WQ0019960_Annual Report_20110218

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CITY OF MARION, NC
2010 ANNUAL REPORT
LANP APPLICATION PROGRAM
NC PERMIT NO. WQ0019960
fl ECEIV ®
i78 28
Asheville Regional Office
A ..
RE. EIVED
FEB 19 7011
Information Procass419 tlnit
DW(alBa'

ANNUAL LAND APPLICATION CERTIFICATION FORM
,..WQ Permit#: WQ0019960 County: McDowell Year:
f�acilfty Name (as shown on permit): City of Marion
and Application Operator: Southern Soil Builders, Inc. Phone:
Land application of residuals as allowed by the permit occurred during the past calendar year?
2 Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A - Residuals Application Summary:
2010
336-957-8909
Total number of application fields in thepermit:
8
Total number of fields utilized for land application during the year:
6
Total amount of dry tons applied during the year for all application sites:
106.98
Total number of acres utilizes for land application during the year-F
89.4
Part B - Annual Compiance Statement:
Facility was compliant during calendar year 2010 with all conditions of the land application permit
(including but not limited to items 1-13 below) issued by the Division of Water Quality. e Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action
to ken.
I ) Only residuals approved for this permit were applied to the permitted sites.
2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or
the limit specified in the permit.
3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies
of laboratory results are attached.
4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached.
5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant
Loading Rates in 15A NCAC 02T .l 105(b) (applicable to 40 CFR Part 503 regulated facilities).
7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part
503 regulated facilities).
8) All monitoring and reporting requirements in 15A NCAC 02T .I I I I were complied with (applicable to 40 CFR Part 503
regulated facilities).
9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
I I ) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as
specified in the permit.
12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
13) All buffer requirements as specified on the permit were maintained during each appar6ofii
Part C - Certification: ((.;,,
"I certify, under penalty of law, that the above information is, to the best of my knowl@Belr& blots', true, accurate,
and complete. I am aware that there are significant penalties for submitting false information, includi the
possibility of fines and imprisonment for knowing violations." informationPProcessingl� a
2 R�l
Permittee Name and Title (type or print) agnature of Pe tt Date
-
-//-</ I/P-1-0
Sidjqturof Preparer* Date Signature of Ladd Applier Date
(if different from Permittee) (if different from Permittee and Preparer)
* Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B
WQ Permit Number: WQ0019960
Facility Name: City of Marion
Residual Source WQ # or
N00031879
NPDES #:
WWTP Name:
Residual Analvsis Data
Laboratory
1)
2)
3)
4)
5)
A&L Eastern Laboratories. Inc.
Parameter
(mg/kg)
Ceiling
Conc.
Limit
Sample or Composite Date
7-7- I 0
Percent Solids (%)
NA
2.76 V
Arsenic
75
7 ,/
Cadmium
85
2 t/
Copper
4,300
371
Chromium
NA
46
Lead
840
53 (/
Mercury
57
2.3 a/
Molybdenum
75
12 V
Nickel
420
23
Selenium
100
3 (/
Zinc
7,500
1010 v
Total Phosphorus
NA
20500
TKN
NA
64100
Ammonia -Nitrogen
NA
13800
Nitrate and Nitrite
NA
1 t/
For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits.
"I certify, under penalty of law, that this document ryas prepared under my direction or supervision in accordance with a system designed
to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant
penalties for submitting false information, includinc, the possibility of fines and imprisonment for knowing violations."
Sign It r �f I' parer * l )tttc
111-eparrr I. defined in -10 ( I R I'tu'( �0 3 V([ 1 ,ind I � A \(';\( ' I 1 ! (I ` (16 )
f)FNR FO FMI 112I20061

ANNUAL METALS FIELD LOADING SUMMARY FORM*
'12
Di
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
ty Name: City of Marion Total Dry Tons Applied (Annual): 15.71
rmit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Marion Deluca Owner: Anna Deebold Predominant Soil Series: Hayesville
Acres Used: 16 Acres Permitted: 16 Site #: K-0I Field #: K-0I
Residual Analvsis Data (Heave Metals and Total Phosphorus use mL,/ke, % Solids use Raw Percent #):
Sample or.
Com-
posite
Date
1
7/7/10
2
3
4
5
6
7
8
9 1
10
ILJ
12
% Solids
2.76
Arsenic 1
7
Cadmium
2
Copper
371
Chromium
46
Lead
53
Mercury
1 2.3
Molyb-
de um
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
Annual Heavv Metal Field Loadinjis (Calculated in Ibs/acre):
o
App.
Event
1 •:
EW
1 1
1 111
1 111
1 111
1 111
1 111
1 111
ffs 111
ff1 111
ffo 111
1 1 ,
.'
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111�
.••
1 •
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 •
1 1.1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•1
1 1�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111�
1 11
1 111
1 111
1 111
1 111
1 111
1 111
or, 1
KIT1711
KITI1
•
1 1 �
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 � I
••
1 1�
WIT,
1 111
1 111
1 111fffl
111
1 111
1 111
1 111
1 111
1 111
1 111
1 1�
1 11.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111Ely,
In1
11•
®
•:�
1 111
1 111
1 ill
1 111
1 111
Nor, 1
1 111
1 111
KITIT,1
1 111
1 111
•:�
Total
••
1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1
.•
"1 certify, under penalty of law, that this document was prepared under my airecnon or supervision in accoroance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations". G$ , ON I,/D ; 613-7
/ Az,
Si ature of LancrApplier
Date
rd
0,y
pdq
R ?q
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
PIlity Name: City of Marion Total Dry Tons Applied (Annual): 38.91
MF -mit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator:
Acres Used:
Marion Deluca Owner:
35.8 Acres Permitted:
Anna Deebold Predominant Soil Series:
35.8 Site #: K-02 Field #:
Hayesville
K-02
Residual Analvsis Data (Heave Metals and Total Phosphorus use me/kt?, % Solids use Raw Percent 4):
Sample or
Com-
posite
Date
1
7/7/ 10
2
3
4
5 j
6
7
8
9
10
11
12
% Solids
2.76
Arsenic
7
Cadmiuml
2
371
46
E
53
2.3
Molyb-
denum
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
Total©
©
0
©
0
• •.
Event
1•
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
.'
1 11�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11•
••.
1 :1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 :1
1 11
1 111
KITIT,1
KIT, 11
1 111
1 111
KITIT,1
WITIT,1
1 111
1 111
1 111
1 11
=�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
ROMMKITI1
1 111
1 111
1 111
MITI 11
ff, 111
KITIT,1
1 111
NITIM
ff1 111
1 111
1 11
�
1 1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
1 1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 1
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11
.®
•.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
••
Total
' •
�� .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
�� •
••
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Si ature of L d Applier
( -.2-7- 1 [
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Irility Name: City of Marion
mit #: WQ0019960
Operator: James Fisher Owner:
19.45
Braddock
Acres Used: 13.7 Acres Permitted: 13.7 Site #: F-0I Field #: F-01
Residual Analysis Data (Heavy Metals and Total Phosnhorus use rne/ka. % Solids use Raw Percent 9):
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
James Fisher Predominant Soil Series:
Sample orl
Com-
posite
Date
1 1
7/7/10
3
4
5 1
6 1
7
8
9
10
11
12
% Solids
2.76
Arsenic
7
Cadmium
2
Copper
371
Chromiu
46
Lead
53
Mercury
2.3
Molyb-
denum
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
Annual Heavy Metal Field Loadings (Calculated in Ibs/acre):
Total
1
2 1
3 j
4 1
5j
6
8j
91
10
11
12
DT/Ac./
_.Lj
App.
i
Event
1.42
Arsenic
0.020v
0.000
0.000
1 0.000
0.000 1
0.000
0.000
0.000 1
0.000
0.000
0.000
-0.000•
0.020
Cadmium
0.006
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.006
Copper
1.054
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1.054
Chromium
0.131
0.000
0.000
0.000
.0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.131
Lead
0.151
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.151
Mercury
0.007
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.007
Molyb-
0.034
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.034
den
Nickel
0.065
1 0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
1 0.000
0.000
0.000
0.065
Selenium
0.009
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.009
Zinc
2.868
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
2.868
Total
Phos-
58.220
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
58.220
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Z4
Si ature of Land Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
lity Name: City of Marion Total Dry Tons Applied (Annual): 4.49
P in 9: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: James Fisher Owner: James Fisher Predominant Soil Series: Braddock
Acres Used: 4.3 Acres Permitted: 4.3 Site #: F-02 Field 4: F-02
Resirinal Analvcis Data (14envv Metals and Total Phosohorus use mz/k2. % Solids use Raw Percent 4):
Sample or
Com-
posite
Date
1 1
7/7/10
2
3j
5
6
7
8
9
10
11
12
% Solids
2.76
Arsenic
7
Cadmium
2
Copper
371
Chromium
46
Lead
53
Mercury
2.3
Molyb-
denum
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
Annnsil Heaw Metal Field I,nndinus (t:alculate(I In ibs/acre):
0p1
DTETAvo/Aetpanc.lo
000000
1 111
1
1 111001
1 111
1 111
1 1
.'
1 11�
1 111
1 111
1 111
1 we11
1 111
MIT, 11
1 111
1 111
1 111
1 111
1 111
1 11�
...-
�
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•.11MMMWIT,1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1•.
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Kim
11MM
1 11
1 111
1 111
1 111
1 111
KIT, 11
1 111
1 111
1 111
1 111
1 111
1 111
1 11
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1
��
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111�
1 11.
1 11Muir,
1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 11.
®
1`
1 111
1 111
1 111
1 111
1 111I
1 ll
1 111
1 111
1 111
1 111
1 111
1•
Total
• •m
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
:1�
. •
"I certify, under penalty of law, that tnls ciocument was preparea unaer my uirecuuu ur supci vibluu i1, a.:tu1 u4i,t-r-
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
-),?-I
) /`
Sig ature of Lan pplier Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
ility Name: City of Marion Total Dry Tons Applied (Annual): 17.20
rmit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: James Fisher Owner: James Fisher Predominant Soil Series: Hayesville
Acres Used: 11.4 Acres Permitted: 11.4 Site #: F-03 Field 9: F-03
Residual Analysis Data (Leavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample orl
Com-
posite
Date
1 1
7/7/ 10
2 1
3 1
4
5
6
7 1
8
9
LOJ
11
12
% Solids
2.76
Arsenic
7
Cadmium
2
Copper
371
Chromium
46
Lead
53
Mercury
2.3
Molyb-
de u
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
Annual Heavv Metal Field Loadings (Calculated in Ibs/acre):
Total
..
1 1
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
girt 1
1 111
1 111
1 1
1 11•
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
t 111
1 111
1 111
1 11•
...
1 111
1 111
1 111
1 111
1 111
1 111
Imm
1 111
1 111
1 111
1 •
Nor, 1
Mir, 1
girl 1
t 111
Nor,11
1 11
more1
Moro 1
1 111
1 111
1 111
1 •
1 •1
1 111
1 111
1 111
1 111
1 111
1 111
ff1 111
1 111
1 111
1 111
1 111
1 .1
rum
1 11
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
Moro 1
1 111
1 11
��
1 1 .
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 111
1 1 •
1 1.•
1 111
ffly,1
1 111
1 111
1 111
1 111
1 111
WIT,
1 111
1 111
1 111
1 1••
®
1 11•
1 111
or, 1
1 111
1 111
1 111
1 111
1 111
1 111
1 I11
1 111
1 111
1 11•
®
1�.
1111
1 111
1 111
1 111
1111
1111
1 Ilt
1111
1111
1 111
1111
1�.
• .
Phos-
__phorus
"I certify, under penalty of law, that this document was prepared under my airection or supervision in accordance
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
Signature of Larff Applier
Date
DENR FORM MFLSF (12/2006)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Pecility Name:
rmit #:
Operator:
Acres Used:
City of Marion
WQ0019960
James Fisher Owner:
8.2 Acres Permitted:
Total Dry Tons Applied (Annual):
Cation Exchange Capacity (non 503 only):
James Fisher Predominant Soil Series:
8.2 Site #: F-04 Field #:
11.22
Hayesville
F-04
Poe;riiial Analvek T)nta Mi-nvv MPtnlc and Tntal Phasnhorus use mg1kg. IN, Solids use Raw Percent #):
Sample or
Com-
posite
Date
1
7/7/ 10
2
_3_j
4
5
6
7
8
9
101
11
12
% Solids
2.76
Arsenic
7
Cadmium
2
Copper
371
Chromium
46
Lead
53
Mercury
2.3
Molyb-
denum
12
Nickel
23
Selenium
3
Zinc
1010
Total
Phos-
horus
20500
A..n 1 t4no.m, Mato] Viald I .naflinae I( 'n1i ll1ntPri In Inwgerel:
..
©
a
o-
©
o
o
a
o
App.
Eventa
...
��
t l
R 1
It It,1
T il,
o Is if
Mir, le
mwm��W=
1 111
111
II 111
ffirom
II 111
1 111
i 111
1TM
�
M�
m
1 lII�
1111�
1 lil
1 11.
��IMMMMMMWMMMMMM
ero.
�
����
����
ll1�
III,
����
ff�m�
�
�
�
Q�
It Ift:
T Ott
Eire I�
ff� IIIe
m a M1
�
KIT,on,
t �11Me
� I M,
Il 111
I lil
I Ii
Total
Phos-
phorus
"I certify, under penalty of law, that this document was preparea unaer my alrecnon or super viswu III ak:wI U411..c
with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted.
I am aware that there are significant penalties for submitting false information, including the possibility of fines and
imprisonment for knowing violations".
f��
Sig ature of Land A plier
dv
Date
DENR FORM MFLSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion
Land Owner: Anna Deebold
Operator: Mario Deluca
d-rnn t Name- Fecrne
WQ Permit #: WQ0019960 Field #: K-01
Annual Dry Tons Applied: 15.7101 Site #: K-01
Predominant Soil Series: Hayesville
Cror) 1 Max. PAN: 202 Crop 2 Name:
Acres Utilized': 16
Acres Permitted: 16
Cation Exchange Capacity (non 503):
Crop 2 Max. PAN:
Volume applied
Volume
Residual Sources
Soil
Precip.
D
<
o
3
z
-
Nitrate
PAN Applied
Name of Crop Type
O
(enter one) Solids/
%
Applied per
(NPDES #, WQ#,
Cond.
Past 24
-
w w
m a
TKN
w o
and
(Ibs/acpe)
Receiving Residual
o
Liquid
Solids
Acre
Fert., Animal
(Dry'
Hrs.
o mow,
h"
> >
m'
Nitrite
Application
Cu. Yds Gallons
(Dry Tons/Ac)
Waste, etc)
Wet
Moist)
inches
a
'
.�
�w
o
mg/kg
mg/kg
mg/kg
Crop I
Crop 2
Crop 1
Crop 2
9-2010
r
136500
2.76
0.982
W00019960
dry
0
s
0.5
0.3
64100
13800
1
43.185
NA
Fescue
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0-000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
;e•.
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this for
TOTALS:
0
136500..
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
43-185
0.000
Lime Applied
Annuallbs/acre
0.014
0.004
0.729
0.090
0.104
0.005
0.024
0.045
0.006
1-984
40.262
Date
lbs/ac
Prior Years Cumulative Ibs/ac
0.109
0.095
13.475
0.448
1.697
0.083
2.348
0.8
0.212
33.322
12-2010
1000
Current Cumulative Ibs/ac
0.123 V
0.099
14.204
0.538,/
1.801,E
0-088,,
2.372„
0.845„
0.218"
35.306
Permitted C. P. L. R.****
36
34
1 NA
1338
1 267
15
1 NA
1 374
T 89
2498
Permit PAN Limit Ist/2nd Crop
202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tnat
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Date `** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
`*C.P.L.R.: Cumulative Pollutant Loadinv_ Rate
DENR FORM FSF (1212006)

ANNUAL LAND APPLICA"PION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: K-02 Acres Utilized: 35.8
Land Owner: Anna Deebold Annual Dry Tons Applied: 38.9011 Site #: K-02 Acres Permitted: 35.8
Operator: Mario Deluca Predominant Soil Series: Hayesville Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
CJ
0 Y
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #. WQ#,
Fert.. Animal
Waste, etc)
Soil
Cond.
(Dr`'
Moen)
Precip
Past 24
firs.
inches
D
.K -
n -
a a
<
w °
0.'
K
z �
= m
�5
TKN
mglkg
z
= �
; 3
a
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
(Ibs/acre )
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop. I
Crop 2
9-2010
338000
2.76
1.087
W00019960
dry
0
s
0.5
0.3
64100
13800
1
47.792
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
338000
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
47.792 1
0.000
Lime Applied
Annual Ibs/acre
0.015
0.004t.-
0.807L-
0.100-
0.115,
0.005,-
0.026-
0.050
0.007
2.196-
44.567
Date
lbs/ac
Prior Years Cumulative lbs/ac
0.101
0.116 ✓
36
0.095
0.099,,
34
13.592
14.399
NA
0.437
0.537
1338
1.701
1.816,
267
0.083
0.088,,
15
2.346
2.372
NA
0.799
0.849,i
374
0.205
0.212
89
33.36
35.556
2498
12-2010
1000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
vn
Signature of Land Applier
1-arl(
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface -0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant LoadinLy Rate
Dt_ N1: FARM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM °
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F-0I Acres Utilized: 13.7
Land Owner: lames Fisher Annual Dry Tons Applied: 19.4505 Site #: F-01 Acres Permitted: 13.7
Operator: James Fisher Predominant Soil Series: Braddock Cation Exchange Capacity (non 503):
Crop 1 Name: Fescue Crop 1 Max. PAN: 239 Crop 2 Name: Crop 2 Max. PAN -
Rr o
02
Volume applied
enter one Solids)
( )
Liquid
Cu. Yds Gallons
o
/o
Solids
Volume
Applied per
Acre
(Dry Tons/AC)
Residual Sources
(NPDES #, WQ#.
Fert.. Animal
Waste. etc)
Soil
Cond.
(Dn"
Wet.
Moist)
Precip.
Past 24
Hrs.
inches
>
R _
n a
w _
K
- r
c i
_
TKN
mg/kg
z 3
D
Qo_ x
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Cro17
Crop 2
Crop I
Crop 2
7-2010
169000
2.76
1.420
W00019960
dry
0
s
0"5
0.3
64100
13800
1
62.443
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
Of
1690001
As
Cd
Cu
Cr
Pb
Hg
Mo
Ni
Se
Zn
P
62.443]F
0.000
Lime Applied
Annual lbs/acre
0.020 y
0.006t.
1.054 V
0.131 w
0.151
0.007 v
0.034 t,
0.065
0.009t-
2"86
58.220
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.021
0.041 ✓
36
0.016
0.022
34
2.346
3.400
NA 1
1.757
1.888
1338 1
0.426
0.577,,
267
0.024
0.031
15
0.136
0.170
NA 1
0.224
0.289
374 1
0.034
0.043
89 1
8.045
10.913
2498
12-2010
1000
Current Cumulative Ibs/ac
Permitted C. P. L. R.****
Permit PAN Limit lst/2nd Crop
1 239
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
Signature of Land Applier Date **" Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
-'" ****C.P.L.R.: Cumulative Pollutant Loadinu Rate
()F NF, F 0f%N1 FSF ( 1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F-02 Acres Utilized: 4_3
Land Owner: James Fisher Annual Dry Tons Applied: 4.4886 Site #: F-02 Acres Permitted: 4.3
Operator: James Fisher Predominant Soil Series: Braddock Cation Exchange Capacity (non 503):
Crop I Name: Fescue Crop I Max. PAN: 239 Crop 2 Name: Crop 2 Max. PAN:_
` s
O
o
C
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry TonsrAc)
Residual Sources
(NPDES #. WQ#.
Fert.. Animal
Waste. etc)
Soil
Cond.
(Dr}
Moist)
Precip.
Past 24
Firs.
inches
�
r;
? a
at.
a °'
-
a
z 3
w
y a
. w
I'KN
mg/kg
?
c 3
c
G.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
Pp
(Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
7-2010
39000
2.76
1.044
WQ0019960
dry
0
s
0.5
0.3
64100
13800
1
45.911
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
1 0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS:
01
39000
As
Cd
Cu
Cr
Pb
Hg
Mo
N1
Se
Zn
P
45.911
0.000
Lime Applied
Annuallbs/acre
0.015
0.004,.-
0.775-
0.096L,
0.111V
0.005v
0.025,E
0.048,r
0.0060
2.109v
42.804
Date
Ibs/ac
Prior Years Cumulative Ibs/ac
0.064
0.079 ✓
36
0.011
0.015
34
1.629
2.404„
NA
1.167
1.263
1338
0.291
0.402
267
0.017
0.022,
15
0.094
0.119,,,
NA
0.153
0.201,,l
374
0.023
0.029,,
1 89
5.492
7.601-
1 2498
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
1 239
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
"Volatilization Rate: Surface - 0.5, Injection/incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant l.oadint! Rate
DFNR F (_1Rtv1 FSF (1212006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED O
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F-03 Acres Utilized:
Land Owner: James Fisher Annual Dry Tons Applied: 17.2063 Site #: F-03 Acres Permitted:
Operator: James Fisher Predominant Soil Series: Braddock Cation Exchange Capacity (non 503): -
Crop 1 Name: Fescue Crop I Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
N
11.4
11.4
Volume applied Volume Residual Sources Soil Precip. D K z D Nitrate Name of Crop Type
y Cond. - ; 3 PAN Applied
(DPast 24 s w ° w w TKN 3 and (Ibs acre) Receiving Residual
°3
Q ry Liquid Solids Acre Fert., Animal Wet Hrs. � c a i w Nitrite Application
Cu. Yds Gallons (Dry Tons/Ac) Waste. etc) Moist) inches mg/kg mg/kg mg/kg Crop I Crop 2 Crop 1 Crop 2
7-2010 149500 2.76 1.509 W00019960 dry 0 s 0.5 0.3 64100 13800 1 66.383 NA Fescue
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0_000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
0.000 0.000 0.000
Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form):
TOTALS: 01 149500As Cd Cu Cr Pb Hg Mo Ni Se Zn P 66.383 0.000 Lime Applied
Annuallbs/acre 0.021 ✓ 0.006 1.120, 0.139 0.160- 0.007ti 0.036L, 0.069v 0.009t, 3.048.- 61.869 Date Ibs/ac
Prior Years Cumulative lbs/ac 0.015 0.009 0.791 1.552 0.232 0.01 0.041 0.115 0.024 4.173
Current Cumulative Ibs/ac 0.036 ✓ 0.015V 1.911✓ 1.691 0.392 0.017,/ 0.077 0.184„ 0.033 7.221,E
Permitted C. P. L. R.**** 36 34 NA 1338 267 15 NA 374 89 2498
Permit PAN Limit lst/2nd Crop 1 202
9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of land Applier
1--71-1(
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
*"Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L..R.: Cumulative Pollutant Loading Rate
W-Nk FORM FSF (12/2006)
9 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
Signature of land Applier
1--71-1(
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
*"Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L..R.: Cumulative Pollutant Loading Rate
W-Nk FORM FSF (12/2006)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion WQ Permit #: WQ0019960 Field #: F-04 Acres Utilized: 8.2
Land Owner: lames Fisher Annual Dry Tons Applied: 11.2215 Site #: F-04 Acres Permitted: 8.2
Operator: James Fisher Predominant Soil Series: Braddock Cation Exchange Capacity (non 503):
Crop I Name: Fescue Crop 1 Max. PAN: 202 Crop 2 Name: Crop 2 Max. PAN:
O s
N e
o
Volume applied
(enter one) Solids/
Liquid
Cu. Yds Gallons
%
Solids
Volume
Applied per
Acre
(Dry Tons/Ac)
Residual Sources
(NPDES #, WQ#.
Fert., Animal
Waste, etc)
Soil
Cond.
D
( n'
t.
Moist)
Precip.
Past 24
Hrs.
inches
>
� �
r. -S
s �•
c w
0
w m
_
r w'
3
z
a:
# w
Y w
0
TKN
mg/kg
z
- 3
3
66 o
�.
mg/kg
Nitrate
and
Nitrite
mg/kg
PAN Applied
( Ibs/acre)
Name of Crop Type
Receiving Residual
Application
Crop I
Crop 2
Crop I
Crop 2
7-2010
97500
2.76
1.368
W00019960
dry
0
s
0.5
0.3
64100
13800
1
60.188
NA
Fescue
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
0.000
Residuals Applications totals on FORM FSF supp ( attach FORM
FSF supp to this form):
TOTALS:
01
97500
As
Cd
Cu
Cr
Pb
Hg
I Mo
Ni
Se
Zn
P
60.188
0. 000
Lime Applied
Annual lbs/acre
0.019 ✓
0.005,.
1.015 t,
0.126
0.145
0.006-
0.033
0.063„
0.008-
2.763-
56.088
Date
Ibs/ac
Prior Years Cumulative lbs/ac
0.025
0.044
36
0.02
0.025 V
34
3.353
4.368 v
NA
1.734
1.860
1338
0.505
0.650
267
0.021
0.027„
15
0.088
0.121
NA
0.241
0.304 ,,
374
0.054
0.062 v
89
9.147
11.910
2498
Current Cumulative lbs/ac
Permitted C. P. L. R.****
Permit PAN Limit Ist/2nd Crop
1 202
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that
qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false
information, including the possibility of fines and imprisonment for knowing violations."
A
Signature of Land Applier
1-)-7-1
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
"Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0
*** Mineralization Rates: Compost -0.1, anaerobially digested -0.2,
aerobically digested -0.3, raw sludge -0.4
****C.P.L.R.: Cumulative Pollutant Loading Rate
DE NR F ORM FSF 02/2006)

4,
PAN
Mineralization
as decimal
ITotal dry
tons/year
Acres
Applied on
Rate
0.3
TKN
64100
NH3
1 13800
NO3
1
NO2
0
% Solids
0.0276
106.98
89.4
PAN Surface
21991 mg/kgmg/kg 43.982 lbs/dry ton
4705.194 Ibs total PAN
52.63081 Ibs PAN/acre
PAN Injection
28891 mg/kgmg/kg 57.782 lbs/dry ton
6181.518 Ibs total PAN
69.1445 Ibs PAN/acre
Dry Tons/1000 gal.
0.115092
1 st year PAN
Surface Ibs.
4705.19436
1st -year PAN
Injected Ibs.
6181.51 336
Ibs./acre
Surface
52.6308094
Ibs./acre
Injected
69.14450067
MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg
mg/kg x .002 =Ibs/dry ton
1000 X 8.34 X %solids X sp. gravity "=dry tons/1000gal."
2000

SAR
Sodium Absorption Ratio
Na M /L
Ca(MglL)
Mq(Mg/L)
Na: Sodium (Mg/L) Equivalent weight: 23
55.2
364.32
121.44
Ca: Calcium (Mg/L) Equivalent weight: 20
Mg: Magnesium (Mg/L) Equivalent weight: 12
Na (ME)
T
Ca ME
M ME
2.4
18.216
10.12
Milli Equivalent = Mg/L / Equivalent weight
The amount of exchangeable sodium ions versus the
amount of exchangeable calcium 8 magnesium ions in a given material.
SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5
power
Permitting guidance is if greater than 10 require ESP in permit.
SAR = 0.6376127 (From Mg/L entered above)
SAR= 0.6375677 (From ME entered below)
Na ME Ca (ME) Mg (ME)
2.4 1 18.22 1 10.12

t f.
Page: t of 2
Report Number: 10-189-0209
Account Number: 46381
Submitted By: ZACH KEY
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
L A&L Eastem Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (80d) 743-9401 Fax [phone]
www.al-tabs-easWn.com
Project: MARION
NC CERT #257
REPORT OF ANALYSIS Date Sampled: 7/7/2010 11:00:00
Lab Number: 77362 Date Received: 07/08/2010 00:00
Sample Id : MARION Date Reported: 07/13/2010
Total Solids
2.76
27600
100.0
JM
U1/UWzu-1U Uy:UU
JIVI-Z041J0
Moisture '
97.24
100.0
JM
07/09/2010 09:00
SM-2540G
Total Kjeldahl Nitrogen
6.41
64100
10.0
JM
07/09/2010 09:15
SM-4500-NH3C-TKN
Total Phosphorus
2.05
20500
100
KM
07/09/2010 13:18
SW-6010B
Total Potassium
0.49
4870
100
KM
07/09/2010 13:18
SW-6010B
Total Sulfur
0.83
8270
100
KM
07/09/2010 13:18
SW-6010B
Total Calcium
1.32
13200
100
KM
07/09/2010 13:18
SW-6010B
Total Magnesium
0.44
4400
100
KM
07/09/2010 13:18
SW-6010B
Total Sodium
0.20
2000
100
KM
07/09/2010 13:18
SW-6010B
Total Iron
22000
1
KM
07/09/2010 13:18
SW-6010B
Total Aluminum
34100
10
KM
07/09/2010 13:18
SW-6010B
Total Manganese
263
1
KM
07/09/2010 13-18
SW-6010B
Total Copper
371
1
KM
07/09/2010 13 18
SW-6010B
Total Zinc
1010
1
KM
07/09/2010 13,18
SW-6010B
Ammonia Nitrogen
1.38
13800
10.0
JM
07/09/2010 09 15
SM-4500-NH3C
Organic N
5.03
50300
10.0
07/09/2010 09:15
CALCULATION
Nitrate+Nitrite-N
<1.00
1 00
JM
07/09/2010 09 15
SM-450ONO3F
Total Cadmium
2.0
1 0
KM
07/09/2010 13 18
SW-6010B
All values are on a dry weight basis except as noted by asterisk Detection lirnit on all N series is on a wet bans
L1Ur repOr!S dniJ (el(CrS d/e IGr `
the chen!S ami -ov 'u r! Ue rCUrplluCe(f m .:nnh• pr pr)r( rrOr (r!JY rur� reterenFlY t7rrr(ufr.
to the w014 the rf`s,14S qr (hP COmp,rny ur .rny ,!(IverhSu!O :rrv:. rPk'ir.l'e nr rrrher pr.phr dnrrnurtr,evnen(S wd1 i aY �!(!ldnurrt) Uur prn rr .wrlPe•n .IUfhUnldUun I �F/ v//
('auric McC;rotlry

Page: 2 of 2
Report Number: 10-189-0209
Account Number: 46381
Submitted By: ZACH KEY
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER, NC 28669
A&L Eastem Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 [phone] Fax [phone]
www.al-labs-eastef-n.com
Project: MARION
NC CERT #257
REPORT OF ANALYSIS Date Sampled: 7/7/2010 11:00:00
Lab Number: 77362 Date Received: 07/08/2010 00:00
Sample Id: MARION Date Reported: 07/13/2010
Total Chromium
46
5
KM
U7/UWZUIU 1.5:10
Jvv-oUIUD
Total Nickel
23
5
KM
07/09/2010 13:18
SW-6010B
Total Lead
53
5
KM
07/09/2010 13:18
SW-6010B
Total Arsenic
7.0
1.0
KM
07/09/2010 13:18
SW-6010B
Total Mercury
2.3
0.4
KM
07/09/2010 12:05
SW-7471A
Total Selenium
3.0
1.0
KM
07/09/2010 13:18
SW-6010B
pH (as received) '
7.84
0.01
JM
07/09/2010 09:15
SW-9045D
Total Molybdenum
12
5
KM
07/09/2010 13:18
SW-6010B
Coinments
All values are on a dry weight basis except as noted by asterisk
Our reports ana ieaers are for the exclusive and confidential u.%C n, our Utents dnd may not he
Detection. limit on all N series Is on a wet basis
reproduced to -hide ,v part not may, dnv reference he rnacte
rw"r�G
mC Gam^' -a
to the work, the tesu", Or the companv,n any advertising rte— •rrrease or other puhtr, .+rrngi,ncerner,ls
wdhnnl ohta,mog our prior wnrle•n turhonzation
1'aunc McGroary

Environmental Testing Solutions, Inc.
Project name: Marion WWTP
Collection date: 15-Apr-10
Date received: 15-Apr-10
Sample identification: CC SL - Grab
Certificate ®f Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number: 100415.506
Sample number: 70492
Parameter
Method
Result
RL
Units
Date
Analyst Footnotes
Analyzed
Percent Solids
SM 2540 G
3.40
%
22-Apr-10
JAB I
pl-1
SM 9045 C
6.4
S. U.
22-Apr-10
AGS 3
Mercury
EPA 7471A
3.10
0.57
mg/kg
28-Apr-10
RWF I
Aluminum
EPA 6010 B
20000
72
mg/kg
22-Apr-10
DJS I
Arsenic
EPA 6010 B
<14
14
nig/kg
22-Apr-10
DJS I
Cadmium
EPA 6010 B
<7.2
7.2
mg/kg
22-Apr-10
DJS I
Calcium
EPA 6010 B
13000
290
mg/kg
22-Apr-10
DJS I
Copper
EPA 6010 B
380
14
mg/kg
22-Apr-10
DJS I
Lead
EPA 6010 B
54
7.2
mg/kg
22-Apr-10
DJS I
Magnesium
EPA 6010 B
4100
72
rn kg
22-Apr-10
DJS I
Molybdenum
EPA 6010 B
<14
14
mg/kg
22-Apr-10
DJS I
Nickel
EPA 6010 B
<29
29
mg/kg
22-Apr-10
DJS I
Potassium
EPA 6010 B
4400
72
mg/kg
22-Apr-10
DJS I
Selenium
EPA 6010 B
16
14
mg/kg
22-Apr-10
DJS I
SOdillnl
EPA 6010 B
1800
430
mg/kg
22-Apr-10
DJS I
zinc
EPA 60I0 B
930
7.3
mg/kg
22-Apr-10
DJS 1
Sample identification: CC RIC - Grab
Sample number: 70493
Parameter
Method
Result
RL
Units
Date te
Analyst Footnotes
Anal
Reactive Cytuiide
SM4500 CN E
<0.12
0.12
mg/kg
19-Apr-10
ECt1EM 2
Reactive Sulfide
SM 4500 S D
3.65
0.24
mg/kg
21-Apr-10
ECHEM 2
h }rpe'nt
SM 846 1010
1
100
3-play-10
ECHEM 2
Sample identification: CC SL Fecal #5
Sample number: 70489
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 3.6 % 15-Apr-10 KEK
Mulitple Tube Fermentation Procedure SM 9221-E 720000 6.5 MPN 15-Apr-10 KEK

This report should not be reproduced, exept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
The results in this report relate only to the samples submitted for analysis.
LA
Environmental Testing Solutions, Inc.
Project name: Marion WWTP
Collection date: 15-Apr-10
Date received: 15-Apr-10
Sample identification: CC SL Fecal #6
Certificate of Analysis
PO Box 7565
Asheville, NC 28802
Phone: [phone]
Fax: [phone]
Project number
100415.506
Sample number: 70490
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 3.6 % 15-Apr-10 KEK
Muliiple Tube Vermentation Procedure SM 9221-E 1620000 6.5 MPN 15-Apr-10 KEK
Sample identification: CC SL Fecal #7
Sample number: 70491
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 3.6 % 15-Apr4o KEK
MUHWIC. Tube Fermentation Procedure SM 9221-E 828000 6.5 MPN 15-Apr-lo KEK
Footnotes:
RL Reporting Limit. Values are reported down to the Reporting Limit only.
I. Sample analyzed by Prism Laboratories, Inc.
2. Analyzed by Enviro Chemists, Inc.
3 Analyzed outside holding tine.

CIO
-0a
Environmental Testing Solutions, Inc.
Project nume: City of Marion
Certificate of Analysis
110 Box 7505
Asheville, NC 28802
Phone: [phone]o-1
I'ax: (828) 3.50-9308
Project number: 100408.504
Collection date:, ARptlmlUuu'`
Date received: 8-A1)1--10
Sample identification: CC Effluent - Composite Sample number: 70282
Parameter WDateAnalyzedResult RL Units Analyzed Analyst Footnotes
Cadmium EPA 200.7 <0.0010 0.0010 mg/L 13-Apr-to Nitzgerald I
Sample identification: CC Effluent- Grab
Sample rtunilier: 70281
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
CyLin ide,'f'otal slyt4500-CNE <0.0050 0.0050 mg/L 13-Apr-io Kcoward l
Sat plc idcntilicution: ,h;�,G1au..,,,;; Sample number:
70283
Parameter Method' Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 4.5 % 8-Apr-10 B[,S
MkIlitplc Tube Fermentation PCOeedure SM 9221-E 202500 8.1 [v1PN 8-Apr-10 KEK
Sample identificutitm: a JecaL# Gtab
Sample number: 70284
parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 4.3 % 8-Apr-10 B US
N<lulitple 'l'ubd Fcnuerttation Procedure SM 9221-E 193500 8.1 MPN 8-Apr-10 KI K
Sample identiticution: �t—cc' j"'fecal:#3 - Gr.glb::.,_ Sample number: 7028-S
parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Percent Solids SM 2540 G 4.6 % 8-Apr-10 BLS
Mulitple"I'uhe Fermentation Procedure SM 9221-E 920000 8.1 MPN 8-Apr-10 hEK
Sample idcntilicalion a, CC_SL Fec��l,#, -, G� ab.;; Sample number: 70286
Parameter Method Result RL Units Date Analyst Footnotes
Analyzed
Perccnl Solids SM 2540 G 4.4 % 8-Apr-10 BLS
N•tuligile'I'ubu Permentution Procedure SIV1 9221-E 644000 8.1 MPN 8-Apr-10 K1::K
This report should not be reproduced, wept in its entirety, without the written consent of Environmental Testing Solutions, Inc.
'Ihe results in this report relate only to the samples submitted for analysis.

Geometric mean calculation sheet
202500
193500
920000
644000
720000
1620000
828000
geomean 581272.3

l
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:.
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
6/1 /201
2
1-2010 1050
1/2010 1345
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.2
769
1.0
14.57 'mg Oxygen/hr
1.82 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rater 1.43mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name. Cor ening Creek
Biosolids Permit Number: WQ 0019960
Date: 6/2/2010
Digester Temperature: 21
Sampling Date/Time:'6
B.-2-2010 0745
Sampled By: Kirb
Analysis Date/Time: 6/2/2010 1030
Analyzed By: R. CARTER
Sample Volume: 1000 milliliters
Total Solids: 0.82 % Dry Solids
Beginning Temperature: 25 degrees Celsius
End Temperature:' ' 25 degrees Celsius
Dissolved Oxygen Level
Slope: 0.3
Intercept: 7.8
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 15.29 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.86 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.469mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically,

Time
(minutes)
0 -
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
facility Name: Coroenino Creek
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
10
10 0800
10 1030
Ililiters
Dry Solids
grees Celsius
grees Celsius
Slope: 0.3
Intercept: 8.0
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 15.66 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.84 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.44 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
151
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:.
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
1
1
1000 milliliters
0.88 % Dry Solids
25 degrees Celsius
25 dearees Celsius
Slope: 0.3
Intercept: 8.0
Correlation Coefficient: 1.0
Oxygen Uptake Rate. 17.72 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.01 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: #ht
g Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Sprea ecuteautomatically:

Time
(minutes)
0
1
2
3
4
5
6
.7
8.
9
1p
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor enin Creek
Biosolids Permit Number: WQ 0019960
Date: 6/7/2010
Digester Temperature: 22
Sampling Date/Time: 6-7-2010 0800
Sampled By:,B. Kirb
Analysis Date/Time: 6/7/2010 1033
Analyzed By: R. CARTER
Sample Volume: 1000 milliliters
Total Solids: 0.88 % Dry Solids
Beginning Temperature: 25 degrees Celsius
End Temperature: 25 degrees Celsius
Dissolved Oxygen Level
Slope: 0.3
Intercept: 8.2
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 15.92 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.81 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rater ' 1.42mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Coroerfina Creek
Biosolids Permit Number:. WQ 0019960
Date: 6/8/20
Digester Temperature:
Sampling Date/Time: 6-8-2010 0800
Sampled By: IML.
Analysis Date/Time: 6/8/2010 1044
Analyzed By: R. CARTER
Sample Volume: 10
Total Solids: l 0.
Beginning Temperature:
End Temperature:'
Dissolved Oxygen Level
Ililiters
Dry Solids
green Celsius
grees Celsius
Slope: 0.3
Intercept: 8.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 16.79 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.89 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: �1 4 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Is
Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor ening Creek
Biosolids Permit Number: WQ 0019960
Date: 6/9/2010'
Digester Temperature: 21
Sampling Date/Time: 6-9-2010 0800
Sampled By: B. Kirb
Analysis Date/Time: 6/9/2010 1044
Analyzed By R. CARTER
Sample Volume: 1000 milliliters
Total Solids: 1.03 % Dry Solids
Beginning Temperature: 25 degrees Celsius
End Temperature:: 25'degrees Celsius
Time Dissolved Oxygen Level
(minutes) (mail)
p 8.09
1 7.68
2 7.27
3 6.9
4 6.5
5 6.12
6 5.72
7 5.35
8 4.94
g 4.52
10 4.15
11 3.79
12 3.42
13 3.06
14 2.67
15 2.28
Slope: 0.4
Intercept: 8.1
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 23.18 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 2.25 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.76 mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name: Coming
Biosolids Permit Number: WQ 00199
Date: 6/
Digester Temperature:
Sampling Date/Time: 6/14/2010
Sampled By: Lee Estes
Analysis Date/Time: 6/14/2010
Analyzed By:. R. Carter
Sample Volume:
Total Solids:
Beginning Temperature:;
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
ree
1000 milliliters
1.02 %Dry Solids
25 degrees Celsius
25 degrees Celsius
0.3
8.1
1.0
17.85 mg Oxygen/hr
1.75 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.37mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

h
V
Time
(minutes)
0
1
2
3
4
5
6
7
8
9
10
11
12
13
14
15
Specific Oxygen Uptake Rate
SOUR
Facility Name:
Biosolids Permit Number:
Date:
Digester Temperature:
Sampling Date/Time:
Sampled By:
Analysis Date/Time:
Analyzed By:
Sample Volume:
Total Solids:
Beginning Temperature:
End Temperature:
Dissolved Oxygen Level
Slope:
Intercept:
Correlation Coefficient:
Oxygen Uptake Rate:
Ambient Specific Oxygen Uptake Rate:
Average Temperature:
Temperature Correction Factor:
WQ 0019960
6/15/201 C
2Z
6/15/2010 0941
Lee Estes
6/15/2010 1240
R. Carter
milliliters
% Dry Solids
degrees Celsius
degrees Celsius
0.3
7.5
1.0
17.39 mg Oxygen/hr
1.70 mg Oxygen/g/hr
25 degrees Celsius
0.783526166
Temperature Corrected Specific Oxygen Uptake Rate: 1.34mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

Specific Oxygen Uptake Rate
SOUR
Facility Name: Cor enin Creek
Biosolids Permit Number: WQ 0019960
Date: 6/17/2010
Digester Temperature: 22
Sampling Date/Time: 6/17/2010 0643
Sampled By: Lee Estes
Analysis Date/Time: 6/17/2010 0940.
Analyzed By: R. Carter
Sample Volume: 1000 milliliters
Total Solids: 0.85 % Dry'Solids
Beginning Temperature: 25 degrees Celsius
End Temperature: 25 decrees Celsius
Slope: 0.2
Intercept: 7.9
Correlation Coefficient: 1.0
Oxygen Uptake Rate: 12.97 mg Oxygen/hr
Ambient Specific Oxygen Uptake Rate: 1.53 mg Oxygen/g/hr
Average Temperature: 25 degrees Celsius
Temperature Correction Factor: 0.783526166
Temperature Corrected Specific Oxygen Uptake Rater 1.20mg Oxygen/g/hr
Instructions: Enter Data in the Blue Boxes. The Calculation and the Spreadsheet execute automatically.

ANNUAL PATHOGEN AND VECTOR ATTRACTION RED UC"IIVIN rutun W-L I Kuies)
Facility Name: City of Marion WQ Permit Number:
"S WWTP Name: Marion WWTP NPDES Number:
WQ0019960
NCO031879
` Monitoring Period: From 1/1/2010 To 12/31/2010
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) ❑ 1
Alt B (Alk Treatment) []
Alt. C (Prior Testing)❑
d
I
Alt.D (No Prior Test) [3Process
to Further Reduce Pathogengs ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying 0
Heat Treatment ❑
Thermophilic ❑
Beta Ray 111
Gamma Ray ❑
Pasteurization ❑
Class B: jAlt.
(1) Fecal Density ❑
Alt. (2) Process to Significantly Reduce Pathogens ❑
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑
Composting ❑
Aerobic Digestion ❑
Anaerobic Digestion ❑
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Sample
Type
na ynica
Tech -
Minimu
Geo. Mean
MaximumUnits
Fecal Conform
2 x 10 to the
6th power
per gram of
total solids
MPN
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Va)fnr Affrar+inn RPtlurtinn (15A NCAC 02T .1107) - Flease indicate alternative performeu:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) ❑
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
JAR. 8 (Drying - Unstable)
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed El
CERTIFICATION STATEMENT (please check the appropriate statement)
❑� "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
reauirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel property gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
L ,4 ,2,2 err c.� �J A �uc�� �-�►
Preparer N me and Title (type or print)
, attire reparer* Date
Dennis Key Southern Soil Builders, Inc.
Land Applier Name and Title (if applicable)(type or print)
Si ature of and Applier (if applicable) Date
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
DENR FORM PVRF 02T (12/2006)

wv ` tir
Page 1 of 2
Report Number: 10-335-0809
Account Number: 46381
www.aleastern.com
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER NC 28669
_.. I.. -A. 1o/1)1 nnln r,..... ! # A..-tac i.- 17/n7/,)nin
A&LEastem Laboratories, Inc.
7621 Whitepine Road Richmond, Vlrginla 23237 (904) 743A401 Fax [phone]
Grower:
MARION. NC Farm ID:
SOIL ANALYSIS REPORT Analytical Method(s):
Mehlich 3
Ante Of RAnort- 12/03/2010
Organic Matter'
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E.0
Sample ID
Lab
ENR
Mehllch 3
Reserve
K
Mg
Ca
Na
Soil
Buffer
H
Field ID
Number
% Rate IbslA
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm
Rate
P H
Index
meq/10og
meq/1Qog
F1
101 W
92 M
289
H
886
M
14
VL
5.8
6.76
1.7
8.8
12929
2.9
M 95
NC=84
NC=47
F2
H
56 L
330
H
936
M
15
VL
6.3
6.84
0.9
8.5
12930
2.5
L 88
157
NC=47
NC=29
F3
215 VH
124 M
H
1652
M
11
VL
6.6
6.85
0.8
13.6
12931
4.5
M 121
1495
NC = 179
NC = 63
F4
51 H
71 L
VH
1034
M
14
VL
72
0.0
8.8
12932
2.2
L 81
1401
NC=42
NC=36
K1
133 VH
199 H
2-22
H
1141
M
12
VL
)
6.65
2.8
10.9
12934
42
M 118
NC=111
NC=102
Percent Base Saturation
Nitrate •
Sulfur
Zinc
Manganese
Iron
Copper
Boron
Soluble Salta
Chloride
Aluminum
Sample ID
K
Mg
Ca
Na
H
NON
S
Zn
Mn
Fe
Cu
B
SS
CI
Al
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm
Rate
ppm Rate
ppm
Rate
ms/cm
Rate
ppm Rate
ppm
F1
0.22
VL
2.7
27.4
50.3
0.7
19.1
F2
0.28
VL
1.7
32.4
55.1
0.8
10.6
F3
0.48
VL
2.3
30.3
60.7
0.4
5.9
F4
0.31
VL
2.1
38.0
58.8
0.7
0.0
K1
0.26
VL
4.7
17.0
52.3
0.5
25.8
Values on this report represent the plant available nutrients in the Explanation of symbols: % (percent). ppm (parts per million), Ibs/A Irns report applies to samolelsI tested Samples are retained a
soil. Rating after each value' VL (Very Low). L (Low). M (Medium). (pounds per acre). ms/cm (milli -mhos per centimeter) n,eqg a../ 100 m- of thirty day. aher resting c GCa,
H (High). VH (Very High). ENR - Estimated Nitrogen Release (milli -equivalent per 100 grams) Conversions ppm x 2 = Ibs/A by p" m
C.E.0 - Cation Exchange Capacity Soluble Salts ms/cm x 640 = ppm analys s preoaretl oy. Aat Easlem Laoorerone. tnc
Paunc McGroary

a•
Page 2 of 2
Report Number: 10-335-0809 J
Account Number: 46381
wwwaieastem.com
Send To: SOUTHERN SOIL BUILDERS
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER NC 28669
A&L Eastem Laboratories, Inc.
7621 Whitepine Road Richmond. Virginia.23237 [phone] Fax (804) 271b146
Grower
MARION, NC
Farm ID_
SOIL ANALYSIS REPORT
Analytical Method(s):
Mehiich 3
Date Received: 12/012010 Date Of Analysis:
12102/2010 Date Of Report: 12/03/2010
Organic Matter
Phosphorus
Potassium
Magnesium
Calcium
Sodium
pH
Acidity
C.E C
Sample ID
Lab
Number
ENR
% Rate
Mehlich 3
Reserve
K
Mg
Ca
Na
Rate
Soil
PH
Buffer
Index
H
meq/100g
mraq/1o0g
Field ID
Ibs/A
ppm Rate
ppm Rate
ppm Rate
ppm
Rate
ppm Rate
ppm
195 VH
79 L
178
M
1317 M
12 VL
�s�
6.73
2.0
10.3
12935
4.1 M 117
NC = 162
NC = 40
v
Iron
Copper
Boron
Soluble Salta
Chloride
Aluminum
Percent Base Saturation
Nitrate
Sulfur
Zinc
Manganese
Sample ID
K
Mg
Ca
Na
H
NO3N
S
Zn
Mn
Fe
Cu
B
SS
Cl
Al
Field ID
%
%
%
%
%
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ppm Rate
ms/cm Rate
ppm Rate
ppm
0.18 VL
K2
2.0
14.4
63.9
0.5
19.0
Explanation of symbols: % (percent), ppm (parts per million), Ibs/A
meq/100g
This report applies to sample(s) tested. Samples are retained a
maximum of thirty days after testing. by
Pic
Ge��
Values on this report represent the plant available nutrients in the —
soil. Rating after each value: VL (Very Low), L (Low), M (Medium),
(p ). ms/cm ( �r centimeter),
(pounds per acre mill'f-mhos
= Ibs/A,
H (High). VH (Very High). ENR - Estimated Nitrogen Release.
(milli -equivalent per 100 grams). Conversions: ppm x 2
Analysis prepared by: ASL Eastem Laboratories.
Inc.
C.E.C. - Cation Exchange Capacity.
Soluble Salts mslcrn x 640 = ppm.
Pauric McGroary

Alnnn i1'iE" ;r. •, is}Y SOP
1.. Annual Land Application Certification Form
• Was a certification form. submitted? e s
• Was land application conducted during the reported year? �}
• Low many dry- tons and dry tons per acre were applied? q (, .Q �' Ca9 �? 1,08 r, �zd� I. ° y qf
• Were the applications within the pe.^r;itted amount?Y65.
• Verify PAN if more than 10 tons/acre
• Did it indicate compliance? y C5
• Was it signed by the appropriate people?'Y y
2. iYlonitoring
• Were the analyses conducted at the required frequency?l� ;09!,
• Were the metals analyses reported -on the Residual Sampling Summary Form7l�S't� ��
a Were the results reported in mg/kg? i�
• . Were the heavy metals within ceiling concentration permit limits? �\�
• If no, were the lab analyses attached? oC11
• Were all the required parameters tested? y�
• Was TCLP analysis conducted? v.iDO P, 4.rros
I�;�,�c�j�l;�� !+� zrdaus �e�ali �0; t✓�c4 = < 140�f f�s�-ifS 5tic r©o�i so c�r/� w/
3. Field Summary P-PA WAS n.4 veri:�led eaA ,
• Were the land application- events recorded on the Field Summary Forms? Y eS,
l 6! t?
• Was a Field Summary Form submitted for each field? ye,5
• Were all the residuals applied to permitted land? pf,3
• Were all the residuals applied from permitted sources?le -
• Were the field loading rates for each metal and PAN calculated (year to date)?Y.z 3-
• Were the cumulative pollutant loading rates calculated7yz 3' ( '•����
• Were the calculations correct? Ico - �
• Were the PAN loading rates -within permit Iimits7j.e,s
• Were the heavy metal cumulative pollutant loading rates within permit limits7YpS'
• Were the residuals applied on a suitable crop?y e-5
• Were the applications conducted during the crop's growing season? ye-S
• Were the Field Summary Forms complete? � .e5
4. Pathogen and Vector Attraction Reduction
• Was a signed copy of the Path®oen and Vector Attraction Reduction Form submitted?Y,�
• Did the form indicate the perit5d of coverage,'the residual class, and the pathogen reduction alternative and the
vector attraction reduction option used? wo. y Ws3 yN
•. Was the appropriate documentation to show path g n and vector attraction reduction included in the report?
• Was pathogen and vector attraction reduction demonstrated according to 40 CPR Part 5037
No -,;;> fire. )a4es' e ,ra U,4(2 5d_e
5. Soil 'Pests L7;> 5O u-2 &&-k R •% no-(
• Was a Standard Soil Fertility Analysis conducted for each application field?� s
• Were the soil H's 6.0 or greater for each application field. No �] k) All 3 �'�zlds ►�'c���� a l+�x�
P
�t Were the copper and zinc indexes in the soil less than 3000 for each
g application field?
1 ySis'� G4I7-n !hn
6. General
• Was the report in the proper format?l0
• Were any parts of the annual report rmssing7 h c o
• Was the report submitted on time7j25
* Any violations of ceiling concentrations should lie reported to-Pretreatmentfor..municipalities- nly. �
$pu.2 7� s
�k N2z .. r� Svk�w:.} pa t��vV�1t, C2 `N�,w• VJ�R (�> �_ q w

Class IB Pathogen Review
Alternative 1 - Fecal Coliform Density
• Was the sampling conducted at the required frequency? PLY
• Were seven samples taken? 1'0-5
• Was the geometric mean calculated and done correctly?y 4__3
• Did the results show compliance (less than either 2,000,000 MPN/gram of total solids or 2,000,000
Colony Forming Units/gram of total solids) yo—Y
• c
Alternative 2 - Use of Process to Significantly Reduce Pathogens (one of five)
• Was the sampling conducted at the required frequency?
Aerobic Digestion
• Was it an aerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was the time and temperature between 40 days at 20°C (68T) and 60 days at 15°C (59T)?
Air Drying
• Were residuals on sand beds or pave or unpaved basins for three months?
• Was theambient.temperature above 0°C (32T) for two months?
• Were the residuals partially digested?
• Were residuals exposed to atmosphere during two months above 0°C (riot snow covered)?
Anaerobic Di eg_stion
• Was it an anaerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was the time and temperature between 15 days at 35°C (95°F) to 550C (131T) and 60 days at 200C
(68-F)?
Composting
• Was it a. composting procedure (not natural decay under uncontrolled conditions)?
• Were logs submitted showing time and temperature?
• Was the temperature raised to 40°C (104T) or higher and remained at 40°C (104T) for five days?
• Did the temperature exceed 550C (13IT) for four hours during the five-day period?
Lime Stabilization
• Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing
kiln dust or fly ash)?
• Were logs submitted showing time and temperature?
• Was the pH raised to - 12 after two hours of contact?
• Were logs submitted showing time and pH?
• Was the temperature corrected to 25°C (77 17)?

Y
Vector Attraction Reduction Review
• Was the sampling conducted at the required frequency?
38% Volatile Solids Reduction
• Was there 38% reduction?
• Were lab sheets/calculations in report?
• Was the reduction on volatile solids (not total solids)?
• Was the samples taken at beginning of digestion process and before application
(Inspection)?
• Were calculations correct?
4.0-Dav Bench Scale Test
• Were residuals from anaerobically digested treatment (Inspection)?
• Were residuals anaerobically digested in lab?
• Was the test run for 40 days?
• Was the test done between 30°C (86°F) and 37°C (99°F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 17%?
• Were lab sheets/calculations in report?
• Were calculations correct?
30-Dav Bench Scale Test
• Were residuals from aerobically digested treatment (Inspection)?
• Were residuals aerobically digested in lab?
• Were residuals 2% or less total solids?
• Was the test run for 30 days?
• Was the test done at 20°C (681F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 15%?
• Were lab' sheets/calculations. in report?
• Were calculations correct?
Specific Oxygen Uptake Rate (SOUR)
• Were residuals from aerobically digested treatment (Inspection)? ye's
• Were residuals 2% or less total solids (dry weight basis) (not diluted)?ye'
• Was the test done between 10°C (50°F) and 30°C (86°F)?. ,,,s
• Was the temperature corrected to 20°C (68°F)? YES
• Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual
solids (dry weight basis)? NO bt, ,A c Aj o 2 Sa��l�s I W i I 1 • ,;j
• Was the sample holding time under two hours? Na �Itili�, (�1311�, 0,1110, pi7110,,wsho, w4ho a-d
• Was the test started withinl 5 minutes of sampling or aeration maintained? W 1.yj,o
N° 4-h 5ha
Ir�he
�oas nab jcG�r� AA_ a�rr' OIn3
V e�-

Environmental Chemists, Inc.
6602 Windmill Way Wilmington, NC 28405
.a [phone] (Lab) • [phone] (Fax)
710 Bowsertown Road • Manteo, NC 27954
ANALYTICAL & CONSULTING [phone]
CHEMISTS NCDENR: DWQ CERTIFICATE #94. DLS CERTIFICATE #37729
Customer:
ENVIRONMENTAL TESTING SOLUTIONS, INC.
PO Box 7565
Asheville, NC 28802
Attn: Kelley .Keenan
Date Sampled:
Sampled By:
Ci .ITDGF-
REPORT OF ANALYSIS
4%W14-0/1-110W
Client
Date of Report: May 3, 2010
Purchase Order #:
Report Number: 10-3475
Report To: Kelley Keenan
Project: Marion WWTP
Reactivity
Lab
Cyanide, Detection Sulfide, Detection
lashpo5,t,
Corrosivity,
Sample ID
ID
mg/Kg Limit mg/Kg limit
Atow
units
mg/Kg mg/Kg
Sludge
# 8252
< 0.12
0.12
3.65
0.24
WOW
6.69
Method Code
EPA 335.4
SM 4500 S D
SW 846,
1010
SM 4500 H B
Date Analyzed
04/19/10
04/21/10
05/03/10
04/21/10
Comments:
Results reported on an as received basis.
Reviewed by:�

fi
Environmental Testing Solutions, Inc.
PO Box 7565, Asheville, NC 28802
Phone: [phone], Fax: [phone]
Project Name: 1-MWIA-11-r-1
CHAIN -OF -CUSTODY / Analytical Request
Client Name:
Address:
Report to:
Phone:
PO Number:
Fax:
I Requested Analyses -1
PH Checked Upon Receipt
C1, 0.2 mpl Upon Receipt
Preservatives
I
Sample Identification
t
z
>
U
1!
U
4.
U
a
C5
r?,
&
z
+
�4
0
Field
~
U
CIO w
14
z
z
Temp. ('C) Comments
G
Temperature ("C)
F-TS
Ct
+
I bv�l S -1 . 0
Received on Ice:
Y N
Sealed Cooler:
Y N
Samples Intact:
I Y N
Additional Comments:
Printe" meZf SZ71er:
Signature of Sampler:
-1

S Southern.
S Soil
g Builders, Inc.
Monday, November 28, 2011
958 Hoots Road Roaring River, NC 28669
[phone] 9 Fax [phone]
Beverly Price
Aquifer Protection Section
Asheville Regional Office
2090 US 70 Highway
Swannanoa, NC 28778-8211
t
Reference: Request for additional information
City of Marion
Permit No. WQOQ19960
Dear Ms. Price
In a recent letter dated November 17, 2011; the Division conducted an inspection
of the City of Marion and found the parameters Copper, Zinc, and Manganese missing
from the soils analysis in the 2010 Annual Report.
I contacted A&L Eastern Laboratories, Inc. concerning the missing parameters; I
found out the following information:
1. The parameters missing had not been analyzed.
2. Too much time has past to have the parameters ran
3. The reason the parameters were not ran was because of confusion on
the chain of custody.
The confusion on the chain of custody came from box S 1 which is a test for
Organic matter, estimated nitrogen release, phosphorus, potassium, magnesium, calcium,
pH, buffer pH, hydrogen, CEC, and %.base saturation; box S2 which is Soluble Salts and
Sodium, and box S3 which is -test S1 plus sulfur, boron, zinc, manganese, copper, and
iron and box S23 which is test S3 plus soluble Salts and Sodium.

When the chain of custody was filled out, box S2 was checked instead the box
right beside it, box 523; which should have been the one marked. In a discussion with
A&L Labs, we have now made it standard practice to automatically run test S23 for all
Soil Samples sent in for analysis from Southern Soil Builders, Inc.
We regret that these three parameters were missing from the 2010 annual report,
however corrective action has been put into place to make sure that all required
parameters will be ran in all future soil analysis. Also, a soil analysis has been taken on
each field that the City of Marion land applied on in the calendar year of 2010 with all
parameters required ran. These samples are at A&L Laboratories, with copies of the
results being sent to the Asheville Regional Office as soon as we receive them, which are
expected early this week.
Also, the inspection noted that the Pathogen and Vecotr Attraction Reduction
(VAR) Form was not properly filled out; an updated copy of the VAR from has been
included with this letter.
Lastly, an updated map to show the reduced acreage for field K-1; due do a new
small vineyard that has a water supply well that has been added to the north east corner of
the field, is being completed and will be sent to the Division for review when it is
completed.
If you have any questions, please feel free to contact me at anytime at
[e-mail] or at [phone].
Zach Key,
Southern Soil Builders, Inc.
Cc: Larry Carver, WWTP Superintendent

ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules),
Facility Name: City of Marion
WWTP Name: City of Marion WWTP
Monitoring Period: From 1/1/2010 To
WQ Permit Number:
NPDES Number:
12/31/2010
WQ0019960
NCO031879
Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed:
Class A:
Alt. A (time/temp) [3Alt
B (Alk Treatment) [3Alt.
C (Prior Testing) ❑
YW
fl
gN
A1t.D (No Prior Test) [3
Process to Further Reduce Pathogengs ❑"
''
If applicable to alternative
performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑��
Class B:
Alt. (1) Fecal Density M
Alt. (2) Process to Significantly Reduce Pathogens ❑
7
If applicable to alternative
performed (Class
B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying ❑ Composting ❑
1 Aerobic Digestion 0
Anaerobic Digestion ❑
K 4 `» *i7. G� L 2X(Y T� e.'!� Ci Rj
ya N �d 3i
If applicable to alternative performed (Class A or Class B) complete the following
monitoring
data:
Parameter
Allowable Level
in Sludge
Pathogen Density
Number ot
Excee-
ces
Frequency
of Analysis
Sample
Type
Analytical
Tech -
m aue
Minimum
Geo. Mean
Maximum
Units
Fecal Coliform
2 x 10 to the
6th power
per gram of
total solids
MPN
202500
561272.3
1620000
_
mpn/g
0
7
grab
sm922le
CFU
1000 mpn per gram
of total solid (dry
weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per 4 grams
total solid (dry
weight)
Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed:
Alt.1 (VS reduction) ❑
Alt. 2 (40-day bench) ❑
Alt. 3 (30-day bench) ❑
Alt. 4 (Spec. 02 uptake) M
Alt. 5 (14-Day Aerobic) ❑
Alt. 6 (Alk. Stabilization ❑
Alt 7 (Drying - Stable) ❑
1 Alt. 8 (Drying - Unstable) ❑
Alt. 9 (Injection) ❑
Alt. 10 (Incorporation) ❑
No vector attraction reduction alternatives were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
0 " I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the
vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note
if you check this statement attach an explanation why you have not met one or both of the
requirements.)
"This determination has been made under my direction and supervision in accordance with the system
designed to ensure that qualified personnel properly gather and evaluate the information used to determine
that the pathogen and vector attraction reduction requirements have been met. I am aware that there are
significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
Dennis Key President Southern Soil Builders, Inc.
Land Applier Name and Title (if applicable)(type or print)
Signature of Preparer* Date Signature of Land
*Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26)
�
Li L
6F _ 0
DENR FORM;i RVRF 02T�(12/2006)�