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WQ0019960_Annual Report_20180226
2017 City of Marion Waste Water Treatment Plant 2017 Annual Report Land Application Program Permit No. WQ0019960 Fr, F:h®F FEe121 2018 INFpR ' SECTION 01PROCESSING UNIT Division rf Water Resources FE6 2 6 2018 Water OLMIRV Reniioral Operations Ashowi lt. / t J ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0019960 Facility Name (as shown on permit) Land Application.Operator: County: McDowell Year: 2017 City of Marion Southern Soil Builders, Inc. Phone: 336-957-7871 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes D No - If No, ship Part A, and Part :B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 1 8 Total number of fields utilized for land application daring the year: F 6 Total amount of dn- tons applied during the year for all application sites: 94.34 Total number of acres utilizes for land application during the year: 72.7 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. H Yes 0 No If no please, provide a written description why the facility was not compliant, the (fates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was perfornied in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory, results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T. 111.1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 l) Vegetative cover was maintained and proper crop management was performed on each site receing residuals., as specified in the permit. 12) No nuioff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Name and Title (type or print) Si d(tire of Permit( Date 2 - /2-/Ff //---'j H,f a S ign a turvofPrep�* Date (if different from Permittee) Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 021' Signature of Land Applier Date (if different from Permittee and Preparer) 1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0019960 Laboratory: 1) Facility Name: City of Marion 2) Residual Source WQ # or NC0031.879 3) NPDES #: 4) WWTP Name: Corpening Creek 5) Residual Analvsis Data ETS Parameter (mg/kg) Conc. Limit (mg/kg)" Sample or Composite Date 2-21-17 Percent Solids (%) NA 2.83 Arsenic 75 17.4 ti` Cadmium 85 6.96.E Copper 4,300 37-3 Chromium NA NA Lead 840 44 V mercury 57 2.3 ✓ Molybdenum 75 17.4 Nickel 420 18.9 Selenium 100 17.4 Zinc 7.500 858 J Total Phosphorus NA 21700 vi TKN NA 61500 V Ammonia -Nitrogen NA 7930 Nitrate and Nitrite NA 2833.3 a For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and' evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Z-/z -/ Y Date DENR FORM RSSF (12/2006) ANNUAL RESIDUAL -SAMPLING SUMMARY FORM B Report all sampling analysis results for parameters not listed in FORM- RSSF that are part of the.WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: W00019960 Facility Name: City of Marion Residual Source NC0031870 . N.PDES # or WQ#: WWTP Name: Corpening Creek Residual Analvsis Data Laboratory:. I) ETS 2)- 3) 4) 5) Parameter (mg/kg) Sample or Composite Date 2-21-17 Aluminum 18100 Calcium 20200 Magnesium 8370 Potassium 4840 Soditun 2430 pH 7.1 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature, of Preparer * Date DENR FORM RSSF - B (12/2006) t. ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): Permit #: WQ0019960 Cation Exchange Capacity (non S03 only): Operator: Mario DeLuca Owner: Mario DeLuca Predominant Soil Series: Acres Used: 16.4 Acres Permitted: 16.4 Site #: K1 Field #: 20.71 Hac KI. Residual Analysis Data (Heavy Metals and Total Phosphorus use mL-/kL-, o Solids use Raw Percent #): Sample or Com- posite Date 1 2/21/17 ?? 3 4 i 5 j 6 j 71 8 9j 101 Llj 12 % Solids 2.83 Arsenic 17.4 Cadmium 6.96 Copper 373 hromiun NA Lead 44 Mercury 2.3 Moh-b- denum 17 4 Nickel 18.9 Selenium 17.4 Zinc 858 Total Plios- honis 21700 Annual heavy ivletal rleld Loadings ((:alculated in lbs/acre): Total 1....1 ? ?.j 41 j 81 10...j 11 l 12 DT/Ac./ _5..1 _6_i _.? 5 App. Event 1.26 Arsenic 0.044 1 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Cadmium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Copper 0.942 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.942 hromiun 994#44 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 #4#4#4 Lead 0.111 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.111 Mcrcury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.006 • lvlolyb- 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 denUm Nickel 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Selenium 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Zinc 2.167 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.167 Total Plhos- 54.81.4 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 54.814 phorus "i certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 1"/,:f - /,J Date J DENR FORM MFLSF (12/2006) t ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: CAN? of Marion Total Dry Tons Applied (Annual): Permit #: WQ0019960 Cation .Exchange Capacity (non -503 only): Operator: Mario DeLuca Owner: Mario DeLuca Predominant Soil Series: Acres Used: -1 Acres Permitted: 30.3 Site #: K2 Field #: 2-.30 Hac K2 Residual Analysis Data (Heavy . Metals and Total Phosphorus use m2/k2. °/o Solids use Raw Percent #): Sample or Com- posite Date 1 2/21 / 17 2 31 4' 5 6. 7' 8; 9' LOJ 11 F 12.1 '%, Solids 2.83 Arsenic 17.4 Cadnuunt 6.96 Copper 373 Chroinitur NA Lead 44 Mercun; 2.3 Molyb- denum 17.4 Nickel 18.9 Selenium 17.4 Zinc 858 Total Phos- L)horus 21700 Annual Heavy lvletal Yield Loadings (Calculated in lbs/acre): Total _1_; _?_i 31 _4] 5j 6...] ? l $_1 ?_ .i ?_.1 1.2..1 DT/Ac./ y o .App. Event 0.84 " Arsenic 0.029 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Cadmium 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 Copper 0.623 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.623 hrontiun 4444#4 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 449444 Lead 0.073 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.073 Mercury 0,004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.029 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.029 denum Nickel 0.032 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.032 Selenium 0.029 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Zinc 1.433 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 1.433 Total P}tos- 36.239 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 36.239 horus I certtry, unaer penalty or taw, tnat tors aocument was preparea under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". v v Signature of Land Applier Date DENR FORM MFLSF (12/2006) ` ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Citv of Marion Total Dry Tons Applied (Annual): 14.57 Permit #: WQ0019960 Cation Exchange Capacity (non iO3 only): Operator: John Fisher Owner: Jolm Fisher Predominant Soil Series: BrB2 Acres Used: 9.9 Acres Permitted: 9.9 Site #: F1 Field #: Fl. Residual Analysis Data (.Reavv Metals and Total Phosphorus use m2/k2, o Solids use Raw Percent #): Sample or Com- posite Date 1 2/21/1.7 2 j 31 4 1 _5j ^6 71 8 9", 101 11 121 % Solids 2.83 Arsenic 17.4 Cadmium 6.96 Copper 373 hromiun NA Lead 44 Mercurn 2.3 Mold b- denum 17.4 Nickel 18.9 Selenium 17.4 Zinc 858 Total Phos- honis 21700 Annual Heavy 1Vletal field Loadings (Calculated in Ibs/acre): Total �.. 21 3 _........ 4' S; 6 7? 8I 9j 10j _ 11' 121' DT/Ac./ _..... _._ o App. &ent 1.47 Arsenic 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.051 Cedininin 0.020 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Copper 1.098 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 1.098 hromiun 494444 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 #94949 Lead 0.130 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.130 Mercury 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Mohfb- 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 denUm Nickel 0.056 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.056 Selenium 0.051 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.051 Zinc 2.526 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.526 Total Phos- 63.885 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 63.885 liorus i certify, unaer penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". V Ii V Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 3.07 Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: John Fisher Owner: Jolm Fisher Predominant Soil Series: BrB2 Acres Used: 2.4 Acres Permitted: 2.4 Site #: F2 Field #: F2 Residual Analysis Data (Heavy Metals and Total Phosphorus use tnOkg, 0/1 Solids use Raw Percent #): Sample or Com- posite Date 1' 2/21/1.7 2 3jl 41 51 6 71 8j 9 10 11 12! % Solids 1 2.83 Arsenic 17.4 Cadmium 6.96 Copper 373 Chromiuni NA Lead 44 Mercury 2.3 Molyb- denLlIll 17.4 Nickel 18.9 Selenium 17.4 Zinc 858 Total Phos- honis 21700 Annual Heavy Metal field Loadings (Calculated in lbs/acre): Total1 2..:i 3;3 41 5Ji 61 ?j 8 9� V 10j 111 12! DT/Ac./ App. Event 1.28 Arsenic 0.044 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Cadmium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Copper 0.953 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.953 hroiniun ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.112 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.112 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Moh b- 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 denunl Nickel 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Selenium 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.044 Zinc 2.193 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.193 Total Phos- 55.465 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 55.465 horus certily, unuer penalty or law, unat tins aocument was preparea under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of LaiApplier - r4, Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City- of Marion Total Dry Tons Applied (Annual): 16.88 Permit #: WQ0019960 Cation .Exchange Capacity (non -503 only): Operator: John Fisher Owner: John Fisher Predominant Soil Series: Hac Acres Used: 7 Acres Permitted: 7 Site #: F3 Field #: F3 Residual Analvsis Data (.Reavv Metals and Total Phosphorus use m-a/kg, 0/► Solids use Raw :Percent #): Sample or Corn- posite Date 1 2/21/ l7 2 31 41 5 3 6 7 8' 91 10 11 1 12 % Solids 2.83 Arsenic 17.4 Cadiniun 6.96 Copper 373 Chroiniuni NA Lead 44 Mercury 2.3 Molyb- dcnLIIn 17.4 Nickel 18.9 Selenium 17.4 Zinc 858 Total Phos- 1lorus 21700 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total �.... ? .............1 4 (� 5 i 6 i _-7 ; 8... 9 ( 1.0 11 12...1 DT/Ac./ c App. in Event 2.41 Arsenic 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Cadmium 0.034 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 1 0.034 Copper 1.799 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.799 111'o1111u11 #44#4 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 944#49 Lead 0.212 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.212 Mercury 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.O i l Molyb- 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 denum Nickel 0.091 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.091 Selenium 0.084 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.084 Zinc 4.137 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 4.137 Total Plios- t04.637 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 #444#4 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Cite of .Marion Total Dry Tons Applied (Annual): 13.81 Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: John Fisher Owner: John Fisher Predominant Soil Series: Acres Used: 6.7 Acres Permitted: 6.7 Site #: F4 Field #: Hac F4 Residual Analvsis Data (Meavv Metals and Total Phosahorus use mE/k2. °/► Solids use Raw Percent #): Sample or Com- posite Date 1' 2/2.1/1.7 21 31 41 51 6 r 7 8' 91 10 11 1 12 % Solids 1 2.83 Arsenic 17.4 y% Cadmium 6.96 ✓ Copper 373 V Chroiniunj NA Lead 44 % Mercur�� 2.3 Molyb denum 17.4 ✓ Nickel 18.9 Selenium 17.4 Zinc 858 J Total Phos- bolus 21700 Annual Heavy Metal rielci Loaclm2s (Ualculated in lbs/acre): Total �.__i ?._i 3 4..1 5 I 8 j 9 i 10 ' 11 ? 121 DT/Ac./ f _6.i ........; _. ...... o 4P. J '- Event 2.06 Arsenic 0.072 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072 Cadmium 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 Copper 1.538 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.538 hromiun 4444#4 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 #444#4 Lead 0.181 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.181 Mercwry 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Molyb- 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.072 denum Nickel 0.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.078 Selenium 0.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.072 Zinc 3.537 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 3.537 Total Phos- 89.447 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 89.447 horns 1 cernly, unuer penalty or iaw, mat tins aocument was preparea inner my airection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 1171. Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND -.APPLICATION FIELD SUMMARY FORM: - - --- - PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facilih, Name: Cite of Marion WQ Permit #: WQ0019960 Field #: KI Acres Utilized: 16.4 Land Owner: Mario DeLuca Annual Dry Tons Applied: 20.7109 1f Site #: KI Acres Permitted: 16.4 Operator: Mario DeLuca Predominant Soil Series: HaC Cation Exchange Capacity (non 5503): Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN: o o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons gb Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NI'DES , WQ#, Fert.,Animal Waste.. etc) Soil Cond. (Div, Wet Moist) Precip. Past 24 Hrs. inches T # - - # :� � * TKN mg/kg z o o mg/kg Nitrate and Ni4ite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop I Crop _ Crop 1 Crop 8-2017 175500 2.83 1.263 WQ0019960 dry 0 s 0.5 0.3 61500 7930 2833.3 57.762 NA Fescue 0.000 0.000 0.000 0.000 0.0,00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.0w) Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 01 175500 As Cd Cu Cr Pb Hg Mo I Ni Se Zn P 57.762 0.000 Lime Applied Atmual lWacre 0.044 V 0.018 0.942 ##; f?,' 0.111 ' ' 0.006 ' 0.044` 0.048` ' 0.044 2.167 74.814 Date lbs/ac Prior Years Cumulative Ibs/ac 0.525 0.152 19.143 1.11 2.485 0.11 / 2.547 1.14 0.339 44.366 0.569 ✓ 0.170 20.085 0##:L## 2.596 0.116 2591 1.188 0.383 46.533 36 1 34 1338 NA 267 15 NA 374 89 2498 202 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit I st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of lines and imprisonment for knowing violations." 119�- Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "*Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 ** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0. l "***C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: K2 Acres Utilized: 30.3 Land Owner: Mario DeLuca Annual Dry Tons Applied: 25.3134 Site #: K2 Acres Permitted: 30.3 Operator: Mario DeLuca Predominant Soil Series: HaC Cation Exchange Capacity (non -503): Crop 1, Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN: ,. o c3 Q VOIUIne applied } } (enter one) Solids; Liquid 9 Cu. Yds Gallons % Solids VOlume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDI S s WQ;r. Fert.. Animal Waste. etc) Soil Cond. (l.)11:. Wet. Moist) Prectp. , Past 24 Firs. inches > K R o T o C _ __ x �' o' - _ N � - �' o _ TKN I mg/kg Z > - _ = = d mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre) Name of Crop Type Receivin. Residual c Application Crop I Crop 2 Crop 1 Crop 2 8-2017 214500 2.83 1 0.835 WQ0019960 dry 0 s 0.5 0.3 61500 7930 1 2833.3 38.211 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTtvs: 01 214500 As Cd Cu Cr Pb Hiz Mo Ni Se Zn P 38.211 0.000 Lime Applied Annual Ibs/acre 0.029 0.012 0.623 ,## 0.073 - 0.004 0.029 0.032i- 0.029 1.433 36.239 Date lbs/ac Prior Years Cumulative Ibs/ac 0.24 0.269 36 0.149 0.161 34 1 18.8 19.423 1338 1.027 0 4#0ff NA 2.447 2.520 267 0.109 0.113 15 2.536 2.565 NA 1.101 1.133 374 0.325 .0.354 89 42.816 44.249 2498 11-17 2000 Current Cumulative Ibs/ac Permitted C. P. L. R..**** Permit PAN Limit 1 st/2nd Crop 202 -I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation zl/ /7l 1-"*Volatilization Rate: Surface - 0. , Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.1 '.'**C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Marion PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0019960 Field #: FI Land, Owner: John Fisher Annual Dry Tons Applied: 14.5744 Site #: FI Operator: John Fisher Predominant Soil Series: BrB2 Crop 1 Name: Fescue Crop 1 Max. PAN: 239 ✓ Crop 2 Name:. Acres Utilized: 9.9 Acres Permitted: 9.9 Cation Exchange Capacity' (non 503): Crop 2 Max. PAN: Y o Q Volume applied } R (enter one) Solids/ Liquid Cu. Yds .Gallons o,, Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPD S #, WQr, Fert.. Animal Waste. etc) Soil Cond. (Dry, Wet Moist) Prec ip. Past Hrs. inches > cs = ¢ ° o ^ c; = o` = # - _ TKN mg/kg Z ?' o ° mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs-acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 8-2017 123500 2.83 1.472 WQ0019960 dry 0 s 0.5 1 0.3 61500 1 7930 2833.3 67.134 1 NA Fescue 0.000 0.000 o:oo0 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0;000 0.000 0.000 0_600 0.000 0.000 0.006 omo 0.00o omo 0.000 0.000 0:006. Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): rar:v s: o' 123500 - As Cd Cu Cr Pb H Mo Ni Se Zn P 67.334 0000 Lime Applied Annual lbs/acre 0.051 0.027 1_098 ###7r-# 0.130 0.007 - 0.051 0.05 0.051 2.526 63.885 t/ Date lbs/ac Prior Years. Cumulative lbs/ac 0.052 0.026 4.179 2.016 0.698 0.315 0.192 0.337 0.05 13.157 Current Cumulative lbs/ac 0.103 0.046 5.277 ' ##r'0" 0.828 0.322 0.243 0.393 0.101 15.68� Permitted C. P. L. R..**** 3G 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 239 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for lmoiving violations." Jl l -16,% Signature of Land Applier l-ld- 'l13 Date *Application Method: S - Surface, IN - Inj'ection, INC Incorporation "Volatilization Rate: Surface - 0.5, Injection/.Incorporation - 1.0 * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 "C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: John Fisher Operator: John Fisher Crop I Name: Fescue WQ Permit #: WQ0019960 Field #: F2 Annual Dry Tons Applied: 3.0683 Site #: F2 Predominant Soil Series: BrB2 Crop 1 .Max. PAN: 239 Crop 2 Name: Acres Utilized: 2.4 Acres. Permitted: 2.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: s Q Volumc applied PP (enter one) Solids/ Liquid Cu. Yds Gallons u- ; Solids Volume Applied per Acre (Dry Tons/AG) Residual Source (NPDES r, WQ , Ferf., Animal Wirste. etc) Soil Cored. t' Moist Precip. Past 24 Hrs: inches 6 * E3, C O _ o _ ¢ " _ TKN mg/kg b Z o - o E! r ° g a J mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs.acre) Name of Crop Type Receivinu Residual Application Crop 1 Crop _ Crop 1 Crop 2 8-2017 26000 2.83 1.278 WQ0019960 dry 0 s 0.5 0.3 61500 7930 2833.3 58.475 NA Fescue 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0:000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp (attach FORM FSF supp to this form): TOTALS: 01 26000 As Cd Cu Cr Pb H9 Mo Ni Se Zn P 58.475 0.000 Lime Applied Annual lbs/acre 0.044 "0.018' 0.953 #rY##' 0.112' 0.006 , 0.04�4 0;048 - 0.044 2.193 55.46 Date Ibs/ac Prior Years Cumulative lbs/aeL 0.088 0.132 36 1 0.154 6.172 34 3.063 4.016 1338 1.365 1 #�r##; 1, NA 0.499 0.611 267 0.026 0.032 15 0,137 �. . 0.181 ' NA 0?4 0.288 74 1 0.034 0.078 89 9.396 11.589 2498 11-17 1000 Current Ctunulative Ibs/ac Pennitted C. P:.L. R.**** Pennit PAN Limit 1st/2nd Crop _: 2391. "I certify, under penalty of law, that this document ivas prepared under my direction or supervision in accordance -with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of lines and imprisonment for knowing violations." iG-- Signature of Land Applier Date "Application Method: S - Surface, IN -Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, InjeetionAncorporation 1.0 * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ***C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE -COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F3 Acres Utilized: 7 Land Owner: John Fisher Annual Dry Tons Applied: 16.8756 Site #: F3 Acres Permitted: 7 Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 202 0/ Crop 2 Name: Crop 2- Max. PAN: o �• s ° Q Volume applied (enter one) Solids: Liquid 9 Cu. Yds Gallons ga Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDF S #, W , Q Fert.. Animal Waste, etc) Soil Cond. (Dry; Wet` Moist) Preci p` o Past 4 Hrs. inches a ° moo_' C r; = # = # ;' # o � TKN mg/kg z Y d - mg/kg Nitrate and Nitrite mg/kg PAN A lied PP ( lbs. acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 8-2017 143000 2.83 2.411 WQ0019960 dry 0 s 0.5 0.3 61500 7930 2833.3 110.266 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0:000 Residuals Applications totals on FORM FSF supp ( attach. FORM FSF supp to, this form): TOTALS: o. .143006 As Cd Cu Cr Pb H . Mo Ni - Se Zn P 110.2661 0.000 Lime Applied Atulual lbs/acre 0.084 O.162 0.246 36 1 0.034 0.066 0.100 34 1.799 3.89 5.689 1338 #i #-'### 1.763 49 ##A'## NA 0.212 0.669 0.881 267 0.011 0.024 0.035 15 6.084 _ 0.21 0.294 NA - 0.091 0._84 0.375 374 1 0.084 /0.1�8 0.242 89 1 4.137 _- 1�.�94 16.731 2498 104.637 ` `" Date Ibs/ac Prior Years Cumulative lbs/ac Current Cmmtlative lbs/ac Permitted C. P. L. R.' *** Permit PAN Limit 1st/2nd Crop p.2U2 "I certify, under penalty of law, that this document ivas prepared' under my direction. or supervision in accordance with a system designedto assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Application Method: S' - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost-0.1, anaerobialle digested -0.2, aerobically digested -0.3, raw sludge -0.4 **C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLiCA.TION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F4 Acres Utilized: 6.7 Land Owner: John Fisher Annual Dry Tons Applied: 13.8073 Site #: F:I Acres Permitted: 6.7 Operator: John Fisher Predominant Soil Series: HaC Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop .1 Max. PAN: 202 Crop.2 Name:, Crop 2 Max. PAN: 0 y o CZ L Volume applied } P (enter one) Solids/ Liquid Cu. Yds Gallons 4 o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (1vP1�1iS i, W Q Fert.. Animal Waste, etc) Soil Cond. (I>i�;, Wet. Moist) > > ' t rtup. Past 24 Hrs. inches > o' z? �• C o ^ _ �' 2 _ CD * TKN mg/kg Z ?' "0 Uq a 2 M. mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibslacre) Name of Crop Type Recciviuc Residual Application Crop 1 Crop 2 Crop 1 Crop 2 8-2017 117000 2.83 2.061 W00019960 dry 0 s 0.5 0.3 61500 1 7930 2833.3 94.258 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 o.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0:000 0.000 6.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ro'r.aLs o t i7000 As Cd Cu Cr Pb H Mo Ni Se Zit P 94.25,8 ` 0.000 Lime Applied Annuallbs/acre 0.072 0.182 0.254 ✓ 36 0.029 0.82 0.849 34 1.538 7.543 9.081 1338 #4 /#1 2.109 ###n7## NA 0.181 1.109 1.290 267 0.009 0.04 0.049 15 0.072 ,0?81 0.353 NA 0.078 0.475 0.553 374 0.072 0.192 0.264 89 3537 18.251 21.788 2498 89.447 Date lbs/ac Prior Years Cumulative lbs/ac Cturent Cutnulative lbs/ac Permitted C. P. L. R..**** Pen -nit PAN Limit I st/2nd Crop 202 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Land Applier I-I"'t I Date *Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *x Mineralization Rates: Compost -0.1, anaerobialky digested -0.2, aerobically digested -0.3, raw sludge-0.4 *"C.P.L.R.: Cumulative PollutantLoadin2 Rate DENR FORM FSF (12/2006) wm, ; n J 1� - „ ` Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Marion WWTP Collection date Date received: 2.1-Feb-17 21-Feb-17 PO Box 7365 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project mm-nber: 17022.1.514 Sample identification: CC Sludge - Grab Sample number: 145014 Parameter Method Result RL Units 0naiDate te yz Analyst Footnotes "Total Solids SM 2540 G 2.83 0.10 % 23-11'eb-17 ANJ 1. Mercury 7471 B 2.3 1.4 mg/kg 7-Mar-17 DER 1. Aluminum 6010C 18100 870 mg/kg 27-Feb-17 MEC 1 Arsenic 601.0C <17.4 17.4 mg/kg 27-1`eb-I? MEC 1 Cadmium 601OC <6.96 6.96 mg/kg 27-1`6-17 MEC 1 Calcituu... 6010C 62Ii200 870 mg/kg 27-1:6-1? MEC ! Copper 6010C 373 6.96 mg/k.g 27-Feb-17 MEC I Lead 6010C 44.0 17.4 mg/kg 27-Feb-17 MEC 1 M_aanesium 601OC 8370 870 mg/kg 2%-Feb-+? MEC 1 Molybdenum 6010C 1.7.4 17.4 mg/kg 274:6-17 MEC I Nickel 6010C 18.9 6.96 mg/kg 27-reb-17 MEC I Potassium 6010C 4840 34.8 mg/kg 27-Feb-17 MEC 1 Selenium 601OC <17.4 1.7.4 mg/kg 27-reb-17 MEC 1 Sodium 601.0C _243Q 69.6 mg/kg 27-r,+-17 MEC 1. Line 601OC 858 17.4 mg/kg 27-Feb-1? MEC 1 Nitrate + Nitrite as N 2833.3 148.05 mg/kg 1-Yiar-1? F;T.•n3;T..Ett 1, 3 Total Phosphorus 601OC 21700 696 mg/kg 27-17eb-17 MEC 1 Total Kjeldahl Nitrogen 351.2 6:1500 1150 mg/kg 1-Mar-17 EDH 1 Total Nitrogen Calculation 64300 1150 mg/kg ?-Mar-17 FIN I 1 Ammonia Nitrogen SM 4500N113 D 7930 138 mg/1<g 23-Fen-17 KEK Percent Solids SM 2540 G 2.9 % 21-Feb-17 KEK pH in Liquid SW 846 9045C 7.1 S.U. 28-Feb-17 KEK 4 N-PAV Calculation 1613898 10-Mar-17 KEK Sodium Absorption Rate Calculation 20.25 10-Ma<-17 KEK. Reactive Cyanide 335.4 <0.013 0.013 mg/kg 28-Feb-17 ECl-IEM 2 Reactive Sulfide SM 4500 S D <0.0259 0.0259 mg/kg 6 :Mar-i7 ECHEM 2 Ignitability SW 846 1030 >212 212.0 OF 23-r.b-17 ECHEM 2 Full Scan TCLP Organics - 8151A See attached sheets 9-Mar-17 ECTIEM. 2 'Footnotes: R.L_ :Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sample analyzed by Rogers & Callcott Environmental. 2. Sample analyzed by Enviro Chemists, Inc. 3. Methods EPA 921 OA and SM 450ONO2 B. 4. Sample analyzed outside hold time. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 �MVQ iy O"kz A, Environmental Testing Solutions, Inc. Project name: City of Marion Collection date: 22-Feb-l7 Date received: 22-Feb-17 Sample identification: CC Sludge - Grab Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 170221.513 Sample number: 145013 - Date Parameter Method Result RL Units :1 nil Dato Analyst footnotes Arsenic -TCLP -- --- 6010 C <0.25 0.25 rnW1 MEC; I Barium - `rCL,P 6010 C <2.50 2.5-0 mg/L I-Mar-l7 N1EC 1 Cadmium -TCLP 6010 C <0.05 0.05 mg/L t-M. ar-17 MF.,C ! Chromium -TCLP 6010 C <0.10 0.10 mg/L, t-Mar-17 MEC 1 Lead -TCLP 6010 C <0.25 0.25 mg/L, 1-Mar-i? M.EC 1 Selenium -TCLP 6010 C <0.25 0.25 mg/L 1-Mor-17 MEC 1 Silver - TCLP 6010 C <0.1.0 0.10 mg/L 1-Mar-17 MEC 1 Mercury -TCLP 7470A <0.0020 0.0020 mg/L. 2-mar-17 DER 1 Full Scan TCLP Organics See attached sheets 1 Footnotes: RL, = Reporting Limit. Vaiues are reported down to the Reporting limit only. 1. Sample analzyed by Rogers 8a Callcott Environmental. Date reviewed: NC; Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 Signature: Ibis report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc The resulu in this report relate only to the samples submitted for analysis. Mineralization ~ as decimal ITotal dry JAcres Applied on Rate TKN NH3 NO3 NO2 % Solids tons/yea / _/ v PAN Surface 4314.981lbs total PAN 59.35323libs PAN/acre PAN Injection 5063.0961lbs total PAN 69.64368libs PAN/acre Dry To s/10DO gal. 1etyear PAN Surface |bs. 4314,979524 lst year PAN Injected lbs. 5063,095724 Surface |bo./acre 59,35322591 |bm./acre Injected 69.3436 MR(TKN-NH3)+ +.6(NH3)+NO3+NO2 =mg/kg MR(TKN-NH3)+1(NH3)+NO3+NO2 =mQ/kg mg/kg x.002 =Ibs/dry ton SAR Sodium Absorption Ratio Na : Sodium (Mg/L) Equivalent weight: 23 Ca : Calcium (Mg/L) Equivalent weight: 20',gJ Mg : Magnesium (Mg/L) Equivalent weight: 12 f r Milli Equivalent = Mg/L / Equivalent weight Na(Mg/L) Ca Mc/L Mq(Mg/L} 67.769 F-5-7-1-6-67 236.871 Nra�.:P !:Ll tME Itm M4Q 2,946478 I 28.583 I 1 9. 73925 The amour amount of SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power Permitting SAR = 0.599439 (From Mg/L entered above) v 0 SAR= O.6 8307 (Fr rri ME erii:er d Na (ME) Ca (ME) Mg (ME) 2.99/ 1 28.58 1 19.74 V V- . W�o $iey�1' �r b A+� .� �r90 itk_ t i Environmental Testing Solutions, Inc. Certificate of Analysis Project name: Collection date: Date received: Marion WWTP 21-Feb-17 21-Feb-17 Sample identification: CC Sludge 91 - Grab PO Box 7565 Asheville. NC.' 28802 Phone: (828) 350-9364 Fax: (328) 350-9368 Project number: 170221.502 Sample number: 144992 Hate Parameter Method Result RL Units Auahzcd Analyst Footnotes %I'S SM 2540 G 2.9 0.10 %, 21-Feb-17 KEK Mulitple Tube Fermentation Procedure SM 9221-L 37700 522 M:PN 21-Feb-17 K.F"K Sample identification: CC Sludge #2 - Grab Sample number: 144993 Parameter Method Result RL Units AnalDate te :analyst Footnotes %rS SM 2540 G 2.9 0.10 % 21-Feb-17 K E, K Mulitple Tube Fermentation Procedure SM 9221-F 37700 522 M P N! 21-Feb-17 KE,K Sample identification: CC Sludge 43 Grab Sample number: 144994 tc Parameter Method Result RL Units AnalDate Analyst Footnotes "/TS SM 2540 G 3.0 0.10 '%u 21-17eb-17 KEX MulitpleTube Fermentationprocedure SM9'_21-E 51000 540 1VIPN 21-Feb-17 KEK Sample identification: CC Slud e #4 Grab Sample number: 144995 Date Parameter MDa Method Result RL Units Anllte Analyst Footnotes %TS SM 2540 G 3.0 (1.1U % 21-Feb-17 KEK UulitnleTube Fermentation Procedure SIM 9221-E 46200 540 MPN 21-Feb-17 KI.;K Footnotes: RL, — Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: Oa'2y-rl Data reviewed by: Kellev E. Keenan Siunatnre iA, NC; Certification dumber: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 'Ibis report should not be reproduced, exept in 71 entirety, without the written consent of Environmental Testing Solutions; Inc. The results in this report relate only to the samples submitted for analysis. ��e 1 r 7� 4,u= J t453 t1 j Environmental Testing Solutions, Inc. Certificate of fC1iA]ySi3 Project name: Collection date: Date received: Marion WWTP 28-Feb-17 28-Feb-17 110 Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: 170228.504 Sample identification: CC Sludge #5 -Grab Sample number: 145111 Parameter Method Result RL Units Date Analyzed Analyst Footnotes % FS SM 2540 G 3.0 0,10 % 28-Fcb-17 KLK Mulitple Tube Fermentation Procedure SM 9221-F 69000 522 M1?N 29-Fe1-17 Pit K Sample identification: CC Sludge #tip - Grab Sample number: 145112 Parameter Method .Result RZ. Units Bate Analyzed Analyst Footnotes %TS SM 2540 G 3.0 0.10 % 28-Feb-17 KE K. Mulitple Tube Fernienmdon Procedure SM 922.1-F., 69000 522 MPN 2s-Feb-17 KFK Sample identification: CC Slud e #7 Grab Sample number. 145113 Parameter Method Result RL Units Date Analyst Footnotes Analyzed V'S SM 2540 G 3.0 0.10 % 28-Feb-17 Kr lc Mulitple Tube Fermentation Procedure SM 9221-C 69000 540 NIPN 28-Peb-17 KCK Footnotes: RL Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley Ei. Keenan SC Certification Number: 99053 NC I)rinidng eater Certification Ntt;rtber: 37786 Signature: This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. The results in this report relate only to the samples submitted ror analysis. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Cor enin Creek Riosolids Permit Number: WQ 0019960 Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 2/16/2017 0635 Lee Estes 2/16/2017 0755 R. Carter t/ A iilliliters Dry Solids egrees Celsius egrees Celsius Slope: 0.3 Intercept: 6.8 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 18.44 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.88 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 V/ Temperature Corrected Specific Oxygen Uptake Rate: ,h 3 47 mg Oxygen/g/hr K.......v..._L�<, Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. �LW1rIF�5 = i c Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility P Biosolids Permit Nu Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level Slope: Intercept: Correlation Coefficient: 14 1 /2017 0820 oo a Estes :1/2017 1000 Carter milliliters 1 M Dry Solids 5-degrees Celsius 5 dearees Celsius 0.3 7.0 1.0 Oxygen Uptake Rate: 19.37 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.94 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate ,d 1 52 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name:kCor enin Creek Biosolids Permit Number:WQ 0019960 Date:. 2/14/2017 Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 4/20� 061 � Estes ° U i-00-011milliliters % Dry Solids 25 degrees Celsius 250dearees Celsius Slope: 0.3 Intercept: 7.4 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 17.25 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.76 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rater 1 38mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9. 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen level Ililiters / Dry Solids V grees Celsius grees Celsius Slope: 0.3 Intercept: 7.9 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 17.52 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.99 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Yi z Temperature Corrected Specific Oxygen Uptake Rate �j� �1.56 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level 0019960 2/17/2017 13' 12017 Estes liliters Dry Solids grees Celsius arees Celsius Slope: 0.3 Intercept: 7.3 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 17.85 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.82 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.43mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rafe SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level in Creek 19960 2/20/2017 13 17 �0735 o J 1 Iiliters Dry Solids grees Celsius grees Celsius Slope: 0.3 Intercept: 7.3 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 19.09 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.93 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius / Temperature Correction Factor: 0.783526166 J Temperature Corrected Specific Oxygen Uptake Rate. 1 51;,mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate SOUR Facility Biosolids Permit N Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: Total Solids: Beginning Temperature: End Temperature: Dissolved Oxygen Level V 3/201 1005 11000 milliliters 1 % Dry Solids 25 degrees Celsius 25 dearees Celsius Slope: 0.3 Intercept: 7.2 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 18.34 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.83 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 / Temperature Corrected Specific Oxygen Uptake Rater I.". mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION .FORM (02T .Rules) Facility Name: City of Marion WWTP Name: Corpening Creek Monitoring Period: From 1/1/2017 To WQ Permit Number NPDES Number 12/31/2017 WQ0019960 NC0031879 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/t.emp) 11 1 Alt B (Alk Treatment)[] Alt. C (Prior Testing) A1t.D (No Prior `rest) 6 Process to Further Reduce Pathogengs If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost Ll Heat Drying El Heat Treatment El Therniophilie 13 Beta RayG R amma av 0 Pasteurization Class B: JAII.. (1) Fecal Density Alt. (2) Process to Significantly Reduce llathoQeils If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization Air Drying 0 Composting Aerobic Digestion Anaerobic .Digestion .... .' If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in in Sludge Pathogen Density um per o ENc,er l,l ce, Frequency -Sample of Analysis Type na vtica Tech - ue Minimum Geo. Maximu Units Fecal Coliform 2 x 10 to the 6th po\ver per gram of total solids MJ,N 37700 52515.28 69000 MPN 0 7 grab sm9221 CFt1 1000 mpll per gram of total solid (dry Nveight) Salmonella bacteria (in lleLl Ot IeCal coliform) 3 MPN per 4 grams total solid (dry vvei Tit) Vector Attraction Reduction (.15A NCAC 02T ..1..107) - Please indicate alternative performed: Alt. t (VS reduction) Alt. 2 (40-day bench) Alt. 3 (30-day bench) El JAIL 4 (Spec. 0, uptake) Alt. 5 (14-Day Aerobic) Alt. 6 (Alk. Stabilization Alt 7 (Drying - Stable) jAlt. 8 (Drying - Unstable) Alt. 9 (Injection) Alt. 10 (Incorporation) No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. 1. am aware that there are significant penalties for false certification including fine and imprisonment." Prepar Name and Title (type or print) 2 ignature o Preparer* Date Dennis Key Southern Soil Builders, Inc. Land Applier Name and Title (if applicable)(type or print) J�-7e Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM PVRF 02T (12/2006) NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL008864 Predictive Client: Mario DeLuca Advisor: Southern Soil Builders, Inc. rG��GULTL•RE,w 1418 Landis Ln. 958 Hoots Rd Soil Report Mehlich-3 Extraction Maggie Valley, NC 28751 Roaring River, NC 28669 Sampled County: McDowell Links to Helpful Information Sampled: 10/05/2017 Received: 10/12/2017 Farm: Not Provided Completed: 10/25/2017 Client ID: 478471 Advisor ID: 231531 Sample ID: K1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrassfTim, M 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in glcrrr3; CEC and Na in meq/100 crrP; NO3-N in mgldrrP]: Soil Class: _ Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.86 0.93 12.7 85 1.9 6.1 275 129 59 22 62 224 150 620 620 426 0.2 1--' 2 it Sample ID: K2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) 1 N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrass/Tim, M 1.0 / 120-200 30 30 0 0 0 0 0 0 Note: 12 2- '. 1/ Test Results [units - WN in glcO; CEC and Na i meq/100 crrr3; NO3-N in mg/da]: Soil Class: Mineral HM% WN CEC BS% Ac f pH , P-I K-I Ca% Mg% S-I Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N f / 1 0.71 0.89 9.5 76 2.2 5.5/ 50 60 57 16 42 158 112 270 270 80 0.2 2 V/ North Carolina 1 Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.neagr.gov/agronomi/ Report No. FY18SL008865 G4`GULTURg�Q Predictive Client: John Fisher Advisor: Southern Soil Builders, Inc. W=FJ4P O0NG 400 Dairy Rd. 958 Hoots Rd x Mehlich-3 Extraction S0�' Rep® Maggie Valley, NC 28751 Roaring River, NC 28669 n b ti.'Ou Sampled County: McDowell ®%011• Links to Helpful Information Sampled: 10/05/2017 Received: 10/12/2017 Farm: Not Provided Completed: 10/25/2017 Client ID: 478472 Advisor ID: 231531 Sample ID: F1 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Fescue/OGrassffim, M 0.0 120-200 100 10 0 0 pH$ 0 0 0 Note: 12 Note: S 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cnt3; NO3-N in mg/dnft Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N / `� 0.51 0.92 11.9 91 1.0 6.5 18 75 76 13 30 199 128 1269 1269 341 0.1 V 1 Sample ID: F2 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrassffim, M 0.5 120-200 70 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cn-P; CEC and Na in meq/100 cnr; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac ;�.pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.56 0.93 8.6 80 1.8 i 5.8 / ' 29 86 57 17 32 220 149 188 188 248 0.1 V 1 Sample ID: F3 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrassfrim, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm�; CEC and Na in meq/100 cO; NO3-N in mg/dnt3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-1 Na ESP SS-1, NO3-N ' j / 0.41 1.02 10.9 88 1.4 6.4 221 41 61 25 41 185 122 273 273 343 0.2 V 2 North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL008865 John Fisher Page 2 of 3 Sample ID: F4 Recommendations: Lime Nutrients (lb/acre) More Crop (tons/afire) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, M '' 0.� 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cnr ; CEC and Na in meq/100 crrr3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac PH;.` P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 0.93 9.6 81 1.8 / 5.9 I 231 105 51 24 49 200 137 397 397 307 0.1 1 • • City of Mkdon wwfp P.0 Box 700 Marion ; NC 2875..2 facs. taiismitW- To:' Fax: o�CJq From: Date: CC: Urgent r . #Foi.RWw 17 PleaseComment: ©Please Reply' Ci PleaseRecyc6e If you have anyguestions please givenvacall82W2. Q !� OW oaf a r^ r ' •' • � ! • ''•t: • • o °. o • . o o • • • • • .• . ■ • • tip . • ° • • • BOOAOOd we9Z:ll Roz 9 000 06 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/13/2017 Time Sampled: 1005 Sampled By: L. Estes Time Started Aeration: 1007 Time Stopped Aeration: 1129 Time Analyzed: 1130 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 40 mins. ) Total time of test includes the time sample was aerated. 800/ZOOd WE9Z:ll 810Z 9 300 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/14/2017 Time Sampled: 0615 Sampled By: L. Estes Time Started Aeration: 0617 Time Stopped Aeration: 0753 ;Time Analyzed: 0755 Analyzed By: R. Carter Total Time of Test: < 2 hrs.( 1 hr. 55 mins. ) Total time of test Includes the time sample was aerated. 1 800/E00d We9Z:ll ROZ 9 I380 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N:C. Method, SM 2710 B-1997 Date: 2/16/2017 Time Sampled: 0635 Sampled By: L. Estes Time Started Aeration: 0637 Time Stopped Aeration: 0754 Time Analyzed: 0755 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 36 mins. ) Total time of test includes the time sample was aerated. 800/VOOd W129Z:11 810Z 9 oea Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B4997 Date: 2/17/2017 Time Sampled: 0700 Sampled By: L. Estes Time Started Aeration: 0705 Time Stopped Aeration: 0829 Time Analyzed: 0830 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 45 mins. ) Total time of test includes the time sample was aerated. 800/900d 029Z:LL ROZ 9 000 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/20/2017 Time Sampled: 0735 Sampled By: L. Estes Time Started Aeration: 0740 Time Stopped Aeration: 0906 Time Analyzed: 0907 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 47 mins. ) Total time of test includes the time sample was aerated. 800/900d Wa9Z:Gl ROZ 9 oaa Specific,4xygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/21/2017 Time Sampled: 0820 Sampled By: L. Estes Time Started Aeration: 0822 Time Stopped Aeration: 0959 Time Analyzed: 1000 Analyzed By: R. Carter Total Time of Test: < 2 hrs.( 1 hr. 55 mins. ) Total time of test includes the time sample was aerated. I 800/Lood WE9Z:li 8LOZ 9 090 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 3/3/2017 Time Sampled: 0605 Sampled By: L. Estes Time Started Aeration: 0608 Time Stopped Aeration: 07" Time Analyzed: 0745 Analyzed By. R. Carter Total Time of Test: < 2 hrs.(1 hr. 55 mins. ) Total time of test includes the time sample was aerated. 800/800d WE9Z4 L 8LOZ 9 080 • City of ]Marion WWTP • ° P•0 Box 700 - Marion ; NC 28752 facs-im-flod bias�ikd- To:' From:��' CGv Date: CC: ❑ Urgent r dot Review ©P[ease Comment' Ct Please Repiy' 0 Please Recycle If you have anyquesfions please jive uvacall 82645?'M r 800AOOd We9Z:ll SGOZ 9 Oa0 r Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/13/2017 Time Sampled: 1005 Sampled By: L. Estes Time Started Aeration: 1007 Time Stopped Aeration: 1129 Time Analyzed: 1130 Analyzed By: R. Carter Total Time of Test < 2 hrs.( 1 hr. 40 mins. ) Total time of test includes the time sample was aerated. 800/Z00d WPSZ:IL ROZ 9 080 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/14/2017 Time Sampled: 0615 Sampled By: L. Estes Time Started Aeration: 0617 Time Stopped Aeration: 0753 iTime Analyzed: 0755 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 55 mins. ) Total time of test includes the time sample was aerated. 800/600d WE9Z:ll 81.0Z 9 000 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marian, KC. Method: SM 2710 B-1997 Date. 2/16/2017 Time Sampled: 0835 Sampled By: L. Estes Time Started Aeration'. 0637 Time Stopped Aeration: 0754 Time Analyzed: 0755 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr_ 35 rains. ) Total time of test includes the time sample was aerated. 800/VOOd WE9Z:4 BLOZ 9 380 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/17/2017 Time Sampled: 0700 Sampled By: L. Estes Time Started Aeration: 0705 Time Stopped Aeration: 0829 Time Analyzed: 0830 Analyzed By: R. Carter Total Time of Test. < 2 hrs.(1 hr. 45 mins. ) Total time of test includes the time sample was aerated. 800/900d We9Z:Il ROZ 9 030 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/20/2017 Time Sampled: 0735 Sampled By: L. Estes Time Started Aeration: 0740 Time Stopped Aeration: 0906 Time Analyzed: 0907 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 47 mins. ) Total time of test includes the time sample was aerated. 800/900d We9Z:ll 8LOZ 9 090 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 2/21/2017 Time Sampled: 0820 Sampled By: L. Estes Time Started. Aeration: 0822 Time Stopped Aeration: 0959 Time Analyzed:1000 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 55 mins. ) Total time of test includes the time sample was aerated. 800/LOOd WRH:: [ 8LOZ 5 300 Specific Oxygen Uptake Rate Sour Test Corpening Creek Wastewater Lab Marion, N.C. Method: SM 2710 B-1997 Date: 3/3/2017 Time Sampled: 0605 Sampled By: L. Estes Time Started Aeration. 0608 Time Stopped Aeration: 07" Time Analyzed: 0745 Analyzed By: R. Carter Total Time of Test: < 2 hrs.(1 hr. 55 mins. ) Total time of test includes the time sample was aerated. 800/800d WE9Z:ll KOZ 9 390