WQ0019960_Annual Report_20070215

CITY OF MARION, NC
2006 ANNUAL REPORT
LAND APPLICATION PROGRAM
NC PERMIT NO. WQOO 19960
r1-_ C F � v E 0
FEB 19 2007
!I Ashevilis Regional Office
Aquifer Protection
RECEIVED
FEB 15 2007
WATER QUALI I Y zz-,c— CION
Information Processing Unit

kPW,-#1.it#: WQ0019960 County:..
Facility Name (as shown on permit):
McDowell Year: 2006
Citv of Marion
Land Application Operator:
Southern Soil Builders, Inc. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calendar year?
2f Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
8
Total number of fields land application occurred during the year:
4
Total amount of dry tons applied during the year for all application sites:
105.6
Total number of acres land application occurred during the year:
46
Part B:
Facility was compliant during calendar year 2006 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. - No
If no please, provide a written description why the facility was not compliant, the dates, Anexplain, IVED
corrective action taken. FE13 15 2007
1 Only residuals approved for this permit were applied to the permitted sites. WATER u ri•Y sECT►ON
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a'401 ` atrgbessing unit
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4 Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5 All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities)
7 All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10 Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of -residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true.
,accurate, and complete. I am aware that there are significant penalties for submitting false information,
'including the possibility of fines and imprisonment for knowing violations."
(Yi4t1)aSee- - 21l v"'1
Permittee Name and'title (type or print) ture of Perrntitte Date
ature of Preparer* Date Sig ature of Land Applier Date
DENR FORM ACF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0019960 Laboratory: 1) ' A&L Eastern Laboratories, Inc.
Facility Name: City of Marion
NPDES # or NCO031879
WQ#:
WWTP Name: City of Marion WWTP
2)
3)
4)
5) -
Sample or
Composite Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
ign t re of Preparer Date
DENR FORM RSSF (5/2003)

. Attach this form to the corresponding: Field Loading Summary Form to be submitted in Annual Report
cility Name:
rmit 4:
aerator:
:res Used:
City of Marion Total Dry Tons Applied (Annual): 41.504
WQ0019960 Cation Exchange Capacity (non 503 only):
Wayne Ross Owner: Wayne Ross
16 Acres Permitted: 16 Site #: R1 Field #: R1
1
1:
1 1 ' 1 1
1 _ •
' 1
1
' �'
e .
1 1
i 1 1 1
•alculated
in lbs/acre):
. 171
1 .
I 1 ,
'I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
.nformation submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
i2 c,. 42- 3- u �
Signature of Land Applier Date DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM y
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: City of Manion Permit th WQ0019960 Annual Dry Tons Applied: 41.503176
owner: Wayne Ross Operator: Wayne Ross Cation Exchange Capacity (non 503):
1;tP li• R1 Field #: RI Acres Utilized: 16 Acres Permitted: 16
S i
Totals
Per
Acre
%
Solids
D Tons Per
Dry
Acre
Residual
(Summarize)
t e
Cond.
- We
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Vola-
till-
nation
Rate**
Miner-
ali=
nation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
0 r.
14
a
-
Cu.Yd.
Report
Totals
in Gal.
=0p,
rop 2
6-206
286,000
17875
3.48
2.5939485
WWTP
dry
0
s
0.5
30%
48300
3700
1
79.0169
##4####
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
y
0
0
4
0
0
0
0
5
0
0
0
0
s
r #
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
As
0.0098572
Cd Cr
0.01038 0.22308
Cu
2.56806
Pb
0.3009
Hg
0.02023
Mo
0.12451
c4
�.
.'
Ni
0.16083
Se
0.0192
Zn
5.86244
P
143.189
0
0
0
PAN 1
79.0169
0
0
0
PAN 2
0
Lime Applied
Date lbs/ac
10
11
12
:>>?
0
0
0
COTALS: 17875
ktutuallbs/acre
--urrent Cumulative lbs/ac
0.0346572 0.02929 0.22308 5.6879 0.85263 0.03871 1.14636 0.33764 0.0718 12.3215
0.0248 0.01891 0 3.11984 0.55173 0.01848 1.02185 0.17681 0.0526 6.45904
36 34 NA 1338 267 15 NA 374 1 89 2498
I 250
'nor Years Cumulative lbs/ac
'ermitted C. P. L. R.***
:r D AM T imit 1 et/Ind C'rnn
`I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
iesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
/ Signature of rid Applier Date "Volatilization Rate:.Surface - 0.5, IniectionAncorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
k*** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form_ The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row 0 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

t;'A7ach this form to the corresponding.Field Loading Summary Form to be submitted in Annual Report
ility Name
mit 9:
erator:
-es Used:
City of Marion Total Dry Tons Applied (Annual): 27.348
WQ0019960 Cation Exchange Capacity (non 503 only):
Wayne Ross Owner: Wayne Ross
12 Acres Permitted: 12 Site #: R2 Field #: R2
1.
•CIMIT-1 61
fill 01,11 Ral 11RUTIV�.
•
.11
.�
: 43MIKI"I
•
•.
1
1
1
1
1
1
1
1
1
1
1
I certify, under penalty of law, that this document was prepared under,my direction or supervision in
.ccordance with a system designed to assure that qualified personnel properly gathered and evaluated the
nformation submitted. I am aware that there are significant penalties for submitting false information,
ncluding the possibility of fines and imprisonment for knowing violations"
1/
iign'ature of Land ApVier Date DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
w -
PLEASE MAKE A COF
'OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
�}
PLACE
A "N/A"
IN A BLANK
OR BOX WHEN NOT APPLICABLE.
City of Marion
Permit #: WQ0019960
Annual Dry Tons Applied:
27.354366
Facility Name:
Operator:
Wayne Ross
Cation Exchange Capacity (non 503):
Owner: Wayne Ross
Field #:
R2
Acres Utilized: 12
Acres Permitted:
12
Site #• R2
S
Site
Inches Appli- Vola- Miner-
Ammo-
Ni-trate
Must Select
Gal. Totals
%
D Tons Per
Dry
Residual
Cond.
Precip. cation tili- ali-
nia- and PAN 1
TKI�1
Crop 1 or Crop
PAN 2 2
Per
Solids
Acre(Summarize)
Sources
Dry,
Wet,
Past 24 Meth- zation zation
Ni-
Nitrite
ra Acre
E
* **
Hrs. od Rate Rate
trogen
Crop 1 Crop 2
9-2006 188,500 15708 3.48
2.2795305
WW P
Moist
dry
0 s 0.5 30%
48300 3700 1 69.4391
####### Fescue
1
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
0
0
Cd Cr
Cu
Pb H Mo Ni
Se Zn P PAN 1
PAN 2 Lime Applied
TOTALS: 15708 :.
Annuallbs/acre
As
0.0086602
0.00912 0.19599
2.25621
0.26436 0.01778 0.10939 0.1413
0.01686 5.15054 125.801 69.4391
0 Date lbs/ac
Current Cumulative lbs/a .
0.0293841
0.03354 0.19599
5.72237
0.69837 0.32423 0.70069 0.31196
0.05016 12.5973 s
Prior Years Cumulative lbs/ac
0.0207239
0.02442 0
3.46616
0.43401 0.30645 0.5913 0.17066
0.0333 7.44676
-•
Permitted C. P. L. R. ***
36
34 NA
1338
267 15 NA 374
89 2498
250
<' `>:
Pernut PAN Limit 1 st/2nd Crop
my rlirertinn or sunervision in accordance with a system
"I certify, under penalty of taw, Lnat L1115 uuLwa1c11L ""- r--r-_ ___1 -- -
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
1/ Signature of Land Applter Date **Volatilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
acility Name:
ermit #:
Iperator:
,cres Used:
City of Marion Total Dry Tons Applied (Annual):
WQ0019960 Cation Exchange Capacity (non 503 only):
James Fisher
13.7 Acres Permitted:
30.1811
_ Owner: James Fisher
13.7 Site #: F-01 Field #: F-01
NONNI
• .
.ee
knnual heavy Metal Yield Loadings (Calculated in lbs/acre):
e
-
e e e : •
0000000
!
000
e e e : •
. �
e : `
00000000000
� � •
.
�0000000000��
e e
0
�
00000000�
e e
-
e ..
00000000000
a ..
. - -
e e
00000000000
e e .
�
• ' � �
o0v00000000
• • ::
•�•.
e
e
e
e
e
e
e
e
e
e
e
I cernry, under penaity of law, that this document was prepared under my direction or supervision in
accordance with asystem designed to assure that qualified personnel properly gathered and evaluated the
nformation submitted. I am aware that there are significant penalties for submitting false information,
ncluding the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date DENR FORM MFLSF (5/2003)

ANNUAL. LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. r�
PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE. „
Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 30.184128
Owner: James Fisher Operator: James Fisher Cation Exchange Capacity (non 503):
;*P it• F-01 Field #: F-0I Acres Utilized: 13.7 Acres Permitted: 13.7
o
„ o
�
Specify
Totals
Per
Acre
15182
%
Solids
3.48
D Tons Per
Dry
Acre
2.203221022
Residual
Sources
(Summarize)
VWdTP
Site
Cond.
Dry,
Wet
Moist6-2006
dry
Inches
Pr eci p�
Past 24
ems.
0
Appli-
cation
Meth-
od*
s
Vola-
till-
zation
Rate**
0.5
Miner-
all-
.
zation
Rate
30%
TKN
48300
Ammo-
nia-
Ni-Nitrite
trogen
3700
Ni-trate
and
1
PAN 1
67.1145
PAN 2
#######
Must Select
Crop 1 or Crop
2
*
1
208,000
Crop 1
Fescue
Crop 2
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0E
0
0
7
0
0
0
0
8
0
0
0
0
19
0
0
0
110
0
0
0
0
11
0
0
0
As
0.0083714
Cd Cr
0.00881 0.18946
Cu
2.18097
Pb
0.25555
HR
0.01718
Mo
0.10574
Ni
0.13659
Se
0.0163
Zn
4.97878
P
121.606
0
PAN 1
67.1145
0
PAN 2
0
Lime Applied
Date lbs/ac
12
TOTALS: 15182
Annual lbs/acre
0.0083714
0.00881
0.18946
2.18097
0.25555
0.01718
0.10574
0.13659
0.0163
4.97878
Current Cumulative Ibs/ac
Prior Years Cumulative lbs/ac
o
0
0
0
0
0
0
0
0
0
Permitted C. P. L. R.***
36
34
NA
1338
267
15
NA
374
89
2498
Tl...-.,.. 7) ANT T :...;r 1 n*/7nli (�rnr.
_
250
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Z 2-U-7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signature of and Applier Date **Volatilization Rate: Surface - 0.5, Iniection/Incor )oration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the
same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1.
DENR FORM FSF (5/2003)

Wttach this form to the corresponding. Field Loading Summary Form to be submitted in Annual Report
lity Name:
nit #:
rator:
�s Used:
City of Marion Total Dry Tons Applied (Annual):
WQ0019960 Cation Exchange Capacity (non 503 only):
James Fisher
4.3 Acres Permitted:
Owner:
4.3
James Fisher
6.6005
Site #: F-02 Field #: F-02
•
.11
rim �.•
••
;�
1
1
1
1
1
1
1
1
1
1
1
:�
••mow
l certify, under penalty of law, that this document was preparea unaer my airecuuu ur 5UPCI v131wI III
:cordance with a system designed to assure that qualified personnel properly gathered and evaluated the
iformation submitted. I am aware that there are significant penalties for submitting false information,
icluding the possibility of fines and imprisonment for knowing violations"
ti a- '7 -0
-igna re of Land Applier Date DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
'
OF BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLEASE MAKE A COPY
THIS
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
r
City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 6.602778
h'
Facility Name:
Operator: James Fisher Cation Exchange Capacity (non 503):
Iwner: James Fisher
Field #: F-02 Acres Utilized: 4.3 Acres Permitted: 4.3
to #: F-02
ite
Inches
Appli-
Vola-
Miner-
Ammo-
Ni-trate
Must Select
Crop 1 or Crop
S iS i
Gal.
Totals
%
D Tons Per
�'
Residual
Sources
Cond.
Dry,
Precip.
cation
till-
ali-
T�
ma-
and
PAN 1
PAN 2
2
�
0
Cu.Yd.
Report
Per
Solids
Acre
(Summarize)
wet
Past 24
Meth-
zation
zation
Ni-
trogen
Nitrite
Crop 1
Crop 2
Totals
Acre
Hrs.
od*
Rate**
Rate
in oral
Moist
VdWT'P
dry
0
s
0.5
30%
48300
3700
1
46.7753
###4###
Fescue
1
.2006
45,500
10581
3.48
1.535529767
0
0
2
0
0
3
0
0
0
0
.
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
8
0
0
0
0
9
0
0
20
0
0
10
0
0
0
0
11
0
0
0
0
12
0
0
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
<z»
'OTALS:
10581
As
0.005833
0.00614
0.13201
].51965
0.17806
0.01197
0.07368
0.09517
0.01136
3.4691
84.732
46.7753
0
Date
lbs/ac
utrtuallbs/acre
0.005833
0.00614
0.13201
1.51965
0.17806
0.01197
0.07368
0.09517
0.01136
3.4691
'
;urrent Cumulative lbs/ac
'rior Years Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
'ermitted C. P. L. R.***
36
34
NA
1338
267
15
NA
374
89
2498
250
•
'ermit PAN Limit 1 st/2nd Crop
under my direction or supervision in accordance with a system
`I certify, under penalty of law, that this document was prepared
and evaluated the information submitted. I am aware that there are
lesigned to assure that qualified personnel properly gathered
false information, including the possibility of fines and imprisonment for knowing violations."
ignificant penalties for submitting
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Date **Volatilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0
Signature of Lan
Applier ***C.P.L.R.: Cumulative Pollutant Loading Rate
Tons Per Acre are to be enteredenticalon the and are his information needs to be into
1numtFiered Si �
the
FSF row # l to MFLSF column #entered
.*** The RSSF Data and the Dry compleSF
FSFh�wSF to te the metals equations. ons
l
the MFLSF as is entered on the y
same numbered column on
DENR FORM FSF (5/2003)

Fiiic1fl'ty dame: _
WNVTP dame: _
Monitoring Period
City of.Marion
City of Marion WWTP
From 1 /1 /2006
Permit Number:
NPDES Number:
To 12/31 /2003
WQOO 19960
NCO031879
D. tk,,. RaAlir6nn ran CIRR ;03.371 - Please indicate level achieved and alternative performed:
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 40
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed Class A only) indicate "Process to Further Reduce Pathogens":
Compost ❑
Heat Drying ❑
Heat Treatment ❑
Thermophilic ❑
Beta Ray 01
Gamma Ray
Pasteurization ❑
Class B:
Alternative 1 C
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed Class B only) indicate "Process to Significantly Reduce Pathogens":
Limc Stabilization ❑ Air Drying Composting ❑ jAerobic Digestion F�
,Anaerobic Digestion❑
If applicable to alternative performed Class A or Class B complete the following monitoring data:
Parameter
Allowable Level
to Sludge
Pathogen Density
um r o
Excee-
requenc)
of
Sample
Type
Analytical
Tech- nryuc
inimu
Geo. Mean
aximu
Units
Fecal Coliform
2 x 10 to the 6th
power MPN per
gram of total
solids or 2 x 10 to
the 6th power
C FU per am of
59859
171428
310345
MPN/g
0
7
grab
sm922 l e
1000 mpn per
gram of total solid
(dry weight)
Salrnonel!a bacteria
fn iru of fecal
colifurm)
3 MPN per 4
grams total solid
(dry weight)
Vector .Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 11 Option 2 ❑ Option 3 ❑ j0ption 4 ❑ j0ption 5 ❑
Option 6 ❑ Option 7 ❑ 1 Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ ' 1 certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
ysed to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Preparer Name and Title (type or print)
na ure reparer Date
Dennis Key Southern Soil Builders
Land Applier Name and Title (if applicable)(type or print)
­71; ,
Sig ture of Land Ap r (if applicable) Date
DENR FORM RF (5/2003)

Rapt-rt Number
R06165-8005 - A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 • [phone]
46381 Fax No. [phone] • Email: [e-mail]
TO: SOUTHERN SOIL BUILDERS FOR: MARION
958 HOOTS ROAD
ROARING RIVER, NC 28669 NC CERT #257
ATTN: DENNIS KEY
LAB NUMBER: 42689
SAMPLE ID: MARION
REPORT OF ANALYSIS
copy: ZACH KEY
DATE SAMPLED: 6/8/2006 1600
DATE RECEIVED: 6/13/2006 1130
DATE REPORTED: 6/16/2006 PAGE: 1
Solids, Total (As is)
148
34800
100
RD
06/13/06
16:00
SM 2540G
Nitrogen, Total Kjeldahl
4.83
48300
100
JM
06/14/06
16:00
EPA 351.3
2.76
27600
100
JM
06/15/06
16:00
SW 846-601OB
Phosphorus
0.46
4600
100
JM
06/15/06
16:00
SW 846-601OB
Potassium
1.07
10700
100
JM
06/15/06
16:00
SW 846-601OB
Sulfur
1.69
16900
100
JM
06/15/06
16,00
SW 846-601OB
Calcium
0.47
4700
100
JM
06/15/06
16:00
SW 846-601OB
Magnesium
0.18
1800
100
JM
06/15/06
16:00
SW 846-601OB
Sodium
28400
1
JM
06/15/06
16:00
SW 846-601OB
Iron
23700
10
JM
06/15/06
16:00
SW 846-601OB
Aluminum
432
1
JM
06/15/06
16:00
SW 846-601OB
Manganese
495
1
JM
06/15/06
15:00
SW 846-601OB
Copper
1130
1
JM
06/15/06
16:00
SW846-6010B
Zinc
Nitrogen, Ammonia (as N)
0.37
3700
10
JM
06/14/06
14:00
EPA 350.2
Nitrogen, Organic (N)
4.46
44600
100
1
DCH
KS
06/14/06
15:00
CALCULATION
SM 4500-NO3F
Nitrogen, NO3+NO2
< 1
2.0
1
JM
06/15/06
16:00
SW 846-601OB
Cadmium
43
5
JM
06/15/06
16:00
SW 846-601OB
Chromium
All values are on a dry weight basis except as noted. `Detection Limit on all N series is on a wet basis
Out /e•I)orl:. aped 10ter ; lira A,[ the exclosrve anti cnnhrlratlal Ilse of ouI (11(el ts. allrl play not be Ieplodur;erl III whole or In pllli not rally ;Ivry Ielerence We nlllrle � {
rn Ihr wnrl: the n•�rdl:. ur (hr• r runpany ru any arJvwh:.utrl nett:; rclr•;C;rr ur a/Llr-I public aliflow nc(",; R./It:, rad1wol nhlarnu)r/ ow pnnr wrIll( -o mIlhpnlahr)rI ,V
PAUL C 11 CHU

Report Number:
R06165-8005
Account Number:
46381
A&L EASTERN LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237 . [phone]
Fax No. [phone] • Email: [e-mail]
TO: SOUTHERN SOIL BUILDERS
958 HOOTS ROAD
ROARING RIVER, NC 28669
ATTN: DENNIS KEY
LAB NUMBER: 42689
SAMPLE ID: MARION
FOR: MARION
NC CERT #257
REPORT OF ANALYSIS
copy: ZACH KEY
DATE SAMPLED: 6/8/2006 1600
DATE RECEIVED: 6/13/2006 1130
DATE REPORTED: 6/16/2006 PAGE: 2
Nickel
31
5
JM
06/15/06
16:00
SW 846-601OB
Lead
58
5
JM
06/15/06
16:00
SW 846-6010B
Arsenic
1.9
0.1
KM
06/15/06
15*00
SW 846-7061A
Mercury
3.9
0.2
KM
06/15/06
15:00
SW 846-7471A
Selenium
3.7
0.1
KM
06/15/06
15:00
SW 846-7741A
Molybdenum
24
5
JM
06/15/06
16,00
SW 846-601OB
All values are on a dry weight basis except as noted. "Detection Limit on all N series is on a wet basis
our teporls and letters are lot the exclusive and conhdenhal use of our cliet its. and play not be reproduced rn whole of in part. nor may any reference be made
to the walk the resrllts. Ot Ih(.! C'Gnmany 11) any a0velb."111y, news release,.. 01 other public antiouricements without obtaining out prior wut(en aumon7atron -��
pAUL C H CHU

BIOSOLIDS SAMPLE TRANSMITTAL FORM/CHAIN OF CUSTODY
A&L Eastern Agricultural Laboratories, Inc.
AIL t inc Road Richmond VA 23237 Tcl: 804-743-9401 Fax: [phone] Email: ofriccW-labs-Castcm-coro
7621 Whu cP
® Customer Information
Copy To
Charge To
1 Submitted By
St J ikfi I� ��I }v.1G^t�l n
Project I /'nu -,'U
Lab Number Co o Information
Sarnpie ID (Lab Use Date Tire
Only) Type
Grab -s`04/�'- y. 'Lf Pn
Corrposite
Grab
Composite
_ Grab
Composite
= Gate
mation
Inlorrttatlon
e Vokxne SL1
ozass
pintgtic
_�iqt_
i
ozlass
pintasticozlass
pintastic
t_
ozUc_pint,
Date Time ReceNed B. S >
Rell B
0..7
Test Pa le Details
SL1: Total Solids (Moisture) Total Kjeldahl Nitrogen, Phosphorus and Potass'um And Zinc
SL2: Basic Test SLI plus Sulfur, Calcium, Magnesium,Sodium, iron` Aluminum, Manganese, Copper
503 Metals: Arsenic. Cadmium, Chromium. Mercury- Molybdat-m. Lead. Nickel. Selenium.
(Copper & Zinc Included in SI2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & organic Nitrogen. Treated Sludge)
CCE: Calcium Carbonate Equivalent or Total neutralization Value For
Lim
IAccount #
. 63
please Check Desired Tests
Volatile
Sl2 503 PN- t AV CI Soils
metals Series —
a
Soaclal Instructions or RematiCs

s � �
Analytical Results
Pace Analytical -Asheville For. 921 18094
2225 riverside Drive
Asheville NC 28804
Enterer! 4/27/2006
Reported: .15/92006
Sample Remark
Sample ID Parameter Cust 1D Result Units Method Date Anatyzed analyst
060427-7.1
% Solids
926913724
2.8
%
SM2540B
4J27/06
MD
060427-7.1
Fecal Coliform MTF
926913724
250000
MPNlg
SM92210E
4127l06
MD
060427-7.2
% Solids
926913732
2.81
%
SM2540B
4/27/06
MD
060427-7.2
Fecal Coliform MTF
926913732
177936
MPN/g
SM92210E
4/27/06
MD
060427-7.3
% Solids
926913740
2.76.
%
SM25408
4/27/06
MD
0427-7.3
Fecal Coliform MTF
926913740
253623
MPN/g
SM92210E
4/27/06
MD
060427-7,4
% Solids
926913757
2.76
%
SM2540B
4127/06
MD
060427-7.4
Fecal Coliform MTF
9269137:57
83333
MPN/g
SIVIMICE
4127/06
MD
060427-7.5
% Solids,
926913765
2.81
°i6
SM25408
4127/06
MD
060427-7.5
Fecal Cordorm MTF
926913765
249110
MPN/g
SM92210E
4127/06
MD
060427-7.6
% Solids
926913773
2.9
SM25408
4/27/D6
MD
060427-7.6
Fecal Coliform MTF
926913773
310345
MPN/g-
SM92210E
4/27/06
MD
060427-7.7
% Solids
92.6913781
2.84
%
SW540B
4127106
MD
060427-7.7
Feral Coliform MTF
926913781
59859
MPN/g
SM9221 CE
4127/06
MD
D60427-7. ;
Geometric Mean
926913781
171428
MPN/g
dry wt. basis
4/28/06
MD
Respectfully submitted,
Drina Myers
NC Cert #440,
NCDW Cert #37755,
EPA NCO0909
P.O. Box 228 • Statesville, North Carolina 28687 ° 701WZ/4697

aceAnalytical
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 926913997
Client Sample ID: CC SL TCLP-(3)
race Analyucal aervrces, utu.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
raves nnaaquw, W-..vw, ...-
2225 Riverside Drive
Asheville, NC 28804
Phone"828.254.7176
Fax: [phone]
Lab Project Number 92118098
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92118098.001 Date Collected: 04/26/06 11:55
Matrix: Soil Date Received: 04/26/06 17:16
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual Re4Lmt
Metals
Trace ICP Metals, TCLP Leach.
Prep/Method:
EPA 3010 /
EPA 6010
Arsenic
NO
mg/l
0.025
04/29/06
17:25
SAJ
7440.38.2
Barium
0.36
mg/l
0.025
04/29/06
17:25
SAJ
7440.39-3
Cadmium
NO
mg/l
0.0050
04/29/06
17:25
SAJ
7440-43.9
Chromium
NO
mg/l
0.010
04/29/06
17:25
SAJ
7440.47-3
Lead
NO
mg/1
0.025
04/29/06
17:25
SAJ
7439.92.1
Selenium
NO
mg/l
0.025
04/29/06
17:25
SAJ
7782.49.2
Silver
NO
mg/l
0.010 -
04/29/06
17:25
SAJ
7440.22.4
Date Digested
04/28/06 09:30
04/28/06
09:30
Metals, Trace ICP
Aluminum
Arsenic
Cadmium
Calcium
Copper
Lead
Magnesium
Molybdenum
'Nickel
Potassium
Selenium
Sodium
Zinc
Date Digested
Prep/Method: EPA 3050 / EPA 6010
370
mg/kg
10.
NO
mg/kg
0.51
`ND
mg/kg
0.10
320
mg/kg
10.
12.
mg/kg
0.21
1.4
mg/kg
0.51
130
mg/kg
10.
NO
mg/kg
0.51
ND
mg/kg
0.51
140
mg/kg
100
ND
mg/kg
0.51
NO
mg/kg
100
23.
mg/kg
1.0
05/01/06
10:45
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Date Digested 04/28/06 13:15
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Hercury ND mg/l
Mercury, CVAAS, in Soil
Mercury
<<1'.�.Wet Chemistry
Percent Moisture
Date: 05/15/06
villa Certification ID
NC Wastewater . 40
NC Drinking Water 37712
Sc 99030
;FL NELAP E87648
Method: EPA 7471
0.032 mg/kg
Method: X Moisture
05/02/06 02:20 JDA1 7429.90.5
05/02/06 02:20 JDA1 7440.38.2
05/02/06 02:20 JDA1 7440.43.9
05/02/06 02:20 JDA1 7440.70.2
05/02/06 02:20 JDA1 7440.50-8
05/02/06 02:20 JDA1 7439.92.1
05/02/06 02:20 JDA1 7439.95-4
05/02/06 02:20 JDA1 7439.98.7
05/02/06 02:20 JDA1 7440.02.0
05/02/06 02:20 JDA1 7440-09.7
05/02/06 02:20 JDA1 7782.49.2
05/02/06 02:20 JDA1 7440.23.5
05/02/06 02:20 JOA1 7440.66.6
05/01106 10:45
04/28/06 13:15
0.00020 05/01/06 12:39 ALV 7439.97.6
0.0054 04/27/06 11:58 ALV 7439.97.6
Page: 1 of 4
REPORT OF LABORATORY ANALYSIS Charlotte Certification IDs
This report shall not be reproduced, except in full, NC Wastewater 12
NC Drinking:Water 37706
without the w9
written consent of Pace Analytical Services, Inc. 90
SC 9006
ACC° °'° FL NELAP E87627
A-:_%1'.

aceAnalyticale
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 926913997
Client Sample ID: CC SL TCLP-(3)
raOC HNatym-ai o01 vivoo, nrv.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92118098
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92118098-001 Date Collected: 04/26/06 11:55
Matrix: Soil Date Received: 04/26/06 17:16
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Qual ReciLmt
Metals
Trace ICP Metals, TCLP Leach.
Prep/Method:,EPA
3010 /
EPA 6010
Arsenic
NO
mg/l
0.025
04/29/06
17:25
SAJ
7440.38-2
Barium
0.36
mg/1
0.025
04/29/06
17:25
SAJ
7440.39.3
Cadmium
NO
mg/l
0.0050
04/29/06
17:25
SAJ
7440.43-9
Chromium
NO
mg/1
0.010
04/29/06
17:25
SAJ
7440.47-3
Lead
NO
mg/l
0.025
04/29/06
17:25
SAJ
7439.92-1
Selenium
NO
mg/1
0.025
04/29/06
17:25
SAJ
7782.49-2
Silver
NO
mg/l
0.010
04/29/06
17:25
SAJ
7440-22.4
Date Digested
04/28/06 09:30
04/28/06
09:30
Metals, Trace ICP
Prep/Method:
EPA 3060 /
EPA 6010
Aluminum
370
mg/kg
10.
05/02/06
02:20
JDA1
7429-90-5
Arsenic
NO
mg/kg
0.51
05/02/06
02:20
JDA1
7440-38.2
Cadmium
NO
mg/kg
0.10
05/02/06
02:20
JDA1
7440.43.9
Calcium
320
mg/kg
10.
05/02/06
02:20
JDA1
7440.70.2
Copper
12.
mg/kg
0.21
05/02/06
02:20
JDA1
7440-50.8
Lead
1.4
mg/kg
0.51
05/02/06
02:20
JDA1
7439.92-1
Magnesium
130
mg/kg
10.
05/02/06
02:20
JDA1
7439.95.4
Molybdenum
ND
mg/kg
0.51
05/02/06
02:20
JDA1
7439.98.7
Nickel
ND
mg/kg
0.51
05/02/06
02:20
JDA1
7440.02.0
Potassium
140
mg/kg
100
05/02/06
02:20
JDA1
7440-09.7
Selenium
ND
mg/kg
0.51
05/02/06
02:20
JDA1
7782-49.2
Sodium
NO
mg/kg
100
05/02/06
02:20
JDA1
7440.23.5
Zinc
23.
mg/kg
1.0
05/02/06
02:20
JDA1
7440.66-6
Date Digested
05/01/06 10:45
05/01/06
10:45
Mercury, CVAAS, TCLP Leachate
Method: EPA
7470
Date Digested
04/28/06 13:15
04/28/06
13:15
Mercury„ CVAAS, TCLP Leachate Method: EPA 7470
Hercury NO mg/l
Mercury, CVAAS, in Soil
Mercury
i p.., Wet Chemistry
Percent Moisture
Date: 05/15/06
Asheville Certification IN
NC Wastewater 40
NC Drinking Water 37712
SC 99030
ti EL NELAP E87648
Method: -EPA 7471
0.032 mg/kg
Method X Moisture
0.00020 05/01/06 12:39 ALV 7439.97.6
0.0054 04/27/06 11:58 ALV 7439.97.6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
1M ACCO40
Page: 1 of 4
harlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

S(6 ?
� J
aceAnalytical
www.pacelabs.com
Lab Sample No: 926913997
Client Sample ID: CC SL TCLP•(3)
rave mitaqui at oG1 VM00, 11/41.
9800 KinceyAvenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: [phone]
1 YVV NIY,�, .r, •.���, ... �.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 92118098
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92118098.001 Date Collected: 04/26/06 11:55
Matrix: Soil Date Received: 04/26/06 17:16
Parameters Results Units Report Limit Analyzed By CAS No. Qual Re Lmt
Percent Moisture 9.7 X 04/28/06 17:05 KDF
Total Percent Solids Method: EPA 160.3
Percent Solids 90.3 X 05/01/06 TNM
Nitrogen, Ammonia Method: EPA 350.1 Modified
Nitrogen, Ammonia 38. mg/kg 10. 05/08/06 10:10 BMF 7727.37.9
Total Kjeldahl Nitrogen, Soil Method: EPA 351.2
Nitrogen, Kjeldahl, Total 1800 mg/kg 11. 05/08/06 20:30 JMW
Nitrogen, Nitrate plus Nitrite Method: EPA 353.2 Modified
Nitrate as N ND mg/kg 9.9 05/12/06 13:44 JDA1
Nitrate -Nitrite (as N) ND mg/kg 9.9 05/12/06 13:44 JDA1 7727.37.9
Phosphorus, Total, Soil
Phosphorus
Plant Available Nitrogen
Nitrogen
GUMS Semivolatiles
Semivolatile Organics, TCLP
1,4•Dichlorobenzene
2,4-Dinitrotoluene
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
2-Methylphenol (o-Cresol)
3&4-Methylphenol
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
Date: 05/15/06
heville Certifi
NC Wastewater 40
NC Drinking Water 37712
Sc 99030
FL NELAP E87648
Method: EPA 365.2
522. mg/kg 56.5 05/10/06 10:20 SAJ 7723.14-0
Method:
550 mg/kg 1.0 05/15/06 SHB 7727.37.9
Prep/Method:
EPA 3510 / EPA 8270
ND
mg/l
0.75
NO .
mg/l
0.013
NO
mg/l
0.050
NO
mg/1
0.013
NO
mg/l
0.30
ND
mg/l
0.050
NO
mg/1
0.010
ND
mg/l
0.20
NO
mg/l
10.
NO
mg/l
0.50
ND
mg/l
40.
NO
mg/l
0.20
50
%
47
X
51
X
24
X
05/10/06 13:47 BET 106.46.7
05/10/06 13:47 BET 121-14.2
05/10/06 13:47 BET 87.68.3
05/10/06 13:47 BET 118 74 1
05/10/06 13:47 BET 67.72-1
05/10/06 1347 BET 95.48.7
05/10/06 13:47 BET
05/10/06 13:47 BET 98-95.3
05/10/06 13:47 BET 87.86.5
05/10/06 13:47 BET 110.86.1
05/10/06 13:47 BET 95.95-4
05/10/06 13:47 BET 88-06.2
05/10/06 13:47 BET 4.165.60.0
05/10/06 13:47 BET 321.60.8
05/10/06 13:47 BET 1718.51-0
05/10/06 13:47 BET '4165.62.2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
without the written consent of Pace Analytical Services, Inc.
�M ACQpRa
� `ti1fA��t
Page: 2 of 4
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
Sc 99006
FL NELAP E87627

�aceAnalytical�
Section A-. -
Re uIred Cllanl Infnrmaflon•
Section B
Reaulred Project Information
(.:MAIN T—UUJ t ULJ T I Hrlaiyiicai nequest uuct ;ern try -
The IN
is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
Section C
Invoice Information:
a ,
Page: of
095135.8
Company ('
Report To: �j�J ` Attention:
((U ✓
REGULATORY AGENCY
1
r L��
❑ NPDES
❑ GROUNDWATER
❑DRINKING WATER
Address
Copy To:
Company Name:
❑ UST
❑ RCRA
❑Other
IV G 2R %S Z'
Address:
•
❑GA OIL ❑IN
❑MI ❑MN ANC
Email To:
Purchase Order No:
Pace Quote Reference:
❑OH ❑SC ❑ WI
❑OTHER
711—/ Sz () 7 Fax / //// Project Name:
"f
Pace'Project Manager.
- iw t/p5 / l
Y�
Filtered (YR4)
Requested Due DatefTAT:
Project Num r:
0
Pace Profile#:
Requested
Analysis:
Vend tdetrbc Codes .
SeCCIOj 'D. Re'qulred•Clle*6tlnformation MATRIX ' CODE
p
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Additlondl Oomrtlent's:
SAMPLER SIGNATURE
NAME AND
_
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m
PRINT 9prne of SAMPLE ` j/
Lee. I-eS
J
----------
E
I sIown IRF f RARM FP,-

Number: umber:
Report Nu 2 A&L Eastern Laboratories, Inc.
Account Number: 7621 Whitepine Road Richmond, Virginia 2323.7 [phone]
Acco
Acco Faz No. [phone] Email: [e-mail]
Send To: SOUTHERN SOIL BUILDERS Grower: SOUTHERN SOIL BUILDERS
958 HOOTS ROAD
ROARING RIVER, NC 28669
SOIL ANALYSIS REPORT
w7i,.)nn7 nate of Report: 2/8/2007
@0
Submitted By: SOUTHERN SOIL BLDRS
Analytical Method(s):
ad a
ion at symbols: % (percent), ppm (parts per million), IbslA (pounds per acre),
Values on this report represent the plant available nutrients A 8 L EASTERN LABORATORIES. INC.
). the soil. Explanation
Ratting after each value: VL (Very Low), L (Low), M (Medium), H (High), VH (Very High). mslcm (milli -mhos per centimeter), meq/100g' (milli -equivalent per 100 grams)- by. S�).J- e --
ENR - Estimated Nitrogen Release. C.E.C. -Cation Exchange Capacity.
Conversions: ppm x 2 = IbsIA, Soluble Salts mslcm x 640 = ppm. Paul Chu, Ph.D.
NC

Report Number:
R07037-0122 - A&L Eastern Laboratories, Inc.
Account Number.
c7621 Whitepine Road Richmond, Virginia [phone]
Fax No. [phone] Email: [e-mail]
To: SOUTHERN SOIL BUILDERS For: SOUTHERN SOIL BUILDERS copy To: SOUTHERN SOIL BLDRS
958 HOOTS ROAD
ROARING RIVER, NC 28669
Attn: DENNIS KEY
Date Received: 02/06/2007 Date Reported: 02/08/2007 BOIL FERTILITY RECOMMENDATIONS
e e ,
4 tons
0.8
50
30
300
0
R1
Fescue
4 tons
0.0
50
30
300
0
R2
Fescue
4 tons
0.8
50
0
170
0
F-01
Fescue
4 tons
1.0
50
0
270
0
F-02
Fescue
Page: 1
Sample F-02: Apply dolomitic lime to raise pH and improve the magnesium level.
Samples R1, R2, F-01, F-02: Apply additional 50 pounds of nitrogen after every cutting.
Samples R1, R2, F-02: The recommended amount of potash is the total amount per acre needed to achieve the yield goal. To prevent salt
injury, single application for K20 should not be over 200 Ibs per acre, split the total amount of K20 into 2 or 3 applications.
"The recommendations are based on research data and experience, but NO GUARANTEE or WARRANTY expressed or implied', concerning crop performance is made!
Our reports and letters are for the exelusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may arty reference be made to the Paul Chu, Ph. D.
work, the results, or the company in any advertising, news release, or other public announcements withoul obtaining our prior written auttortzetion. Copyright 1977.

"41 o f Mor`'o'-1
Annual Report Review Sop
1.. Annual Land Application Certification Form
• Was a certification form submitted? y25
• Was land application conducted during the reported year? yes
• How many dry tons and dry tons per acre were applied? 105, la -r-,T
• Were the applications within the permitted amount?YO
• Verify PAN if more than 10 tons/acre td A
• Did it indicate compliance? �0-5
• Was it -signed by the appropriate people? ye.s
2. Monitoring
• Were the analyses conducted at the required frequency? JC5
• Were the metals analyses reported on the Residual Sampling Summary Form?�►�
• Were the results reported in mg/kg?yle-5
• : Were the heavy metals within ceiling concentration permit limits?*4,eS
SP
�Uj5old "J-r%
tn�� i
• If no, were the lab analyses attached? s .r 0e id
• Were all there required parameters tested? . yr n� 1^S
• q p B¢n2enei �x ��}o Te iracJ�lO ides Chlo�o�tne� Cl Ia.o �cn2ell 1 eiN
Was TCLP analysis co ducte ?�le� ,ob f _ Revd .�Al-P, 1,2-Ditl�lor�e}Hcn�1 - �hle� �v G �ndr n HrrlQuilCy, Li,da2 ei
Cdrivf�pp-AG ..'y�yr�� j 10 ��.ftnpXL hlor rralhl l
g 3. Field Summary S c-
y_, rkpe4o�e� Te�rAc�Iaro�i�l 7okc?',pAi�e,ie'-i
For oT
• � Were the land application. events recorded on the Field Summary FormsN s
• Was a Field Summary Form submitted for each field? y
• Were all the residuals applied to permitted land?e5
• Were all the residuals applied from permitted sources?jzS
• Were the field loading rates for each metal and PAN calculated (year to date)? Y2S
• Were the cumulative pollutant loading rates calculated?14--s
• Were the calculations correct?yo-5
• Were the PAN loading rates. within permit limits? Ye'
• Were the heavy metal cumulative pollutant loading rates within permit limits? yzf
• Were the residuals applied on a suitable crop? y-eS
• Werethe applications conducted during the crop's growing season?yas
• Were the Field Summary Forms complete? .../e,S
Larry] Avv�Lr
W y 1 �1r
d
,p4yIlk
lgnl�./ ..4
ar &Jgse 5
4. Pathogen and Vector Attraction Reduction '
• Wasa signed copy of the Pathogen and Vector Attractioneduction Form submitted? yes
• Did the form indicate the Period of coverage, the residual class, and the pathogen r de uction alternative and the
vector attraction reduction option used? � _ ��,� du wtng
• Was the appropriate docume ati 1 slow atho�en a��d vector attraction reduction included in the report?
• Was pathogen and vector a,cci n reductio ,�erosiQsirafed according to 40 CFR Part 503'?
3$dlo Pad+ t7� . W&S noA- �A� 2
5. Soil Tests "� h' l s�"'P/� rolfea�✓�� yoof�rFl
• Was a Standard Soil Fertility Analysis conducted for each application field? Ye's `
• Were the soil pH's 6.0 or greater for each application field? NO R-1 5.1 �-o t $.7 �-e�2 5• S
• Were the copper and zinc indexes in the soil less than 3000 for each application field? r14- C-
��1Sc�p �M►SSino�-�'�ch//�� �^�e.��b9 � oci�u���.s�ac�n�r��// °u"l��o`�"�� .ask t.Str .a��`�.*n
6. General
hA'n_.Ean�, z�� rc�d dtrri inS ,�t��—OK. _ V�• J✓
• Was the report in the proper format? -y e3 P <G c \\02i . Rd
• Were any parts of the annual report missing?;,5_e
• Was the report submitted on time? �,� #l-� rcvd
P 7ae k
* Any violations of ceiling,concentrations should be reported to Pretreatment for municipalities only. owne.4 re�_

L( tA,,b.) Y. (i-Ik-w T NW3) + Cb. S x C��13-N ) I + C►`�b2 + Nbs
0.3 X Hg O— 3700 —1 L 0. 5 x 3700] + I
= i� � 31 r•o, � 1z�
.06 = 36.1& 16s IDT x
79.0/6 r-6fAc.
SJ i�!f
F,eA 2i
= �� rr,a �� o b0 2 ©. /0 (z Ib�DT X A.5° 39 5 9'�
6
J � , ozaz3 ibj�,
x .06Z = oo-7 .394/y!!�7—
0vz= 30 .'4(" X z. �795`3oSr �q. �t3416 gc.
bo3� )c
�_ 2 Z� 2 .2-795-3o
x
�n � 193� ►� ��i .00
4 4 11as Di X
i61ac.

Division of Parks and Recreation --Hanging Rock State Park, Get Directions
Page "44"
N.C. Division of Parks. and Recreation .1615 MSC • Raleigh, NC 27699.[phone]
http://ils.une.edu/parkproject/visit/haro/directions.html 3/12/2007

VS in
VS out
VSFR= 1.469238
VS
Un
03 Gut
o �-75

CITY OF. MARION
CORPENING CREEP WASTE
TREATMENT PLANT
LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEE T
Standard Methods 20TH Edition —Method 2540 E
RUN DATE:5-15-06
TIME IN:1111
TEMP IN: 103*C
ANALY3T:R. Carter
TIME WEIGHED: 13,VS'
TIME OUT:1211
TEMP OUT:103*C
ANALYST:R. Carter
TIME IN: /51-/Z
TEMP IN:552 *C
TIME WEIGHED: 16
TIME OUT:/,1(32-
TEMP OUT5s3*C VSS
A
C A
B
A-B
SAMPLE
DATE
: Sample
Filter
FILTER +
FILTER
Residue
FILTER +.ASH
ASH +
COLLECT
Vol.
#
Residue before
WEIGHT
Wt., Gr.
After Ignition
FILTER
ML
ignition, Gr.
(GRAMS)
(GRAMS)
(GRAMS)
Blk
71
c!
1.4799
930.
0 oB
CC MLSS
5/15120061
5 1
14 1
65-1.91 1
1.4750
p. oq-3
[01
" Du
5`
16
1.4835
o,c)g33
<0 101
1035�
CC RAS
5
11
/, S 3 3,S
1.4811
p. b59
A '20
F0, 0.44('T
CC INF. 1 1 25 1 31 1 / ,5-Z 85 1 1.527d 1 0, 001
DILUTION - 1000000
FACTOR = ML OF SAMPLE
Mg Volatile Solids / L = LA - B) X 1000000
Sample Vol.,. ML.
Mg Fixed Solids / L B - C) X 1000000
Sample Vol., ML.
% Volatile Solids = Total VSS
Tot. Vss + Tot. Fixed
** BALANCE CALIBRATED DA
BALANCE CALIBRATION B
LOT #'S
GLASS FIBER FILTER: 51634

CITY OF MARION
CORPENING CREEK WASTE TREATMENT PLANT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
Standard Methods 20TH Edition —Method 2540 E
RUN DATE:,,; -4-66 TIME IN: og3� TEMP IN: /63 `C
ANALYST: R� TIME WEIGHED: /z5P TIME OUT://35'� TEMP OUT:in3*C
ANALYST: W TIME IN: TEMP IN: ss/ *C
TIME WEIGHED: 151/0 TIME OUT: /3S d TEMP OUTS9(*C
A r A -f' I . R
VSS FIXED
_!.A_R R-C
• •
TOTAL
MOM
i
!�WA
DILUTION 1000000
FACTOR = ML OF SAMPLE
Mg Volatile Solids / L = j A - B ) X 1000000
Sample Vol., ML.
Mg Fixed Solids / L = j B - C) X 1000000
Sample Vol., ML.
% Volatile Solids = Total VSS
Tot. Vss + Tot. Fixed
* BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CALIBRATION BOOK
LOT #'S .

1�5aceAnalyficaf
wim. pacelabs.co",
31
Lab Sample No: 926913997
Client Sample ID: CC SL TCLP-(3) —�
Pace Analytical Services, Inc.
9800 Kincey Avenue, Suite 100
Huntersville, NC 28078
Phone: [phone]
Fax: 704.875,9091
Pace Analytical Services, Inc,
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax., 828.252.4618
Lab Project Number: 92118098
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 92118098-001 Date Collected: 04/26/06 11:55
Matrix: Soil Date Received: 04/26/06 17:16
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No. Oual RegLmt
2-Fluorophenol (S)
34
%
05/10/09
13:47
BET
367-12-4
2,4,6-Tribromophenol (S)
48
%
05/10/06
13:47
BET
118-79-6
Date Extracted
05/09/06
05/09/06
GC Semivolatiles
Pesticides, TCLP Leachate
Prep/Method:
EPA 3535 /
EPA 8081
gamma-BHC (Lindane)
ND
mg/1
0.040
05/11/06
02:11
JEM
58-89-9
Chlordane
ND
mg/l
0.0030
05/11/06
02:11
JEM
57-74-9
Endrin
ND
mg/l
0.0020
05/11/06
02:11
JEM
72-20-8
Heptachlor
ND
mg/l
0.00080
05/11/06
02:11
JEM
76-44-8
Methoxychlor
ND
mg/1
1.0
05/11/06
02:11
JEM
72-43-5
Toxaphene
ND
mg/1
0.050
05/11/06
02:11
JEM
8001-35-2
Tetrachloro-m-xylene (S)
82
%
05/11/06
02:11
JEM
877-09-8
Decachlorobiphenyl (S)
93
%
05/11/06
02:11
JEM
2051-24-3
Date Extracted
05/09/06
05/09/06
^--C/MS Volatiles
.)latile Organics, TCLP Leach,
Method: EPA
8260
Benzene
ND
mg/1
0.0050
05/03/06
20:38
DLK
71-43-2
2-Butanone (MEK)
ND
mg/l
0.10
05/03/06
20:38
DLK
78-93-3
Carbon tetrachloride
ND
mg/1
0.0050
05/03/06
20:38
DLK
56-23-5
Chlorobenzene
ND
mg/l
0.0050
05/03/06
20:38
DLK
108-90-7
Chloroform
ND
mg/l
0.0050
05/03/06
20:38
DLK
67-66-3
1,4-Dichlorobenzens
ND
mg/1
0.0050
05/03/06
20:38
DLK
106-46-7
1,2-Dichloroethane
ND
mg/l
0.0050
05/03/06
20:38
DLK
107-06-2
1,1-Dichloroethene
ND
mg/1
0.0050
05/03/06
20:38
DLK
75-35-4
Tetrachloroethene
ND
mg/l
0.0050
05/03/06
20:38
DLK
127-18-4
Trichloroethene
ND
mg/1
0.0050
05/03/06
20:38
DLK
79-01-6
Vinyl chloride
ND
mg/l
0.0050
05/03/06
20:38
DLK
75-01-4
Toluene-d8 (S)
90
%
05/03/06
20:98
DLK
2037-26-5
4-Bromofluorobenzene (S)
79
%
05/03/06
20:38
DLK
460-00-4
Dibromofluoromethane (S)
106
%
05/03/06
20:38
DLK
1868-53-7
1,2-Dichloroethane-d4 (S)
96
%
05/03/06
20:38
DLK
17060-07-0
Date: 05/15/06
Asheville Certification IDs REPORT OF LABORATORY ANALYSIS Charlotte Certification IOs
NC Wastewater 40 This report shall not be reproduced, except in full, NC Wastewater 12
- NG Drinking Water 3771.2 Athout the written consent of Pace Analytical Services, Inc. NG Drinking Water 37706
SC Environmental 99030 $C 99006
FL NELAP E87648 P NELAP E87627
Page: 3 of 4

Analytical Environmental Services, Inc.
Date: 05-May-06
CLIENT: Pace Analytical Services, Inc. Client Sample ID: 926914052
Project: 92118098 Collection Date: 4/26/2006 11:55:00 AM
Lab ID: 0604G 18-001 Matrix: AQUEOUS
Analyses
Y
Result
Reporting
Limit
Qual Units
BatchID
llttution
Factor
Date Analyzed
HERBICIDES, TCLP
SW1311/8151A
(SW3510B)
Analyst: BJ
2,4,5-TO (Silvex)
BRL
0.50
mg/L
70418
1
5/4/2006 3:09 PM
2,4-D
BRL
0.50
mg/L
70418
1
5/4/2006 3:09 PM
Surr: DCAA
98.2
21.3-162
%REC
70418
1
6/4/2006 3:09 PM
Qualifiers: ' Value exceeds Maximum Contaminant Level E Estimated (Value above quantitation range)
BRL Below Reporting Limit S Surrogate Recovery outside accepted recovery limits
H Holding times for preparation or analysis exceeded Narr See Case Narrative
N Analyte not NELAC certified NC Not Confirmed
B Analyte detected in the associated Method Blank Page I of 1

777
PRECISION PETROLEUM LABS, INC.
5915 Star Lane Houston, TX, 77057
Ph.713-680-9425 Fax:[phone]
COMPANY:
INVOICE No.:
LAB REFERENCE No.:
PRODUCT ID:
DATE RECEIVED:
AUTHORIZED BY:
Ph
I-pitabift. (Flesh Pout), PMCC
1iefctivo Cyanides; PPM
Reactivb Sulfides, PPM
CERTIFICATE OF ANALYSIS
PACE ANALYTICAL
300032
2006-04-999-012
926914086 04-26-2006
04-28-2006
TOM WILLIAMS
TEST
METHOb
S.W. 0040
EPA 1010
S.W. 9010
S.W. 9030
RFPORTING
LIMIT
RESJjLn
0.01
5.12
-106F'
> 230
0.01
ML
1.0
BRL
Vw
BRL = BELOW REPORTING LIMIT
PRECISION PETROLEUM LABS, I NVS RESPONSIBIIM FOR THE AAOVE ANA -AS,
OPINIONS OR INTERPRETATIONS IS LDGTED TO TIC INVOICE AMOUNT.'

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fli-I Mn-A10)k1jx-AiF(2) Zn
S*?fl crass aw W/V CBC $3% Ac p X-1 Ca!6 —Mr4li 11 Z,?-41 CV-1 S-1 SS-1 NO3^ N NW4-A Na
KIN 0.97 V. 03 8'.0 1-5. 5,8 119 47 61,C 25-0 74Fie[.li1 for' 6-
185 185;. 1-69 5,2
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05 Z?; B Atli seeA'ae
R2Pes,�C-0.�in,i4SCrroP:1 ZCI-20C 0 10-0 5
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Sod (W& YN% IV/Tl
CR( 85% Ac� p 11 P-1 K-1 ca% 11$ 6m &,_1 S71 sS4 X63"N -.yjf4-,v Al'a
:Nlr 0.97 l,08
$-9 820 A 5.8 76 66 53.0 20 L91 134 .0 9 9( k .3 47 0.3
Phoue:-"(91
. W ­ . 19). 3-2655- Wob:Site; "W.
A04%b
Aff 7
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SLBUG -K-Cr. R17SIDENTSYDR OVER 6( Yl'..:V.-S
NCO
5'etitlif rp'Soil fluildeirs [tic.
958 Hoots U
Roaring Rj4r, KG, 28669
Farm:
.McDowell CoWity

, M -7 1 r- . I ".'Y
0.9/2007 15:13 3369578940
Cril ITUCDKICr)Tl DI ITI CDC DAr--C, m) / m)
SOUTHERNSOILBUILERS PAGE 01/02
S Southern
S. Soil
B- I[-.B-ul-l--ders, Inc.
27
FROM
DATE
COVER.PAGE PLUS I
COMMENTS
9.58 Hoots Road.-%aftn
(3g- . P-Iver,. NC 2866--g.
-3-6.)- 95'7--B.9()g i'Fa-
x (3n6) 957'8940

zo@7 15:13 3369578940 SDUTHERNSOILBUILERS PAGE 02/02
EXC-ffAMEABLE SODIUM PERCENTAGE (ESP)
FIELD ESP
Rl
2.65%
E2
2.92%
Pi
.2'2 8 o/o
F2
2.83%