WQ0011260_2004 Annual Report_20050125

fifD
FOUNDED IN 1870
P.O. BOX 520
OLD FORT, NORTH CAROLINA 28762
January 12, 2005
DENR / DWQ / Water Quality Section
Daryl Merritt
Non -Discharge Compliance / Enforcement Unit
1617 Mail Service Center
Raleigh, NC 27699-1617
.,� I:Offic hanyo
tin iiND+rirrr s rz»N..
Jq IV 2 5 2005
Subject: Town of Old Fort Annual Biosolids report, (calendar year 20 ha e ECT.'(OiV
ACe Eni
To Whom It May Concern: o rsP
Ali 1 /05-
The Town of Old Fort operates a 1.2 MGD wastewater treatment plant (NPDES (,4
NC0021229) with an approved modified pretreatment program.
The Town has a bioresidual management permit, # WQ0011260, to process class A
bioresiduals to be sold or given away to the public. The process consists of two 0.75 MG
sludge holding tanks, a 0.7 meter belt press and an RDP lime pasteurization process with
a covered storage pad.
The solids are mixed with quicklime to raise the pH up to 12 or higher after two hours
and 11.5 or greater after 22 hours to satisfy the vector attraction reduction requirement,
and heat the solids to 70 degrees Celsius or greater to satisfy the PFRP requirement.
The Town's bioresiduals management facility underwent renovation in 2004, with a new
larger storage pad and storage shed constructed and a new pasteurization vessel installed.
The covered and enlarged storage pad increases our storage capacity while sheltering the
biosolids from the weather. The pasteurization vessel guarantees that the minimum
temperature of 70 degrees Celsius is maintained for at least 30 minutes.
The Town had 23.57 tons of biosolids in storage at the beginning of 2004. During 2004,
the Town produced 73.90 tons of biosolids. As part -of the WWTP renovation, the Town
was scheduled to receive a spreader truck to distribute biosolids in April 2004. Due to
manufacturing delays, the delivery date was pushed back several times. We did not
receive the truck until October and as of December 31, had still not received the title to
the truck. As a result, the Town did not distribute any biosolids in the year 2004. As

r
soon as the title and tag for the truck are received, we will begin biosolids distribution,
probably February 2005.
Each recipient of biosolids receives a handout that included a description of the product,
intended uses, restrictions of use and a copy of the laboratory analysis:
Enclosed with this narrative are copies of the operational logs and laboratory analysis of
the bioresiduals. If you have any questions or require further information, please contact
me at 828-668-4561.
Sincerely,
Anthony West
Town of Old Fort W®VTP ORC
P.O. Box 520
Old Fort, NC 25762
JAN 2 5 2005
WATER QUALITY SECTION
N1101cherge Com�,I,.oce Ent.

ANNUAL LAND APPLICATION CERTIFICATION FORM
' Pr rmit#: WQ0011260 County: McDOWELL Year: 2004
Facility Name (as shown on permit): TOWN OF OLD FORT
Land Application Operator: ANTHONY WEST Phone: [phone]
Land application of residual solids as allowed by the permit occurred during the past `calender year?
0 Yes 11 No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
Part A:
Total number of application fields in permit:
0
Total number of fields land application occurred during the year:
0 .
Total amount of dry tons applied during the year for all application sites:
0
Total number of acres land application occurred during the yea—r.-F
0
Part B:
Facility was compliant during calendar year 2004 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. M Yes 0 No
If no please, provide a written description why the facility was not compliant, the dates, and explain
corrective action taken:
1. Only residuals approved for this permit were applied to the permitted sites.
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year and three
(3) copies of laboratory results are attached.
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached.
5. All other monitoring was performed in accordance with the permit and reported during the year as required
and three (3) copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table 2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations. RECEIVED
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan. JAN 2 5 2005
11. No runoff of residuals from the application sites onto adjacent property or neff RgBJMyq�" has occurred.
12. All buffer requirements as specified on the permit were maintained during ell pp4cQ*&0f Usiduals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations."
WAYNE STAFFORD, MAYOR
Permittee Name and Title (type or print)
Signature of%reparer*
(if different from Permittee)
. /- o ,gs,
Signatu of Permitta Date
Date Signature of Land Applier Date
(if different from Pew g6RIfC1AiLr--*1 003)

ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FOR]
PERMIT #: WQ0011260 FACILITY NAME: TOWN OF OLD FORT
PRONE: 828-6684561 COUNTY: McDOWELL OPERATOR: ANTHONY WEST
FACILITY TYPE (please check one): Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only)
® Distribution and Marketing (complete Parts A, B, and C)
Was the facility in operation during the past calendar year? Yes Mo No If No skip parts A, B, C and certify forr
Part A*: Part B*:
Volume d ) tons Reci ient Information
Month
Sources(s) (include NPDES # if
applicable)
(
p
Admendment/
Bulking Agent
Residual In
Product Out
Name(s)
January
Town of Old Fort WWTP
0
0
0
NO
February
NCO021229
0
0
0
March
8.24
5.79
14.03
April
10.12
6.68
16.8
May
6.71
4.31
11.02
2O o
June
4.73
3.79
8.52
July
1.9
1.53
3.43
Au st
1.72
1.26
2.98
September
0
0
0
October
3.54
2.36
5.9
November
4.71
3.16
7.87
December
2.03
1.33
3.36
Totals:
Annual d tons :
43.7
30.21
73.91
Adme=hi ent s used:
LIlVM
B�lkin A Ent s used:
Volume (dry tons)
LU o
LU
It
*If more space than given is required, please attach additional information sheet(s). ® Check box if additional sheet(s) are attached
Part C:
Facility was compliant during calendar year 2004 with all conditions of the permit (including but not limited to items 1-3 below)
Division of Water Quality. . Yes -� No If No, please provide a wriiien description why the facility was not coy
L All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory res
2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the E
Quality.
3. No contravention of Ground Water Quality Standards occurred at a monitoring well.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I
that there are significant p realties for submitting false iaiformaiton; includin the ossibility of fines and imprisonment for knowing
Signature OfTer'mit4ee Date Signature of P er** �Dpa�tep��t
(if different from Permittee) **Preparer is definrd. 4FUOR11/1UlVfSDF (5/2003)

ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQOO11260
Facility Name: TOWN OF OLD FORT
NPDES # or
WQ#: NC0021229
WWTP Name: TOWN OF OLD FORT WWTP
Residual Analvsis Data
Laboratory:
Ln
o
o
t-- C.>
b�
N
®
e�
LU
n
1)
2)
3)
4)
5)
PACE ANALYTICAL
Sample or
Composite Date
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significan penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
V Z V dJ�J �• �^��V'' ! � f � •�S
Signature of Prep er Date
--I DENR FORM RSSF (5/2003)

ANNUAL_RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Permit Number: WQ0011260 Laboratory:
Facility Name: TOWN OF OLD FORT
NPDES # or
WQ#: NCO021229
WWTP Name: TOWN OF OLD FORT WWTP
Residual Analysis Data
1) PACE ANALYTICAL
2)
3)
4)
5)
Sample or
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
l V
Signature of Prepay r Date
!4k . DENR FORM RSSF-B (5/2003)

ANNUAL METALS FIELD LOADING SUMMARY FORM*
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name: TOWN OF OLD FORT Total Dry Tons Applied (Annual): 0
Permit #: WQ0011260 Cation Exchange Capacity (non 503 only):
Operator: ANTHONY WEST Owner: TOWN OF OLD FORT
Acres Used: 0 Acres Permitted: 0 Site #: N/A Field #: _ N�,
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw. Percent #);
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
o
H
5
o
Arsenic
0
0
0
0
0
0
0
0
0
0
0
0
Cadmium
0
0
0
0
0
0
0
0
0
0
0
0
Chromiurr
0
0
0
0
0
0
0
0
0
0
0
0
Copper
0
0
0
0
0
0
0
0
0
0
0
0
Lead
0
0
0
0
0
0
0
0
0
0
0
0
Mercury
0
0
0
0
0
0
0
0
0
0
0
0
Molyb-
0
0
0
0
0
0
0
0
0
0
0
0
denum
Nickel
0
0
0
0
0
0
0
1 0
0
0
0
0
Selenium
0
0
0
0
0
0
0
0
0
0
0
0
Zinc
0
0
0 1
0
0 1
0
0
0
.0
0
0
0
Total
Phos-
0
0
0
0
0
0
0
0
0
0
0
0
horus
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Signature of Land Applier Date
DENR FORM MFLSF (5/2003)

ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND'SUBMITTED FOR EACH APPLICATION FIELD.
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Facility Name: TOWN OF OLD FORT WWTP
Owner:
TOWN OF OLD FORT Operator:
Site #: N/A
Field #: N/A
Permit #: WQ0011260 Annual Dry Tons Applied: #VALUE!
ANTHONY WEST Cation Exchange Capacity (non 503):
Acres Utilized: N/A
Acres Permitted:
0
o
0
o
Specify
Totals
Per
Acre
%
Solid
s
I
Dry Tons Per
Acre
Residual
Sources
(Summarize)
i e
Cond.
Dry,
Wet
Moist
Inches
Precip.
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ali-
zation
Rate
TKN
Ammo
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
p p
2
Gal.
Cu.Yd.
LA
ReportA Totals
in Gal.
Crop 1
Crop 2
######I
#VALUE!
#######
#######
######I
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#######
#######
######
#VALUE!
#########
##### ###
TOTALS:
#####
As
Cd
Cr
Cu
Pb
H
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0
0
0
0
0
0
0
0
0
0
0
0
0
Date
lbs/ac
Current Cumulative lbs/ac
0
0
0
0
0
0
0
0
0
0
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
t
••I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signature of Land Applier
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5, Iniection/Incorporation -1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
* * * * The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into
' the some numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF column # 1,
y` DENR FORM FSF (5/2003)

ANNUAL, PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM
i Facility Name: TOWN OF OLD FORT WWTP Permit Number: WQOO11260
WWTP Name: TOWN OF OLD FORT WWTP NPDES Number: NCO021229
Monitoring Period:. From l/1/2004 To 12/31/2004
Pathogen Reduction (40 CFR 503.32) -.Please Indicate level achieved and alternative performed:
Class A: I Alternative 113 1 Alternative 2 ® . . Alternative 3
r
Alternative Alternative 5 ® Alternative 6.
If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens":
Compost 13 1 Heat Drying I Heat TreatmentO I Thermophilic13
Beta Ray 131 Gamma Ray 13 1 Pasteurization
Class B: 7 Alternativel-CF I Alternative 2 Alternative 3
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens":
Lime Stabilization Air Drying Composting Aerobic Digestion
Anaerobic Digestio
If applicable to alternative performed (Class A or Class B) complete the following monitoring data:
Allowable Level Pathogen Density Number ot Frequency iSanplq�alytical
Parameter in Slud e Excee- y Type qg im Geo. Mean axim Units rienePe of Anal sis h-ni ul
Fecal Colifontn
(in lieu of fecal
2 x 10 to the 6th
power NWN per
gram of total
solids or 2 x 10 to
the 6th power
. 1000 mpn per
gram of total solid
S MYN per 4
grams total solid
WE
0 1 ND I MPN/G
0 17/YEARI GRAB 19 zz 1g/E
Vector Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
CERTIFICATION STATEMENT (please check the appropriate, statement)
® "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 Have been met."
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements:)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment."
ANTHONY WEST, WWTP ORC
Prep er Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print)
_I1-lIt
Signature of P pa_rer Date Signature of Land Applier OWPIRO f) RF (5/2003) Date

r y.Rh:i
�ccnalytical °
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 924419625
Client Sample ID: SLUDGE 6/30
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9270641
Client Project ID: SLUDGE ANALYSIS 6/30
a
Project Sample Number: 9270641-001 Date Collected: 06/30/04 10:45
Matrix: Soil Date Received: 06/30/04 15:40
Parameters Results Units Report Limit Analyzed By CAS No. Qua] RegLmt
Microbiology p, 0
Fecal Coliform MPN Solid Method: SM 9221E ,IV
�
Coliform, Fecal ND 06/30/04 MMG ✓ o
Metals
Trace ICP Metals, TCLP Leach
Arsenic
Barium
Cadmium
Chromium
Lead
Selenium
Silver
Date Digested
Metals, Trace ICP
Aluminum
Arsenic
Cadmium
Calcium
Chromium
Copper.
Lead
Magnesium
Molybdenum
Nickel
Potassium
Selenium
Sodium
Zinc
Date Digested
qN
►�q Zoos
Prep/Method:
EPA 3010
/ EPA 6010
/Ilp7,p�R�QU,Q(��,
0.064
mg/l
0.025
07/07/04
17:06
LBG
7440-38- fge C V @�
0.18
mg/l
0.025
07/07/04
17:06
LBG
7440-39-3 7/
ND
mg/l
0.0050
07/07/04
17:06
LBG
7440-43-9
ND
mg/l
0.010
07/07/04
17:06
LBG
7440-47-3
ND
mg/l
0.025
07/07/04
17:06
LBG
7439-92-1
0.030
mg/l
0.025
07/07/04
17:06
LBG
7782-49-2
ND
mg/l
0.010
07/07/04
17:06
LBG
7440-22-4
07/02/04
07/02/04
Prep/Method: EPA 3050 / EPA 6010
4800
mg/kg
23.
07/01/04
10:13
ALV
7429-90-5
3.8
mg/kg
1.1
07/01/04
10:13
ALV
7440-38-2
0.35
mg/kg
0.23
07/01/04
10:13
ALV
7440-43-9
220000
mg/kg
23.
07/01/04
10:13
ALV
7440-70-2
41.
mg/kg
0.45
07/01/04
10:13
ALV
7440-47-3
190
mg/kg
0.45
07/01/04
10:13
ALV
7440-50-8
11.
mg/kg
1.1
07/01/04
10:13
ALV
7439-92-1
4400
mg/kg
23.
07/01/04
10:13
ALV
7439-95-4
1.7
mg/kg
1.1
07/01/04
10:13
ALV
7439-98-7
5.3
mg/kg
1.1
07/01/04
10:13
ALV
7440-02-0
1800
mg/kg
230
07/01/04
10:13
ALV
7440-09-7
2.0
mg/kg
1.1
07/01/04
10:13
ALV
7782-49-2
1900
mg/kg
230
07/01/04
10:13
ALV
7440-23-5
170
mg/kg
2.3
07/01/04
10:13
ALV
7440-66-6
07/01/04 02:30
07/01/04
02:30
Mercury., CVAAS, TCLP Leachate Method: EPA 7470
Date Digested 07/01/04
Mercury, CVAAS, TCLP Leachate Method: EPA 7470
Mercury ND mg/l
Date: 07/19/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FL NELAP E87648
07/01/04
0.00020 07/06/04 05:30 ALV 7439-97-6
REPRO' OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
, ne ac
Page: 1 of 30
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NFLAP F87697

^ten
n
r �
A ce nautical °
.! m
www.pacelabs.com
Lab Sample No: 924419625
Client Sample ID: SLUDGE 6/30
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9270641
Client Project ID: SLUDGE ANALYSIS 6/30
Project Sample Number: 9270641-001 Date Collected: 06/30/04 10:45
Matrix: Soil Date Received: 06/30/04 15:40
Parameters
Results
Units Report Limit
Analyzed
By
CAS No. Qual RegLmt
Mercury, CVAAS, in Soil
Method: EPA
7471
Mercury
0.089
mg/kg
0.010
07/06/04
06:45
ALV
7439-97-6
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
58.9
%
07/01/04
10:34
TSE
Total Percent Solids
Method: EPA
160.3
Percent Solids
41.1
%
07/08/04
KDF
Nitrogen, Ammonia
Method: EPA
350.1 Modified
Nitrogen, Ammonia
180
mg/kg
21.
07/01/04
22:30
BMF
7727-37-9
Total Kjeldahl Nitrogen, Soil
Method: EPA
351.2
Nitrogen, Kjeldahl, Total
14000
mg/kg
240
06/30/04
18:52
ARH
Nitrogen, Nitrate plus Nitrite
Method: EPA
353.2 Modified
Nitrate as N
41.
mg/kg
24.
07/07/04
10:32
ARH
Nitrate -Nitrite (as N)
61.
mg/kg
24.
07/07/04
10:32
ARH
7727-37-9
Phosphorus, Total, Soil
Method: EPA
365.2
Phosphorus
1660
mg/kg
26.4
06/30/04
22:20
BMF
7723-14-0
pH
Method: EPA
9045
pH
11.6
units
07/09/04
18:12
CD1
1
Plant Available Nitrogen
Method:
Nitrogen
4300
mg/kg
1.0
07/13/04
08:15
ARH
7727-37-9
GUMS Semivolatiles
Semivolatile Organics, TCLP
Prep/Method:
EPA 3510 / EPA
8270
1,4-Dichlorobenzene
ND
mg/l
0.75
07/08/04
18:41
BET
106-46-7
2,4-Dinitrotoluene
ND
mg/l
0.013
07/08/04
18:41
BET
121-14-2
Hexachloro-1,3-butadiene
ND
mg/l
0.050
07/08/04
18:41
BET
87-68-3
Hexachlorobenzene
NO
mg/l
0.013
07/08/04
18:41
BET
118-74-1
Hexachloroethane
NO
mg/l
0.30
07/08/04
18:41
BET
67-72-1
2-Methylphenol (o-Cresol)
NO
mg/l
0.050
07/08/04
18:41
BET
95-48-7
3&4-Methylphenol
NO
mg/l
0.010
07/08/04
18:41
BET
Nitrobenzene
NO
mg/l
0.20
07/08/04
18:41
BET
98-95-3
Date: 07/19/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
FI AIFI AP ' F87648
Page: 2 of 30
REPORT OF LABORATORY ANAILYSS
This report shall not be reproduced, except in full, Charlotte Certification IDs
without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
o%N.A000gO NC Drinking Water 37706
SC 99006
FL NELAP F87627

aceA, Pica I °
www.pacelabs.com
Lab Sample No: 924419625
Client Sample ID: SLUDGE 6/30
Parameters
Pentachlorophenol
Pyridine
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
Nitrobenzene-d5 (S)
2-Fluorobiphenyl (S)
Terphenyl-d14 (S)
Phenol-d5 (S)
2-Fluorophenol (S)
2,4,6-Tribromophenol (S)
Date Extracted
GC Semivolatiles
Pesticides, TCLP Leachate
gamma-BHC (Lindane)
Chlordane
Endrin
Heptachlor
Methoxychlor
Toxaphene
Tetrachloro-m-xylene (S)
Decachlorobiphenyl (S)
Date Extracted
Acid Herbicides, TCLP Leachate
2,4-D
2,4,5-TP (Silvex)
2,4-DCPA (S)
Date Extracted
GUMS Vol ati l es
Volatile Organics, TCLP Leach
Benzene
2-Butanone (MEK)
Carbon tetrachloride
Chlorobenzene
Chloroform
1,2-Dichloroethane
1,1-Dichloroethene
Date: 07/19/04
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FI NIFI AP
- FR7F48
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9270641
Client Project ID: SLUDGE ANALYSIS 6/30
Project Sample Number: 9270641-001
Matrix: Soil
Results
Units
Report Limit
Analyzed
By
ND
mg/l
10.
07/08/04
18:41
BET
ND
mg/l
0.50
07/08/04
18:41
BET
ND
mg/l
40.
07/08/04
18:41
BET
NO
mg/l
0.20
07/08/04
18:41
BET
55
%
07/08/04
18:41
BET
55
%
07/08/04
18:41
BET
81
Y.
07/08/04
18:41
BET'
18
Y.
07/08/04
18:41
BET
29
%
07/08/04
18:41
BET
79
%
07/08/04
18:41
BET
07/07/04
07/07/04
Prep/Method: EPA 3510 / EPA 8081
Date Collected: 06/30/04 10:45
Date Received: 06/30/04 15:40
87-86-5
110-86-1
95-95-4
88-06-2
4165-60-0
321-60-8
1718-51-0
4165.62-2
367-12-4
Qual RegLmt
NO
mg/l
0.040
07/08/04
17:59
JEM
58-89-9
ND
mg/l
0.0030
07/08/04
17:59
JEM
57-74-9
ND
mg/l
0.0020
07/08/04
17:59
JEM
72-20-8
0.00088 mg/l
0.00080
07/08/04
17:59
JEM
76-44-8 2
NO
mg/l
1.0
07/08/04
17:59
JEM
72-43-5
NO
mg/l
0.050
07/08/04
17:59
JEM
8001-35-2
56
%
07/08/04
17:59
JEM
877-09-8
55
%
07/08/04
17:59
JEM
2051-24-3
07/07/04
07/07/04
Prep/Method:
EPA 3510
/ EPA 8151
ND
mg/l
1.0
07/12/04
17:09
JEM
94-75-7
ND
mg/l
0.10
07/12/04
17:09
JEM
93-72-1
145
Y.
07/12/04
17:09
JEM
19719-28-9
07/07/04
07/07/04
Method: EPA
8260
0.012
mg/l
0.010
07/14/04
14:17
RWS
71-43-2 3
1.8
mg/l
0.010
07/14/04
14:17
RWS
78-93-3 3
ND
mg/l
0.010
07/14/04
14:17
RWS
56-23-5
ND
mg/l
0.010
07/14/04
14:17
RWS
108.90-7
ND
mg/l
0.010
07/14/04
14:17
RWS
67-66-3
ND
mg/l
0.010
07/14/04
14:17
RWS
107-06-2
NO
mg/l
0.010
07/14/04
14:17
RWS
75-35-4
Page: 3
of 30
REPORT OF LABORATORY ANALYS93
This report shall not be reproduced, except
in full,
Charlotte Certification IDs
without the
written consent of Pace Analytical
Services, Inc.
NC Wastewater
12
NC Drinking Water
37706
Sc
99006
`'
FL NFI AP
F97627

Pace Analytical Services, Inc.
2225 Riverside Drive
:Analytical" Asheville, NC 28804
Phone: [phone]
www. pacelabs. com Fax: [phone]
Lab Project Number: 9270641
Client Project ID: SLUDGE ANALYSIS 6/30
Lab Sample No: 924419625 Project Sample Number: 9270641-001 Date Collected: 06/30/04 10:45
Client Sample ID: SLUDGE 6/30 Matrix: Soil Date Received: 06/30/04 15:40
Parameters
Results
Units
Report Limit
Analyzed
By
CAS No.
Qual RegLmt
Tetrachloroethene
0.022
mg/l
0.010
07/14/04
14:17
RWS
127-18-4
.3
Trichloroethene
ND
mg/l
0.010
07/14/04
14:17
RWS
79-01-6
Vinyl chloride
ND
mg/l
0.010
07/14/04
14:17
RWS
75-01-4
Toluene-d8 (S)
70
Y.
07/14/04
14:17
RWS
2037-26-5
4
4-Bromofluorobenzene (S)
63
Y.
07/14/04
14:17
RWS
460-00-4
4
Dibromofluoromethane (S)
0
Y.
07/14/04
14:17
RWS
1868-53-7
4
1.2-Dichloroethane-d4 (S)
107
Y.
07/14/04
14:17
RWS
17060-07-0
Date: 07/19/04 Page: 4 of 30
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
fnaac,_
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC 99006
FL NELAP E87627

Pace Analytical Services, Inc.
2225 Riverside Drive
:Analytical' Asheville, NC 28804
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9270641
Client Project ID: SLUDGE ANALYSIS 6/30
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method 9071B modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
ND Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
(S) Surrogate
[1] Analysis conducted in excess of EPA recommended holding time.
[21 Analyte is found in the associated blank as well as in the sample (CLP B-Flag).
[31 The reported result may b biased high due to matrix interference with the internal standard. This was
confirmed by reanalysis of the sample.
[41 Low surrogate recovery was confirmed as a matrix effect by a second analysis.
Date: 07/19/04
Asheville Certification IDs
NO Wastewater
40
NO Drinking Water
37712
SC Environmental
99030
FL NELAP
E87648
ET OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
O �N ACCpgo
l
aW�' fact
Page: 5 of 30
Charlotte Certification IDs
NO Wastewater 12
NO Drinking Water 37706
SC 99006
FL NELAP F87627

A %J1J i 0 HIIU1YL1t;U1 nt:gUUbL UUE;U F11It:HL
��CeA%�aI ICaI
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed.accurately..
c �
www.pacelabs.com
Re wired Client Information: Section B
.
�S , l t
Report To:
Required Client Information: Section A
4
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Page:
To Be Completed b Pace. Analytical and Client SeCtlOn C
Company,— -"
Copy To:
Quote Reference;
-f
Client Information (Check quote/contract):
Address.: r'."
Invoice To:
Requested Due Date:
*TAT: /
Project Manager:
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*Turn around time less than 14 days subject to
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Rush Turnaround Surcharge.
Project #: /
cr 1
Project Name: , ,. ,
Profile #:
`, r
Turn Around Time (TAT) in calendar days.
Phone
L ;
Fax
Project Number:
Requested
Analysis' .0
Section D Re uired Client Information:
q
valid Matrix codes
MATRIX CODE
a:
Preservatives
DRINKING WATER
GROUNDWATER
DW
GW
w
❑
wn
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SW
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START
END
W (AZ, 0-9
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DATE
TIME
DATE
TIME
Sample IDs MUST BE UNIQUE
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OTHER OT
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:t--I,,NC ❑ SC ❑ GA ❑ NPDES ❑ GROUNDWATER ❑ DRINKING
❑ Other ❑ UST ❑ RCRA ._ >EFOther_
SAMPLE CONDITION SAMPLE NOTES
Temp in oC
{
Received on Ice,�fY,
N" i
Sealed Cooler
Sa„ples Intact ;
IYIFV
Additional Comments:
PRINT Name of SAMPLER:
SIGNATURE of SAMPLER:-" DATE Signed: (MM / DD / YY)
max.
SEE REVERSE SIDE --FOR INSTRUCTIONS Form C0001 Rev. 0304

aceAnalytical°
www.pacelahs.com
Solid results are reported on a dry weight basis
Lab Sample No: 924964257
Client Sample ID: SLUDGE GRAB 4
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: 828,254.7176
Fax: 828.252,4618
Lab Project Number: 9281441
Client Project ID: SLUDGE FECAL ANALYSIS
Project Sample Number: 9281441.001 Date Collected: 11/11/04 10:55
Matrix: Soil Date Received: 11/11/04 15:53
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E
Coliform, Fecal ND 11/12/04 MMG
Date: 11/23/04
REPORT OF -LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 w
SC Environmental 99030
Page: 1 of 5
Charlotte Certification IDs.
NC Wastewater 12
NC Drinking Water 37706
Sc 99006

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical o Asheville, NC 28804
Phone: [phone]
www.paceiahs.com Fax [phone]
Lab Sample No: 924964281
Client Sample ID: SLUDGE GRAB 5
Microbiology
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 11/23/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
11 —1 — 1-1—
Lab Project Number: 9281441
Client Project ID: SLUDGE FECAL ANALYSIS
Project Sample Number: 9281441-002 Date Collected: 11/11/04 10:50
Matrix: Soil Date Received: 11/11/04 15:53
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: SM 9221B/E
ND 11/12/04 MMG
Page: 2 of 5
REPORT OF LAOORATRY ANALYSIS
This report shall not be reproduced, except in full, Charlotte Certification IDs
without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
N ACCOR NC Drinking Water 37706
Wo•;ta ,,\�� Sc 99006

Analytical °
www, pacelabs. com
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281441
Client Project ID: SLUDGE FECAL ANALYSIS
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method 90716 modified to use ASE.
All pH. Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
NO Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Date: 11/23/04
Page: 3 of 5
REPORT OF LABORATORY ANALYSIS
Asheville Certification IN This report shall not be reproduced, except in full, Charlotte. Certification IN
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N A��oRo NC Drinking Water 37706
SC Environmental 99030 Sc 99006

�;' r
>-aceAnalytical
a®■ •i ru ® w■ v�o . ■ yr • i a I—ly I—, . 111— vI o
The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
�'
4 y �s
www.pacelabs.com
Re uired Client Information:
Section B
f
`—'' I x
a
Required Client Information: Section A
Report To:.,...--_ -'
r `
Page: # of j
Section C
To Be Completed by Pace Analytical and Client
Company----
Copy To:
Quote Reference:
Client Information (Check quote/contract):
Address
Invoice To:
Requested Due Date:
TAM)
Project Manager: /
}t
19
P.O.
*Turn around time less than 14 days subject to
Project #:
h r 7, ) ram
laboratory and contractual obligations and may result in a
j
Project Name:
Profile #:
Rush Turnaround Surcharge.
Turn Around Time (TAT) in calendar days.
Phone
Fax
Project Number:
Requested u
Analysis:
.. _,
Section D Re uired Client Information:
q
valid Matrix codes
MATRIX CODE
a
..
Preservatives
-
DRINKING WATER DW
GROUNDWATER GW
w
0
w 2
d0
o_ z
5 O
r,
AMPLE 1'f [
S A M P L E I®
SURFACE WATER SW
O
W U
~ w
WASTE WATER WW
ODUCT 6L
SOIL
d¢
COLLECTED
d O
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COO
One character per box.
OIL OL
Q
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START
END
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WIPE WP
M
Coo
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20
N
Y
Sample IDS MUST BE UNIQUE
OTHER OAIR T
DATE
TIME
DATE
TIME
2
=
=
Z
Z
2
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+J
7
�
4
Temp in °C
Received on Ice:
`YIN
Sealed Cooler
Y/N
.Sar.nples Intact
'Y/N
Additional Comments:
�.d
PRINT Name of SAMPLER: �..-
_ �a ; i_ i;
SIGNATURE of SAMPLER: = " " DATE Signed: (MM / DID/ W)
Form cI-
SEE REVERSE SIDE FORINSTRUCTIONS
_ n

t
Analytical
www.pacelabs.com
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28604
Phone: [phone] '
Fax: [phone]
Lab Project Number: 9281083
Client Project ID: SLUDGE ANALYSIS (Fecal MPN)
Lab Sample No: 924949217 Project Sample Number: 9281083-001 Date Collected: 11/09/04 10:20
Client Sample ID: SLUDGE GRAB 1 Matrix: Soil Date Received: 11/09/04 14:44
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E
Coliform, Fecal ND 11/10/04 MMG
Wet Chemistry
Percent Moisture Method: 7 Moisture
Percent Moisture 53.8 Y. 11/16/04 09:11 DHW
Date: 11/22/04
REPORT OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full,
NC Wastewater 40 - without the written consent of Pace Analytical Services, Inc.
NC Drinking Water 37712 N 0.CCCRo
SC Environmental 99030
Page: 1 of 7
Charlotte Certification IDs
NC Wastewater 1.2
NC Drinking Water 37706
SC — 99006

a
aceAnalytical °
www.pacelahs.com
Lab Sample No: 924949225
Client Sample ID: SLUDGE GRAB 2
Parameters
Microbiology
Fecal Coliform MPN Solid
Coliform, Fecal
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 11/22/04
Results
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281083
Client Project ID: SLUDGE ANALYSIS (Fecal MPN)
Project Sample Number: 9281083-002 Date Collected: 11/09/04 10:25
Matrix: Soil Date Received: 11/09/04 14:44
Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: SM 9221B/E
ND
Method: % Moisture
59.2 %
11/10/04 MMG
11/16/04 09:12 DHW
Page: 2 of 7
RAP®RT in
OF LABORATORY ANALYSIS
Asheville Certification IDs This report shall not be reproduced, except in full, Charlotte Certification IDs
NC Wastewater 40 without the written consent of Pace Analytical Services, Inc. NC Wastewater 12
NC Drinking Water 37712 N ^��oRo NC Drinking Water 37706
0
SC Environmental 99030 Sc 99006

u
ace Analytical °
www.pacelabs.com
Lab Sample No: 924949233
Client Sample ID: SLUDGE GRAB 3
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: 828.252,4618
Lab Project Number: 9281083
Client Project ID: SLUDGE ANALYSIS (Fecal MPN)
Project Sample Number:.9281083-003 Date Collected: 11/09/04 10:30
Matrix: Soil Date Received: 11/09/04 14:44
Parameters Results - Units Report Limit Analyzed By CAS No. ual RegLmt
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E
Coliform, Fecal ND 11/10/04 MMG
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 50.6 Y. 11/16/04 09:12 DHW
Date: 11/22/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030^
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCpq
Page: 3 of 7
Charlotte Certification IN
NC Wastewater . 12
NC Drinking Water 37706
Sc 99006_

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical o Asheville, NC 28804
Phone: [phone]
www. pace/abs. com Fax: [phone]
Lab Project Number: 9281083
Client Project ID: SLUDGE ANALYSIS (Fecal MPN)
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method 9071E modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
NO Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Date: 11/22/04
Asheville Certification IDs
NC Wastewater * 40
NC Drinking Water 37712
SC Environmental 99030
M NIM AD C:Q7anQ
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
„�ACCpq
Page: 4 of 7
Charlotte Certification IN
NC Wastewater
12
NC Drinking Water
37706
SC .
ri KIM An
99006
rn�f n�

`� �' �nt►l�V-hlr-l�dJZ+ I UUY / Anaiyucai mequest ®®current
.. , aceAnalyticel c The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
f `,
www.pacela6s.com Required Client Information: Section S . ; �,� ..,�. 9
Report To:.-
uired Client Information: Section A�Bge: f Of
pany- -
To Be Completed by Pace Analytical and Client Section C
Copy To:
Client Information (Check q
ass _ Invoice To: Requested Due Date:
P.O. `Turn around time less t
'= laboratory and contract
Project Name: Rush Turnaround Surc
Turn Around Time (TA
-none Fax _ F
I ,
Section D Required Client Information:
S M P E ID
One character per box.
W (AZ, 0-9 / .-)
Sample IDs MUST BE UNIQUE
Temp in °C
Received on Ice
'Y/.N
Sealed Cooler
Y/N
Samples Intact
Y/N
AuclAtional Comments:
Number:
Valid Matrix Codes
MATRIX CODE
a
DRINKING WATER DW
GROUNDWATER GW
.0
ILO
SURFACE WATER SW
O
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WASTE WATER WW
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PROSOIILDUCT SL
a ¢
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an 14 days subject to
Project #:
al obligations
arge.
calendarin days.
Preservatives
Remarks Lab ID
11 son
■®■■■■■■■N
■
■
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on
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DATE
TIME
AC.GEP
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SAMPLER NAMEAND SIGNiATUREiIPRINT
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Name ot 8AMPLER:
..
SEE REVERSE SIDE FOR INSTRUCT10KIR Form C0001 Rev. 0304

aceAnaly ical°
www.pacelabs.com
Solid results are reported on a dry weight basis
Lab Sample No: 924982861
Client Sample ID: SLUDGE GRAB 6
Parameters
Microbiology
Fecal Coliform MPN Solid
Coliform, Fecal
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 11/29/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
GI N[I nn Co70no
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281789
Client Project ID: SLUDGE FECAL ANALYSIS
Project Sample Number: 9281789-001 Date Collected: 11/17/04 11:00
Matrix: Soil Date Received: 11/17/04 12:32
Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Method: SM 9221B/E
ND 11/18/04 MMG
Method: % Moisture
51.5 Y.
11/18/04 09:38 DHW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�N ACCOA
Page: 1 of 6
Charlotte Certification IDs
NC Wastewater 12
NC Drinking Water 37706
SC99006 ^r ^^ '

aceAnalytical °
www.pacelabs.com
Lab Sample No: 924982887
Client Sample ID: SLUDGE GRAB 7
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Phone: [phone]
Fax: [phone]
Lab Project Number: 9281789
Client Project ID: SLUDGE FECAL ANALYSIS
Project Sample Number: 9281789-002 Date Collected: 11/17/04 11:05
Matrix: Soil Date Received: 11/17/04 12:32
Parameters Results Units Report Limit Analyzed By CAS No. Qual RegLmt
Microbiology
Fecal Coliform MPN Solid Method: SM 9221B/E
Coliform, Fecal ND 11/18/04 MMG
Wet Chemistry
Percent Moisture
Percent Moisture
Date: 11/29/04
Asheville Certification IDs
NC Wastewater
40
NC Drinking Water
37712
SC Environmental
99030
M RIM AD
CQ7FAQ
Method: % Moisture
51.2
11/18/04 09:38 DHW
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
�N RC�R
R
Page: 2 of 6
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
M NCI AD
CQ7G77

Pace Analytical Services, Inc.
2225 Riverside Drive
Analytical o Asheville, NC 28804
Phone: [phone]
www.pacelabs.com Fax: [phone]
Lab Project Number: 9281789
Client Project ID: SLUDGE FECAL ANALYSIS
PARAMETER FOOTNOTES
Inorganic Wet Chemistry and Metals Analyses were performed at our Pace Asheville laboratory and Organic
testing was performed at our Pace Charlotte laboratory unless otherwise footnoted.
Method 9071E modified to use ASE.
All pH, Free Chlorine, Total Chlorine and Ferrous Iron analyses conducted outside of EPA recommended immediate
hold time.
NO Not detected at or above adjusted reporting limit
NC Not Calculable
J Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit
MDL Adjusted Method Detection Limit
Date: 11/29/04
Asheville Certification IDs
NC Wastewater 40
NC Drinking Water 37712
SC Environmental 99030
ri nin nn rn'rAn
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
\N ACCpRO
t�OS. C\•9v
�JM A��✓A91
Page: 3 of 6
Charlotte Certification IDs
NC Wastewater
12
NC Drinking Water
37706
SC
99006
rl RIP] AP
GA7F')7

.1 r vv Y i Hnaiyucai nequest u®cum` ent
` ,.,,PaceAnalytical ® The Chain -of -Custody is a LEGAL DOCUMENT. All relevant fields must be completed accurately.
j www.pacelabs.com Required Client Information: Section R
` Report To:
Required Client Information: Section A Page: r Of To Be Completed b Pace Analytical and Client Section
Company— - Copy To: Quote Reference:
Client Information (Check quote/contract):
Address Invoice To: Requested Due Date: 'TAT:
/) Project Manager: w�
_. i 1 t f J
- — P.O. `Turn around time less than 14 days subject to Project #: rr)
laboratory and contractual obligations and may result in a J
Project Name: Rush Turnaround Surcharge. Profile #:
Turn Around Time (TAT) in calendar days.
Phone Fax _ _ Project Number: Requested
Analysis:
�+ `
Jecti®n D Required Client Information: Valid Matrix Codes ODE a Preservatives .
DRINKING WATER DW w w2 n.Z
�` t ' ®
IL
GROUNDWATER GW
SURFACE WATER SW
❑
O
o-O
Y❑
z O
w 1--
-
WASTE WATER WW
X
w0
~ w
'o
One character per box.
PRODUCT P
OIL OIL o�
¢
E m
��
COLLECTED
J J
2 L)
o
START
END
(A Z, 0-9 I.
WIPE
mC%I
�
C Q
O
CO
O
cis
—
Sample IDs MUST BE UNIQUE
AIR AR
OTHER OT
C
C
CO
cli
N
DATE
TIME
DATE
TIME
_
_
=
Z
Z
2iO
Remarks Lab ID
TIT
r
Temp in °C
`,<
Received on Ice;
Y/N
Sealed Cooler
A
Sam]ples Intact
,Y'
Additional Comments:
1;
r.
-11 _ 1
SIGNATURE of SAMPLER:-- DATE Signed: (MM / DID / W)
i
SEE REVERSE SIDE FOR INSTRUCTIONS Form C0001 Rev. 0304

TOWN OF OLD FORT BIORESIDUAL HANAGEKENT FACILITIES OPR LOG
DATE:
lbs. of dry wt. lbs. of lime Temp. Fo
Solids from gpm to Solid to Sludge Lime feed Per lb. of of Final Prac
Time Digestor belt press /Lime blender rate lbs/hr. Sludge dry wt. in heat bi
0700
�(
e 12
L3 G Or
0800
U� 00-7
L
G' 1 C - lc� ! /
�� C
iirl D ilf hl
^
0400
r
2c)qr
1000
1100
- `e l �c%i�J
Ij2�
.1
1200
j
iJA
e he-- `h - 3
a7 6
1300
/
-2
2 06
1400
1500
1600
1700
1800
,-
2- S
��
1900
2000
2100
2200
2300
?400
Solids
from Belt Press
I 1 %,1
% Solids of Final Product)
T of Final
After 2 hrs.
Time off Belt
Time Analyzed
of Sample',
OPR
roduct
�9-3
LTempo
3 of Final
After 22 hrs
Time off Belt
Time Analyzed
Temp Co of Sample
OPR
-oduc t
tal Vol.
of Bioresiduals run dry wt. lbs.
'3 '?i.
Total Vol. of Lime Used lbs.
3�(G,`
tal Vol.
of Bioresiduals + lime + moisture
in Tons
udge Meter reading at start up
At End of Run
l !
me Meter
-Tn i i- TT—
reading at start
T.m 011 1 1 7 r A
up t,t 1 -r
At End of Run

Ll
TOWN OF OLD FORT BIORESIDUALS MANAGEMENT FACILITY OPERATIONS LOG
DATE: 3 -- Ll - 0 L4 PERMIT*: W00011260
7—
TIME
% SOLIDS
FROM
DIGESTER
GALLONS
PER FE
14!h,
FROM lloof
DIGESTER
LSS, OF DRY
WEIGHT
SOLIDS TO
BLENDER
LIME
FEED
RATE
LBS./HR
L B S. / L I N7 E'7T
PER
LBSJDRY
t/VT. SLUDGE
TEA UP7 F
PV.
Kv,
INLET
TEMP. *F
P.V.
OUTLET
0930
20
-3(,,-7
2�
3
1000
-g
J
1030
i too
-2 0
1-7 ?
1130
1200
c)
-7 1-1
c 0
1230
Ll
1300
1330
vili
1400
(a
/-79
1430
09
1630
cl
1630
1700
1730
1800
1830
1900
1930
2000
5
..........
/t
SLUDGE @ START: 3& F-ta," —t,..QP SLUDGE @ ENDb5 " Fvn --4) TOTAL GAL: 7S C,
SLUDGE TOTAL DRY Wr LBS: 2 3 3 1
LIME @START: LIME Q END: U (� Z3 TOTAL LESS: - 3 Ll c)
% SOLIDS FROM BELT PRESS: R ,, --% SOLIDS OF FINAL PRODUCT;. S-0, (-) -
TOTAL VOLUM, E OF BIORESIDUALS + LIME + MOISTURE IN TONS: 5.9-3
AFTER 2 HRS AFTER 22 HRS.
FINAL PRODUCT PH:
TIME/DATE COLLECTED:
3-L(-OBI
0 0 () 3 -
TIME/ELATE ANALYZED:
-.3- Ll
S-c.
TEMP. *C OF SAMPLE:
2- 3-0
TEMP. CORRECTION TO 25* C:
OPERATOR INITIALS:
IV6

cc 0 f-f
k ­­ 7",
TOWN OF OLD FORT BIORESIDUALS MAMM37EMENT FAXILFTY OPERATIONS LOG
DATE: 3 -- ' - 0 '1 PERMIT V: to 0011260
SOLIDS,
LLONIS
LS. FDRYLIME
LBS.1-11ME
7 TF -
TEMP.
Mi F_
E 4".
TIME
FRO
PER HOUR
WEIGHT
ILBS,/,4R
FEED
PER
T
P.V.
P.V.
DIGESTER
FROM
SOLIDS TO
RA71 E
LBS,/DRY
INLET
OUTLE:T
DIGESTER
BLENDER
— - - - - - - - - - - - -
INT. SLUDGE
1-0856
0900
3 q
0-930-
0_6 T__
(000
J 7c7
C90
1 CIO
/71
(a cl c)
,To—o-
4� C)
1230
1300
Z-
1400
1430
500
1530
1600
1630
1700
17310
F I Boo
11 E3O
1900
1930
.2000
4z
S'-,'Ar,7 O�3'5'
s 70 P III 75b
SLUDGE @ START-,:- SLUDGE @ END: 5 TOTAL GAL: 0
SLUDGE TOTAL DRY WT LBS: �qoj
LIME 0,START: LIME@ END.--/ 3 2 13 TOTAL LBS: 3 3o Lt
%SOLIDS FROM BELT PRESS: 16,q %SOLIDS OF FINAL PRODUCT:
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS-, to
AFTER 2 HRS AFTER 22 HRS.
TFINAL PRODUCT PH:
TIMEMATE COLLECTED:
12-1-17
0/-
TIMEMATE ANALYZED:
TEMP. "C OF SAMPLE:
TEMP. CORRECTION TO 26" G:
0 - to
OPERATOR INITIALS:
:!wI-
7

TOWN'OF OLD FORT BIORESIDUALS MANAGEfifiENT FACILITY OPERATIONS LCW---
DATE: 3 — / & - 0 Ll PERMIT;g: W0001 1260
TIME
% SOLI S
FROM
PER HOUR
—6 —,,77
LBS. OF DRY
WEIGHT
7 1 �t*
LIM
FEED
T"§,' _� TFR_
L �. L Ef E *F
PER P.V.
P. f, i
DIGESTER
FROM
SOLIDS TO
RATE
ILBS./HR
LBS.IDRY INLET
UTLET
DIGESTER
BLENDER
T. SLUDGE
0800
08130
—co 35- .
0900
& i S
.2 p 0
0930
19-2.
1000
(clLf
1030
57.9-
101)
5 5 5-
IS-7
1200
5
1230--,-
_5 _�j
54 i
f
1300
5,15-
16,
I Z
1330
5 L4
1400
Lq
1430
f
1530
1630
1700
11
1730
18,30
1830
1900
1930
2000
STA97 0-7��O
5TJ P /'700
SLUDGE QD STAR: 28' SLUDGE @ END: -7 a r TOTAL GAL: 3 3 0 0 ()
SWDGE TOTAL DRY WT LBS:
LIME Cg START: 2_'�;'_ LIME @ END: 24 0 7 /&,B- -1 TOTAL LBS: 5 2� Li
%SOLIDS FROM BELT PRESS: 15,30 %SOLIDS OF FINAL. PRODUCT: 5/, 34
I-OT,il',L VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS:
AFTER 2 RRS AFTER 22 HRS.
F114AL PRODUCT PH:
12, 1-1� -
_3�1'
TIME/DNFE COLLECTED:
0 PI' 3-1&-01-f -
0,31,q- 3—f(o_ocf
TIME/DATE ANALYZED:
o 7 3- 04
0-7 0 3 - OL/
TEMP. *G OF SAMPLE:
21.6- 1
TEMP. CORRFrTION T5_25* C:
C), / 0
OPERATOR INITIALS:
VI-Ij
P AA� I
U

TOAUNN OF OLD FTY-71
THMIE RFROP,43 WE
79DUALS MANAGEMENT F Al-ClUrif OPERA-HOwS LOG
PERNiff 9: VVQ00l -12(36
S. OF DRY,!Llrk'.fiE L JUNIE �TEHRAF'. 'F ENIP'11
9
tj v D V A. IiO RVVEIC"FIT PFEE PER IPV
0 ! SOLIDS TO RA- F E LBS--,./DRY I M L. k--- T (XJTLFT
.s
t ER BLENDER gLss.mR kh,,n-. 13LUDQYE�
M -7
SE- S-
Cl
0930
1000
IQ310 39'
J-9 6
-112-
S-,
1200
-71
1,330
!To C)
1500 J-� 5-
-17 00
1800
1830
Sm
1930
vetom 16 p
f* 7 If -00
E@D END: TOTAL (37A .
SLUDGE @) ST/V�7- -29 --SLUDG L- 2
SLUDGE TOTAL
UNME @ END: TOTAL LBS:
UNIE @ START: 0 3 6
%SOLIDS FROM BELT PRFSS:-_-j_6j­-,4 SOLIDS OF FINAL PRODUCT:
TOTAL VOLUME OF WORESIDUALS + LjjVjE + MOISTURE 11\1 TONS:
AFTER 2 HRS AFTER 22 FIR&
FINAL PRODUCT PH
TRV',E/[7VkTE COLLEC-l'ED.
AHALYZED: o 5'-0 2
E-sMull Rrt'§ OF SAMPI"J_4E-
0
2 1.')
/0
17 7

TMPVN0F 0"Ll) FOR SlOiRE-SiDUALS OPE' ATiONS LOG
PER'Naff -�PWQOC 11260
P!TIMF
,I:-Rollq
IPER HOUR WEIGHT
FEED :PEA
lp v �p
DIGESTFI'FROW'i
SOUDS T
J���6T.E
Y
­
I iJz�T OUTLET
a
=o
r
IDIGES tIER BLEKIDER �LJHRWT.
U;,SS.iDF
JLU
G
coo
0930
M111-L
J__1
Itio 0
Soo
1230
I 3oo
L 2,�oq
1430
1530
,PTO
i 7 ILI U.
�(AC- -1 �0-7,,l �';_
SL_UDGE @ STA.R7: SLU136E DE NC: -----TOTAL. CL...3 3 0 0 0
SLUDGE TOTAL DRY WT
'I ME @ START:__- ILIME @ END:
LBS
% SOLIDS FROMI BELT PRFSS: cl/oSOLIDS OF FINAL PRODUGT: 14q"?
TOTAL VOLUP4E OF PMORESIDUALS. + LIME + WiSTUREM TOMB:
;rA,I--TFR 9 PIRS AFTER 22 HR5.
I FINAL PRODUCT PH:
3 9
-ATE COLLECED.
0 914�: 0 Lf
L4 -
f RiE76EFt Fff- -A-HALYZe n-:
-0
6--)410 t4
TEMP, 'C OF ISAMPLE:
2 1.
TEMP. CORRECTION TO,215* C-.
- 01 IL_
nPERATOR MITIALS-
5 DSO

TOWN OF 01-D F�$IRT BIORESIDUALSIMANAGEMEN T FACILITY OPERATCONS LOB
DAT E. PERMIT 9: VV0001 1260
TIME
% SOLIDS
FROM
DIGESTER
'Er i�
s
PER HOUR
FROM
DIGESTER
6 R Y
WEIGHT
WEIGHT D_ To
SOLIDS
SOLIDS TO
BLENDER
ENDER
BLENDER
f IRA LBS./LIME TEMO *F 'F
LIME TEA
FEED PER P.V. P.V.
RATE LESS./DI lfqLF:ri OUTLET
RATE
LBS 3El
LBS./HR WT. SLUDGE
cl cl
0800
0830
1100
57
11-30
-17 3 A
1200
SI 0 1�2 7 -
1 -7
300
1300
0
L4
1430
1500
1530
1 630
1700
1-73Q
1800
'1830
1900
1930
2000
's 0­7 ti *. 9-
5rolq I � it,,
SLUDGE START- SLUDGE @ END- q -1 OTAL GAL: _� 6 00 0 -
SLUDGE TOTAL DRY VVT LBS:__35 73_
LIME @STIART: LIME @ END: TOTAL LBS: _Sz Ll 3
% SOLIDS FROM BELT PRESS: 16.2- %SOLIDS OF FINAL PRODUCT: L) I-L
TOTALVOLUME OF BIORESIDUALS + LIME + MOISTURE ilk TONS:_ /6.2+3
Ar-TFR ? HR-S AFTER 22 FIRS.
PRODUCT PH:
7T_3 Cf
2-FINAL
TIME/DATE COLLECTED:
TiME/DATE ANALYZED:
I I
TEMP. *C OF SAMPLE:
ITEMP. CORRECTION TO 25- C:
C9,1 z
OPERATOR INITIALS:
f� _-AN _1Aff'

TOVUH Ow OLD FGRT 0WRESIDUALS WIANAGEPMENT 6 -AC14LFVFY OPEff"Wf sNWLOG
FROM
D R Y "CRAFff
L5-SJLMf_- "
TMrV
WE-1MV-9
FIME
PER HOUR
pi'VVEIGHT FEED
PER
P.V.
P .V.
0800
F_,'3
DlGTER
2.
�P2 7 r
FOMIR
DIGESTER
SOLIDS TO RATE
IBLE[VEDER LBUHR
LBSJDRY
Aff. SLUDGES
OUT LET
0830
ill&6
1-73
-71
.1130
1200
S30
5 3 30
1,71
01
177
/7L(
t Ac
---
1300
-1330
30
1
77
17S-
1 1.400
18- 9_1
1430
1500
'i
1730
S"29 S_
L
—J
1830
i got)
15
1930
1
1*1
2 001
S TAW. -7 0 9"'0
pcU,.4) oq4 5-
SLUDGE Ogg START-, 2 7 SLUDGE ENE : ".__TQTFps_ CAL. S-0 0
SLUDGE TOTAL DRY WT
UME CcvSTART: 3 LIME @ END:
JOTAL
Kira SOLIDS FROM BELT PRE-Ss:._L2e_V'Z 9/o SOLIDS OF FINAL PRODUCT, AA
TOTAL. VOLUME OF WRESIDUALS + IJME +
AFTER 2 HRS, AFTER -42 FIRS.
FINAL PRODUCT PHI:
ITv,jiEjc.)jvrE- COLLECTED-
I
0940 L4 _�La _014
oc) Lie)
TIMEMATE ANALYZED:l
TEMP. *0 OF SAMPLE:
TEMP. CORRECTION TO 28* C--
OPIE-RATOR INITIALS:
1 > I '-l­2-(5,ofj
2
J Z_
Lt
- &,To

MONTH /YEAR: F& � zoo q
CALIBRATION
BUFFERS
DATE, TIME
COLLECTED
DATE, TIME
ANALYZED
TEMP
*C
PH
St. UNIT
TEMP
CORR
TRUE
PH, S.U.
TIME
CAL.
®PER
INIT.
12.45
2-2(6- /,5-60�23,0
12,lo
-0.0(.
12,5'1
/0,,�)
12
Z 5,
o S 60
;--2- 3,
)'75-0
_L
1.(2,
21 -
112�59
-0,/&
2:q 1-/
0? 1 t�
0
O'�-690
7p
Elf
/0, 0
12-
-:7-4-6
e'?61
93, D
1.2, �o
2, �Z'5'
0
%(4
��/D
/21
U.,
073
7 i '
10.0
1:2 -
170
:-23
logo(-)
3-2LI
0-11
/0,C)
12, li S-
A
xe
07/1�-
0
�-2'
0,//
l
0-730
)0,0-
12
071f0
1,
2.
-0,t7
0, 3 1
07'� 5-
/0-0
1,2, (1 1;-
09110
pl'22,36-
-Y-09V0
4-0,02-
L,�.3�'
/(91()
12- 111
LZ
-)ILI
/A'L�2
6 k
L—
I LI), o
/ -" I'/
)�7-j
-L2't'
12. Lj 30
7
12. 14`'
Unless otherwise indicated, pH meter is calibrated the same day as the sample is analyzed.
TEMP. CORR. = Temperature correction t® 25 deg. C.
Z-
0
D

T9vVN OF OLD F01IRT BIORESIDUALS MANAGEMENT FACILF1 Y OPERA iONS LOG
DATE: Ll I-) _,li
- N - c., -I PERMIT t WQ001 1260
TIME
0800
0830
oploo
DS
FROM
DIGESTER
GALLONS!
PER HOUR
FROM
DIGESTER
LSS. OF DRILIME
WEIGHT
SOLIDS TO
BLENDER
LBS.ILIME TEMP ',F
ffED PER `P.v_
IRATE LBS./DRY I INLET
LBS.1HR WT. SLUDGE,
.. TEW-717�,
gp.v.
OUTLET
"L J L
1 -70
0930
71
1000
1030
9171
go
/ 7 9
I
11,00
f_a1130
Z_
61
A
1.200
1230
-7
1300
T_
1-7'
)7 ci
1330
6
i 70
-7
140
S
1`71
j 7 __3
1430
1 -1 Z
03
I
1t101530
1.91-c
174,
030
700
1736*::�
'12
1800
1830
i9oo
2000
S 7AP-7 0'-73<;-
- ---------
0 __0
SLUDGE @_ p START: SLUDGE @ END: TOTAL GAL. 3,1
SLUDGE TOTAL DRY WT LBS:
LIME @ START: _LIME @ END: TOTAL LBS: 73
% SOLIDS FROM BELT PRESS:_ 63% SOLIDS OF FINAL PRODUCT:
TOTAL VOLUME OF SIORESIDUALS + LIME + MOISTURE IN TONS:
AFTER 2 HRS AFT ER 22 HRS.
FINIAL PRODUCT PH:
1,2. 14
2.4 3
TIMIE/DATE COLLECTED:
0936 LI%IV- qL
41-lk-o
'TITVlEIRATE ,ANALYZED:
TEMP. *G OF SAMPLE:
;L 3. 4)
TEMP, CORRECTION TO 25" C-_
�oel
OPERATOR iNITIALS:
S L U

J
TOWS OF 0, LD FORT BIORESIDUALS MANAGEMENT FAC&IY OPERNFIGNS LOG
ITHAVIE
iF/l, —SOLTEDS I G111-TIC! 1 iAS ILBS. OF DRY
I
111-IME LBS.111-111"WE ''F ITEMP. F
ff'MF�r
'FEED EPER.
om PER GHT
_FR 14 0 Ll R I VVE - i
'r'C'u % P.V.
jpm.
C-1 G E ST E Rl F R C, 114 ISOLIDS To
11L� E R A
IDICESTER IBLENDER
RATE 'LBS/DRY 11 NI L E
�AATE
�LBS'.i[R IV VT S L I rij G E
rLET
. 0 37o
Z Tot:_�
Goo
IS-7
1030
-5 5-
jg-
113-0
Ll 1)
IE-0
13UG
1-7A
1330
'1400
I
do q 0
i630
1700
1730
0,
"1110
-------------------
Tl�
oill Z &5-() Ll Ll 0 = off
SLUDGE QSTART: '_ Ic SLUDGE @ END,-1-3 0 TOTAL GAL� 3 iii1/ o
SLUDGE TOTAL DRY WT LBS: , 31
LIME @ START: LIME @ END: -rOTAL LBS:
% SOL-IDS FROM BELT PRESS: 17. / —%,'-,OL;DS OF Flfl.IAL PRODUCT: LI-7.6
TOTAL VOLUfifiE OIORESIDUALS + LIME + WIS TURE IN TONS. IR, 7 Z_
AFTFR 2 HRS AFTER 22 HRS.
HINIAL PRODUICT PH-
Ll
j 2. 3
TIME/DfiVrE COLLECTIED.
TiMlEIDATE ANALYZED:
TEMP. *C OF SAMPLE:
TEWW. CORREG110H TO 25— C:
5-5-o-
0. C)
0
P_ -1•0
C). 0 C9
OPERATOR lftNrl IALS:
Nn
"q

TOWN OF OLD FORT BIORESIDUALS MANAGEMEMT FACILITY OPERATIONS LOG
DATE: 5`11-OLq PERMIT #: W0001 1260
1% SOLIDS RGALLONS ILBS.OFDRY ILIME . ILBS./LIME jTEMP. �FjTEMP. *F
ME FROM PER HOUR %EIGHT FEED PER P.v. P.V.
DIGESTER FRO ISOLIDS TO RATE LBS./DRY INLET OUTLET
cl)
S TA iz, 7 0-2 3 0
0830
s- 5- .A
I I (P. 0
0900
L-I -3
0930
1430
19 2-
1000
j -76)
1 1�,Li
1030
—0
/79-
1100
q 10
170
1130
Ll zlo
i 67
(-?L(
1200
173
/ -17-Z-
1230
C3
1 -7
7 -L
1300
1 &1;-
1 *7 0 .
1330
L4 S
1-76
1& 1
1400
4 L) f)
I & �
I ? -7
1430
rst O
it
/ '7 1
1500
z6L
1530
1
1600
1630
1700
ec 0,71t r 0 R)
1730
L
1800
1830
22
nwz
1900
1930
2000
OF cw?wAt<
SLUDGE @ START:
SLUDGE Q END: GAL: '3 6
SLUDGE TOTAL DRY WT LBs: 2 0/ 9 o
LIME @ START: 20333
LIME @ END: A, �) a% TOTAL LBS:
Ll 7 9,5::�
% SOLIDS FROM BELT PRESS:
- & % SOLIDS OF FINAL PRODUCT: L-1
-7 /1
*
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: �,lq
F 3 -wnZ613 210MAAM oZ
IFINAL PRODUCT PH:
4
):2
TIME/DATE COLLECTED:
0930 3-11-0L/
0130
TIMEIDATE ANALYZED:
5i:.�
TEMP. *C OF SAMPLE:
2Q. )
TEMP. CORRECTION TO 25* C:
o.ro-' 0
OPERATOR INITIALS:
<LV
'3C-LT PR>67.55 SL P0/4 P C rc [Z o u 7 rz f),;-;
fr
t-Lo,&;D C TCel4 bvd 13 -\.5 o P- wC, D
I

1-11445!'
TOWN OF OLD FORT. BIGRESiDUALS MANAGEMENT FACILITY OPERAT IONS LOG
DATE. �- - 2 27, - C) (4 PERMIT #: W0001 1260
HOUR
FEED PER*-""- P.V. P.
DS TO RATE -LBS./DRY INLET oul
' I R -"" IWT. SLUD DE ... ILBS./HR GE!
HT
1 0830 1 i i I f � 6- 5-- 1 /. 9 0 1 19-0 1 9 4 i
1000
1030
1100
1130
1200
1230
300
1330
1400
1430
1500
1530
1600.
1630
1700'
1730
1800
1830
1900
1930
2000
57A IZ 7 0 � 0 0
Ll & 5- 17,7 --li—z
—L�) 1'7'7
ilo Itl 1: 1J
�j :3 6) 1-7q
5-
!.±30 L,'7 17
�L 36 -- - J 7 Zor,
14 30 J I-/
L le-
e7
L7
h
SLUDGE @ START: SLUDGE Q END: 9/ TOTAL GAL: , 2 Ll S-- CD
SLUDGE TOTAL DRY WT LBS:
LIME @START: ;t I Z LIME @ END AT Ze , & 5-_TOTAL LDS: 7
% SOLIDS FROM BELT PRESS: 7. 6 .% SOLIDS OF FINAL PRODUCT: LP %7
TOTAL VOLUME OF BIORESIDUALS; +11ME + MOISTURE IN TONS-,-- 6. ILI
ya-019W�1
FINAL PRODUCT PH-
I )-.VR;
t 2.14
TiME/DATE COLLECTED:
t"jo g-.2-1>-04-
03()
TIME/DATE ANALYZED:
ig o 2 5- - ?��- env
0,735- ; -a(o-dl
TEMP. *C OFSAMPLE:
Z-
'2Cam. 0
TEMP. CORRECTION TO 25* C:
0 3
6.0
OPERATOR INITIALS:
4�CDLT IPRCS-S SLUD6( P014 4A
& 41 'D C T� ,e//l WZ73 i,� Y A," 0

TOliffiN OF OLD F0fZlr BtOftE IDUALS R&4NAGEMENT FACILITY OPERAVONS LOG
DXTE: .- IR- , E� PERMIT #: W0001 1260
I,—,—
V IAP
4% SOLIDS
LLONS L65. OF DRY
PER HOUR WEIGI IT
LIME LSS. EMP-72,
�l /LI Tf F Fff-MENWIP-77"l,
TPI P.v�
FEED PER Pv.
-1 iE
'FROM
LIB_
Ll _
F 800
IDIGESTER
FROM SOLIDS TO
DIGESTER BLENDER
RATE LBS.IDRY INLET JOUTLE-r
LBS,./HR INT. SLUDGE
8 3 0
0
0930
o
1100
1-77 1
1500
1. 11:30
1200
1230
1,3-0 t77
6-0 1-7 -7 V77
L)
133T
4 '7 1-7 -7 1
1400
1430­
1500
1530
L4 6 5-
bi le
1.600
1630
1700
If
1730
.1800
1836
10
_L —bk
1900
10, /_ V 0-n
ze It 1.j�6 , I
SLUDGE @ START:_2 SLUDGE @ END: TOT/' L GAL:_35_614 0
- 'S60 SLUDGE TOTAL DRY VV Tf LDS:- 3 -7q
LIME @START. /- -LIME @ END,_�3j_" f ___j0TAL LBS:
%SOLIDS FROM BELT PRESS: % SOLIDS OF FINAL PRODUCT,
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS., 0. 2
AFTER 2 HRS AFTER 22 FAR a.
FINAL PRODUCT PH:
TIMEIDATE COLLECTED:
TIMEIDATE ANALYZED- 0 Y
TEMP. OF SAMPLE- 2 I-�- ;2 3, 0
EMP. CORRECTION TO 25* C: o C)
jaffB�TqR WT�ALL
F rZ
L 0"D 0 L),O
A5 77-)

(o - 29 - 0 L--(
TOWN OF OLD FORT ll�'BIGRESIDUALS MANAGEMENT FACILIrY 0PERKFH)N8 LOG
DATE: PERMIT S: W0001 1260
G,'reGA9C-V Aq-
6667 P1'1�5 1-
j,jMZ_7 j)9l_lV&t241
qv, pAlFfj *7
PSI AIEWC
TIME
N-P-MIGALLONIS BS. OF DRY LIME LBS./LIME
Ala SQ On If D SQ S
FROM PER HOUR EIGHT FEED PER
L � H
DIGESTER FROM SOLIDS TO RATE LBS./D.RY
OL S T
LF
I 8L_ 1
DIGESTER ENDER LBSJHR WT. SLUDGE.
TEar-W. MP. �F
'F r P.%
P.V. PY,
INLET OUTLET
ot
1 1
01300,.
0830
0900
0930
203 /95-
1000
Silo
I o3o
1100
S 2
1130
t4 IK 1
1200
L4 %-o
1230
L4 -7 5-
Sr
1300
14 4
1330
Ll & �
1400
Lt. C4
1430
LALK
1-7-3 f-79
1500
�lT
1630
600
1630
5-1
-
1700
- _!
1730
ibdo___
1830
1900
1930
2000
S'sAe-7 OV;jo
it
SLUDGE@ START: SLUDGE@ END.- —TOTAL GAL: 3 300 0
SLUDGE.TOTAL DRY WT LBS: 1 q 7
LIME @ START: LIME @ END. � 5 -1 OTAL LBS: 2-
%SOLIDS FROM BELT PRESS, J'jr'Ll % SOLIDSCIFFINAL PRODUCT:
TOTALVIOLUME OF BIORESIDUALS + LIME + MOIST URE IN TONS: (6-11
AFTER 2 HRS AFTER 22 HRS.
FINAL PRODUCT PH:
TIME DATE COLLECTED.
12. t4 V
69 &_ i -OL(
12.5-1
0-,)LI(3 a -,xl)-at
TIMEIDATE ANALYZED:
it 55
� .0- oy.
TEMP. *C OF SAMPLE:
2 �- Z
2,3.-57
TEMP. CORWECTION TO 25"' C:
0. 0 0
—0-05-
OPERATOR INITIALS:
6.41_Lo,m> 9L/ ,llt�:A-50P-FV6

I Iz
TOW104 OF OLD FORT BIGRE WUALS MANAL GENIENT F-ACiLITY OPERALTEGNS LOG
DATE: PERIV.,IT #. '010011260
%SOLIDS
GALLOTWIKS LBS. OF DR E
IM,
-0.0-11tilE 4-11 EMP. "F
'TEIMP, *F
ITIWIE FROM
PER HOUR EIGHT FEED
PER P.V.
gI6T{k�..E-
p.V.
DIGESTEFt
FIKIMA SOLIDS 170 RATE
CI
LRS.. Y 1-
' OUTLET
!GEST E{BLENDER LBS.IHR
,Arr. rD, c-
low
Z�
0930
1000
f--
It 1,00
'6'
Z
17 L4
S7
1230
"70--
14-00
1430
1600
11530
_-LA-L
1600
_L_4_1�
16-30
-1-36-
1730
1800
-T87qo—
11-1110
1
------ - - - - - - - - - - -
2000
� T,,vrr--f 09-00
SLUDGE @ START: .2 (4 -SLUDGE @_ END:___J_l TOTAL GAL:_ 30360
SLUDGE TgrAL DRY 101T LBS-.- 3 0 S_
c* 0 TOTAL LBS.- 3
LIME Q. START: 0 .—LIMIE @ END:,jV.J
% SOLJDS FROM BELTPRESS:__['6. . % SOLID'S OF FINAL PRODUCT: iq
TOT,fi& VOLUME OF StORESIDUALS + LIME + W101,11' 7TURE IN TONS: 7. 1 1�
AFTER 2 HRS AFTER 22 HRS.
FINAL PRODUCT PH:
12- 7-
TIME/lATE COLLECIED:
TIMEIDATE ANALYZED:
I Zo 1,7_13-oci
0-9W) 7-t 2 -0
C OF SAM:
TEMP. ' SAMPLE:
TBAP. CMDREC710K? TO 25C:
7- S7. Lt
0
23.0
A4 --rz o u
4 g/�Fj) 2 16t7
611 c),�
To

L 1 jv, C GV) I P C fU,74S&O 1,13- - I Q 0 Y
TOWN OF OLD FORT BIORESIDUALS MANAGEMENT FACILrrY OPERY-ATIONS LOG
DATE: PERMIT #. VVQ001 1260
UTIMAEFROP411
% SOLIDS
SOLIDS
or 3 :�E-
DI�GESTER
GALLONS
PER HOUR
FROM
DIGESTER
LBS. OF DRY
��nl)F 1)
WEIGHT
SOLIDS TO
SLENDER
LIME
SEED
"RATE
"RATE
LBS./LIME
PER
LBS./DRY
WT. SLUDGE
T E Noll P. F
V-
P.V.
INLET701JTLET
T
T MP. -F I
PE�
P'V.
OU I
0800
0830
I
S, '7 15-
ogoo
0930
1000
1 030
L) L/ 0
1100
cto
1130
L 15
1
7
iz-
1, 33
�-
1230
L-1 r
j S-Ll
17 q
13�i0—
1 S-0
is_
1330
1430
1500
1530
C
y
1630
1700
1730
1800
1830
1900
1930
2000
r --
s c ) � 0
SLUDGE @ START: ✓ SLUDGE @ END: TOTAL GAL:— 0 Lq C)
SLUDGE TOTAL DRY WT LBS:
LIME @ START: 0 LIME A- END: oq 419 TOTAL LBS:
% SOLIDS FROM BELT PRESS: 17. (, % SOLIDS OF FINAL PRODUCT:.- - _ H ?--
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: 6.31
AFTFR 2 HRS AFTER 22 HRS.
FINAL PRODUCT PH:
TIME/DATE COLLECTED:
0
TIMEIDATE ANALYZED:
I -a- -,I tt - o t
675 0 � �-.: - �i
TEMP. *C OF SikMPLE:
---�• �-
TEMP. CORRECTION TO 25* C:
67-00
-
OPERATOR INiTIALS:
o u 0 �Z)3 e
C--SS 5LU-00' PO4P tAA't-:�-Te
UP- I q , J6 D

/() - 5- -- 0 9
TOWN OF OLD FORT BIORESIDUALS MAMA GEMENT FACILITY OPERATIONS LOG
DATE: PERMIT #: W00011260
ITIME
0800
—578 36-
% SOLIDS
FROM
DIGESTER
6�)��--
1
IGALLONS
PER HOUR
FROM
DIG ESTER
LBS,'OF DRY
WEiGHT
11SOLIDS TO
BLENDER
LIME
FEED
RATE
ILBS./]HRWT.
mzw
LBS./LIME
PER R'
LBS.IDRY
L BS y
SLUDG E
TEMP. *F
P.V.
It L
INLET
TEMP. *7
P.V.
OUTLET
CUTLET
T
6
0900
0930
1000
10130
11100
r
Ll -7o
1130
Li -7 o
1200
i7,- Ll 0
1230
Ll
1300
1330
1400
16
94;
1-430----
1500
1530
1600
1630
1700
1730
1800
1830
1900
1930
2000
S--
- ,A17-7 OrSOrO
0 G C PO ?A r
SLUDGE@ START: SLUDGE @ END: &I TOTAL GAL: 2 ';-(D 8- 0
SLUDGE TOTAL DRY WT LBS: 2 -,3 (!' 9
LIME @ START: 3 Ll 9 0 LIME@ END: 9-- & 3 TOTAL LBS: 3 �7- 3
%SOLIDS FROM BELT PRESS: )7?�Ll %SOLIDS OF FINAL PRODUCT: Ll'c,O
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: -6-9s
AFTER 2 HRS AFTER 22 HRS.
FINAL PRODUCT PH:
TIME/DATE COLLECTED:
0 Lf
TIME/DATE ANALYZED:
I -q-ol(
0-7S70 )0-6-OQ
TEMP. *G OF SAMPLE:
2 q, 6
2,
TEMP. CORRECTION TO 25* C:
-
OPERATOR INITIALS:
L U'DC('- POA P A/1 t i 2.
o L)
ori-r-)
--A D C- TEekj 1,4jFt) -5o)atv6
D16J

/ () - 2 L/ - (D 1-(
TOWN OF OLD FORT BIORESIDUALS NIANAGEMENT FACILITY OPERATIONS LOG
DATE- PERMIT #: WQ0011 1260
'DRY E - -
LIM
% SOLIDS GALLONS LBS. OF DRY LIME
i E
Le&-/ V
LBS./LIME
TEMP. *F
TMM P. -
I
TEMP. �F i
TIME
FROM PER HOUR WEIGHT FEED
PER
P.V.P.V.P
PV
P,
LO7.
DIGESTER FROM SOLIDS TO RATE
LBS./DRY
INLET
OUTLET
14P
DIGESTER BLENDER LBS./HR
p
VVrl. SLUDGE
SLUDGE
08 0-
0930
1000
1,2
1030
V7
1,100
4)
1130
1200:
1230
1300
0
1330
1400
1_0
1430
1,70
/41-7
1500
n
16301
a 0 o
1
-1--si
1600
)01 1
16130
1700
1730
80-0
1830
1900
1930
2000
3-i'PiU2, ­7 C�ll "Q',- 10
SLUDGE @ START: 2-9 -SLUDGE @ END: —TOTAL GAL: -A 2, 0
SLUDGE TOTAL DRY WT LBS:_ 3 5'
LIME @ START: le)`R LIME @ END:_TOTAL LB a:
% SOLIDS FROM BELT PRESS: d-7, 77 % SOLIDS OF FINAL PRODUCT: 9 7
TOTAL VOLUME OF SIORESIDUALS + LIME + MOISTURE IN TONS:
AFTER 2 HRS AFTER 22 HRS-
tL
POW' Aft-; fc

TOWN OF OLD FORT 'WASTEWATER TREATM, ENT PLANT
LAND APPLICAT` OF BWOLIDS
FINAL PRODUCT PH'
N4011TH / YEAR:
[c7ik-!] U-1 R-; �: r 1-0 t-11
UFFERS
17P -ER
INIT.
�DATE, TIME
V�
COLLIECTED
ao 0
DATE,'TIME TEMP
ANALYZED "C
E
> IHI 35 Ig
PH
St. UNITCORR
j 12 1
TEMP
- T , RUE
PH, S.U.
tH, S.U-
TIME
CAL.
CAL-
r' =10. 0
.10.0
12.45
.710
7
10, C)
12-
/000
L/O
0
).2. 3 Z-
Ci? 3 5-
/0, 0
4
0,
071/0,25"0
.qL/
0.061
2 5 5-
/0-0
12,
c' 210
s --Z
+ 6
/,2, H 9
01V
/0,0
a
IQA-)
26, 0
4Y
1,2,eq-V
0130
/0,0
/Z
'ZK-
3-
-7 11S,3
#S
,'061
0--
-
1 A,AM
0715-
/0,62
1:2. 11C
\1
4
qL-1
C'
12, -S
7 /WL
/0,0
12. t(S--
_LL-61
_1,2,
-,Z
/.
jg7, 0,0
1�,,41ff
0-235
/I
0 07(4
-0,027
/2, --1
0-1.'-)(3
10.0
)2, 4 q
1Q1'J
-2- 5,0
_j
12, Z S-
-ao
12,2
0 730
10,0
7
0, 0
UJ4
L-2-4
-2
'9,-25 0750.2 .6
12. 'S7 -3
-o,o
QLO
0711
io-D
12. C/�-
v-2'1
/0 7
09 9 c5-,
10-5-
-0,01
1,2.L/L)
(),70()
10, C)
/0-5
075-0 25-,'0
Q23 9
k9l)o
le2.3�
0'790
1-0,c)
Q. Lt
'7L-/
io.-2V
�//0-2Y
j2i,;- 270
12,3'
b'71 0
19111'
VQ:2LI
0/ 4;-
j o 25 (T/S 23,t1
0
Unless otheNvise indiczated, pH meter is calibrated the same day as the :ample is analyzed.
TEMP. CORR. = Temperature correction to 25 deg. C.

T0V4N OF OLD FORT BIORESIDUALS MANAGEMENT FACILIrf OPERA IONS LOG
DATE: PERMIT;& W0001 1280
TIME
%SOLIDS
FROM
D I T:
IGESTER
L
GALLONS
PER HOUR
FROM
DIGESTER
L OF DRY LIME
WEIGHT FEED
SOLIDS TO RATE
BLENDER LBS. HR
LBS./LIME
PER
LBS./DRY
WT. SLUDGE
TEMP. *F
P.V.
INLET
TEiMP.'F
P.V,
OUTLET
0 08 00
800
c-
0330
IS, Lf
1030
i
Ll
0
i I":
1130
1200
7
1230
-7 1'
L/
1300
9 ' 7
--3
1330
'1400
Aq— 0
12
1430
e7
1500
s-
5L
115-00
1630
1700
e. lyy
1730
1800
2ff Tii
1830
1900
1930
2000
SLUDGE @ START: :11 13 SLUDGE @ END: 2,61( TOTAL GAL: Iq
SLUDGE TOTAL DRY WT LBS: -fT.�ST
LIME @START: LIME @ END: —I-Ik,-? V= I _-JOTAL LBS: Ll L/ (9 %,SOLIDS FROM BELT PRESS: / 7. (f % SOLIDS OF FINAL PRODUCT: L4 7,
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: '7M2 'ei-
AFTER 2 HRS AFTER 22 HRS.
---------- --
FINAL PRODUCT PH:
f2
L/
TIVIE/DATE COLLECTED:
it-LI.-OLi
// - t/ - o 9
TIME/DATE ANALYZED:
2
1/-
TEMP. *C OF SAMPLE.-
z 2.
TEMP. CORRECTION TO 25" C:
OPERATOR INITIALS:
L S t- u 'D C; 0/4 P

STJ Ip & 70 0 S.
Pe"21-4c't A 32o'
TOWN OF OLD FORT BIORESIDUALS MANAGEMENT FAACILiTY OPERMATIONS LOG
GATE-: PERMITA- VNI0081 1260
TIME
0800
% SOLIDS
FROM
DIGESTER
GAd.LONS
L S
PER H
LOUR
R
FROM
,aDIGESTER
I-B DRY
F DRY
1- BS 0'
VE H
WEIGHT
SOLIDS TO
BLENDER
LIME
FEEE
RATE
LBSA./HR
ILBS./LIME
/L ME
PER
LB dDRY
W. SLUDGE
T -F
1p
EMP.
P.V.
INLET
TEM
P.v.
OUTLET
0
1000
c;
21-
1030
iT Z L)
1
1100
1130
o
21--
/IS,
1200
iRl
1230
Z0 0
& fv
R li-
1300
01
1330
1400
T-
vat
1430
1500
1530
It
iWo
9 0
1630
1700
z2z
1730
�-/&
LL
-1
1830
1900
1930
7
:3 93 4- f zl*:�
SLUDGE @ START: SLUDGE @ END: TOT AL GAL: 3 eo�;f
T
SLUDGE TOTAL DRY WT LBS:- 3 3 -2
LIME@START: /L/,'I-Ll
4 LIME @ END: TOTALLBS: 5 Ot2
% SOLIDS FROM BELT PRESS, SI- - -2 % SOL*I6`S' bF FINAL PRODUCT: �6, I
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: l/. / I -
Ar-TFP 9 HRR AFTER 22 HRS-
FINAL PRODUCT PH:
12. 4 7 -
9 1-1
TIME/DATE COLLECTED:
0 1-1 7 - 0 LL
L► L-I'y
TIMEIDATE ANALYZED:
1)-17-04-
050
TEMP.'kC OF SAMPLE:
23,/
1.
TEMP. CORRECTION TO 25* C:
- 0,0&
OPERATOR INITIALS:
8cL)A'o ,mot,mot-j"�5 ., - tZ0 U 7, 0 c'q 1?- 1.3 e- a
-1-7- F1-2c-ss

C'j
-,j
TOWN OF OLD FORT 810RESIDUALS MANAGE ENT FACILITY OPERATIONS LOG
DATE: PERMIT #- W0001 1260
fj,S j:i) 6 i>.,:,) L
A L4601-f
r -
TIME
W60 -L I-D-S9 I-
FROM
DIGESTER
�GA ALLOW
PER HOUR
FRO110
DIGESTER
:'LBO OFM'D DRY
WEIGHT
SOLIDS TO
BLENDER
L I I Vi E
L W
FEED
RATE
LBS.lHR
-S
LBS./ 114,AE
PER
LBS,/DRY
S./,
IA
WT. SLUDGE
aIT-EMP.*F
Rv.
�V
INLET
lit L�T
TEMP. "F 1
P.V
OUTLET
OUTLET
�6
0800
:--�
0830
- 7.) C15L
cl
1'77
-0930---
1000
-7
1030
1100
1130
1200
1230
"1 cl
1300
5� Li
-T3�1 0
1400
i
C
14�30
1500
1530
1600
1630
1700
I ZZ,
1730
1800
830
1900
1930
2000
o Aj
SLUDGE@ START: 2 SLUDGE @ END: 7 TOTAL GAL:
��
SLUDGE TOTAL DRY WT LESS:
, - S
S: -
LIME @ START: '/9 LIME @ END: t? 9 TOTAL LBS: L 10
% SOLIDS FROM BELT PRESS: %SOLIDS OF FINAL PRODUCT:
TOTAL VOLUME OF BIORESIDUALS + LIME + MOISTURE IN TONS: � ! '3 Ll
AFTER 2 HRS AFTER 22 HRS.
F - INAL PRODUCT PH:
2,3T
TI[AE/DATE COLLECTED:
I
TIME/DATE ANALYZED:
SAM
TEMP. *C OF, i PLE:
vz I's 12----0
-1
')5.
6 �3Z 772-, -1 o , OV
TEMP. CORRECTION TO 25* C:
010 6
OPERATOR INITIALS: _
J177
-ALP--
5 S L 0
ou-7- or,-Dcre-
TD tec41-

aco�/
Annual Retort Review SOP
1. Annual Land Application Certification Form
• Was a certification form submitted? ieS
• Was land application conducted during the reported year? MO
• How many dry tons and dry tons per acre were applied? O
• Were the applications within the permitted amount?)N A
• Verify PAN if more than 10 tons/acre N
• Did it indicate compliance? y65
• Was it signed by the appropriate people? Y655
2. Monitoring
• Were the analyses conducted at the required frequency? 12ss"ijwt1 An4-1yS;s-V4! 7"c1,P-jZS; F{a n-y.e S
• Were the metals analyses reported on the Residual Sampling Summary Form?yes
• Were the results reported in mg/kg?yzS
• Were the heavy metals within ceiling concentration permit limits?*yeS
• If no, were the lab analyses attached? JY4
• Were all the required parameters tested?yet', 2�s�� �na��scS, -ru-P,
• Was TCLP analysis conducted? V e.5
3. Field Summary Dtd. fomT 4Ppi-Y 70 qNy F716l.B /N
• Were the land application events recorded on the Field Summary Forms? /0 �
• Was a Field Summary Form submitted for each field? AtA
• Were all the residuals applied to permitted land? kft
• Were all the residuals applied from permitted sources? N a
• Were the field loading rates for each metal and PAN calculated (year to date)? Nd
• Were the cumulative pollutant loading rates calculated? � A'
• Were the calculations correct? NO
• Were the PAN loading rates within permit limits? N
• Were the heavy metal cumulative pollutant loading rates within permit limits? N A
• Were the residuals applied on a suitable crop? NR
• Were the applications conducted during the crop's growing season? N
• Were the Field Summary Forms complete?yes
4. Pathogen and Vector Attraction Reduction
• Was a signed copy of the Pathogen and Vector Attraction Reduction Form submitted? YaS
• Did the form indicate the period of coverage, the residual class, and the pathogen reduction alternative and the
vector attraction reduction option used?VtS es
• Was the appropriate documentation to show pathogen and vector attraction reduction included in the report?
-r • Was pathogen and vector a rt a lion reduction demonstrated according to 40 CFR Part 503?
CLM fl I PrHuAeL4iv2 5 P-FPPo A-Or�ac+4,oA Y4sk- "I
5. Soil Tests
• Was a Standard Soil Fertility Analysis conducted for each application field? 1J11
• Were the soil pH's 6.0 or greater for each application field? Ofl
• Were the copper and zinc indexes in the soil less than 3000 for each application field? MR
6. General
• Was the report in the proper format?' e,5
• Were any parts of the annual report missing?
Was the report submitted on time? UPS
* Any violations of ceiling concentrations should be reported to Pretreatm nt for municipalities only.
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