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WQ0019960_Annual Report_20040218
CITY OF MARION, NC 2003 ANNUAL REPORT LAND APPLICATION PROGRAM NC PERMIT NO. WQ0019960 D FEB 2 4 t09 WATER QUALITY SECTION ! ���1�2p04 ANNUAL LAND APPLICATION CEIt'1 WIC:A4ION hUKlvt A Permit#: WQ0019960 County: f'-acilit-v Name (as shown on permit): Land .Application Operator: McDowell Southern Soil Builders, Inc. Year: 2003 City of Marion Phone 336 957 8909 Land application of residual solids as allowed by the permit occurred during the past calender year? 'Z Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A: Total number of application fields in permit: 1 6 Total number of fields land application occurred during the year-F 5 Total amount of dry tons applied during the year for all application sites: 53.34 Total number of acres land application occurred during the year:1 94 Part B: Facility was compliant during calendar year 2003 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. Ca Yes ❑ No I f'no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1. Unl\ residuals approved for this permit were applied to the permitted sites. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3..Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4.:\nnual TCLP analysis was performed and three (3) copies of certified laboratory results are attached. 5..All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. o Hie facility did not exceed any of the Pollutant Concentration Limits in Table I of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). s.:\11 operations and maintenance requirements in the permit were complied with or, in the case of a deviation. prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 11. No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13..All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true. accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." ::: .� ��- Mil naty,, r o Permittee Name and Title (type or print) a afore of Perm' e Date i�unature of Preparer* Date Signiture of La' d Applier Date ii' different from Permittee) (if different from Permittee and Preparer) . Preparer is defined in 40 CFR Part 503.9 (r) DENR FORM ACF (5/2003) r ANNUAL RFSIDUAL SAMPI.IN(: SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this forrn. Permit Number: WQ0019960 Laboratory: 1) Pace Analytical Facility Name: NPDES # or WQ#: WWTP Name: City of Marion 2) NC0031879 3) City of Marion WWTP 4) 5) Residual Anat sis liara Sample or Composite Date 2-07-03 Percent Solids 1 Arsenic ND Cadmium 3.4 Chromium NA Ito Copper 280 �d Lead 35 g Mercury 1 y Molybdenum 75 13 Nickel Selenium ND Zinc 680 Total Phosphorus 170000 TKN 166000 Ammonia -Nitrogen 662 Nitrate and Nitrite 1 84 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." signalurc O PrcParcr Dmc f)ENR FORM RSSF (5/2003) ANNUAL Mt IALJ VILLI) LUAVIINU OUIVI AA1 rv,.171 4 Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report "Facility Name: Permit #: Operator: Acres Used: City of Marion Total Dry Tons Applied (Annual): 19.5 WQ0019960 Cation Exchange Capacity (non 503 only): Toua & Tong Khang Owner: Toua & Tong Khang 38 Acres Permitted: 38 Site #: K2 Field #: K2 Racidvini Analvcic Data (Heavy Metals and Total Phosphorus use mgfkp,, % Solids use Raw Percent #): Sample or Com- posite Date 1 1 2/7/03 _2j 3j 5j jj 7 ji 9 10 11 12 % Solids I Arsenic 0 Cadmium 3.4 Chromium 0 Copper 280 Lead 35 \1ercurn I Molyb- denum 75 Nickel 13 Selenium 0 Zinc 680 Total Phos- horus 170000 A n n nal Heavy Metal Field Loadings (Calculated in lbs/acre): milli �o000ov�00ov00 � 00000000000 �000 � 000000000 0000�000��0 ;, ... a000000■�000 . , . . "I certify, under penalty of law, that this document was prepared under my direction or supervision to accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" >u 30-rn.l Signature of�Lanc'Applier Date See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 19.5 )wner: Toua & Tong Khang Operator: Toua & Tong Khang Cation Exchange Capacity (non 503): ,ite #: K2 Field #: K2 Acres Utilized: 38 Acres Permitted: 38 o S ecift Totals Per Acre o /o Solids Dry Tons Per Acre Residual Sources (Summarize) 1 e Cond. Dry, Wet, Moist Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Voli- tila- zation Rate** Miner- ala- zation Rate TKN Ammo- nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Cro 1 or Crop Crop p p 2 dal Cu.Yd. .. Report Totals In Gal. Crop 1 Crop 2 {-2003 468,000 12316 1 0.513568421 WWTP Dry 0 s 0.5 30% 166000 662 84 51.3737 ####### corn 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 — ,, — ---_ 10 i "C\ 0 0 0 0 'OTALS: 12316<;<;:;' As Cd Cr Cu Pb H" Mo Ni Se Zn �nnuallbs/acre 0 0.00347 0 0.2856 0.0357 0.00102 0.0765 0.01326 0 0.6936 .urrent Cumulative Ibs/ac 0.004 0.00947 0 1.4456 0.2516 10.00832 1 0.4065 10.06926 0.017 3.0636 'rior Years Cumulative lbs/ac 0.004 0.006 NA 1.16 0.2159 0.0073 0.33 0.056 0.017 2.37 'ernutted C. P. L. R.*** 36 34 NA 1338 267 15 NA 374 89 2498 'ernut PAN Lmut 1st/2nd Crop (j I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance 21 lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am awat! V ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knows i Cj1 12 4,ki"U3 3� � y *Application Method: S - Surfa Si re of Land Applier Date **Volitilization Rate: Surface - C' ^ ***C.P.L.R.: Cumulative Pollul �` *** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically ------ into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 fo MFLsr DENR FORM FSF (5/2003) ANNUAL METALS HEL11 LOAL11NU aUMMAA1 rvnivi Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: City of Marion Total Dry Tons Applied (Annual): 12.7 Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Toua & Tong Khang Owner: Toua & Tong Khang Acres Used: 16 Acres Permitted: 16 Site #: KI Field #: K1 Vs --!-I —I A..-i—:. n..t., tun.. MPtale and Tntnl Phnsnhorus use me/kt=_, % Solids use Raw Percent #): -- . m o©© o© o 0 0 o m �0000�0000�v0� :. � � • � o00000000ao � • . . l ,. .. ... . . "I certify, under penalty of law, that tilts clocumeni was preparvu uuucl wy u.I%,%.kIV— ,,.r. • . accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Lan Applier Date See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE. MAKE A COPY OF THIS BLANK FORM TO BF: COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE: A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Permit #: WQ0019960 Annual Dry Tons Applied: 12•7 Operator: Toua &Tong Khang Cation Exchange Capacity (non 503): )wner: Toua & Tong Khang v t FiPlrii #- K 1 Acres Utilized: 16 Acres Permitted: uic D Tons Per Dry Acre Residual Sources (Summarize) t e Cond. Dry, Wet, Inches Precip. Past 24 Hrs. Appli- cation Meth- od* Voli- tila- zation Rate** Miner- ala- nation Rate TKN Ammo- nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop I or Crop 2 ca o a S cith- Totals Per AcreMoist % Solids Gal. Cu.Yd. Report Totals to Gal. Crop 1 Crop 2 0.796209375 WWTP Dry 0 s 0.5 30% 166000 662 84 79.6471 ####### fescue 1 2 7-2003 305,500 19094 1 0 0 0 0 0 0 0 0 3 4 0 0 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 1 0 0 0 0 11 0 0 Cd Cr 0.00541 0 Cu 0.44576 Pb 0.05572 Hig 0.00159 Mo 0.1194 Ni 0.0207 Se 0 Zn 1.08256 P 270.64 0 PAN 1 79.6471 0 PAN 2 0 Lune Applied Date lbs/ac 12 0 0 TOTALS: T90941 As knnuallbs/acre 0 0.02141 0.016 34 0 0 NA 1.04376 0.598 1338 0.57202 0.5163 267 0.01859 0.017 15 1.1074 0.988 NA 0.1908 0.1701 374 0.054 0.054 89 6.89356 5.811 2498 250 furrent Cumulati�-e lbs/ac 0.0287 0.0287 36 ?rior Years Cumulati� e lbs/ac Perinitted C. P. L. R.*** 'C1lllll rtll� LlllLl IJUuIu �.i v�. -- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." /' 3C• -�'/ *Application Method: S - Surface, IN - Injection, INC - Incorporation l lvLlrtr Sign re of land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** 'rhe RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFI-SF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row N 1 to MFLSF DENR FORM FSF (5/2003) ANNUAL METALS FIELD LOAD11Vl. 6WVhV1AjK1 rUniri Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report `Facility Name: City of Marion Total Dry Tons Applied (Annual): 7.86. Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Voua Yang Owner: Voua Yang Acres Used: 12 Acres Permitted: 12 Site #: Y1 Field #: Y1 Qo�i.i,�ai A.,ni.,��� nary lHpaw Metalc and Total PhosDhorus use mg/kg, % Solids use Raw Percent #): I Fi 1 Calculated in lbetnilre a © © o-ream . �o0�v00ovOv �000�000000000 • 0 � o0v0�OVOvRM ;. ' '' 00000000000 • . s 000000 � 0�00 �0�000000��000 Total Phos- .. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Signature of Land Afplier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) It ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE. MAKE A COPY OFTHIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR 13OX WHEN NOT APPLICABLE. Facility Name: City of Marion Permit #: WC)0019960 Annual Dry Tons Applied: 7.86 Jwner: Voua Yang Operator: Voua Yang Cation Exchange Capacity (non 503): iite. H. Y I Field #: Y I Acres Utilized: 12 Acres Permitted: 12 S.etih t e Inches Appli- Voli- Miner- Ammo- Ni- Must Select Coal. o r�6 Totals o �o D Tons Per Dry Residual Cond. Precip. cation tila- ala- nia- trate PAN I PAN 2 Crop 1 or Crop 0.) o ca � CuNd. Per Solids Acre Sources (Summarize) Dry, Past 24 Meth- nation nation TKN Ni- and 2 Report � Totals Acre WetHrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 ill Gal. Moist 3-2003 188,500 15708 1 0.6550375 W WTP Dry 0 s 0.5 30% 166000 662 84 65.5252 ####9#9 fescue t 0 0 0 0 2- 0 0 0 0 3 0 0 0 0 4 0 0 0 0 15 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 1 0 0 0 0 11 0 0 0 0 12 ['OTALS: 1157081 As Cd Cr Cu Pb H- Mo N1 Se Zn -- nn-N-I. PAN JLirne Applied 0.89081 0.89081 'j � 0 1 - 2498� 4:ZS �t- Z annual lbs/acre 0 0.00445 0 0.3668 0.04585 0.00131 0.09825 0.01703 0 urrent Cumulative Ibs/ac 0 0.00445 0 0.3668 0.04585 0.00131 0.09825 0.01703 0 'rior Years Cumulative Ibs/ac 0 0 0 1 0 0 0 0 0 0 'ertnitted C. P. L. R.*** 36 34 NA 1 1338 267 15 NA 374 89 lerniit PAN Lunit 1st/211d Carp I i- 'I certify, under penalty of law, that this document was prepared under my direction or supervision in accordant 7 lesigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am ay ignificant penalties for submitting false information, including the possibility of fines and imprisonment for kno'• / - 3 U -, `( *Application Method: S - St Sig6ture of Land Applier Date **Volitilization Rate: Surfal ***C.P.L_R.: Cumulative PJ **+ The RSSF Data and the Dry "Pons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathemati( into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete 03) J ANNUAL ML IALJ kILLI) LUAVIIN • JUlvlivlttAl r..ixi.l Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report }:acility Name: City of Marion Total Dry Tons Applied (Annual): 5.42 Permit #: WQ0019960 Cation Exchange Capacity (non 503 only): Operator: Wayne Ross Owner: Wayne Ross Acres Used: 16 Acres Permitted: 16 Site#: Rl Field #: R1 D..M—I A naluc:e data (Npaw Metals and Total Phosnhorus use mi/ks, % Solids use Raw Percent #): • . Phos- phoruslMENEENEENE00- Annual Heave Metal Field Loadings (Calculated in lbs/acre): �v00�000ov�000 � 000000000ov '�'o0v0000�000ov � - • � 00000ov0000 � o0v00000000 • ; . , .. a0000000000 .. , . . . . ho . . I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" 6L Signature of LA Applier Date See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICA HON FIELD SUMMARY FORM I"LEASE MAKE A C0PY OF'fHIS BLANK FORM TO BE ('OMI'Ll"TED AND SUBMITTFID FOR FACII APPLICATION FIELD. PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: City of Marion Permit ti: WQ0019960 Annual Dry Tons Applied: 5.42 Owner: Wayne Ross Operator: Wayne Ross Cation Exchange Capacity (non 503): Site #: R 1 Field #: R 1 Acres Utilized: 16 Acres Permitted: 16 S _ cite I e Inches Appli- Vol*- Miner- Ammo- Ni- Must Select .. c:�;,l. Totals Residual Cond. Crop I or Crop 0 c Cu l- % Dry Tons Per PrecIp. cation tila- ala- T.KN nia- trate PAN 1 PAN 2 2 o Per Sources Dry, c Report Solids Acre (Summarize) Wei Past 24 Meth- zation zation Ni- and Q Totals Acre Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gal. Moist I 3-2003 130,000 8125 1 0.3388125 WWTP Dry 0 s 0.5 30% 166000 662 84 33.8924 ###9### fescue 1 0 0 0 0 2 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 0 0 6 0 0 0 0 7 0 0 -- __ 0 0 8 +� 0 0 5 0 0 0 0 0 0 1' 0 1 0 0 0 0 � 1 7i As Cd Cr Cu Pb Hey N ' 4 2 Lime Applied TOTALS: 81-- Aruivallbs/acre 0 0.00231 0 0.18984 0.02373 0.00068 O.0 �� Date Ibs/ac Current Cumulative Ibs/ac 0.0248 0.01891 0 3.11984 0.551.73 0.01848 1. Prior Years Cumulative lbs/ac 0.0248 0.0166 0 2.93 0.528 0.0178 Permitted C. P. L. R.*** 36 34 NA 1338 267 15 (`„1 Permit PAN L*nut 1 st/211d Crop "I certify, under penalty of law, that this document was prepared under my directi ^ (� designed to assure that qualified personnel properly gathered and evaluated the it significant penalties for submitting false information, including the possibility of f S* �tureof Land Applier Date +*** The RSSF Data and the Drn Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are ma—_ t ` into the same numbered column on the N1FI.SF as is entered on the identically numbered FSF roµ to properly completc `ttie Pion, INC - Incorporation /Incorporation - 1.0 Rate ,information needs to be entered ins. ic. FSF row H F to MFLSF DFNR FORM FSF (5/200:- ANNUAL METALS YIELD LUADI1NU JUIVINIAKY CVKM Facility Name: Permit #: Operator: Acres Used: a Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report City of Marion Total Dry Tons Applied (Annual): 7.86 WQ0019960 Cation Exchange Capacity (non 503 only): Wayne Ross Owner: Wayne Ross 12 Acres Permitted: 12 Site #: R2 Field #: R2 1 Tntol Phnenhnrnc nw. mP/kg. % Solids use Raw Percent #): —Total Phos- phorus 1. � ������� 1 1 1 1 1 •71W' IIIY11 II 0��� L'iyiyWlW1��000��� ••. 1 1 1 1 1 1 1 1 1 1 1 "I certify, under penalty of law, that is document wasN� accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information W*mitted. I gm aware tbpt there are significant penalties for submitting false information, including tV possibility of fines and.4iprisonment for knowing violations" Signature of Land plier Date * See bottom of FSF Form for helpttimtructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2QQ3) J ANNIIAI. LAND AI'1'1,1('A'I'ION FIELD SUMMARY FORM PLEASE; MAKE: A t'011" OF THIS BLANK FORM TO BF, COMPIA "l'l:D AND 51113MITTED FOR F:ACII APPLICATION FIELD. .� PLACE A "N/A" IN A BLANK OR 13OX WHEN NOT APPLICABLE. -acility Name: City of Marion Permit #: WQ0019960 Annual Dry "Tons Applied: 7.86 )wner: Wayne Ross Operator: Wayne Ross Cation Exchange Capacity (non 503): ite #: R2 Field #: R2 Acres Utilized: 12 Acres Permitted: 12 S �ecih )Ite Inches Appli- Voli- Miner- Ammo- Ni- Must Select 5 '� Totals % D Tons Per '� Residual Cond. Precip. cation tila- ala- TKN nia- trate PAN 1 PAN 2 Crop I or Crop Gal. 1) r~ 0 CL1.Yd. Per Solids Acre Sources (Summarize) Dry, Past 24 Meth- zation zation Ni- and 2 Report Totals AcreHrs. Wet, od* Rate** Rate trogen Nitrite Crop 1 Crop 2 in Gat. 15708 1 0.6550375 WWTP Dry 0 s 0.5 30% 166000 662 84 65.5252 4###### fescue 1 -2003 188,500 0 0 0 0 2 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 1 0 110 0 0 0 11 0 0 0 As Cd Cr Cu Pb Ho Mo Ni Se Zn P 0 PAN 1 0 PAN 2 Lime Applied 12 0 'OTALS: 15708 0 0.00445 0 0.3668 0.04585 0.00131 0.09825 0.01703 0 0.8908 222.7 165.5252 0 Date lbs/ac ,nnuallbs/acre 'urrent Cumulative lbs/ac 0 0.00445 0 0.3668 0.04585 0.00131 0.09825 0.01703 0 0.8908 rior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 ermitted C. P. L. R.*** 36 34 NA 1338 267 15 NA 374 89 2498 250 emit PAN Limit Istnd Crop / I certify, tinder penalty of law, that this document was prepared under my direction or supervision in accordance with a system esigned to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are ignificant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." .2,� *Application Method: S - Surface, IN -Injection, INC- Incorporation Signatidire of Land Applier Date **Volitilization Rate: Surface- 0.5. Iniection/Incorporation - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading- Rate * * The RSSF Data and the I)ry cons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered ie. FSF N I to MFLSF into the tame numbered column on the MFLSF as is entered on the identical[.) numbered FS1 ro-w to properly- complete the metals equations. row DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM I FacilitN Niame: City of Marion Permit Number: �N-\N'TP Name: City of Marion WWTP NPDES Number Monitoring Period: From I/l/2003 To 12/31/2003 WQ001996U NCO031879 Pathogen Reduction (40 CFR 503.32) - Please indicate level achieved and alternative performed: Class Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ 11'applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying Heat Treatment ❑ Thermophilic ❑ Beta Rai 01 Gamma Ray Pasteurization ❑ Class B: I Alternative 1pf Alternative 2 ❑ Alternative 3 ❑ If applicable to alternative performed Class B onl indicate "Process to Si nifica tly Reduce Patho ens": I.m< Stabilization ❑ Air Drying❑ Composting ❑ Aerobic Digestion - lmel-oblc Digestion❑ If applicable to alternative performed (Class A or Class B) complete the following monit ring data: Parameter Level in Pathogen Density limhei— o Excee- , requellc\ of Sample Type A11,1kil,.1i teci,-niqu` tnrmun Geo. Mean Maximum Units 1:ecal Coliform _' \Ill t�i I le 6t11 power MPN per gram of total ,oIl,ls 01- 2 s Ili to the 6th power F1.1 ,er avail of 40000 WOW 30k, 90 d, a 2400000 MPN 0 1 grab - sm922 INO nlpn per gi-alll Ot total so11d (dry weight) r— r .airll,l K11:1erlti i in lieu of fecal ,:oliform) ; MPN per 4 grams total solid I (dry weight) Vector Attraction Reduction (40 CFR 503.33) - Please indicate Uptioll l Option 2 ❑ Option 3 ❑ 10p.tion 4 option 6 ❑ 10ption 7 ❑ 10ption 8 ❑ Option 9 eccoi attraction reduction options were performed ❑ OF RTIFICATION STATEMENT (please check the appropriate "I certify, under penalty of law, that the pathogen requl attraction reduction requirement in 40 CFR 503.33 have ❑ • I certify, under penalty of law, that the pathogen requ attraction reduction requirement in 40 CFR 503.33 hav this statement attach an explanation why you have not i -This determination has been made under my direction and supervision to accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." I- q ♦��� Preparcr Name and Title (type or print) Land Applier Nike and Title (if applicable)(type or print) 2-co ,sk y u ature'of Preparer Date Signature'of nd Applier (if applicable) Date DENR FORM RF (512003) y aceAnalytical® www.pacelahs.com Pace Analytical Services, Inc. 2225 Riverside. Orive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client:Project ID: DIGESTER SLUDGE ab Sample No: 931494678 Project Sample Number: 9337151.003 Date Collected: 02/28/03 12:00 lient Sample ID: DIGESTER SLUDGE GRAB -FECAL #3 Matrix: Water Date Received: 02/28/03 14:05 arameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt icrobiology =ecal Coliform MPN Water Method: SM 9223 Coliform, Fecal 40000 02/28/03 ACL Date: 03/13/03 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 37712 FL NELAP E87648 without the written consent of Pace Analytical Services, Inc. y �CC99 Page: 3 of 13 Laboratory Certification IDs TN Drinking Water 02980 SC Environmental 99030 aceAnalytical® www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252. 4618 Lab Project Number: 9337151 Client Project ID: DIGESTER SLUDGE _ab Sample No: 931494686 Project Sample Number: 9337151.004 Date Collected: 02/28/03 12:00 ,lient Sample ID: DIGESTER SLUDGE GRAB -FECAL #4 Matrix: Water Date Received: 02/28/03 14:05 'arameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt licrobiology Fecal Coliform MPN Water Method: SM 9223 Coliform, Fecal 80000 02/28/03 ACL .N Date: 03/13/03 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. FL NELAP E87648 N �CCORO Page: 4 of 13 Laboratory Certification IDs TN Drinking Water 02980 SC Environmental 99030 y ace Analytical www. pacelahs.com Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client:Project ID: DIGESTER SLUDGE 931494694 Project Sample Number: 9337151.005 Date Collected: 02/28/03 12:00 Lab Sample No: Client Sample ID: DIGESTER SLUDGE GRAB -FECAL #5 Matrix: Water Date Received: 02/28/03 14:05 Results Units Reaort Limit Analyzed By CAS No. Qual RegLmt Parameters Microbiology Fecal Coliform MPN Water Method: SM 9223 Coliform,,Fecal 2200000 02/28/03 ACL Date: 03/13/03 aboratory Certification Qs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. FL NELAP E87648 Page: 5 of 13 Laboratory Certification IDs TN Drinking Water 02980 SC Environmental 99030 7acieAnalytical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside.Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client:Project ID: DIGESTER SLUDGE b Sample No: 931494702 Project Sample Number: 9337151.006 Date Collected: 02/28/03 12:00 ient Sample ID: DIGESTER SLUDGE GRAB -FECAL #6 Matrix: Water Date Received: 02/28/03 14:05 rameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt icrobiology ecal Coliform MPN Water Method: SM 9223 Coliform, Fecal 1,700.000 02/28/03 ACL R Date: 03/13/03 Laboratory Certification IN REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. FL NELAP E87648 0 Page: 6 of 13 Laboratory Certification IN TN Drinking Water 02980 SC Environmental 99030 ace Analytical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client:Project ID: DIGESTER SLUDGE Lab Sample No: 931494710 Project Sample Number: 9337151.007 Date Collected: 02/28/03 12:00 Client Sample ID: DIGESTER SLUDGE GRAB -FECAL #7 Matrix: Water Date Received: 02/28/03 14:05 Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt Microbiology Fecal Coliform MPN Water Method: SM 9223 Coliform, Fecal 2.400.000 02/28/03 ACL Date: 03/13/03 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 2 3771 FL NELAP 377without the written consent of Pace Analytical'Services, Inc. 1p ACCp�o Page: 7 of 13 Laboratory Certification IDs TN Drinking Water 02980 SC Environmental 99030 ace Analytical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828, 254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client Project ID: DIGESTER SLUDGE b Sample No: 931494652 Project Sample Number: 9337151.001 Date Collected: 02/28/03 12:00 ient Sample ID: DIGESTER SLUDGE GRAB -FECAL #1 Matrix: Water Date Received: 02/28/03 14:05 rameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt icrobiology 'ecal Coliform MPN Water Method: SM 9223 Coliform, Fecal 230000 02/28/03 ACL Date: 03/13/03 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 NC Drinking Water 37712 This report shall not be reproduced, except in full, FL NELAP E$7648 without the written consent of Pace Analytical Services, Inc. M �LLOR Page: 1 of 13 Laboratory Certification IN TN Drinking Water 02980 SC Environmental 99030 ace Analytical www.pacelabs.com Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828.252.4618 Lab Project Number: 9337151 Client Project ID: DIGESTER SLUDGE Project Sample.Number: 9337151.002 Date Collected: 02/28/03 12:00 ab Sample No: 931494660 #2 Matrix: Water Date Received: 02/28/03 14:05 lient Sample ID: DIGESTER SLUDGE GRAB -FECAL Results Units Report Limit Analyzed By CAS No, Qual RegLmt arameters licrobiology Fecal Coliform MPN Water Method: SM 9223 02/28/03 ACL Coliform, Fecal 40000 ,,. Date: 03/13/03 Page: 2 of 13 Laboratory Certification Ds REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs NC Wastewater 40 TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 FL NELAP 7648 without the written consent of Pace Analytical Services, Inc. \q ^�CCOf „ 0 t Jiii�Y17 �\� • Pace Analytical Services, Inc. 2225 Riverside Drive ace Analytical ® Asheville, 28804 Phone: 828.2.254.7176 www.pacelabs.com . Lab Project Number: 9336579 Fax: 828.252.4618 Client Project ID: CORP.CREEK SLUDGE ANALYSIS Lid results are reported on a dry weight basis Lab Sample No: 931474555 Project Sample Number: 9336579.001 Date Collected: 02/07/03 09:00 Client Sample ID: CORP. CR. SLUDGE GRAB Matrix: Soil Date Received: 02/07/03 15:10 Parameters Results Units Report limit Analyzed By CAS No. Qual RegLmt Metals retals, ICP, trace -level Prep/Method: EPA 3050 / EPA 6010 Aluminum 9200 mg/kg 660 02/11/03 16:20 EWS 7429 90 5 Arsenic ND mg/kg 26. 02/11/03 16:20 EWS 7440.38.2 Cadmium 3.4 mg/kg 2.6 02/11/03 16:20 EWS 7440.43.9 Calcium 8400 mg/kg 260 02/11/03 16:20 EWS 7440.70.2 Copper 280 mg/kg 13. 02/11/03 16:20 EWS 7440.50.8 Lead 35. mg/kg 26. 02/11/03 16:20 EWS 7439.92.1 Magnesium 3300 mg/kg 260 02/11/03 16:20 EWS 7439.95.4 Molybdenum 75. mg/kg 13. 02/11/03 16:20 EWS 7439.98.7 Nickel 13. mg/kg 13. 02/11/03 16:20 EWS 7440.02.0 Potassium 6600 mg/kg 1300 02/11/03 16:20 EWS 7440.09.7 Selenium ND mg/kg 53. 02/11/03 16:20 EWS 7782.49.2 Sodium 4400 mg/kg 660 02/11/03 16:20 EWS 7440.23.5 Zinc 680 mg/kg 53. 02/11/03 16:20 EWS 7440.66-6 Date Digested 02/10/03 02/10/03 _ c Chemistry Percent Moisture Method:.X Moisture Percent Moisture 99.0 X 02/10/03 WCB Total Percent Solids Percent Solids Ammonia, Soil Nitrogen, Ammonia Method: EPA 160.3 1.0 X Method: EPA 350.3 662. mg/kg Total Kjeldahl Nitrogen, Soil Method: EPA 351.2 Nitrogen, Kjeldahl, Total 166000 mg/kg Nitrogen, Nitrate plus Nitrite Method: EPA 353.2 Nitrate -Nitrite (as N) 84. mg/kg PH, Soil PH Method: EPA 9045 5.53 units Plant Available Nitrogen Method: Nitrogen 50000 Date: 02/21/03 mg/kg 02/10/03 WCB 114. 02/19/03 ALA 7727.37.9 116. 02/18/03 ALA 40. 02/20/W EWS 7727.37-y 02/14/03 WCB 1.0 02/20/03 EWS 7727.37.9 Page: 1 of 12 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs NC Wastewater 40 TN Drinking Water 02980 NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030 FL NELAP E87648 without the written consent of Pace Analytical Services, Inc. ACC._ aceAnalytical" www.pacelabs.com Solid results are reported on a dry weight basis Lab Sample No: 931474555 Client Sample ID: CORP. CR. SLUDGE GRAB Pace Analytical Services, Inc; 9800 Kiray Avenue, Suite 100 Hunte/sville, NC 28078 Phone: 704,875.9M Far 704,875.M Lab Project Number: 9241270 Client Project ID: Marion 9336579 Project Sample Number: 9241270-001 Date Collected: 02/07/03 09:00 Matrix: Soil Date Received: 02/07/03 15:10 Parameters Results Units Report Limit Dom_ Analyzed By CAS No. Oual ReaLmt Metals Trace ICP Metals, TCLP Leach. Method: EPA 6010 Date Digested 02/13/03' 02/13/03 Trace ICP Metala, TCLP Leach Arsenic Barium Cadmium Chromium Lead Selenium Silver Date Digested Prep/Method: EPA 3010 / EPA 6010 0.0080 mg/l 0.0050 0.11 mg/1 0.0050 NO mg/1 0.0010 0.0062 mg/1 0.0020 0.025 mg/l 0.0050 0.012 mg/1 0.0050 ND mg/1 0.0020 02/19/03 Mercury, CVAAS, TCLP Leachate Method: EPA 7470 Mercury ND mg/l Mercury, CVAAS, in Soil Mercury Wet Chemistry Percent Moisture Percent Moisture Phosphorus, Total, Soil Phosphorus GC/MS Semivolatiles Semivolatile Organics", TCLP 1,4-Dichlorobenzene 2,4-Dinitrotoluene Hexachloro-1,3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol (o-Cresol) 3&4-Methylphenol Nitrobenzene Pentachlorophanol Data: 02/19/03 Method: EPA 7471 1.0 mg/kg Method: % Moisture 99.1 it 1.0 02/19/03 13:48 DJR 7440-38-2 1.0 02/19/03 13:48 DJR 7440-39.3 1..0 02/19/03 13:48 DJR 7440-43-9 1.0 02/19/03 13:48 DJR 7440-47-3 1.0 02/19/03 13:48 DJR 7439-92-1 1.0 02/19/03 13:48 DJR 7782-49-2 1.0 02/19/03 13:48 DJR 7440-22-4 02/19/03 0.00020 1.0 02/19/03 LBG 7439: 97-6 0.38 94.5 02/19/03" LBO 7439-97-6 Method: EPA 365.1 Modified 170000 mg/kg 5400 Prep/Method: EPA 3510 / EPA 8270 ND mg/1 0.75 ND mg/1 0.013 NO mg/l 0.050 ND mg/1 0.013 ND mg/1 0.30 ND mg/1 20. ND mg/1 20. ND mg/1 0.20 ND mg/1 10. 1.0 02/14/03 18:15 HEH 5430 02/14/03 BYR 7723-14-0 1.0 02/18/03 16:19 BET 106-46-7 1.0 02/18/03 16:19 BET 121-14-2 1.0 02/18/03 16:19 BET 87-,68-3 1.0 02/18/03 16:19 BET 118-74-1 1.0 02/18/03 16:19 BET 67-72-1 1.0 02/18/03 16:19 BET 95-48-7 1.0 02/18/03 16:19 BET 1.0 02/18/03 16:19 BET 9.8-95-3 1.0 02/18/03 16:19 BET 87-86-5 t aeoratory Cerfiticatlon IDs I ahoratory Certification IDs NC Wastewater 12 - REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water 37706 This report shall not be reproduced, except In full, VA Drinking Water 213 Sc 99006 without the written consent of Pace Analytical Services, Inc. FL NELAP E87627 Page, 1 of 17 aceAnalytical" W11nv. p8Ce18bS.CDa3 Lab Sample No; 931474555 Client Sample ID: CORP. CR. SLUDGE GRAB Pace Analytical Services, Inc, 98X Kincey Avenue, Suite 100 Nunteisville, NC 28076 Phone:704.875.9M far: 704.875.9091 Lab Project Number: 9241270 Client Project ID: Marion 9336579, Project Sample Number: 9241270-001 Date Collected: 02/07/03 09:00 Matrix: Soil Date Received: 02/07/03 15:10 Results Unite Report Limit DF _ Analyzed By CAS No. oual ReaLmt Parame ere ND mg/1 0.010 1.0 02/19/03 03:33 BCK 79-01-6 Trichloroethene ND mg/1 0.010 1.0 02/19/03 0303 BCK 75-01-4 Vinyl chloride 91 ti 1.0 02/19/03 03:33 BCK 2037-26-5 Toluene-d8 (S) i 1.0 02/19/03 03:33 BCK 460-00-4 4-Bromofluorobenzene (S) 98 1.0 02/19/03 03:33 BCK 1868-53-7 Dibromofluoromethane (S) 96 i 1.0 02/19/03 03:33 BCK 17060-07-0 1,2-Dichloroethane-d4 (S) 101 i Page; 3 of 17 Date: 02/19/03 t a6oratory Certlllratlon IDs oratory Certification Ins NC Wastewater 12 REPORT OF LABORATORY ANALYSIS KY Drinking Water 90090 NC Drinking Water 37706 This report shall.nol be reproduced, except in full, VA Drinking Water 213 Sc 99005 without the written consent of Pace AnalyticalServices, Inc. Fl. NEIAP E87627 !J aceAnalytical® www.pacelabs.com .ab Sample No: 931494728 ;lient Sample ID: DIGESTER SLUDGE GRAB Pace Analytical Services, Inc. 2225 Riverside Drive Asheville, NC 28804 Phone: 828.254.7176 Fax: 828,252.4618 Lab Project Number: 9337151 Client Project ID: DIGESTER SLUDGE Project Sample Number: 9337151-008 Date Collected: 02/28/03 12:00 Matrix: Water Date Received: 02/28/03 14:05 'arameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt 3ioassay pH Method: EPA 150.1 pH 6.60 units 03/06/03 KAS rlet Chemistry Total Volatile Solids Method: EPA 160.4 Total Volatile Solids 12000 mg/1 1.00 03/06/03 WCB Date: 03/13/03 Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS NC Wastewater 40 This report shall not be reproduced, except in full, NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. FL NELAP E87648 Y �CCpgo Page: A of 13 Laboratory Certification IDs TN Drinking Water 02980 SC Environmental 99030 SOLIDS WORKSHEET VOLATILE SUSPENDED METHODS 18TH EDITION --- METHOD 42540E STANDARD o� 13 � S� 6 3 TIME IN: o RUN DATE: %"��" TIME OUT: /3-5-6 Sig G ANALYST: l�� TIME WEIGHED: VSS FIXED ANALYST: B A-B, B -C C A SAMPLE DATE Sample Filter FILTER FILTER + FLLTER +ASH After Ignition ASH + FILTER ASH TOTAL FixMGSLOIids TOTAL vss MG/L % vss 4 WEIGHT Residue before COLLECT Vol. '� (GRAMS) Ignition, Gr. GRAMS (GRAMS) (GRAMS) GRAMS ML CZ �L /33S-' S • / i 20 Z A S /./io , /�ss/.S D, 039/ D.b/SO o60 .. 3-0 D. b/8 a2C0 a S? O 76 /3Y 70 0, 0 /•/�3 3 79 0.06�� O, DDOS b �- 2S T� + 37 DILUTION 1000000 FACTOR = ML OF SAMPLE Mg Volatile Solids / L = ( A - B) X 1000000 Sample Volt ML. Mg Fixed Solids / L = B - C) X 1000000 Sample Vol., ML. % Volatile Solids = Total VSS Tot. Vss + Tot. Fixed •` BALANCE CALIBRATED DAILY AND RECORDED IN THE ANALYTICAL BALANCE CALIBRTION BOOK LOT #'S GLASS FIBER FILTER: -? 3 (-./2- -�l NCDA Agronomic Division 4300 Reedy Creek Road Southern Soil Builders, Inc. Col)ies to: C/ol*owll of Spruce Pine W-111 sitcs 958 1 loo(s Rd. Roaring; River, NC 28669 AV Iann: 0 IF Test Report R 11/14/03 SERVING N.C. CITIZENS FOR OVER 50 YEARS Wilkes County C 12, $ Agronomist Comments: Field Inform_ ation _Applied Lime Recommendation's See Note Sample No. Last Crop Mo Yr TIA Crop or Year Lime N P205 ISO Mg Cu Zn B Mn NW21 Fes/OG/rim,M 1st Crop: Fes/OG/Tim,M 0 120-200 0 70-90 0 0 0 pH$ 12 2nd Crop: Test Results Soil Class HM% WIV CEC BS106 Ac pH P-1 K-I Ca% Mg% Mn-1 Mn-AI (1)Mn-AI (2) Zn-I Zn-Al Cu-I S-1 SS-j NC&-N AV*-N Na MIN 0.41 1.08 11.8 4.0 0.7 6.6 126 28 67.0 26.0 116 77 1473 1473 507 47 0'. 1Field 9 77 77 Information lied: Lime �RccojWme#Otidos. See Nt Sample No. Last Crop ko- Yr TIA Crop or Year Lime N P20 5 ko Mg Cu Zn B Mn oe NW22 Fes/OG/rim,M I st Crop: Fes/OG/Tim,M -5T 120-200 0 0 0 0 0 0 12 2nd Crop: Test Results -Al (1) Mn-Al (2) Zn-1 Zn-Al Cu-1 S-1 SS -I NC8-N A7A-N Na Soil Class HM% WIV CEC BS016 Ac pH P-1 K-I Ca% M9% Mn-1 Mn MIN 0.41- 1.13 8.1 83.0 1.4 5.7 150 88 54.0 24.0 100 77 1046 1046 712 54 .0.1 yieta-Information Applied Lime Recommendations Mg Cu Zn B Mn See Note Sample No. Last Crop Mo Yr TIA Crop or Year Lime N P205 Iko RI Fes/OG/Tim,M 1st Crop: Fes/OG/Tim,M .9T 120-200 0 2040 0 0 0 0 12 do� I 2nd Crop: Test Results Mn-AI 7 N 'n-1 Zn-Al Cu-1 S-I SS-1 NO3-NAH-N Na Soil Class HM% WIV CEC BS016 Ac pH P-I K-I Ca% Mg% Mn-1 Mn 0.1 MIN 0.76 0.93 13.0 85.0 2.0 5.5 189 60 61.0 22.0 99 76 378 378 185 57 0.1 NCDA Agronomic Division q Suu Icee(ly l,reeK Koau "uclgu, n�, L' i vv I -vzv/ \/. // , Southern Soil Builders, Inc. 958 Ilouts Rd Roaring River, NC 2.8669 Report 02l estl.arm: 6/ 2/03 SERVING N.C. CITIZENS FOR OVER 50 YEARS Wilson County Agronomist Comments: Col) cs lo: C -- 12, $, 3 Field Information lied Lime Recommendations I�0 Cu Zn B Mn See Note Sample No. Last Crop o Yr T/A Crop or Year Lime N R05 FS01 Fes/OG/Tim,M 1st Crop: Fes/OG/Tim,M 0 120-200 60-80 50-70 0 0 0 0 pH$ 12 2nd Crop: Test Results CEC BS•0 Ac pH P-I K I Ca% Mg% Mn-I Mn-AI (1) Mn-AI (2) Zn-I Zn-AI Cu-I S-I SS-1 NO3 NIA-N Na Soil Class HM% W/V 6.7 29 39 60.0 33.0 199 126 88 ss 48 32 0.1 MIN 0.32 1.06 8.8 94.0 0.5 Field Information lied Lime Recommendations Mg Cu Zn B Mn See Note Sample No. Last Crop o Yr T/A Crop or Year Lime N RUs 12 FS02 Fes/OG/Tim,M Ist Crop: Fes/OG/Tim,M 0 120-200 70-90 10-30 0 0 0 0 2nd Crop: Test Results CEC BS% Ac pH P-I K-I Ca% Mg% Mn-I Mn -AI (1)Mn-AI (2) Zn-I Zn-AI Cu-1 S-I SS-1 NC$-N AB-N Na Soil Class HM% W/V 1.14 5. 86.0 0.8 6.4 23 63 55.0 27.0 462 288 5 5 42 23 0.1 MIN 0.51 Feldd Information lied time Recommendations' ' n = I�0 Mg Cu Zn B Mn See Note Sample No. Last Crop o Yr T/A Crop or Year Lime N P205 K2 Corn,Silage 1st Crop: Corn,Silage .7T 180-220 0-20 50-70 0 0 0 0 3 d 2nd Crop: Test Results CEC BS•0 Ac pH P-I K-1 Ca% Mg% Mn-I Mn-AI (1) Mn-AI (2) Zn-I Zn-AI Cu-I S-I SS -I NC$-N AB-N Na Soil Class HM% W/V MIN 1.25 0.96 < .6 , 81.0 L8 5.6 76 69 68.0 10.0 259 172 213 213 79 48 0.0 Field Information Applied Lime Recommendations RO5 le0 Mg Cu Zn B Mn See Note Sample No. Last Crop o Yr T/A Crop or Year Lime N 12 FI Fes/0G/Tim,M 1st Crop: Fes/OG/Tim,M 0 120-200 0 20-+0 0 0 0 0 2nd Crop: 'Pest Results BS% Ac pH P-1 K-I Ca% Mg% Mn-I Mn-AI (1) Mn-AI (2) Zn-1 Zn-AI Cu-1 S-I SS -I N0.3-N Nlf,-N Na Soil Class HM% W/V CEC 6.2 199 58 c 7).0 8.0 1 1 / i 8_ 227 227 638 44 0.0 MIN 0.76 1.03 9-9 900 1.0 Fieldnffir-hiation Liii�c -Recoiiiifi"c'.'iidati"o"n'.s* S-7*-ky),.*.x�-I,-,,L.97,,:) qurower: aouuicrp )oii pjiq'dq§, I!i,, Rep OIL 12 vr.Oo: 04. 2 -Appifed Sam/We No. Lasl Crop Ho Yr T/A Crop or Year Lime N ED 5 KO Afg Cu Z11 See Nole 1 1.) 2002 I. I S1 Clop: 1:(,S/O(;/I,illl,m 7T 120-200 0 12 2nd Cr(-p: Test Results Soil Class HM016 W/V CEC BA Ac PH P-1 K-1 Ca% Mg% Mn-1 Mn-AI (1)Mn-AI (2) Zn-AI Cu-1 S-1 SS-1 NO3-N Nlb-N- Na MIN 0.56 0.95 13.0 88.0 1.5 5.3 267 384 47.0 27.0 599 376 153 153 170 64 0.1 n Fie .%,,1, ormatnonAp 7777777"..'', Sample No. Last Crop Mo Yr TIA Crop or Year Lime N R05 &0 Mg Cu Zn B Mn See Note Yi Fes/OWFim,M ammumb 1st Crop: Fes/OG/rim,M -5T 120-200 50-70 50-70 0 0 0 0 12 2nd Crop: Test Results Soil Class HMI W/V CEC BS% Ac pH P-1 K-I Ca% Mg% Mn-1 Mn-AI (1) Mn-A, (2) Zn-1 Zn _A-1 Cu-1 S-I SS-1 Nc,5-N Nn-N Na MIN 0.56 1.26 6.6 82.0 1.2 5.6 33 41 62.0 17.0 929 574 104 104 78 40 0.1 Sample No. Last Crop Mo Yr TIA Crop or Year Lime N P205 bo Mg Cu Zn B Mn See Note Ki Fes/OG/riin,M 1st Crop: Fes/OG/Tim,M 0 120-200 0 0 0 0 0 0 12 40� 1 1 2nd Crop: Test Results Soil Class HM?lo W/V CEC BS106 Ac pH P-I K-1 Ca%b M9% Mn-1Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-1 S-1 SS -I Na-NAB-N Na MIN 0.51 1-.,12 10.3 91.0 0.9 6.0 118 125 72.0 14.0 329 214 218 218 107 46 0.1 4 Sample No. Last Crop Mo Yr TIA Crop or Year Lime N R05 ko Mg Cit Ziz B Mn See Note 12 Fes/OG/Fim,M 1st Crop: Fes/OG/rini,M 0 120-200 50-70 0-20 0 0 0 0 12 Test Results Soil Class HM016 W/V CEC BS% Ac PH- P-1 K-1 Ca% Mg% Mn-IMn-AI (1)Mn-A1(2) Zu-1 Zn-Al Cu-1 S-1 SS-1 NO3-N AH-N. Na MIN 0.97 1.02 .6 91.0 0.9 6.2 33 1 56.0 31.0 161 111 67 67 59 46 0.1 F>leld Information .8. kp pt Sample No. Last Crop Mo Yr TIA Crop or Year Lime N R05 &0 Mg Cu Zn B Mn See Note GD22 FcsA)GfFijn,M 1st Crop: F(-s/OG/,'Fiin,M 0 120-200 10-30 10-30 0 0 0 0 12 rest Results Soil Class HM% W/V CEC BS% Ac pH P-1 K-1 Ca% M9% Mn-1Mn-AI (1)Mn-AI (2) Zn-1 Zn-AI Cu-I S-1 SS -I NO;-N 1VJh-N Na WN 0.46 1.1U 16.3 96o 0.6 6.3 52 63 82.0 13.0 927 569 296 296 220' 59 0.1