HomeMy WebLinkAboutWQ0002349_Annual Report_20070209ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit#: WQ0002349 County: Mitchell - Year: 2006
Facility Name (as shown on permit): Town of Spruce Pine
Land Application Operator: Southern Soil Builders, Inc Phone: 336-957-8909
Land application of residual solids as allowed by the permit occurred during the past calender year?
® Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were
generated but not land applied, please attach an explanation on how the residuals were handled.
1) e
Total number of application fields in permit-
7
Total number of fields land application occurred during the year:
2
Total amount of dry tons applied during the year for all application sites:
70.9
Total number of acres land application occurred during the year:
11.7
Part B:
Facility was compliant during calendar year 2006 with all conditions of the land application permit
(including but not limited to items 1-12 below) issued by the Division of Water Quality. Yes" ❑ No
If no please, provide a written description why the facility was not compliant, the dates, and Ixpla n
corrective action taken.rn
�q
. Y
1. Only residuals approved for this permit were applied to the permitted sites. CD
2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil nn oftat F,
least 6.0 or the limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residuals during the past calendar year nd�hre o
(3) copies of laboratory results are attached. 0
4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached
5. All other monitoring was performed in accordance with the permit and reported during the year as rTqufr'ed
and three (3) copies of certified laboratory results are attached.
5. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the
Pollutant Loading Rates in Table'2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities).
7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were
complied with (applicable to 40 CFR Part 503 regulated facilities).
8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation,
prior authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of
violations are attached to include appropriate actions and remediations.
10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed
in accordance with the crop management plan.
1 l . No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12. All buffer requirements as specified on the permit were maintained during each application of residuals.
"I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true,
accurate, and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowin violations."
w4-�`O 7o uy ^� Y1/� `ti,N' e W 4 ' 0 ?
Permittee Name and Title (type or print) Signature of Permittee Date
Signature of Preparer*
(if different from Permittee)
' Preparer is defined in 40 CFR Part 503.9 (r)
'7
R F re of Land Applier Date
�(iifferent from Permittee and Preparer)
t- k��
-�„ ► iot4
ptocessin9 UnYL
lnformat10n
DENR FORM ACF (5/2003)
E',
1-,
ANNUAL RESIDUAL SAMPLING SUMMARY FORM
Attach this form to the corresponding Annual Report
Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form.
Ic
Permit Number: WQ0002349
Facility Name: Town of Spruce Pine
NPDES # or NCO021423
W Q#:
WWTP Name: Town of Spruce Pine WWTP
Residual Analysi
Sample or
Composite Date
Percent Solids
Arsenic
Cadmium
Chromium
Lead
Nickel
Selenium
Zinc
Data
Total Phosphorus
TKN
Ammonia-Nitroger.
d Nitrite
10-31-06
3.56
2.8
3
52
486
46
1.5
7
38
6.5
774
27,100
49,700
1400
62
Laboratory: 1) A&L Eastern Laboratories, n .
2) —
4)
5)
0n
Nrtrate an
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to .assure that qualified personnel properly gathered and evaluated t e information submitted.
r sonmeent for knowing wmg violat ons. am aware tht there are
significant nalties f su itting false information, of fines and imP
including the possibility
Signature of Preparer Date DENR FORM RSSF (5/2003)
ANNUAL METALS FIELD LUADIA(i aUMMAKY rUltivl-'
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Town of Spruce Pine Total Dry Tons Applied (Annual):
WQ0002349 Cation Exchange Capacity (non 503 only):
KT Feldspar Corp. Owner: Penland -Bailey Company
7.2 Acres Permitted: 7.2 Site #: SP-01 Field #:
54.88
SP-01
Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #):
Total
• •M
•.ENEEMENEENE
Annual Heavy Metal Field Loadings (Calculated in lbs/acre):
WPM
1 1'
000000�0000
1 1'
1 1
00000000000
1 1MR
71.it'iii�1:'
1 •
00000000000
1
...•
- .
00000000000
•'
m
l l
000000000�0
1 1
• yl
®
1 1 •
�00000000��
1 1 • •
••.
1
1
1
1
1
1
1
1
1
1
1
PI certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Sii4ture of Land A'ppfier Date
• See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Spruce Pine
Owner: Penland -Bailey Company
Site #: SP-01 A
Field #
Operator:
SP-01 A
Permit 9: WQ0002349
KT Feldspar Corp.
Acres Utilized: 7.2
Annual Dry Tons Applied: 54.88
Cation Exchange Capacity (non 503):
Acres Permitted: ' 7.2
o
� o
ra
Specify
Totals
Per
Acre
Solids
�' Tons Per
Acre
Residual
Sources
(Summarize)
' e
Cond.
Dry
Wet,
Moist
Inches
Preci p�
Past 24
Hrs.
Appli-
cation
Meth-
od*
Voli-
tila-
zation
Rate**
Miner-
ala-
zation
Rate
TKN
Ammo-
nia-
Ni-
trogen
Ni-
trate
and
Nitrite
PAN 1
PAN 2
Must Select
Crop 1 or Crop
2
*
Gal.
Cu.Yd.
Report
Totals
€ in Gal.
Crop 1
Crop 2
2-06
30,000
4166.7
3.56
0.61855
WWTP
dry
0
s
0.5
30%
49700
1400
62
18.8682
#######
Fescue
1
3-06
32,500
4513.9
3.56
0.670095833
WWTP
dry
0
s
0.5
30%
49700
1400
62
20.4406
#######
Fescue
2
4-06
82,500
11458
3.56
1.7010125
WWTP
dry
0
s
0.5
30%
49700
1400
62
51.8877
##44###
Fescue
3
6-06
70,000
9722.2
3.56
1.443283333
WWTP
dry
0
s
0.5
30%
49700
1400
62
44.0259
#######
Fescue
4
5-06
10,000
1388.9
3.56
0.206183333
WWTP
dry
0
s
0.5
30%
49700
1400
62
6.28942
#######
Fescue
5
6-06
30,000
4166.7
3.56
0.61855
WWTP
dry
0
s
0.5
30%
49700
1400
62
18.8682
#######
Fescue
6
7-06
62,500
8680.6
3.56
1.288645833
WWTP
dry
0
s
0.5
30%
49700
1400
62
39.3089
#######
Fescue
7
8-06
52,500
7291.7
3.56
1.0824625
WWTP
dry
0
s
0.5
30%
49700
1400
62
33.0194
#######
Fescue
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
12
TOTALS:
51389
As
Cd
Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.042728
0.04578
0.79352
7.41636
0.70196
10.02289
0.10682
0.57988
0.09919
11.8112
1413.546
1232.7081
0
Date
Ibs/ac
Current Cumulative lbs/ac
0.163028 0.12713 0.79352 98.0269 68.7521 0.40714 0.44978 3.92364 0.32277 110.165
0.1203 0.08135 0 90.6105 68.0501 0.38425 0.34296 3.34376 0.22358 98.3534
36 34 NA 1338 267 15 1 NA 374 1 89 2498
250
Prior Years Cumulative Ibs/ac
Permitted C. P. L. R.***
Pernut PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
� -/ -6, 7 *Application Method: S - Surface, IN - Injection, INC - Incorporation
Signatere of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)
AINNUAL 1v1LIALa r1JVLU LVL MUIV 0UlriiVatXi%a i'viv.a
Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report
Facility Name:
Permit #:
Operator:
Acres Used:
Spruce Pine Total Dry Tons Applied (Annual):
WQ0002349 Cation Exchange Capacity (non 503 only):
Unimin Co. Owner: Penland Bailey Co.
4.5 Acres Permitted:
4.5
16.02
Site #: U-02 Field #: U-02
Raeiriival Analvcic natn (Aeaw Metals and Total Phosphorus use mg/kz, % Solids use Raw Percent #):
•
11
Annual Heaw Metal Field Loadings (Calculated in lbs/acre):
•
W.1
I IT, 1 .
-
1 11 `
•.
`•
�� .••
1
1
1
1
1
1
1
1
1
1
1
�� •"
.-
"I certify, under penalty of law, that this document was prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gathered and evaluated the
information submitted. I am aware that there are significant penalties for submitting false information,
including the possibility of fines and imprisonment for knowing violations"
Sig6ture of Land Applier Date
* See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form
DENR FORM MFLSF (5/2003)
ANNUAL LAND APPLICATION FIELD SUMMARY FORM
PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD.
Facility Name:
PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE.
Town of Spruce Pine
Owner: Penland Bailey Co. Operator:
Site #: U-02 Field #: U-02
Permit #: WQ0002349
Unimin Co.
Acres Utilized: 4.5
Annual Dry Tons Applied: 16.02
Cation Exchange Capacity (non 503):
Acres Permitted: 4.5
S i
t e
Inches
Appli-
Voli-
Miner-
Ammo-
Ni-
Must Select
Gal.
o
Totals
%
Dry Tons Per
Residual
Cond.
Precip.
cation
tila-
ala-
TKN
nia-
trate
PAN 1
PAN 2
Crop 1 or Crop
p p
N
„ o
Cu.Yd.
per
Solids
Acre
Sources
(Summarize)
Dry
past 24
Meth-
zation
zation
Ni-
and
2
;.` Report
Q
Totals
Acre
Wet
Hrs.
od*
Rate**
Rate
trogen
Nitrite
Crop 1
Crop 2
i in Gal.Moist
5-06
25,000
5555.E
3.5E
0.824733333
WVTrP
dry
0
s
0.5
30%
49700
1400
62
25.1577
#######
Fescue
1
0
0
0
0
2
0
0
0
0
3
0
0
0
0
4
0
0
0
0
5
0
0
0
0
6
0
0
0
0
7
0
0
0
0
8
0
0
0
0
9
0
0
0
0
10
0
0
0
0
11
0
0
0
0
1121
TOTALS: 5556
As
Cd Cr
Cu
Pb
Hg
Mo
Ni
Se
Zn
P
PAN 1
PAN 2
Lime Applied
Annuallbs/acre
0.00461832
0.00495 0.08577
0.80161
0.07587
0.00247
0.01155
0.06268
0.01072
1.27664
44.6987
25.1577
0
Date
lbs/ac
Current Cumulative lbs/ac
0.13287832 0.17493 0.08577 28.3727 2.84454 0.2938 0.3169 1.71894 0.27554 50.7767
0.12826 0.169981 0 27.5711 2.76867 10.29133 0.30535 1.6562E 10.26482 49.5001
36 34 1 NA 1338 267 15 NA 1 374 89 2498
250
la •�S
LS
Prior Years Cumulative lbs/ac
Permitted C. P. L. R.***
Permit PAN Limit 1 st/2nd Crop
"I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a sySle111
designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are
significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations."
Signatur of Land Applier
-%-0
Date
*Application Method: S - Surface, IN - Injection, INC - Incorporation
**Volitilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0
***C.P.L.R.: Cumulative Pollutant Loading Rate
**** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered
into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF
DENR FORM FSF (5/2003)
ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUC I WiN rUtuvi
Facility Name: Town of.Spruce Pine Permit Number:
WWTP Name: Town of Spruce Pine WWTP NPDES Number:
Monitoring Period: From 1/1/2006 To 12/31/2006
lAn nVn Cn2 2i,% _ Dlnoon ;"riiratp IPvpl achipvP.d and alternative performed:
WQ0002349
NCO021423
Class A:
Alternative 1 ❑
Alternative 2 ❑
Alternative 3 ❑
Alternative 40
Alternative 5 ❑
Alternative 6 ❑
If applicable to alternative performed Class A only indicate "Process to Further Reduce Pathogens":
Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑
Beta Ray ❑
Gamma Ray ❑
Pasteurization ❑
Class B:
Alternative 1jS I
Alternative Z ❑
Alternative 3 ❑
If applicable to alternative performed Class B onl indicate "Process to Si nificantly Reduce Pathogens":
Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion
Anaerobic Digestion❑
If to alternative Class A or Class B complete the following monitoring data:
applicable performed
Pathogen Density
um er o
requeney
Sample
Anahtical
Parameter
Level in
F.xcee-
of
YP
Type
Tech-nique
imu
Geo. Mean
aximu
Units
2x 10to e6th
power MPN per
1635
2068
2548
MPN/g
0
7
grab
sm9221
gram of total
solids or 2 x 10 to
Fecal Coliform
the 6th power
CFU per Pjam of
1000 mpn per
gram of total solid
(dry weight)
Salmonella bacteria
3 MPN per 4
din lieu of fecal
grams total solid
colilorm)
(dry weight)
vPrtor Attraction Reduction (40 CFR 503.33) - Please indicate option performed:
Option 1 ❑ Option 2 ❑ Option 3 P§ Option 4 ❑ Option 5 ❑
Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑
No vector attraction reduction options were performed ❑
CERTIFICATION STATEMENT (please check the appropriate statement)
"I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have been met."
❑ "I certify, under penalty of law, that the pathogen"requirements in 40 CFR 503.32 and the vector
attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check
this statement attach an explanation why you have not met one or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the
system designed to ensure that qualified personnel properly gather and evaluate the information
used to determine that the pathogen and vector attraction reduction requirements have been met. I
am aware that there are significant penalties for false certification including fine and imprisonment.
Preparer Name and Title (type or print)
Signature of Preparer
Southern Soil Builders, Inc Dennis Key
Land Applier Name and Title (if applicable)(type or print)
Date Signature of Land plier (if applicable) Date
DENR FORM RF (5/2003)
Report Number:
R06307-8006 A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401
46381 Fax No. (804) 271-6446 - Email: office@al-labs-eastern.com
TO: SOUTHERN SOIL BUILDERS FOR: SPRUCE PINE
958 HOOTS ROAD
ROARING RIVER, NC 28669 NC CERT #257
ATTN: DENNIS KEY
LAB NUMBER: 44778
SAMPLE ID: SPRUCE PINE
REPORT OF ANALYSIS
copy: ZACH KEY
DATE SAMPLED: 10/31/2006 1230
DATE RECEIVED: 1 1 /3/2006 1400
DATE REPORTED: 1 1 /8/2006 PAGE: 1
Solids, Total (As is)
3.56
35600
100
JM
11/03/06
16:00
SM 2540G
Nitrogen, Total Kjeldahl
4.97
49700
100
JM
JM
11/06/06
11/06/06
16:00
16:00
EPA 351.3
SW 846-601OB
Phosphorus
2.71
0.57
27100
5700
100
100
JM
11/06/06
16:00
SW 846-6010E
Potassium
0.79
7900
100
JM
11/06/06
16:00
SW 846-601OB
Sulfur
1.55
15500
100
JM
11/06/06
16:00
SW 846-601OB
Calcium
0.53
5300
100
JM
11/06/06
16:00
SW 846-601OB
Magnesium
0.16
1600
100
JM
11/06/06
16:00
SW 846-601OB
Sodium
18900
1
JM
11/06/06
16:00
SW 846-601OB
Iron
22400
10
JM
11/06/06
16:00
SW 846-601OB
Aluminum
1410
1
JM
11/06/06
16:00
SW 846-601OB
Manganese
486
1
JM
11/06/06
15:00
SW 846-601OB
Copper
774
1
JM
11/06/06
16:00
SW846-6010B
Zinc
Nitrogen, Ammonia (as N)
0.14
1400
10
JM
11/06/06
14:00
EPA 350.2
CALCULATION
Nitrogen, Organic (N)
4.83
48300
62
100
1
DCH
KS
11/06/06
15-00
SM 4500-NO3F
Nitrogen, NO3+NO2
3.0
1
JM
11/06/06
16.00
SW 846-601OB
Cadmium
52
5
JM
11/06/06
16:00
SW 846-601OB
Chromium
All values are on a dry weight basis except as noted. 'Detection Limit on all N series is on a wet basis
Out reports and lenets are tot the exclusive and confidential use of our clients, and may not be reproduced in whole or in pan. not may any tefeience be made n
to the wok. the results. or the company to any adveoising. news release, of other public announcements without obtatnrng out pilot wlillen authorizalion PAUL C H CHU
Report Number:
R06307-8006 A&L EASTERN LABORATORIES, INC.
Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401
46381 Fax No. (804) 271-6446 • Email: office@al-labs-eastern.com
TO: SOUTHERN SOIL BUILDERS FOR: SPRUCE PINE
958 HOOTS ROAD
ROARING RIVER, NC 28669 NC CERT #257
ATTN: DENNIS KEY
copy: ZACH KEY
REPORT OF ANALYSIS DATESAMPLED: 10/31/2006 1230
LAB NUMBER: 44778 DATE RECEIVED: 1 1 /3/2006 1400
SAMPLE ID: SPRUCE PINE DATE REPORTED: 1 1/8/2006 PAGE: 2
Nickel
38
5
JM
11/06/06
16:00
SW 846-6010B
Lead
46
5
JM
11/06/06
16:00
SW 846-6010B
Arsenic
2.8
0.2
KM
11/06/06
15:00
SW 846-7061A
Mercury
1.5
0.4
KM
11/07/06
15:00
SW 846-7471A
Selenium
6.5
0.2
KM
11/06/06
15:00
SW 846-7741A
Molybdenum
7
5
JM
11/06/06
16:00
SW 846-6010B
All values are on a dry weight basis except as noted. "Detection Limit on all N series is on a wet basis
Our repots and letters are lot the exclusive and confidential use of our clients, and may not be reproduced in whole or in part. nor may any reference be made
to the work, the results, or the company it; any advertising, news release, or other public announcements without obtaining our prior written authorization.
PAUL C. H. CHU
OLIDS SAMPLE TRANSMITTAL FORM/CHAIN OF � CUSTODY I Account #
BIOS 63gi
Ego
A&L Eastern Agricultural Laboratories, Inc.
7621 Wlutepine Road Richmond VA 23237 Tel: 804-743-9401 Fax: 804-271-6446 Email: officeQal-labs-eastem.com
Customer Information
Submitted By
Charge To Copy To
5 Southern Southern
01
Builders '
0o s ass Hoots Rd
p Rc i RC River, P! . 28M
011-1 No
Project S rve e C � t-
e.
Sam le Information
Collection irtiorrrtat on Container Information Please Check Des(red Tests
Lab Number 503 Nitrogen p Volatw Others
Sample ID (Lab Use Number Type VdL" SL1 SIZ Metals Series pH. CCE Ag Solids
Only) Type Date Ttrte of Bottles tj Y
S X Grab 10`31-0 l�' 30 rr Xp IasUc Pint
Conte _ _cit
oz
Grab —Glass pint
— Composite _ Plastic
at
oz
Grab _Glass —piastic pint
_ Composite at
_ oz
— Grab — GP Inc pint
— Composite
Rell B . natum
Date Time Received B . S ature Date Time
Special Instructions or Remarks
Test Package Details
SLl: Total Solids (Moisture) Total Kjeldahi Nit ogee, Phosphorus and Potassium Copper And Zinc
SL2: Basic Test SL1 plus Sulfur, Calcium, Ma esium,Sodium, iron, Aluminum, manganese, ppe
503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenlum.
(Copper & Zinc included in SL2)
Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & organic Nitrogen.
CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge)
L
R
TORIES, INC.
www.pariabs.com
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
Phone: 704-588-8333; Fax: 704-588-8335
NC Cert # 20; SC Cert # 99003
REPORT OF ANALYSES
Attn: DENNIS KEY
SOUTHERN SOIL BUILDERS PROJECT NAME: OCT 06
958 HOOTS ROAD DATE: 11/29/06
ROARING RIVER, NC 28669-0000
SAMPLE NUMBER.-
1.1684
SAMPLE ID- SPRUCE
PINE
SAMPLE. MATRIX- SO
DATE SAMPLED-
10/26/06
LOCA11ON- SPRUCE
DATE RECEIVED-
10/26/06
SAMPLER- ZACH KEY
RECEIVED BY- MJ
TIME RECEIVED-
1215
DELIVERED BY- ZACH
KEY
TYPE SAMPLE- Grab
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD
DATE TIME BY
RESULT UNITS
FECAL COLIFORM
(GEOM. MEAN) SM 9221 E
11/02/06 IS30 GJ
2068 MPN/9
Y
LABORATORY DIRECTOR
t � �
1;0=
ABORATORIES, INC.
www.parlabs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704) 588-8335
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing)
SOUTHERN SOIL BUILDERS
Address
958 HOOTS RD
City, State & Zip Code
ROARING RIVER, NC 28669
Point of Contact & Telephone Number
COMMENTS/SPECIAL
INSTRUCTIONS
Sample taken by:
IS THIS FOR STAT or EPA REPORTING? YES NO
*Sample type: DW WW _.)C GWMW HW Soil Other
Sample Temp at time of sampling: °C Sample Temp upon receipt: °C
* * Preserved: Yes No Teflon. Liner/ Zero Headspace: Yes No N/A
Client Sample I.D.
(Sample Location. b.Nbmber).,'
Comp
Grab
Pre'sery
?Set Up;,
pate/Time
Collection'
Date/Tlme
Analyses
Requested
S
m-a6��
c.t
F I
uate/ I e
_,�,�-�� leas � c c jai 5
Relinqu' hed by: Date/Time Received by: Date/Time
' C=Composite G=Grab DW=Drinking Water WW = Wastewater GWMW = Groundwater Monitoring Well HW=Hazardous Waste
* See Other Side
7 � �
RAR
LABORATORIES, INC.
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
NC Cert # 20; SC Cert # 99003001
1 S S B 74684
1 10/26/06
1 FECAL COLIFORM, GEOMETRIC MEAN
��SM 9221 E
1
e H OM
5263
MALZL.
3.00
1754. 333333
• 0
3.2441
2
7018
4.29
1635.897436
3.2138
3
10526
4.52
2328.761062
3.3671
4
7018
3.27
2146.17737
3.3317
5
10526
4.13
2548.668281
3.4063
6
8772
4.49
1953.674833
3.2909
7
7893
1 3.48
2268.103448
3.3557
Fecal Coliform
Geometric Mean=�
H
Log Ave.
Log/Sum •
L ► 12/ 15/ 2006 11; 44 7045666333 FAK 1_Abi D UMAK N1:
PAR Loborotoriev, fne.
2217 Graham Park Diivo
PO Box Al 1463
Charlotte, NC 282d1-1d83
Phan(-.; 704-585.0335; Fcn; 7Q4S99$334
NC GDR M TO SC Cnrt 0 .4.9W2
wwwpsMbs. a)m
REPORT OF ANALYSES
Attn, 178NNIS KEY
SOUTHERN SOIL BUILDERS PROJECT NIaME; OCT 06
958 HOOTS ROAD DATE: 12/15/06
ROARING RIVER, NC 20669-0000
SAMPLE NUMBER-
14685
SAMPLE ID- SPRUCE PINE
SAMPLE MATRIX- SO
DATE FAMPTi n-
11/2A,MF
Tin iMnN, S4$.UCE FINE
TIMID CP,MPL® 0700
DATE RECEIVED-
10/26/06
SAMPLER- ZACH KEY
RECEIVED BY-- Md
T?MF RFf FTVR11-
171 5
MIvtRFD ➢Y. TACR KEY
Tl`ME OXMPLO- G-mL-
Page 1 of 1
ANALYSIS
ANALYSIS
METHOD DATE TIME BY
RESULT UNITS
30 DAY nIiN:!lITOP DI3E2Tt5XI, ITS 361
INITIAL START UP
503
END WEEK 1
503
END WEEK 2
503
END WEEK 3
503
END WEEK 4
503
30 DAY EENCHTOP DIGESTION,
*VS 503
INITIAL START U?
503
LND wrMit 2
SU.s
END WEEK 2
503
END WEEK 3
503
END WEEK ,.
503
TOTAL I VS LOSE
502
.LU/ Lb/'Ub ,LbUU W
10/26/06
1600
GJ
3.66 $
10/2VQ1
1G44
w
3.98 is
10/26/06
1600
GJ
3.62
10/26/06
1660
CG7
3.26 'k
10/26/06
1600
GJ
3.23
10/26/D6
1500
GJ
10/26/06
1600
GJ
$6.43
iU/26/U6
1600
GJ
56.09 t
10/26/06
1.600
GJ
55.62 4
10/26/06
1660
GJ
55.28 %
10/26/06
1600
GJ
55.42 %
10/26/06
1600
GJ
4.00 fi
LABORATORY DIRECTOR
1 e 12/15/2006 11:44 7045888333 PAR LABS CHAR NC HAGL 02
BENCH TOP PERCENT 'TTOTAL SOLIDS and
TOTAL VOLITILE SOLIDS
VAN KLZ3K FORMULA
S S B Start! 10/26/09 1600
74685 Ende 11/30/06
TARE
17.327
10/26 1600
0,56425406
m15 smpl
18.5
DRIED WT.
LEi.004
u
BURNED 'WT.
17.622
5.16216226
t
solids
3.66
TVs
0.382
0,677
% TVs-
56.43
TVS g/L
20,d4864E6
0.56425406
TAM
16.351
11/2 1540
0.56086037
mis smpi
19.3
0.9940018
DRIED WT.
17.041
0
BURNED Wr,
16.65i
5.01295337
4
Solids
3.58
TV$
0.307
0.69
b TV$-
56.09
TV6 g/L
20.0518135
0.56086957
4
VS LOhO
0.60
TARE
18.498
11/9 1600
0.55817378
mlr. 9mpl
18.767
0,99519357
nRTRTI WT
1 q 177
n
BURNED wT.
18.798
5.04875579
%
solidt
3.62
TVS
0.379
0,679
$ TVs
55.82
TV0 g/L
20.1D50232
0.53017170
V
VC L065
0.49
7AKE
13.843
11/19 1415
0.95275382
mle empl
18.316
0.99030774
DRIED WT.
16.442
0
BUM= wT,
16.112
4.50425657
4
Solids
3.26
TVS
0 . 33
0 .597
E TV.9
Mal
TVS g/L
18.0170343
0,55276302
4
V9 LOSS
0.97
TARE
17.678
11/23 1530
0.554i958
mis smpl
17,598
1.00259059
DRIBA WT,
28.25
0
2URDTYD WT.
17.932
4.6033G366
ti
Eolidb
3.2E;
TVs
0,317
0.372
96 TVs-
5$"kn
TVS g/L
18.01.34106
0,5541958
$
V9 LOSS
-0.26
�,it!l�hCt.i��.�, ���i;,f";����iial�1�11?I �,�E��4•,6fl�14�;�,,
12/15/2006 11:44 704588833:a
r
AP?BORAr0 tas, INC.
WWW. .aom
PAR-J AFS MAR -NC
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-18333
Fax (704) 688-9335
PAGE 03
Shipping: Mailing:
2217 Graham Park Drive PO Box 411483
Charlotte, NC 28273 Charlotte, NC 28241.1483
It is essential that al Information reCOrded on this Chain of Custody dooumont for accorAince by PAR Laboratories. InC, and tM North
Carollna oeportment of Environmental and Netural Rasoureos.
Company Neme WIlIngi
SOUTHERN SOIL BUILDERS
Address
088 HOOTS RD
City, State & ZIP Code
ROARING RIVER, NC 28689
Point of ContnM 1 Talap),b„o Nu❑1w,
f UJ-2137MJ
Samplo taken by: I, y -
COMMENTS/SPECIAL
INSTRUCTIONS
IS THIS FOR STq4 or EPA REPORTING? YES � No
•Sarrlple type: W _ WW �, (3WMW _ HW Soil _ Other
Samplo Tamp of tuna: of sampling: �► •C Sample Te-
mp upon receipt: 9C
"* Preaerved; Yes No — Teflon Liner/ Zero Headspabe: Yes _- No � N/A
(,' ' C ■ Compoeito 0 =Orab DW=D*king Weter WW -Wastewater GWMW =Groundwater Monitoring Wnil HW z Hazardoue Woote
" Sen Other Side
0
LPA R
LABORATORIES, INC.
www.parlabs.com
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
Phone: 704-588-8333; Fax: 704-588-8335
NC Cert N 20; SC Cert N 99003
REPORT OF ANALYSES
Attn: DENNIS KEY
SOUTHERN SOIL BUILDERS PROJECT NAME: SEP 06
958 HOOTS ROAD DATE: 09/21/06
ROARING RIVER, NC 28669-0000
SAMPLE NUMBER- 73702
SAMPLE ID- SPRUCE
PINE
DATE SAMPLED- 08/31/06
TIME SAMPLED- 14i;:0
DATE RECEIVED- 09/05/06
SAMPLER- ZACH KEY
RECEIVED BY- MJ
TIME RECEIVED- 1350
DELIVERED BY- ZACH KEY
TYPE SAMPLE- Crab
Page 1 of 3
ANALYSIS
ANALYSIS
METHOD
DATE
TIME
BY
RESUI.,T
UL`'ITS
TCLP CHARACTERISTICS
TCLP
09/05/06
1600
CRB
pH VALUE
TCLP
09/05/06
1600
CRB
6.64
S.U.
CORROSIVITY
TCLP
09/05/06
1600
CRB
< NON
REACTIVITY
TCLP
09/05/06
1600
CRB
< NON
FLASH POINT
TCLP
09/05/06
1600
CRB
> 140
degree; F
IGNITABILITY
TCLP
09/05/06
1600
CRB
< NON
PAINT FILTER TEST
TCLP
09/05/06
1600
CRB
<: NFL
TCLP METALS
TCLP
09/OS/06
1600
CRB
ARSENIC
TCLP
09/05/06
1600
CRB
< 0.5
ppm
BARIUM
TCLP
09/05/06
1600
CRB
< 10
ppm
CADMIUM
TCLP
09/05/06
1600
CRB
< 0.1
ppm
CHROMIUM
TCLP
09/05/O6
1600
CRB
< 0.5
ppm
LEAD
TCLP
09/05/06
:1.60n
C..,R.B
0.
r. rm
MERCURY
TCLP
09/05/06
1600
CRB
< 0.02
ppm
SELENIUM
TCLP
09/05/06
1600
CRB
< 0.1
ppm
SILVER
TCLP
09/05/06
1600
CRB
< 0.5
ppm.
TCLP PESTICIDES
TCLP
09/05/06
1600
CRB
ENDRIN
TCLP
09/05/06
1600
CRB
< 0.002
ppm
LINDANE
TCLP
09/05/06
1600
CRB
< 0.04
ppm
METHOXYCHLOR
TCLP
09/05/06
1600
CRB
< 1
ppm
TOXAPHENE
i r-•
TCLP
09/05/06
1600
CRB
< 0.05
ppm
L
R
ATORIES, INC.
www. parlabs. com
Page 2 of 3
PAR Laboratories, Inc.
2217 Graham Park Drive
PO Box 411483
Charlotte, NC 28241-1483
Phone: 704-588-8333; Fax: 704-588-8335
NC Cert # 20; SC Cert # 99003
CONTINUATION OF DATA FOR SAMPLE NUMBER 73702
ANALYSIS
ANALYSIS METHOD DATE TIME BY RESULT UNITS
CHLORDANE
TCLP
09/05/06
1600
CRB
< 0.003
ppm
HEPTACHLOR (AND ITS EPDXIDE)
TCLP
09/05/06
1600
CRB
< 0.0008
ppm
TCLP HERBICIDES
TCLP
09/05/06
1600
CRB
2,4-D
TCLP
09/05/06
1600
CRB
< 1
ppm
2,4,5-TP(SILVEX)
TCLP
09/05/06
1600
CRB
< 0.1
ppm
TCLP ORGANICS
TCLP
09/05/06
1600
CRB
BENZENE
TCLP
09/05/06
1600
CRB
< 0.05
ppm
CARBON TETRACHLORIDE
TCLP
09/05/06
1600
CRB
< 0.05
ppm
CHLOROBENZENE
TCLP
09/05/06
1600
CRB
< 10
ppm
CHLOROFORM
TCLP
09/05/06
1600
CRB
< 0.6
ppm
o-CRESOL
TCLP
09/05/06
1600
CRB
< 20
ppm
p-CRESOL
TCLP
09/05/06
1600
CRB
< 20
ppm
m-CRESOL
TCLP
09/05/06
1600
CRB
< 20
ppm
1,4-DICHLOROBENZENE
TCLP
09/05/06
1600
CRB
< 0.75
ppm
1,2-DICHLOROETHANE
TCLP
09/05/06
1600
CRB
< 0.05
ppm
1,1-DICHLOROETHYLENE
TCLP
09/05/06
1600
CRB
< 0.07
ppm
2,4-DINITROTLUENE
TCLP
09/05/06
1600
CRB
< 0.013
ppm
HEXACHLOROBENZENE
TCLP
09/05/06
1600
CRB
< 0.013
ppm
HEXACHLOROBUTDIENE
TCLP
09/05/06
1600
CRB
< 0.05
ppm
HEXACHLOROETHANE
TCLP
09/05/06
1600
CRB
< 0.3
ppm
METHYL ETHYL KETONE
TCLP
09/05/06
1600
CRB
< 20
ppm
NITROBENZENE
TCLP
09/05/06
1600
CRB
< 0.2
ppm
PENTACHLOROPHENOL
TCLP
09/05/06
1600
CRB
< 10
ppm
PYRIDINE
TCLP
09/05/06
1600
CRB
< 0.5
ppm
TETRACHLORETHYLENE
TCiJP
09/05/06
1600
CF.Fi
< 0.071
ppm
TRICHLOROETHYLEivE
TCLP
09/05/06
1600
CRB
<; 0.05
ppm
2,4,5-TRICHLOROPHENOL
TCLP
09/05/06
1600
CRB
< 40
ppm
2,4,6-TRICHLORPHENOL
TCLP
09/05/06
1600
CRB
< 0.2
ppm
VINYL CHLORIDE
TCLP
09/05/06
1600
CRB
< 0.02
ppm
J/ e
LABORATORY
DIRECTOR
PAR
LABORATORIES, INC.
MW
www.parlabs.com
Shipping:
2217 Graham Park Drive
Charlotte, NC 28273
CHAIN OF CUSTODY
PAR Laboratories, Inc
Phone (704) 588-8333
Fax (704) 588-8335
Mailing:
PO Box 411483
Charlotte, NC 28241-1483
It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North
Carolina Department of Environmental and Natural Resources.
Company Name (billing)
SOUTHERN SOIL BUILDERS
Address
958 HOOTS RD
City, State & Zip Code
ROARING RIVER, NC 28669
Point of Contact & Telephone Number
..�.. ,� ea-, none
COMMENTS/SPECIAL
INSTRUCTIONS
Sample taken by:
IS THIS FOR STAT or EPA REPORTING? YES x NO
*Sample type: D WWC)":f GWMW HW Soil Other
Sample Temp at time of sampling: °C Sample Temp upon receipt: °C
* * Preserved: Yes No Teflon Liner/ Zero Headspace: Yes — No __ NIA —
Client Sample I.D.
(Sample Location / Number)
Comp
Grab ,Preserv.
$et Up.
Date/T.iite
Collection
Date/Time
nalyses
Requested
fie f (� ^�
Z) U
�C a T
Relinquished by:� Date/Time Rec Iv d 1by: Date/Time
o\\,
R nquished by: Date/Time Received by: Date/The
C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste
•' See Other Side
NCDA&CS At -- Division Phone: (919)733-2655 Web Site: Mvw.n
12ni2oo6
Agronomist Continents
Soil Test Report
SERVING N C. RESIDENTS FOR OVER 60 YL'ARS
,agr.com/agrononii/
Gruruer: Southern
958 Hoots R
Roaring Rivc
Farm:
Gaston Co
Field Information
Applied Lime
Iecommendations
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
63
1st Crop: Fes/OG/rim,M
0
120-200
211d Crop: Fes/OG/rim,M
0
120-200
Test Results
Soil Class HM% W/V
CEC BS%
Ac p H P-1 K I
72 O Mg
19 Mn-]
MIN 0.71 1.17
12.3 95.0
0.6 6.8 63 49
Fiefd,Information...
Applied Lime
Recorliregdati.ons
Sample No. Last Crop
Mo Yr T/A
Crop or Year
Lime
91
1st Crop: Fes/OG/I'im,M
0
120-200
211d Crop: Fes/OG/rim,M
0
120-200
Test Results
Soil Class HM% W/V
MIN 0.46
Field Information
Sample No. Last Crop
SP1
Test Results
Soil Class HM% W/V
MIN 0.27 1.18
Field Information
Sample No. Last Crop
U2
Test Results
F
l Class HM% WlV
MIN 0.41 1.14
CEC BS% Ac pH P-I K-I
12.0 98.0 0.2 7.2 109 29
kpplied Lime Recommendations
Mo Yr T,'A Crop or Year
1st Crop: Fes/OG/rim,M
211d Crop: Fes/OG/rim,M
CEC BS% Ac pH P-I K-I
4.2 48.0 2.2 4.9 360 36
kpplied Lime Recommendations
Mo Yr T/A Crop or Year
I st Crop: Fes/OG/rim,M
211d Crop: Pes/OG/rim,M
CEC l3S% AC p H P-1 K-1
n ()t1 a 2.0 5.0 340 50
Ca% Mg% Mn-I Mn-
85.0 12.0 783
Lime "
I.AT 120-200
0 120-200
Ca% Pig% Mn-I rKn
34.0 9.0 86
Lime "
1.31' 120-200
0 120-200
Rennrt No: 14129
;oil Builders, Inc.
Copies To:
l
r, NC 2s669
Linty
C -- 12, $
P205 K20 Mg S
Cu Zn
B
Mn
See A'ote
0-20 30-50
0 0
0
0
.0
pH$
12
0-20 30-50
0 0
0
0
.0
pH$
12
II(I)Mn-AI(2) Zn-I
Zn-AI
Cu-I
S-I
SS-1
NO3-N NH4-N
Na
96 196 451
451
706
114
0.2
*^ :.
P205 K20 Mg S
Cu
Zn
B
Mn
See Note
0 70-90
0 0
0
0
.0
pH$
12
0 70-90
0 0
0
0
.0
pH$
12
AI(1)Mn-AI(2) Zn-1
Zn-AI
Cu-1
S-I
SS-1
NO3-N NH4-N
Na
i69 469 583
583
560
39
0.4
P205 K20 '
Pig S
Cu
Zn
B
Mn
See Note
0 60-80
0
0
0
.0
0
12
0 60-80
0
0
0
.0
0
12
AI(1)Mn-AI(2) Zn-1
Zn-AI
Cu-1
S-1
SS -I
NO3-N NH4-N
Na
69 69 393
393
446
28
0.1
P205 K20
Mg S
Cu
Zn
B
Mn
See Note
0 30-50
0 0
0
0
.0
0
12
0 30-50
U o
0
0
.0
0
12
Al(1)Mn-AI(2) Zn-1
Z"-AI
Cu-I
S-1
SS-1
NO3-N NH4-N
Na
0.I
110 ()-7
0-7
Q8
37
Ca% Mg% Mn-1 Mn
43.0 13.0 118 88