WQ0019960_Annual Report_20050222

ANNUAL LAND APPLICATION CERTIFICATION FORM r( v
Permit#: WQ0019960 County:
McDowell Year: 2004
I
Facility Name (as shown on permit): City of Marion
Land Application Operator: Southern Soil Builders, Inc. Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past calender year?
M Yes [3No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A: "-
Total number of application fields in permit: 8
Total number of fields land application occurred during the year: 3
— 170.26
Total amount of dry tons applied during the year for all application sites•
Total number of acres land application occurred during the year
66
Part B: application permit
Facility was compliant during calendar year 2004 with all conditions of the land app ' p
(including but not limited to items 1-12 below) issued by the Division of Water Quality. M Yes ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken.
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached. a
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 13 pin the
es 0
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regu§114 fac 1 Vn
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503`T,43vere�
complied with (applicable to 40 CFR Part 503 regulated facilities).,, CD
emit were complied with or, in the case of aexiatig,
3. All operations and maintenance requirements m e p r.
prior authorization was received from the Division of Water Quality.
�. No contravention of Ground.Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
11, No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
Cc'{'►I Markl�v
Permittee Name and Title (type or print)
2
Signature of Preparer* Date
(if different from Permittee)
' Preparer is defined in 40 CFR Part 503.9 (r)
igna e of Permittee U Date
Signiture of LA Applier Date
(if different from Permittee and Preparer)
DENR FORMACF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number:
Facility Name:
NPDES # or
WQ#:
WQ0019960 Laboratory: 1) A&L Eastern Agricultural Labs Inc.
City of Marion
NCO031879
WWTP Name: City of Marion WWTP
2)
3)
4)
5)
Sample or
Composite Date
Percent So —lids
Y----_--_
. , •
• 11
w
-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance w►tn a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
4*iggnaure of Preparer Date
DENR FORM RSSF (5/2003)
1

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 44.32
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Toua & Tong Khang Owner: Toua & Tong. Khang
Acres Used: 16 Acres Permitted: 16 Site #: K1 Field #: KI
1 Phnqnhorus use m0ce, % Solids use Raw Percent #):
Non
Non
Annual
tieavy ivietxr
1
rteru
2
a.va—gam
3
��
4
a....,..�. ..-
5
6
-.
7
8
9
10
t1
12
_G
yw
b d
w
w Y
o'
2.77
0
0
0
0
0
0
.0
0
0
0
0
0.0182
Arsenic
0.0182
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0
0.0133
0
2.1938
0.3767
0.0199
Cadmium0.0133
Chrorniun
0
0
0
Copper
2.1938
Lead
0.3767
0
Mercury
0.0199
0
Molyb-
0.3823
0
0
0
0
0
0
0
0
0
0
0
0.3823
d
0
0
0
0
0
0
0
0
0
0
0.1.163
Nickel
0:1163
0
0
0
0
0
0
0
0
0
0
0
0.0244
Selenium
0.0244
0
0
0
0
0
0
0
0
0
0
0
4.5871
Zinc
4.5871
0
Total
Phos-
107.48
0
0
0
0
0
0
0
0
0
0
0
107.48
11ot1]S
a ...a
,. ...., A_i
+inn
ar ettrtvrviS
tnn in
"I certify, under penalty of law, that tills aocumeut was Pi uPal ` 'u" '••7 _' --r-. "----
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land pplier Date
' See bottom of FSF Form for helpful' instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (512003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Permit #• W00019960 Annual Dry Tons Applied: 44.32
Facility Name: City of Manon
Toua & Tong Khang Cation Exchange Capacity (non 503):
owner: Toua & Tong
Khang Operator:
16 Acres Permitted: 16
'site #: K1
Field #: K1
Acres Utilized:
i
Inches
Apph-
Voli-
Miner-
Ammo-
Ni-
Must Select
Crop 1 or Crop
Totals
o
/o
Dry Tons Per
Residual
Cond
preci p
cation
tila-
ala-
TKN
ma-
trate
PAN 1
PAN 2
2
a�
rReport
Solids
Acre
SourcesPer
(Summarize)
'
Wet
Past 24
Meth-
zation
zation
Ni-
and
Nitrite
Crop 1
Crop 2
Acre
Hrs.
od*
Rate**
Rate
trogen
dry
0
s
0.5
30%
60400
2100
39
103.128
#######
Fescue
1
WWTP.
8-04
279,500
17469
3.81
2.775382594
0
0
2
0
0
�
�
0
0
3
3
0
0
v
0
O
0
�
s �
1'rl
0
0
5
0
0
0
0
E
0
0
M
0
0
i
0
0
-
0
0
f
0
0
0
0
c
0
0
ZZ
0
0
1
0
0
0
0
1
0
0
0
0
1
0
0
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN I
PAN 2
Lime Applied
Cd
Cr
TOTALS:
17469
As
2.19384
0.37672
0.01989
0.38226
0.11634
0.02443
4.58712
107 476
103 128
0
Date
lbs/ac
0.0182266
0.0133
0
Annual lbs/acre
3.2376
0.94874
0.03848
1.48966
0.30714
0.07843
11.4807
Current Cumulative lbs/ac
0.0469266
0.03471
0
Prior -Years Cumulative lbs/ac
0.0287
0.02141
0
1.04376
0.57202
0.01859
1.1074
0.1908
0.054
6.89356
Permitted C. P. L. R.***
36
34
NA
72338
267
15
NA
374
89
2498
Permit PAN Limit lst/2nd Crop
under my direction
or supervision in accordance with a system
"I certify, under penalty of law, that this document was prepared
and evaluated the information submitted. I am aware that there are
designed to assure that qualified
personnel properly gathered
information, including the possibility of fines and imprisonment for knowing violations"
significant penalties for submitting
false
3 loe .3
*Application Method: S - Surface, IN -Injection, INC -Incorporation
1.0
Date
**Volitilization Rate: Surface - 0.5, Iniection/Incorporation -
Signat&e of Land
Applier
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)

a ,t, ANNUAL METALS FIELD LOADING bUN IMAKI V VM
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City Ci of Marion Total Dry Tons Applied (Annual): 29.94
---
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Wayne Ross Owner: Wayne Ross
Acres Used: 12 Acres Permitted: 12 Site #: R2 Field #: R2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
—,1,1 1010 in I Hi 1121 1
or Com-
posite
Date
4/10/04
% Solids
3.81
Arsenic
3.29
Cadmiurn
2.4
Chromium
0
Copper
396
Lead
68
Mercury
3.59
Molyb-
dcnum
69
Nickel
21
Selenium
4.41
Zinc
828
Total
Phos-
19400
Annual
,� S. I �,•.1....
rITIM
"I certify, under penalty oI law, LHUL UU5 UU%,U1.C;JUi ....' E...-r— - - ---- - - - -
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
v-as
Signature of Land plier Date
" See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. 29 94
Owner: Wayne Ross Operator:
Facility Name: City of Marion Permit #: W00019960 Annual Dry Tons Applied:
Wayne Ross Cation Exchange Capacity (non 503):
� 12 Acres Permitted: 12
Cite #• R2 Field #: R2 Acres Utilized:
- S 1 t
5 t"Report
Totals % Tons
o Per
� Solids Acre
Q Acre
5-04 1 188,500
ALS:
2.495692875
0
0
0
0
0
0
0
0
0
0
0
As
0.0164171
Site
Inches Appli-
Residual
Cond.
Precip.
cation
Sources
Dry'
past 24
Meth -
(Summarize)
Wet
'
Hrs.
od*
Voli-
Miner-
tila-
ala-
I KN
zation
zation
Rate**
Rate
�nmo- Ni-
ma- trate
Ni- and
trogen Nitrite
2100 1 39
Cd Cr Cu Pb Hsz Mo Ni Se I Zn P
0.01198 0 1.97604 0.33932 0.01791 0.34431 0.10479 0.02201 4.13172 96.806
84 0 38517 001922 044256 0.12182 0.02201 5.02252
Must e ec
Crop 1 or Crop
'AN 1
PAN 2
2
Crop 1
Crop 2
92.735
#######
Fescue
1
0
0
2
0
0
3
0
0
4
0
0
5
0
0
E
0
0
0
0
f
0
0
c
0
0
1
0 0
1
0 0
1
PAN 1 PAN 2
Lime Applied
92L. 735 0
Date
I lbs/ac 4.
a- aY
fac=/4�
Current Cumulative lbs/ac 0.0164171 0.0.1643 0 2.342
Prior Years Cumulative lbs/ac 0 0.00445 0 0.3668 0.04585 0.0013] 0.09825 0.01703 0 0.8908
Permitted C. P. L. R
*** 36 34 NA 1338 267 15 NA 374 89 2498
2so
Permit PAN Limit I st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
*Application Method: S - Surface, IN - Injection, INC - Incorporation
Sigriatur of Land Applier Date **Volitilization Rate: Surface - 0.5. Iniection/Incorvoration - 1.0
***C.P.L.R: Cumulative Pollutant Loadine Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
4t w # 1 to MFLSF
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF ro
DENR FORM FSF (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: City of Marion Total Dry Tons Applied (Annual): 96
Permit #: WQ0019960 Cation Exchange Capacity (non 503 only):
Operator: Toua & Tong Khang Owner: Toua & Tong Khang
Acres Used: 38 Acres Permitted: 38 Site #: K2 Field #: K2
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
or Com-
posite
Date
4/10/04
% Solids
3.8.1
Arsenic
3.29
Cadmium
2.4
Chromium
0
Copper
396
Lead
68
Mercury
3.59
Molyb-
11111
69
NickelF44
SeleniumZincTotal
Phos-
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
—3
1
4
3
o
� � d
w �
0
2.5
Arsenic
0.0165
0
0
Cadmium
0.012
0
0
hromi _
0
0
0
Copper
1.98
0
0
Lead
0.j
Mercury
0.0
Molyb-
denum
0.3
Nickel
0.0
Selenium
0.00Zinc
4.0Total
Phos-
0
rus
t'
11
��vvv�oo
�000v00000
0 I 0 I 0 I 0 I 0 I 0 I 0 I 0 I 0 I 97
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
? �-IU OS
j L•v3►'till
Date
Signature of Land pplier
LSF Form and the mathematically linked FSF Form
* See bottom of FSF Form for helpful for this MP
ful in
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD
PLACE A N/A IN A BLANK OR BOX WHEN NOT APPLICABLE.
'acility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied:
caner: Toua & Tong Khang Operator: Toua & Tong Khang Cation Exchange Capacity (non 503): —
I{2 Acres Utilized: 38 Acres Permitted:
96
38
to #: K2 Field #:
Select
=: S i
t eust
Inches Appli- Voli- Miner- Ammo- Ni-Ni-
Crop 1 or Crop *
Gal. Totals %
Dry Tons Per,
Cond. nia- trate PAN 1 PAN 2
Residual Preci cation tila- ala-
p TKN 2
3 o Cu.Yd. Per
Report Solids Acre
Sources ' Past 24 Meth- zation zation Ni- and
(Summarize) Wet, ** tro Nitrite Crop I Crop 2
a Totals Acre
* en
Hrs. od Rate Rate g
in Gal•p
moist
0 s 0.5 30% 60400 2100 39 33.324 ####### Fescue 1
5-04 214,500 5644.7 3.81 0.896818855
0 s 0.5 30% 60400 2100 39 60.5891 ####### Fescue 2
8-04 390000 10263 3.81 1.630579737
WWTP dry
0 0 3
0 0
0 0 4
0 0
0 0 -`
0 0
0 0 E
0 0
0 0
0 0
0 0 f
0 0
0 0 c
0 0
0 0 1
0 0
0 0 l
0 0
0 0 l
0 0
Cu Pb H Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied
COTALS: 15908 As
Cd Cr
0 1.98 0.34 0.01795 0.345 0.105 0.02205 4.14 97 93.9131 0 Date lbs/ac
�nnuallbs/acre 0.01645
0 3.4256 0.5916 0.02627 0.7515 O.i7426 0.03905 7.26361 lov'rior
�urrent Cumulative lbs/ac 0.02045
0 1.4456 0.2676 0.00832 0
0.06926 0.7 9g6?ermitted
Years Cumulative lbs/ac 0.004
MO.O12
N4065
1338
C. P. L. R.*** 36
NA 250
?ermit PAN Limit 1 sU2nd Crop
under my direction or supervision in accordance with a system
"I certify, under penalty of law, that this document
was prepared
the information submitted. I am aware that there are
designed to assure that qualified personnel properly gathered and evaluated
the of fines and imprisonment for knowing violations."
significant penalties for submitting false information,
including possibility
lam' �S *Application Method: S - Surface, IN - Injection, INC -Incorporation
- 1.0
Date **Volitilization Rate: Surface - 0.5, Iniection/Incorooration
' her
Signature Land App
***C.P.L.R-: Cumulative Pollutant Loading Rate
Data the Dry Tons Per Acre
are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this 'information needs to be entered
the metals equations. ie. FSF row # 1 to WLSF
**** The RSSF and
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete
DENR FORM FSF (5/2003)

t ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
Facility Name: City of Marion Permit Number:
WWTP Name: City of Marion WWTP NPDES Number:
Monitoring Period: From 1/l/2004 To 12/31/2004
WQ0019960
NCO031879
P h R Auction (40 CFR 503 32) - Please indicate level achieved and alternative performed:
at ogen e
Class A:
Alternative 1 ❑
Alternative 2 ❑
Altern�313Alternative
4❑
Alternative 5 ❑
Altern
If applicable to alternative performed Class A only)indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑ Gamma Ray Pasteurization ❑
Class B:
Alternative IEl
Alternative 2 ❑
Alternative 3 ❑
If applicable to alternative performed Class B only indicate "Process to Si nin _ cant, Reduce Pathogens":
Lime Stabilization ❑ Air Drying Ing ❑ jAerobic Digestion .0
Anaerobic Digestion❑
If applicable to alternative performed Class A or Class B complete the following monit ring data:
mmwauie Pathogen Density Number ot Frequency Sample Analytical
Parameter Level in Excee- of r e "Tech-niqu
im Geo. Mean MaximumUnits denoes Analysis
2x 10to e6th
power NTN per
r78947.4
831694.5
iHHHH49
MPN
0
7
grab
sm9221 b
gram of total
solids or 2 x 10 to
Fecal Coliform
the 6th power
CFU = suam of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
3 MPN per 4
(in lieu of fecal
grams total solid
coliform)
(dry weight) _
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 BSI j6ption 2 ❑ 1 Option 3 ❑ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
* "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction reuirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
Prepar r Name and Title (type or print)
Signature,0 Preparer Date
(Inn,
5 /`t �/rS5�.� 1���
Land Applier ame and Title (if applicable)(type or print)
Signature of d Applier (if applicable) Date
DENR FORM RF (512003)

L
RRIES, INC.
www.parlabs.com
Attn: DENNIS KEY
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cert M 20; SC Cert M 99003
REPORT OF ANALYSES
SOUTHERN SOIL BUILDERS PROJECT NAME: APR 04
958 HOOTS ROAD DATE: 04/28/04
ROARING RIVER, NC 28669-0000
SAMPLE NUMBER- 56121 SAMPLE ID- SSB MARION SAMPLE MATRIX- SO
DATE SAMPLED- 04/07/04 TIME SAMPLED- 1200
DATE RECEIVED- 04/08/04 SAMPLER- ZACH KEY RECEIVED BY- MJ
TIME RECEIVED- 1250 DELIVERED BY- ZACH KEY TYPE SAMPLE- Grab
Page 1 of 3
ANALYSIS
METHOD
DATE
TIME
BY
RESULT
UNITS
ANALYSIS
TCLP CHARACTERISTICS
TCLP
04/14/04
0800
TL
TCLP
04/14/04
0800
TL
6.3
S.U.
pH VALUE
TCLP
04/14/04
0800
TL
< NON
CORROSIVITY
TCLP
04/14/04
0800
TL
< NON
REACTIVITY
TCLP
04/14/04
0800
TL
> 200
degrees F
FLASH POINT
TCLP
04/14/04
0800
TL
< NON
IGNITABILITY
TCLP
04/14/04
0800
TL
< FL
PAINT FILTER TEST
TCLP METALS
TCLP
04/16/04
0954
CT
TCLP
04/16/04
0954
CT
< 0.5
ppm
ARSENIC
TCLP
04/16/04
0954
CT
< 10
ppm
BARIUM
TCLP
04/16/04
0954
CT
< 0.1
ppm
CADMIUM
TCLP
04/16/04
0954
CT
< 0.5
ppm
CHROMIUM
TCLP
04/16/04
0954
CT
< 0.5
ppm
LEAD
TCLP
04/16/04
0954
CT
< 0.02
ppm
MERCURY
TCLP
04/16/04
0954
CT
< 0.1
ppm
SELENIUM
TCLP
04/16/04
0954
CT
< 0.5
ppm
SILVER
TCLP
04/14/04
0800
TL
TCLP PESTICIDES
TCLP
04/14/04
0800
TL
< 0.002
ppm
ENDRIN
TCLP
04/14/04
0800
TL
< 0.04
ppm
LINDANE
TCLP
04/14/04
0800
TL
< 1
ppm
METHOXYCHLOR
TCLP
04/14/04
0800
TL
< 0.05
ppm
TOXAPHENE

I t
ffAR
BORATORIES, INC.
www.parlabs.com
Page 2 of 3
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
Phone: [phone]; Fax: [phone]
NC Cart # 20; SC Cart # 99003
CONTINUATION OF DATA FOR SAMPLE
NUMBER
56121
ANALYSIS
ANALYSIS
METHOD
DATE
TIME
BY
RESULT
UNITS
CHLORDANE
TCLP
04/14/04
0800
TL
< 0.003
ppm
HEPTACHLOR (AND ITS EPDXIDE)
TCLP
04/14/04
0800
TL
< 0.0008
ppm
TCLP HERBICIDES
TCLP
04/14/04
0600
TL
2,4-D
TCLP
04/14/04
0800
TL
< 1
ppm
2,4,5-TP(SILVEX)
TCLP
04/14/04
0800
TL
< 0.1
ppm
TCLP ORGANICS
TCLP
04/14/04
0800
TL
BENZENE
TCLP
04/14/04
0800
TL
< 0.05
ppm
CARBON TETRACHLORIDE
TCLP
04/14/04
0800
TL
< 0.05
ppm
CHLOROBENZENE
TCLP
04/14/04
0800
TL
< 10
ppm
CHLOROFORM
TCLP
04/14/04
0800
TL
< 0.6
ppm
o-CRESOL
TCLP
04/14/04
0800
TL
< 20
ppm
p-CRESOL
TCLP
04/14/04
0800
TL
< 20
ppm
m-CRESOL
TCLP
04/14/04
0800
TL
< 20
ppm
1,4-DICHLOROBENZENE
TCLP
04/14/04
0800
TL
< 0.75
ppm
1,2-DICHLOROETHANE
TCLP
04/14/04
0800
TL
< 0.05
ppm
1,1-DICHLOROETHYLENE
TCLP
04/14/04
0800
TL
< 0.07
ppm
2,4-DINITROTLUENE
TCLP
04/14/04
0800
TL
< 0.013
ppm
HEXACHLOROBENZENE
TCLP
04/14/04
0800
TL
< 0.013
ppm
HEXACHLOROBUTDIENE
TCLP
04/14/04
0800
TL
< 0.05
ppm
HEXACHLOROETHANE
TCLP
04/14/04
0800
TL
< 0.3
ppm
METHYL ETHYL KETONE
TCLP
04/14/04
0800
TL
< 20
ppm
NITROBENZENE
TCLP
04/14/04
0800
TL
< 0.2
ppm
PENTACHLOROPHENOL
TCLP
04/14/04
0800
TL
< 10
ppm
PYRIDINE
TCLP
04/14/04
0800
TL
< 0.5
ppm
TETRACHLORETHYLENE
TCLP
04/14/04
0800
TL
< 0.07
ppm
TRICHLOROETHYLENE
TCLP
04/14/04
0800
TL
< 0.05
ppm
2,4,5-TRICHLOROPHENOL
TCLP
04/14/04
0800
TL
< 40
ppm
2,4,6-TRICHLORPHENOL
TCLP
04/14/04
0800
TL
< 0.2
ppm
VINYL CHLORIDE
TCLP
04/14/04
0800
TL
< 0.02
ppm
//X/
LABORATORY DIRECTOR

u
Pi4R::
LABORATORIES.!INC.
www, par/a s, com
CHAIN -OF.'CUSTODY
PAR Laboratories, Inc
Phone [phone]
Fax (704) .588-8335 .
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina
Department of Environmental and Natural Resources.
- ---- ------
Company Name (billing) COMMENTS/SPECIAL
SOUTHERN SOIL BUILDERS INSTRUCTIONS
Address
958 HOOTS RD
City, State & Zip Code
ROARING RIVER, NC 28669
Point of Contact & Telephone Number
DENNIS KEY 336-957-8909
Sample taken by:
IS THIS FOR STAT or EPA REPORTING? YES XC NO
*Sample type: DW WW _e�C GWMW HW Soll Other
Sample Temp at time of sampling: —?-)_ °C Sample Temp upon receipt: °C
** Preserved: Yes No �_ Teflon Liner/ Zero Headspace: Yes No _ N/A
lient Sample I.D.
(Sample Location / Number)
Comp
Grab
Preserv.
Set Up
Date/Time
Collection
Date/Time
Analyses
Requested
on
0
7,fLl�o s
�
a
i
i
Relinquished by: Date/Time Received by: - Datefrime
71mqutsriW uy.
uatei I Ime Received by:
Date/The
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste —See
Other Side
Z)

CITY OF MARION
CORPENINC CREEK WASTE TREATMENT PLANT LABORATORY
VOLATILE SUSPENDED SOLIDS WORKSHEET
STANDARD METHODS 18TH EDITION -- METHOD #2540E
_ _ c
RUN DATE: /�-= 'U`f TIME IN:
ANALYST: yyti TIME OUT: /S// SZ�
ANALYST: 7 TIME WEIGHED:
VSS FIXED
o A _R R-(-
SAMPLE
DATE
COLLECT
Sample
Vol.
ML
Filter
#
FILTER
WEIGHT
(GRAMS)
FILTER +
Residue before
Ignition, Gr.
FILTER+ ASH
After Ignition
(GRAMS)
ASH +
FILTER
(GRAMS)
ASH
GRAMS
TOTAL
Fixed Solids
MG/L
TOTAL
VSS
MGlL
_
%VSS
TS
, /3saA
133!�
Dz-
p. a37 Z
G, 0°3
. 0087s
L5S
ass
ZZ
��
lJ
cz
z .
/, oZIS'.J�f
b
o31
AL
• /zSS
< / /
DD J1
�
s
. //7
DILUTION
1000000
FACTOR =
ML OF SAMPLE
Mg Volatile Solids / L
= (A - B) X 1000000
Sample Vol., ML-
Mg Fixed Solids / L =
f B - C) X 1000004
Sample Vol., ML.
% Volatile Solids=
Total VSS
Tot. Vss + Tot. Fixed
BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL
BALANCE CAUBRTION BOOK
LOT #'S
GLASS FIBER FILTER:
�3 "2

g6tc 10 04 :.2:Olp CITY OF MRRION Sze 65S IS53 P•1U
VS In 0.81
uS out 0.71
ySFR= 0.425713

t Dmc 10 04 :,2o00p CITY OF MRRION
828 6b9 1y58 P•d
aceAnalytical
www.pace/abs.com
Lab Sample No: 924103864
Client Sample I0: CC SLUDGE #7
Pace Anslyhcal $eN1Ces, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone. [phone]
Fax: [phone]
Lab Project Number: 9264662
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 9264652.002 Date Collected: 04/13/04 11:15
Matrix: Soil Date Received: 04/13/04 16:26
Parameters Results 'nits Rgpprt Limit Analyzed By CAS No. Qu�l_ ReqLmt
Microbiology
Fecal Coliform Mi'N Solid Method: SM 9221B/E
Coliform, Fecal 128,205.12 04/14/04 MMG
Wet Chemistry
Percent Moisture Method: X Moisture
Percent Moisture 96.1 X 04/15/04 14:27 EDF
Total Percent Solids Method: EPA 160.3
Percent Solids 3.9 %
Date: 05/18/04
04/22/04 DHW
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NO Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NO Drinking Water 37712 • �;_�
SC Environmental 99030
Pape 2 of 7
Charlotte Gerification IDs
NC Wastewater 12
NO Drinking Water 37706
sC a4nnF,

• De'c 10 OAF :.1:59a CITY OF MARIOM 626 659 1959 P•
Pace Analytical Services, Inc.
2225 Riverside Drive
1® Asheville, WC 28804
AIr alytica, I Phone:[phone]
www.psceiabs.com Fax: 826,252, 4616
Lab Project Number: 9264662
Client Project ID: CDRPENING CREEK SLUDGE
Solid result, are reported on a.dry weight basis
10385o
1038
924103856
Project Sample
Number: 9264662.001
Date Collectea: u4rleruq 11:17
Lab Sample Nc:
Matrix: Soil
Date Received: 04/13/04 16:26
Client Sample IDc CC #fi
RPtults nU its Reoort Limit
Analyzed
B
CAS No. Qual SELL
Parameters
Microbiology
Fecal Colifc:rm MPN Solid
Method: SM 92218iE
04/14/04
MMG
Coliforn. Fecal
78,947.368
Wet Chemistry
Percent Moisture
Method: X Moisture
04/15/04 14:26
EDF
Percent Moisture
96.2 X
Total Percent Solids
Method: EPA 160.3
04/22/04
0H4i
Percent So' ids
3.8 - 4
Date; 05/18/04
• A�hevii�e Certificat � I
NO Wastewater 40
NO Drinking Water 37712
60 Environmental 99030
•n F �
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except In cull,
without the written consent of Pace Analytical Services, Inc.
Page: 1 of 7
Charlotte Certillcatlon IDs
NC Wastewater 112
NO Drinking Water 37706
SC 99000

.( 'Dec 10 04 :.1:58a CITY OF MRRION 020 659 1959 P•6
;aceAnaVical
/ www.11acelabs.com
Pace Analytical ServICBJ, Inc.
2225 Riverside Drive
Asheville, NO 28804
Phone: [phone]
Fax: 828,252.4616 i
Lab Project Number: 9264215
Client Project ID: CORPENING CREEK SLUDGE
dab sample No: 924030534 Project Sample Number: 9264215.002 Date Collected: 04/07/04 11:10
Matrix: Soil Date Received: 04/07/04 13:30
Client Sample ID: CC SAGE FECAL #5
Results Units art Ltmit Analyze By _CAS No. ual ReoLmt
Pa r aneter s--------
Mficrobiolo9Y
Fecal Coliform MM Solid Method: 5M 92216/E 04/08/04 MMG
Col•,form, Fecal 5625000
Wet Chemistry
Percent Moisture Method: X Moisture 04/12/04 14:30 EDF
Percent Moisture 98.4 %
Total Percent Solids Method: EPA 160.3
Percent Solids
1.6 X 04/12/04 KDF
Peve- 1 of 7
Date: 04/14/04
REPORT Of LABORATORY ANALYSIS
This report shall not be reproduced, except In full,
Charlotte CertflCatlon
IDS
tevilla cartlficatian IDs
the written consent of Pace Analytical Services, Inc.
NC Wastewater
12
Wastewater 40
without
NC Drinking Water
37706
Drinking +Hater 37712
"''
♦ err
$t;
99006
Environmental 99030
��f1'P`,*-.
G� r�Fi ao
FR7F97

• ` `' Be"c 10 04 :.1 :57a CITY OF MFIRION
820 659 1959 P•5
ace Analytical
www.paceiabs.com
I
Solid results are reported on a dry weight basis
Lab Sample No: 924080Zb
Client Sample ID: CC SLUDGE FECAL #4
pace Analytical Services, Me.
W5 Riverside Drive
Asheville, NC 26604
Phone: [phone]
Fox; 828.252.4618
Lab Project Number: 9264215
Client Project 1D: CORPENING CREEK SLUDGE
PrujeLl GaNple Number: 0264216 0a1 Data Colloctad: 06/07/04 11:10
matrix: Soil Date Received: 04/07/04 13:30
nesults Uni o R�y�rl L it ! Amalvred B CAS DIO. �1_ G.9.L4�
Parameters -----
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E 04/08/04 fMG
Coliform, Fecal 230000
Wet Chemistry
Percent Moisture Method: X Moisture
Percent Moisture 99.0 X 04/12/04 14;29 EDF
;ota'. Percent Solids Method: EPA 160.3
Percent Solids 0.9 z
Dace: 04/11/04
9 h� evflle C rt fg Ication iC;.
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
04/12/04 KDF
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1 of 7
charlotte CertfiGatdn IDS
NC Wastewater 12
NC Drinking Water 37706
SC 99006

• 11 {De- 10 04 :.1:56a CITY OF MARION
020 659 1959 P•4
aceAnal icai®
I/ww. pecelabs.com
Pace Analytical Services, lac,
2225 Riverside Drive
Asheville, NC 26804
Phone, 826.254.7176
Fax: [phone]
Lab Project Number:
9264104
.Client Project
ID:
CORFENING CREEK SLUDGE
Lab Sample No: 924075252
Project Sample Number: 9264104.002
Cate Collected: 04/06/04 1::28
Client Sample ID: CC SLUDGE
FECAL 3
Matrix: Soil
Date Received: 04/06/04 14:27
Parametzrs
Results Units
Report Limit Analyzed
BY
CAS No. Qual ReaLmt
Microbiology
Fecal Coliforn MPH Solid
Method: SM 92216/E
Coliform, Fecal
>4324324.3
04/U7/04
MMG
Wet Chemistry
Percent Moisture
Method: X Moisture
Percent Moisture
96..3 S
04l07/04 11:14
DHW
Total Percent Solids
Method: EPA 160.3
Percent Solids
3.7 X
04/07/04
OHk'
Date: 04/12/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification 10s This report shall not be reproduced, except In full,
NO Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712
SC Environmental 99030
Page 2 of 7
Charlot:e Certification i0s
NO Wastewater 12
NC Drinking Water 37706
SC 9.W6

` vec 10 04 ::1:56a CITY OF MRRION
626 659 1959 P•3
I
eAnaVical'
www. paoalabs. com
Solid results are reported on a dry weight basis
Lab 5 :; 924075245
Client Sample 10: CC SLUDGE FECAL 2
Pace Analp1101 Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number; 9264104
Client Project ID: CORPENING CREEK SLUDGE
Project Sample Number: 9264104.001 Date Collected: 04/06/04 11:25
Matrix: Soil Date Received: 04/06/04 14:27
Parameters Resultsilni s Report Limit _ Analyzed By CAS No. Qua' Re4Lrt
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E 04/07/04 KMG
Coliform, Fecal >4444444.4
Wet Chemistry
Percent Moisture Meth96. k Moisture
4 R 04/07/04 11:13
Percent Moisture 96.OHk
Total Percent Solids Method: EPA 160.3
Percent So'ios 3•7 %
Date: 04/12/04
Ashevil:e COrtific•tI n i
NC Wastewater 40
NO Onnking WatEr 37712
cr oannn
04/07/04 DNW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services; Inc.
Page: 1 of 7
Charlotte Ceriilicaiion IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006

• ` ``Ded 10 04 ::1:55a CITY OF MRRION
020 659 1959 P•e.
Pace Analytical S01VIC85, Inc.
2225 Rfv6506 Dr lve
Asheville, NO 28604
e AnalyticalPhone: 828.254.7176
Fax: [phone] f 8
www.pacelabs.com
Lab Project Number: 9264007
Client Project 10; CORPENING CREEK -SLUDGE
Solid results ere reported on a dry weight basis
Project Sample
Number: 9264007.001
Date Collected: 04/05/04 12;38
Lab Sample No: 924069826
Matrix: Soil
Date Received: 04/05/04 13:41
Client Sample 10: CC SLUDGE
FECAL
Results n�- .— Reoort Limit
Analyzed
3Y
CAS No•Qua' Regl.mL
Parameters
Microbiology
Fecal Coliform MPN Solid
Method: SM 92'L16/E
04/05/04
MMG
Colifora., Fecal
1093750
Wet Chemistry
Percent Moisture
Method: X Moisture
04/12/04 10:'s0
EDF
Percent Moisture
96.5 x
Total Percent Solids
Method: EPA 160.3
04/07/04
DHk'
Percent Solids
3 2 X
Page: I or 5
Gate: 04133/04
REPORT OF LABORATORY ANALYSIS
Asheville Certiticatipil lDs This reportshall.not be reproduced, except in full, NC WWasi
S4!>SJCertification i
without the written conaent of Pace Analytical Servicos, Inc. astewater 12
PJC Wastewater 40 NO Drinking Water 37706
NO Drinking Water 37712 °
,� ��. ����,. sc 99006
SC Environmental 99030
u /i11��•�e CI AI[I AD C0700'1

no
icDivisionPhn(99)Copies
0 rp ye�s T3`o`R"NCDA&CGrower Southern Soil Builders, Inc. Gx
958 Hoots Rd
Roaring River, NC 28669
S' J
o Z I�TestRo1jortFarm:
1!7/2005 SERVING N.C. RESIDENTS FOR OVER 60 YEARS Wilkes County C 12,3
Agronomist Comments
_ anon A lied Lune .Recommen Cu Zn B Mn See Note
Field Inform PP.. , dat N P2Os K2O Mg
ions .,�. ..�...: � ._: .
w Lime 0 12
40
Sample No. Last Crop Mo Yr T/A Crop or Year 0 120-200 50-70 0 0 0 0 .0
1st Crop: Fes/OG/Iim,M
06
2nd Crop:
Test Results
Soil Class HM% W/V CEC BS% Ac pH P-I K I Ca% MNa
g'/6 M38 Mn-AI(1)Mn-AI(2) 292 Zn Cu 266 51 SS -I NO3 N¢ A' 0.1
MIN 0.81 1.05 17.9 96.0 0.8 6.4 33 108 80.0 13� -
0 _ c f ti
,."ti.. e_."-,"x;•_+'".aLi .. .e-:. .>...- , , �",a�•tea- '�"..ms;.:`Crs. �''"w`r,.r'
«. 4 ?�PP1t�dZini ; IZeco ."- _
Psnd<Lt1Q usa A `� `
tiou Lime N P2O5 K2O Mg Cu Zn B Mn See Not
Sample No. Last Crop Mo Yr T/A Crop or Year AT 180-220 0 20-40 0 0 0 .0 0 3
K2 12 2003 1.0 1st Crop: Corn,Silage
2nd Crop:
Test Results Zn-1 Zn-AI Cu-I S-I SS -I NO3-N NH4-N Na
Soil Class HM% W/V CEC BS% Ac pH P-I KI Ca% Mg•.6 Mn-I Mn-AI(1)Mn-AI(2) 300 300 168 71 0.1
MIN 0.97
1.09 13.7 90.0 1.4 5-8 149 91 73.0 13.0 337 219

Division 4300 Reedy Creek Road
3,-
s� oil est.
10/13/04 SERVING N.C. CITIZENS FOR OVER
Agronomist Comments:
h, NC 27607-6465 [phone]
Grower- Southern Soil Builde
958 Hoots Rd
Roaring River, NC 28669
Ro ort
� Farm.
WARS Wilkes County
Inc. Copies to:
No: 06860
C -- 12,$1
rxclu,iiu illla�ivii
Sample No. Last Crop
o
aauu Jpxxxz.
Yr T/A Crop or Year
Lime
N PlOs h0
Mg Cu
Zn
B
Mn
See Note
•fir
1st Crop: Fes/OG/rim,M
0
120-200 0 70-90
0 0
0
pH$
12
2nd Crop:
Test Results
Soil Class HM% W/V
CEC
BS%
Ac pH P-I K-I
Ca%
Mg%
Mn-I Mn-AI (1) Mn-AI (2) Zn-1
Zn-AI
Cu-I
S-I
SS -I
NO3-N NIh-N Na
MIN 0.41 1.06
13.2
7.0
0.4 6. 106 31
80.0
16.0
371 226 536
536
501
4
0.2
Field4Informatlon:.. ,
: AP
Recommendatiions
'.
KO
Mg Cu
Zn
B
Mn
See Note
Sample No. Last Crop
Mo
Yr T/A
Crop or Year
Lime
N` Pa05
1st Crop: Fes/OG/rim,M
0
120-200 0 0
0 0
0
pH$
12
2nd Crop:
Test Results
Soil Class HM% W/V
CEC
BS%
Ac pH P-I K I
Ca%
Mg%
Mn-I Mn-AI (1) Mn-AI (2) Zn-1
Zn-AI
Cu-I
S-I
SS -I
NO3-N AH-N Na
MIN 0.6 0.98
16.2
95.0
0.8 6.5 81 127
67.0
24.0
209 135 677
677
642
62
0.1
;Field Informatiot<; _:
lied Lime Recommendations
R05 h0
Mg Cu
Zn
B
Mn
See Note
Sample No. Last Crop
o
Yr T/A
Crop or Year
Lime
N
K1
1st Crop: Fes/OG/rim,M
0
120-200 0 30-50
0 0
0
0
12
2nd Crop:
Test Results
Soil Class HM% W/V
CEC
BS%
Ac pH P-I K-I
Ca%
Mg%
Mn-I Mn-AI (1) Mn-AI (2) Zn-1
Zn-AI
Cu-I
S-I
SS -I
NQ3-N AIB N Na
MIN 0.46 1.07
12.0
88.0
1.4 6.1 85 52
69.0
17.0
399 255 331
331
156
51
0.1
Field Information
Appliedlime
Recommendations
P205 h0
Mg Cu
Zn
B
Mn
`
See Note
Sample No. Last Crop
Mo
Yr T/A
Crop or Year
Lime
N
V6'tw
1st Crop: Fes/OG/rini,M
0
120-200 0 0
0 0
0
pH$
12
2nd Crop:
Test Results
Soil Class HM% W/V
CEC
BS%
Ac pH P-1 K-1
Ca%
Mg%
Mn-1 Mn-AI (1) Mn-AI (2) Zn-1
T,n-AI
Cu-1
S-1
SS -I
NO3-N NIA-N Na
MIN 0.76 1.00
19.3
97.0
0.5 6.9 130 106
81.0
14.0
382 233 773
773
959
59
0.1

a AT7/./.r
NCDA&CS'Agronomic Division Phone: [phone] Web Site: www.ncagr.com/agronomy
Grower: Southern Soil Builders, Inc-
1WFUL < 11V- lJz-I�
(.Dies "1•6:
•
xt�
9" hoots Rd
Roaring Rkr, NC 28669
.a
ozl
esto rt
Re
�
Farm:
12/8/2004
SERVING N.C. RESIDENTS FOR OVER 60 YEARS
Wilkes County
Agronomist Comments
C 12
-Field Information :;
. �Appli7!2ndCrop:
endations
-
NN
~Sample No. Last Crop Mo
Nis
Year Lime
Fes/OG/rim,M 1.1T
P205 K2
120-200 0 10-30
Mg Cu
0 0
Zn
0
B Mn See Note
.0 0 12
Test Results
Soil Class HM%
MIN 0.81
Feldlnformation
W/V CEC BS%
1.10 6.7 70.0
A hed.hime
Ac pH P-I K-I Ca% Mg%
2.0 5.2 166 62 52.0 13.0
Recommendations.:_
Mn-I Mn-AI(1)Mn-AI(2) Zn-I Zn-AI
121 90 850 850
h.
_202_..: __
Cu-I
1051
S-I SS-1 NO3-N NH4-N Na
63 0.1
„ PP
Sample No. Last Crop Mo Yr T/A
Crop or Year Lime
Ist Crop: Fes/OG/rim,M 0
N P205 K2
120-200 0 10-30
Mg Cu
0 0
Zn
0
B Mn See Note
.0 0 12
2nd Crop:
Test Results
Soil Class HM%
MIN 0.71
W/V CEC BS%
1.14 1o.4 90.0
Ac pH P-1 KI Ca% Mg%
1.0 6.1 277 64 69.0 19.0
Mn-I Mn-AI(1)Mn-AI(2) Zn-I
105 78 595
Zn-AI
595
Cu-I
477
S-1 SS -I NO3-N NH4-N Na
63 0.1
Field Information
Applied Lime
Recommendations
Sample No. Last Crop
R2
Mo Yr T/A
Crop or Year Lime
1st Crop: Fes/OG/rim,M .3T
N P205 K2
120-200 0 0
Mg Cu
0 0
Zn
0
B Mn See Note
.0 0 12
2nd Crop:
Test Results
Soil Class HM%
MIN 0.71
W/V CEC BS•0
1.11 10.1 87.0
Ac pH P-1 K-I Ca% Mg%
1.3 5.8 146 121 58.0 23.0
Mn-1 Mn-A1(1)Mn-AI(2) Zn-1
422 270 168
Zn-AI
168
Cu-1
98
S-1 SS-1 NO3-N NH4-N Na
67 0.1
:Field°:Information..
::
Applied1ime
Recommendations
Sample No. Last Crop
ap"
Mo Yr T/A
Crop or Year Lime
1st Crop: Fes/OG/rim,M .6"r
N P205 K20
120-200 U 0-20
Mg Cu
0 0
Zn
0
B Mn See Note
.0 0 12
2nd Crop:
Test Results
Soil Class IIM%
MIN 0.81
W/V CEC BS%
1.06 6.9 77.0
Ac pH P-1 K-1 Ca% Mg%
1.6 5.6 84 71 6o.o I2.o
Mn-1 Mn-AI(1) Mn-AI(2) Zn-1
152 108 144
Zn-AI
144
Cu-1
284
S-1 SS-1 NO3-N NH•s-N Na
53 0.1

A&L EASTERN AGRICULTURAL LABORATORIES, INC.
7621 Whitepine Road • Richmond, Virginia 23237 - [phone]
Fax No. (804) 271-644
REPORT NUMBER: I�C�94-22 ACCOUNT # 46 381 Ai�E ].
SOUTHERN SOIL BUILDERS MARION DENNIS KEY
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER NC 2SG69
LAO NUMBER = 41337
SAMPLE ID = MARION
RESULT RESULT
PARAMETER ( Z ) (MG/KG)
EMAIL
NC CERT #257
ANALYSIS REPORT
DATE SAMPLES` 04/10/04
GATE RECEIVED 04/14/04
DATE REPORTED 04/16/04
DETECTION
LIMIT ANALYSIS
(MG/KG) ANALYST DATE TIME METHOD REFERENCE
SOLIDS(AS IS)
3.81
38100
160
JCS:
04/14/04
16:00
SM
2540 G
NITROGEN(TKN)
6.04
60400
100
KCS
04/15/04
15:45
EPA
351-3
PHOSPHORUS
1.34
19400
100
JCM
04/15/04
1G:00
SW
846—E010B
POTASSIUM
0.35
3500
100
JUM
04/15/04
16:00
S#
846—GOIGB
0,85
8500
100
JCm
04/15/04
16:00
SH
04G—G010B
SULFUR,
1.20
12 000
100
_1EM
04/15/04
1G:00
SW
8e6—GOIOB
CALCIUM
0.30
3000
100
JCM
04/15/04
16:00
SW
846—GOIOB
MABNESIUM
0.11
1100
100
JCM
0.4115104
16:00
SW
846—GOIOB
SODIUM
-
=1000
1
JCM
04/15/04
1G:00
Sid
946•—GOIOB
IRON
Y
1.0
JCM
04/15/04
16:00
SSE
84G—G010B
ALUMINUM23000
Lot
1
JCM
04/15/04
1G:00
SW
846-60i0B
MANGANESE
39G
1
JCS:
04/15/04
16:00
SW
846-6010B
COPPER
828
1
JCM
04/15/04
16:00
SW
84G-6.010B
ZINC
AMMONIA —NITROGEN
0.21
2100
• 100
KCS
04/15/04
12:00
EPA
350.2
39
10
KCS
04/15/04
14:20
SM
4500—NO3 F
NO3—NO2 NITROGEN
2.4
1
JEM
04/15/04
16:00
Sw
846-6010B
CADMIUM
1
5
jCM.
04/15/04
16:00
Sw
846-6010B
NICKEL
68
5
JCM
04/15/04
16:00
SN
846—GOIOB
L E A ED
_
ALL VALUES ARE ON A DRY WEIGHT BASIS EXCEPT AS NOTED.
This report applies only to the sample(s) tested. Samples are retained a maximum of thirty days after testing.
A&L EASTERN AGRICULTURAL LABORATORIES, INC.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part,
nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public
announcements without obtaining our prior written authorization. Copyright 1977 by ��—� _ •N-� byI Paul Chu

A&L EASTERN AGRICULTURAL
LABORATORIES, INC. ',
•
7621 Whitepine Road •Richmond, Virginia 23237 • [phone]
D
Fax No. [phone]
REPORT NUMBER: R094-221
ACCOUNT # 4 G 3 8 1
PAGE
EMAIL
SOUTHERN SOIL BUSLDERS
MARION
DENNIS KEY
DENNIS KEY
958 HOOTS ROAD
ROARING RIVER NC 28b-69
NC CERT #257
ANALYSIS REPORT
DATE SAMPLED 04/10/0
LAB NUMBER = 41337
DATE RECEIVED 04/14/04
SAMPLE ID = MAR ION
DATE REPORTED 04/16/04
DETECTION
RESULT RESULT
LIMIT ANALYSIS
PARAMETER
--------------------
( X ) (Mo/KG)
---------------
'%MG/KG) ANALYST DATE TIME
----------------------- -----
METHOD REFERENCE
------------------------
ARSENIC
3.29
0.2 KMM 04/15/04 15:00
SH 84G-7061A
MERCURY
3.59
0.2 KMM 04/15/04 15:00
SH 846-7471A
SELEINIUM
4.41
0.1 KMM 04/15/04 15:00
SW 846-7741A
PH (STD.UNITS,AS IS)
6.80
RD 04/15/04 12:30
EPA 150.1
ORGANIC NITROGEN
5.83 58300
100 DCH 04/15/04
CALCULATION
MOLYBDENUM
69
5 JCM 04/15/04 16:00
SW 846-6010B
ALL VALUES ARE ON A DRY WEIGHT BASIS EXCEPT AS NOTED.
This report applies only to the sample(s) tested. Samples are retained a maximum of thirty days after testing
A&L EASTERN AGRICULTURAL LABORATORIES. INC.
Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or in part. /� ^ ��
nor may any reference be made to the work. the results. or the company in any advertising. news release. or other public \\ Vl /1� .�
wnnnunnnmanta without ohtaininn —r nrinr....:ne...,...'....:__.:__ r.__..__u .n-r-� � •

--
CHAI N OF
SAMPLING LOG # A & L EASTERN AGRICULTURAL LABS, 1HC RECORD AND ANALYSIS
®g 7621. whitepine Road RECORD
U Richmond, VA 23237
tUSTOMER Jov���,._y j o � ��,,, � 804/743-9401 FAX: [phone]
i'
T I attest that the proper field sampling
PROJECT MANAGER:procedures were used during the col-
lection of these samples_
Phone: �27/i S Z_S(�j 4 7
SZ?ER
HEW
SNPLING SAWLE TYPE # OF DATE I � PRESERVED S11IPPED
A & L -LAB # �� OOtiTAINERS
SPMIPIE I.0_ LOCATION
3:
13 3 f
Gc lan
ime Received by: lCS_
Relinquished by Saapler: J� l�1�la;vH. /a.00 hb30
Time Receivp�d by:- �LD
Relinquished by
me ReceWed by:
ReTngiiistied by:
SRECI.L INSTRUCTIONS:
ANALYSIS REQUEST Se Volatile MD Cl
�ANPLE
_Y4=xp SL1 SL2 NH'4-N NO3-N Organic - Cd (' Ni As e0_ Solids
N
M Aa "Of
'SL1: Total Soli (NbisUre),Total KJeldahl Nitrog, Phosphor"s, nPatassiun
aid Zinc
url Sodium Iron, Alutrirxm. Mangan. Cover.
512: Basic Test Al plus Sulfur, Calcium, ►iagies-
i

of I4rrm 0jq oo W 0
Annual Report Review SOP al OOq
1. Annual Land Application Certification Form
• Was a certification form submitted?p S
• Was land application conducted during the reported year? YES
• How many dry tons and dry tons per acre were applied? 170- Q to a • 58 dT 0 �
• Were the applications within the permitted amount?/e5
• Verify PAN if more than 10 tons/acre /vi4
• Did it indicate compliance? yt5
• Was it signed by the appropriate people?ye,5
2. Monitoring
• Were the analyses conducted at the required frequency?y�&S
• Were the metals analyses reported on the Residual Sampling Summary Form?ye-3
• Were the results reported in mg/kg? y e5
• . Were the heavy metals within ceiling concentration permit limits?*yZ.3 Ma 11bdmu,,-, al/f,,5 close- -69 cer1.3=
• If no, were the lab analyses attached? 7S
• Were all the required parameters tested? y4,-S
• Was TCLP analysis conducted? yes
3. Field Summary
• Were the land application events recorded on the Field Summary Forms?ye,s
• Was a Field Summary Form submitted for each field?YZ5
• Were all the residuals applied to permitted land?yiO
• Were all the residuals applied from permitted sources? yC5
• Were the field loading rates for each metal and PAN calculated (year to date)?. 'Of
• Were the cumulative pollutant loading rates calculated? yey
• Were the calculations correct? y.,_5
• Were the PAN loading rates within permit limits?Y&S
• Were the heavy metal cumulative pollutant loading rates within permit limits?y ai
• Were the residuals applied on a suitable crop? y4a
• Were the applications conducted during the crop's growing season?y ,S
• Were the Field Summary Forms complete? a
4. Pathogen and Vector Attraction Reduction
• Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? je,S
• Did the form indicate the period of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction reduction option used?Y.65
• Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? '?
• Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? > valu-4S �0f some-
lts cv,alcjS&S -MO Lv43 f-o
5. Soil Tests vi"a co�Y4p a—
• Was a Standard Soil Fertility Analysis conducted for each application field? y.e,s
• Were the soil pH's 6.0 or greater for each application field? Ka=Si-G K1=0 � R-1v S -���ed (zl�.
• Were the copper and zinc indexes in the soil less than 3000 forIch application field?res
41
6. General
• Was the report in the proper format? yvs
• Were any parts of the annual report missing?r/o
• Was the report submitted on time? Ic-5
* Any violations of ceiling concentrations should be reported to Pretreatment for municipalities only

9,a/ e /� Coj)�,I, - T�,- in,446,d
9,2aAy mg,,b-&,4 F"Aler_Feca(
f a .11 -9 r- fa / Co%XIS felm¢�,ii+-AO-7 Tcc 1,�, t� cc 7,1,6, .44�,- - V pie S c�.��r�%-� � Co.o �a�eA

a
0. 7/
sw�:/

rPM/= o°�CC�6,�ip0_ ��a�Jt 39� a/fla
0
30 % \\
° 1�/y90 -F t3Y
P��) =/$.) 5 7� /b�
$ 7 69 X oa z= �7 /S�" lb�DeT X 177,r3.3
! i Q G
o�b sa l,ds = 3, 1 As = 3 a q ^^� lk�5
x .0�2= 0. (go 6 �� X �.77 0•0/72-
Or /l /�