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HomeMy WebLinkAboutWQ0019960_Annual Report_20150223City of Marion City of Marion, NC Waste Water Treatment Plant 2014 Annual Report Land Application Program NC Permit No. WQ0019960 GENE® bivision of Water Resources FEB 2 3 2015 Water Quallty Regional Operations Asheville Regional Office �p RECEIVED FEB 13 2015 DWR SECTION INFORMATION PROCESSINd UNiT A1N11 V AL ],^INV ArrLIUA I ILV1V %_JU K I III11;A 11V1V r VK1Vl WQ Permit#: WQ0019960 County: Facility Name (as shown on permit): McDowell Year: 2014, Land Application Operator: Southern Soil Builders, Inc. _Phone: 336• 957-8909 Land application of residuals as allowed by the, permit occurred during the past calendar year? Yes U No --If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part Ai!- ResidualsApplication Summary: Total number of application fields in the permit: 8 Total number' of fields utilized for land application during the year:' .6 Total amount of dry tons applied during the year for all application sites: 117.23 Total number of acres utilizes for land application during the year: 113.7 Part R- Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (includ ng'but not limited to items 1-13 below) issued by the Division of Water Resources. 21 Yes No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the, limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are'aaached. 5) All. other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did'not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .I 105(a) or the Pollutant Loading Rates in 15A NCAC 02T 1105(b) (applicable to 40 CFR Part 503 regulated facilities). . 7) Alt general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All, monitoring and reporting.requirements in 15A NCAC 02T. 1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All: operations and maintenance requirements in the permit were complied with or, in the case of a deviation,; prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals as specified in the permit. 12) No.runoff of residuals from the application sites onto adjacent property or nearby surface waters. has occurred. 13) All•buffer requirements as specified on the permit were maintained during each application of residuals. Part'C : Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false'information, including the possibility, of fines and imprisonment for knowing violations." vr z- - Is Permittee Name and Title (type or print) SSature of Per ' ee Date of Date of (if different from Permittee) (if different from Permittee and Preparer) *.Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2008) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional -parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0019960 Laboratory: 1) ETS Facility Name: City- of Marion 2) Residual Source WQ # or NCO031879 3) NPDES #: 4) WWTP Name: Corpening Creek WWTP 5) Residual Analvsis Data Parameter (mpg) Cone. Limit m a Sample or Composite Date 4-7-14 Percent Solids (%) NA 2.5 ►- Arsenic 75 19.9 Cadmium 85 7.95 Copper 4,300 343 v Chromium NA NA Lead 840 49.8 Mercury 57 0.8 Molybdenum 75 19.9 Nickel 420 14.2 Selenium 100 19.9 Zinc 7,500 912, Total Phosphorus NA 27400 - TKN NA 5580.0. Ammonia -Nitrogen NA 2000 Nitrate and Nitrite NA 949.97 rur surrace aisposai iacuines me ceumg concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law; that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the. information submitted. I am aware that there are significant penaltun for -gubmu-in--gb f- »lep .1-1:4.V4r r---.Qn.7 ' � 1- jVxP7jivauaJl 11GA u 11PHISVl11er1LlU-1 knowing Vlolatlons.. Sli6attire of Preparer * Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF. (12/2006) L-11\i\UTAJL,iViL'lAL311L+LLLVALPIUNkTk')UlV11V1AKY IVVK1V1" is Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): Permit #: WQ0019960 _ Cation Exchange Capacity (non 503 only): Operator: Nancy Ross _ Owner: Nancy Ross - Predominant Soil Series: Acres Used: 19.4 Acres Permitted: 19.4 Site #: Residual Analysis Data (Heavy Metals and Total Phosphorus use me/kg, 30.50 Hayesville R-01 Field #: R-01 % Solids use Raw Percent #): . • Com- posite Date N N o n E� ,00 W.M. ® • • �_ __� ___ • . • . •ONE MEN Annual Heavy Metal Vield Loadmgs (Calculated in lbs/acre): Total 1 21 3 4 5 6 7 L8J 9 10 111112 App. Event 1.57 4 Arsenic 0.063 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.000 1 0.000 0.063 Cadmium 0.025 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.000 0.025 Copper 1.078 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.078 Chromium ###### 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead ' 0.157 0.000 0.000 0 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.157 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0000 0.003 Molyb0.063 denum denum 0.000 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Nickel 0.045 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.045 Selenium 0.063 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.063 Zinc 2.867 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 2.867 Total Phos- 86.146 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 86.146 horus rrr •r 1 cerEuy, under penalty of law, that tams document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sign Kure of Land Applier Date DENR FORM MFI RF (iq/gnnm Li1N1vUALi NMIAL6 r'1ELL LVAl)MG SUMMARY FORM* ' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): _ 16.26 Permit #: , WQ0019960 Cation Exchange Capacity (non 503 only): _ Operator: Nancy Ross - Owner: Nancy Ross _ Predominant Soil Series: _ Mayesyille Acres Used: 22.9 Acres Permitted: 22.9 Site #: R-02 Field #: R-02 Residual Analysis Data (Heavy Metals and Total Phosnhorus use mu/kff_ 0/., Cnl;rlc nen R.ur Pot•..ot,+.4N. Sample 1 2 - 3 41 5 -- 1-- 6 -- --- ��- ---a'--b7 l,VRlb rr). or 7 8 9 10 11 12. Com- posite Date 4/7/14 % Solids 2:5 Arsenic 19.9 _ Cadmium 7.95 Copper 343 Chromium NA Lead 49.8 _ Mercury 0.8 Molyb- denum 19.9 _ Nickel 14.2 Selenium 19.9 Zinc 912 Total Phos- 27400 horus rAuuuai iiUavy iV1Gy2U JVjIVIU UUUUIHP_S (Calculated In Instacrp)' Total 1 _2 3 4 15 6 7/ 8 9 10 11 12 DT/Ac./ I o App. �I 0 Event 0.71 Arsenic 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0.00 0.000 0.000 0.028 Cadmium 0.011 0.0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.487 0.000. 0.000 0.()00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.487 Chromium ###### 0.000 0.000 0.000 6.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000, ###### Lead 0.071 0.000 0.000 0.(100 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.071 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- denum 0.028 0.000 0.000 O.C100 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Nickel 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.02 0 Selenium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.02 Zinc 1.295 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.295 Total Phos- 38.908 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 38.908 horus "I certify under anal ' f 1 th t ' d y w , p to a, a t Ins ocument was prepared under my direction or supervision in accordance with a system designed to: assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of La Applier Date M r1FAlp Gn0r%A ival cc: r�nrnnnn_� AuviN UAL i UlALS FIELD LOADING SUMMARY FORM* ' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): _ 12.88 Permit #: WQ0019960- Cation Exchange Capacity (non 503 only): _ Operator: !Mario DeLuca. Owner: Anna Deebold Predominant Soil Series: _ Hayesville Acres Used: 16 Acres Permitted: _ 16 Site #: K-01 Field #: _ K-01 Residual Analvsis Data (Heave Metals and Tn+nl Phnenhnrne ,men .. /i_ o/ Q_i.,A .. n Sample or Com- posite Date 1 4/7/14 2 3 4 5 5 7 8 9 10 11 12 % Solids 2.5 Arsenic 19.9 _ Cadmium 7.95 _ Copper 343 Chromium NA Lead 49.8 _ Mercury 0.8 Molyb- denum 19.9 _ Nickel 14.2 Selenium 19.9 Zinc 912 Total Phos- horus 27400 ■ . . � . .. . A...... -I LT,..._._.IS-4-,_1 r+__7.7 T Total 1 21 L3J_ 4 151 1 5 7 181 19 1111 112J DT/Ac./ f App. 0 Event 0.81 y Arsenic 0.032 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.032 Cadmium 0.013 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 0.552 ` 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.552 Chromium ###### 0.000, 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.080 0.000i 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0 _ _ 0.080 Mercury 0.001 0.00.0 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.001 Molyb- denum 0.032 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.032 Nickel 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.023 Selenium 0.032 0.000'. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000' 0.032 Zinc 1.468 0.000 0.000 0.()00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 t 0.000 1.468 Total Phos- 44.114 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 44.114 horus nnnnl4-� ln... = 411-. ,7,...__�_-. -_-_ _ nT oPrfifv nndar __ ­. , ___ »....»...--- ,.- F-. F", %,u UUUUX MY U11VU UH ur supervision In accordance . with a system designed to assure that ilualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier, . Date r%mAln r-e' nRA AEI- ^ram .�.r..... AivlvuAL iv KIALS FIELD LOADING SUMMARY FORM* t Attach this form to the corresponding Field" Loading Summary Form to be submitted in Annual ]Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 31.18 01 Permit #: WQ09960 Cation Exchange Capacity (non 503 only): _ Operator: Mario DeLuca Owner: _ Anna Deebold _ Predominant Soil Series: _ Hayesyille Acres Used: 35.8 Acres Permitted: - 35.8 Site # K-02 Field #: K-02 Residual Analvsis Data (Heave 1 wf9le anti rn+.i ni n - Sample or Com- posite Date 1 4/7/14 2 3 4 L5 L6j _0V. r,,z.r�, .0 .Mils 9 use 10 tcaw rercent 11 1*): 12 % Solids 2.5 Arsenic 19.9 Cadmium 7.95 Copper 343 Chromium NA Lead 49.8 _ Mercury Molyb- denum 0.8 - 19.9 _ Nickel 14.2 Selenium 19.9 Zinc 912 Total Phos- horus 27400 - Annual Heaw Metal Pipet_.- ---- Total I1 L21 L3J_4I DT/Ac./ J A 5 6 7 8 9 10 11 12 App. J 0 Event 0.87 v Arsenic 0.035 1 0,000' 0.000 0.000 0.0.00 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.035 Cadmium 0.014 0.000! 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.014 Copper 0.598 0.000; 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.598 Chromium 44#### 0.000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ###### Lead 0.087 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.087 ✓ Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.0001 0.001 Molyb- 0.035 0.000 0.000 0.000. denum - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.035 Nickel 0.025 0.000 0..000 0.000 0 000 0.000 0.000 0.000 0.000 0.000 0.0 00 0.000 0.025 Selenium 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Zinc 1.589 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1,589 Total Phos- 47.731 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 47.731 horus "I certify, under penalty of law, that this document was prepared under my direction or with a system designed to, assure that qualified personnel properly gathered and evaluated supervision in accordance I am aware that there are' significant for the information submitted. penalties submitting false information, imprisonment forknowing violations". including the possibility of fines and y- Signa re of Land Applier ' Date J Mr - __ - . . .._. _- . t&i'NII IAIj IV 1AM5 rirMED LVAJUL Iti 6WV11V1AKY FVKMI "Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): _ 14.23 Permit #: iWQ0019960 - Cation Exchange Capacity (non 503 only): _ Operator: ,James Fisher - Owner: _ James Fisher Predominant Soil Series: Hayesville Acres Used: 21.4 Acres Permitted: 11.4 Site #: F-03 Field #: F-03 Residual Analysis Dat` (Heavy Metals and Total Phosphorus use m /k ° ... . '�'i1 d i7 �'] E] Q7 93 0 Com- posite Date, Total P mom h Hnnual neavy ivietar rieia Loadrnps (Ualcuiated in lbs/acre): Total 1 2 { 1 3] 141 j 5 6 7 8 9 10-J 11ii-12 DT/Ac./ I o App. �f Event 1.25. Arsenic 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000' 0.050 Cadmium 0.020 0.000: 0.000 O.Ci00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Copper 0.856 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 0.856 Chromium ###### 0.000; 0.000 0.Ci00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' ###### Lead 0.124 1 0.000 s 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.124 Mercury 0.002 0.000 ' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 i Molyb- enum denumd 0.050 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Nickel 0.0335 0.000 0.000 0.000 0.060 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Selenium 0.050 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.050 Zinc 2.276 0.000, 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 2.276 Total Phos- 68.390 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000' 68.390 horus "T ..a,.... is . ! r_�_ .L_. �■�•_ ,_ Wly, uuuva Ncuaaiy vi law, LuaL uus uucument was prepared under my airection or supervision in accordance with a system designed to; assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that thereare significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". IS Signature of Land Applier ; Date nFNR FnRhn NAPI .F (1,)i,)nnrN U A1V1V UAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 12.19 Permit #: ! WQ0019960- Cation Exchange Capacity (non 503 only): Operator: James Fisher Owner: James Fisher Predominant Soil Series: Hayesville Acres Used: 8.2 Acres Permitted: 8.2 Site #: F-04 Field #: F-04 Residual Analysis Data (Heavy Metals and Total Phosphorus use mag, % Solids use Raw Percent #): Sample or LU 1 2j 3 4 5 6 7 8 9 10 11 12 Com- posite Date 4/7/14 1 % Solids 2.5 Arsenic 19.9 j Cadmium 7.95 Copper 343 Chromiu NA } Lead 49.8 Mercury Molyb- denum 0.8 19.9 { Nickel 14.2 Selenium 19.9 I - Zinc 912 Total Phos- horus Annual 27400 Hones Mpfa Ti';pla I T .,�,a;,, - e� �r .� __�_�_ Total DT/Ac./ App. Event 1 -1-21 ( V 1.49 j k 1415 " 1" JLLYJ/aut 6� Up 7 8 9 10 of ✓ 11 12 y y Arsenic Cadmium 'Copper Dhromiu Lead 0.059 0.024 1.020 ###### 0.148 1 0.000; 1 0.000': 0.000 � 0.000' 0. 00 0.000 0.000 0.000 0.000 0.000 0.00.0 0.000 0.000 0.000 0.0100 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000', 0.059 0.000 0.000 0.000 OA24 0.000 0.000 0.000 1.020 0.000 0.000 0.000' ###### 0.000 0.000 0.000 0.000 0.148 Mercury. Molyb- denum 0.002 0.059 0.000 0.000 0-000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0-.000 0.000 0.000 0.000 0.000 0.000 0,002 0.000 0.000 0.000 0.000 0.059 Nickel Selenium 0.042 0.059 0.0001 0.00.0 i 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 0.000 0.000 0.000 0.000 0.042 0.000 0.000 0.000 0.000 0.059 Zinc Total Phos- bhorus 2.712 81.488 0.000 , 0.000 i 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 O 000 0.000 0.000 2.712 0.000 0.000 0.000 0.000 81.488 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of LanApplier 11 Date ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Nancy Ross Operator: Nancy Ross Crop 1 Name: Vescue WQ Permit #: WQ0019960 Annual Dry Tons Applied: 30.4931 Field #: R-01 Site #: R-01 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 1 202 Crop 2 Name: Acres Utilized: 19.4 Acres Permitted: 19.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° y Volume applied Volume Residual Sources Soil Cond. Preci . p a Ks C o _Z Y Nitrate Name of Crop Type ° enter one Solids/ ( ) o /o Applied per DES #, W # (NP Q , Past 24 10 9 w TKN o and PAN Applied pp Receiving Residual +, o Liquid Solids Acre Fert., Animal D ( n', Hrs. ' o w , . 0 N' �' j * J °4 o Nitrite lbs/acre ( ) Application Q Cu. Yds Gallons (Dry TonslAc) Waste, etc) We Moist) inches Q. ^ * 0 * o o * * ~= mg/kg �• mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 5-2014 1 292500 2.5 1.572 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 56.868 NA Fescue 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 . 0.000 0.000 0.000 0.000 0.000 500 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form). 'OTALS: 01 292500 As Cd Cu Cr Pb A Ni Se Zn P 56.868 0.000 Lime A %nnual lbs/acre 0.063. V 0.025 1.078 ####### 0.157 O3 t20 0.045 0.063 2.867 86.146 Date lbs/ac 'rior Years Cumulative lbs/ac 0.064 0.127 i/ 36 0.043 0.068 34 7.723 ' 8.501 NA 1.348 #######' 1338 1.203 1.360 ' 267 0.05 0.053 15 1.264 1 NA 0.495 0.540 ' 374 0.102 6.165 +�2498 89 19.6 2.467 10-14 2000 :urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'enmt PAN Limit 1 st/2nd Crop 202 _rJ '1 certify, under penalty of law, that this document was prepared under my direction or.supervision in accordance with a system designed to assure that uahfied personnel properly gathered and evaluated the information submitted_. I_am aware, that there are_significant-penalties_ for- submitting-false- __- 1 �_ P __ P 1? Y g _ _ _ � _ nformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Nancy Ross Operator: Nancy Ross Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: R-02 Acres Utilized: 22.9 Annual Dry Tons Applied: 16.2630 Site #: R-02 Acres Permitted: 22.9 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 9.Volume 0 ° Q applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Sod Cond. (Dry, Moist) Precip. Past 24 Hrs. inches > 4 o w o - � ?: C' �, 9 m � CD w TKN mg/kg Z o °4 ° r, mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of CropT ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 5-2014 156000 2.5 0.710 WQ0019960 dry 0 s 0.5 0.3 55800 2000 1 949.97 25.694 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 _ Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): oTALs: _ 01 156000 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 25.694 0.000 Lime A , �nnuallbs/acre 0.028 0.038 0.066 36 0.011. w 0.037. 0.048- 34 0.487 6.481 6.968 NA ####### 0.0278 #######' 1338 0.071 0.796 0.867 1 267 0.001 0.326 0.327 ' 15 1 0.028 0.715 0.743 NA 0.020 0.354 0.374 1 374 0.028 0.057 0.085 89 1.295 14.75 16.045 2498 38.908 ' Date s/ac 3rior Years Cumulative lbs/ac 10-14 2000 .urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit lst/2nd Crop _ _ ._ . _.. . . _ :.1 262 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for_submitting nformation, including the possibility of fines and imprisonment for knowing violations." / 'P _ ��_q- *Application Method: S - Surface, IN - Injection, INC - Incorporation /7--__ �� **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate r DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: Anna Deebold Operator: Mario DeLuca Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: K-()l Annual Dry Tons Applied: 12.8749 Site #: K 01 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 16 Acres Permitted: 16 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ti +, Q Volume applied PP enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre D Tons/Ac (Dry ) Residual Sources DES #, W # Q ' Fert., Animal Waste, etc) Soil Cond. (Dry, We Moist) Precip. Past 24 Hrs. inches a t, co - o' o �; Z o � - * N ° � 7y �, ?= '. o :Z TKN mg/kg Z q ao O CD R. mg/kg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of CropType YP Receiving Residual Application PP Crop 1 Crop 2 Crop 1 Crop 2 12-14 123500 2.5 0.805 WQ0019960 dry 0 s 1 0.5 0.3 55800 1 2000 949.97 29.113 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: Q1 1235001 As Cd Cu I Cr Pb Hf4 Mo Ni Se Zn I P 29.113 0.000 Lime Applied \rmuallbs/acre 0.032 .161 0.193 36 0.013 0.114 v.127 34 0.552 17.065 1 i 7.o.i 7 ' NA ####### 0.94 ###### 1338 0.080 2.215 2.295 267 0.001 0.102 0.103 15 0.032 2.442 2.474 NA 0.023 1.015 1.038 374 0.032 0.245 0.277 89 1.468 39.249 40.717 2498 44.114 Date lbs/ac 'rlor Years Cumulative sac 1 :ur r ent Cumulative ibs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit 1st/2nd Crop - 202 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the i_nformation_submitted. I am aware that there are significant penalties for_ submitting -false.. nformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date **" Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion WQ Permit #• WQ0019960 Field #: V Land Owner: Anna Deebold _ _02 Annual Dry Tons Applied: 31.1708 Acres Utilized: 0 �S,g Operator: Mario DeLuca Site #: K-02 Acres Permitted: 35.8 Predominant Soil Series: Hayesville Cation Exchange Capacity g p ty (non 503): Crop 1 Name: Fescue _ Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN: o Volume applied Volume Residual Sources Soil Precip. a o Z Y o(enter one) Solids/ o /o Applied per (NPDES #, WQ#, Cond. Past 24 -a c �' w `; TKN o Nitrate Name of Crop Type PAN Applied Q Liquid Solids Acre Fert., Animal (Dry, Hrs. o w N' �, w o and ReceivingResidual (lbs/acre) Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, a: �. .� w o• � * •* � w Nitrite Application WQ0019960 Moist) dry inches 0 a m /k s s m !k 9 9 m /k 9 9 Crop 1 Crop 2 Crop 1 Crop 2 12-14 ' 299000 2.5kjO.811 s 0.5 0.3 55800 2000 949.97 31.502 NA Fescue.000.0000.000 0.000000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o.000 0.0oo 0.000 0000 0.000 0.000 o to.000 0.00 00.000 iviru,a:l Ul GyyUUUI - knnual lbs/acre ?rior Years Cumulative lbs/ac current Cumulative lbs/ar_. ?ermitted C. P. L. R. * * * * 'ermit PAN Limit 1 st/2nd As Residuals Cd Applications Cu totals Cr on FORM Pb FSF Hg supp ( attach Mo FORM Ni FSF supp Se to this form): Zn P 31.502 0.000 Lime 0.035 0.014 0.598 ####### 0.087V 0.001 0.035 0.0�O.035 1039.914 f1 L067 374 !1 1 ,,.278 89 1.589 t Cn 4,.503U. 2498 47.73]0.159 Date I 0.117 17.67 0.997 2.29 0.105 2.452 194 n 131 , Q ��o_ I lJ6 1 %_Ll� 1 u/ 36 34 NA 1338, 267 15 NA _. _. certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information submitted I am aware that there are significant penalties for submitting false__ .... nfar-mation includin -the ossibili - - --------_____;- _ __ . _. g p ty-offines-and-imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: City of Marion Land Owner: James Fisher Operator: James Fisher Crop 1 Name: Fescue PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0019960 Field #: F-03 Annual Dry Tons Applied: 14.2301 Site #: F-03 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres iltilized: 11.4 Acres Permitted: 11.4 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° ° rZ ° A Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources DES # W # (NP Q , Fert., Animal Waste, etc) Soil Cond. �D> We Moist) Precip. past 24 Hrs. inches a b o w n o `y N' �, o o w C Pi " CD * - TKN mg/kg o °Q ° o 0 � E mg/kg ° Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of CropType Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 12-14 136500 2.5 1.248 WQ0019960 dry 0 s 0.5 0.3 55800 2000 949.97 45.162 NA Fescue 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.000 0.000 1 0.000 0.000 0.000 0.000 C.CCC 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: 0 136500 AS Cd Cu Cr Pb H Mo Ni Se Zn P 45.16 0.000 Lime Applied �rmuallbs/acre 0.050 0.042 0.092 36 0.020 0.018 0.038 34 0.956 1 2.531 1 3.387 10#0011 NA ####### 1.763 D38 0.124 0.475 0.599 267 0.002 0.019 0.021 Lr 15 0.050 0.09 0.140 1 NA 0.035 0.219 0.254 1 374 0.050 0.038 0.088 89 2.276 9.034 11.310 2498 68.390 Date lbs/ac 'rior Years Cumulative lbs/ac :urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** 'ermit PAN Limit lst/2nd Crop _ 202 `I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that Iualified_personnel_properly_gathered-and_evaluate_d_theinformation_submitted._I..am.awar_e_.that_there.ar_e_significant-penalties-for submitting -false ----- - nformation, including the possibility of fines and imprisonment for knowing violations." Al r Signature of Land Applier 0 _,j ,,j- Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate r DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Land Owner: James Fisher Operator: James Fisher Crop 1 Name: Fescue WQ Permit #: WQ0019960 Field #: F-04 Annual Dry Tons Applied: 12.1973 Site #: F-04 Predominant Soil Series: Hayesville Crop 1 Max. PAN: 202 Crop 2 Name: Acres Utilized: 8.2 Acres Permitted: 8.2 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Y 0 o Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet,ao Moist) Precip. Past 24 Hrs. inches a ��, 5 o o w o �y �; C' � 4 ;o x N TKN mg/kg Z q �o o mglkg Nitrate and Nitrite mglkg PAN Applied (Ibs/acre) Name of CropType Receiving Residual APP lication Crop 1 Crop 2 Crop 1 Crop 2 12-14 117000 2.5 1.487 WQ0019960 dry 0 s 1 0.5 0.3 55800 2000 949.97 1 53.817 NA Fescue 0.000 0. 000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): 'OTALS: 01 117000 ' As Cd Cu I Cr Pb I Hg I Mo I Ni I Se I Zn I P 53.8.17 0.000 Lime lied knnuallbs/acre 0.059 0.066 0.125 36 0.024 0.035 0.059 34 1.020 6.114 ' 7.134 NA ####### 2.109 1 ### ##' 1338 0.148 0.904 1 i.052 267 0.002 0.036 0.038 1 15 0.059 It 0.165 1 0.2244 NA 0.042 0.409 0.451 374 0.059 1 0.076 0.135 89 2.712.4 14.495 i7.20r 2498 81.488 DatV lbs/ac 'rior Years Cumulative lbs/ac :u�,ent 'Cumulative lbs/ac ' 'ermitted C. P. L. R.**** 'ermit PAN Limit lst/2nd Crop 202 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that lualified personnel properly gathered and evaluated the information_ submitted. I am aware that t_here_ are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2005) i _ Environmental Testing Solutions, Inc. Project name: Marion WWTP Collection date: 14-Apr-14 Date received: 14-Apr-141 Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828)350-9368 Project number: Sample identification: CC Sludge #4 - Grab Sample number: 140414.502 115180 Parameter Method Result RL, Units Date Analyst ]Footnotes _ Analyzed %TS SM 2540 G 2.6 0.10 % 14-Apr-14 KEK Mulitple'1•ube Femientation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KEK Sample identification: CC Sludge #5 - Grab Sample number: 115181 Parameter ]Method Result RL Units Date Analyst Footnotes _ Analyzed WFS SM 2540 G 2.6 0.10 % 14-Apr-14 KEK - Mulitple Tube Fermentation Procedure SM 9221-E 5200_ 4.7 MPN 7-Apr-14 KEX Sample identification: CC Sludge 96 - Grab Sample number: 115182 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.6 0.10 % H-Apr-14 KLX - Mulilple Tube Fennentation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KEK Sample identification: CC Sludlze #7 - Grab Sample number: 115183 Result RL Units,Date Analyst Footnotes Parameter Method Analyzed %TS SM 2540 G 2.6 0.10 % 14-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 9221-E 5200 4.7 MPN 7-Apr-14 KEK Footnotes RL = Reporting Limit. Values are reported down to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 990.53 Signature: NC Drinking Water Certification Number: 37786 This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, inc. The results in this report relate only to the samples submitted For analysis. r, Wit.. } :( Environmental Testing Solutions, Inc. Prqiect name: Marion WM"rP Collection date: 7-Apr-141 Date received: 7-Apr-141 Certificate of AnalyMs Sample identification: CC Sludge #1 - Grab PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 140407.503 Sample number: 114920 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.5 0.10 % 7-Apr-14 KEK Mulitple "Cube Fermentation Procedure SM 9221-E 19500 4.5 MPN , 7-Apr-14 KEK Sample identification: CC Sludge #2 - Grab Sample number: 114921 Parameter Method Result RL Units Date Analyst Footnotes Analyzed %TS SM 2540 G 2.6 0.10 % 7-Apr-14 KEK Mulitple Tubc Fermentation Procedure SM 9221-E 59800 4.7 MPN 7 .Apr-t4 KEK Sample identification: CC S1uolge #3 Grab Sample number: 114922 Parameter Method Result RL Units Date Analvsi Footnotes _ Analyzed %TS SM 2540 G 2.6 0.10 % 7-Apr-14 KEK Mulitple Tube Fermentation Procedure SM 9221-E 33800 4.7 MPN 7-Apr-14 KEK v Footnotes: RL = Reporting Limit. Values are reported dovNm to the Reporting Limit only. Date reviewed: NC Certification Number: 600 Data reviewed by: Kelley E. Keenan SC Certification Number: 99053 Signature: NC Drinking Water Certification Number: 37786 This report should not be reproducdd, exept in its entirety, I consent �ol �P.nvirontnental Testing Solutions, Inc. 055' The: results in this report relate only to the samples submitted for analysis. hFFl,h� e G 7- -nr}•} .......... L Environmental Testing Solutions, Inc. Project name: Marion W W'Fp Collection date: 7-Apr--14 Date received: 7-Apr.44 Sample identification: CC Sludge - Grab Certificate of Analysis PO Box 7565 Asheville, NC 28802 Phone: (828) 350-9364 Fax: (828) 350-9368 Project number: 140407.504 Sample number: 1I4923 Parameter Method Result RL Units Date Analyst Footnotes Analyzed Percent Solids SM 2540 G 2.50 0.10 % 9-Apr-14 ASI3 1 Mercury 747113 0.80 0.79 mg/kg 16-Apr.14 DER I Aluminum 601OC 11800 1990 mg/kg 10-Apr.14 MEC ] Arsenic 6010C <19.9 19.9 mg/kg 10-Apr.14 MEC 1 Cadmium 6010C <7.95 7.95 mg/kg 10-Apr-14 MEC 1 Calcium 6010C 13300 1990 mg/kg 10-Apr-14 MEC 1 Copper 6010C 343 7.95 mg/kg 10-Apr-14 MEC 1 Lead 601OC 49.8 19.9 mg/kg 10-Apr-14 MEC 1 Magnesium 6010C 6320 1990 mg/kg 10-Apr-14 MEC 1 Molybdenum 6010C <19.9 19.9 mg/kg 10-Apr-14 MEC 1 Nickel 601OC 14.2 7.95 1n g/kg 10•Apr-14 MEC 1 Potassium 601OC 7010 39.8 mg/kg 10-Apr-14 MEC 1 Selenium 601OC <19.9 19.9 mg/kg I0-Apr-14 MEC 1 Sodium 601OC 2850 1990 mg/kg 10-Apr-14 MEC 1 Zinc .6010C 912 19.9 mg/kg 10-Apr-14 MEC I ,cNitrate- Nitrittnasrl��,'j -949:9-71 160.59 mg/kg 16-Apr-14 LDP/REH 1, 3 Total Phosphorus 601OC 27400 795 mg/kg 10-Apr-14 MEC l Tvital--I 351.2 �6580JOA 1070 mg/kg 23•Apr-14 LDP I Total i litrogen 1 -,zCalculatiarlY -,56-800 1070 mg/kg 23-Apr-14 LDP I AtnxnaniaNitrogen SM 4500 NH3 D �2000& 150 mg/kg 11-Apr-14 KEK Percent Solids pH in Liquid SM 2540 G 2.7 % 7-npr-14 KEK SW 846 9045C 6.6 - S.U. 7-Apr-14 KEK 4 Reactive Cyanide 335A <0.134 0.134 mg/kg 23-Apr-14 ECHEM 2 Reactive Sulfide SM 4500 S D 0.67 mg/kg 23-Apr•14 ECHEM 2 Ignitabilit}, SW 846 1010 >212 212 OF 11-Apr-14 ECHEM 2 N-PAV Calculation 1645950 29-Apr-14 KEK Sodium Absorption Rate Calculation 46 29-Apr-14 KEK Footnotes: RL = Reporting Limit. Values are reported down to the Reporting Limit only. 1. Sampie analyzed by -Rogers & Callcott Environmental. 2. Sample analyzed by`Enviro Chemists, Inc. 3. Methods EPA 921 OA and SM 450ON0213 by LDP and REH. 4. Sample analyzed outside ihold time. Date reviewed: dy 241-(N Data reviewed by: Kelley E. Keenan Signature: NC Certification Number: 600 SC Certification Number: 99053 NC Drinking Water Certification Number: 37786 This report should not be reproduced', exept in its entirety, without the written consent of Environmental Testing Solutions, Inc. m The results in this report relate only to the samples submitted for analysis. Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Specific Oxygen Uptake Rate, SOUR Facility Name: Cor enin . Creek Biosolids Permit Number: WQ 0019960 Digester Temperature: Sampling Date/Time: 4/28/14 0825 Sampled By: Lee:Estes Analysis Date/Time: 4/28/14 0954 Analyzed By: R. Carter Sample -Volume: Beginning Temperature: End Temperature: Dissolved Oxygen Level �illiliters� 6-Dry-Solids egrees Celsius / egrees Celsius t/ Slope: 0.3 Intercept: 6'.2' Correlation Coefficient: 1.0 Oxygen Uptake Rate: 15.87 mg Oxygen/hr Ambient Specific Oxygen Uptake Rater 1.89 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.48 mg Oxygen/g/hr Instructions: Enter Data in- the Blue Boxes-. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Coreenin2 Creek Biosolids Permit Number: WQ 0019960 Date: 4/25/2014 / Digester Temperature: 16 +� Sampling Date/Time: 4/26/14 0815 Sampled By: Lee -Estes Analysis Date/Time: 4/25/14 0956 Analyzed By: R. Carter Sample Volume: - 1000 milliliters Total -Solids -0.81 % Dry Solids Beginning Temperature: 25 degrees Celsius End Temperature: 25 degrees Celsius Slope: 0.3 Intercept: 7.0 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 15.77 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.95 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.53 mg Oxygen/g/hr Instructions: Enter Data in the B16(r Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Na Biosolids Permit Num Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: __ -,Total Solids: Beginning Temperature: End Temperature, Dissolved Oxygien Level Slope: Intercept: Correlation Coefficient-, 4 - 1000 milliliters =-.:0..7.9 %- Dry Solids 25 degrees Celsius ✓ 25 degrees Celsius 0.2 6.7 1.0 Oxygen Uptake Rate: 13.95 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.77 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.38 mg Oxygen/g/hr Instructions:, Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically, Specific Oxygen Uptake Rate SOUR Facility Name: Corpeninq Creek Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume: .....Total. Solids: Beginning Temperature: End Temperature: Time (minutes) 0 1 2 3 4 5 6 7 -8 9 10 11 '12 13 14 15 4 091 milliliters W Dry Solids degrees Celsius degrees Celsius Slope: 0.3 Intercept: 6.9 Correlation Coefficient: 1.0 Oxygen Uptake Rate: 16.99 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.89 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rater 1.48 mg Oxygen/g/hr Instructions: Enter Data in the Blue,Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name: Corpening Creek Biosolids Permit Number: VV 0019960 Date: 4/3/201 Digester Temperature: Sampling Date/Time: 4/3/14 Sampled By: Lee-Esi Analysis Date/Time: 4/3/14 Analyzed By: R. Carh Sample Volume: ------ _.Total olids .--_- Beginning Temperature: End Temperature; Slope: Intercept: Correlation Coefficient: Oxygen Uptake Rate: Ambient Specific Oxygen Uptake Rate: Average Temperature: Temperature Correction Factor: 10 d A milliliters %o.D y Solids.degrees Celsius degrees Celsius 0.3 7.0 1.0 16.45 mg Oxygen/hr 1.91 mg Oxygen/g/hr 25 degrees Celsius 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate: 1.50 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Uptake Rate SOUR Time (minutes) 0 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 Facility Name Biosolids Permit Number Date Digester Temperature Sampling Date/Time Sampled By Analysis DatefTime Analyzed By Sample Volume Total. Solids :Beginning Temperature. End Temperature Coreening Creek WQ 0019960 4/2/2014 18 412/14 0817 Lee_Estes 4/2/14 0930 R. Carter •1000 - --:_ -w 25 25 Slope: 0.3 Intercept: 7.5 Correlation Coefficient: 1.0 t/ milliliters %.Dry Solids 9egrees Celsius legrees Celsius Oxygen Uptake Rate: 17.45 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 2.01 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature Correction Factor: 0.783526166 Temperature Corrected Specific Oxygen Uptake Rate:= 1.57 mg Oxygen/g/hr Instructions: Enter Data in the Blu"Ei�Boxes. The Calculation and the Spreadsheet execute automatically. Specific Oxygen Vptake Rate SOUR Facility Name: Biosolids Permit Number: Date: Digester Temperature: Sampling Date/Time: Sampled By: Analysis Date/Time: Analyzed By: Sample Volume.j Beginning Temperature: End Temperature: - Time (minutes) 0 1 2 3 .4 5 6 7 .8 9 10 11 12 13 14 15 Creek milliliters %-Dry.Solids degrees Celsius degrees Celsius Slope: 0.3 Intercept: 6:9 Correlation Coefficient: 1;0 Oxygen Uptake Rate: 15.30 mg Oxygen/hr Ambient Specific Oxygen Uptake Rate: 1.72 mg Oxygen/g/hr Average Temperature: 25 degrees Celsius Temperature'Correction Factor: 0.783526166. Temperature Corrected Specific Oxygen Uptake Rate: 9.36 mg Oxygen/g/hr Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically. 7L-,irachem"': ANALYTICAL &,CONSULTING CHEMIISTS Environmental Testing Solutions, Inc. Post Office BOX 7665 Asheville NC 28802 Attention: Kelley Keenan (ETS) Environmental Chemists, Inc.4. 6602 Windm ll Way ° Wilmington, NC 28405 (910) 392 0223 (Lab) • (910) 392-4424 (Fax) 710 Bowsertown Road ° Manteo, NC 27954 (252) 473-5702 NCDENR: DWQ CERTIFICATE #94. DI.S CERTIFICATE 4137729 Date of Report: Apr 24, 2014 Customer PO #: Report #: 2014-04144 Report to: Kelley Keenan (ETS) Project ID: Marlon WWTP Lab ID Sample ID: Collect Date/Time Matrix Sampled by 14-09977 • Site: CC -Sludge 4/7/2014 7:05 AM Solid/Sludge Client Test Method Results Date Analyzed RCI Cyanide EPA=A <0.134 mg/kg 04/23/2014 Sulfide SM',W0 S n 0.67 mg/kg 04/23/2014 Ignitability SW M method 1010 >212 °fi 04/11 /2014 Comment: Reviewed by: �-- 2 Report #:: 2014-04144 Pago 1 of 1 � t11111`1Au rA1J11VkYh1N AM) VECTOR ATTRACTION REDUCTION FORM (02T Rules) acility Name: City of Marion I WQ Permit Number: WQ0019960 WWTP Name: Corpeiiin'g'Cree — 7-�- - -� Mo nitoring Period: From 1/1/2014 NPDES Number: NC0031819 To 12/31/2014 Path2Reduction 1 — _gen Redu tion (15A NC.AC, 02T Please indicate level aChi6ved- and alt ernativeTpe -formed:Class A: AltAfim6/tem ( Alt B Alk Treament)U 'Alt. C (Prior Testing) Alt-D (No Prior Test) Lj Process to Further Redude Patliogeli_fl__ If applicable to alternative perfdrme (Class A CompostHeat-------- ((Cla only) indicate "Process to Further Redu,ce'Pathogefis!': MP� 'Drying Q Heat Treatment ElThermophilic El — Beta Ray ❑ Gamma Ra n Y❑ Pasteurizatio ❑ Class B: JAlt. (1):Fecal Density Alt. (2) Process to Significantly Reduce Pathogen If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization 0 Air Drying Cl COm ostin 13 Aerobic Digestion LjAnaerobic Digestion .... .......... ........ .......... 11applicable toalternative perr red (Class A or Class B) complete the foll6wing-monitori' g data: Allowable Level Pathogen Density UM Parameter Arial Units Sam" le in Sludge ts Excee- of Analysis p N*Murr, Geo. Me Type Tech - an $Waximurr Units of Analysis 2 x 10 to the niaue T WN 5200 11481.53 59800 MpN 6th power 0 7 grab sm9221 per gram of Fecal Coliform total solids CFU 1000 mpn per gin a o f total solid (dry Salrnonella bacteria 5 WN pet 4':,grams (in lieu of fecal total solid (dry coliform) weiaht) Ve�ct0ei,Attraction Red uk"ti CAC-.02T .1107) - Plea'se indicate,... alt6 a ive'"heff6rtne Alt. I (YS reduction) U Alt'. 2 (4 1 -day bench) 3 (30m. Alt'. day V,en6h) 4 �(Spec,. uptake) Alt. 5 (14-Day Aerobic) El Alt. 6 on El Alt 7 (Drying - Stable) 13 Alt. 8 (Drvi g - Unstable) Ej Alt. 9 (1jection) i i EJ Alt. 10 (tco� =oration) F1 XT—vertor.9ttrac',tion reduction alternatives n'f corporation) CERTIFICATION W—A-11EMEN !�, I . vesw6rePe formed. [I T iplease check the appropriate statement) "I certify, under penalty off law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction qucti-ed ti o4 requirement in 15A NCAC 02'T J107 have been met." re uc I 461c 1 certify, under Penalty. 9f law, that the pathogen requir' _ pments�in 15A.N CC02T 110.6 and. the vector attraction reduction requirement in 15A NCAC 02T .1101 h6ve not ,be�en'me. 0' (Please.fiolte if you check this statement attach an explanation why you, have not met one or both of the requirements.) ............. "This Oeterminatio'n has been made 'under my direction and supervision in accordance with thesystem designed to ensure that qualified pq'sonnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." 1"tiZn �-/ C,442 U e,-i Dennis Key Southern Soil Builders, Inc. Prepar6i:Name and"Title (type or Land Applier Name and Title if applicable)(type or print) " Signal of —Preparer* Date Signature of Larid Applier (if applicable) Date *Preparor is defined in 40 CFR Part 503 : .9,(r) and 15A NCAC 2T .1102 (26) M­­ ­­ ­ ._- Report Number: 14-349-0719 ft Account Number:46381 j W W Send To: SOUTHERN SOIL BUILDERS www.aleastern.com DENNIS KEY 958 HOOTS ROAD ROARING RIVER NC 28669 Date Received: 12/15/2014 Date Of Analysis: 12/16/2014 A&L Eastern Laboratories 7621 Whltepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Grower: SOUTHERN' SOIL BUILDERS SOIL ANALYSIS REPORT Analytical Method(s): Mehlich 3 Date Of Report: 12/1R/?t114 1-ar l l l ILt: r•• Organic Matter Phosphorus Potassium Magnesium Calcium Sodium Acidity Sample ID Lab pH C.E.0 Field ID Number % Rate ENR Mehlich 3 R Reserve K M 9 Ca Na Soil Buffer H Ibs/A ppm Rate prim Rate ppm Rate pm '?� Rate n, ppm Rate ate R�• ppm„ ate u p• • index ,��� negr 100g nmeq/100g K1 (- 11778 5.1 H 142 I 46 M 49 VL 237 VH 851 M 16 VL I I I ^!C=38 I I N I I I I 6.4 I 0.6 I 7.1C=25 I I K2 11779 4.3 M 124 130 VH 99 M VH 1084 M 17 VL NC=108 NC 1328 6.9 0.1 8.6 11780 4.3 M 128 24 L 31 VL 163 H 678 M 23 VL NC=20 NC=16 5.9 6-83 1.0 5-9 11781 5-3 H 146 182 H 1 123 M 155 H 735 M 21 VL NC=68 NC=63 1 5.5 6.74 1-9 7.2 � 11783 3.6 M 111 46 M 74 L 191 HP80 M 21 VL = NC 38 NC=38 5.6 6.75 1.8 7.5 Sample ID Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Field ID K Mg Ca Na H NON S Zn Mn Fe Cu B SS Cl AI ° ° % % � ppm Rate ririm Rate .. ppm Rate m Rate pp... ppm Rate ppr. Rate ppm Rate ms/cm Rate ppm Rate ppm 1.8 27.8 59.9 1.0 8.9 14 L 2.5 M 26 H 183 VH 2.5 H 0.4 L NC=29 NC=62.5 NC=163 1 1 NC=125.0 <2 3.0 31.8 63-0 0.9 - 1.4 13 L 14.5 H �35 H 1182 VH 14.4 VH 10.5 L NC=27 NC=112.5 NC=219 NC=220.0' 1.3 23.0 57.5 1 17-3 16 M 4-8 H 101 VH 193 VH 16.5 VH 0.4 L --T NC = 33 NC = 120.0 NC = 631 NC = 325.0 4-4 17.9 51-0 1.3 1 25.9 118 M 7.3 H 128 H 1170 VH 1 5.7 VH 0.4 L NC = 37 NC = 182.5 NC = 175 NC = 285-0 2.5 21.2 52.0 12 23 4 15 L 4.0 H 76 VH 117 VH 4.8 VH 0.3 VL 1 1 I I I I NC=31 I NC=100.0 I NC=475 I I NC=240.0 •^•��� �•• •••• ••-ram • •�r•��•-••• •• � r•� •a-���a��� ����� �_���� �� �nprdnauon or symoots: -/o (percent), ppm (parts per million), Ibs/A This report applies to sample(s) tested. Samples are retained a oil. Rating after each value: VL (Very Low), L (Low), M (Medium), (pounds per acre), ms/cm (milli -mhos per centimeter), meq/100g maximum of thirty days after testing. I (High), VH (Very High). ENR - Estimated Nitrogen Release. (milli -equivalent per 100 grams). Conversions: ppm x 2 = Ibs/A, Soluble nap y by P�'c Al m G :.E.C. - Cation Exchange Capacity. Salts ms/cm x 640 = ppm. Analysis prepared b : A&L Eastern Laboratories, Inc. Pauric McGroary NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006830 " r r f Client: Southern Soil Builders, Inc. Advisor: , Predictive 958 Hoots Rd r =: .g"�=:�'ti Roaring River, NC 28669 Soil Report Mehlich-3 Extraction Sampled County: McDowell Sampled: Received: 09/25/2014 Completed: 10/06/2014 Farm: Links to Helpful information Sample ID: F3 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- Test Results [units - iiVfi in g/c0; CEC and Na in meg1100 crrr3; NO3-N in mg/da]: Soil Class: Minerai HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 1.12 8 82 1.4 6.2 107 38 54 26 36 159 110 121 / 121 226 ✓ 0.1✓ 1 Sample ID: F4 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 40 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na / ESP / SS-1 NO3-N 0.56 1.10 7.6 79 1.6 119 49 52 24 37 127 93 137 ✓ 137 236 ✓ 0.1 1 Sample ID: R1 Recommendatio : Lime Nutrients (lb/acre) More Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu B Information Lime History: 1 - Fescue/OGrass/Tim, 1 0.0 120-200 70 100 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cm3; CEC and Na in meq/100 crn3; NO3-N in mg/drrP]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na / ESP / SS-1 NO3-N 0.41 1.00 8.3 84 1.4 Q 27 21 57 25 47 58 52 62 ✓ 62 103 0.2 t/ 2 ^ North Carolina Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL006830"' Page 2 of 3 Sample ID: R2 V Lime History: Recommendations: Lime Crop (tons/acre) N P2O5 1-Fescue/OGrass/Tim, 1 0.8 120-200 120 2.- Nutrients (lb/acre) Cu B 0 0 More Information Note: 12 K2O 110 Mg S Mn Zn 0 0 0 0 Test Results [units - W/V in g/cm3; CEC and Na in meq/100 crn3; NO3-N in mg/dnn ]: Soil Class: Mineral HM% WN CEC BS% Ac p P-1 K-1 Ca% Mg% S-1 0.46 1.09 6.0 68 1.9 5.6 11 15 46 21 40 Mn-I 133 Mn-All Mn-AI2 97 Zn-I Zn-AI 27 ✓ 27 Cu-I NaESP SS-1 NO3-N ✓ 42 ✓ 0.1 2 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL 686830 Page 3 of 3 1 Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Report Abbreviations Lime Ac exchangeable acidity If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either B boron ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. BS% % CEC occupied by basic cations For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at Ca% % CEC occupied by calcium one time, even if the report recommends more. You can apply the rest in similar increments every six months until the CEC cation exchange capacity full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Cu-I copper index ESP exchangeable sodium percent Fertilizer HLq% percent humic matter Recommendations for held crops or other large areas are listed separately for each nutrient to be added (in units of K-1 potassium index lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies K20 potash for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they Mg% % CEC occupied by magnesium are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is MIN mineral soil class an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear Mn manganese only on reports for greenhouse soil or problem samples. Mn-All Mn-availability index for crop 1 Mn-Al2 Mn-availability index for crop 2 Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH,. C or Z Mn-I manganese index notations appear on the soil report, refer to sNote: secondary Nutrients and Micronutrients• In general, homeowners do not M-O mineral -organic soil class need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit N nitrogen ncagr.gov/agronomi/pubs.htm. Na NO3-N sodium nitrate nitrogen ORG organic soil class Recommendations forsmall areas, such as home lawnslgardens, are listed in units of Ib/1000 sq ft. If you cannot pH current soil pH find the exact fertilizer grade recommended on the report, visit www.ncagr.govlagronomi/oboart4_htm#tfs to find P-1 phosphorus index information that may help you choose a comparable alternate. For more information, readA Homeowner's Guide to Fertilizer P20s phosphate S-1 sulfur index Test Results SS-1 soluble salt index WN weight per volume The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The Zn-AI zinc availability index remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not Zn-I zinc index routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit wiryw.ncagr.govlagronomiluvrsthtm for more information. Annual Report Review SOP Class B Land Application Reporting Period: :1 /t Att - /-21311/L/ Permit Details: C 4-� of IA& W Q Cd 1 a g G() • Is 503?.1e.5 • Class A or B? l3 Maximum Dry Tons Per Year: a Q U Number of acres permitted: 151, 70 Number of fields in permit: Counties that land is permitted for: Monitoring Frequency for TCLP: 1 x Monitoring Frequency for Residuals Analysis: 44 nL Monitoring Frequency for Pathogen & Vector Attraction Reduction: ,4,i•-.c-cL Groundwater monitoring: N/A: 1. Annual Land Application Certification Form , Was a certification form submitted?y0-S. Was land application conducted during the reported year? y S' How many dry tons and dry tons per acre were applied? l 1 7, A 3 Were the applications within the permitted amount? 1,,e-5 Verify PAN if more than 10 tons/acre? Did it indicate compliance? y C s Was it signed by the appropriate people? S 2. Monitoring Were the analyses conducted at the required frequency? Was, an analyses taken for each source that was, land applied? �+ Were the metals analyses reported on the Residual Sampling Summary Form? �e-S Were the results reported in mg/kg? �( Were the pH's 6.0 or greater for each residual sample? y"-s Were the heavy metals. within ceiling concentration permit limits? v-5 Were the lab analyses attached? -I S Were all the required parameters tested? e S Was TCLP analysis conducted? Were the TLCP contaminants within regulatory limits? N Was a corrosivity, ignitability, and reactivity analysis conducted? y e s 3. Field Summary _... ...... .. Were-theland.application. events recorded_on.the-Field_Summary-Forms?---------=------ How many fields were applied on this year? 6 Was a Field Summary Form submitted for each field? yes Were all the residuals applied to permitted land? Y4-3 Were all the residuals applied from permitted sources? `�eS Were the field loading rates for each metal and PAN calculated (year to date)?y s Were the cumulative pollutant loading rates calculated?y -a Were the calculations correct. jF e-S' Were the PAN loading rates within permit limits?YO-5 Were the heavy metal cumulative pollutant loading rates within permit limits? t4-S Were the residuals applied on a suitable crop?v-y Were the applications conducted during the crop's growing season? Y,?s Were the Field Summary Forms complete? Ye_S' Was lime application on Field Summary Form? No lime applied. Y-e-9 -' Q--a 1 2WO 16, b,Z sty t G. 4. Pathogen and Vector Attraction Reduction • Was a signed copy of the Patho en and Vector Attractioneduction Form submitted? YeX Did the form indicate the per' d of coverage; the residual class, and the pathogen reduction alternative and the vector attraction reduction option used? • Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? • Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? Class B Pathogen Review Alternative 1— Fecal Coliform Density Was the sampling conducted at the required frequency? es Were seven samples taken? Ya Was the geometric mean calculated and done correctly?'V-5 Did the results show compliance (less than either 2,000 0, 00 MI'N/gram of total solids or 2,000,000 Colony Forming Units/gram of total solids)? YES Alternative 2 — Use of Process to Significantly Reduce Pathogens (one of five) • Was the sampling conducted at the required frequency? 1. Aerobic Digestion • Was it an aerobic process (Inspection)? -'Were logs submitted showing time and'temperature? Were temperatures within range for complete'time period? Was the time and temperature between 40 days at 20°C (68T) and 60 days at 150C (590F)? 2. Air Drying • Were the residuals on sand beds or pave or unpaved basins for three months? Was the ambient temperature above 0°C (32°F) for two months? Were the residuals partially digested? Were residuals exposed to atmosphere during two months above 0°C (not snow covered)? 3. Anaerobic Digestion • Was it an anaerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? -Was the time and temperature between 15 days.at 35°C (95°F) to 550C (1310F) and 60 days at 200C (680F)? 4. Composting (usually will be. Class A when composting is used) Was it a composting procedure (not natural decay under uncontrolled conditions)? Were logs submitted showing time and,temperature? Was the temperature raised to 40 5. Lime Stabilization • Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? Were logs submitted showing time and temperature? Was the pH raised.to 12 after two hours of -contact? Were logs submitted showing time and pH? Was temperature corrected to 25°C (771F)? Alternative 3 — Use of Processes'Equivalent-to RSRP (Not commonly use. See White House Manual page 100-103, tables 11-1 and 11-2.) Vector Attraction Reduction Review Was the sampling conducted at the; required. frequency?�C S Option 1— 38% Volatile Solids Reduction Was there 3 8% reduction? Were lab sheets/calculations in report? Was the reduction on volatile solids (nottotal solids)? Were the samples taken at beginning of digestion process and before application (Inspection)? Were calculations,correct? Option 2—'40-Day.Bench.Scale.Test Were residuals from anaerobically digested treatment (Inspection)? Were residuals anaerobically digested -in lab?: Was the test run for 40 days?. Was the test done between 30°C (86°F) and 37°C (99°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less.than 17%? Were lab sheets/calculations in'report? Were calculations correct? Option 3 — 30-Day Bench Scale Test Were residuals from aerobically: digested treatment (Inspection)? Were residuals aerobically digested in lab? Were residuals 2% or less total solids? If not 2% total solids, was the test ran on, a sample diluted to 2% with unchlorinated effluent? Was the test run for 30 days? Was the test done at 20°C (68°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 15%? Were lab sheets/calculations in report? Were calculations correct? . Option 4 — Specific Oxygen Uptake Rate(SOUR) Were residuals form aerobically digested treatment (Inspection)? yes Were residuals 2% or less total solids (dry weight basis) (not diluted)? yzz s Was the test done between 100C (50°F) and 300C (860F)? Was the temperature corrected to 200C (680F)?Yt_v Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids -(dry weight basis)?�,� 8 Was the sampling holding time two hours? Was the test started within 15 minutes of sampling or aeration maintained? Option 5 —14-Day Aerobic Process Were the residuals from aerobically digested treatment (Inspection)? Were the residuals treated for 14 .days? Was the residuals temperature higher than 40°C (1041F) for a 14-day period? Was the average residuals temperature higher than 45. C (113°F)? Option 6 — Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? Did the pH of residuals remain at 12 or higher for two hours without the addition of more alkali? Did the pH of residuals remain at 11.5 or higher for an additional twenty4wo hours without the addition of more alkali? Was the pH corrected to.251C (77°F)? Option 7 — Drying of Stabilized Residuals Does the residuals contain any unstabilized residuals? Were the residuals mixed with any other materials? Were the residuals dried up to 75% total solids? Option 8 — Drying of Unstabilized Residuals Were the residuals mixed with any other materials? Were the residuals dried to 90% total solids? Option 9 — Injection Was there any significant amount of residuals on land surface one hour after injection (Inspection)? Was injection done on pasture or hay field? Was injection done at time that crop was growing? If Class A with respect to pathogen, -were residuals injected With eight hours after discharge from pathogen treatment? 5. Soil Tests • Was a Standard Soil FertilityAnalysis conducted for each application field? kl� If no was lime aWere the -soil pplied l eed to thoser for each R, iapzeication db field? I_�CF'4{b 1) Fq �n1° PN pP 6y 3t • Were the copper and zinc indexes in the soil lessIthan 2000 for each application. field? K I Was sodium less than 0.5 meq/100 cm^3? i-eS L Was the exchangeable sodium percentage (ESP) less than 15%? �•eS N o a 6.General Was the report in the proper format? .`S' Was the annual report complete?4,e Was the report submitted on time? T&f Cu DPP kllugl� �if s�� a,