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Home My WebLink AboutWQ0009267_Monitoring - 02-2022_20220427 (2)Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * February Report Information Type * Revised - GW-59 WQ0009267 City of Jacksonville WWTP Confirmation Email Address:* Name of Submitter: * Signature: Year:* 2022 Upload Document* REVISED April 2022 with 8.39MB updated signature WQ0009267 February 2022 Resample from December 2021 GW-59 MW Report, VOCs attached.pdf PDF Only Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). apalaschak@jacksonvillenc.gov Amy E. Palaschak 1. � Date of submittal: Initial Review Reviewer: Gerald, Wanda Is the project number correct?* WQ0009267 Is the monitoring report accepted?* Yes No Regional Office* Wilmington Reviewer: _anonymous Review Date: 12/7/2022 4/27/2022 This will be filled in automatically CTW-59A COMPLIANCE PLIANC E Eli-0,f'C)R"C k'()RM Permit tt WQC)009267 (Submit onc„cach 11 loll period with GW 59 tbrms.) j Enter date monitoring results were due. (03/31/2022) Will this monitoring report (GW-59 and GW-59A) be YES NO submitted after the established due date? 2 Was any required information missing on the GW-59 report forms? YES NO IF the answer to question 1 or 2 is "YES', list in the space provided below the well identification number(s) and explain the problems encountered in obtaining the required information. 3 Are any of the monitor wells in need of repair or maintenance (damaged casing, unlocked or missing cap, missing YES NO identification plate, area overgrown, etc.)? If the answer is "Yes", contact the Regional Office for guidance. q Are any monitored constituents equal to or above the established standards? YES NO If the answer to question 4 is "NO", skip to section 8. If the answer to question 4 is "YES' list the affected wells individually with constituent(s) and concentration(s) exceeding standards in the space provided below: February 2022— Resampling of MW2 and MW 11. VOCs were not detected in either well. (NOTE: MW2 and MW11 were resampled due to positive results received during December 2021 sampling.) 5 For the constituents identified in question 4 above, have standards been exceeded previously for the same YES NO constituent(s) in the same well(s) in the last two years? If the answer to question 5 is "NO", skip to section 8. If the answer to question 5 is "YES", list in the space provided below, each well with constituent(s) exceeding standards, concentration(s) reported, and sample collection date for each occurrence (for the last two years). MW 2 - 12/2020 Chloromethane = 1.90 ug/L - 12/2021 Bromomethane = 1.60 ug/L, Chloromethane = 1.14 ug/L MW 11 - 12/2020 Chloromethane = 1.22 ug/L - 12/2021 Bromomethane = 1.44ug/L, Chloromethane = 1.06 ug/L 6 Are the monitoring wells listed in section 5 located at or beyond the review boundary? YES NO If the answer is "YES', a groundwater quality problem may be occurring. CONTACT THE REGIONAL OFFICE IMMEDIATELY FOR GUIDANCE. If the answer is "NO", monitoring wells may be improperly located; contact the Regional Office. (Jan 2022) Contacted Tom Tharrington and Helen Perez at NC DEQ Wilmington Regional Office to notify them of the presence of VOCs (Chloromethane/Bromomethane) in December 2021 quarterly MW samples 2 and 11. - Env. Specialist 11, Helen Perez, advised that we resample the wells positive for VOCs. 7 Is the permittee implementing previously approved actions required by the Division involving this groundwater YES NO quality problem? If the answer to question 7 is "YES', describe those actions in the space provided below. If the answer to question 7 is "NO", contact the Regional Office within 90 days; an evaluation may be required to determine the impact the waste disposal system is having at the review and compliance boundaries surrounding this facility. Failure to do so may subject the permittee to a Notice of Violation, fines, and/or penalties. Under the guidance of the NC DEQ Wilmington Regional Office, MW2 and MW11 were resampled on 2124/22. VOCs were not detected in either of the wells resampled February 2022. Env. Specialist 11, Helen Perez, was contacted with the results on 3/8/22. - Attached are the corresponding GW-59 forms for the resampled monitoring wells. g The person completing this portion (GW-59A) of the monitoring report should sign below and submit this form with GW-59 forms for required wells to the address provided at the top of the current GW-59 form. I hereby acknowledge that the above information was evaluated and the information submitted in this report (Compliance Report GW-59A) is true and complete to the best of my knowledge Signature o rmittee(or Authorized Agent) Date GW-59A 12/8/200.1 # ! 0 - SUBMIT FORM ON YELLOW PAPER ONLY Print Gleamy or Type Facility Name: City of Jacksonville Land Treatment System Permit Name (if different): Facility Address: 716 Firetower Road Jacksonville N C County Onslow P Contact Person: Amy Palaschak Telephone#: (910)938-3620 Well Location/Site Name MW-11 No. of wells to be sampled: 17 PERMIT Number: Expiration Date: 4/3012022 Non -Discharge WQ0009267 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-11 Date sample collected: 2/2412022 FIELD ANALYSES: WAS Well Depth: 22.2 ft, Well Diameter: 2 in. pH 00400: 4.8 units Temp. 000lc 16.9 °C DRY at Depth to Water Level 82546: 11 ft. below measuring point Screened Interval: 5 ft. to 20 ft. Spec. Cond. 00094: µMhos time of sampling,check Measuring Point is 2.25 ft. above land surface Relative M.P. Elevation: 8.75 ft. Odor 00085: Volume of water pumped/bailed before sampling: 5,38 gallons Appearance here: Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES ❑ NO L-1 LABORATORY INFORMATION Date sample analyzed: 2/24/2022 Laboratory Name: 1. Jacksonville 2, Environmental Chemists Certification No, 1, 128 2, 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00335 mg/L Nitrite (NO2) as N 00615 Coliform: MF Fecal 31616 /100ml- Nitrate (NO3) as N 00620 Coliform: MF Total 31504 /100ml- Phosphorus: Total as P 00665 (Note: Use MPN method for highly turbid samples) Orthophosphate 70507 7issolved Solids:Total 70300 mg/L Al - Aluminum oil o5 pH (Lab) 00403 4.82 units Ba - Barium 01007 TOC oo68o mg/L Ca - Calcium 00916 Chloride 00940 mg/L Cd - Cadmium 01027 Arsenic 01002 ug/L Chromium: Total 01034 Grease and Oils 00552 mg/L Cu - Copper 01042 Phenol 32730 ug/L Fe - Iron 01045 Sulfate 00945 mg/L Hg - Mercury 71900 Specific Conductance 00095 µMhos K - Potassium 00937 Total Ammonia ooelo mg/L Mg - Magnesium 00927 (Ammonia Nitrogen; NH�as N; Ammonia Nitrogen, Total) Mn -Manganese 01055 TKN as N 00625 mg/L Ni - Nickel 01067 mg/L mg/L mg/L mg/L mg/L ug/L mg/L ug/L ug/L mg/L ug/L ug/L mg/L mg/L ug/L ug/L Pb - Lead olo51 Zn - Zinc 01092 W. Other (Specify Compounds and Concentration Units): ORGANICS: (by GC, GC/MS, HPLC) (Specify test and method #. ATTACH LAB REPORT.) Lab Report Attached? 21 Yes (1) ❑ No (0) VOC 7873 method # SM 6200C method # method # method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg1L Effluent Total VOCs: mg/L VOC Removal% Wally Hansen - Public Services Director Permittee (or Authorized Accent) Name and Title - Please print or type GW-59 Rev, 8/2013 SUBMIT FORM ON YELLOW PAPER ONLY Please Print Clearly or Type Facility Name: City of Jacksonville Land Treatment System Permit Name (if different): Facility Address: 716 Firetower Road Jacksonville NC 285-40 County Onslow tact Person: Amy Palaschak Telephone#: (910)938-3620 1 Location/Site Name MW-2 No. of wells to be sampled: 17 WELL ID NUMBER (from Permit): MW-2 Date sample collected: Well Depth: 17.0 ft. Well Diameter: Depth to Water Level 82546: 5.5 ft. below measuring point Screened Interval: Measuring Point is 2.4 ft. above land surface Relative M.P. Elevation: Volume of water pumped/bailed before sampling: 5,52 gallons 2/24/2022 PERMIT Number: Expiration Date: 4/3012022 Non -Discharge WQ0009267 UIC NPDES Other TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery X Spray Field ❑ Remediation: ❑ Rotary Distributor ❑ Land Application of Sludge ❑ Water Source Heat Pump ❑ Other: 2 in. 3 ft. to 13 ft. 3.1 ft. Samples for metals were collected unfiltered: X YES ❑ NO and field acidified: X YES FIELD ANALYSES: pH 00400: 4.8 units Spec. Cond. 00094: Odor 00085: Appearance Temp. 000lc 16.8 oC uMhos Date sample analyzed: 2/24/2022 Laboratory Name: 1. Jacksonville 2. Environmental Chemists Certification No. 1. 128 2. 94 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD 00935 mg/L Nitrite (NO2) as N oo615 mg/L Pb - Lead 01051 ug/L Coliform: MF Fecal 31616 /100mL Nitrate (NO3) as N 00620 mg/L Zn -Zinc 01092 mg/L Coliform: MF Total 31504 /100mL Phosphorus: Total as P 00665 mg1L (Nate: Use MPN method for highly turbid samples) Orthophosphate 70507 mg/L Other (Specify Compounds and Concentration Units): )issolved Solids:Total 70300 mg/L Al - Aluminum oilo5 mg/L pH (Lab) 00403 4.77 units Ba - Barium 01007 ug/L TOC 00680 mg/L Ca - Calcium 00916 mg/L Chloride 00940 mg/L Cd - Cadmium 01027 ug/L Arsenic 01002 ug/L Chromium: Total 01034 ug/L Grease and Oils 00552 mg/L Cu - Copper 01042 mg/L ORGANICS: (by GC, GC/MS, HPLC) Phenol 32730 ug/L Fe - Iron 01045 ug/L (Specify test and method #. ATTACH LAB REPORT.) Sulfate 00945 mg/L Hg - Mercury 71900 ug/L Lab Report Attached? ® Yes (1) ❑ No (0) Specific Conductance 000ss µMhos K - Potassium 00937 mg/L VOC 7873 method # SM 6200C Total Ammonia oo6lo mg/L Mg - Magnesium 00927 mg/L method # (Ammonia Nitrogen: NH3 as N, Ammonia Nitrogen, Total) Mn - Manganese 01055 ug/L method # TKN as N 00625 mg/L Ni - Nickel 01067 ug/L method # For Remediation Systems Only (Attach Lab Reports) 1"ifi .�[TZ+I+0 mg/L Effluent Total VOCs: mg/L VOC Removal% If WELL DRY at time of sampling, check here: ❑ IV V V-VV rNCv. 01 LV 10 ANALYTICAL & CONSULTING CHEMISTS Environmexital Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 9 910.392.0223 Lab a 910.392.4424 Fax 710 Bowsertown Road, Man teo, NC 27954 * 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347,5843 Lab/Fax info('i�environmentaleliemists.coni City of Jacksonville Date of Deport: Mar 04, 2022 Post Office Box 128 Customer PO #: Jacksonville NC 28541 Customer ID: 08110015 Attention: Amy Palaschak Report #: 2022-03561 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-08427 Site: MW-2 2/24/2022 8:22 AM Water NB Test Method Results Date Analyzed 1,1,1,2-Tetrachloroethane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,1,1-Trichloroethane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,1,2,2-Tetrachloroethane SM6200B-2011 <0.50pg/L 3/1/2022 1,1,2-Trichloroethane SM6200B-2011 <0.50pg/L 3/1/2022 1,1-Dichloroethane SM6200B-2011 <0.50pg/L 3/1/2022 1,1-Dichloroethane SM6200B-2011 <0.50pg/L 3/1/2022 1, 1 -Dichloropropene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2,3-Trichlorobenzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2,3-Trichloropropane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2,4-Trichlorobenzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2,4-Trimethylbenzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2-Dibromo-3-Chloropropane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2-Dibromoethane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2-Dichlorobenzene SM6200B-2011 <0.50pg/L 3/1/2022 1,2-Dichloroethane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,2-Dichloropropane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,3,5-Trimethyl benzene SM 6200 B-2011 < 0,50 pg/L 3/1/2022 1,3-Dichlorobenzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,3-Dichloropropane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 1,4-Dichlorobenzene SM6200B-2011 <0.50pg/L 3/1/2022 2,2-Dichloropropane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 2-Chlorotoluene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 4-Chlorotoluene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 Benzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 Bromobenzene SM 6200 B-2011 < 0.50 pg/L 3/1/2022 Bromochloromethane SM 6200 B-2011 < 0.50 pg/L 3/1/2022 Report #:: 2022-03561 Page 1 of 6 ANALYTICAL aCONSULTING CHEMISTS Environmental �� Chemists, Inc* 6602Windmill Way, Wilmington, NC284U5 ° 910392.0223[ab ° 9I0392.4424Pvx 7l0Uows,r|owoRoad, &dun,co'0C27954 ~ 252.473.5702L*6/Fax 255'/\Wilmington Highway, Jacksonville, NC28540 ° 910.347.5843Lnb/9ax info( en,b nmontnbher`iots.com City ofJacksonville Date ofReport: Mar O4.2O22 Post Office Box 128 Customer PO#/ Jacksonville NC 28541 Customer ID: 08110015 Attention: ArnyPa|oeohak Report#: 2022-03581 Project ID: Monitoring Wells Bromodich|oromathana m*om«ae» 1 <O.5Opg/L 3/1/2022 Dromoform smsm»a-2m11 <O.5Opg/L 3/1/2022 8romomethana sm»u«»a'z»11 < 0.50Ug/L 3/1/2022 Carbon tetrachloride ow*2»»a'u»11 < 0.50pg/L 3/1/2022 Ch|orobenzonn uMo2»»a'o»11 « 0.50UQ/L 3/1/2022 Oh|oroethane »w«u»oa'2o11 < 0.50pg/L 3/1/2022 Chloroform om»u«»n-2»11 < 0.50pg/L 3/1/2022 Ch|onnmethane «m«c»»y'o»11 < 0.50pg/L 3/1/2022 cis- 1.2-0oh|omethene ows2«oo-u»11 <O.S0pg/L 3/1/2022 cis- 1.3-Dioh|ompropmne sm«u»»e'u»11 < 0.50pg/L 3/1/2022 Dibromoch|oromethone »w«u»«o-u»11 < 0.50pg/L 3/1/2022 Dibrumomothane »mec»oa'c»11 ^ 0.50pg/L 3/1/2022 Diuh|orodif|uornnnethane »m*uo»e'o»11 < 0.50pg/L 3/1/2022 Ethy|benzene »m«u»»a'c»11 <O.5Upg/L 3/1/2022 Hexaoh|onobutadiena smnu»«e'2»11 < 0.50pg/L 3/1/2022 |eopnopy|benzene smeo»»o'u»11 <8.5Opg/L 3/1/2022 [N+pXy|onn »mso»»a'»o11 < 1.00pg/L 3/1/2022 Methylene chloride oMsu»»a'2»11 <U.5DpQ/L 3/1/2022 Naphthalene »m»z»»a-u»11 < 0.50Ug/L 3/1/2022 n-8uty|benzene »meo»»o'z»1/ < 0.50pg/L 3/1/2022 n-Propy|benzene oMsu«»a'a«11 <O.5OpQ/L 3/1/2022 ortho-Xy|ene amae»»a-u»11 < 0.50pg/L 3/1/2022 p-|ouprnpy|to|uone em6z»»m'u«11 < 0.50Ug/L 3/1/2022 sec-8uhy|benzene am»:»oa-2»1/ <8.5Opg/L 3/1/2022 Styrene omee»»n'u»11 < 0.50pg/L 3/1/2022 tert-8uh/|benzene :meo»»a-2«11 <D.5Op0/L 3/1/2022 Totraoh|omethana um«x»»o'co11 < 0.50pg/L 3/1/2022 Toluene ow»e«»o'»»11 < 0.50pg/L 3/1Q022 Trans-1.2-Dioh|000ethone em»u»»e'»»11 < 0.50pg/L 3/1/2022 Trans-1.3-dich|000pnopene oMsu»»»'o»11 <D.5Upg/L 3/1/2022 nvv"nw:: uooz'onom Page un/n ANALYTICAL aCONSULTING CHEMISTS Environmental Chemists, 6602 Windmill Way, Wilmington, NC28405 ^ 9103920223Lu6 ° 90.392.4424Tax 710bowsc uwnDoad'Mauten NC27Y54 " 252.4735702L*b/gax 255'A Wilmington Highway, Jacksonville, NC28540 ° 910.347.5843Lab/Iax i ukbumimx.cnm City mfJacksonville Date ofReport: Mar O4.2D22 Post Office Box 128 Customer PO#: Jacksonville NC 28541 Customer ID: 08110015 Attention: AnnyPu|aaohak Report #: 2022'03561 Project ID: Monitoring Wells Trinh|omeiheno »mou»»a-2m11 < 0.50pO/L 3/1/2022 Vinyl chloride mw*20oa-2u11 * 0.50pg/L 3/1/2022 *O.5Opg/L 3/1/2822 ANALYTICAL aCONSULTING CHEMISTS Environmental Chemists, ��]1�`��t�UK ��i��sInc. 6602Windmill Way, Wilmington, mC2x405 ° 910.392.0223Lab ° 910.392.4424Fax 7l0Do=oortownRoad, Mvntc"'y4C27954 ° 252.473.5702Lnb/Fxx 255-6Wilmington Highway, Jacksonville, yVC2854O ~ 910.347.5845Lab/Pax info((!�eiivmoninulchemiots,mm City ufJacksonville Date ofReport: Mar 04.2O22 Post Office Box 128 Customer FU#: Jacksonville NC 28541 Customer ID: 08110015 Attention: AmyPe|oachak Report#: 2022'03581 Project ID: Monitoring Wells Lab ID Sample ID: Collect Date[Time Matrix Sampled by Results Date Analyzed 1.1.1.2-Tohaoh|oroethane omam»o-2»11 <O.SUpg/L 3/1Q023 1.1.1'Thuh|onoethane am»20»a-2»11 <U.5Opg/L 3/1/2022 1.1.2.2-Tetnsoh|onoethone »w6o»»a-2m11 < 0.50Ug/L 3/1/2022 1.1.2-Thoh|omathane sMou»»o-2»11 <0.5Opg/L 3/1/2022 1.1-Dioh|oronthano «muu«»a-2m11 <O.5Opg/L 3/1/2032 1.1-Dich|onoethona sm»x«oo-2m11 < 0.50pg/L 3/1/2022 1.1-Dioh|onopropene «woc»»a-2»11 < 0.50Ug/L 3/1/2022 1.2.3-Thoh|ombenzene umec»«au»1/ < 0.50pg/L 3/1/2022 1.2.3'Thch|nnopmpane awoumo-2»11 < 0.50pg/L 3/1/2022 1.2.4-Thch|orobenzeno »w»u»»o-2m11 < 0.50pg/L 3/1/2022 1.2.4-Trimethyl benzene am«u»na'c«1 1 <O.5Opg/L 3/1/2022 1.3'Dibromo-3-Ch|ompmpeno mm*c»»a-2»11 < 0.50pg/L 3/1/2022 1.2-Oiboomoethane amum»o-2m11 « O.SDpg/L 3/1/2022 1.2-Dioh|onobanrane »m/o»«o-2m11 <O.5Opg/L 3/1/2022 1.2-Uich|oroethane omn2m»B-2m11 < 0.50pg/L 3/1/2022 1.2-Dich|oropropanm »M»2»»a-2»/1 < 0.50pg/L 3/1/2022 1.3.5-Thmethy[banzene omeu»»a-2»/1 <0.bOpA/L 3/1/2022 1.3-D|oh|orobonzeno aM«x»»u-2»`1 <O.58Ug/L 3/1/2022 1.3-Dinh|oropmpone mw«u»»o-2m1` < 0.50pg/L 3/1/2022 1.4-Oich|orobenzene aw«2»oa-2a/I < 0.50pg/L 3/1/2022 2.2-Oich|nmpropane omm»»o-2»11 < 0.50Ug/L 3/1/2022 2-Ch|nvoto|uene am«uo»o'2m11 < 0.50pg/L 3/1/2022 4-Ch|oudo|uene om62»«o-2»11 <U.5OUg/L 3/1/2022 Benzene amno»»a-2m11 <0.50pg/L 3/1/2022 8mmobonzene amm»»a-2«11 <O.5Opg/L 3/1/2022 Bnumooh|onomethene awmo»a-2«11 <D.5Opg/L 3/1/2022 ANALYTICAL mCONSULTING c*sI ImrS Environmental Chemists, � J��»�'��p��7�U�� L��s, Inc. 6602Windmill WaWilmington, NC28405 ~ 910.392.0223Iab ° 910.392.4424Fnx 710Dovvoer/m"nDo�d'Munuv'NC27954 ° 252,473,5702Lah/Fux 255'/\Wilmington Highway, Jacksonville, NC28540 ° 910347.5043Loh/Fux info(,�!;en,mnmcou|demis'umm City ofJacksonville Date ofReport: Mar D4.2O22 Post Office Box 128 Customer PC]#: Jacksonville NC 28541 Customer ID: 08110015 Attention: AmyPe|eeohak Report#: 2022-03561 Project ID: Monitoring Wells Bromodich|ommathane ama20»a-2o1 <O.5Opg/L 3/1/2022 Bn»moform omsmoo-2m11 ^ 0.50Ug/L 3/1/2022 8romnmethane »ms2m»a-2»11 < 0.50pg/L 3/1/2022 Carbon batnaoh/ohda omsu»»aan11 < 0.50pg/L 3/1/2022 Ch|onobenzeno am«2m«a-2m11 <U.5OpA/L 3/1/2022 Ch|oroethane emoz»»aou11 <D.5Opg/L 3/1/2022 Chloroform om»u»»a-2»11 < 0.50pg/L 3/1/2022 Ch|000methona amez»»o-2»11 < 0.50pg/L 3/1/2022 cis- 1.2-Dioh|oroethono amm»»u-2»/1 <O.SOpg/L 3/1/2022 cis- 1.3-Oinh|oroprupene uw»u»»o-2»11 <0.5Opg/L 3/1/2022 Oibnnmonh|omm*thane »mm»»a-2m1 i < 0.50pO/L 3/1/2022 Oibvumomethane am6u»»a-2m11 ^0.6Opg/L 3/1/2022 Dich|onodiUuoromethana awam»o-2m11 «O.58pg/L 3/1/2022 Ethy|benzono aMo/»»a-2»11 <8.60pg/L 3/1/2022 Hexouh|orobutadiane om6m»oou»11 <U.5Opg/L 3/1/2022 |aopropy|benzanm »m»u«»o'2o11 <0.5Opg/L 3/1/2022 &1+PXy|mne sm»uo»a-2»11 <1.O0Ug/L 3/1/2022 Methylene chloride amou»»e-2»11 < 0.50pg/L 3/1/2022 Naphthalene Swez»«o-2»11 <O.5Dpg/L 3/1/2022 n'Buh/|banzene «mm»»o'2m11 <0.5Oug/L 3/1/2022 n-Propy|benzane uMum»u'e»11 <O,5Opg/L 3/1/2022 nrtho-Xy|eno emp2«»o-2m11 <O.50pg/L 3/1/2022 p-|oopnopy|to|uene amuu«»o;m11 « 0.50pg/L 3/1/2022 sec-Buty|benzene mmnu»»o-2»11 xB,GOpO/L 3/1/2022 Styrene amo2»»a'2»11 < 0.50pg/L 3/1/2022 tert-Buh/|bonzeno »Mnc»»a'u»1/ <O.5Opg/L 3/1/2022 Tetranh|omeihene amou»»a'co11 < 0.50pg/L 3/1/2022 Toluene Sm»u»»a'm1/ < 0.60pg/L 3/1/2022 Trans- 1.2-Dich|oroethane smn2«»a-2»11 < 0.50pg/L 3/1/2022 Trans- 1.3-d|nh|oropropone awnc«»o'c»11 < 0.50Ag/L 3/1/2022 nonv^#:: 2022'03561 Page suro Environmental Chemists, ��'i�^��\��[�� s, Inc. 6602Windmill VYay,Y0bn 0C 28405 ° 910392.0223[ab ° 910.392.4424fax 7I0Bowoc mnoRoad'Manten 0C27954 ° 252473.5702Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 v 910.347.5843 Lab/Fax ANALYTICAL aCONSULTING CHEMISTS City ofJacksonville Date of Report: Mar O4.2U22 Post Office Box 128 Customer PO#: Jacksonville NC 28541 Customer ID: 08110015 Attention: AmyPa}asohoh Raport#: 2022-03561 Project ID: Monitoring Wells Trioh|onoathene owou»oo-2»11 < O. 50pg/L 3/1/2022 *O.G0pg/L 3/1/2022 *D.5Opg/L 3/1/2022 Comment: Reviewed by: nuponm: 2022-03561 Page oma Environmental Chemist, inc., Wilmington, NC Lab #94 66O2WindmiUWay Wilmington, NC 28405 Sample Receipt Checklist 910.392-0223 O Dab�— � Report Number: _ Client Delivery EJ n PS So Were custody seals present the cooler? ----.— y sea re en on Original temperature upon cut they intact/unbroken? receipt C HOW temperature taken: 1— re,, upon receip—t----- Corrected ternperatu 13 Temperature Blank - W Against Bottles YES EJ No If ure Of cooler exceeded 6-C, was Pr ect Mgr-/QA notified? YES El NO YES 0 6._Were samples ID's listed on sample containers? NO YES 0 NO 7 1 . Were collection date and time listed on—th—e—C—O—C—?--------- YES 0 NO 8. Were tests to be performed listed on the COC? 9. Did samples arrive in proper con ainers for each test? YES YES EJ NO 12, Were `4'es received within Proper holding time for requested tests? 13. Were acid preserved samples received at a pH of <2? YES El NO 15. Were sulfide samples receiovod at a pH >9? YES El NO YES 11 NO 16. Were NH3/TKN/PhenoI received at a chlorine residual Of <0,5 m/L? IT ere Sulfide/Cyanide YES 0 NO received at a chlorine residual of <0.5 M/L? 18. Were orthophosphate samples filtered in the tield within 15 minutes? **TO[/Vo!aU/sare pHchecked attime o�ana��sand rmo�ednnthe bendsheet ' Bacteria samples are checked �r[h|ohneaitime nfanalysis and recorded onthe benchsheet. ample Preservation: S (Must be completed for any sample(s) incorrec—tly p—res—erve—do—r S ample(s) with headspace) were received incorrectly preserved and were adjusted accordingly Lbd.din'b (circle one) by adding (circle one): H2SO, HNO3 HCI NaOH Time of preservation: If more than one prese I rvative is needed, notate in comments below \Jote: Notify customer service imrn2diately for incorrectly preserved samp;es, Obtain a newsarriple or loth�l the state lab if directed to ana�yzed by the customer. Who Was notified, date and time: ^C ENVIRONMENTAL 4M NCDENR: .0 .. Analytical & Consulting Chemists wol CLIENT: City of Jacksonville PROJECT NAME: Monitoring Wells (Jacksonville LTS) REPORT NO: ADDRESS: PO Box 128 CONTACT NAME: PO NO: 225042 Jacksonville, NC 28540 REPORT TO: Amy Palaschak PHONEIFAX: COPY TO: E-MAIL: apalaschak@jacksonvillenc.gov SAMPLE TYPE: I = Influent E = Effluent W = Well ST = Stream SO = So'I SL = SI d Sample Identification Collection nm E r o a `o cC? o` v° c= o t=s E Dint m g z PRESERVATION 1 1 l , u ge, OthCt. APIALYSIS REQUESTED Da Time Temp z ° z = o` N z x _ °a z _o w o BMW 2 W X VOC (SM 6200 C) G G MW 11 � cI pp 1 W X VC}C (SM 6200 G) G G I NOTICE - DECHLORINATION: Samples for Ammonia, TKN, Cyanide, Phenol and Bacteria must be dechlorinated (0.2 ppm or less) in the field at the time of collection. See reverse for instructions Transfer Relinquished By: Date/Time l�16 Received By: DatelTime 2. Tem erattire when R i d — p ece,ve Accepted: Delivered By: Received By: Comments: Resample R qu ted: _Date: - Time: ' TUR AR UND: