: Fes/OG/Pim,M
.6T
120-200
40-60
60-80
0 0
0
0
•0
0
12
2nd Crop: Fes/OG/rim,M
0
120-200
40-60
60-80
0 0
0
0
.0
0
12
Test Results
Soil Class
HM106 iV/V
CSC
BS%
Ac pH P-I K-1
Ca% Mg'06
Mn-I
Mn-AI(1)
Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-I
SS -I
NO3-N NH4-N
Na
MIN
1.43 1.05
8.7
78.0
1.9 5.7 38 34
50.0 27.0
87
69
69 87
87
78
50
0.1
Field"Information = -Applied
Lime
Recommendations
Sample No.
Last Crop
No Yr
T/A
Crop or Year
Lime
N
P2O5
K2O
Mg S
Cu
Zn
B
Mn
See Note
R-2
1st Crop: Fes/OG/PIm,M
0
120-200
20-40
0
0 0
0
0
.0
0
12
2nd Crop: Fes/OG/ lm,M
0
120-200
20-40
0
0 0
0
0
•0
0
12
Test Results
Soil Class
IBM% 1V/V
CSC
BS106
Ac pH P-1 K-1
Ca% MgS6
Mn-I
Mn-AI(1)
Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-1
SS -I
NO3-N NH4-N
Na
MIN
1.19 0.98
12.6
89.0
1.4 6.3 50 93
56.0 29.0
144
99
99 104
104
87
47
0.1

Heavy Metal Soil Test Report Rom, David ReuorM 43374
2545 Pax UjU Rd
HLIeH-3 EXTRACTION MOTganfon, NC 28655
McDowell County
Questions concerning these analyses should be referred to the Aerono
Cd N,
Sarnp[e Cadnrlum. Nickel
P6
lead
Se .0
� �
Fe
- --- ----------------------__-----_--
Selenium Chromium
/rlrrp3 �niurn
---------------------
Arsen k Alumfnwn
--- ------
iron
R-2 0.10 0,40
0.00
0.30
0.00 0.20
4.70 1,274.00
179.90
0.00 0.20
3.40 1,026.00
I64. I0

Report Number:
R06263-0068 A&L EASTERN LABORATORIES, INC.
Acount Number: 7621 Whitepine Road • Richmond, Virginia 23237 • [phone]
46368 Fax No. [phone] - Email: [e-mail] U
TO: BRANCH RESIDUALS & SOILS LLC RE: DAVID ROSS - 2006-51 BOB BRANCH
311 B S WESTGATE DR NC CERT #257
GREENSBORO, NC 27407
ATTN: BOB BRANCH
Date Received: 9/19/06 Date Reported: 09/22/2006 REPORT OF ANALYSIS Page: 1
18058 R-1 Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
Molybdenum (Mo)- Mehlich-3
0.3
ppm
NCR-13 No. 221, 1998
18059 R-2 Mercury - Mehlich-3
< 0.2
mg/kg
SW 846-7471A
Molybdenum (Mo)- Mehlich-3
0.3
ppm
NCR-13 No. 221, 1998
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made � C� —
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. v
Paul Chu, Ph.D.