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HomeMy WebLinkAboutNC0006254_Groundwater Monitoring Report November 2022_20221130PO Box 604 ▪ Fletcher, NC 28732 ▪ Cell: 828-508-4510 November 30, 2022 Mr. Brett Laverty NCDEQ Division of Water Resources Asheville Regional Office 2090 US Highway 70 Swannanoa, NC 28778 RE: Groundwater Analytical Results – November 9, 2022 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Mr. Laverty: On November 9, 2022, Singleton Environmental, Inc. (SEI) visited the Blue Ridge Tissue site located at 1427 Yadkin River Road in Patterson, North Carolina, to collect groundwater samples from monitoring wells MW-1, MW-3, MW-4, MW-7 and MW-8. Monitoring wells MW-2 and MW-6 were dry, therefore, they were not sampled. The depth to groundwater in the remaining monitoring wells ranged from 6.05 feet in MW-4 to 20.73 feet in MW-3. Refer to Table 1 for all monitoring well groundwater depths and Figure 1 for all monitoring well locations. All groundwater samples, except for MW-2 and MW-6, were collected using a peristaltic pump connected to a Horiba U52-2 water quality meter with a flow-through-cell to collect groundwater parameters (temperature, pH, specific conductivity, dissolved oxygen, ORP, and turbidity). The groundwater samples were submitted on ice to Pace Analytical for the analysis of VOCs by EPA Method 6200B, 8-RCRA Metals, pH, ammonia, TKN, sulfate, nitrogen, nitrite and nitrate. The laboratory analysis of groundwater sample MW-1 detected concentrations of total iron and total manganese above the NCAC 2L groundwater standards. Both compounds were detected at concentrations higher than the July 2022 concentrations. The laboratory analysis of groundwater sample MW-3 detected concentrations of arsenic, total iron, total manganese, and ammonia above the NCAC 2L groundwater standards. All concentrations were higher than the July 2022 concentrations. The laboratory analysis of groundwater sample MW-4 detected concentrations of total iron and total manganese above the NCAC 2L groundwater standards. Both concentrations were higher than the July 2022 concentrations. The laboratory analysis of groundwater sample MW-7 detected concentrations of total iron above the NCAC 2L groundwater standards. The concentrations of total iron were higher than the July 2022 concentrations. Singleton Environmental, Inc. Singleton Environmental, Inc. Laboratory analysis of groundwater sample MW-8 did not detect any concentrations exceeding the NCAC 2L groundwater standards, however, the concentrations that were detected did increase from July 2022. The analytical results are shown on Table 2 and the attached laboratory data sheets. During the April 2017 groundwater sampling event, AECOM reported a possible sheen on the groundwater in monitoring well MW-4. During the November 2022 event a sheen was not observed; however, VOC samples were collected at all monitoring wells that contained enough water to sample. All of the monitoring well samples at the site were non-detect for VOCs during the November 2022 event. The compound levels detected in the groundwater analysis for the November 2022 sampling event detected relatively higher concentration levels in monitoring wells MW-1, MW-3, MW-4 and MW-7 compared to the July 2022 concentrations. Therefore, Singleton Environmental, Inc. recommends sampling the monitoring wells again in March 2023 to continue tracking the groundwater concentration and groundwater levels. If you have any questions, you can reach me at (828) 508-4510. Sincerely, Chris Singleton, P.G. Singleton Environmental, Inc. cc: Dave Hallock, Blue Ridge Tissue Corporation Attachments @A @A @A @A @A @A @A @A MW-2 MW-3 MW-4 MW-1 @A MW-5 MW-7 MW-6 MW-8 1 2 8 0 12 6 0 1 3 2 0 1340 1360 1380 1 2 4 0 142 0 1240 1420 Source: Esri, DigitalGlobe, GeoEye, Earthstar Geographics, CNES/AirbusDS, USDA, USGS, AEX, Getmapping, Aerogrid, IGN, IGP, swisstopo, and theGIS User Community Figure 60540673 1 May 2017 § 0 200 400Feet 1 inch = 200 feet Y a d k i n R i v e r R d Whisn a n t R d Yad k i n R i v e r Y a d k i n R i v e r Roby M a r t i n R d #0 Site Layout MapBlue Ridge Tissue CorporationPatterson, North Carolina Legend Property Boundary Yadkin River Flow Direction# Land Surface Elevation Contour (ft above mean sea level) Monitoring Well Location Abandoned Water Well#0@A Well ID Date Installed Total Depth (feet bls) Screened Interval (feet bls) Top of Casing Elevation (feet msl) Date Water Level Measured Depth to Water (feet BTOC) Groundwater Elevation (feet msl) MW-1 02/08/11 11 6-11 1253.71 11/09/22 12.41 1,241.30 MW-2 08/12/09 50 40-50 1323.03 Dry N/A N/A MW-3 08/13/09 20 10-20 1299.02 11/09/22 20.73 1,278.29 MW-4 08/13/09 15 5-15 1247.23 11/09/22 6.05 1,241.18 MW-5 08/16/11 21 11-21 1285.46 N/A N/A N/A MW-6 08/06/14 29 19-29 1341.55 Dry N/A N/A MW-7 08/06/14 24 14-24 1274.41 11/09/22 20.21 1,254.20 MW-8 08/06/14 20 10-20 1253.14 11/09/22 14.95 1,238.19 Notes: bls - feet below land surface BTOC - below top of casing msl - above mean sea level NG - not gauged AECOM Table 1 Monitoring Well Construction and Groundwater Elevations Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina Sample ID MW-1 MW-2*MW-3 MW-4 MW-6 MW-7 MW-8 Sample Date 11/09/22 11/09/22 11/09/22 11/09/22 11/09/22 11/09/22 11/09/22 Temperature (°C)NS 17.1 N/A 17.70 20.14 N/A 18.60 18.30 pH (standard units)NS 5.94 N/A 6.10 6.00 N/A 6.00 6.30 Specific Conductivity (mS/cm)NS 0.484 N/A 0.75 0.274 N/A 0.251 0.117 Dissolved Oxygen (mg/L)NS 0.71 N/A 2.10 1.94 N/A 4.70 4.60 ORP (mV)NS 70.0 N/A 12.00 102.0 N/A 80.0 86.0 Turbidity (NTU)NS 5.3 N/A 7.10 8.5 N/A 3.1 8.6 Gallons Pumped NS 2 N/A 0.5 2.5 N/A 1.5 2.5 Cloudy/Odor No/No No/Odor N/A Cloudy/Odor No/No N/A No/No No/No Total Barium (ug/L)700 130 N/A 5100 111 N/A 60 13 Total Iron (ug/L)300 35200 N/A 179000 16300 N/A 870 170 Total Manganese (ug/L)50 2800 N/A 5700 1600 N/A 23 2.9 Arsenic (ug/L)10 1.1 N/A 56 3.1 N/A ND ND Chromium (ug/L)10 1.8 N/A 5.9 2.3 N/A 1.7 ND Lead (ug/L)15 2.6 N/A 14 ND N/A ND ND Sulfate (mg/L)N/A ND N/A 19.6 8.5 N/A 2.1 18.8 Ammonia (mg/L)1.5 0.75 N/A 16 0.99 N/A ND ND TKN (mg/L)N/A 0.62 N/A 14.8 1.2 N/A ND ND Nitrogen NO2 plus NO3 (mg/L)N/A ND N/A ND ND N/A 1.5 2.1 Nitrate (mg/L)10 ND N/A ND ND N/A 1.5 2.1 Nitrite (mg/L)1 0.041 N/A 0.043 ND N/A ND ND pH (standard units)N/A 6.5 N/A 6.5 6.6 N/A 6.6 6.4 Total Disolved Solids (mg/L)N/A N/A N/A N/A N/A N/A N/A N/A EPA Method 6200B for VOCs N/A ND N/A ND ND N/A ND ND Notes: Samples analyzed for total and dissolved iron, barium and manganese by EPA Method 200.7 2L Standard - North Carolina groundwater quality standards established in Title 15A of the North Carolina Administrative Code, Subchapter 2L, Section 0.20 °C - degrees Celsius µS/cm - microsiemens per centimeter EPA - United States Environmental Protection Agency mg/L - milligrams per liter mV - millivolt NA - Not analyzed NS - No standard NTU - Nephelometric Turbidity Unit RCRA - Resource Conservation Recovery Act Bold samples indicate concentrations above the 2L Standard *MW-2 purged with disposable bailer, water quality parameters collected from same bail as sample. 2L Standard Field Parameters Analytical Parameters Table 2 Blue Ridge Tissue Corporation 1427 Yadkin River Road Patterson, North Carolina #=CL# November 30, 2022 LIMS USE: FR - CHRIS SINGLETON LIMS OBJECT ID: 92635728 92635728 Project: Pace Project No.: RE: Chris Singleton Singleton Environmental 105 Charlotte Highway Asheville, NC 28803 Blue Ridge Tissue Corp. 11/9 Dear Chris Singleton: Enclosed are the analytical results for sample(s) received by the laboratory on November 09, 2022. The results relate only to the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the laboratory's Quality Manual, where applicable, unless otherwise noted in the body of the report. The test results provided in this final report were generated by each of the following laboratories within the Pace Network: • Pace Analytical Services - Asheville • Pace Analytical Services - Charlotte If you have any questions concerning this report, please feel free to contact me. Sincerely, Lorri Patton lorri.patton@pacelabs.com Project Manager 1(828)254-7176 Enclosures REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 1 of 35 #=CP# CERTIFICATIONS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Pace Analytical Services Charlotte South Carolina Laboratory ID: 99006 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Laboratory ID: 99006 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DoH Drinking Water #: LA029 Virginia/VELAP Certification #: 460221 Pace Analytical Services Asheville 2225 Riverside Drive, Asheville, NC 28804 Florida/NELAP Certification #: E87648 North Carolina Drinking Water Certification #: 37712 North Carolina Wastewater Certification #: 40 South Carolina Laboratory ID: 99030 South Carolina Certification #: 99030001 Virginia/VELAP Certification #: 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 2 of 35 #=SA# SAMPLE ANALYTE COUNT Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Lab ID Sample ID Method Analytes Reported LaboratoryAnalysts 92635728001 MW-1 EPA 200.8 Rev 5.4 6 PASI-ACRW, DBB1 SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-AYEG EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-AARJ EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92635728002 MW-3 EPA 200.8 Rev 5.4 6 PASI-ACRW, DBB1 SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-AYEG EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-AARJ EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92635728003 MW-4 EPA 200.8 Rev 5.4 6 PASI-ACRW, DBB1 SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-AYEG EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-AARJ EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92635728004 MW-7 EPA 200.8 Rev 5.4 6 PASI-ADBB1 SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-AYEG EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-AARJ EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO 92635728005 MW-8 EPA 200.8 Rev 5.4 6 PASI-ADBB1 SM 6200B 63 PASI-CSAS SM 4500-H+B-2011 1 PASI-AYEG EPA 300.0 Rev 2.1 1993 1 PASI-ACDC EPA 350.1 Rev 2.0 1993 1 PASI-AARJ EPA 351.2 Rev 2.0 1993 1 PASI-AMFO EPA 353.2 Rev 2.0 1993 3 PASI-AMFO PASI-A = Pace Analytical Services - Asheville PASI-C = Pace Analytical Services - Charlotte REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 3 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-1 Lab ID:92635728001 Collected:11/09/22 10:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4 Pace Analytical Services - Asheville 200.8 MET ICPMS Arsenic 0.0011 mg/L 11/28/22 19:47 7440-38-211/28/22 09:280.0010 1 Barium 0.13 mg/L 11/28/22 19:47 7440-39-311/28/22 09:280.0010 1 Chromium 0.0018 mg/L 11/28/22 19:47 7440-47-311/28/22 09:280.0010 1 Iron 35.2 mg/L 11/29/22 16:58 7439-89-6 M111/28/22 09:281.0 20 Lead 0.0026 mg/L 11/28/22 19:47 7439-92-111/28/22 09:280.0010 1 Manganese 2.8 mg/L 11/29/22 16:58 7439-96-5 M111/28/22 09:280.040 20 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/13/22 12:37 71-43-20.50 1 Bromobenzene ND ug/L 11/13/22 12:37 108-86-10.50 1 Bromochloromethane ND ug/L 11/13/22 12:37 74-97-50.50 1 Bromodichloromethane ND ug/L 11/13/22 12:37 75-27-40.50 1 Bromoform ND ug/L 11/13/22 12:37 75-25-20.50 1 Bromomethane ND ug/L 11/13/22 12:37 74-83-95.0 1 n-Butylbenzene ND ug/L 11/13/22 12:37 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/13/22 12:37 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/13/22 12:37 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/13/22 12:37 56-23-50.50 1 Chlorobenzene ND ug/L 11/13/22 12:37 108-90-70.50 1 Chloroethane ND ug/L 11/13/22 12:37 75-00-31.0 1 Chloroform ND ug/L 11/13/22 12:37 67-66-30.50 1 Chloromethane ND ug/L 11/13/22 12:37 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/13/22 12:37 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/13/22 12:37 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/13/22 12:37 96-12-81.0 1 Dibromochloromethane ND ug/L 11/13/22 12:37 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/13/22 12:37 106-93-40.50 1 Dibromomethane ND ug/L 11/13/22 12:37 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/13/22 12:37 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/13/22 12:37 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/13/22 12:37 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/13/22 12:37 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/13/22 12:37 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/13/22 12:37 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/13/22 12:37 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/13/22 12:37 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/13/22 12:37 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/13/22 12:37 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/13/22 12:37 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/13/22 12:37 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/13/22 12:37 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/13/22 12:37 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/13/22 12:37 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/13/22 12:37 108-20-30.50 1 Ethylbenzene ND ug/L 11/13/22 12:37 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 4 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-1 Lab ID:92635728001 Collected:11/09/22 10:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/13/22 12:37 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/13/22 12:37 98-82-80.50 1 Methylene Chloride ND ug/L 11/13/22 12:37 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/13/22 12:37 1634-04-40.50 1 Naphthalene ND ug/L 11/13/22 12:37 91-20-32.0 1 n-Propylbenzene ND ug/L 11/13/22 12:37 103-65-10.50 1 Styrene ND ug/L 11/13/22 12:37 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/13/22 12:37 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/13/22 12:37 79-34-50.50 1 Tetrachloroethene ND ug/L 11/13/22 12:37 127-18-40.50 1 Toluene ND ug/L 11/13/22 12:37 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/13/22 12:37 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/13/22 12:37 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/13/22 12:37 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/13/22 12:37 79-00-50.50 1 Trichloroethene ND ug/L 11/13/22 12:37 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/13/22 12:37 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/13/22 12:37 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/13/22 12:37 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/13/22 12:37 108-67-80.50 1 Vinyl chloride ND ug/L 11/13/22 12:37 75-01-41.0 1 m&p-Xylene ND ug/L 11/13/22 12:37 179601-23-11.0 1 o-Xylene ND ug/L 11/13/22 12:37 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)101 %11/13/22 12:37 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %11/13/22 12:37 460-00-470-130 1 Toluene-d8 (S)104 %11/13/22 12:37 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.5 Std. Units 11/14/22 14:52 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate ND mg/L 11/10/22 22:20 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.75 mg/L 11/10/22 15:11 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 0.62 mg/L 11/17/22 05:44 7727-37-911/16/22 16:240.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 5 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-1 Lab ID:92635728001 Collected:11/09/22 10:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/10/22 02:090.040 1 Nitrogen, Nitrate ND mg/L 11/10/22 02:09 14797-55-80.040 1 Nitrogen, Nitrite 0.041 mg/L 11/10/22 02:09 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 6 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-3 Lab ID:92635728002 Collected:11/09/22 10:35 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4 Pace Analytical Services - Asheville 200.8 MET ICPMS Arsenic 0.056 mg/L 11/28/22 20:06 7440-38-211/28/22 09:280.0010 1 Barium 0.51 mg/L 11/29/22 17:10 7440-39-311/28/22 09:280.020 20 Chromium 0.0059 mg/L 11/28/22 20:06 7440-47-311/28/22 09:280.0010 1 Iron 179 mg/L 11/30/22 00:27 7439-89-611/28/22 09:282.5 50 Lead 0.014 mg/L 11/28/22 20:06 7439-92-111/28/22 09:280.0010 1 Manganese 5.7 mg/L 11/30/22 00:27 7439-96-511/28/22 09:280.10 50 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/13/22 12:55 71-43-20.50 1 Bromobenzene ND ug/L 11/13/22 12:55 108-86-10.50 1 Bromochloromethane ND ug/L 11/13/22 12:55 74-97-50.50 1 Bromodichloromethane ND ug/L 11/13/22 12:55 75-27-40.50 1 Bromoform ND ug/L 11/13/22 12:55 75-25-20.50 1 Bromomethane ND ug/L 11/13/22 12:55 74-83-95.0 1 n-Butylbenzene ND ug/L 11/13/22 12:55 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/13/22 12:55 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/13/22 12:55 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/13/22 12:55 56-23-50.50 1 Chlorobenzene ND ug/L 11/13/22 12:55 108-90-70.50 1 Chloroethane ND ug/L 11/13/22 12:55 75-00-31.0 1 Chloroform ND ug/L 11/13/22 12:55 67-66-30.50 1 Chloromethane ND ug/L 11/13/22 12:55 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/13/22 12:55 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/13/22 12:55 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/13/22 12:55 96-12-81.0 1 Dibromochloromethane ND ug/L 11/13/22 12:55 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/13/22 12:55 106-93-40.50 1 Dibromomethane ND ug/L 11/13/22 12:55 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/13/22 12:55 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/13/22 12:55 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/13/22 12:55 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/13/22 12:55 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/13/22 12:55 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/13/22 12:55 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/13/22 12:55 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/13/22 12:55 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/13/22 12:55 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/13/22 12:55 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/13/22 12:55 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/13/22 12:55 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/13/22 12:55 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/13/22 12:55 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/13/22 12:55 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/13/22 12:55 108-20-30.50 1 Ethylbenzene ND ug/L 11/13/22 12:55 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 7 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-3 Lab ID:92635728002 Collected:11/09/22 10:35 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/13/22 12:55 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/13/22 12:55 98-82-80.50 1 Methylene Chloride ND ug/L 11/13/22 12:55 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/13/22 12:55 1634-04-40.50 1 Naphthalene ND ug/L 11/13/22 12:55 91-20-32.0 1 n-Propylbenzene ND ug/L 11/13/22 12:55 103-65-10.50 1 Styrene ND ug/L 11/13/22 12:55 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/13/22 12:55 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/13/22 12:55 79-34-50.50 1 Tetrachloroethene ND ug/L 11/13/22 12:55 127-18-40.50 1 Toluene ND ug/L 11/13/22 12:55 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/13/22 12:55 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/13/22 12:55 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/13/22 12:55 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/13/22 12:55 79-00-50.50 1 Trichloroethene ND ug/L 11/13/22 12:55 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/13/22 12:55 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/13/22 12:55 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/13/22 12:55 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/13/22 12:55 108-67-80.50 1 Vinyl chloride ND ug/L 11/13/22 12:55 75-01-41.0 1 m&p-Xylene ND ug/L 11/13/22 12:55 179601-23-11.0 1 o-Xylene ND ug/L 11/13/22 12:55 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %11/13/22 12:55 17060-07-070-130 1 4-Bromofluorobenzene (S)100 %11/13/22 12:55 460-00-470-130 1 Toluene-d8 (S)103 %11/13/22 12:55 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.7 Std. Units 11/14/22 14:53 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 19.6 mg/L 11/10/22 22:36 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 16.0 mg/L 11/10/22 15:12 7664-41-70.20 2 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 14.8 mg/L 11/17/22 05:45 7727-37-911/16/22 16:240.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 8 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-3 Lab ID:92635728002 Collected:11/09/22 10:35 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/10/22 02:100.040 1 Nitrogen, Nitrate ND mg/L 11/10/22 02:10 14797-55-80.040 1 Nitrogen, Nitrite 0.043 mg/L 11/10/22 02:10 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 9 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-4 Lab ID:92635728003 Collected:11/09/22 13:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4 Pace Analytical Services - Asheville 200.8 MET ICPMS Arsenic 0.0031 mg/L 11/28/22 20:10 7440-38-211/28/22 09:280.0010 1 Barium 0.11 mg/L 11/28/22 20:10 7440-39-311/28/22 09:280.0010 1 Chromium 0.0023 mg/L 11/28/22 20:10 7440-47-311/28/22 09:280.0010 1 Iron 16.3 mg/L 11/29/22 17:13 7439-89-611/28/22 09:281.0 20 Lead ND mg/L 11/28/22 20:10 7439-92-111/28/22 09:280.0010 1 Manganese 1.6 mg/L 11/29/22 17:13 7439-96-511/28/22 09:280.040 20 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/13/22 13:13 71-43-20.50 1 Bromobenzene ND ug/L 11/13/22 13:13 108-86-10.50 1 Bromochloromethane ND ug/L 11/13/22 13:13 74-97-50.50 1 Bromodichloromethane ND ug/L 11/13/22 13:13 75-27-40.50 1 Bromoform ND ug/L 11/13/22 13:13 75-25-20.50 1 Bromomethane ND ug/L 11/13/22 13:13 74-83-95.0 1 n-Butylbenzene ND ug/L 11/13/22 13:13 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/13/22 13:13 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/13/22 13:13 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/13/22 13:13 56-23-50.50 1 Chlorobenzene ND ug/L 11/13/22 13:13 108-90-70.50 1 Chloroethane ND ug/L 11/13/22 13:13 75-00-31.0 1 Chloroform ND ug/L 11/13/22 13:13 67-66-30.50 1 Chloromethane ND ug/L 11/13/22 13:13 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/13/22 13:13 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/13/22 13:13 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/13/22 13:13 96-12-81.0 1 Dibromochloromethane ND ug/L 11/13/22 13:13 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/13/22 13:13 106-93-40.50 1 Dibromomethane ND ug/L 11/13/22 13:13 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/13/22 13:13 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/13/22 13:13 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/13/22 13:13 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/13/22 13:13 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/13/22 13:13 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/13/22 13:13 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/13/22 13:13 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/13/22 13:13 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/13/22 13:13 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/13/22 13:13 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/13/22 13:13 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/13/22 13:13 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/13/22 13:13 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/13/22 13:13 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/13/22 13:13 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/13/22 13:13 108-20-30.50 1 Ethylbenzene ND ug/L 11/13/22 13:13 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 10 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-4 Lab ID:92635728003 Collected:11/09/22 13:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/13/22 13:13 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/13/22 13:13 98-82-80.50 1 Methylene Chloride ND ug/L 11/13/22 13:13 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/13/22 13:13 1634-04-40.50 1 Naphthalene ND ug/L 11/13/22 13:13 91-20-32.0 1 n-Propylbenzene ND ug/L 11/13/22 13:13 103-65-10.50 1 Styrene ND ug/L 11/13/22 13:13 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/13/22 13:13 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/13/22 13:13 79-34-50.50 1 Tetrachloroethene ND ug/L 11/13/22 13:13 127-18-40.50 1 Toluene ND ug/L 11/13/22 13:13 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/13/22 13:13 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/13/22 13:13 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/13/22 13:13 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/13/22 13:13 79-00-50.50 1 Trichloroethene ND ug/L 11/13/22 13:13 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/13/22 13:13 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/13/22 13:13 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/13/22 13:13 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/13/22 13:13 108-67-80.50 1 Vinyl chloride ND ug/L 11/13/22 13:13 75-01-41.0 1 m&p-Xylene ND ug/L 11/13/22 13:13 179601-23-11.0 1 o-Xylene ND ug/L 11/13/22 13:13 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)103 %11/13/22 13:13 17060-07-070-130 1 4-Bromofluorobenzene (S)103 %11/13/22 13:13 460-00-470-130 1 Toluene-d8 (S)102 %11/13/22 13:13 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.6 Std. Units 11/14/22 15:01 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 8.5 mg/L 11/10/22 22:52 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia 0.99 mg/L 11/10/22 15:17 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total 1.2 mg/L 11/17/22 05:47 7727-37-911/16/22 16:240.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 11 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-4 Lab ID:92635728003 Collected:11/09/22 13:00 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 ND mg/L 11/10/22 02:210.040 1 Nitrogen, Nitrate ND mg/L 11/10/22 02:21 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/10/22 02:21 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 12 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-7 Lab ID:92635728004 Collected:11/09/22 12:10 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4 Pace Analytical Services - Asheville 200.8 MET ICPMS Arsenic ND mg/L 11/28/22 20:14 7440-38-211/28/22 09:280.0010 1 Barium 0.060 mg/L 11/28/22 20:14 7440-39-311/28/22 09:280.0010 1 Chromium 0.0017 mg/L 11/28/22 20:14 7440-47-311/28/22 09:280.0010 1 Iron 0.87 mg/L 11/28/22 20:14 7439-89-611/28/22 09:280.050 1 Lead ND mg/L 11/28/22 20:14 7439-92-111/28/22 09:280.0010 1 Manganese 0.023 mg/L 11/28/22 20:14 7439-96-511/28/22 09:280.0020 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/13/22 13:31 71-43-20.50 1 Bromobenzene ND ug/L 11/13/22 13:31 108-86-10.50 1 Bromochloromethane ND ug/L 11/13/22 13:31 74-97-50.50 1 Bromodichloromethane ND ug/L 11/13/22 13:31 75-27-40.50 1 Bromoform ND ug/L 11/13/22 13:31 75-25-20.50 1 Bromomethane ND ug/L 11/13/22 13:31 74-83-95.0 1 n-Butylbenzene ND ug/L 11/13/22 13:31 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/13/22 13:31 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/13/22 13:31 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/13/22 13:31 56-23-50.50 1 Chlorobenzene ND ug/L 11/13/22 13:31 108-90-70.50 1 Chloroethane ND ug/L 11/13/22 13:31 75-00-31.0 1 Chloroform ND ug/L 11/13/22 13:31 67-66-30.50 1 Chloromethane ND ug/L 11/13/22 13:31 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/13/22 13:31 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/13/22 13:31 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/13/22 13:31 96-12-81.0 1 Dibromochloromethane ND ug/L 11/13/22 13:31 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/13/22 13:31 106-93-40.50 1 Dibromomethane ND ug/L 11/13/22 13:31 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/13/22 13:31 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/13/22 13:31 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/13/22 13:31 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/13/22 13:31 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/13/22 13:31 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/13/22 13:31 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/13/22 13:31 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/13/22 13:31 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/13/22 13:31 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/13/22 13:31 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/13/22 13:31 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/13/22 13:31 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/13/22 13:31 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/13/22 13:31 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/13/22 13:31 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/13/22 13:31 108-20-30.50 1 Ethylbenzene ND ug/L 11/13/22 13:31 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 13 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-7 Lab ID:92635728004 Collected:11/09/22 12:10 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/13/22 13:31 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/13/22 13:31 98-82-80.50 1 Methylene Chloride ND ug/L 11/13/22 13:31 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/13/22 13:31 1634-04-40.50 1 Naphthalene ND ug/L 11/13/22 13:31 91-20-32.0 1 n-Propylbenzene ND ug/L 11/13/22 13:31 103-65-10.50 1 Styrene ND ug/L 11/13/22 13:31 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/13/22 13:31 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/13/22 13:31 79-34-50.50 1 Tetrachloroethene ND ug/L 11/13/22 13:31 127-18-40.50 1 Toluene ND ug/L 11/13/22 13:31 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/13/22 13:31 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/13/22 13:31 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/13/22 13:31 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/13/22 13:31 79-00-50.50 1 Trichloroethene ND ug/L 11/13/22 13:31 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/13/22 13:31 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/13/22 13:31 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/13/22 13:31 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/13/22 13:31 108-67-80.50 1 Vinyl chloride ND ug/L 11/13/22 13:31 75-01-41.0 1 m&p-Xylene ND ug/L 11/13/22 13:31 179601-23-11.0 1 o-Xylene ND ug/L 11/13/22 13:31 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)100 %11/13/22 13:31 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/13/22 13:31 460-00-470-130 1 Toluene-d8 (S)105 %11/13/22 13:31 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.6 Std. Units 11/14/22 14:59 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 2.1 mg/L 11/10/22 23:08 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 11/10/22 15:18 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 11/17/22 05:48 7727-37-911/16/22 16:240.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 14 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-7 Lab ID:92635728004 Collected:11/09/22 12:10 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 1.5 mg/L 11/10/22 02:170.040 1 Nitrogen, Nitrate 1.5 mg/L 11/10/22 02:17 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/10/22 02:17 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 15 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-8 Lab ID:92635728005 Collected:11/09/22 11:30 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 200.8 Rev 5.4 Preparation Method: EPA 200.8 Rev 5.4 Pace Analytical Services - Asheville 200.8 MET ICPMS Arsenic ND mg/L 11/28/22 20:18 7440-38-211/28/22 09:280.0010 1 Barium 0.013 mg/L 11/28/22 20:18 7440-39-311/28/22 09:280.0010 1 Chromium ND mg/L 11/28/22 20:18 7440-47-311/28/22 09:280.0010 1 Iron 0.17 mg/L 11/28/22 20:18 7439-89-611/28/22 09:280.050 1 Lead ND mg/L 11/28/22 20:18 7439-92-111/28/22 09:280.0010 1 Manganese 0.0029 mg/L 11/28/22 20:18 7439-96-511/28/22 09:280.0020 1 Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Benzene ND ug/L 11/13/22 13:49 71-43-20.50 1 Bromobenzene ND ug/L 11/13/22 13:49 108-86-10.50 1 Bromochloromethane ND ug/L 11/13/22 13:49 74-97-50.50 1 Bromodichloromethane ND ug/L 11/13/22 13:49 75-27-40.50 1 Bromoform ND ug/L 11/13/22 13:49 75-25-20.50 1 Bromomethane ND ug/L 11/13/22 13:49 74-83-95.0 1 n-Butylbenzene ND ug/L 11/13/22 13:49 104-51-80.50 1 sec-Butylbenzene ND ug/L 11/13/22 13:49 135-98-80.50 1 tert-Butylbenzene ND ug/L 11/13/22 13:49 98-06-60.50 1 Carbon tetrachloride ND ug/L 11/13/22 13:49 56-23-50.50 1 Chlorobenzene ND ug/L 11/13/22 13:49 108-90-70.50 1 Chloroethane ND ug/L 11/13/22 13:49 75-00-31.0 1 Chloroform ND ug/L 11/13/22 13:49 67-66-30.50 1 Chloromethane ND ug/L 11/13/22 13:49 74-87-31.0 1 2-Chlorotoluene ND ug/L 11/13/22 13:49 95-49-80.50 1 4-Chlorotoluene ND ug/L 11/13/22 13:49 106-43-40.50 1 1,2-Dibromo-3-chloropropane ND ug/L 11/13/22 13:49 96-12-81.0 1 Dibromochloromethane ND ug/L 11/13/22 13:49 124-48-10.50 1 1,2-Dibromoethane (EDB)ND ug/L 11/13/22 13:49 106-93-40.50 1 Dibromomethane ND ug/L 11/13/22 13:49 74-95-30.50 1 1,2-Dichlorobenzene ND ug/L 11/13/22 13:49 95-50-10.50 1 1,3-Dichlorobenzene ND ug/L 11/13/22 13:49 541-73-10.50 1 1,4-Dichlorobenzene ND ug/L 11/13/22 13:49 106-46-70.50 1 Dichlorodifluoromethane ND ug/L 11/13/22 13:49 75-71-80.50 1 1,1-Dichloroethane ND ug/L 11/13/22 13:49 75-34-30.50 1 1,2-Dichloroethane ND ug/L 11/13/22 13:49 107-06-20.50 1 1,1-Dichloroethene ND ug/L 11/13/22 13:49 75-35-40.50 1 cis-1,2-Dichloroethene ND ug/L 11/13/22 13:49 156-59-20.50 1 trans-1,2-Dichloroethene ND ug/L 11/13/22 13:49 156-60-50.50 1 1,2-Dichloropropane ND ug/L 11/13/22 13:49 78-87-50.50 1 1,3-Dichloropropane ND ug/L 11/13/22 13:49 142-28-90.50 1 2,2-Dichloropropane ND ug/L 11/13/22 13:49 594-20-70.50 1 1,1-Dichloropropene ND ug/L 11/13/22 13:49 563-58-60.50 1 cis-1,3-Dichloropropene ND ug/L 11/13/22 13:49 10061-01-50.50 1 trans-1,3-Dichloropropene ND ug/L 11/13/22 13:49 10061-02-60.50 1 Diisopropyl ether ND ug/L 11/13/22 13:49 108-20-30.50 1 Ethylbenzene ND ug/L 11/13/22 13:49 100-41-40.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 16 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-8 Lab ID:92635728005 Collected:11/09/22 11:30 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: SM 6200B Pace Analytical Services - Charlotte 6200B MSV Hexachloro-1,3-butadiene ND ug/L 11/13/22 13:49 87-68-32.0 1 Isopropylbenzene (Cumene)ND ug/L 11/13/22 13:49 98-82-80.50 1 Methylene Chloride ND ug/L 11/13/22 13:49 75-09-22.0 1 Methyl-tert-butyl ether ND ug/L 11/13/22 13:49 1634-04-40.50 1 Naphthalene ND ug/L 11/13/22 13:49 91-20-32.0 1 n-Propylbenzene ND ug/L 11/13/22 13:49 103-65-10.50 1 Styrene ND ug/L 11/13/22 13:49 100-42-50.50 1 1,1,1,2-Tetrachloroethane ND ug/L 11/13/22 13:49 630-20-60.50 1 1,1,2,2-Tetrachloroethane ND ug/L 11/13/22 13:49 79-34-50.50 1 Tetrachloroethene ND ug/L 11/13/22 13:49 127-18-40.50 1 Toluene ND ug/L 11/13/22 13:49 108-88-30.50 1 1,2,3-Trichlorobenzene ND ug/L 11/13/22 13:49 87-61-62.0 1 1,2,4-Trichlorobenzene ND ug/L 11/13/22 13:49 120-82-12.0 1 1,1,1-Trichloroethane ND ug/L 11/13/22 13:49 71-55-60.50 1 1,1,2-Trichloroethane ND ug/L 11/13/22 13:49 79-00-50.50 1 Trichloroethene ND ug/L 11/13/22 13:49 79-01-60.50 1 Trichlorofluoromethane ND ug/L 11/13/22 13:49 75-69-41.0 1 1,2,3-Trichloropropane ND ug/L 11/13/22 13:49 96-18-40.50 1 1,2,4-Trimethylbenzene ND ug/L 11/13/22 13:49 95-63-60.50 1 1,3,5-Trimethylbenzene ND ug/L 11/13/22 13:49 108-67-80.50 1 Vinyl chloride ND ug/L 11/13/22 13:49 75-01-41.0 1 m&p-Xylene ND ug/L 11/13/22 13:49 179601-23-11.0 1 o-Xylene ND ug/L 11/13/22 13:49 95-47-60.50 1 Surrogates 1,2-Dichloroethane-d4 (S)102 %11/13/22 13:49 17060-07-070-130 1 4-Bromofluorobenzene (S)101 %11/13/22 13:49 460-00-470-130 1 Toluene-d8 (S)104 %11/13/22 13:49 2037-26-570-130 1 Analytical Method: SM 4500-H+B-2011 Pace Analytical Services - Asheville 4500H+ pH, Electrometric pH at 25 Degrees C 6.4 Std. Units 11/14/22 14:56 H30.10 1 Analytical Method: EPA 300.0 Rev 2.1 1993 Pace Analytical Services - Asheville 300.0 IC Anions 28 Days Sulfate 18.8 mg/L 11/10/22 23:24 14808-79-81.0 1 Analytical Method: EPA 350.1 Rev 2.0 1993 Pace Analytical Services - Asheville 350.1 Ammonia Nitrogen, Ammonia ND mg/L 11/10/22 15:20 7664-41-70.10 1 Analytical Method: EPA 351.2 Rev 2.0 1993 Preparation Method: EPA 351.2 Rev 2.0 1993 Pace Analytical Services - Asheville 351.2 Total Kjeldahl Nitrogen Nitrogen, Kjeldahl, Total ND mg/L 11/17/22 05:49 7727-37-911/16/22 16:240.50 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 17 of 35 #=AR# ANALYTICAL RESULTS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Sample:MW-8 Lab ID:92635728005 Collected:11/09/22 11:30 Received:11/09/22 15:15 Matrix:Water Parameters Results Units DF Prepared Analyzed CAS No.QualReport Limit Analytical Method: EPA 353.2 Rev 2.0 1993 Pace Analytical Services - Asheville 353.2 Nitrogen, NO2/NO3 unpres Nitrogen, NO2 plus NO3 2.1 mg/L 11/10/22 02:110.040 1 Nitrogen, Nitrate 2.1 mg/L 11/10/22 02:11 14797-55-80.040 1 Nitrogen, Nitrite ND mg/L 11/10/22 02:11 14797-65-00.040 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 18 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 739454 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 200.8 MET Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3847558 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed Arsenic mg/L ND 0.0010 11/28/22 19:39 Barium mg/L ND 0.0010 11/28/22 19:39 Chromium mg/L ND 0.0010 11/28/22 19:39 Iron mg/L ND 0.050 11/28/22 19:39 Lead mg/L ND 0.0010 11/28/22 19:39 Manganese mg/L ND 0.0020 11/28/22 19:39 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3847559LABORATORY CONTROL SAMPLE: LCSSpike Arsenic mg/L 0.0500.05 101 85-115 Barium mg/L 0.0510.05 102 85-115 Chromium mg/L 0.0510.05 103 85-115 Iron mg/L 1.31.2 105 85-115 Lead mg/L 0.0500.05 100 85-115 Manganese mg/L 0.0510.05 103 85-115 Parameter Units MS Result % Rec Limits Qual% RecConc. 3847560MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635728001 3847561 MSD Result MSD % Rec RPD MSDMS Spike Conc. Arsenic mg/L 0.05 100 70-13099 10.050.0011 0.051 0.050 Barium mg/L 0.05 95 70-130100 20.050.13 0.18 0.18 Chromium mg/L 0.05 99 70-130100 10.050.0018 0.051 0.052 Iron mg/L M11.2 -41 70-130-116 31.235.2 34.6 33.7 Lead mg/L 0.05 101 70-13099 20.050.0026 0.053 0.052 Manganese mg/L M10.05 -239 70-130-378 30.052.8 2.7 2.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 19 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736729 SM 6200B SM 6200B 6200B MSV Laboratory:Pace Analytical Services - Charlotte Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3834279 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed 1,1,1,2-Tetrachloroethane ug/L ND 0.50 11/13/22 09:19 1,1,1-Trichloroethane ug/L ND 0.50 11/13/22 09:19 1,1,2,2-Tetrachloroethane ug/L ND 0.50 11/13/22 09:19 1,1,2-Trichloroethane ug/L ND 0.50 11/13/22 09:19 1,1-Dichloroethane ug/L ND 0.50 11/13/22 09:19 1,1-Dichloroethene ug/L ND 0.50 11/13/22 09:19 1,1-Dichloropropene ug/L ND 0.50 11/13/22 09:19 1,2,3-Trichlorobenzene ug/L ND 2.0 11/13/22 09:19 1,2,3-Trichloropropane ug/L ND 0.50 11/13/22 09:19 1,2,4-Trichlorobenzene ug/L ND 2.0 11/13/22 09:19 1,2,4-Trimethylbenzene ug/L ND 0.50 11/13/22 09:19 1,2-Dibromo-3-chloropropane ug/L ND 1.0 11/13/22 09:19 1,2-Dibromoethane (EDB)ug/L ND 0.50 11/13/22 09:19 1,2-Dichlorobenzene ug/L ND 0.50 11/13/22 09:19 1,2-Dichloroethane ug/L ND 0.50 11/13/22 09:19 1,2-Dichloropropane ug/L ND 0.50 11/13/22 09:19 1,3,5-Trimethylbenzene ug/L ND 0.50 11/13/22 09:19 1,3-Dichlorobenzene ug/L ND 0.50 11/13/22 09:19 1,3-Dichloropropane ug/L ND 0.50 11/13/22 09:19 1,4-Dichlorobenzene ug/L ND 0.50 11/13/22 09:19 2,2-Dichloropropane ug/L ND 0.50 11/13/22 09:19 2-Chlorotoluene ug/L ND 0.50 11/13/22 09:19 4-Chlorotoluene ug/L ND 0.50 11/13/22 09:19 Benzene ug/L ND 0.50 11/13/22 09:19 Bromobenzene ug/L ND 0.50 11/13/22 09:19 Bromochloromethane ug/L ND 0.50 11/13/22 09:19 Bromodichloromethane ug/L ND 0.50 11/13/22 09:19 Bromoform ug/L ND 0.50 11/13/22 09:19 Bromomethane ug/L ND 5.0 11/13/22 09:19 Carbon tetrachloride ug/L ND 0.50 11/13/22 09:19 Chlorobenzene ug/L ND 0.50 11/13/22 09:19 Chloroethane ug/L ND 1.0 11/13/22 09:19 Chloroform ug/L ND 0.50 11/13/22 09:19 Chloromethane ug/L ND 1.0 11/13/22 09:19 cis-1,2-Dichloroethene ug/L ND 0.50 11/13/22 09:19 cis-1,3-Dichloropropene ug/L ND 0.50 11/13/22 09:19 Dibromochloromethane ug/L ND 0.50 11/13/22 09:19 Dibromomethane ug/L ND 0.50 11/13/22 09:19 Dichlorodifluoromethane ug/L ND 0.50 11/13/22 09:19 Diisopropyl ether ug/L ND 0.50 11/13/22 09:19 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 20 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3834279 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed Ethylbenzene ug/L ND 0.50 11/13/22 09:19 Hexachloro-1,3-butadiene ug/L ND 2.0 11/13/22 09:19 Isopropylbenzene (Cumene)ug/L ND 0.50 11/13/22 09:19 m&p-Xylene ug/L ND 1.0 11/13/22 09:19 Methyl-tert-butyl ether ug/L ND 0.50 11/13/22 09:19 Methylene Chloride ug/L ND 2.0 11/13/22 09:19 n-Butylbenzene ug/L ND 0.50 11/13/22 09:19 n-Propylbenzene ug/L ND 0.50 11/13/22 09:19 Naphthalene ug/L ND 2.0 11/13/22 09:19 o-Xylene ug/L ND 0.50 11/13/22 09:19 sec-Butylbenzene ug/L ND 0.50 11/13/22 09:19 Styrene ug/L ND 0.50 11/13/22 09:19 tert-Butylbenzene ug/L ND 0.50 11/13/22 09:19 Tetrachloroethene ug/L ND 0.50 11/13/22 09:19 Toluene ug/L ND 0.50 11/13/22 09:19 trans-1,2-Dichloroethene ug/L ND 0.50 11/13/22 09:19 trans-1,3-Dichloropropene ug/L ND 0.50 11/13/22 09:19 Trichloroethene ug/L ND 0.50 11/13/22 09:19 Trichlorofluoromethane ug/L ND 1.0 11/13/22 09:19 Vinyl chloride ug/L ND 1.0 11/13/22 09:19 1,2-Dichloroethane-d4 (S)%102 70-130 11/13/22 09:19 4-Bromofluorobenzene (S)%103 70-130 11/13/22 09:19 Toluene-d8 (S)%102 70-130 11/13/22 09:19 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3834280LABORATORY CONTROL SAMPLE: LCSSpike 1,1,1,2-Tetrachloroethane ug/L 53.250 106 60-140 1,1,1-Trichloroethane ug/L 53.950 108 60-140 1,1,2,2-Tetrachloroethane ug/L 51.850 104 60-140 1,1,2-Trichloroethane ug/L 50.550 101 60-140 1,1-Dichloroethane ug/L 50.250 100 60-140 1,1-Dichloroethene ug/L 52.650 105 60-140 1,1-Dichloropropene ug/L 57.650 115 60-140 1,2,3-Trichlorobenzene ug/L 47.850 96 60-140 1,2,3-Trichloropropane ug/L 52.250 104 60-140 1,2,4-Trichlorobenzene ug/L 49.550 99 60-140 1,2,4-Trimethylbenzene ug/L 49.750 99 60-140 1,2-Dibromo-3-chloropropane ug/L 48.550 97 60-140 1,2-Dibromoethane (EDB)ug/L 53.150 106 60-140 1,2-Dichlorobenzene ug/L 50.750 101 60-140 1,2-Dichloroethane ug/L 50.350 101 60-140 1,2-Dichloropropane ug/L 49.550 99 60-140 1,3,5-Trimethylbenzene ug/L 52.150 104 60-140 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 21 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3834280LABORATORY CONTROL SAMPLE: LCSSpike 1,3-Dichlorobenzene ug/L 51.150 102 60-140 1,3-Dichloropropane ug/L 50.750 101 60-140 1,4-Dichlorobenzene ug/L 49.450 99 60-140 2,2-Dichloropropane ug/L 53.850 108 60-140 2-Chlorotoluene ug/L 48.150 96 60-140 4-Chlorotoluene ug/L 48.150 96 60-140 Benzene ug/L 47.850 96 60-140 Bromobenzene ug/L 51.350 103 60-140 Bromochloromethane ug/L 54.150 108 60-140 Bromodichloromethane ug/L 51.850 104 60-140 Bromoform ug/L 55.850 112 60-140 Bromomethane ug/L 47.550 95 60-140 Carbon tetrachloride ug/L 53.150 106 60-140 Chlorobenzene ug/L 51.650 103 60-140 Chloroethane ug/L 46.150 92 60-140 Chloroform ug/L 50.850 102 60-140 Chloromethane ug/L 58.150 116 60-140 cis-1,2-Dichloroethene ug/L 52.050 104 60-140 cis-1,3-Dichloropropene ug/L 52.350 105 60-140 Dibromochloromethane ug/L 53.950 108 60-140 Dibromomethane ug/L 50.250 100 60-140 Dichlorodifluoromethane ug/L 56.850 114 60-140 Diisopropyl ether ug/L 51.750 103 60-140 Ethylbenzene ug/L 50.450 101 60-140 Hexachloro-1,3-butadiene ug/L 52.650 105 60-140 Isopropylbenzene (Cumene)ug/L 50.750 101 60-140 m&p-Xylene ug/L 102100 102 60-140 Methyl-tert-butyl ether ug/L 51.450 103 60-140 Methylene Chloride ug/L 49.550 99 60-140 n-Butylbenzene ug/L 52.150 104 60-140 n-Propylbenzene ug/L 50.450 101 60-140 Naphthalene ug/L 48.850 98 60-140 o-Xylene ug/L 52.150 104 60-140 sec-Butylbenzene ug/L 50.550 101 60-140 Styrene ug/L 52.550 105 60-140 tert-Butylbenzene ug/L 43.850 88 60-140 Tetrachloroethene ug/L 53.050 106 60-140 Toluene ug/L 49.650 99 60-140 trans-1,2-Dichloroethene ug/L 53.250 106 60-140 trans-1,3-Dichloropropene ug/L 51.650 103 60-140 Trichloroethene ug/L 51.950 104 60-140 Trichlorofluoromethane ug/L 49.150 98 60-140 Vinyl chloride ug/L 57.950 116 60-140 1,2-Dichloroethane-d4 (S)%99 70-130 4-Bromofluorobenzene (S)%102 70-130 Toluene-d8 (S)%98 70-130 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 22 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3834648MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92634524004 3834649 MSD Result MSD % Rec RPD MSDMS Spike Conc. 1,1,1,2-Tetrachloroethane ug/L 20 105 60-14088 1820ND21.0 17.5 1,1,1-Trichloroethane ug/L 20 111 60-14097 1320ND22.2 19.4 1,1,2,2-Tetrachloroethane ug/L 20 104 60-14087 1920ND20.8 17.3 1,1,2-Trichloroethane ug/L 20 103 60-14092 1120ND20.7 18.5 1,1-Dichloroethane ug/L 20 105 60-14091 1420ND21.0 18.2 1,1-Dichloroethene ug/L 20 112 60-14099 1220ND22.4 19.9 1,1-Dichloropropene ug/L 20 122 60-140106 1420ND24.4 21.2 1,2,3-Trichlorobenzene ug/L 20 97 60-14086 1320ND19.5 17.1 1,2,3-Trichloropropane ug/L 20 86 60-14075 1320ND17.1 15.0 1,2,4-Trichlorobenzene ug/L 20 99 60-14083 1720ND19.7 16.6 1,2,4-Trimethylbenzene ug/L 20 99 60-14083 1720ND19.8 16.7 1,2-Dibromo-3-chloropropane ug/L 20 97 60-14077 2420ND19.5 15.4 1,2-Dibromoethane (EDB)ug/L 20 106 60-14090 1620ND21.1 18.0 1,2-Dichlorobenzene ug/L 20 98 60-14086 1320ND19.6 17.1 1,2-Dichloroethane ug/L 20 104 60-14091 1320ND20.7 18.1 1,2-Dichloropropane ug/L 20 101 60-14087 1520ND20.2 17.4 1,3,5-Trimethylbenzene ug/L 20 106 60-14090 1620ND21.2 18.0 1,3-Dichlorobenzene ug/L 20 100 60-14086 1620ND20.1 17.2 1,3-Dichloropropane ug/L 20 101 60-14083 1920ND20.2 16.7 1,4-Dichlorobenzene ug/L 20 95 60-14084 1320ND19.1 16.7 2,2-Dichloropropane ug/L 20 112 60-14094 1820ND22.4 18.8 2-Chlorotoluene ug/L 20 103 60-14087 1620ND20.5 17.4 4-Chlorotoluene ug/L 20 103 60-14087 1620ND20.5 17.4 Benzene ug/L 20 101 60-14087 1520ND20.2 17.4 Bromobenzene ug/L 20 100 60-14084 1720ND19.9 16.8 Bromochloromethane ug/L 20 109 60-14095 1420ND21.8 18.9 Bromodichloromethane ug/L 20 107 60-14092 1420ND21.3 18.5 Bromoform ug/L 20 107 60-14085 2320ND21.3 16.9 Bromomethane ug/L 20 111 60-140103 820ND22.2 20.5 Carbon tetrachloride ug/L 20 113 60-14098 1420ND22.6 19.7 Chlorobenzene ug/L 20 104 60-14086 1920ND20.8 17.2 Chloroethane ug/L 20 124 60-140111 1120ND24.8 22.2 Chloroform ug/L 20 107 60-14090 1820ND21.4 18.0 Chloromethane ug/L 20 119 60-140106 1120ND23.7 21.2 cis-1,2-Dichloroethene ug/L 20 109 60-14095 1420ND21.7 19.0 cis-1,3-Dichloropropene ug/L 20 107 60-14090 1720ND21.4 18.1 Dibromochloromethane ug/L 20 103 60-14088 1520ND20.6 17.7 Dibromomethane ug/L 20 105 60-14088 1820ND21.0 17.6 Dichlorodifluoromethane ug/L 20 110 60-14098 1120ND22.0 19.7 Diisopropyl ether ug/L 20 99 60-14083 1820ND19.9 16.6 Ethylbenzene ug/L 20 103 60-14089 1520ND20.6 17.7 Hexachloro-1,3-butadiene ug/L 20 112 60-14095 1620ND22.4 19.0 Isopropylbenzene (Cumene)ug/L 20 103 60-14088 1620ND20.6 17.5 m&p-Xylene ug/L 40 103 60-14088 1640ND41.1 35.0 Methyl-tert-butyl ether ug/L 20 100 60-14085 1720ND20.0 17.0 Methylene Chloride ug/L 20 91 60-14076 1720ND18.1 15.3 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 23 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. Parameter Units MS Result % Rec Limits Qual% RecConc. 3834648MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92634524004 3834649 MSD Result MSD % Rec RPD MSDMS Spike Conc. n-Butylbenzene ug/L 20 108 60-14092 1620ND21.6 18.3 n-Propylbenzene ug/L 20 104 60-14088 1720ND20.8 17.6 Naphthalene ug/L 20 98 60-14082 1920ND19.7 16.3 o-Xylene ug/L 20 104 60-14089 1620ND20.8 17.8 sec-Butylbenzene ug/L 20 106 60-14089 1720ND21.1 17.8 Styrene ug/L 20 100 60-14084 1820ND19.9 16.7 tert-Butylbenzene ug/L 20 93 60-14079 1720ND18.6 15.8 Tetrachloroethene ug/L 20 105 60-14088 1820ND21.0 17.5 Toluene ug/L 20 104 60-14090 1520ND20.8 17.9 trans-1,2-Dichloroethene ug/L 20 111 60-14098 1220ND22.3 19.7 trans-1,3-Dichloropropene ug/L 20 106 60-14090 1620ND21.2 18.1 Trichloroethene ug/L 20 108 60-14093 1520ND21.6 18.5 Trichlorofluoromethane ug/L 20 111 60-14098 1320ND22.3 19.6 Vinyl chloride ug/L 20 123 60-140106 1520ND24.6 21.2 1,2-Dichloroethane-d4 (S)%99 70-130105 4-Bromofluorobenzene (S)%102 70-130102 Toluene-d8 (S)%101 70-130101 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 24 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736888 SM 4500-H+B-2011 SM 4500-H+B-2011 4500H+B pH Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Dup Result QualifiersRPDResult 92635712002 3834909SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 9.8 H309.7 Parameter Units Dup Result QualifiersRPDResult 92635728003 3834910SAMPLE DUPLICATE: pH at 25 Degrees C Std. Units 6.6 H316.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 25 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736138 EPA 300.0 Rev 2.1 1993 EPA 300.0 Rev 2.1 1993 300.0 IC Anions Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3831098 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed Sulfate mg/L ND 1.0 11/10/22 20:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3831099LABORATORY CONTROL SAMPLE: LCSSpike Sulfate mg/L 48.750 97 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3831100MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635596001 3831101 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L 50 101 90-110103 15012.1 62.8 63.7 Parameter Units MS Result % Rec Limits Qual% RecConc. 3831102MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635647003 3831103 MSD Result MSD % Rec RPD MSDMS Spike Conc. Sulfate mg/L M1508290-11095 450110151157 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 26 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736113 EPA 350.1 Rev 2.0 1993 EPA 350.1 Rev 2.0 1993 350.1 Ammonia Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3831041 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed Nitrogen, Ammonia mg/L ND 0.10 11/10/22 14:47 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3831042LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Ammonia mg/L 5.25 104 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3831043MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92634991001 3831044 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 105 90-110106 05ND5.3 5.3 Parameter Units MS Result % Rec Limits Qual% RecConc. 3831045MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635037001 3831046 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Ammonia mg/L 5 103 90-110103 051.5 6.6 6.6 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 27 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736902 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 351.2 TKN Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3834994 Associated Lab Samples:92635728001, 92635728002, 92635728003, 92635728004, 92635728005 Matrix:Water Analyzed Nitrogen, Kjeldahl, Total mg/L ND 0.50 11/17/22 05:57 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3834995LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Kjeldahl, Total mg/L 9.210 92 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3834996MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92634542001 3834997 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Kjeldahl, Total mg/L M11011490-110138 61024.6 36.0 38.4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 28 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736066 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728001, 92635728002, 92635728005 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3830929 Associated Lab Samples:92635728001, 92635728002, 92635728005 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 11/10/22 01:38 Nitrogen, Nitrite mg/L ND 0.040 11/10/22 01:38 Nitrogen, NO2 plus NO3 mg/L ND 0.040 11/10/22 01:38 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3830930LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 99 90-110 Nitrogen, Nitrite mg/L 0.981 98 90-110 Nitrogen, NO2 plus NO3 mg/L 2.52.5 99 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3830931MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635543001 3830932 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 97 90-11097 01.51.1 2.6 2.6 Nitrogen, Nitrite mg/L 1 97 90-11099 21ND1.0 1.0 Nitrogen, NO2 plus NO3 mg/L 2.5 99 90-11099 02.51.1 3.6 3.6 Parameter Units MS Result % Rec Limits Qual% RecConc. 3830933MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635495003 3830934 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 99 90-110100 11.50.40 1.9 1.9 Nitrogen, Nitrite mg/L 1 99 90-110102 31ND1.0 1.0 Nitrogen, NO2 plus NO3 mg/L 2.5 99 90-110101 12.50.40 2.9 2.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 29 of 35 #=QC# QUALITY CONTROL DATA Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Results presented on this page are in the units indicated by the "Units" column except where an alternate unit is presented to the right of the result. QC Batch: QC Batch Method: Analysis Method: Analysis Description: 736067 EPA 353.2 Rev 2.0 1993 EPA 353.2 Rev 2.0 1993 353.2 Nitrate + Nitrite, Unpres. Laboratory:Pace Analytical Services - Asheville Associated Lab Samples:92635728003, 92635728004 Parameter Units Blank Result Reporting Limit Qualifiers METHOD BLANK:3830935 Associated Lab Samples:92635728003, 92635728004 Matrix:Water Analyzed Nitrogen, Nitrate mg/L ND 0.040 11/10/22 02:14 Nitrogen, Nitrite mg/L ND 0.040 11/10/22 02:14 Nitrogen, NO2 plus NO3 mg/L ND 0.040 11/10/22 02:14 Parameter Units LCS Result % Rec Limits Qualifiers% RecConc. 3830936LABORATORY CONTROL SAMPLE: LCSSpike Nitrogen, Nitrate mg/L 1.51.5 100 90-110 Nitrogen, Nitrite mg/L 0.981 98 90-110 Nitrogen, NO2 plus NO3 mg/L 2.52.5 99 90-110 Parameter Units MS Result % Rec Limits Qual% RecConc. 3830937MATRIX SPIKE & MATRIX SPIKE DUPLICATE: MSSpike Result 92635728004 3830938 MSD Result MSD % Rec RPD MSDMS Spike Conc. Nitrogen, Nitrate mg/L 1.5 96 90-11095 01.51.5 3.0 2.9 Nitrogen, Nitrite mg/L 1 96 90-11096 01ND0.97 0.96 Nitrogen, NO2 plus NO3 mg/L 2.5 96 90-11096 02.51.5 3.9 3.9 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 30 of 35 #=QL# QUALIFIERS Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 DEFINITIONS DF - Dilution Factor, if reported, represents the factor applied to the reported data due to dilution of the sample aliquot. ND - Not Detected at or above adjusted reporting limit. TNTC - Too Numerous To Count J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL - Adjusted Method Detection Limit. PQL - Practical Quantitation Limit. RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and bias for a specific analyte in a specific matrix. S - Surrogate 1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is a combined concentration. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean-Up U - Indicates the compound was analyzed for, but not detected. Acid preservation may not be appropriate for 2 Chloroethylvinyl ether. A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA Method 8260. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as "Total" may vary slightly from the sum of the reported component parameters. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. ANALYTE QUALIFIERS Sample was received or analysis requested beyond the recognized method holding time.H3 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.M1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 31 of 35 #=CR# QUALITY CONTROL DATA CROSS REFERENCE TABLE Pace Project No.: Project: 92635728 Blue Ridge Tissue Corp. 11/9 Lab ID Sample ID QC Batch Method QC Batch Analytical Method Analytical Batch 92635728001 739454 739527MW-1 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 92635728002 739454 739527MW-3 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 92635728003 739454 739527MW-4 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 92635728004 739454 739527MW-7 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 92635728005 739454 739527MW-8 EPA 200.8 Rev 5.4 EPA 200.8 Rev 5.4 92635728001 736729MW-1 SM 6200B 92635728002 736729MW-3 SM 6200B 92635728003 736729MW-4 SM 6200B 92635728004 736729MW-7 SM 6200B 92635728005 736729MW-8 SM 6200B 92635728001 736888MW-1 SM 4500-H+B-2011 92635728002 736888MW-3 SM 4500-H+B-2011 92635728003 736888MW-4 SM 4500-H+B-2011 92635728004 736888MW-7 SM 4500-H+B-2011 92635728005 736888MW-8 SM 4500-H+B-2011 92635728001 736138MW-1 EPA 300.0 Rev 2.1 1993 92635728002 736138MW-3 EPA 300.0 Rev 2.1 1993 92635728003 736138MW-4 EPA 300.0 Rev 2.1 1993 92635728004 736138MW-7 EPA 300.0 Rev 2.1 1993 92635728005 736138MW-8 EPA 300.0 Rev 2.1 1993 92635728001 736113MW-1 EPA 350.1 Rev 2.0 1993 92635728002 736113MW-3 EPA 350.1 Rev 2.0 1993 92635728003 736113MW-4 EPA 350.1 Rev 2.0 1993 92635728004 736113MW-7 EPA 350.1 Rev 2.0 1993 92635728005 736113MW-8 EPA 350.1 Rev 2.0 1993 92635728001 736902 737658MW-1 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92635728002 736902 737658MW-3 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92635728003 736902 737658MW-4 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92635728004 736902 737658MW-7 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92635728005 736902 737658MW-8 EPA 351.2 Rev 2.0 1993 EPA 351.2 Rev 2.0 1993 92635728001 736066MW-1 EPA 353.2 Rev 2.0 1993 92635728002 736066MW-3 EPA 353.2 Rev 2.0 1993 92635728003 736067MW-4 EPA 353.2 Rev 2.0 1993 92635728004 736067MW-7 EPA 353.2 Rev 2.0 1993 92635728005 736066MW-8 EPA 353.2 Rev 2.0 1993 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC.Date: 11/30/2022 03:21 PM Pace Analytical Services, LLC 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Page 32 of 35 Page 33 of 35 Page 34 of 35 Page 35 of 35