WQ0019960_Annual Report_20130204

City Of
Marion
City of Marion, NC WWTP
2012 Annual Report
Land Application Program
NC Permit No. WQ0019960
FEB 0 4 ZQ13
VVATr--p. F Y. OUALSECTION
INFORMAT'10IN PROCESSING UNIT

3-
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: W00019960 Laboratory: 1)
Facility Name: City of Marion 2)
Residual Source WQ # or 3)
NPDES #: NC0031879 4)
WWTP Name: 5)
A&L Eastern Labs
�:�rm7��� •
Parameter
.(mg/kg)a-
.
Limi
. - • • .• �.
Arsenic�0--_--___--_
Chromium
Molybdenum
Selenium
Total Phosphorus•
11
-_�-_-�-_�_
a For surface disposal facilities the ceiling concentration limits ustea in ims Corm are not appncav,c. 1-1--1- 1.1 r-• ••••- - - -
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for su"itting false information, including the.possjbility of fines and imprisonment for knowing violations."
Si
*
Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DENR FORM RSSF (12/2006)

AINA UAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: ---------------------------------
City of Marion Total Dry Tons Applied (Annual): 25.28
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Nancy Ross . Owner: Nancy Ross Predominant Soil Series: Hayesville
Acres Used: 19.4 Acres Permitted: 19.4 Site #: R-01 Field #: R-01
Residual Analvsis Data (Neaw MPfale and Tm-.,l ,,, r
Com-
posite
D.
;
--
Total
DT/Ac./
App.
Event
--__­ d -
Llj
1.30
------ _
2 J
­.
3
E+ 0 J,�aaa.uia•c4
4
151
lII lUJ/illa-CJ:
6
L7J
L8J9
10
Li12
y
0
Arsenic
Cadmium
Copper
Chromium
0.010
0.005
1.016
0.117
0.000
1 0.000
0.000
0.000
0.000
0.000.
0.000
0.000-
0.000.
0.000
.0.000.
0.000
0.00.0
0.000,
. 0.000
0.000
0.000
0.000
0:000 .
0,000
0.000
0.000
:0.000,
'0.000.
0.000
0.000
0.000
0.000.
0.000
0.000
0.000
.0.000-..
0.000
0.000
0.000
.0.000.
0.000
0.000
0.00.0
0.000
0.004•
0.010
0.000
0.005
0.000
1 1.016
0.000
0.117
Lead
0.136
0.000
0.000
0.000
0.000
'0.000 .
.4.000
0:000
'0.000
0:000
0.000
0.000
0.136
Mercury
Molyb-
denum
0.003
0.021
0.000 ..
0.000
.0.000. ,
0:000 :
0.000
0.000
:0.000
0:000 .
0.0001
0.000 .
0 :000_
. .
' Oc000
0.000
0.000
.0.000`
0.006
. 0.000
0:000
0.000
0.000
0.003
0.000
0.000
0.021
Nickel
0.057
0.000
0.000
'0.000.
0.000
.0:000
0.000
0:000
0:060'
.0.000
0.000
0.000
0.057
Selenium 0.008 0.000 0.000 0.000. 0.000 0.000, .0:000.
Zinc 2.971 0.000 0.000 0.000 �.0:000 0.000-`: .0.000
Total
0.000. :0.000
0.000 0..000,
0:000
0:000
0.000
0.000
0.000
0.000
0.008
2.971
Phos- 69.059 0.000 0.000 0.000 0.000 0.000- 0.000
horus
0:000 0.000
0:000
0.000
0.000
69.059
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signa re of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: R-01 Acres Utilized: 19.4
Land Owner: Nancy Ross Annual Dry Tons Applied: 25.2835 Site #• R-01 Acres Permitted: 19.4
Operator: Nancy Ross
Crop 1 Name: Fescue
Predominant Soil Series: Hayesville
Crop 1 Max. PAN: 202 Crop 2 Name:
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
° y
° c
°
Volume applied
(enter one) Solids/
Li Liquid
4
Cu. Yds Gallons
%
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Mist)
Precip.
Past 24
Hrs.
inches
D
F
E• F
o m
a o.
o
;� w
w s
�, --
D N'
w
5
Pc =
w
cc
a
TKN
mg/kg
z Y
q 9
o �
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
P yP
Receiving Residual
Application
PP
Crop 1
Crop 2
Crop 1
Crop 2
4-2012
344500
1.76
1.303
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
49.160
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
I
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
0
344500
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
49.160
0.000
Lime A lied
Annuallbs/acre
0.010
0.005
1.016
0.117
0.136
0.003
0.021
0.057
0.008
2.971
69.059 1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.042
0.052
36
0.033
0.038 J
34
5.785
6.801 X
NA
1.139
1.256
1338 1
0.952
1.088
267
0.043
0.046
15
1.164
1.185
NA
0.389
0.446 vr
374 1
0.082
0.090
89
14.112
17.083
2498
11-2012
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit 1 st/2nd Crop
202
• i. certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
i
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: K-01 Acres Utilized: 16
Land Owner: Anna Deebold Annual Dry Tons Applied: 12.4032 Site #: K-01 Acres Permitted: 16
Operator: Mario Deluca Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
O
p
Q
Volume applied
enter one Solids/
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
A lied er
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Wet
Moist)
Precip.
Past 24
Hrs.
inches
a
¢ w
*
o
2
_
co
* w'
o'
0
4
7c =
w -,
=
* w
o
TKN
mg/kg
Z
o
°C,° a
CD M.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4-2012
71500
1.76
0.328
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
12.371
NA
Fescue
11-2012
97500
1.76
0.447
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
16.870
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
169000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
I P
29.24,1
0.000
Lime Applied
Annuallbs/acre
0.006
0.147
0.153
36
0.003
.108
0.111
F 34
0.605
15.87
16.475
1 NA
0.070
0.811
0.881
T 1338
0.081
2.06
2.141
267
0.002
0.098
0.100LY2.431
15
0.012
2.419
NA
0.034
0.949
0.983
374 1
0.005
0.232
0.237
89
1.767.
35.871
37.638
2498
1 41.075 1
Date
lbs/ac
Prior Years Cumulative lbs/ac
11-2012
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop I
"1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
'�"'
�/ *Application Method: S - Surface, IN - Injection, INC - Incorporation
t- 0-\3 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion
Land Owner: Anna Deebold
Operator: Mario Deluca
Crop 1 Name: Fescue
WQ Permit #: WQ0019960 Field #: K-02
Annual Dry Tons Applied: 27.1917 Site #: K-02
Acres Utilized: 35.8
Acres Permitted: 35.8
Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
`' .c
+�
a3 0
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NpDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
(Dry,
Moil)
Precip.
Past 24
Hrs.
inches
D
K �
n �?
�,
a
°
o
w
�,
* w'
6
w
n ??
w'
0
TKN
mg/kg
z Y
q
o
? a
E.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(lbs/acre)
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4-2012
130000
1.76
0.267
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
10.053
NA
Fescue
11-2012
240500
1.76
0.493
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
18.597
NA
Fescue
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
3705001
As
Cd
Cu
Cr
Pb
HE
Mo
Ni
Se
Zn
P
28.650
0. 000
Lime Applied
Annuallbs/acre
0.006
0.003
0.593
0.068
0.079
0.002
0.012
0.033
0.005
1.733-
40.280
J
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.144
0.11
16.359-
0.858
2.121
0.1
2.427
0.971
0.229
36.221
11-2012
2000
Current Cumulative lbs/ac
0.150
0.113
16.952
0.926
2.200 1,
0.102 v
2.439 6
1.004
0.234 u
37.954
Permitted C. P. L. R.****
36
34
1 NA
1338
267
15
NA
374
89
2498
Permit PAN Limit 1 st/2nd Crop
1 202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
I - �-D. 03
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM `
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F3 Acres Utilized: 11.4
Land Owner: James Fisher Annual Dry Tons Applied: 9.0639 Site #: F3 Acres Permitted: 11.4
Operator: James Fisher Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Cron 2 Max. PAN -
0 �
Volume applied
PP
Solids/
Volume
Residual Sources
Soil
CDond.
Precip.
�
<
o
�
�
A
z B
Nitrate
PAN Applied
Name of Crop Type
c
(enter one)
%
Applied per
PP P
(N Q
PDES #, W #,
Past 24
a v
cv
w w
w ,
TKN
o
and
Receiving Residual
o
Q
Liquid
Solids
Acre
Fert., Animal
(Dry,
Hrs.
0 0
o w
¢
0 ..-
N'CD
* iv
0000
=
Nitrite
( Ibs/acre)
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Wet,
Moist)
inches
w
* 0
mg/kg
mg/kg
mg/kg
Crop 1
Crop 2
Crop 1
Crop 2
4-2012
1
123500
1.76
1 0.795
WQ0019960
dry
0
s
0.5
0.3
56800
9090
2
29.990
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
123500
As
Cd
Cu
Cr
Pb
HR
Mo
Ni
Se
Zn
P
29.990
0.000
Lime Applied
Annuallbs/acre
0.006
0.003
0.620
0.072
0.083
0.002-
0.013
0.055
0.005
1.813
42.135
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.036
0.042
36
0.015
0.018
34 1
1.911
2.531 v
NA 1
1.691•
1.763 ✓
1338
0.392
0.475�
267
0.017
' 0.019.
15
0.077.
0.090
NA
0.184
' 0.219v
374
0.033
0.038
89
7.221
9.034
2498
11-2012
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
202
GGI Illy, Ul ucl PUBUILy Ul JUW, Lnal ims aocument was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface -0.5, Injection/Incorporation - 1.0
Signatur of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DENR FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion
Land Owner: James Fisher
Operator: James Fisher
Crop 1 Name: Fescue
WQ Permit #: WQ0019960 Field #: F4
Acres Utilized: 8.2
Annual Dry Tons Applied: 8.1098 Site #: F4 Acres Permitted:
Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503):
Crop 1 Max. PAN: 202 Crop 2 Name:
Crop 2 Max. PAN:
8.2
Y o(enter
Q
Volume applied
one) Solids/
Liquid
Cu. Yds Gallons
�/a
Solids
Volume
Applied per
PP P
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#,
Fert., Animal
Waste, etc)
Soil
Cond.
D
( n',
Wei
Moist)
Precip.
Past 24
Hrs.
inches
>
b
00. w
* 0
o
w
w �.
CD
* �'
o'
X �,
* w
TKN
mg/kg
Z >
q
a"a o
CD
`w
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
lbs/acre
( )
Name of Crop Type
Receiving Residual
Application
Crop 1
Crop 2
Crop 1
Crop 2
4-2012
110500
1.76
0.989
WQ0019960
dry
0
s
0.5
0.3
1 56800
9090
2
37.305
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
o
11050o
As
Cd
Cu
Cr
Pb
H
Mo
Ni
Se
Zn
P
37.305
0.000
Lime A lied
Annuallbs/acre
0.008
0.004
0.771
0.089
0.103
0.003
0.016
0.044
0.006
2.255
52.417 1
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.058
0.066
36
0.031
0.035
34
5.343
6.114
1 NA
2.02
2.109
1338
0.801
0.904
267
0.033
0.036 v
15 1
0.149
' 0.165
NA 1
0.365
0.409
374 1
0.07
0.076
89
12.24
14.49
2498
11-2012
2000
Current Cumulative lbs/ac
Permitted C. P. L. R.**** 1
Permit PAN Limit 1 st/2nd Crop 1
1 202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
/ **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier
Date
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
i
DENR FORM FSF (12/2006)

Page: 1 of 2
Report Number: 12-130-0205� A&L Eastern Laboratories, Inc.
Account Number: 46381 7621 WhRepine Road Richmond, Virginia 23237 (604) 743-S4Wt Fax [phone]
Submitted By: ZACH KEY
wWwaleastern.com
Send To: SOUTHERN SOIL BUILDERS Project: MARION
DENNIS KEY NC CERT # 257
958 HOOTS ROAD
ROARING RIVER, NC 28669
REPORT OF ANALYSIS Date Sampled: 5/8/2012 11:00:00
Lab Number: 87806 Date Received: 05/09/2012 00:00
Sample Id: MARION Date Reported: 05/15/2012
Moisture
Total Kjeldahl Nitrogen
Total Phosphorus
Total Potassium —
Total Sulfur
Total Calcium
Total Magnesium
Total Sodium
Total Iron
Total Aluminum
Total Manganese
Total Copper
Total Zinc
Ammonia Nitrogen
Organic N
Nitrate+Nitrite-N
Total Cadmium
98.24
5.68
56800
2.65
26500
--- - 0.76-------
7570-.
1.00 .
10000
2.20 --
22000
0.64
6370
0.36
3550
21600
29000
454
390 t/
1140
0.91 9090
4.77 47710
<2.00
2.0
100.0
10.0
100
100
100
100
100
1
10
1
1
1
10.0
10.0
2.00
1.0
— — BW 05/09/2012-43-59---------
SM-2540G----------
BW
05/09/201213:59
SM-2540G
JM
05/10/2012 07:54
SM-4500-NH3C-TKN
KM
05/10/2012 16:46
SW 6010C
KM.--.-----
05%10-/2072 6:46----
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
KM
05/10/2012 16:46
SW 6010C
JM
05/10/2012 07:54
SM-4500-NH3C
05/10/2012 07:54
CALCULATION
JM
05/10/2012 07:55
SM-450ONO3F
KM
05/10/2012 16:46
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
-0.
Debbie Holt

Page: 2 of 2
Report Number: 10205 A&L Eastern Laboratories, Inc.
Account Number: 46381 6381 7621 Whitepine Road Richmond, Virginia23237 (soa)743-saol Fax (804)M-64"
Submitted By: ZACH KEY
Www.aleastern.com
Send To: SOUTHERN SOIL BUILDERS Project: MARION
DENNIS KEY NC CERT # 257
958 HOOTS ROAD
ROARING RIVER, NC 28669
REPORT OF ANALYSIS Date Sampled: 5/8/2012 11:00:00
Lab Number: 87806 Date Received: 05/09/2012 00:00
Sample Id: MARION Date Reported: 05/15/2012
Total Nickel
Total Lead
Total Arsenic
Total Mercury
Total Selenium
PH (Standard Units)
Total Molybdenum
OG-
22 ✓
5'--
KM
05110/2012 16:46
SW 6010C -
52 %1-
5
KM
05/10/2012 16:46
SW 6010C
4.0 ✓
1.0
KM
05/10/2012 16:46
SW 6010C
00 /2201215:00
SW-T471B
3.0 ✓
-----------------------------------------
1.0
KM
05/10/2012 16:46
SW 6010C
7.22
-------- ----
--
JM
05/10/2012 07:54
SW-9045D
8 ✓
5
KM
05/10/2012 16:46
SW 6010C
Comments:
SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES
—QUALIFIER:�MATR-ICE-SPIKE-WAS-OU-T-OF1L-IMfT-S-FOR='Na!AND"Se—ALL-OTHER-QC-DAT-4-I-S-ACCEPTABLE--
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made
to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization.
Debbie Holt

M\
Mineralization
as decimal
ITotal dry
tons/year
Acres
Applied on
Rate
0.3
TKN
56800
NH3
9090
NO3
2
NO2
0
% Solids
0.0176
1 94.96
1 113.7
PAN Surface
18860 m /k 37.72 lbs/dry ton
3681.891 Ibs total PAN
31.503 Ibs PAN/acre
PAN Injection
23405 1 mg/kgmg/kg 46.81 lbs/dry ton
P34=054079
78 Ibs total PAN
1 lbs PAN/acre
Dry Tons/1000 gal.
0.073392
1st year PAN
Surface lbs.
3581.8912
lstyear PAN
Injected lbs.
4445.0776
lbs./acre
Surface
31.50300088
lbs./acre
Injected
39.0947898
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity
2000
"=dry tons/1000gal."

SAR
Sodium Absorption Ratio
Na: Sodium (Mg/L) Equivalent weight: 23
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg : Magnesium (Mg/L) Equivalent weight: 12
Milli Equivalent = Mg/L / Equivalent weight
Na M /L Ca M /L Mg(Mq/L)
62.48 1 387.2 1 112.11
Na ME
Ca ME
Mg (ME)
2.716522
19.36
9.3425
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power
7757
SAR = 0.717081 (From Mg/L entered above)
SAR= 0.715391 (From ME entered below)
Na (ME)
Ca ME
M ME
2.71
1 19.36
1 9.34
The amour
amount of E
Permitting

'A,N-22-2013 TUE 03:42 PM MARION*WWF-T
FAX ; 8286691943 P, 0V
Is6o 0- -FC--GT5-
-S--r) o _ g Lo
t

JQ-2Z—LUIJ TUli; UJ:41 F-M MAR IUld*WWFT IiAL828-5591943 F. 006
1.
Environmental Testing Solutions, Inc.
Certi#ieabe. of Analysiis-
PO Sox 7365
Asheville, NC 2880E
Phonc: [phone]
Fax: [phone],64
Project.narn4; Marion.'WWTP Project number: 120313S{14
Collection date: 13-Mar-12
Dale reenived: 13-Mar-12
Stemple i.0 =OI ic:tltian: CC Slud a #F1 -Crab Sample number, 11)1811
it Date s Parauictrr iWIt;[bod. ttesult kK�.. I,�Q. � Aaalt F1/Utnutch Anaiy'rrii X'
%I'S SM 2540 G 2A 011-0 % 14-1rtar-12 MUF
Mulitpla'1'ubd Ve,tlterltHti611 PrOC6LIUCn SM 9221-P <432' 432 MPN 14-Nt:Y-12 K-EK
Sample identification: CC Sludge i#2 - Graf$ Sample: number: 91372
1'aratnCicr Method Result RL Units Date Analyzed Auz.lys[ Footnotes
%TS SNi 2540 G 2.3 0.10 °!o Ml U.,
Niulitplf-, Tube N;rmentuiion Prouddure S1b2 9221-E <414- 414 MPNt 1.i-Mar-12 KEK
S:lrnple iticntircadun: CC Siud-e #3 Grab Saniple.nurnber: 91873.
Parameter Method result RL Units Date AnAlyst Footnotes
AoLklyzed
%TS SM 2540 G 2.1 0110 % L-i- 1.,,12 M111
Mulitple Tube Fermentation Procedure SM 9221-E <378 _ 378 MPN Kl, K
Sample idcnd ieation: CC. Sludge #4 Cxrab Sumplc number- 91874
Puraineter ❑ate
14ttluti result � Units Anaiyiad Aaslyst Footnotes
%TS SM 2540 0 2:4 0.10 No 14-Mu42 Ml1P
Mulilple'fube Fermentation Vrocodurc SM 9211-L' 480 432- MPN 111-roar-13 KEFL
1' oolnvlt:s;
.RL = Reporting Limit. Vulues are reported down to the. Reporting Limit -only.
Dale reviewt:-d;
Data reviowW by: Kelley R. Keenan
Signature:
NC Certification Number, 600
SC Certification Number: 99053
NC DrIn inb Water Caltiticatioll Number: 37786
This report should not be reproduced, exepr in ipt entirety, without the wriuun consent of Environmenutl Testing Solutions, Inc,
The m-whs in (ilis report relnta only to Ose- sump)ts submitted fur analysis.

W:KbtbU IHj i. UUt
•�.J yE'rht''���
Etiviranmental Testitlg 5ol4tions, Inc
ProJ%xt nurYme.' Marlon WWTV
CoLluciiun data; 2t-Feb-12
Daw rCCeicCd; 21'-Net)-12
Certificate of Analysis
5ampte idontilivuLiUn: CC Studee N4 - Gra4
110 Bvx 7505
Ashev'IH4, NC 28802
Phone: [phone]
I uz: [phone]
Project number: 120221,545
Sample number: 91473
_ ..,....-bit
Parameter Method* Result RL Units Aa:Ile Analyst F:outn.otcs
°ru"1'S SM 2540 G 1.9 0.10 % 21-Peb.1' Ml I
l�4uli[ rle: Cubs I'rrnl�n[ntiun (yntccdurc SM 9221-E <342 342 MPN 22-Feu-12 KI K
tiamplu idcntiticalian; CC Slud-e �+- Grab Sample number.
91474
-.. __ •-------- Date
Parameter Method- tesult RL Units Atlrilyzed Analyst Footnotes
SM 2540 c 14 0,10 % MFIF
Mulil lc l'ube Fern1<nt�tion Prucc�iurc SM 9221-6 <324 324 N1PN 214cb-42 KEK
Sumplt: idcnlili=ioll: CC SIud t #G Grab 9ampl4 !lumber;
91475
Bate
1'aratl�utcr Method Result ilL Units Analyzx4t A>�tyat Fuotnote�
aio 1 y SM 2540 G 1.8 0.10 OA MH P
Mulil.Ie'1'ube RzilicnLatiurt Pruwdwo- SM 922I-F. -Q" 324 MPN IZ-Fcb-12 KLK
Sample identitiCali Oil: CC Sludge #7 Grab Sample number: 91476
Duce :-nat st footnotes
ParameterNicthod Result RL UnitsDuce
y
%TS SM 2540 G 1.8 0.10 % 22-FEW Z M H C=
A 'Jit te'1'ubc FermenLalion Procedure SM 9221-F C324 324 MPN 33•Fab-!: KLK
1'UL1LlIJlCS;
RL Reporting Limit. Valucs are reported down 10 the Reporting Limit only.
Dula rfviev.eJ: Cz' -
1)uta vevivwgv by! Kelley E. Keenan
Sigrlatw c:
NC Ccrtilication Number: 600
SC C•CrtitieuLion Number. 99033
NC Drinking Water Certiticatiun Number: 37786
- This report 00010 not be reprmiuct . exrpt in its entlrety, without the writren constant of Environ^tental Tvsling.ti.UlL�Qnns, Lie.
i�Le r"5 &$ in this sport relate only to Lhe samtles subrniaed ror anAlysis.

JAB-22-2013 TU& 03:40 PM MAR-ION*WWPT
FAX: HH591943 P, 004
cm
J
Environmental Testing Solutions, Inc.
Project namC: Marion. WWTP
Culictaiott date: 14-Feb-12
Daft reCcived: 14-Feb-12
Ccr. d icate- of ,t nMysis
,) . It; i�lenti l is utitm: CC Sludge #i -Grab
110 Bux 7565
AshcvillC, NC 28802
Pbt)nv: [phone]
Fax: [phone]
Prc)jcet number: 120214.528
Sampl(3 numi;w: 91214
Parameter Method Result R1L.. Units Date Adialyst footnotsy
A nulyzed
%T", SM 2540 G 1.9 0110 % ls-P4b-12 Mlip
Mttlitpl,;Tube Pcm)cntation Procedurc SM 9221-C -342 342 MPN is-Fau-ia KP.K
tilu»ple, idell lili�.;alion: CC Sludyc #2 - Grab Samplc number:
`}12tS
Parameter Method Result RL Units Daw a.ttulyst Footnotes
Analyzed
SM 2540 0 1.4: 0.10 °lc Is-(tts t: N1141V
Mulitpla *Nbe rfmientadon Procedure SM 922 L-E <342 -342 MPN ICM
Sample iJentiticatiun: CC Sludge #3 - Grab Sample number: 91216
Date. Parameter Method Result Rl.. Units A,lu
late. d Anslyst Footnotes
Ly
%rs $M 234p Q 1.9 0.10 % ,s-Fcu-ta MHF
MutilpIc Tube Ferrueulsatiun Procedure SM 9221-1, -e342 342 MPN is-F u-i2 KL3K
UCicltntitC.i t
RI = Reporting limit. Values are reported down to the Reporting Limit only.
Lulu n:virwzd: N.-.Zi-tZ
Dutu revirwed by: Kelley E. Keenan
Signaturo: -�
NC Certification Number. 600
SC Ccrtisicaliton NurntK r: 99033
NC Drinking Water Certification Number: 37786
This report should not be reproductid, 4ktQr it its S'N[rif@ty, wit ov i o twigv COn9en= oFEnvironmcntpl Testing $olutions Inc.
'rho results in this ropon miete pnty to the stunples submitted l'or analysis.

JAA-ZZ-ZUfi TU USAU YK 1AXIAMP-T
FAX:[phone])
J' P-1 OOJ
.4, 1
PQ Box 7565'
Asheville, NC 28802
Phone: (82b) 350-9364
Fax; (V8) 350-9368
EnvironrnGnftl Testing Solutions, Inc. Certificate of Analysis
Project name; Marion WWTP Projcct number: 120214.527
collccLion dale: 14-Feb-12
Date received: 14-Feb-12
Sample idi:nOtJuLion: CCSIudge-Crab Sample number: 9(213
rurninater Mathud Rvouh. KL Undia Date
Anxlyzcd
purcent Solids. SM 7,540 0 1.70 0.100 % i7-F.L� iz JAB I
Wrcury 7471R e1.2 1.2, rngfkL7.r.b.12 BGM
- L!
Aluminum 6010C 22000 130 mg/kg LC-F.b-12 130M
Arsenic 6010C �Is [5 mg/kg t6-Fro-i2 BGM
Cadmium 60 1 Oc <15 15 mg/kg 16-Fab-12 90- M
Culv.ivm 601 OC 22000 590 mg/kg 1&.Pqi.12 BGM
Copper 6010C 380 29 mg/kg i�peb-a BGM
L-ead. 6010C 56 14 mg/kg LTB L
Magnesium 6010C 6400 150 mg/kg H,-F,:LI12 BGM 1
Molybdenum 60I0C -429 29 Mg/kg 16-FO;-42 BGM
Nickel 6010C <59. 59 mg/kg irt.bo BGM
Potassium 6010C 8400 730 mg/kg t6-F�m BGM
Selenium 6010C <79 29 mg/kg to-r.o-a BG?vl
Sodium 6010C 3700 730 mg/kg wml ti BGM
Zinc 6010C 1100 140 m&U 2o-Fctio3 LTS
Nitrate + Nitrite SM 4500 NUS F • IMO 2900 rng/kg- -,aFaiz RSL
Total Phosphorus SM 4500 PT 31000 2900 mg/ko 22-F.i,. 12 CLS
Total Kjeldahl Nitrogen 351.2 3500.0 29000 ni" zt.r4wz RSL I
Total Nitrorcn Calculation 53000 37.000 mg/kg zL-rib-la RSL I
Ammonia Nitrogen
SM 4500 NH3 0 1406 53 mg/kg L7-PO- i a KEK
Percent Solids SM 2540 G- 1.9 VO MI -IF
."pl-I in Soil SW 846 9045.0 3,7 15-Fen-12. NIH F
---Rcw;t.ivt- Cyanide. 335.4 <0. 122 0.122 Mg&- 2140Z E~CHEM 2
#-'Reactive SW fide SM 4500 S D ,O 245 0 45 mg/kg i6-r.b.-tz ECHEM 2
.,'Fha,shpoint SW 846 1010 >212 212 ac 2-M.112 ECHEM 2
Arsenic - TCUP 6010 C <0.050 0.050 m_izfL r-ftb-i2 BGM I
Barium - TCLP 6010 C <5.0 5.0 mel- -Feb-ii BGM I
Cadmium -TCLP 6010 C <0.025 0,025 m_WL 23.Feb- 12 BGM 1
Chromium -TCLP 6010 C <0.25 0.25 mgfL 23.-rcb-12 BGM I
Lead - TCLP 6010 C <0,050 0-050 mg/L 23-F.b-t2 BGM I
Selenium -TOLP 6010 C -W'.16 9.10 ing/L 23-r.b.m 80M I
Silver-TCL? ' 60I0 C .0.25 0.23 MVL 23-Vib-L2 BGM I
Mercury -'TCLP 6010 C �0.010 0.010 mgtL 2s-iiab-i2 BGM 1
Full Scan TCLP Organics See attached sheets 1,3
N-PAV Calculation 1026700- 6T.Vt3r-12 KEK
Sodium Absorption Bata Calculation // �3
Mzir- 12 KEK
This report should not be reprodumd, exapt in its crrtircty, without the wntien i on eat of EnvtipiimentalTesUrig Suns,—inc.
The ft4vlt$ irl thi$ report telate 001y W the samples Auhrnim:d for nn&lysi&

, jhN-22-2U13 `I'llli U3-.3-9- FM MARIONMYT
FAX, 8-286591943 P. 002
""PRISM
RfSM I FUII-$i;,Nicu FnaiYtical 8
�,y Envuonmunmt Solmiony
Environmental Testing Solutions Project Marion WWTP
Attn: Kelley Keenan
PO Box 7565
Asheville, NC 28802 Sample Matrix: Solid
Laboratory Report
112102.12012
Client Sample 1D_ CC Sludge
Prism Sample ID: 2020345-01
Prism Work Order. 2020345
'rime Collected; 02114112 09:55
Time Submitted: 02/1511211;37
Parameter
Result
Units
Report Mt74
btltd;en
Method Analysis
Analyst
Batch
Limit
FActar
Qatr/TStne-
1D
Pyridine
BRL
mg1L
0.25 0.011
1
'8270D 31111219:21
KC
P280497
SurrySate
Recovery
Canrro[ Lvnits
2,4,04dbromophenal
95 %
49-709
2•Fluarabiphenyl
88 %
55-96
2-FIu0MphC1101
50%
27.74
Nitrobenzene-d5
74 %
53-99
Phenol-d5
35%
itvS2
Terphenyl-d14
99 %
42-133
TGLP Volatile Organic Compounds by GC11NS
1,1.Dlaftrocthyiene
BRL
ugrL
35 0.076
1
•0260B 2124112 1:45
MOO
P280458
1,2-Dichloroethene
BRL
uy1L
25 0.14
1
*moos 2124/t2 1-.48
MOB
P2B0458
1,4DichlarDbert2etle
iSRL
uq/L
980 0.068
1
`82608 V24/12 1:45
M08
P200458
Benzene
BRL
uglL
25 0.072
1
'82608 2124/12 1-,45
UGB
P290468
Carbon Tetrathioride
BRL
u911,
25 0.12
1
182608 2124/12 1:45
MGB
P280458
Chlorobtxizeric
BRL
ug1L
5000 0.051
1
182605 2124112 1:46
mG8
P260458
CNorarorm
BRL
ug(L
t00 0.082
1
'8260tt 2124112 1:46
MG8
P2BD458
Methyl t ihyl Ketone (2-Butanone)
BRL
ug/L
1D000 BAD
1
"8280B 2/24112 1:45
WS
P250458
Tevachlorpc+hYlene
BRL
uy1L
35 0.069
1
rB260B 2/24112 1:46
MG8
P26045A
Tnchloreed,yleric
BRL
ufl1L
25 0.064
1
182605 2/24/12 1:45
MG8
P260458
vinyl ahieride
BRL
ugA,
10 0.16
1
-a2606 2/24112 1.45
MGB
P211D458
SuRogate
Rccov®ry
COMM[ Limits
4-Bmmnfluorahenzene
f01 sE
BD-124
Dibromofluoromethene
101 %
75.129
Toluene48
100
77-123
Total Metals
Aluminum
22000
r„SM9 dry
150
59
— 1
16010c
2h611T ZZ:1Z.
56W
PM3Z4
mercury
BRL
mg/k1_ dry
1.2
0.14
1
*74718
2117112. 11:18
@GM
P?80320
Amaenit:
BRL
Mg/kg dry
15
3.9
t
16010C.
2/15h2- zz-12
BGM
P2B0324
Cadmium
5RL
mglkgdry
15
1,s
1
•BD10G
2l16/12-22:12-
BC,SA
P260l24
Calcium
22DDO
mglkg_6ry.
590.
230.
1
'501DC
2H6112.2z t2
BGAA
P260324
Copper
380
mglkg-dry
29
10
1
'661.8G.
21102 22:12
UGM
P2eJD324
Lead
58
-aft d+K
14
3.0
1
'6D10C.
2Z0112- 23:51-
Va
P213OM
Magnesium
MOB
mglkg Cty
ISO.
is-
1
'6010G
2118112 22;12
SGM
F200324
Molybdenum
BRL
m9/kg tlry
29
2.2
1
-6010C
2110112 22;12
BGM
P29D324
Nickel
8RL
mg(kQ dry
59
1&
1
•3010G
2(10112 r;12
BGM
P280324
Potassium
8400
mglkg dry
73q_
51
1
'6D14C
71W2 22:12
l3Gu
P2,R=4
Selenium
SRL
mglkg dry
22-
3.9
1
raalDC
2/16/12 22:12
80M
P220324
Sodium
3709
mg!(tg it
730.
91
1
'601aC
2116H2 22:12
BG)k
1`2W324
Zinc
1190
-Wks dry
140
15
1
16010C
2120112 23:51
LTB
P28M
This report should-nat tee feptadtkxd, except in its eAtift, without the written consent er Prism Le4071Orses, Inc.
440 Sprirrgbiook ROAD - P,O. Box 246343 - Charletffi, NC 28224•QR3
Phon= 764152S-6364- Toll tree Number V80015Yff.6.3m - F3Y: 7DA1625-.04" P� j6 4 of 25

JA4-2272013 TUE 03., 39- PM. MARIOIdONIFT
FIX 8.2 8559-19-4JO F. 001
YYY ll. CnvtronmenTgl gvWUone-
Environmental Tatting. Solutions -
Anil: Kelley Keenan
PO Box 7565
Asheville, NO 28$02
Project: Marion VTW.rP
Sample Matrix: Solid
Laboratory Report
08/0212012
Client Sample ID: CC sludge
Prism Sample -ID: 2020345.01
Prism.Work Order. 2020348
Time Collected: 02/14/12 09;55
Time Submitted: 02115/12 11:37
Parameter
ReaUit
Units
—RepoPt
M0L
Dilution
Melhod Analysis
An*st
Batch
Llmk
Factor
DateTme
It)
General Chemistry Parameters
Total Nihpgvn
53000
m9/kg.dry.
32000.
2800-
10
-rOtil Nitrogen ZIM/1% 5-A&
RSL
[CALq
SO&
1.70
Y-by.
0.100
0A00
1
^StBZWG Z117112 CL-00
JAB
P2B8 O
Weigle
NrtrateMitn'te as N
18000
mglkg dry
2900
320
10
•884500-NO3 F 4MM Z 12;D4
RSL
FZB0370
Pnoaptroruti Total
31000
rng/1q dry
2WG
730
20
-31*1500-P F Z=2 9�4
OLB
PM030
Total KJoldam N"gesc
35D0o
mglltg dry
29000
24D0
2
*351.2 2121i12 8:49
RSL
P2S0375
TCLP Extraction by EPA Isi
TCLP Extraction
Complete
N/A
1
•1311 2HE 2123M2 &30
ANG
P2B0437
TCI.P Extraction
Complete
N/A
1
'1311 2/23/12 10:00
LTS-
?2B0559
TCLP UeUl5
Merr,ry
BRL
mg1L
0.010`
0-ODO014
1
•7470A
=&/1213:T9
BGM
P28041a
Arsanic
BRL
MWL
0.050-
D-010
1
•a01 pC
Z23112 21:17
BGM
P250442
Barium
BRL
mg/l
5.0'
0 p19
1
'8010C
212W12 21:17
BGM
P2BO442
C+rdmium
SAL
Mg/L
0.025
O:DOM3
1
'0010C
=3112 2117
BGM
P28W42
r.hMMbjrn
0RL
mglL
0:25-
0.00085
1
18010C
2123112 21:17
BGM
P28p442
I eAa
SRL
mg1L
0.050
0;0038
1
"8010C
MA112 16.59
BGM
P280442
Selcnlum
,BRL
mg11
0:10
D:012
1
16010C
2123/12 21;17
BGM
P280442
$fiver
BRL
mglL
0:25-
0:0017
1
-8010C
2/23/12 21:17
BGM
p2B044x
TCLP Qrganochlorina PeWcides -by GC(ECCD
tordane
BRL
u 91L
IS
0,70
1
180818
229112 12:48
J1N1i V
F2B049S3
04drin
SAL'
u$IL
0.90
D.042
i
-80818
2129/12 12:40
JMV
P2804e9
Ehddn
BRL
ugtL
0.50
G.085
1
180816
2/29/12 1248
JMV
P2WM
9amrrx-13HC
BRL
ugk:
D.50
O.D48
1
•80818
Z/P9/12 12:48
JMV
P2RO499
Heptachlor
BRL
ugn,
0.50
0.005
1
-80815
M9112 12:43
JMV
P280499
Heptachlorepoide-
BRL
ug/L-
0;50
G-G68
1
•awl
=911212;48
JMV
P280499
Methnxychlor
BRL
ug1L
0;50,
0.12
1
•80818
2/29/12 12:48
JMV
P280499
Toxaphene
__......
BRL
__ .......-- - - -- .—.—T_..
up/L
•------
25
-
0.72
1
•0081$
229112 12;48
JMV
P290499
Surrogate
ControlLimis
Decachlorobiphenyi
107 %
13.180
Tetrachlomgr►xylem
87 %
40-134
TCLP Semivob0le, Organic Compounds by GgMS
Z4.5•TricMorophenol
BRL
mq/L
0.25 - `
" 6.610
1
•8270D
SM/12 12:21
KC
P2fi0497
2,4,6-Trichlorcohan01
BRL
mg1t.
0.10
0.911
1
18270D
3/1112 19:21
KC
P200497
3.4-binxr Mucn®
BRL
m911.
0.050
0.005g
1
'8270D
311M2 19;21
KC
P200497
2-kft ylphen0i
BRL
mg/L
0.050
11.012
1
'82700
. 3M/12 19;21
KC
P280407
3/4-,me nylphenpl
BRL
mglL
0.050
0.0093
1
-w7PD
3/1112 19:21
KC
P250497
HeyaOhlorooen;rne'
HRL
my/L
0.050
0,0039
1
•8270D
3/V12 19:21
KC
P250497
HexarhlorgWtad"e
BRL
mg/L
O.D50
0.016
1
•8270D
W1112 10:21
KC
P280497
Hexactrtoeocthane
BRL
m914
0.050
0,018
1
'82700
311/12 19:21
KC
P250497
Mrobcnzene
BRL
mg1L
0.050
0.014
1
•827DD
3/1112 T9:21
KC
P280497
Pentactlarupht,8i
BRL
ftWL
0-26
0.0092
1
'8270D
311112 19:21
KC
P2BO497
This report 9110 A not be reprodtmad, axt.W 14 its entirety, without the written cansent of Prism Laboratories; Im
449 SAringbro" Road -P.O. Box 240M - Chertatte, NG 282244m3
PHomx; 704I52M384-Toll Free kwober.1-800152MU4-Faux 70NS254M

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules)
Facility Name: City of Marion WQ Permit Number: WQ0019960
WWTP Name: City of Marion NPDES Number: NCO031879
Monitoring Period: From 1/1/2012 To 12/31/2012
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑
Alt B (Alk Treatment) ❑
Alt. C (Prior Testing) ❑
A1t.D (No Prior Test) ❑
I Process to Further Reduce Pathogengs ❑
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ra ❑
Pasteurization ❑
Class B:
jAlt. (1) Fecal Density R11
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion estion
If applicable to alternative performed (Class A or Class B) complete the following
monitoring data:
Parameter
Allowable Level
in
in Sludge
Pathogen Density
Number ot
Excee-
Frequency
of Analysis
y
Sample
Type
Analytical
Tech -
ni
inim
Geo. Mean
axim
Unitsdences
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
324
370.5
432
MPN
0
7
grab
sm9221 e
CFU
1000 mpn per gram
of total solid (dry.
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench)
jAlt. 3 (30-day bench) ❑I
Alt. 4 (Spec. OZ uptake) 0
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization
jAlt 7 (Drying - Stable) ❑Wt.
8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation)
INo vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
�4AA,1 CCU.., t > 0-rp 6 u p . Dennis Key Southern Soil Builders, Inc.
Preparer ame and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
gnat re o reparer* Date Sigriature of Land Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No.
FY13-SL008941
„•�,
Client.
Southern Soil Builders,
Inc.
Advisor:
°
Predictive
958 Hoots Rd
Roaring River, NC
28669
Soil Report Mehlich-3 Extraction
County:
McDowell
,tix�rn
Links to Helpful Information
Sampled: Received:10/09/2012
Completed: 10/16/2012
Farm:
Sample ID: F3
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1 - Fes/OG/Tim, M 0.0
120-200 0
0
0 0
pH$ 0
0 0
Note: 12 Note:
2 -
\
$pH
Test Results [units - WN in g/cd; CEC and Na in meq/100 crrr;; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.60 0.90
11.0 95 0.5 6.8 ✓ 87 80
59 33 33
152
96
214 214
219 0.1
1
Sample ID: F4
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1 -Fes/OG/Tim,M 0.0
120-200 0
20
0 0
pH$ 0
0 0
Note: 12 Note:
2 -
$pH
Test Results [units - W/V In g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.60 0.83
9.8 93 0.7 6.6 ✓ 71 63
58 32 44
204
130
229 229
364 0.1
1
Sample ID: R1
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5
K2O
Mg S
Mn Zn
Cu B
Information
Lime History:
1- Fes/OG/Tim,M 1.2
120-200 0
70
0 0
0 0
0 0
Note: 12
2 -
-
$pH
Test Results [units - WN in g/cd; CEC and Na in meq/100 cd; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN
CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1
Mn-I
Mn-All Mn-AI2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.81 0.91
9.4 75 2.4 5.4 93 34
54 19 39
83
67
233 233
174 0.1
1
North Carolina
�'`
fi�haiiu Trust Fund G>m1%1'won
Reprogramming of the laboratory -information -management system that makes this report possible is being funded
through a grant from the North Carolina Tobacco Trust Fund Commission.
Thank you for using agronomic services to manage nutrients and safeguard environmental quality.
- Steve Troxler, Commissioner of Agriculture

NCDA&CS Agronomic Division Phone: [phone]
Website: www.ncagr.gov/agronomi/
Report No. FY13-SL008941
Southern Soil Builders, Inc.
Page 2 of 3
Sample ID: R2
Recommendations: Lime
Nutrients (lb/acre)
More
Crop (tons/acre)
N P2O5 K2O
Mg
S
Mn Zn
Cu B
Information
Lime History:
1-Fes/OG/Tim,M 0.0
120-200 0 0
0
0
0 0
0 0
Note: 12
2 -
$pH
Test Results [units - W/V in glca; CEC and Na in meq/100 ca; NO3-N in mg/dd]:
Soil Class:
Mineral
HM% WN CEC BS% Ac pH P-1 K-1
Ca% Mg% S-1 Mn-I
Mn-All
Mn-Al2
Zn-I Zn-AI
Cu-I Na ESP SS-1 NO3-N
0.81 0.99 10.6 89 1.2 6.3 V-1,207 82
67 18 43 119
85
169 169
69 0.1 1

NCDA&CS Agronomic Division Phone: [phone] Website: www.ncagr.gov/agronomi/
Report No. FY13-SL008941
Southern Soil Builders, Inc.
Page 3 of 3
Understanding the Soil Report: explanation of measurements, abbreviations and units
Recommendations
Report Abbreviations
Lime
Ac
exchangeable acidity
If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either
B
boron
ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting.
BS%
% CEC occupied by basic cations
For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 ton/acre (50 Ib/1000 sq ft) at
Ca%
% CEC occupied by calcium
one time, even if the report recommends more. You can apply the rest in similar increments every six months until the
CEC
cation exchange capacity
full rate is applied. If MG is recommended and lime is needed, use dolomitric lime.
Cu-1
ESP
copper index
exchangeable sodium percent
Fertilizer
HM%
percent humic matter
Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of
K-1
potassium index
lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on research/field studies
K20
potash
for the crop being grown, not on soil test results. K-I and P-1 values are based on test results and should be > 50. If they
Mg%
% CEC occupied by magnesium
are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is
MIN
mineral soil class
an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear
Mn
Mn-All
manganese
Mn-availability index for crop 1
only on reports for greenhouse soil or problem samples.
Mn-AI2
Mn-availability index for crop 2
Mn-I
manganese index
Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z
M-O
mineral -organic soil class
notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients. In general, homeowners do not
N
nitrogen
need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit
Na
sodium
ncagr.gov/agronomVpubs.htm.
NO3-N
nitrate nitrogen
ORG
organic soil class
Recommendations for small areas, such as home lawns/gardens, are listed in units of Ib/1000 ft. If you cannot find
pH
current soil pH
the exact fertilizer grade recommended on the report, visit www.ncagrgoy/agronomi/obparf4.htrm#fs to find information
P-1
phosphorus index
that may help you choose a comparable alternate. For more information, read A Homeowner's Guide to Fertilizer.
P205
phosphate
S-1
sulfur index
SS-1
soluble salt index
Test Results
WN
weight per volume
The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its deghee of acidity. The
Zn-AI
Zn-I
zinc availability index
zinc index
remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn-AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not
routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit www.ncagr.gov/agronomi/uyrst.htm
for more information.

NCDA&CS Agronomic Division
Phone: [phone] Web site: www.ncagr.gov/agronomi/
Report No: 37339
��\C.\IITURF,„I, ii
Grower:
Deluca, Mario
Copies To:
460 Wilson Valley Dr
Soa
Test Report
Marion,
NC 28752
Farm:
SERVING N.C. RESIDENTS FOR OVER 60 YEARS
Received: 03/08/2012
Completed:
04/03/2012 Links to Helpful Information
McDowell County
Agronomist Comments
12 8 4
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
01S
1slCrop: Fes/OG/rim,M
.5T
120-200
0
0
0
0
0
0
.0 0
12
2nd Crop: Fes/OG/rim,M
0
120-200
0
0
0
0
0
0
.0 0
12
Test Results
Soil Class HM%
W/V
CEC B5196 Ac pW P-I K I
Ca%
Mg%
Mn-1
Mn-AI(1)
Mn-AI(2)
Zn-I
Zn-AI
Cu-1
S-I
SS -I NO3-N
NH4-N
Na
MIN 0.86
0.88
10.2 82.0 1.8 5.8 203 101
60.0
17.0
302
198
198
525
525
297
62
0.2
Field Information
-
Applied Lime
Recomnk dations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
INS
1st Crop: Fes/OG/Irn,M
0
120-200
0
0-20
0
0
0
0
.0 0
12
2nd Crop: Fes/OG/rim,M
0
120-200
0
0-20
0
0
0
0
.0 0
12
Test Results
Soil Class HM%
W/V
CEC BS% Ac pH P-I K-I
Ca%
Mg%
Mn-1
Mn-AI(I)
Mn-AI(2)
Zn-1
Zn-AI
Cu-I
S-I
SS-1 NO3-A'
NN4-N
Na
MIN o.60
o.86
11.1 89.0 1.2 6.4 L/ 97 75
66.0
20.0
223
145
145
267
267
125
45
0.1
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zu
B M,;
See Note
02S
1st Crop: Fes/OG/rim,M
.6T
120-200
0
0
0
0
0
0
.0
12
2nd Crop: Fes/OG/fim,M
0
120-200
0
0
0
0
0
0
.0 0
12
Test Results
Soil Class HM%
W/V
CEC BS•*6 Ac P-I K-I
Ca%
Mg%
Mn-1
Mn-AI(1)
Mn-AI(2)
Zn-I
Zn-AI
Cu-I
S-I
i�
SS -I NO3-N
NH4-N
Na
MIN 0.86
0.88
10.9 83.0 1.9 15.7 198 100
63.0
15.0
217
147
147
457
457
254
46,
0.1
Field Information
Applied Lime
Sample No. Last Crop
Mo Yr T/A
-Recommendations
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
2NS
Isl Crop: Fes/OG/rim,M
0
120-200
0
0
0
0
0
0
.0 0
12
2nd Crop: Fes/OG/r1m,M
0
120-200
0
0
0
0
0
0
.0 0
12
Test Results
---
Soil Class HM%
W/V
CEC BS•.6 Ac pH /P-1 K-I
Ca%
Mg%
Mn-1
Mn-AI(1)
Mn-AI(2)
Zn-1
Zn-AI
Cu-I
S-1
SS-1 NO3-N
NH4-N
Na
MIN 0.66
0.90
11.5 93.0 0.8 6.4 V 144 88
71.0
18.0
315
200
200
277
277
123
48
0.2

1

TtcDUS.AVonsie Divisittts
lPhnsae; �1 })733�2655 Web
Report No: 37339
Grog cr:
Deluca, Mario
4601t7Qsan VMey Dr
Copies 1'o:
£. t
a
Marfon:
NC 28752
Soil
AL
n eport
Farm..
SERVING N.C. RESIDENTS FOR OVLR 60 WARS
Received: 03108/2012 Completed: 04/0312012 Links to 11e1tNLtnformatian
McDowell County
Agronomist comments
�t 3
vid Ififormation
Sample lt0. L
Xo Yr TIS
Crop or Year
lime
N
P203
K-,O
'14
S
Cu
Zia
B3 31t1
see Vote
0tS
1st Crop: Fes/owrhn,m
5T
120-200
6
0
0
0
0
0
0 U
�U
2nd Crop: Fes/OG/TIm,M
0
120-200
0
0
0
0
0
0
,0 0
2
Test Results
SniI Cuss N. ; Cf'J1'
GhC BS96 Ac pH I'»I IC-u
Ga% tifg i
:'"fje-T
jfit-Aj()
yln-AI(2)
Zu-I Zn-fll
C44
S-1
SS-1 -VOj-,V
A N
a
MIN 0.86 038
16.2 810 1.8 5S 203 101
60.0 ITT
302
198
1988
525
525
21ri
62
0.2
;Field Inforti°�tida �'. �;
. �.pplied"dine Recoendatioiis .'; "
-
_,
✓ ".,.
t/
`.
Sample Bt*o. Lasi Crop
Alo Yr TtA Crop or Year
Lime
IV
P203
Kati
41S
S
Cu
Zat
B Aln
See Jvote
ItiS
1st Grog: Fes10G/r1m,M
0
120-200
0
0-20
0
0
0
0
.0 0
12
2ndCrop: Fes/OC/f1rn,N1
Q
120.200
G
0-20
0
0
0
0
.0 0
12
Test Results
sail Class "1% 1; /V
Ci=C BS% Ac p H P-1 K 1
Ca% ill
,11u4
Jln-AB(7)
Aln-AI(2)
Zn-I
Zn-AI
Cu-1
S-1
5S-1 ,VOJ-1
IN714-,v
Na
MIN 0.60 0.86
11.1 89.0 1.2 6,4. V 97 75
66:0 20.0
223
145
N5
267
267
125
45
0.1
Field Into sa#IttU . ,
Sp11ea1"T s u+e
""Reca ►entisiticr r , `
SarrtHe A10. Lust Crop
i Mo 'r AA
Crop or rear
ilrue
IV
P20-1
K20
htg
S
t tx
Zis
B Aln
See iota
02S
i
Ist Crop. res:"OG/rirn.N1
6T
120.200
0
0
0
0
0
0
eo 0
12
2nd Grope Fes 06/ ird M
0
120.200
0
0
0
0
0
0
.0 0
Test Results
Soil Class HJi v1 WAI
CEC B5 Ac pA P 7 K-I
Ca4b 14 v
Aln-1
Jfa 41(l)
AlIn.A1(2)
Zn-1
Zrt-Al
Cta-I
S-1
SS-1 VO3-s1'
tt714-ly
.4'a
MIN 0:86 0 Ss
119 83.0 119 5:7 198 100
63.0 .15,0
217
147
147
457
�57
254
46
0.1
i�ieldl"Itiiottu tint
pplied- auae
:'Recommctldatio s
✓.
✓
Sample lYn, Last Crop
So Yr TIA
Crop or Year
Lithe
,'F
P203
KzO
xg
S
Cat
Zn
P Mn
See Xote
2NS
Is( Crop: Fes 001ni'm
0
120-200
0
0
0
0
0
0
.0 "0
12
2nd Crop; Fes/06:"fina,m
0
120-200
0
a__
0
0
0
0
.0 0
%,�'
Test Results
j Soil Class 11J11% WIY
CEC BS% AC pH ✓ P-I K=t
Ca% xg%
Met-1
Aitt riC(Lj .
AlwiV(2)
Zn-I
7W-Al
Crt-I
S-I
SS-1 A'O3-JN'
VH4 ,V
Ilya
MIN 0,66 0 90
1).5 93.0 0.8 G A 144 89
71,0 180
315
200
200
277
277
123
48
0.2

NG4➢WS nomic ftisision
Oboac. (19)733-2 55
Gr,6 er. Deluca, Alario
No; 37339
Pg,2
Field Information
AppliWLime
Recommendations
Sample 0. Least Crap
Ato Yr 1%A i
Crop or fear
Little
Al
PaQs
K 0
A1,g
S
Of
Zia
& ft
See A'ote
03S
j
Ist C ropy Fes'OCYrillx,AI
3T
120.200
0
0-20
0
0
0
6
.0 0
i?
i
2odCrop; Fe ,100Yiim,hl
0
120-200
0
0-20
0
0
0
0
.0 0
12
Test Results
Soil Class 11W96 WIN
CGC BS
Ac p11 P-1 K1
Ca%
tfg%
Agra-1
3tnAl(1)
ffir.AI(2)
7.n-1
Ztt-:il
Ca4
S-1
SS-1 rt°03-N
A'114-Ar
,Ma
MIN 0,71 0,89
13.3 8.5.0
?.O 5.9 34F
m
80
66.0
16.0
14
121
121
710
�30
352
51
0A
Fieldlnformativra
Applied, use
fttcumWeadations
✓
✓
sample, Ara Least Crop
Ale Yr i` A
Cratj3 or Yearrime
N
1'205
&10
jig
S
Cra
7tt
B '11n
See Rule
03V
1st Crc,p; Grape,Nl
0
hate l8
0
0-2Ct
O
Q
O
0
5 0
t
2nd Crop: Grtpe,Ai
0
Note I8
0
0-20
0
0
0
0
.5 0
118
Test Results
Sell Class H.,V% W/V
CBC BSA
Ac p K P-1
K-1
Ca%
A1gl%
:eft€-1
Afn AI(l)
Alta-AI(2)
bi-1
7t€-N
Cu-1
S 1
SS-1 X03 .y'
aim-x
va
MIN 1,31 0,88
11.6 84.0
V
l,s 6.1 1g0
38
66.0
15,0
295
192
192
414
414
230
53
0.1
Field Information
Appiied.I iaite
Reco nsi endations
✓
✓
Sample'N'O. Last Crop
Ato Yr VA
Crop rtr Year
lime
4
P20.5
K20
mg
S
c a
Zn
B mn
See !vote'
004
ist Crop. Fes/Oc"'711101
0
1.20-200
0
10-30
0
0
0
0
.0 0
l
2ndCrop; FesYOGJirO,hl
0
120.200
0
10-30
0
0
0
0
.0 0
1L2
Test Results `
Sail Class 11M W/V
CBC BS o
Ac p 11 FYI
K-1
Co%
jf,
m-1
Aft-AI(i)
Ala-AI(2)
Zu-1
Zta-AI
Ca-1
S-1
SS-1 :1'03-AT
lfl4 -.jV
Iva
MIN 0.?0 018$
12,3 85,0
1.9 6.0 L/ 300
68
6-.0
:6,0
132
c'rG
96
(141
W
309
56
0:2
Field Information"
Applied -Lime
Recommendations
Sa uple .A`o. Last Crop
Aln Yr PA
j Crop or Year
Bate
IV
P205
K2O
Sig
S
Cn
Zta
B AIR
See (vote
005
1 "A crop: Fcs/06711111, f
0
120.200
0
0-20
0
0
0
0
.0 0
L2
2nd Crop: resi0GAIn,A9
0
120-200
0
0-20
0
0
0
0
.0 O
"T
Test Results
Son Clam II,31% t1IV
CBC BSA
Ac pit P-I
K-C
Cad£
Afg%
Ala-[rli'ta-AI(7j
Ain-AI(2)
7tr-1
Zn-AI
Cu-1
S-I
SSd A103-IN'
A714 ,Y
lVaa
INTIN O. s0 0,87
1144 56.0
✓
1:6 6.1 21.3
80
68,0
15.0
296
193
193
464
464
288
50
t1.2
Field information
Applied Lime
Recommendations
S;aaaPle ha. Last Crop
410 Yr 7' A
Craft or Year
Little
ti
P205
KzO
r11g
S
Cu
7tt
B mw
See Vole
;
06S
1st Crop: Fes/OGYTim,M
0
120-200
0
0
0
0
0
t)
0 PH$
j1
!i
1
2nd Crop; Ee5io(Yfi(n,M
0
120-200
0
0
0
0
0
0
.0 pHS
3 L
Test Results
Soliclass HAf% WIN
CgC BS%
Ae jtli P-1
K-1
Ca%
j(g,%
A1n-1
AW-r41(1)
Aft-d1(2)
Zu-1
Zn-AI
Cu-1
S-I
SS -I NO; ,1°
,V`I14-,V
MIN 0.51 O.87
11.7 9310 -
OS 6.7 123
94
70.0
20,0
362
224
>_24
319
319
246
49
0.2

�N.CDA& S,A ronemie' i%i lon
Phaiie: (19}733- 6 web slit www.p r goVagrononii/
Grog: i eluca, Maria
Report Nci: 31 39 ..
P 3
field lu%rwatioa`AvoliedLime
Rcetiulmend
Sample "Va Last Crop
AM Yr TIA
Crgp or Year
_.
Lime
41
P20..$
K20
.i1g S
Cu
Z11
8 41)1
See Note
j (AS
1S1 Crop_ I' 061fifil m
0
120-200
40-60
0
0 0
0
0
.0 0
2nd Crop. Fe0(WTiin,1i
0
120-200
4"0
0
0 {}
0
0
.0 0
1'2
Test Results
so//Class KAI% tC/V
CBC SP.'
At PH 1'-i K-1
Ca%
.V
�qn-1
ljfn-Ajq)
�qn-ail(2)
z11-1 its -AI
Cu-1
S-1
SS-1 , 03-V
'kW4-N
Sa
NIIN 0.51 0,83
8.1 88:0
1,0 6.3 36 87
59.0
23.0
339
216
216
144 144
102
84
0.1 4
Flela'Isxforn atlon,
Agpli d ilme
Rct6numea , tlon$
�::
; ✓
Sample,'Yo. Last crop
316 Yr 7M
Crop or fear
Lime
Ar
P203
IKO
AIS S
Ca
Zrt
B- Afn
See'vole
007
1st Crop: re rOG/Tim,M
0
120.200
30-50
0
0 0
0
0
.0 0
1_2
j
f
2nd Crop: Fes,/46,lim,&I
0
.120-200
30-50
0
0 0
0
0
.0 0
12
Teri Results
Soil Clnss HY% W/V
CEC BS%
At p H P-I ICI
Ca%,
Ug,%
3104
Afn-Al(T)
.3 n-A 2)
Zn-1 Zn-Al
Cn-1
S-1
SS-1 X03 .+V
AW-4-N
:fit
I+1i ti 0:46 0.77
10:6 89:0
1.2 6.2 42 177
77.0
24.0
266
I74
174
310 310
98
144
0.1
Field"""lulorsilation
Ap
ons =,
; , `°
,✓
✓
Sample 1'Yo. Last Crop
f11v Yr TIA
Crap or Year
iron
x
P205
K20
:mg S
CH
Zn
B gin
See Agate
OOS
IA Crop;, Fes/OG/lirri'm
0
120-200
0-20
0
0 0
0
0
.0 0
12
?nd Crap; FCS166, lm,m
0
120200
0-20
0
0 0
0
0
.0 0
i2
Test Results
soil Clan /IN% W/V
CEC BS96
At PH / P-1 K1
Ca%
Afg4a,
ilrt-1
Mtt-t1t(7)`
:1tn•Ai(2)
Zn-I Zit-A1
Cu-1
S-1
SS-1 n0J ,V
.1W44V
?Ya
NUN 0:36 0,90
10.3 89.0
1 J 6.3 Ski 119
610
22.0
444
279
279
16o 160
83
61
0.1
PI d,l fez T3on °�� `
pplled;Lime.
"
'° ecommenrlabtPUS . , �
.-
S'ample mo. last Crop
rtla Yr TIA
Crop or Year
Lime
rti
P20:1
X20
rlig S
Cu
Zn
B Alit
See Able
1406
let Crap: Fes/O(;1TIm,&J
0
120-200
60-80
0
0 0
0
0.
0 0
12
2nd Crop; fmto/ `insi
0
120.200
6o-8o
0
0 0
0
0
_0 0
2
Test Results
soil Cass MV% WIV
aC BS04
At PH P-1 K4
Ca
Xg%
1Vn-1
Agri-AI(1)
Zn-1 Zn-Ai
C11-1
S-1
SS-1 ,VO3-14
X1144'
ya ,
MIN OM 0.91
811 89.0
✓
0,9 6.4 29 114
54:0
28;0
5A
319
319
78 78
61
91
0.1.
Fidld,Tnnruaatin
„<..
; ApTslied 1Cime "
ecnriielsdatsiois ";
✓
✓
Sample No. Last G"op �
' -M1lo Yr,. TIA
Crop or Year
Lurie
h'
P201
K20
mg S
Gu
Z1a
B . airs
See;1vote
H07
1st Crop: Fes,/0G/7ifn,.M
0
120.200
0-20
0
0 0
0
0
.0 0
12
2nd Crop: Fes/oG;T1mm
0
120-200
6-20
0
0 0
0
0
.0
Kest Results
sr ll Class 11,31°3 W/V
CEC BS%
At pN ✓ P-1 K-1
CaS
s31g96
Mn-1
41n-Ai(l)
9tr-Al(2)
Z44 Zn-Al
Cu-1
S-1
SS-1 Y034
i�111-l'
Na
hllti 0.51 0,87
9.6 89:0
1.1 6A 59 160
50.0
30.0
521
324
324
98 9869
53
0.2
✓ ✓

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
1.2
13
14
15
Specific Oxygen Uptake Rate
- . SOUR
Facility Name: Corpening Creek
Biosolids Permit Number: WQ 0019960
Date: 4/5/2012
Digester Temperature: 19
Sampling Date/Time: 4/5/2012----- 0815
Sampled By:
Analysis Date/Time:
Analyzed By:
.Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
2-----0941
ar
1000 milliliters
1.8 % Dry Solids
25 degrees Celsius
25 degrees Celsius
Slope: 0.0
Intercept: 8.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.72 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.15 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 0.12 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Ar
.,r
Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Std. Methods 20th Edition
SM 2710B
Date: 4/5/2012
Time Sampled: 0815
Sampled By: L. Estes
Time Started Aeration: 0820
Time Stopped Aeration: 0940
Time Analyzed: 0941
Analyzed By: R. Carter
Total Time of Test: 1 hr. 41 mins.
Total time of test includes the time sample was aerated.

t
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor enin Cr
Biosolids Permit Number: WQ 0019960
Date: 4/4)
Digester Temperature:
Sampling Date/Time. 4/4/2012-----C
Sampled By: Lee Estes
Analysis Date/Time: 4/4/2012 ----- 1
Analyzed By: R. Carter
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.141
8.
8.
8
M
7,
7
7.
7.
1
1000 milliliters
0.61 % Dry Solids
25 degrees Celsius
25 dearees Celsius
Slope: 0.0
Intercept: 8.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.43 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.40 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rater 0.31 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Std. Methods 20th Edition
SM 271OB
Date: 4/4/2012
Time Sampled: 0933
Sampled By L. Estes
Time Started Aeration: 0938
Time Stopped Aeration: 1008
Time Analyzed: 1009
Analyzed By: R. Carter
Total Time of Test: 51 mins.
Total time of test includes the time sample was aerated.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Cor enin Creek
Biosolids Permit Number:
WQ 0019960
Date:
4/3/2012
Digester Temperature:
18
;
Date/Time:
4/3/2012--0915
1/Sampling
Sampled By:
Lee Estes
"
Analysis Date/Time:
4/3/2012-1058
Analyzed By:
Sample Volume:
R. Carter -
milliliters
1000
Total Solids:
0.37
% Dry Solids
Beginning Temperature:
25
degrees Celsius
End Temperaturel
25
degrees Celsius
Time
Dissolved Oxygen Level
(minutes)
m /l
0
7.7
1
7.62
2
7.54
3
7.48
4
7.41
5
7.34
6
7.22
7
7.15
8
7.12
.
9.
7M
10
6.94
1" 1
6.89
12
6.87
13
6.83
14
6.76
15
6.68
Slope: 0.1
Intercept: 7.7
Correlation Coefficient: 1.0
-
Oxygen Uptake Rate: 4.05 mg Oxygen/hr
Ambient
Specific Oxygen Uptake Rate: 1.10 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate:' 0.86 mg Oxygen/g/hr
Instructions:
Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab.
Marion, N.C.
Std. Methods 20th Edition
SM 2710B
Date: 4/3/2012
Time Sampled: 0915
Sampled By: L. Estes
Time Started Aeration: 0925
Time Stopped Aeration: 1058
Time Analyzed: 1059
Analyzed By: R. Carter
Total Time of Test: 1 Hr. 59 mins.
Total time of test includes the time sample was aerated.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor enin Creek
Biosolids Permit Number: WQ 0019960
Date: 3/27/201
Digester Temperature: 1
Sampling Date/Time.
3/27/12--09
Sampled By:
Lee Estes
Analysis Date/Time:
3/27/12--11
Analyzed By:
R. Carter
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Time
Dissolved Oxygen Level
(minutes)
Im /l
0
8.47
1
8.45
2
8.43
3
8.41
4
8.39
5
8.38
6
8.36
7
8.34
8
8.33
9
8.31
1'0
8.29
11
8.27
12
8.25
13
8.23
14
8.21
15
8.19
1000 milliliters
1.36 % Dry.Solids
25 degrees Celsius
25 degrees Celsius
Slope: 0.0
Intercept: 8.5
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.10 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.08 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166 /
Temperature Corrected Specific Oxygen Uptake Rate: r 0.06 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
STD, METHODS 20th Edition
SM 2710 B
DATE: 3 '.2'"12—
Time sampled: 0 F �S
Sampled By: 1-E
Time started aeration: ,�9 9s
Time stopped aeration: //00
Time analyzed: // 0,5J
Analyzed By: Ci _
Total time of test: 1 A" S—PL; '
Total time of test includes the time sample was aerated.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:pCorening CrBiosolids Permit Number:0019960
Date:31281
Digester Temperature:
Sampling Date/Time: L3/28/12--l
8/12--0
Sampled By:e Estes
Analysis Date/Time:
Analyzed By: R. Carter
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
18
00 milliliters
65 % Dry Solids"
25 degrees Celsius
25 deorees Celsius
0.1
8.5
1.0
Oxygen Uptake Rate: 3.22 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.50 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rater 0.39`mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Std. Methods 20th Edition
SM 2710B
Date: .3 - "->.v-/Z
Time Sampled:y 9V D
Sampled By:
Time Started Aeration: 09,�S
Time Stopped Aeration:_ /D-.SJ
Time Analyzed:®025�
Analyed By: e, C
Total time of Test: f JI P-t'
Total time of test includes the time sample was aerated.

Specific Oxygen Uptake Rate
SOUR
Facility Name:
Cor enin Creek
Biosolids Permit Number:
WQ 0019960
Date:
3/29/2012
Digester Temperature:
17
Sampling Date/Time:
3/29/12--0705
Sampled By:
Lee Estes
Analysis Date/Time:
3/29/12--0730
Analyzed By:
R. Carter
'Sample Volume:
1000
milliliters
Total Solids:
1.4
% Dry Solids
Beginning Temperature:
25 degrees Celsius
End Temperature: 25 degrees Celsius
Time
Dissolved Oxygen Level
(minutes)
mg/l)
0
6.75
1
6.67
2
6.62
3
6.56
4
6.51
5
6.46
6
6.43
7
6.39
8
6.35
9
6.31
10
6.28
11
6.24
12
6.21
13
6.16
14
6.13
15
6.09
Slope: 0.0
Intercept: 6.7
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 2.50 mg Oxygen/hr
Ambient
Specific Oxygen Uptake Rate: 0.18 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166 /
Temperature Corrected Specific Oxygen Uptake Rate: 0.14 mg Oxygen/g/hr,
Instructions:
Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Std. Methods 20th Edition
SM 2710B
Date:_3129/2012
Time Sampled:_0705
Sampled By:,L. ESTES
Time Started Aeration:,_NhA
Time Stopped Aeration:_N/A
Time Analyzed:_0730
Analyed By:_R. Carter
Total time of Test: 40 mins.
Total time of test includes the time sample was aerated.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor enin Creek
Biosolids Permit Number: WQ 0019960 -
Date: 4/2/2012
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
8.55
8.52
8.5
8.47
8.44
8.41
8.38
8.35
8.32
8.29
8.27
8.23
8.2
8.17
8.14
12--0800 '
stes
12--0940
ter
1006 milliliters
0.6 % Dry Solids Ll
25 degrees Celsius
25 dearees Celsius
Slope: 0.0
Intercept: 8.6
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 1.75 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 0.29 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166 /
Temperature Corrected Specific Oxygen Uptake Rate: 0.23 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
Sour Test
Corpening Creek Wastewater Lab
Marion, N.C.
Std. Methods 20th Edition
SM 2710B
Date: 4/2/2012
Time Sampled: 0800
Sampled By: L. Estes
Time Started Aeration: 0805
Time Stopped Aeration: 0940
Time Analyzed: 0941
Analyzed By: R. Carter
Total Time of Test: 1 Hr. 56 mins.
Total time of test includes the time sample was aerated.