NCG060411_2022 DMR_20220729

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Mor+itoring Report ID_MR} Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional office.
Certificate of Coverage No. NCG060411
Person Collecting Samples: Linda Cortes
Facility Name: Amazon.com Services LLC - DRT8
Laboratory Name: Eurofins Test America Savannah
Facility County: Durham
Laboratory Cert. No.: 269
Discharge during this period: 0 Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes 0 No
If so, which Tier (I, Il, or lil)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.goy/Forms/SW-DMR ✓❑ Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Code
Parameter
Outfall001
Outfall002
Outfall
Outfall
Outfall
N/A
Receiving Stream Class
WS-V;NSW
WS-V;NSW
N/A
Date Sample Collected MM/DD/YYYY
6/8/2022
6/8/2022
46529
24-Hour Rainfall in inches
0.18
0.19
C0530
TSS in mg/L (100 or 50*)
<2.5
16
pH in standard units (6.0 — 9.0 FW,
00400
6.8-8.5 SW)
7.1
7.29
Fecal Coliform per 100 ml of
31616
freshwater (if required) (1000)
N/A
N/A
61211
Enterococci per 100 ml of saltwater
N/A
N/A
(if required) (500)
Chemical Oxygen Demand in mg/L
00340
(120)
20
110
Additional parameters for outfalls in drainage areas that use>SS gallons per month of new hydraulic oil on average
NCOIL
Estimated New Motor/Hydraulic Oil
N/A
N/A
Usage in gal/month
00552
Non -Polar Oil & Grease in mg/L (15)
<0.74
1.9
* Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of SO mg/L. All other water classifications have a benchmark of 100 mg/L
FW (Freshwater) SW (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted i , to the est of my knowle a and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false infor is ion, yh luding jhe pps i)5il y of firygs and imprisonment for knowing violations."
5ignatt{ of Permittee or
[e-mail]
Email Address
Authorized Individual
Da
[phone]
Phone Number

urofins
Environment Fasting
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 6 80-216811-1
Client Project/Site: Storm Water - Amazon Warehouses DRT8
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Roxa.OWu � zeros
Authorized for release by:
6/22/2022 4:59:27 PM
Roxanne Cisneros, Senior Project Manager
[phone]
roxanne.cisneros [e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
I�

DefinitionslGlossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT8
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration Is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report,
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoD/DOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoDlDOE)
MCL EPA recommended "Maximum Contaminant Level'
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MAN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative 1 Absent
POS Positive 1 Present
PQL Practical Quantitation Limit
PRIES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 680-216811-1 --
Eurofins Savannah
Page 2 of 14 6/22/2022

Sample Summary
Client: ERM-West Job ID: 680-216811-1
Project/Site: Storm Water - Amazon Warehouses DRT8
Lab Sample ID Client Sample ID Matrix Collected Received
680-216811-1 1511T8 Sample Point_01_20220608 Water 06/08/22 20:03 06/10/22 10:30
680-216811-2 DRT8_Sample_Point_02 20220608 Water 06/0812219:42 06/10/2210:30
Page 3 of 14 Eurofins SAMMIN2

Case Narrative
Client: ERM-West Job ID: 680-216811-1
Project/Site: Storm Water - Amazon Warehouses DRT8
Job ID: 680-216811-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-216811-1
Comments
No additional comments
Receipt
The samples were received on 6/10/2022 10:30 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 5.51 C.
General Chemistry
Methods 166413: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate/sample duplicate
(MSIMSDIDUP) associated with preparation batch 680-727048.
Methods 166413: Analysis for Hexane Extractable Material (HEM) was performed for the following sample:
DRT8_Sample_Point_01_20220608 (680-216811-1). Since the HEM result(s) was below the reporting limit (RL), the result(s) for Silica
Gel Treated - Hexane Extractable Material (SGT-HEM) was reported as a non -detect. All HEM quality control criteria were met.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
Eurofins Savannah
Page 4 of 14 6/22/2022

Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT8
Client Sample ID: DRT8—Sample_Point-01-20220608
Date Collected: 06108/22 20:03
Date Received: 06/10122 10:30
(General Chemistry
Analyte
SGT-HEM (TPH)
Chemical Oxygen Demand
i Total Suspended Solids
Job ID: 680-216811-1
Lab Sample ID: 680-216811-1
Matrix: Water
Result Qualifier
RL
NIDL
Unit
D Prepared Analyzed
Dil Fac8
o0.74
2.6
0.74
mg/L
06/22/22 08:30 06/22/22 10:24
1
20
10
5.0
mg/L
06/21/22 M28
1
<2.5
2.5
2.5
mg/L
06114/22 08:17
1
Eurofins Savannah
Page 5 of 14 6/22/2022

Client Sample Results
Client: ERM-West Job ID: 680-216811-1
Project/Site: Storm Water - Amazon Warehouses DRT8
Client Sample ID: DRT8_Sample_Poinf_02_20220608 Lab Sample ID: 680-216811-2
Date Collected: 06/08/22 19:42 Matrix: Water
Date Received: 06110122 10:30
General Chemistry
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
SGT-HEM (TPH) 1.9 J 2.6 0.73 mg1L 06/22122 08:30 06/22/22 10:24 1
Chemical Oxygen Demand 110 10 5.0 mg1L 06/21/22 12:32 1
Total Suspended Solids 16 5.0 5.0 mg/L 06/14/22 08:17 1
Eurofins Savannah
Page 6 of 14 6/22/2022

QC Sample Results
Client: ERM-West
Job ID: 680-216811-1
ProjecttSite: Storm Water - Amazon Warehouses DRT8
Method: 1664B - HEM and SGT-HEM
Lab Sample ID: MB 680-727048/1-A
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TotallNA
Analysis Batch: 727079
Prep Batch: 727048
MB MB
Analyte Result Qualifier
RL MDL Unit D Prepared Analyzed Dil Fac
SGT-HEM (TPH) <1.4
5.0 1.4 mg1L 06/22122 08:30 06/22/22 10:24 1
Lab Sample ID: LCS 680-727048/2-A
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: TotallNA
Analysis Batch: 727079
Prep Batch: 727048
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
SGT-HEM (TPH)
20.0
15.40 mg1L 77 64- 132
Lab Sample ID: LCSD 680-72704813-A
Client Sample ID: Lab Control Sample Dup
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 727079
Prep Batch: 727048
Spike
LCSD LCSD %Rec RPD
Analyte
Added
Result Qualifier Unit D %Rec Limits RPD Limit
SGT-HEM (TPH)
20.0
14.60 mg1L 73 64 - 132 5 34
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-72684013
Client Sample ID: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 726840
MB MB
Analyte Result Qualifier
RL MOL Unit D Prepared Analyzed Dil Fac
Chemical Oxygen Demand <5.0
10 5-0 mg1L 06/21/22 10:28 1
Lab Sample ID: LCS 680-72684014
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 726840
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit D %Rec Limits
Chemical Oxygen Demand
50.0
53.0 mg1L 106 90 - 110
Lab Sample ID: MB 680-72684813
Client Sample ID: Method Blank
Matrix: Water
Prep Type: TotallNA
Analysis Batch: 726848
MB MB
Analyte Result Qualifier
RL IVIDL Unit D Prepared Analyzed Dil Fac
Chemical Oxygen Demand <5.0
10 5.0 mg1L 06/21122 12:32 1
Lab Sample ID: LCS 680-726848/4
Client Sample ID: Lab Control Sample
Matrix: Water
Prep Type: TotallNA
Analysis Batch: 726848
Spike
LCS LCS %Rec
Analyte
Added
Result Qualifier Unit ❑ %Rec Limits
Chemicaf Oxygen Demand
50.0
51.7 mg/L 103 90 - 110
Eurof€ns Savannah
Page 7 of 14 6/22/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT8
Method: SM 2540D - Solids, Total Suspended (TSS)
Lab Sample ID: MB 680-725613/1
Matrix: Water
Analysis Batch: 725613
MB MB
Job ID: 680-216811-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <2.5 2.5 2.5 mg/L 06/14/22 08:17 1
Lab Sample ID: LCS 680-72561312 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 725613
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 951 806 mg/L 85 80 - 120
Lab Sample ID: LCSD 680-725613/3 Client Sample ID: Lab Control Sample Dup
Matrix: Water Prep Type: Total/NA
Analysis Batch: 725613
Spike LCSD LCSD
Analyte Added Result Qualifier Unit
Total Suspended Solids 951 774 mg1L
%Rec RPD
D %Rec Limits RPD Limit
81 80-120 4 25
Eurofins Savannah
Page 8 of 14 6/22/2022

QC Association Summary
Client: ERM-West
Job ID: 680-216811-1
Project/Site: Storm Water
- Amazon Warehouses DRT8
General Chemistry
Analysis Batch: 725613
[Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-216811-1
DRT8_Sample_Point_01_20220608
Total/NA
Water
SM 2540D
660-216811-2
DRT8_Sample_Point_02_20220608
Total/NA
Water
SM 2540D
MB 680-72561311
Method Blank
TotalINA
Water
SM 2540D
LCS 680-725613/2
Lab Control Sample
Total/NA
Water
SM 2540D
LCSD 680-72561313
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Analysis Batch: 726840
FLab
Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-216811-1
DRT8_Sample_Point_01_20220608
Total/NA
Water
5220D-2011
MB 680-726840/3
Method Blank
TotallNA
Water
5220D-2011
LCS 680-72684014
Lab Control Sample
Total/NA
Water
5220D-2011
Analysis Batch: 726848
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-216811-2
DRT8_Sample_Point_02_20220608
Total/NA
Water
52200-2011
MB 680-72684813
Method Blank
Total/NA
Water
5220D-2011
LCS 680-72664814
Lab Control Sample
TbtalINA
Water
5220D-2011
Prep Batch: 727048
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-216811-1
DRTS_Sample_Point_01_20220608
TotallNA
Water
1664B
680-216811-2
DRT8_Sample_Point_02_20220608
Total/NA
Water
1664E
MB 680-72704811-A
Method Blank
Total1NA
Water
1664B
LCS 680-727048/2-A
Lab Control Sample
TotaUNA
Water
1664E
LCSD 680-727048/3-A
Lab Control Sample Dup
TotallNA
Water
16646
Analysis Batch: 727079
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-216811-1
DRT8_Sample_Point_01 20220608
TotallNA
Water
1664E
727048
680-216811-2
DRT8_Sample_Point_02_20220608
TotallNA
Water
1664B
727048
MB 680-72704811-A
Method Blank
Total/NA
Water
1664E
727048
LCS 680-72704812-A
Lab Control Sample
Total/NA
Water
1664E
727048
LCSD 680-72704813-A
Lab Control Sample Dup
Total/NA
Water
1664E
727048
Eurofins Savannah
Page 9 of 14 6/22/2022

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water- Amazon Warehouses DRT8
Job ID: 680-216811-1
Client Sample ID: DRT8_Sample_Point_01_20220608 Lab Sample ID: 680-216811-1
Date Collected: 06/08/22 20:03 Matrix: Water
Date Received: 06/10122 10:30
r
Batch Batch
Prep Type
Type Method
TotatlNA
Prep 1664B
Total/NA
Analysis 1664B
Instrument ID: NoEquip
TotaVNA
Analysis 5220D-2011
Instrument ID: SPC7
Total/NA
Analysis SM 2540D
Instrument ID: NOEQUIP
❑il
Initial
Run Factor
Amount
951 mL
1
1
2 mL
1
1000 mL
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
500 mL
727048
06/22/22 08:30
YR
TAL SAV
727079
06/22122 10:24
YR
TAL SAV
2mL
726840
06/21/2210:28
ALG
TAL SAV
1000 mL
725613
06/14/22 08:17
PG
TAL SAV •
Client Sample ID: DRT8_ Sample_Point_02_20220608 Lab Sample ID: 680-216811-2
Date Collected: 0610812219:42 Matrix: Water
Date Received: 06/10/22 10:30
Batch Batch
Dil
Initial
Final
Batch
Prepared
Prep Type
Type Method
Run Factor
Amount
Amount
Number
or Analyzed
Analyst
Lab
Tota(/NA
Prep 1664E
955 mL
500 mL
727048
06/22122 08:30
YR
TAL SAV
Tota)INA
Analysis 1664B
1
727079
06/22/22 40:24
YR
TAL SAV
Instrument ID: NoEquip
Total/NA
Analysis 5220D-2011
1
2 mL
2 mL
726848
06/21122 12:32
ALG
TAL SAV
Instrument ID: SPC7
Total/NA
Analysis SM 2540D
1
500 mL
1000 mL
725613
06/14122 08:17
PG
TAL SAV
LInstrument ID: NQEQUIP
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 10 of 14
Eurofins Savannah
6/22/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT8
Laboratory: Eurofins Savannah
The accreditations/certifications listed Wow are aDolicable to this report.
FAuthortty
Arkansas DEQ
North Carolina (WWISW)
Job ID: 680-216811-1
Program Identification Number Expiration Date
State 19-015-0 02-01-23
State 269 12-31-22
Eurofins Savannah
Page 11 of 14 6/22/2022

Method Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT8
Job ID: 680-216811-1
Method
Method Description
Protocol
Laboratory
1664B
HEM and SGT-HEM
1664E
TAL SAV
522OD-2011
Chemical Oxygen Demand
SM
TAL SAV
SM 2540D
Solids, Total Suspended (TSS)
SM
TAL SAV
16648
HEM and SGT-HEM (Aqueous)
1664B
TAL SAV
Protocol References:
1664E = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 12 of 14 6/22/2022

-A
N
N
N
O
N
N
Eurofins Savannah
5102 LaRoche Avenue
Savannah GA 31404
Phone.[phone] Fax:[phone]
Chain of Custody Record
eurofins
- Er •[-r+tn; TdR ng
Inerica
Client Information
Sampler
! I- ;€ = f`��j
Lab PM.
Cisneros Roxanne
Corner Tracking No(s)
CDC No.
240.93301-33334 1
Client Contact
Doug Wade
1
i :1ir 1" Iihi
E-Mail
roxanne.cisneres@Eurofinsetcom
Slate of On "n
Page,
Page 1 of 1
Company, `
ERM-West
PWSlD
Analysts Requested
Job 9
.address-
1920 Main Street Sure300
Dee Date Requested. `"k
:`i
0
Z
`o
-
m d
r'0
a
m in
m zr
Z CZ6
o
O
Y1
ce
H
e
ro
5
c
0
E
a
I t°
Preservation Codes.
A -HCL M- Hexane
B NaOH N - None
C Zn Aceiale 0 AsNo02
D Nitric Acid P Na204S
E NaHSO4 Q - Na2503
F Me OH R-Na2S203
G - Amonlor S - H2SO4
H AscorbicAad T- TSPCodecahydrate
t Ice lJ - Acetone
J - Di Water V MCAA
K EDTA W pH 4-5
L ECA Z-other(specify)
Other
City
Irvine
TAT Requested (days):,
Staff nip:
CA, 92614
Compliance Pro)ecu a Yes p No
Phone:
443-812-0046(Teq
POP
DRT8
Email:
doug wade@elm cont
WO #:
Project Name:
Storm Water - Amazon Warehouses
Project#:
24024260
Site F I .T
i�
1 i �
SSOWtt;
tlln
Sam Ee Identification
Sample Date
Sample
Time
Sample
Type
(C-Comp,
G=grab)
Z7
Matrix
SpoiW.
o-,..nwe;t .d
RT rT w,anu.)
Special InstructionslNote
Preservation Code.
XXS
IS
IN
water
J
Water
Llill
in L11i
Possible Hazard Identification
Non -Hazard © Flammable Skin Irritant © Poison B Unknown © Radiologrcal
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
© Retum To Client = Disposal By tab Archive For Months
Deliverable Requested I If ill 1V Other (specify)
Special Instruction%= Requirements
Empty KR Relinquished by- Date. Time: Method of Shipment. =
t.
Rebn ' a�y ✓ ,
0atelTme:
Compsy n`
ReceivM by,
Dalemme: /� r— f �,� C>
L/ v L
Company
Re4KquNkied by
Ratelfilfie
company
Received by
Datefiime:
Company
Relinquished by
DateiTime:
Company
Received by
DaterTme:
Company
Custody Seals Intact:
A Yes A No
CUStody Seal No
C00%r Temperalure(s) °C and Other Remarks. (�
` '
Vcr- Ub1WV2Ull

Login Sample Receipt Checklist
Client: ERM-West .lob Number: 680-216811-1
Login Number: 216811
List Number.1
Creator: Watters, David
Question
List Source: Eurol ins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection dateitimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, Incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 14 of 14
6/22/2022