WQ0019960_Annual Report_20080222

jS.i
CITY OF MARION, NC
2007 ANNUAL REPORT
LAND APPLICATION PROGRAM
NC. PERMIT NO. WQ0019960
tJ,1 CLQ
FEB 2 7 2060
A 'hvwills P,--)giallaf Offi
W-protection
RECEIVED
FEB 2 2 2008
WATER UUNL,:; -_ ,JN
Information Processing Unit

K d )I;
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0019960 County:
Facility Name (as shown on permit):
Land Application Operator:
McDowell
Year: 2007
City of Marion
Southern Soil Builders, Inc. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
❑ Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit: 19
Total number of fields land application occurred during the year: 4
Total amount of dry tons applied during the year for all application si—te;.TF 188,144
Total number of acres land application occurred during the year: 1 71.8
Part B:
Facility was compliant during calendar year 2007 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. (S Yes O No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation.
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Permittee Name and Title (type d print)
gature of Preparer*
(if different from Permittee)
Preparer is defined in 40 CFR Part 503.9 (r)
2-1 g - OE- )� �l
Date gnature of Land Applier
(if different From Permittee and Preparer)
j-a,�0-2
Date
DENR FORM ACF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0019960
Facility Name:
NPDES # or
WQ#:
City of Marion
NCO031879
WWTP Name: Corpening Creek WWTP
Laboratory: 1)
2)
3)
4)
5)
A&I_ Eastern laboratories, Inc.
Sample.1 WIVO—Pol- —
•
Composite Date
Percent Solids
It
--_
oil
Total• • •
11
-----------
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
G1 - Z (8—v4f
i at re of Preparer Date
V
DENR FORM RSSF (5/2003)

�. k , � ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Marion Total Dry Tons Applied (Annual):
WQ0019960 Cation Exchange Capacity (non 503 only):
James C. Fisher Owner: James C. Fisher
8.2 Acres Permitted: 8.2 Site #: F4 Field #:
27.388
F4
Recirlual Analvsis Data (Heavy Metals and Total Phos®horus use mtJki!. % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
3/20/07
2
3
4
5j
6
7
8
9
10
11
12
% Solids
3.37
Arsenic 1
2
Cadmium
Chromium
43
Copper
479
Lead
52
Mercury
2.2
Molyb-
denum
9
Nickel
24
Selenium
5.7
946
LPh
17700
Annual Heavv Metal Held Loadings (Ualculateci in Ibs/acre):
googol
00000000000
�
00000000000
�'�'
:
00000000000
...
..
00000000000
..
..
00000000000�
00000000000
.
00000000000
,
clerl um
�
.
00000000000
.
�
:
00000000000
®•
00000000000
• .
Total
P.E
..000000000000
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 27.403155
Owner: James C. Fisher Operator: James C. Fisher Cation Exchange Capacity (non 503):
Site #: F4 Field #: F4 Acres Utilized: 8.2 Acres Permitted: 8.2
o
„ o
CZ
CZ �
S eci
Totals
per
Acre
%
Solid
s
D Tons Per
Dry
Acre
Residual
Sources
(Summarize)
ite
Cond.
Dry.
Wet,
l,nches
precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
tili-
zation
Rate**
Miner-
all-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop l or Crop
2
Gala
Cu.Yd.
Report
Totals
in Gal.
Crop 1
Crop 2
3-20071
195000
23780
3.37
3.341848171
W WTP
dry
0
s
0.5
30%
61700
7400
1
133.614
#44#4#«
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
23780
As
Cd
Cr v1
Cu v
Pb
Hg
Mo.v
Ni
Se vi
Zn ✓
P
PAN I
PAN 2
Lime Applied
Annual lbs/acre
0.01336 v
0.0133C
0.28724
3.19972
0.34736
0.0147
0.06012
0.16032
0.03808
6.31928
118.236
133.614
0
Date
Ibs/ac
Current Cumulative Ibs/ac
0.01336 0.01336 0.28724 13.19972 0.34736 0.0147 0.06012 0.16032 0.03808 6.31928
0 0 0 0 0 0 0 0 0 0
36 34 1 ]338 267 15 NA 374 89 2498
2M
Prior Years Cumulative Ibs/ac
Permitted C. P. L. R.***
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepared under my utrecuun ur 5uNCrvIswu III accvIuau%.c wIuA a O.Yall...
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC- Incorporation
Signature of Land Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incort)oration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1.
DENR FORM FSF (5/2003)

, R j I ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 6.336
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: James C. Fisher Owner: James C. Fisher
Acres Used: 9.6 Acres Permitted: 9.6 Site #: F3 Field #: F3
Residual Analvcic Data (Heavy Metals and Total Phosuhorus use mp-/kg. % Solids use Raw Percent #):
Sample
or Com-
posite
Date
1
3/20/07
2
3
4
5
_6j
7
8 j
9
10
11
12
% Solids
3.37
Arsenic
2
Cadmiuml
2
Chromium
43
'i
Copper
479
Lead
52
Mercury
2.2
Molyb-
denum
9
Nickel
24
Selenium
5.7
Zinc
946
Total
Phos-
horus
17700
Anneal Heaw Metal VieId I.narlinus If'aleulatea In InVaerel:
My
1 11 •
�����������
1 11 •
.'®
1 1M1,
�����������
11 •
1 1 • :
���������0�
1 1 •
, ,
1 1 '
®�O���oO���
1 1 •
•
NO
Total
••
•
1
1
1
1
1
1
1
1
1
1
1
.'
.•
"I certify, under penalty of taw, that this document was preparea unaer my alrecnon or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
includin the possibility of fines and imprisonment for knowing violations"
I- jA- a$
Signa re of Land Ap ier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE' CONIPLETED AND SUBNII TIED FOR EACII .APPLICATION FIELD.
Y
PLACE A "N/A" IN A 131-ANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit 9: \\i(, 0019960 Annual Dn- Tons Applied: 6.39.40095
Owner: James C. Fisher Operator: Janies C. 1=ishcr Cation Exchangv Capacity (nun 503):
Site #: F3 Field #: F3 Acres Utilized: 9�6 .Acres Permitted: 9.6
oTotals
=
oPer
co
co 7Acre
eci
%
Solid
s
O Tons Per
Dry
Acre
Residual
Sources
(Summarize)
(e
Cond.
Dry.
Wet.
Moist
Inches
Precip.
Past 24
11rs.
Appli-
cation
Meth-
od *
Vol-
ill'
zation
Ratc *Y<
Ming-
ali-
ration
Retc
7 KN
I
Ammo
nia-
Ni-
troLen
Ni-
gate
and
\'iuite
PAN 1
I AN ,
Mus1 Select
Crop 1 or Crop
I p
-,
rRepo
Crop 1
Crop
3-2007
45500
4739.6
3.37
0.666048906
WV'T13
dry
0
S
304/t,
P.1700
7400
1
26.63
4t:=
1'eSCuc
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
()
0
12
TOTALS:
4740
As ✓
Cd
Cr
Cu tr
Pb ✓
1{ ✓
Mov
Ni V
Sc
7_11 ✓
P
PAN I
PAN2
Lime Applied
Annual lbs/acre
0.00264
0.00264
0.05076
0.63228
0.06864
0.0029
0.01189
0.03168
0.o0752
1.24872
23.364
26.63
0
Date
Ibs%ac
Current Cumulative lbs/ac
0.00264 0.00264 0.05676 0.63228 0.06864 0.0029 0.01189 0.03168 0.0(052 1.24872
0 0 0 0 0 0 0 0 0 0
36 34 1 NA 1338 267 15 NA 374 8() 2498
250
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit Ist/2nd Crop
"I certify, under penalty of law, that this document was prepares under my atrectton or supervision to accuruaucc .1 rill a svarcrrr
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
2.- l a8'�8 *Application Method: S - Surface, IN - Injection, INC- Incorporation
Signature ofland Applier Date **Volatilization Rate: Surface - 0.5, Injection/Incori)ora(ion - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the N-wt.SF Form. "rite FSF an (I NIFI-Su, are mathematically linkerISO this infonnarion needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row in properly complete the metals erluntions. ie. FSF ro V I to -NtF1.SF column # I.
DENR FORM FSF (5/2003)

I • ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
City of Marion . Total Dry Tons Applied (Annual):
WQ0019960 Cation Exchange Capacity (non 503 only):
Mario Deluca Owner: Mario Deluca
34.72
16 Acres.Permitted: 16 Site #: KI Field 0: KI
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Sample
or Com-
posite
Date
q
3/20/07
_2j
3j
4
5
6
7j
81
91
10j
11
12
% Solids
3.37
Arsenic
2
Cadmium
2
Chromium
43
Copper
479
Lead
52
Mercury
2.2
Molyb-
denum
9
Nickel
24
Selenium
5.7
Zinc
946
Total
Phos-
horus
17700
Annual Heavy Metal Field Loadings Calculated in lbs/acre :
WPM
e :
00000�00000
e
t
00�00�00�00
1 15 M
��00000000000©
•
00000�000�0
•
Molyb-
denurn
'
0000�000000
'
00000000000
i
Total
Phos-
.•
"I certify, under penalty of law, that this document was prepared under my direction or supervision to
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 34.710663
Owner: Mario Deluca Operator: Marion Deluca Cation Exchange Capacity (non 503):
Site #: K 1 Field #: K I Acres Utilized: 16 Acres Permitted: 16
Seci
e
Inches
Appli-
Vola-
Miner-
m
Amo
Ni-
Must Select
*
Gal.
L s
°
Totals
%
DryTons Per
Residual
Cond.
Precip.
cation
tili-
ali-
nia-
trate
Crop 1 or Crop
i=
C °
Cu.Yd.
per
Solid
Acre
Sources
Dry,
Past 24
Meth-
zation
zation
TKN
Ni-
and
PAN 1
PAN 2
2
*.
Report
Crop l
Crop 2
Totals
Acre
s
(Summarize)
Wet,
Hrs.
od
Rate
Rate
trogen
Nitrite
in Gal.
Moist
I
11.2007
247000
15438
3.37
2.169416438
WWTP
dry
0
s
0.5
30%
61700
7400
1
86.7376
####s###
Fescue
]
0
0
0
0
2
0
0
0
0
3
0
j
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
1
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
15438
As ,i
Cd
Cr,,
Cu,/
Pb
H ,i
Mo,/I
NiZ
Se
Zn ,/
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.00868
0.00868
0.18662
2.07886
0.22568
0.00955
0.03906
0.10416
0.02474
4.10564
76.818
86.7376
0
lbs/ac
Current Cumulative lbs/ac
0.07768 0.0846 0.18662 l l.1959 1.4296 0.07165y 2.3070 0.6661 0.1617 28.274
0.069 0.076 0 9.117 1.204 0.0621 2.268 0.562 0.137 24.169
36 34 NA 1338 267 15 NA 374 89 2498
250
pDate
Prior Years Cumulative lbs/ac
Pennitted C. P. L. R.***
Permit PAN Limit 1st/2nd Crop
"I certify, under penalty of law, that this document was prepareu uuuci my U[ICCIwII "I ,.UvuI V1311i■■ ■■■ a«�...a••.. •••-•• ���-�---
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
l d-S, *Application Method: S - Surface, IN - Injection, INC - Incorporation
ignature of1, d Applier Date **Volatilization Rate: Surface- 0.5. Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data.and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

_ , , ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 119.7
Permit #:
Operator:
Acres Used:
WQ0019960 Cation Exchange Capacity (non 503 only):
K2
Residual Analvsis Data (Heave Metals and Total Phosphoric ice mo/ka- 0/. CnlidQ 11QP Raw PPrrnnt 14�.
38
Mario Deluca Owner: Mario Deluca
Acres Permitted: 38 Site #: K2 Field #:
Sample
or Com-
posite
Date
3/20/07
L2J
3
4
L 5j
L 6j
7
8
9
10
11
12
% Solids
3.37
Arsenic
2
Cadmiumi
2
Chromium
43
Copper
479
Lead
52
Mercury
2.2
Molyb-
denum
Nickel
24
Selenium
5.7
Zinc
946
Total'
Phos-
horus
17700
r+lluual ncavy ivieta i rieia L,oautngs (Catcuiatea in ins/acrei:
-
©
©
in
�71W' iffffft'�Sb
1 1 •
���������1
�1
�
1 1 • '',
®
o o'
�����������
• •'
•
1
1
1
1
1
1
1
1
1
1
1
• •
1 «l Uly, u11uC1- pralully U.1 law, ulal finis uocument was preparea unaer my airection or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
i7�� Z/__�_/ /-c�-3-u�
Signature of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 119.730708
Owner:
c;#A 41- K2
Mario Deluca
Field #:
Operator:
K2
Marion Deluca
Acres Utilized: 38
Cation Exchange Capacity (non 503):
Acres Permitted:
38
S eci
e
Inches
Appli-
Vola-
Miner-
Ammo
Ni-
Must Select
Gal.
L s
Totals
%
D Tons Per
Residual
Cond.
Precip.
cation
till-
all-
nia-
trate
Crop 1 or Crop
Per
Solid
ry
Sources
Dry,
TKN
Ni-
PAN l
PAN 22
Acre
(Summarize)
Wet
Past 24
Meth-
zation
zation
and
VTeoptaort
Acre
s
Hrs.
od*
Rate**
Rate
trogen
Nitrite
Crop 1
Crop 2
3-2007
429500
422500
11303
11118
3.37
3.37
1.588347513
1.562460592
WWTP
WWTP
dry
dry
0
0
s
s
0.5
0.5
30%
30%
61700
61700
7400
7400
1
1
63.5053
62.4703
######4
#######
Fescue
Fescue
]
2
11-2007
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS: 122421
As Cd Cr Cu ✓ Pb,- H v Mo Ni ✓ Sevi Zn v P PAN 1 PAN 2
Lime Applied
Annuallbs/acre
0.0126 +� 0.0126 0.2709 3.0177 0.3276 0.01386 0.0567 0.1512 0.03591 5.9598 111.51 125.976 0
Date
lbs/ac
Current Cumulative lbs/ac
0.0816 ,/ 0.0886 0.2709 12.1347 1.5316 0.0759 2.3247 0.7132 0.1729 30.1288 +/
0.069 0.076 0 9.117 1.204 0.0621 2.268 0.562 0.137 24.169
36 34 NA 1338 267 15 NA 374 89 2498
250
ja J:��
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of -law, that tnts aocumeni was preparcu u„uu, ,,,y l �..�,.. _.�•�•• ••• ----�� _-_._ _ ______
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
l --i8'0J *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of La Applier Date **Volatilization Rate: Surface - 0.5. Iniection/Incomoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # I to MFLSF column # 1.
DENR FORM FSF (5/2003)

z , • ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: _
W WTP Name: _
Monitoring Period:
City of Marion
Corpening Creek WWTP
From l/l/2007 To
Permit Number:
NPDES Number:
12/31 /2007
WQ0019960
N00031879
Pathop-en Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed:
Class A:
Alternative l ❑
Alternative 2 ❑
LAlternative 3 ❑
Alternative 40 1
Alternative 5 ❑ 1
Alternative 6 ❑
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 10
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization ❑
Air Drying
Composting jAerobic
Digestion
Anaerobic Digestion[]
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Parameter
Allowable Level
in Sludge
g
Pathogen Density
Number o
Excee-
Frequency
of Analysis
Sample
Type
Analytical
Tech-niqu
Minimum
Geo. Mean
aximu
Unitsences—
Fecal Coliform
2x 10tothe 6th
power MPN per
gram of total
solids or 2 .r 10 to
the 6111 power
CFU per gram of
29412
########
4248366
MPN/g
0
8
grab
sm9221 e
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
(in lieu of fecal
coliform)
3 MPN per
grams total solid
(dry weight)
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 10ption 2 ❑ 1 Option 3 ❑ 1 Option 4 ❑ 10ption 5 ❑
Option 6 10ption 7 ❑ 10ption 8 ❑ 10ption 9 ❑ 10ption 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
Yg)re of Preparer Date
Dennis Key President Southern Soil Builders, Inc.
Land Applier Name and Title (if applicable)(type or print)
Signature of Lan Applier (if applicable) Date
DENR FORM RF (5/2003)

Report Number
1307081-8006 A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond. Virginia 23237-2290
46381 Phone (80-4 )7-t 3-9401 • Fax [phone]
Websitc: ol'l'icc@iil-laps-ca,tern.com
TO: SOUTHERN SOIL BUILDERS FOR: MARION
958 HOOTS ROAD
ROARING RIVER, NC 28669 NC CERT #257
ATTN: DENNIS KEY
LAB NUMBER: 41637
SAMPLE ID: MARION
REPORT OF ANALYSIS
copy: ZACH KEY
DATE SAMPLED
DATE RECEIVED
DATE REPORTED
EP
3/20/2007 0500
3/22/2007 1200
3/27/2007 PAGE: 1
Solids, Total (As is)
3.37
33700
100
JM
03/22/07
16:00
SM 2540G
Nitrogen, Total Kjeldahl
6.17
61700
100
JM
03/23/07
16:00
EPA 351.3
Phosphorus
1.77
17700
100
JM
03/23/07
16:00
SW 846-601013
Potassium
0.37
3700
100
JM
03/23/07
16:00
SW 846-6010B
Sulfur
0.96
9600
100
JM
03/23/07
16:00
SW 846-6010B
Calcium
1.43
14300
100
JM
03/23/07
16:00
SW 846-6010B
Magnesium
0.39
3900
100
JM
03/23/07
16:00
SW 846-6010B
Sodium
0.17
1700
100
JM
03/23/07
16:00
SW 846-6010B
17700
1
JM
03/23/07
16:00
SW 846-601013
Iron
18400
10
JM
03/23/07
16:00
SW 846-6010B
Aluminum
303
1
JM
03/23/07
16:00
SW 846-6010B
Manganese
479
1
JM
03/23/07
15:00
SW 846-6010B
Copper
946
1
JM
03/23/07
16:00
SW846-6010B
Zinc
Nitrogen, Ammonia (as N)
0.74
7400
10
JM
03/23/07
14:00
EPA 350.2
Nitrogen, Organic (N)
5.43
54300
100
DCH
CALCULATION
< 1
1
DH
03/23/07
15:00
SM 4500-NO3F
Nitrogen, NO3+NO2
2.0
1
JM
03/23/07
16:00
SW 846-6010B
Cadmium
43
5
JM
03/23/07
16:00
SW 846-6010B
Chromium
All values are on a dry weight basis except as noted. 'Detection Limit on all N series is on a wet basis
Out reports atul letters are for the ea elusive and confidential use of our clients, arid may not he reprodtu;ed rn whole or rn part nor may any reference he tnade �aJ
to the work the results, or the company in any advertising, news release. or other public announcements without obtaining ow poor wntten autftOr12atton PAUL C H CHU

Report Number
R07081-8006 A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237-2296
46381 Phone [phone] • Fax [phone]
Websitr: www.al-labs-eastern.com • t -mail: [e-mail]
To: SOUTHERN SOIL BUILDERS FOR: MARION
958 HOOTS ROAD
ROARING RIVER, NC 28669 NC CERT #257
ATTN: DENNIS KEY
LAB NUMBER: 41637
SAMPLE ID: MARION
REPORT OF ANALYSIS
ffAtLg
copy: ZACH KEY
DATE SAMPLED: 3/20/2007 0500
DATE RECEIVED: 3/22/2007 1200
DATE REPORTED: 3/27/2007 PAGE: 2
Nickel
24
5
JM
03/23/07
16:00
SW 846-601OB
Lead
52
5
JM
03/23/07
16:00
SW 846-601OB
Arsenic
2.0
0.2
KM
03/23/07
15:00
SW 846-7061A
Mercury
2:2
0.4
KM
03/26/07
15:00
SW 846-7471A
Selenium
5.7
0.2
KM
03/23/07
15:00
SW 846-7741A
Molybdenum
9
5
JM
03/23/07
16:00
SW 846-601OB
All values are on a dry weight basis except as noted. 'Detection Limit on all N series is on a wet basis
Our reports and letters are for the exclusive and confidential use of out clients. and may not be reproduced rn whole or in part. not may any reference be made qa,,L
to the work, the results, or the company in any advertising, news release, of other public annourrcemetits without obtaining our prior written authorization
PAUL C H CHU

A&L Eastern Laboratories, Inc.
7621 Whitepine Road Richmond VA 23237 Tel: [phone] Fax: [phone] Email: officc al-labs-eastem.com
Biosolids Sample Transmittal Form - Chain of Custody
® Customer Information
Charge To Name &Address) Copy To (Name & Address)
ame & Address) 9
foil -
U 5 Builders ,.�Q�
fd `^ Roa:f£:n IFiIYe�, INC 28M
'FDJCCA
Sample Inform
Coltectlon information Container Into
Lab Number
Sample ID (Lab Use
Only) Type Date Time of Bottles Type
?� `3-ao 0 7 y`: o p _Glass
Grab
Composite
Glass
Grab -- Plastic
Composite
Glass
Grab — Plastic
Composite
Glass
Grab — Plastit
Composite
Account #
g63.91
Lion
oration
please Check Desired Tests
Vitals
Nitrogen
pH
OCE
Ag
C!
Volatile
SL1
SL2
Series
ol�rs
pVodlurnne
Y
k
x
—a�
oz
pint
_ oz
pint
_ oz
pint
t

Jail CJ ua 11: 1'fa 1.1 l r ur 11FIN lull
ace Analytical v
i
www.pacelabs.com
Pace Analytical Services, Inc.
Pace Analytical Services, Inc.
9800 Kincev Avenue, suite 100
2225 Riverside Orile
Huntersviile, NC 28078
Asheville, NC 28804
Phone: [phone]
Fhone: 628 254. 7176
Fax: [phone]
Fax: [phone]
Lab Project Number: 92138304
Client Project ID: CORPENING CREEK SLUDGE
Solid results are reported on a dry Height basis
Lab Sample No: 92C019926 Project Sample Number: 92138304.001 Date Collected: 02/16/07 10:42
Client Sample ID: CC PH/CORR S1 Matrix: Soil . Date Received: 02/16/07 12:30
Parameters Results Units Report Limit Analyzed By CAS No. ual P.egLat
Wet Chemistry
PH Method:'EPA 9045
DH 6.83 units 02/22/07 16:00 MDK
Date: 02/2e107
Asheville Certification ID
NC Wastewater 40
NC Drinking Water 37712
SC 99030
FL NEL,AP 587648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�`nAhr
Page: l of 5
Charlotte Certification
IDs
NC Wastewater
12
NC Drinking Water
31706
SC
99006
FL NELAP
E87627

g Jan.25 08 11:14a CITY OF MARION
aceAnalytical
www, pacelabs. com
Lab 5anple No: 928020007
Client Sample ID: CC TCLP-3. 51
828 658 1858 P.e
Pace Analytical Services, Inc. Pace Analytical Servicas, Inc.
9800 Kincey Avenue. Suite 100 2225 Riverside Drive
Nuntersville, NC 28078 Asheville, NC 28804
Phone: [phone] Phone: [phone]
Fax: [phone] Fax: [phone]
Lab Project Ntmber: 92138304
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92138304.002 Date Collected: 02/16/07 10:47
Matrix: Soil Date Received: 02/16/07 12-30
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual RegLnt
Metals
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
0.065
mg/l
0.025
02/22/07
13:57
EWS
7440.38.2
-Barium
0.13
ng/1
0.025
02/22/07
13:57
EWS
7440-39-3
Cadmium
NO
ng/l
0.0060
02/22/07
13:57
EWS
7440.43.9
Chromium
NO
ng/l
0.025
02/22/07
13:57
EWS
744C•41.3
Lead
NO
Mg/1
0.025
02/22/07
13:57
EWS
7439-92.1
Selenium
NO
ng/l
0.050
02/22/07
13:67
EWS
7782.49.2
Silver
NO
109/1
0.025
02/22/07
13:57
EWS
7440.22.4
Date Digested
02/21/07 07:00
02/21/07
07:00
Metals, Trace [CP
Aluminum
Ar5eric
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
Nickel
Potassium
Calani iim
Sod i um
Z-,nc
Date Digested
Mercury, CVAAS, TCLP Leachate
Date Digested
Mercury, CVAAS, TCLP Leachate
Mercury
Mercury, CVAAS, in Soil
Mercury
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 02128/0,
Asheville Certification Ids
NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
Prep/Method: EPA 3050 / EPA 6010
3900
mg/k.g
280
ND
mg/kg
14.
NO
mg/kg
2.8
3000
mg/kg
280
82,
mg/kg
14.
NO
ng/kg
14.
1000
ng/kg
280
NO
mg/kg
14.
NO
ng/kg
14.
NO
mg/kg
2800
hin
nn 14 n
'iG
NO
mg/kg
2800
88.
mg/kg
28.
02/23/07 06:45
Method: EPA 7470
02/19/07 13:30
02/23/07 20:00 EWS 7429.90.6
02/23/07 20:00 EWS 7440-38.2
02/23/07 20:00 EWS 7440.43-9
02/23/07 20:00 EWS 7440.70.2
02/23/07 20:00 EWS 7440.50.8
02/23/07 20:00 EWS 7439.92.1
02/23/07 20:00 EWS 7439.95.4
02/23/07 20:00 EWS 7439.98.7
02/23/07 20:00 EWS 7440.02.0
02/23/07 20:00 EWS 7440.09-7
niin,?rn-r )n.nn rwr iinn en n
02/23/07 20:09 EWS 7440.23.5
02/23/07 20:00 EWS 7440.66.6
02/23/07 06:45
02/19/07 13:30
Method: EPA 7470
0.00036 mg/1 0.00020 02/20/07 11:29 ALV 7439.97.6
Method: EPA 7471
2.9 ng/kg 0.13 02/20/07 12:50 ALJ 7439.97.6
Method: X Moisture
95.9 X 02/20/07 18:06 TNM
Page. 2 of 5
REPORT OF LABORATORY ANALYSIS Charlotte
Certification
ertificatio 10s
This reporl shall not be reproduced, except in fu
ll NC Water 37706
12
without the written consent of Pace Analytical Services. Inc. SC 99006
` FL NELAP E87627
n�1ar �

,a Janw25 06 11:15a CITY OF MRRIUN
Udb btu 1zj�z� ► . 0
aceAnalytjcal®
www.pacelabs.com
Lao Sample No: 928020007
Client Sample ID: CC TCLP-3- S1
Pace Analytical Services, Inc, Pace Analytical Services, Inc.
9800 Kincey Avenue. Suite 100 2225 Riverside Drive
Huntersville, NO 28076 Asheville, NC 28804
Phone: 704.87 5,9092 Phone: [phone]
Fax: [phone] fax: [phone]
Lab Project Number: 92138304
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92138304.002 Dalle Cullected: 02/16/07 10:47
Matrix: Soil Date Received: 02/16/07 12:30
Parameters Results Units Report Limit Anal/zec By CAS No. Qual Reg(.nt
Total Percent Solids Method: EPA 160.3
Percent Solids 3.1 X 02/21/07 TNM
Nitrogen, Ammonia Method: EPA 350.1 Modified
Nitrogen, Ammonia 2900 ng/kg 340
Total Kjeldahl Nitrogen, Soil Method: EPA 351.2
Nitrogen, Kjeldahl, Total 59000 ng/kg 3100
Nitrogen, Nitrate plus Nitrite Method: EPA 353.2 Modified
Nitrate as N ND ng/kg 27,
Nitrate -Nitrite (as N) 81. ng/kg 27.
Phosphorus, Total, Soil
Phosphorus
Plant Available Nitrogen
Nitrogen
GC/MS Semivolatiles
Semivolatile Organics, ICLP
1.4-Dichlorobenzene
2,4-Dinftrotoluene
Hexachloro•1,3.butediene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Nitrobenzene
Pentachlorophenol
Pyridine
2 4,5-Trichlorophenol
2.4,6•Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl•d14 (S)
Phencl•d5 (S)
2•Fluorophenol (S)
2,4,6-Tribromophenol (5)
Date: 02128/0'
Asheville Certification as
.NC Wastewater
40
NC Drinking Water
37712
Sc
99030
FL NELAP
E87648
Method: EPA 365.2
13100 mg/kg 160.
02/21/07 15:28 JMW 7727.37.9
02/28/07 20:05 JMW
02/27/07 14:28 EWS
02/27/07 14:a EWS 7127.37.9
02/28/07 13:19 WWB 7723.14.0
Method:
18000 mg/kg 1.0 02/28/07 SHB 7727.37.9
Prep/Method:
EPA 3510 / EPA 8270
NO
ng/l
0.75
ND
ng/l
0.013
NO
ng/l
0.050
NO
ng/l
0.D13
NO
ng/l
0.30
NO
ng/l
0.050
NO
ng/l
0.010
NO
ng/l
0.20
NO
ng/1
0.050
NO
mg/l
0.50
NO
ng/l
0.25
NO
11g/l
0.20
69
X
62
X
76
X
29
X
43
X
58
X
02/27/07 09:21 BET 106.46.7
02/27/07 09:21 BET 121.14.2
02/27/07 09:21 BET 87.68.3
02/27/07 09:21 BET 118.74.1
02/27/07 09:21 BET 67.72.1
02/27/07 09:21 BET 95.48.7
02/27/07 09:21 BET
02/27/07 09:21 BET 98.95-3
02/27/07 09:21 BET 87.66.5
02/27/07 09:21 BET 110.86.1
02/27/07 09:21 BET 95.95.4
02/27/07 09:21 BEf 88-06.2
02/27/07 09:21 BET 4165-60.0
02/27/07 09:21 SET 321.60.8
02/27/07 09:21 SET 1716.51.0
02/27/07 09:21 BET 4165.62.2
02/27/07 09:21 BET 367.12.4
02/27/07 09:21 BET 118.79.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
'nP6ar �.
Page: 3 of 5
lotte Certification
NC Wastewater
12
NC Drinking Water
37706
SC
99DO6
F!_ NELAP
E87627

N {. Jafn«25 08 1 1 : 15a CITY OF MAR I ON
AcieAnalyfical
www.paceiabs.com
626 659 1959 p.4
Pace Analytical Services, Inc. Pace Analytical Services, Inc,
9600 Kincrtry Avenue, Suite 100 2225 Riverside Orlve
Huntersv,,1e, .NC 28078 Asheville, .NC 78804
Phone: [phone] Phone., 828.254.7176
Fax, 704.675.9091 fax: [phone]
Lab Project Number: 92138304
Client Project ID: CORPENING CREEK SLUDGE
LaD Sample No; 928020U07 _ !^ ✓roject Sample Number. 9C1a8304.00? Date Collected: 02/16/07 10:47
Client Sample ID: CC TCLP-3- S1 Matrix; Soil Date Received: 02/16/07 12:30
Parameters Results Units Report Limit Analyzeo _ by CAS No. q0L F.egLmt
Date Extracted 02/25/07 02/25/07
GC Serrivolatiles
Pesticides. TCLP Leachate
gamma-BHC (Lindane)
Chlordane
Endrin
deptachlor
4ethoxychlor
Toxaphene
Tetrachloro.m.xylene (S)
Decachlorobiphenyl (3)
Date Extracted
GUMS Vol ati l es
Volatile O,ganics, TCLP Leach
Benzene
2 Butanone (MEK)
Carbon tetrachloride
Chlorob=nzene
Chloroform
1.4.Oichlorobenzene
1.2-Dichloroethane
1.1.Oichloroethene
Tetrachloroethene
Trichloroethene
Vinyl chloripe
Toluene-d3 1S!
4-Bromofluorobenzene (S)
Dibromofluoromethane (S)
!.2-Dichloroethane-04 (S)
Date: 02/28/07
hev li ii0!i r I s
NC Wastewater
40
NC Drinking Water
37712
SC
99030
FL NELAP
E87648
Prep/Method: EPA 3535 1 EPA 8081
ND
rig/l
0.040
02/27/07
01:35 RCSI
58.39.9
ND
mg/1
0.0030
02/27/07
01:35 RCS1
57.74.9
NO
n9/1
0.0023
02/27/07
01:35 RCSI
72.20.8
NO
rig/l
0.0D080
02/27/07
01:35 RCSI
76.44.8
NO
rig/l
1.0
02/27/07
01:35 RCSI
72-Q- 5
NO
ng/1
0.050
02/27/07
01:35 RCSI
8001.35.2
52
4
02/27/07
01:35 RCSI
877.09.8
46
%
02/27/07
01:35 RCS1
2051.24.3
02/26/07
02/26/07
Method: FPA
8260
ND
mg/l
0.12
02/27/07
21:46 OLK
71.43.2
ND
mg/l
2.5
02/27/07
21:46 OLK
78-93.3
NO
mg/l
0.12
02/27/07
21:46 DLK
56.23 5
ND
mg/l
0.12
02/27/07
21:46 DLK
108 90.7
NO
mg/l
0.12
D2/27/07
21:46 DLK
67.66.3
NO
mg/l
0,12 .,
02/27/07
21:46 DLK
106.46-7
ND
mg/l
0.12
02/27/07
21:46 DLK
107.06.2
ND
mg/l
0.12
02/27/07
21:46 OLK
75.35.4
ND
mg/l
0.12
02/27/07
21:46 IDLY,
127 18 4
ND
ng/l
0.12
02/27/07
21:46 OLK
79.01.6
ND
ng/l
0.12
02/27/07
21.:46 DLK
75.01.4
lei
X
02/27/07
21:46 IDLY,
2037.26 5
97
t
02/27/07
21:46 OLK
460 00.4
101
k
02/27/07
21:46 DLit
1868.53.7
95
4
02/27/07
21.46 OLK
17060-07.0
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in ful .
withrul the Written consent o` Pace Analvtical Services, Inc.
,y •:,'0,0
nAlnrr•.
page: d of 5
Criarl9ltgC�rtifj�ti n I g
NC 4Nasiawater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87C2.7

.'Jan,25 08 11:15a CITY OF MARION 828 659 1959
e
P.5
Analytical Environmental Services, Inc, Date: 26-Feb_01
CLIENT':
Pace Analytical Services, Inc.
Client Semple ID; 928020023
Lab Order:
0702960
Tag .Number;
Project:
92 i3S304
Cvllection Date: �1;6/2007 10.52 OG AM
Lab Ill:
0702560.001A
Rlatrix: AQUEOUS
Analyses
Result
Limit Qual Units Batch11) DF Date Analyzed
HERBICIDES; rCLP
SW131110151A (SW3510B) Analyst: El
2.4.5-TP (Silyex)
BRL
0.50 mg1L 82997 1 M112007 4-25:00 PM
2.4-D
BRL
0.50 rrc,1/L 82997 212112007 4:25:00 Pfvl
Surr: DCAA
98.2
25.2.164 %REC 82997 1 2/21/2007 4:25:OC PM
Qu.lillers; Valuc exceedc Maximum Cantamir.ant Looel B Analytc dncctct i , Ito hledtod Blank
r^ BRL Below R:poning Limit E Valuc above yuantitation range
H Holding :irrx's Per preparation or analysis excouded 1 Analyst detecmd belm, quanii:ution limits
V Analytc not NELAC certified ? NELAC a ialyua ccrtifc•uton wrding pp
Rpt Linut Reporting Limit S Sptkv Recovery JUl51de acc:p:cc rcxov,ty`IYfitS Of 1

*!Jan.25 08 11:16a CITY OF MARION 828 668 1855 P.b
PRECISION" PETROLEUM LABS, INC.
5915 Star Lane Houston, TX, 77057
Ph.713-6S0-9425 Fax:[phone]
CERTIFICATE OF ANALYSIS
COMPANY: PACE ANALYTICAL
INVOICE No.: 33069
LAB REFERENCE No.: 2007-02-442
PRODUCT D: 92SU20056 PROJECT 492138304 2-16-2007
DATE RECEIVED: 02-21-2007
AUTHORIZED BY: TOM WILLIAMS
TEST
M_ ETHOD
REPORTING
lgnirability (Flash Point), PMCC
EPA-1010
-110��
> 230ULTS
Reactive Cyanides, RFm
S.W. 9010
0.01
BRL
Reactive Sulfides, PNM
S.W. 9030
1.0
BRL
__BRL = BELOW REPORMC LBUT
PRECISION P£TROLEV741 LABS, LNc.,s RESI'ONBIBILITX FOR TIM ABOVE AIiALY5I5,
DEMONS OR INURPREZAnONS IS IaUED TO THE LNVOICE AMOUNT

,►'Jan .25 08 11:16a
CITY OF MRR I OfN
828 659 1855
P•V
Analytical Results
Pace Analytical-Ashevilie For: 92139247
2225 Riverside Drive
Asheville NC 28804
Entered 3/2/2007
Reported; 3/6/2007
Sample Remarc
Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst
07032-5.1
% Solids
928073576
1.21
%
SM2540B
3/2/07
CL
07032-5.1
Fecal Coliform MTF
928073576
132,231
MPN/g
SM92210E
3l2/07
CL
07032-5.2
% Solids
928073594
1.02
%
SM25403
3/2107
CL
07032-5.2
Fecal Coliform MTF
928073584
29,412
MPN/g
SM9221 CE
3/2107
CL
"1032-5.3
% Solids
928073592
1.01
%
SM2540B
312/07
CL
J32-5.3
Fecal Coliform MTF
928073592
89,109
MPN/g
SM92210E
312/07
CL
07032-5.4
% Solids
928073600
1.19
%
SM2540B
312/07
CL
07032-5.4
Fecal Coliform MTF
928073600
42,017
MPN/g
SM92210E
3007
CL
Respectfully submitted,
Dena Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 • Statesville, North Carolina 28687 9704/872/4607

AU an ,db UH 11; 1-7a Lily Ur 1'HKLUI`I
?28 252 4619 PACE ANALYTICAL AS
re0 lb [UU/ 17;%3bHM ytateSville Rnalt1tical
Analytical Results
Pike Analytical-Aeh®vtlle For, 92137999
2225 Riverside give
Aahevihe NC 28804
Entered 2J14/2W7
Rwrtw: 2/10/2007
6tw4ft Rwm*
U C U U. zl 1;j D J
04 37 43 p.m 07.23-71107 4 14
7U4-878-2787 P.3
StMPIS 10
Paramsfer
Cost ID
Result
units
tiigitilod
Date An.ysW
Mellrrt
070214-3.1
% Goad.
92SM258
3.06
%
SWUM2F14/07
MD
07M14-3.1
Few-C #1wm-mTf;
92SM25l
4,248,38
MPwp
SM92210E
W14107
JAp
070214-3.2
% Wide
921004266
2 15
%
SM254GB
2/14JD7
LID
070214-3.2
FecalCoMormNTF
.92W"266
2,372,881
MPN/A
8MMICE
V14/07
MD
070214-3.3
% Bowe
928004274
2.9
%
SM2MM
2114M7
UD
0702143.3
F@cW Camofm NTF
92S004274.
1,034,483
MPWV
SM92210E
ZMW07
MD
070214-3.4
% SoWs
92SN4282
2.82
%
SW5408
2/1407
MO
079214-3.4
FUI CD61orm M F
92&0G M
1,773,050
MPN/Q
SM92210E
2l14/07
MCI
Rea ly Bubmifted,
Dw a Myers
NO Cert #r440,
NCDW Ce►t #37755.
EPA NCODWS
P.O. &rx 228 9 StateevWe, North CaL'QURa 28687.7M72/4697
r•Q

„ *J�n.25 06 11:16a CITY OF MHRION 82H 65U 1y5U p.lu
VS in 0.89
VS out 0.7 14
VSFR= 0.71161
o. gg - alb 0 I q
-7 0
0�267
Da 51

CITY OF MARION
CORPENING CREEK WASTE TREATMENT PT.ANT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
Standard Methods 20TH Edition —Method 2540 E
RUN DATE: 3 -/ 3 _p 7 TIME 114: /O!'O TEMP IN: /03 'C
ANALYST: d' TIME WEIGHED' /yz / 1IME OUT: i 1EMPOUTA3"C
ANALYST: TIME IN. TEMP INNS 2_'C
TIME WEIGHED: `� TIME OUT: jj3D TEMP OUT�3C
VSS FIXED
A_R A-C
SAMPLE
DATE
COLLECT
Sample
Vol.
ML
Filter. FILTER+
# Residue before ,
Ignition, Gr.
FILTi=R
WEIGHT
GRAMS)
id
Residue
Wt., Gr.
FILTER +ASH
After Ignition
(GRAMS)
ASH +
FILTER
(GRAMS)
ASH
GRAMS
TOTAL
Fixed Solids
MG/L
TOTAL
VSS
MG/L
% VSS
`
- 3-07
5
!L'
y
0. Y 70
(Py p
f�
ems"
D
S/7/7
0.88
D d
0•a4
/05
So
lop
0. 01 S?
SZ,
r , o o Z
0, 0t2&
1
�
D
�.a —3
Sz. 06 el
of
SZ , D .
0. 0oy
Z�
� S7o
�i f�o
j
DILUTION 1000000
FACTOR = ML OF SAMi-LE
Mg Volatile Solids / L = A - B) X 1000000
Sample Vol„ VL.
Mg Fixed Solids / I_ _ ( B - C) X OOOOCK)
Sample Vol., ML
% Volatile Solids = Total VSS
Tot. Vss + Tot. Fixed
BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CALIBRATION BOOK
LOT IFS
GLASS FIBER FILTER: 51634
3S37iF

CITY OF MARION
I
CORPENING CREEK WASTE. TREATMENT PLAINT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
Standard Methods 20TH Edition --Method 25Q E
RUN DATE:
TIME IN:
TEMP IN:
'C
ANALYST_ TIME WEIGHED:
TIME OUT:
TEMP OUT:
'C
ANALYST:
TIME IN:
TEMP IN:
'C
TIME WEIGHED:
TIME OUT:
TEMP OUT:
'C
A
(_
A -C R
VSS FIXED
A_R B-C
Em
�.
WEIGHT
•
W1, G
After Ignition
DI
•
•
VSS
-
it".
9�1
DR-UTION
1000000
FACTOR =
ML OF SAMPLE
Mg Volatile Solids I L = ( A - B) X 1000000
Sample Vol_, ML.
Mg Fixed Solids / L =
( B - C) X 1.000000
Sample Vol_, ML.
% Volatile Solids =
Total VSS
Tot. Vss + Tot. Fixed
BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CALIBRATION BOOK
'Pp (O
VO4,

CITY OF MARION
CORPENING CREEK WASTE TREATMENT PLANT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
Standard Methods 20TH Edition —Method 2540 E
RUN DATE: TIME IN: TEMP IN: C
ANALYST: TIME WEIGHED: TIME OUT: TEMP OUT: `C
ANALYST: TIME IN: -TEMP IN: `C
TIME WEIGHED: TIME OUT. TEMP OUT: `C
o C A-C B
vSS FIXED
A-B B-C
•After
•
•
.
•
Ignition
•
OTAL
Rv 1 a
rho
/ i
1 N lli/r.
r u r
ZZIM
DILUTION 1000000
FACTOR = ML OF SAMPLE
Mg Volatile Solids / L = (A - B) X 1000000
Sample Vol., ML.
Mg Foxed Solids / L = f B - C) X 1000000
Sample Vol., ML.
% Volatile Solids = Total VSS
Tot Vss + Tot. Foxed
BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CALIBRATION BOOK
vo-f

1
CITY OF MARION
CORPENING CREEK M'!1STE TREATMENT PLANT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
Standard Methods 20TH Edition —Method 2540 E
a
RUN DATE: 3 -/3 -01 TIME IN: /pS�O TEMP IN: 1-03 `C
ANALYST: TIME WEIGHED: / q- r• TIME OUT: /32-0 TEMP OUTp3•C
ANALYST: TIME IN: TEMP IN:5S z'C
TIME WEIGHED:j TIME OUT: /S3a TEMP OUTS-g3C
VSS FIXED
n n R -f
_ •
• •
• -
Wt-, Gr.
FILTER +ASH
After Ignition
(GRAMS)
—ASH4
FILTER
(GRAMS)
TOTAL
Fixed • •
MGfI_
TOTAL
Dii_UTION
1000000
FACTOR
ML OF SAMPLE
Mg Volatile Solids / L= t o- B i X 1000000
Sarnple Vol., t,".L
I
Mg Fixed Solids / L _
(B - Q X 1000003
Sarnple Vol., ML.
% Volatile Solids = Total VSS
Tot Vss + Tot_ Fixed
BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CALIBRATION BOOK
LOT #'S
GLASS FIBER FILTER: 51634
;5371�

NCDA&CS Agronomic Division Phone: [phone] Web Site: www.ncagr.com/agronomi/
Report No: 22161
Grower:
Southern Soil Builders, Inc.
Copies To:
958 Hoots Rd
Roaring
River, NC 28669
rsn .c
oil Test Report
Farm:
02/12/2008
SERVING N.C. RESIDENTS FOR OVER 60 YEARS
McDowell County
Agronomist Comments
C -- 12, $
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
F3 ✓
1st Crop: Fes/OG/Pim,M
0
120-200
0
90-110
0
15-20
0
0
.0 pH$
12
2nd Crop:
15-20
Test Results
Soil Class HM%
W/V CEC BS% Ac pH P-I K-I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-1
Zn-AI
Cu-1
S-I
SS -I NO3-N
NH4-N
Na
MIN 0.51
1.02 8.4 93.0 0.6 6.9 118 22
61.o
30.0
127
80
97
97
159
25
0.1
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
F4 ✓
1st Crop: Fes/OG/fim,M
0
120-200
30-50
60-80
0
0
0
0
.0 pH$
12
2nd Crop:
0
Test Results
Soil Class HM%
W/V CEC BS106 Ac pH P-I K-I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-1
Zn-AI
Cu-1
S-I
SS-1 NO3-N
NHa-N
Na
MIN 0.46
0.89 9.1 96.0 0.4 6.8 41 35
61.0
32.0
157
99
137
137
277
28
0.1
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
K1C ✓
1st Crop: Fes/OG/Pim,M
LIT
120-200
0
0
0
0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM%
W/V CEC BS% Ac pH 1 P-I K-I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-I
Zn-AI
Cu-I
S-I
SS -I NO3-N
NH4-N
Na
MIN 0.92
1.04 10.5 80.0 2.1 5.3 J 201 135
62.0
12.0
256
171
360
360
187
76
0.1 -
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg
S
Cu
Zn
B Mn
See Note
K2A ✓
1st Crop: Fes/OG/Pim,M
0
120-200
0
0
0
0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM%
W/V CEC BS% Ac p H P-I K 1
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-I
Zn-AI
Cu-1
S-I
SS-1 NO3-N
NH4-N
Na
MIN 0.81
1.00 11.0 90.0 1.1 6.2 128 110
73.0
12.0
221
147
303 .
303
213
48
0.1
,o

NCDAKS Agronomic Division
Phone: [phone] - Web Site: www.ncagr.com/agronomi/
Grower: Southern Soil Builders,
Report No: 22161
Pg 2
Field information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg S
Cu
Zn
B Mn
See Note
K211
1st Crop: Fes/OG/fim,M
0
120-200
0
20-40
0 0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM% W/V
CEC BS%
Ac pH P-1
K-1
Ca%
Mg%
Mn-I
Mn-A!(1)
Mn-AI(2)
Zn-1 Zn-AI
CO-1
S-I
SS-1 NO3-N
NH4-N
Na
MIN 0.60 0.96
12.9 91.0
1.1 6.4 194
59
75.0
15.0
124
85
424 424
331
43
0.1
Field Information
Applied Lime
Recommendations
Sample No., Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg S
Cu
Zn
B Mn
See Note
K2C
1st Crop: Fes/OG/fim,M
.6T
120-200
0
10-30
0 0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM% W/V
CEC BS%
Ac pH RI
K-I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-1 Zn-A1
Cu-1
S-1
SS-1 NO3-N
NH4-N
Na
MIN 0.86 1.07
11.1 84.0
1.8 5.7 253
68
70.0
11.0
115
86
453 453
242
46
0.2
Field Information
Applied Lime
Recomme dations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg S
Cu
Zn
B Mn
See Note
K2E
1st Crop: Fes/OG/rim,M
0
120-200
0
0-20
0 0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM% W/V
CEC BS916
Ac pH P-1
K I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-1 Zn-AI
Cu-1
S-I
SS -I NO3-N
NH4-N
Na
MIN 0.97 0.99
12.1 92.0
1.0 6.4 203
82
76.0
13.0
241
156
354 354.
189
58
0.1
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
N
P205
K20
Mg S
Cu
Zn
B Mn
See Note
K2F
1st Crop: Fes/OG/rim,M
0
120-200
0
20-40
0 0
0
0
.0 0
12
2nd Crop:
0
Test Results
Soil Class HM% W/V
CEC BS%
Ac pH RI
K-I
Ca%
Mg%
Mn-I
Mn-AI(1)
Mn-AI(2)
Zn-1 Zn-Al
Cu-1
S-I
- SS I NO3-N
NH4-N
Na
MIN 0.81 1.00
12.7 91.0
1.2 6.4 240
61
77.0
12.0
170
113
382 382.
216
41
0.1
ti

OF WATFn
0\ 7nG Michael F. Easley, Governor
William G. Ross Jr., Secretary
North Carolina Department of Environment and Natural Resources
Y Alan W. Klimek, P.E. Director
Division of Water Quality
Aquifer Protection Section
July 21, 2008
Mr. J. Robert Boyette
City Manager
City of Marion
Post Office Drawer 700
Marion, North Carolina 28752
Subject: 2007 Annual Report Review
Additional Information Request
City of Marion
Land Application of Residual Solids (503)
Permit No. WQ0019960
McDowell County
Dear Mr. Boyette:
The Asheville regional office has completed a review of your 2007 Annual Report. Your permit requires a Sodium
Absorption Ratio (SAR) calculation. The SAR calculation was not included in the 2007 Annual Report. Please submit the
requested information in triplicate within 10 days of receipt of this letter to the attention of Ed Hardee at:
NCDENR
Division of Water -Quality
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh NC 27699-1636
If you should have any questions regarding this matter, please do not hesitate to contact me at [phone].
Sincerely, ;
Beverly Price
Environmental Specialist
Cc: Larry Carver, WWTP ORC
Dennis Key, Land Application ORC Southern Soil Builders 958 Hoots Road Roaring River, NC 28669
Noe Carolina
North Carolina Division of Water Quality — Asheville Regional Office 2090 US. Highway 70 Swannanoa, NC 28778 Phone [phone]
Aquifer Protection Section FAX [phone]
Customer Service 1-877-623-6748
Internet: h2o.enr.state.nc.us
An Equal Opportunity/Affirmative Action Employer— 50% Recycletl110% Post Consumer Paper

S Southern
S Soil
g Builders, Inc.
Tuesday, July 29, 2008
Ed Hardee
NCDENR
Division of Water Quality
Aquifer Protection Section
Land Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
958 Hoots Road Roaring River, NC 28669
[phone] 9 Fax [phone]
RECEIVED I DENR I DWQ
AQUIFF1ZpR0JF0T*N SECTION
0611�2008
Subject: 2007 Annual Report Review,
-, Additional lnformation Request
E V E 0
Achp,viva Regional Office
The Asheville Regional Office has requested a Sodium Absorption Rate (SAR)
calculation for the City of Marion, Permit No. WQ0019960. Below you will find the
SAR calculation.
SAR=NA meq / [0.5 (CA meq + Mg meq)] 1/2
Meq = wet weight / (atomic wt. / valence)
Percent Solids = 3.37
Sodium = 1,700 �9IK9 = $9 ;Z9 P9 lL
Calcium = 14,300 o j I9`9 = tiQ1'RO'"g 1L
Magnesium = 3,900 —51 1,9 � rit• 43'^)/L
SAR= 2.49: / [0:5 (24.09 +, 10.95)]
Sodium Absorption Ratio (SAR) = 0.
. I i I, 1 0• q SD ;,� q

If you should require any additional information of have any questions or concerns, feel
free to contact me at anytime.
Thank you,
;ach Key
Southern Soil Builders, Inc.
Cc: Mr. J. Robert Boyette, City of Marion
Larry Carver, City of Marion WWTP

Annual Report Review SOP Class B Land Application
1. Annual Land Application Certification Form
• Was a certification form submitted? �4-5
• Was land application conducted during the reported year? Y eS
• How many dry tons and dry tons per acre were applied? 188.1 1VIV D T
• Were the applications within the permitted amount?2s'
• Verify PAN if more than 10 tons/acre .
• Did it indicate compliance?y e.5
• Was it signed by the appropriate people? q-e-5
3.3 9 o. 66W Z /6, ✓.6'X
2. Monitoring
• Were the analyses conducted at the required frequency? Y"_5
• Were the metals analyses reported on the Residual Sampling Summary Form? ye-5
• Were the results reported in mg/kg? ye-5
• Were the metals within ceiling concentration permit limits?yes
• If no, were the lab analyses attached?
• Were all the required parameters tested? N o . 5 F1 R " ' "' k•
• Was TCLP analysis conducted? +��5 9 Corr-5 /-b;,�
• Were the TCLP contaminants within regulatory limits? Yes
3. Field Summary
• Were the land application events recorded on the Field Summary Forms?V�
• Was a Field Summary Form submitted for each field applied on? y es-
• Were all the residuals applied to permitted land?yam
• Were all the residuals applied from permitted sources? J eS
• Were the field loading rates for each metal and PAN calculated (year to date)? Yes
• Were the cumulative p6llutant loading rates calculated? YZy
• Were the calculations correct?Nr,S
r • Were the. PAN loading rates within permit limits? +&F
• Were the heavy metal cumulative pollutant loading rates within permit limits?�,es
• Were the residuals applied on a suitable crop? Y'd
• Were the applications conducted during the crop's growing season?
0 Were the Field Summary Forms complete? O, e5
• Was lime application on Field Summary Form? JyNA,-io De lucA K-I {C�
4. Pathogen and Vector Attraction Reduction
• Was a signed copy of. the Pathen and Vector Attractions eduction Form submitted?ye.S
• Did the form indicatethe period of coverage, the residual class, and the pathogen reducl on alternative and the
vector attraction reduction option used? ,/ >� S e e rp.+.a-' e)e_V_4 Paj -O_
• Was theappropriate documentation to show pathogen and vector attraction reduction included in the report?
• Was pathogenand vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T?
(VAR p .,. )
5. Soil Tests
• Was a Standard Soil Fertility Analysis conducted for each field applied on? 1'e,5
• Were the soil pH's 6.0 or greater for each application field? No K1C �S •3 v_%C 5.'
• Were the copper and zinc indexes in the soil less than 3000 for each application field (state soils lab)? y.P—s
6. General
• Was the report in the proper format? yes
• Were any parts of the annual report missing? N o
• Was the report submitted on time? cg

Class B PathoLien Review
Alternative 1 - Fecal Coliform Density
• Was the sampling conducted at the required frequency? -0- 5
• Were seven samples taken? y 1 ed o� Pli�, lllvq 2
• Was the geometric mean calculated and done correctly? Wo - Nod i �d��
• Did the results show compliance (less than either 2,000,900 MPN/gram of total solids or 2,000,000
Colony Forming Units/gram of total solids) yzS C-44- close.. 1x�, 8P
o
Alternative 2 - Use of Process to Sianiflcantly Reduce Pathogens (one of five
• Was the sampling conducted at the required frequency?
Aerobic Digestion
• Was it an aerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was the time and temperature between 40 days at 20°C (68°F) and 60 days at 15°C (59°F)?
Air Dryin
• Were residuals on sand beds or pave or unpaved basins for three months?
• Was theambient.temperature above 0°C (32°F) for two months?
• Were the residuals partially digested?
• Were residuals exposed to atmosphere during two months above 0°C (not snow covered)?
Anaerobic Digestion
• Was it an anaerobic process (Inspection)?
• Were logs submitted showing time and temperature?
• Were temperatures within range for complete time period?
• Was the time and temperature,between 15 days at 35°C (95°F) to 55°C (131°F) and 60 days at 20°C
r (68°F)?
Composting
• Was it a composting procedure (not natural decay under uncontrolled conditions)?
• Were logs submitted showing time and temperature?
• Was the temperature raised to 40°C (104°F) or higher and remained at 40°C (104°F) for five days?
• Did the temperature exceed 55°C (131OF) for four hours during the five-day period?
Lime Stabilization
• Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing
kiln dust or fly ash)?
• Were logs submitted showing time and temperature?
• Was the pH raised to 12 after two hours of contact?
• Were logs submitted showing time and pH?
• Was the temperature corrected to 25°C (770F)?

Vector Attraction Reduction Review
• Was the sampling conducted at the required frequency?
°/ 38% Volatile Solids Reduction'
• Was there 3 8 % reduction? � -05
• . Were lab sheets/calculations in report? `'I,e.<
® Was the reduction on volatile solids (not -total solids)? y.e,57
• Was the samples taken at beginning of digestion process and before application (69 �
(Inspection)? N o scar- p i UJ -er� co t to ���7 Ce -la t 47
• Were calculations correct?, (N o+ or-
27
40-Day Bench Scale Test n' 36r
• Were residuals from anaerobically digested treatment (Inspection)?
• Were residuals anaerobically digested in lab?
• Was the test run for 40 days?
• Was the test done between 300C (86°F) and 37°C (99°F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 17%?
• Were lab sheets/calculations in report?
• Were calculations correct?
30-Day Bench Scale Test
• Were residuals from aerobically digested treatment (Inspection)?
• Were residuals aerobically digested in lab?
• Were residuals 2% or less total solids?
• ` Was the test run for 30 days?
• Was the test done at 20°C (68°F)?
• Was the reduction on volatile solids (not total solids)?
• Was the reduction less than 15%?.
• Were lab sheets/calculations. in report?
• Were calculations correct?
Specific Oxygen Uptake Rate (SOUR)
• Were residuals from aerobically digested treatment (Inspection)?
• Were residuals 2% or less total solids (dry weight basis) (not diluted)?
• Was the test done between 10,1C (50°F) and 30°C (86°F)?
• Was the temperature corrected to 20°C (68°F)?
• Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual
solids (dry weight basis)?
• Was the sample holding time under two hours?
• Was the test started withinl5 minutes of sampling or aeration maintained?

14-DayAerobic Process
e Were residuals from aerobically digested treatment (Inspection)?
• Were the residuals treated for 14 days?
• Was the residuals temperature higher than 40°C (104T) for the 14-day period?
• Was the average residuals temperature higher than 45°C (11.3T)?
Alkaline Stabilization
• Was the pH of the residuals raised to 12 or higher by the addition of alkali?
• Did the pH of residuals remain at 12 or higher for two hours without the addition
of more alkali?
• Did the pH of residuals remain at 11.5 or higher for an additional twenty-two
hours without the addition of more alkali?
• Was the pH. corrected to 250C (770F)?
Drying of Stabilized Residuals
• Does the residuals contain any unstabilized residuals?
• Were the residuals mixed with any other materials?
• Were the residuals dried to 75% total solids?
Drying of Unstabilized Residuals
Were the residuals mixed -with any other materials?
• Were the residuals dried to 90% total solids?.
Inj ection
• Was there any significant. amount of residuals on land surface one hour after
injection (Inspection)?
• Was injection done on pasture or hay field?
• Was injection done at time that crop was growing?
• If Class A with respect to pathogen, were residuals injected within eight hours
after discharge from pathogen treatment?
Incorporation
• Were the residuals incorporated into the soil within six hours after application?
• Was incorporation done on pasture or hay field?
• Was incorporation done at time that crop was growing?
• If Class A with respect to pathogen, were residuals incorporated within eight
------------ hoursafter--disehar-ge--frorr�pathogen-tr-eatment?____-------_--------------------