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HomeMy WebLinkAboutWQ0002349_Annual Report_20070209ANNUAL LAND APPLICATION CERTIFICATION FORM Permit#: WQ0002349 County: Mitchell - Year: 2006 Facility Name (as shown on permit): Town of Spruce Pine Land Application Operator: Southern Soil Builders, Inc Phone: 336-957-8909 Land application of residual solids as allowed by the permit occurred during the past calender year? ® Yes ❑ No If No, skip Part A, and Part B and proceed to the certification. Also, if residuals were generated but not land applied, please attach an explanation on how the residuals were handled. 1) e Total number of application fields in permit- 7 Total number of fields land application occurred during the year: 2 Total amount of dry tons applied during the year for all application sites: 70.9 Total number of acres land application occurred during the year: 11.7 Part B: Facility was compliant during calendar year 2006 with all conditions of the land application permit (including but not limited to items 1-12 below) issued by the Division of Water Quality. Yes" ❑ No If no please, provide a written description why the facility was not compliant, the dates, and Ixpla n corrective action taken.rn �q . Y 1. Only residuals approved for this permit were applied to the permitted sites. CD 2. Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil nn oftat F, least 6.0 or the limit specified in the permit. 3. Annual soils analysis were performed on each site receiving residuals during the past calendar year nd�hre o (3) copies of laboratory results are attached. 0 4. Annual TCLP analysis was performed and three (3) copies of certified laboratory results are attached 5. All other monitoring was performed in accordance with the permit and reported during the year as rTqufr'ed and three (3) copies of certified laboratory results are attached. 5. The facility did not exceed any of the Pollutant Concentration Limits in Table 1 of 40 CFR Part 503.13 or the Pollutant Loading Rates in Table'2 of 40 CFR part 503.13 (applicable to 40 CFR Part 503 regulated facilities). 7. All general requirements in 40 CFR Part 503.12 and management practices in 40 CFR Part 503.14 were complied with (applicable to 40 CFR Part 503 regulated facilities). 8. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 10. Vegetative cover as specified in the permit was maintained on this site and the crops grown were removed in accordance with the crop management plan. 1 l . No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 12. All buffer requirements as specified on the permit were maintained during each application of residuals. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowin violations." w4-�`O 7o uy ^� Y1/� `ti,N' e W 4 ' 0 ? Permittee Name and Title (type or print) Signature of Permittee Date Signature of Preparer* (if different from Permittee) ' Preparer is defined in 40 CFR Part 503.9 (r) '7 R F re of Land Applier Date �(iifferent from Permittee and Preparer) t- k�� -�„ ► iot4 ptocessin9 UnYL lnformat10n DENR FORM ACF (5/2003) E', 1-, ANNUAL RESIDUAL SAMPLING SUMMARY FORM Attach this form to the corresponding Annual Report Please note that your permit may contain additional parameters to be analyzed than those required to be summarized on this form. Ic Permit Number: WQ0002349 Facility Name: Town of Spruce Pine NPDES # or NCO021423 W Q#: WWTP Name: Town of Spruce Pine WWTP Residual Analysi Sample or Composite Date Percent Solids Arsenic Cadmium Chromium Lead Nickel Selenium Zinc Data Total Phosphorus TKN Ammonia-Nitroger. d Nitrite 10-31-06 3.56 2.8 3 52 486 46 1.5 7 38 6.5 774 27,100 49,700 1400 62 Laboratory: 1) A&L Eastern Laboratories, n . 2) — 4) 5) 0n Nrtrate an "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to .assure that qualified personnel properly gathered and evaluated t e information submitted. r sonmeent for knowing wmg violat ons. am aware tht there are significant nalties f su itting false information, of fines and imP including the possibility Signature of Preparer Date DENR FORM RSSF (5/2003) ANNUAL METALS FIELD LUADIA(i aUMMAKY rUltivl-' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Town of Spruce Pine Total Dry Tons Applied (Annual): WQ0002349 Cation Exchange Capacity (non 503 only): KT Feldspar Corp. Owner: Penland -Bailey Company 7.2 Acres Permitted: 7.2 Site #: SP-01 Field #: 54.88 SP-01 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Total • •M •.ENEEMENEENE Annual Heavy Metal Field Loadings (Calculated in lbs/acre): WPM 1 1' 000000�0000 1 1' 1 1 00000000000 1 1MR 71.it'iii�1:' 1 • 00000000000 1 ...• - . 00000000000 •' m l l 000000000�0 1 1 • yl ® 1 1 • �00000000�� 1 1 • • ••. 1 1 1 1 1 1 1 1 1 1 1 PI certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Sii4ture of Land A'ppfier Date • See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Spruce Pine Owner: Penland -Bailey Company Site #: SP-01 A Field # Operator: SP-01 A Permit 9: WQ0002349 KT Feldspar Corp. Acres Utilized: 7.2 Annual Dry Tons Applied: 54.88 Cation Exchange Capacity (non 503): Acres Permitted: ' 7.2 o � o ra Specify Totals Per Acre Solids �' Tons Per Acre Residual Sources (Summarize) ' e Cond. Dry Wet, Moist Inches Preci p� Past 24 Hrs. Appli- cation Meth- od* Voli- tila- zation Rate** Miner- ala- zation Rate TKN Ammo- nia- Ni- trogen Ni- trate and Nitrite PAN 1 PAN 2 Must Select Crop 1 or Crop 2 * Gal. Cu.Yd. Report Totals € in Gal. Crop 1 Crop 2 2-06 30,000 4166.7 3.56 0.61855 WWTP dry 0 s 0.5 30% 49700 1400 62 18.8682 ####### Fescue 1 3-06 32,500 4513.9 3.56 0.670095833 WWTP dry 0 s 0.5 30% 49700 1400 62 20.4406 ####### Fescue 2 4-06 82,500 11458 3.56 1.7010125 WWTP dry 0 s 0.5 30% 49700 1400 62 51.8877 ##44### Fescue 3 6-06 70,000 9722.2 3.56 1.443283333 WWTP dry 0 s 0.5 30% 49700 1400 62 44.0259 ####### Fescue 4 5-06 10,000 1388.9 3.56 0.206183333 WWTP dry 0 s 0.5 30% 49700 1400 62 6.28942 ####### Fescue 5 6-06 30,000 4166.7 3.56 0.61855 WWTP dry 0 s 0.5 30% 49700 1400 62 18.8682 ####### Fescue 6 7-06 62,500 8680.6 3.56 1.288645833 WWTP dry 0 s 0.5 30% 49700 1400 62 39.3089 ####### Fescue 7 8-06 52,500 7291.7 3.56 1.0824625 WWTP dry 0 s 0.5 30% 49700 1400 62 33.0194 ####### Fescue 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 12 TOTALS: 51389 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.042728 0.04578 0.79352 7.41636 0.70196 10.02289 0.10682 0.57988 0.09919 11.8112 1413.546 1232.7081 0 Date Ibs/ac Current Cumulative lbs/ac 0.163028 0.12713 0.79352 98.0269 68.7521 0.40714 0.44978 3.92364 0.32277 110.165 0.1203 0.08135 0 90.6105 68.0501 0.38425 0.34296 3.34376 0.22358 98.3534 36 34 NA 1338 267 15 1 NA 374 1 89 2498 250 Prior Years Cumulative Ibs/ac Permitted C. P. L. R.*** Pernut PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." � -/ -6, 7 *Application Method: S - Surface, IN - Injection, INC - Incorporation Signatere of Land Applier Date **Volitilization Rate: Surface - 0.5, Iniection/Incorvoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF DENR FORM FSF (5/2003) AINNUAL 1v1LIALa r1JVLU LVL MUIV 0UlriiVatXi%a i'viv.a Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Spruce Pine Total Dry Tons Applied (Annual): WQ0002349 Cation Exchange Capacity (non 503 only): Unimin Co. Owner: Penland Bailey Co. 4.5 Acres Permitted: 4.5 16.02 Site #: U-02 Field #: U-02 Raeiriival Analvcic natn (Aeaw Metals and Total Phosphorus use mg/kz, % Solids use Raw Percent #): • 11 Annual Heaw Metal Field Loadings (Calculated in lbs/acre): • W.1 I IT, 1 . - 1 11 ` •. `• �� .•• 1 1 1 1 1 1 1 1 1 1 1 �� •" .- "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations" Sig6ture of Land Applier Date * See bottom of FSF Form for helpful instructions for this MFLSF Form and the mathematically linked FSF Form DENR FORM MFLSF (5/2003) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH APPLICATION FIELD. Facility Name: PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Town of Spruce Pine Owner: Penland Bailey Co. Operator: Site #: U-02 Field #: U-02 Permit #: WQ0002349 Unimin Co. Acres Utilized: 4.5 Annual Dry Tons Applied: 16.02 Cation Exchange Capacity (non 503): Acres Permitted: 4.5 S i t e Inches Appli- Voli- Miner- Ammo- Ni- Must Select Gal. o Totals % Dry Tons Per Residual Cond. Precip. cation tila- ala- TKN nia- trate PAN 1 PAN 2 Crop 1 or Crop p p N „ o Cu.Yd. per Solids Acre Sources (Summarize) Dry past 24 Meth- zation zation Ni- and 2 ;.` Report Q Totals Acre Wet Hrs. od* Rate** Rate trogen Nitrite Crop 1 Crop 2 i in Gal.Moist 5-06 25,000 5555.E 3.5E 0.824733333 WVTrP dry 0 s 0.5 30% 49700 1400 62 25.1577 ####### Fescue 1 0 0 0 0 2 0 0 0 0 3 0 0 0 0 4 0 0 0 0 5 0 0 0 0 6 0 0 0 0 7 0 0 0 0 8 0 0 0 0 9 0 0 0 0 10 0 0 0 0 11 0 0 0 0 1121 TOTALS: 5556 As Cd Cr Cu Pb Hg Mo Ni Se Zn P PAN 1 PAN 2 Lime Applied Annuallbs/acre 0.00461832 0.00495 0.08577 0.80161 0.07587 0.00247 0.01155 0.06268 0.01072 1.27664 44.6987 25.1577 0 Date lbs/ac Current Cumulative lbs/ac 0.13287832 0.17493 0.08577 28.3727 2.84454 0.2938 0.3169 1.71894 0.27554 50.7767 0.12826 0.169981 0 27.5711 2.76867 10.29133 0.30535 1.6562E 10.26482 49.5001 36 34 1 NA 1338 267 15 NA 1 374 89 2498 250 la •�S LS Prior Years Cumulative lbs/ac Permitted C. P. L. R.*** Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a sySle111 designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signatur of Land Applier -%-0 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volitilization Rate: Surface - 0.5. Iniection/Incornoration - 1.0 ***C.P.L.R.: Cumulative Pollutant Loading Rate **** The RSSF Data and the Dry Tons Per Acre are to be entered on the MFLSF Form. The FSF and MFLSF are mathematically linked so this information needs to be entered into the same numbered column on the MFLSF as is entered on the identically numbered FSF row to properly complete the metals equations. ie. FSF row # 1 to MFLSF DENR FORM FSF (5/2003) ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUC I WiN rUtuvi Facility Name: Town of.Spruce Pine Permit Number: WWTP Name: Town of Spruce Pine WWTP NPDES Number: Monitoring Period: From 1/1/2006 To 12/31/2006 lAn nVn Cn2 2i,% _ Dlnoon ;"riiratp IPvpl achipvP.d and alternative performed: WQ0002349 NCO021423 Class A: Alternative 1 ❑ Alternative 2 ❑ Alternative 3 ❑ Alternative 40 Alternative 5 ❑ Alternative 6 ❑ If applicable to alternative performed Class A only indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ Class B: Alternative 1jS I Alternative Z ❑ Alternative 3 ❑ If applicable to alternative performed Class B onl indicate "Process to Si nificantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion Anaerobic Digestion❑ If to alternative Class A or Class B complete the following monitoring data: applicable performed Pathogen Density um er o requeney Sample Anahtical Parameter Level in F.xcee- of YP Type Tech-nique imu Geo. Mean aximu Units 2x 10to e6th power MPN per 1635 2068 2548 MPN/g 0 7 grab sm9221 gram of total solids or 2 x 10 to Fecal Coliform the 6th power CFU per Pjam of 1000 mpn per gram of total solid (dry weight) Salmonella bacteria 3 MPN per 4 din lieu of fecal grams total solid colilorm) (dry weight) vPrtor Attraction Reduction (40 CFR 503.33) - Please indicate option performed: Option 1 ❑ Option 2 ❑ Option 3 P§ Option 4 ❑ Option 5 ❑ Option 6 ❑ Option 7 ❑ Option 8 ❑ Option 9 ❑ Option 10 ❑ No vector attraction reduction options were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have been met." ❑ "I certify, under penalty of law, that the pathogen"requirements in 40 CFR 503.32 and the vector attraction reduction requirement in 40 CFR 503.33 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment. Preparer Name and Title (type or print) Signature of Preparer Southern Soil Builders, Inc Dennis Key Land Applier Name and Title (if applicable)(type or print) Date Signature of Land plier (if applicable) Date DENR FORM RF (5/2003) Report Number: R06307-8006 A&L EASTERN LABORATORIES, INC. Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 46381 Fax No. (804) 271-6446 - Email: office@al-labs-eastern.com TO: SOUTHERN SOIL BUILDERS FOR: SPRUCE PINE 958 HOOTS ROAD ROARING RIVER, NC 28669 NC CERT #257 ATTN: DENNIS KEY LAB NUMBER: 44778 SAMPLE ID: SPRUCE PINE REPORT OF ANALYSIS copy: ZACH KEY DATE SAMPLED: 10/31/2006 1230 DATE RECEIVED: 1 1 /3/2006 1400 DATE REPORTED: 1 1 /8/2006 PAGE: 1 Solids, Total (As is) 3.56 35600 100 JM 11/03/06 16:00 SM 2540G Nitrogen, Total Kjeldahl 4.97 49700 100 JM JM 11/06/06 11/06/06 16:00 16:00 EPA 351.3 SW 846-601OB Phosphorus 2.71 0.57 27100 5700 100 100 JM 11/06/06 16:00 SW 846-6010E Potassium 0.79 7900 100 JM 11/06/06 16:00 SW 846-601OB Sulfur 1.55 15500 100 JM 11/06/06 16:00 SW 846-601OB Calcium 0.53 5300 100 JM 11/06/06 16:00 SW 846-601OB Magnesium 0.16 1600 100 JM 11/06/06 16:00 SW 846-601OB Sodium 18900 1 JM 11/06/06 16:00 SW 846-601OB Iron 22400 10 JM 11/06/06 16:00 SW 846-601OB Aluminum 1410 1 JM 11/06/06 16:00 SW 846-601OB Manganese 486 1 JM 11/06/06 15:00 SW 846-601OB Copper 774 1 JM 11/06/06 16:00 SW846-6010B Zinc Nitrogen, Ammonia (as N) 0.14 1400 10 JM 11/06/06 14:00 EPA 350.2 CALCULATION Nitrogen, Organic (N) 4.83 48300 62 100 1 DCH KS 11/06/06 15-00 SM 4500-NO3F Nitrogen, NO3+NO2 3.0 1 JM 11/06/06 16.00 SW 846-601OB Cadmium 52 5 JM 11/06/06 16:00 SW 846-601OB Chromium All values are on a dry weight basis except as noted. 'Detection Limit on all N series is on a wet basis Out reports and lenets are tot the exclusive and confidential use of our clients, and may not be reproduced in whole or in pan. not may any tefeience be made n to the wok. the results. or the company to any adveoising. news release, of other public announcements without obtatnrng out pilot wlillen authorizalion PAUL C H CHU Report Number: R06307-8006 A&L EASTERN LABORATORIES, INC. Account Number: 7621 Whitepine Road • Richmond, Virginia 23237 • (804) 743-9401 46381 Fax No. (804) 271-6446 • Email: office@al-labs-eastern.com TO: SOUTHERN SOIL BUILDERS FOR: SPRUCE PINE 958 HOOTS ROAD ROARING RIVER, NC 28669 NC CERT #257 ATTN: DENNIS KEY copy: ZACH KEY REPORT OF ANALYSIS DATESAMPLED: 10/31/2006 1230 LAB NUMBER: 44778 DATE RECEIVED: 1 1 /3/2006 1400 SAMPLE ID: SPRUCE PINE DATE REPORTED: 1 1/8/2006 PAGE: 2 Nickel 38 5 JM 11/06/06 16:00 SW 846-6010B Lead 46 5 JM 11/06/06 16:00 SW 846-6010B Arsenic 2.8 0.2 KM 11/06/06 15:00 SW 846-7061A Mercury 1.5 0.4 KM 11/07/06 15:00 SW 846-7471A Selenium 6.5 0.2 KM 11/06/06 15:00 SW 846-7741A Molybdenum 7 5 JM 11/06/06 16:00 SW 846-6010B All values are on a dry weight basis except as noted. "Detection Limit on all N series is on a wet basis Our repots and letters are lot the exclusive and confidential use of our clients, and may not be reproduced in whole or in part. nor may any reference be made to the work, the results, or the company it; any advertising, news release, or other public announcements without obtaining our prior written authorization. PAUL C. H. CHU OLIDS SAMPLE TRANSMITTAL FORM/CHAIN OF � CUSTODY I Account # BIOS 63gi Ego A&L Eastern Agricultural Laboratories, Inc. 7621 Wlutepine Road Richmond VA 23237 Tel: 804-743-9401 Fax: 804-271-6446 Email: officeQal-labs-eastem.com Customer Information Submitted By Charge To Copy To 5 Southern Southern 01 Builders ' 0o s ass Hoots Rd p Rc i RC River, P! . 28M 011-1 No Project S rve e C � t- e. Sam le Information Collection irtiorrrtat on Container Information Please Check Des(red Tests Lab Number 503 Nitrogen p Volatw Others Sample ID (Lab Use Number Type VdL" SL1 SIZ Metals Series pH. CCE Ag Solids Only) Type Date Ttrte of Bottles tj Y S X Grab 10`31-0 l�' 30 rr Xp IasUc Pint Conte _ _cit oz Grab —Glass pint — Composite _ Plastic at oz Grab _Glass —piastic pint _ Composite at _ oz — Grab — GP Inc pint — Composite Rell B . natum Date Time Received B . S ature Date Time Special Instructions or Remarks Test Package Details SLl: Total Solids (Moisture) Total Kjeldahi Nit ogee, Phosphorus and Potassium Copper And Zinc SL2: Basic Test SL1 plus Sulfur, Calcium, Ma esium,Sodium, iron, Aluminum, manganese, ppe 503 Metals: Arsenic, Cadmium, Chromium, Mercury, Molybdenum, Lead, Nickel, Selenlum. (Copper & Zinc included in SL2) Nitrogen Series: Total Kjeldahl, Ammonium, Nitrate & organic Nitrogen. CCE: Calcium Carbonate Equivalent or Total neutralization Value (For Lime Treated Sludge) L R TORIES, INC. www.pariabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert # 20; SC Cert # 99003 REPORT OF ANALYSES Attn: DENNIS KEY SOUTHERN SOIL BUILDERS PROJECT NAME: OCT 06 958 HOOTS ROAD DATE: 11/29/06 ROARING RIVER, NC 28669-0000 SAMPLE NUMBER.- 1.1684 SAMPLE ID- SPRUCE PINE SAMPLE. MATRIX- SO DATE SAMPLED- 10/26/06 LOCA11ON- SPRUCE DATE RECEIVED- 10/26/06 SAMPLER- ZACH KEY RECEIVED BY- MJ TIME RECEIVED- 1215 DELIVERED BY- ZACH KEY TYPE SAMPLE- Grab Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS FECAL COLIFORM (GEOM. MEAN) SM 9221 E 11/02/06 IS30 GJ 2068 MPN/9 Y LABORATORY DIRECTOR t � � 1;0= ABORATORIES, INC. www.parlabs.com Shipping: 2217 Graham Park Drive Charlotte, NC 28273 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Environmental and Natural Resources. Company Name (billing) SOUTHERN SOIL BUILDERS Address 958 HOOTS RD City, State & Zip Code ROARING RIVER, NC 28669 Point of Contact & Telephone Number COMMENTS/SPECIAL INSTRUCTIONS Sample taken by: IS THIS FOR STAT or EPA REPORTING? YES NO *Sample type: DW WW _.)C GWMW HW Soil Other Sample Temp at time of sampling: °C Sample Temp upon receipt: °C * * Preserved: Yes No Teflon. Liner/ Zero Headspace: Yes No N/A Client Sample I.D. (Sample Location. b.Nbmber).,' Comp Grab Pre'sery ?Set Up;, pate/Time Collection' Date/Tlme Analyses Requested S m-a6�� c.t F I uate/ I e _,�,�-�� leas � c c jai 5 Relinqu' hed by: Date/Time Received by: Date/Time ' C=Composite G=Grab DW=Drinking Water WW = Wastewater GWMW = Groundwater Monitoring Well HW=Hazardous Waste * See Other Side 7 � � RAR LABORATORIES, INC. PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 NC Cert # 20; SC Cert # 99003001 1 S S B 74684 1 10/26/06 1 FECAL COLIFORM, GEOMETRIC MEAN ��SM 9221 E 1 e H OM 5263 MALZL. 3.00 1754. 333333 • 0 3.2441 2 7018 4.29 1635.897436 3.2138 3 10526 4.52 2328.761062 3.3671 4 7018 3.27 2146.17737 3.3317 5 10526 4.13 2548.668281 3.4063 6 8772 4.49 1953.674833 3.2909 7 7893 1 3.48 2268.103448 3.3557 Fecal Coliform Geometric Mean=� H Log Ave. Log/Sum • L ► 12/ 15/ 2006 11; 44 7045666333 FAK 1_Abi D UMAK N1: PAR Loborotoriev, fne. 2217 Graham Park Diivo PO Box Al 1463 Charlotte, NC 282d1-1d83 Phan(-.; 704-585.0335; Fcn; 7Q4S99$334 NC GDR M TO SC Cnrt 0 .4.9W2 wwwpsMbs. a)m REPORT OF ANALYSES Attn, 178NNIS KEY SOUTHERN SOIL BUILDERS PROJECT NIaME; OCT 06 958 HOOTS ROAD DATE: 12/15/06 ROARING RIVER, NC 20669-0000 SAMPLE NUMBER- 14685 SAMPLE ID- SPRUCE PINE SAMPLE MATRIX- SO DATE FAMPTi n- 11/2A,MF Tin iMnN, S4$.UCE FINE TIMID CP,MPL® 0700 DATE RECEIVED- 10/26/06 SAMPLER- ZACH KEY RECEIVED BY-- Md T?MF RFf FTVR11- 171 5 MIvtRFD ➢Y. TACR KEY Tl`ME OXMPLO- G-mL- Page 1 of 1 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS 30 DAY nIiN:!lITOP DI3E2Tt5XI, ITS 361 INITIAL START UP 503 END WEEK 1 503 END WEEK 2 503 END WEEK 3 503 END WEEK 4 503 30 DAY EENCHTOP DIGESTION, *VS 503 INITIAL START U? 503 LND wrMit 2 SU.s END WEEK 2 503 END WEEK 3 503 END WEEK ,. 503 TOTAL I VS LOSE 502 .LU/ Lb/'Ub ,LbUU W 10/26/06 1600 GJ 3.66 $ 10/2VQ1 1G44 w 3.98 is 10/26/06 1600 GJ 3.62 10/26/06 1660 CG7 3.26 'k 10/26/06 1600 GJ 3.23 10/26/D6 1500 GJ 10/26/06 1600 GJ $6.43 iU/26/U6 1600 GJ 56.09 t 10/26/06 1.600 GJ 55.62 4 10/26/06 1660 GJ 55.28 % 10/26/06 1600 GJ 55.42 % 10/26/06 1600 GJ 4.00 fi LABORATORY DIRECTOR 1 e 12/15/2006 11:44 7045888333 PAR LABS CHAR NC HAGL 02 BENCH TOP PERCENT 'TTOTAL SOLIDS and TOTAL VOLITILE SOLIDS VAN KLZ3K FORMULA S S B Start! 10/26/09 1600 74685 Ende 11/30/06 TARE 17.327 10/26 1600 0,56425406 m15 smpl 18.5 DRIED WT. LEi.004 u BURNED 'WT. 17.622 5.16216226 t solids 3.66 TVs 0.382 0,677 % TVs- 56.43 TVS g/L 20,d4864E6 0.56425406 TAM 16.351 11/2 1540 0.56086037 mis smpi 19.3 0.9940018 DRIED WT. 17.041 0 BURNED Wr, 16.65i 5.01295337 4 Solids 3.58 TV$ 0.307 0.69 b TV$- 56.09 TV6 g/L 20.0518135 0.56086957 4 VS LOhO 0.60 TARE 18.498 11/9 1600 0.55817378 mlr. 9mpl 18.767 0,99519357 nRTRTI WT 1 q 177 n BURNED wT. 18.798 5.04875579 % solidt 3.62 TVS 0.379 0,679 $ TVs 55.82 TV0 g/L 20.1D50232 0.53017170 V VC L065 0.49 7AKE 13.843 11/19 1415 0.95275382 mle empl 18.316 0.99030774 DRIED WT. 16.442 0 BUM= wT, 16.112 4.50425657 4 Solids 3.26 TVS 0 . 33 0 .597 E TV.9 Mal TVS g/L 18.0170343 0,55276302 4 V9 LOSS 0.97 TARE 17.678 11/23 1530 0.554i958 mis smpl 17,598 1.00259059 DRIBA WT, 28.25 0 2URDTYD WT. 17.932 4.6033G366 ti Eolidb 3.2E; TVs 0,317 0.372 96 TVs- 5$"kn TVS g/L 18.01.34106 0,5541958 $ V9 LOSS -0.26 �,it!l�hCt.i��.�, ���i;,f";����iial�1�11?I �,�E��4•,6fl�14�;�,, 12/15/2006 11:44 704588833:a r AP?BORAr0 tas, INC. WWW. .aom PAR-J AFS MAR -NC CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-18333 Fax (704) 688-9335 PAGE 03 Shipping: Mailing: 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28273 Charlotte, NC 28241.1483 It is essential that al Information reCOrded on this Chain of Custody dooumont for accorAince by PAR Laboratories. InC, and tM North Carollna oeportment of Environmental and Netural Rasoureos. Company Neme WIlIngi SOUTHERN SOIL BUILDERS Address 088 HOOTS RD City, State & ZIP Code ROARING RIVER, NC 28689 Point of ContnM 1 Talap),b„o Nu❑1w, f UJ-2137MJ Samplo taken by: I, y - COMMENTS/SPECIAL INSTRUCTIONS IS THIS FOR STq4 or EPA REPORTING? YES � No •Sarrlple type: W _ WW �, (3WMW _ HW Soil _ Other Samplo Tamp of tuna: of sampling: �► •C Sample Te- mp upon receipt: 9C "* Preaerved; Yes No — Teflon Liner/ Zero Headspabe: Yes _- No � N/A (,' ' C ■ Compoeito 0 =Orab DW=D*king Weter WW -Wastewater GWMW =Groundwater Monitoring Wnil HW z Hazardoue Woote " Sen Other Side 0 LPA R LABORATORIES, INC. www.parlabs.com PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert N 20; SC Cert N 99003 REPORT OF ANALYSES Attn: DENNIS KEY SOUTHERN SOIL BUILDERS PROJECT NAME: SEP 06 958 HOOTS ROAD DATE: 09/21/06 ROARING RIVER, NC 28669-0000 SAMPLE NUMBER- 73702 SAMPLE ID- SPRUCE PINE DATE SAMPLED- 08/31/06 TIME SAMPLED- 14i;:0 DATE RECEIVED- 09/05/06 SAMPLER- ZACH KEY RECEIVED BY- MJ TIME RECEIVED- 1350 DELIVERED BY- ZACH KEY TYPE SAMPLE- Crab Page 1 of 3 ANALYSIS ANALYSIS METHOD DATE TIME BY RESUI.,T UL`'ITS TCLP CHARACTERISTICS TCLP 09/05/06 1600 CRB pH VALUE TCLP 09/05/06 1600 CRB 6.64 S.U. CORROSIVITY TCLP 09/05/06 1600 CRB < NON REACTIVITY TCLP 09/05/06 1600 CRB < NON FLASH POINT TCLP 09/05/06 1600 CRB > 140 degree; F IGNITABILITY TCLP 09/05/06 1600 CRB < NON PAINT FILTER TEST TCLP 09/05/06 1600 CRB <: NFL TCLP METALS TCLP 09/OS/06 1600 CRB ARSENIC TCLP 09/05/06 1600 CRB < 0.5 ppm BARIUM TCLP 09/05/06 1600 CRB < 10 ppm CADMIUM TCLP 09/05/06 1600 CRB < 0.1 ppm CHROMIUM TCLP 09/05/O6 1600 CRB < 0.5 ppm LEAD TCLP 09/05/06 :1.60n C..,R.B 0. r. rm MERCURY TCLP 09/05/06 1600 CRB < 0.02 ppm SELENIUM TCLP 09/05/06 1600 CRB < 0.1 ppm SILVER TCLP 09/05/06 1600 CRB < 0.5 ppm. TCLP PESTICIDES TCLP 09/05/06 1600 CRB ENDRIN TCLP 09/05/06 1600 CRB < 0.002 ppm LINDANE TCLP 09/05/06 1600 CRB < 0.04 ppm METHOXYCHLOR TCLP 09/05/06 1600 CRB < 1 ppm TOXAPHENE i r-• TCLP 09/05/06 1600 CRB < 0.05 ppm L R ATORIES, INC. www. parlabs. com Page 2 of 3 PAR Laboratories, Inc. 2217 Graham Park Drive PO Box 411483 Charlotte, NC 28241-1483 Phone: 704-588-8333; Fax: 704-588-8335 NC Cert # 20; SC Cert # 99003 CONTINUATION OF DATA FOR SAMPLE NUMBER 73702 ANALYSIS ANALYSIS METHOD DATE TIME BY RESULT UNITS CHLORDANE TCLP 09/05/06 1600 CRB < 0.003 ppm HEPTACHLOR (AND ITS EPDXIDE) TCLP 09/05/06 1600 CRB < 0.0008 ppm TCLP HERBICIDES TCLP 09/05/06 1600 CRB 2,4-D TCLP 09/05/06 1600 CRB < 1 ppm 2,4,5-TP(SILVEX) TCLP 09/05/06 1600 CRB < 0.1 ppm TCLP ORGANICS TCLP 09/05/06 1600 CRB BENZENE TCLP 09/05/06 1600 CRB < 0.05 ppm CARBON TETRACHLORIDE TCLP 09/05/06 1600 CRB < 0.05 ppm CHLOROBENZENE TCLP 09/05/06 1600 CRB < 10 ppm CHLOROFORM TCLP 09/05/06 1600 CRB < 0.6 ppm o-CRESOL TCLP 09/05/06 1600 CRB < 20 ppm p-CRESOL TCLP 09/05/06 1600 CRB < 20 ppm m-CRESOL TCLP 09/05/06 1600 CRB < 20 ppm 1,4-DICHLOROBENZENE TCLP 09/05/06 1600 CRB < 0.75 ppm 1,2-DICHLOROETHANE TCLP 09/05/06 1600 CRB < 0.05 ppm 1,1-DICHLOROETHYLENE TCLP 09/05/06 1600 CRB < 0.07 ppm 2,4-DINITROTLUENE TCLP 09/05/06 1600 CRB < 0.013 ppm HEXACHLOROBENZENE TCLP 09/05/06 1600 CRB < 0.013 ppm HEXACHLOROBUTDIENE TCLP 09/05/06 1600 CRB < 0.05 ppm HEXACHLOROETHANE TCLP 09/05/06 1600 CRB < 0.3 ppm METHYL ETHYL KETONE TCLP 09/05/06 1600 CRB < 20 ppm NITROBENZENE TCLP 09/05/06 1600 CRB < 0.2 ppm PENTACHLOROPHENOL TCLP 09/05/06 1600 CRB < 10 ppm PYRIDINE TCLP 09/05/06 1600 CRB < 0.5 ppm TETRACHLORETHYLENE TCiJP 09/05/06 1600 CF.Fi < 0.071 ppm TRICHLOROETHYLEivE TCLP 09/05/06 1600 CRB <; 0.05 ppm 2,4,5-TRICHLOROPHENOL TCLP 09/05/06 1600 CRB < 40 ppm 2,4,6-TRICHLORPHENOL TCLP 09/05/06 1600 CRB < 0.2 ppm VINYL CHLORIDE TCLP 09/05/06 1600 CRB < 0.02 ppm J/ e LABORATORY DIRECTOR PAR LABORATORIES, INC. MW www.parlabs.com Shipping: 2217 Graham Park Drive Charlotte, NC 28273 CHAIN OF CUSTODY PAR Laboratories, Inc Phone (704) 588-8333 Fax (704) 588-8335 Mailing: PO Box 411483 Charlotte, NC 28241-1483 It is essential that all information recorded on this Chain of Custody document for acceptance by PAR Laboratories, Inc. and the North Carolina Department of Environmental and Natural Resources. Company Name (billing) SOUTHERN SOIL BUILDERS Address 958 HOOTS RD City, State & Zip Code ROARING RIVER, NC 28669 Point of Contact & Telephone Number ..�.. ,� ea-, none COMMENTS/SPECIAL INSTRUCTIONS Sample taken by: IS THIS FOR STAT or EPA REPORTING? YES x NO *Sample type: D WWC)":f GWMW HW Soil Other Sample Temp at time of sampling: °C Sample Temp upon receipt: °C * * Preserved: Yes No Teflon Liner/ Zero Headspace: Yes — No __ NIA — Client Sample I.D. (Sample Location / Number) Comp Grab ,Preserv. $et Up. Date/T.iite Collection Date/Time nalyses Requested fie f (� ^� Z) U �C a T Relinquished by:� Date/Time Rec Iv d 1by: Date/Time o\\, R nquished by: Date/Time Received by: Date/The C=Composite G=Grab DW=Drinking Water WW=Wastewater GWMW=Groundwater Monitoring Well HW=Hazardous Waste •' See Other Side NCDA&CS At -- Division Phone: (919)733-2655 Web Site: Mvw.n 12ni2oo6 Agronomist Continents Soil Test Report SERVING N C. RESIDENTS FOR OVER 60 YL'ARS ,agr.com/agrononii/ Gruruer: Southern 958 Hoots R Roaring Rivc Farm: Gaston Co Field Information Applied Lime Iecommendations Sample No. Last Crop Mo Yr T/A Crop or Year Lime 63 1st Crop: Fes/OG/rim,M 0 120-200 211d Crop: Fes/OG/rim,M 0 120-200 Test Results Soil Class HM% W/V CEC BS% Ac p H P-1 K I 72 O Mg 19 Mn-] MIN 0.71 1.17 12.3 95.0 0.6 6.8 63 49 Fiefd,Information... Applied Lime Recorliregdati.ons Sample No. Last Crop Mo Yr T/A Crop or Year Lime 91 1st Crop: Fes/OG/I'im,M 0 120-200 211d Crop: Fes/OG/rim,M 0 120-200 Test Results Soil Class HM% W/V MIN 0.46 Field Information Sample No. Last Crop SP1 Test Results Soil Class HM% W/V MIN 0.27 1.18 Field Information Sample No. Last Crop U2 Test Results F l Class HM% WlV MIN 0.41 1.14 CEC BS% Ac pH P-I K-I 12.0 98.0 0.2 7.2 109 29 kpplied Lime Recommendations Mo Yr T,'A Crop or Year 1st Crop: Fes/OG/rim,M 211d Crop: Fes/OG/rim,M CEC BS% Ac pH P-I K-I 4.2 48.0 2.2 4.9 360 36 kpplied Lime Recommendations Mo Yr T/A Crop or Year I st Crop: Fes/OG/rim,M 211d Crop: Pes/OG/rim,M CEC l3S% AC p H P-1 K-1 n ()t1 a 2.0 5.0 340 50 Ca% Mg% Mn-I Mn- 85.0 12.0 783 Lime " I.AT 120-200 0 120-200 Ca% Pig% Mn-I rKn 34.0 9.0 86 Lime " 1.31' 120-200 0 120-200 Rennrt No: 14129 ;oil Builders, Inc. Copies To: l r, NC 2s669 Linty C -- 12, $ P205 K20 Mg S Cu Zn B Mn See A'ote 0-20 30-50 0 0 0 0 .0 pH$ 12 0-20 30-50 0 0 0 0 .0 pH$ 12 II(I)Mn-AI(2) Zn-I Zn-AI Cu-I S-I SS-1 NO3-N NH4-N Na 96 196 451 451 706 114 0.2 *^ :. P205 K20 Mg S Cu Zn B Mn See Note 0 70-90 0 0 0 0 .0 pH$ 12 0 70-90 0 0 0 0 .0 pH$ 12 AI(1)Mn-AI(2) Zn-1 Zn-AI Cu-1 S-I SS-1 NO3-N NH4-N Na i69 469 583 583 560 39 0.4 P205 K20 ' Pig S Cu Zn B Mn See Note 0 60-80 0 0 0 .0 0 12 0 60-80 0 0 0 .0 0 12 AI(1)Mn-AI(2) Zn-1 Zn-AI Cu-1 S-1 SS -I NO3-N NH4-N Na 69 69 393 393 446 28 0.1 P205 K20 Mg S Cu Zn B Mn See Note 0 30-50 0 0 0 0 .0 0 12 0 30-50 U o 0 0 .0 0 12 Al(1)Mn-AI(2) Zn-1 Z"-AI Cu-I S-1 SS-1 NO3-N NH4-N Na 0.I 110 ()-7 0-7 Q8 37 Ca% Mg% Mn-1 Mn 43.0 13.0 118 88