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HomeMy WebLinkAboutNCG060420_2022 DMR_20220729NCDEQ Division of Energy, Mineral and Land Resources SLui-n-twater Disctlarge iVou-HI iuritrr, nGNVrL tuivfrsl rullrt tur ivLuuovvuv Food and Kindred Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional office. Certificate of Coverage No. NCG060420 Person Collecting Samples: Linda Cortes and Rachel Kohnke Facility Name: Amazon.com Services LLC - DRT7 Laboratory Name: Eurofins Test America Savannah Facility County: Wake Laboratory Cert, No.: 269 Discharge during this period: ❑✓ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Ter response actions this sample period for any benchmark exceedances? ❑ Yes ❑ No If so, which Tier (f, fl, or III)? Tier A copy of this DMR has been uploaded electronically via Inttps://edocs.deq.nc.gov/Forms/SW-DMR 0 Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red) Parameter Code Parameter Outfall001 Outfall002 Outfall003 Outfall Outfall N/A Receiving Stream Class C;NSW C;NSW C;NSW N/A Date Sample Collected MM/DD/YYYY 6/17/2022 6/27/2022 6/17/2022 46529 24-Hour Rainfall in inches 0A 0.1 0.1 C0530 I TSS in mg/L !1nn ^r 50*; 51 23 16 pH in standard units (6,0-9.0 FW, 00400 e o a C CIAO% 5.5 7.66 6.0 Fecal Coliform per 100 ml of 31616 freshwater (if required) =r.T) N/A N/A N/A Enterococci per 100 ml of saltwater 61211 (if required) 1,50n) N/A N/A N/A Chemical Oxygen Demand in mg/L 00340 110 20 150 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A N/A 00552 Non -Polar Oil & Grease in mg/L (15) <1.6 <2.7 <1.6 * Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of So mg/L. All other water classifications have a benchmark of 100 rng/L FW (Freshwater) SVd (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submi d is, the Est of m knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false of rmn, i cluding tM possibility of fines and imprisonment for knowing violations." Sign ure of Permittee df Delegifed Authorized Individual me elin@amazon.com Email Address Z-X 2 2 Date( (404) 590-7247 Phone Number urofins i-._ - - - -- *91 ..4 a -. .... Envi�`onment 1esting America ANALYTICAL ICAL REPORT Eurofns Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-217189-1 Client Project/Site: Storm Water - Amazon Warehouses DRT7 For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade o?"CL vu �ai!"tt17J5 Authorized for release by: 711512022 10:58:52 AM Roxanne Cisneros, Senior Project Manager (615)301-5761 rxanne.cis neros(d�et.eurofinsus.corn The test results in this report meet all 2003 NELAQ 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. 711 Definitions/Glossary Client: ERM-West Job ID: 680-217189-1 Project/Site: Storm Water - Amazon Warehouses DRT7 Glossary Abbreviation These commonly used abbreviations may or may not be present in this report a Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoD/DOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DOD/DOE) LOQ Limit of Quantitation (DOD/DOE) MCL EPA recommended "Maximum Contaminant Level' MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive 1 Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Eurofins Savannah Page 2 of 15 7/15/2022 Sample Summary Client: ERM-West ProjectlSite: Storm Water - Amazon Warehouses DRT7 Lab Sample ID Client Sample ID Matrix Collected Received 680-217189-1 DRT7_Sample_Point_01_20220617 Water 06t17/2219:15 08121/2210:40 680-217189-2 DRT7_Sample_Point_03_20220617 Water 06/17/22 20:00 06/21/22 10:40 Job ID: 680-217189-1 Page 3 of 15 Eurofins Sar�lA&M2 Case Narrative Client: ERM-West Job ID: 680-217189-1 Project/Site: Storm Water - Amazon Warehouses DRT7 Job ID: 680-217189-1 — - Laboratory: Eurofins Savannah Narrative Job Narrative 680-217189-1 Comments No additional comments Receipt The samples were received on 6/21/2022 10:40 AM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 5.90 C. General Chemistry No analytical or quality issues were noted, other than those described in the Definition slGlossary page. Organic Prep Methods 1664B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MSlMSD) associated with preparation batch 400-584672. No additional analytical or quality issues were noted, other than those described above or in the DefinitionslGlossary page. Eurofins Savannah Page 4 of 15 7/15/2022 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Client Sample ID: DRT7_Sample_Point_01_20220617 Date Collected: 06/17/22 19:15 Date Received: 06121/2210:40 General Chemistry Analyte Result Qualifier RL SGT-HEM <1.6 4.5 Total Suspended Solids 51 10 Chemical Oxygen Demand 110 10 Client Sample ID: DRT7_Sam ple_Point_03_20220617 Date Collected: 06/17/22 20:00 Date received: 06/21/22 10:40 FGeneral Chemistry 1 Analyte 1 SGT-HEM Total Suspended Solids Chemical Oxygen Demand Result Qualifier <1.6 16 1.Ri0 RL 4.6 5.0 100 Page 5 of 15 MDL Unit 1.6 mg/L 10 mg/L 5.0 mg/L MDL Unit 1.6 mg/L 5.0 mg/L 50 mg1L Job ID: 680-217189-1 Lab Sample ID: 680-217189-1 Matrix: Water D Prepared Analyzed Dil FacLa 0711312214:47 07/14/2212:24 1 06122/2211:13 1 07/01/22 12:53 1 Lab Sample ID: 680-217189-2 Matrix: Water D Prepared Analyzed Dil Fac 07/13/2214:47 0711412212:24 1 06/22/22 11:13 1 D7101122 12:53 10 Eurofins Savannah 7/15/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Method: 1664E - HEM and SGT-HEM Lab Sample ID: MB 400-58467211-A Matrix: Water Analysis Batch: 584793 MB MB Analyte Result Qualifier RL MDL Unit Job ID: 680-217189-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 584672 U Prepared Analyzed Dil Fac SGT-HEM <1.4 4.0 1.4 mg1L 07/13/2214:47 07/1412212:24 1 Lab Sample ID: LCS 400-58467212-A Client Sample ID: Lab Control Sample Matrix: water Prep Type: iotaiiNA Analysis Batch: 584793 Prep Batch: 584672 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits LSGT-HEM 20.0 17.40 mg1L 87 64 - 332 it .ab Camnle In: LCSD 400_58467213_n Clion} Sample !D: Lab Control CSmnlo Ilim Matrix: Water Prep Type: Total/NA Analysis Batch: 584793 prep Batch: 584672 -r Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit LSGT-HEM 20.0 18.50 mg1L 92 64 -132 5 34 Method: 254OD-2015 - Total Suspended Solids (Dried at 103-1050C) Lab Sample ID: MB 680-72709711 Client Sample ID: Method Blank Matrix: Water Prep Type: TotallNA Analysis Batch: 727097 MB MB Analyte Result Qualifier Total Suspended Solids <2.5 LLab Sample ID: LCS 680-727097/2 �uu �n. uw�' Analysis Batch: 727097 Analyte Total Suspended Solids Lab Sample ID: LCSD 680-727097/3 Matrix: Water Analvsis Batch: 727097 Analyte LT otal Suspended Solids Spike Added 951 Spike Added 951 RL 2.5 Method: 5220D-2011 - Chemical Oxygen Demand LdU Scilliple IG. RED 680-72862313 Matrix: Water I Analysis radtCu. 71208823 NIB MB Analyte Result Qualifier RL Chemical Oxygen Demand MDL Unit D Prepared Analyzed DII Fac 2.5 mglL 06/22/22 11:13 1 Client Sample ID: Lab Control Sample n- - M,pc. T..a-.I 6.t A 1 IGF IyNI:. 1— II ivi LCS LCS %Rec Result Qualifier Unit D %Rec Limits 814 mglL 86 80 -120 Client Samole ID: Lab Control Samole Duo Prep Type: TotallNA LCSD LCSD %Rec RPD Result Qualifier Unit D %Rec Limits RPD Limit 804 mglL 85 80.120 1 25 /C1!_._t n_.__ l.11rlll adIIIlJIC ID: IYIeIFIVU alalli5 Prep Type: Total/NA MDL Unit D Prepared Analyzed Dil Fac 5.0 mg/L 07101/2212:53 1 EUrDfinS Savannah Page 6 of 15 7/15/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Method: 5220D-2011 - Chemical Oxygen Demand (Continued) Lab Sample ID: LCS 680-728823/4 Matrix: Water Analysis Batch: 728823 Spike LCS LCS Analyte Chemical Oxygen Demand Job ID: 680-217189-1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Added Result Qualifier Unit 50.0 54,3 mg/L %Rec D %Rec Limits log 90-110 Eurofins Savannah Page 7 of 15 7/15/2022 QC Association Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 General Chemistry Prep Hatch: 584672 FLab Sample ID Client Sample ID Job ID: 680-217189-1 Prep Type Matrix Method Prep Batch 680-217189-1 DRT7_Sample_Point_01_20220617 Total/NA Water 1664E 680-217189.2 DRT7 Sam ple_Point_03_20220617 Total/NA Water 1664E MB 400-58467211-A _ Method Blank Total/NA Water 1664B LCS 400-584672/2-A Lab Control Sample Total/NA Water 1664B LLCSD 400-58467213-A Lab Control Sample Dup Total/NA Water 1664B Analysis batch: 584793 I Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217189-1 DRT7 _Sample_Point 01_20220617 TotaYNA Water 1664B 584672 680-217189-2 DRT7 Sampie_Point_03 20220617 TotaUNA Water 1664E 584672 MB 400.584672/1-A Method Blank Total/NA Water 1664B 584672 LCS 400-58467212-A Lab Control Sample Total/NA Water 1664B 584672 LLCSD 400-584672/3-A Lab Control Sample Dup TotaUNA Water 1664E 584672 rvraryai5 catch. 721007 rLab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217189-1 DRT7_Sample_Point_01_20220617 TotaUNA Water 254OD-2015 680-217189.2 DRT7_Sample_Point_03_20220617 TotaYNA Water 2540D-2015 MB 680-727097/1 Method Blank TotalINA Water 2540D-2015 LCS 680-72709712 Lab Control Sample TotalINA Water 2540D-2015 LLCSD 680-72709713 Lab Control Sample Dup TotaUNA Water 254OD-2015 Analysis Batch: 728823 LLab Sample IA Client Sample ID Prep Type Matrix Method Prep Batch 680-217189-1 DRT7_Sample_Point_01_20220617 Total/NA Water 5220D-2011 680-217189-2 DRT7_Sample_Point_03_20220617 TotaIINA Water 5220D-2011 MB 680-72882313 Method Blank Total/NA Water 5220D-2011 LLCS 680-72BB23/4 Lab Control Sample Total/NA Water 5220D-2011 Eurofins Savannah Page 8 of 15 7/15/2022 Lab Chronicle Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Client Sample ID: DRT7_ Sample_Point_01_20220617 Date Collected: 06/17/22 19,15 Date Received: 06121/22 10:40 r Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 885 mL Total1NA Analysis 1664E 1 Instrument ID: J.T. Baker 1&2 Total/NA Analysis 254OD-2015 1 250 mL Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 Instrument ID: SPC7 1 2 mL Client Sample ID: DRT7_ Sample_Point_03_20220617 Date Collected: 06/17/22 20:00 Date Received: 06/21/22 10:40 r— Batch Batch Dil Initial Prep Type Type Method Run Factor Amount TotallNA Prep 1664E 873 mL Total/NA Analysis 1664B 1 Instrument ID: J.T. Baker 1&2 TotallNA Analysis 2540D-2015 1 500 mL Instrument ID: NOEQUIP Job ID: 680-217189-1 Lab Sample ID: 680-217189-1 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 1000 ml- 584672 07/13/22 14A7 ARE TAL PEN 584793 07/14122 12:24 ARE TAL PEN 1000 mL 727097 06/22/22 11:13 PG TAL SAV 2 mL 728823 07/01/22 12:53 ALG TAL SAV Lab Sample ID: 680-217189-2 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 1000 mL 584672 07/13/22 14:47 ARE TAL PEN 584793 07/14/22 12:24 ARE TAL PEN 1000 mL 727097 06/22/22 11:13 PG TAL SAV TotaUNA Analysis 5220D-2011 10 2 mL 2 mL 728823 07/01/22 12:53 ALG TAL SAV L Instrument 1D: SPC7 Laboratory References: TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 9 of 15 7/15/2022 Accreditation/Certification Summary Client: ERM-West Job iD: 680-217189-1 ProjectlSite: Storm Water - Amazon Warehouses DRT7 Laboratory: Eurofins Savannah The accreditationslcertifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WWISW) State 269 12-31-22 Laboratory: Eurofins Pensacola All accreditations/certifications held by this laboratory are listed. Not all accreditationslcertifications are applicable to this report. Authority Program Identification Number Expiration Date Alabama State 40150 06-30-23 ANAB ISOIIEC 17025 L2471 02-23-23 Arkansas DEQ State 88-0689 09.01-22 California State 2510 06-30-23 Florida NELAP E81010 06-30-23 Georgia State E81010(FL) 06-30-23 Illinois NELAP 200041 10-09-22 Kansas NELAP E-10253 10-31-22 Kentucky (UST) State 53 06-30-23 Kentucky (WW) State KY98030 12-31-22 Louisiana (All) NELAP 30976 06-30-23 Louisiana (DW) State LA017 12-31-22 Maryland State 233 09-30-22 Michigan State 9912 06-30-23 North Carolina (WWISW) State 314 12-31-22 Oklahoma NELAP 9810 08-31-22 Pennsylvania NELAP 68-00467 01-31-23 South Carolina State 96026 06-30-23 Tennessee State TN02907 06-30-23 Texas NELAP T104704286 09-30-22 US Fish & Wildlife US Federal Programs A22340 06-30-23 USDA US Federal Programs P330-21-00056 05-17-24 Virginia NELAP 460166 06-14-23 West Virginia DEP State 136 03-31-23 Eurofins Savannah Page 10 of 15 7/15/2022 Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Method Method Description Protocol Laboratory 1664E HEM and SGT-HEM 1664B TAL PEN 254OD-2015 Total Suspended Solids (Dried at 103-105"C) SM TAL SAV 522OD-2011 Chemical Oxygen Demand SM TAL SAV 1664E HEM and SGT-HEM (Aqueous) 1664B TAL PEN Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL PEN = Eurollns Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 11 of 15 7/15/2022 N O N N Eurofins Savannah 5102 LaRoche Avenue Savannah GA 314D4 Phone 912-354-7858 Fax:912-352-0165 Chain of Custody Record „• eurofins Client Information Sampler ��-t a S[�a Lab PM- Cisneros Roxerne Carrier Tracking NDIs) CCC No, 240-93304-33337 1 Diem Contact Doug Wade�� Ph p��� E-Mail: roxanne cisneros@Eurofinset.com State of Odgn. %1Ci Page: Page 1 of 1 Company ERIA-west PWSID Analysts Requested Job t Address, 1920 Main Street Suite 300 Due Date Requested- l [� Q .: Z O o m z. } o m E W eJ m g a o cr a o w Z ' N `m L c 0 0 E i t°- Preservation Codes A - HCI, M - Hexane N None C Zn Acetate D- N Acid P Na20 S E • NaHSC4 Q Na2SO3 F McOH R N32S303 G • Amehlor S H2504 H Ascorbic Acid T - TS❑ DodeCahydrate I tce U Acetone J- DtWater V-MCAA K - EDTA W - pH 4-5 L - EDA Z other [spemfy) other C,ty Irvine TAT Requested (days): n „1 C� Stale. Zip' CA, 92614 Compliance Project b Yes A No Phone: 443 812-0OA6(Te!) PC ih DRIi Email- dougwade@ermcom WO#: Project Name-, Storm Water -Amazon Warehouses Pro)ect #: 24024260 SSOW#� a� Sample Identification Sample Date Sample Time Sample Type (C=comp, G= rah) Matrix eT,n.ay..�wi I, Special Instructions/Note Preservation Code: S S N O� 1 `4 l4CU� 1l1�L�vY � l 11 �� C l . 4Gj C� Water I� I e, ii Water XJX Water 68(>-217189 Chain of Custody Possible Hazard ldenI ficatron M Non -Hazard © Flammable Skin Witant Poison B © Unknown Radiological Sample Disposal (A fee may be assessed if samples are retained longer than Y month) 0 Retum To Client © Disposal By Lab Archive For Months Deliverable Requested ( (I lit fV Other (speedy) Special Instructions= Requirements. Empty Kit Relinquished by Date. Time Method or Shipment Relinquished by Date/Tim Co n ReCe+ved by DbteJTim.: Company Relinquished Daten5rne: Company Received by- Daterr ne: Company Relinquished by W:,p nme_ Company Received by Dalernme: Company Custody Seals Intact: A Yes A No Custody Seal NQ L —1 Cooler Tempemrure(s) °C and Other Rema*s- Ver 0610S/3021 -4 N O N N Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Phone: 912-354--r 858 Fax: 912-352-016E Chain of Custody Record t� UtI�Ut1� I ~-'- eUtOfinS I Ame�ocnment Testing smear Lille PM Carder Tradatg "s): CDC No Client Information (Sub Contract Lab) Cisneros, Roxanne 680-700927.1 Client Contact Phone E•Maii: State of Origin, Page Shipping/Receiving roxanne.cisnaros@et.euro8nsus.com North Carolina Page 1 of 1 Compapr I Accreditabons Required (See note). Job a Eurofins Environment Testing Southeast, State Program-- North Carolina (WW1SW) 680-217189-1 Address, Due Date Requested: Preservation Codes: 3355 Mclemore Drive, 7/5/2022 Analysis Requested M -Mariana, A-NBO N-None a • Ns� City: TAT Requested (days): Pensacola O - AsNaO2 C • 2n acetate P - Na2045 D • Nrtnc Acid O•Na2S03 State, Tip FL, 32514 E-NaHSO4 F • McOH R - Ns2S2O3 G -Amchbr Pierre O a' 850-474-1001(Tel) 850-478-2671(Fax) ze w T- T P Dodecehydrate H- Ascorbicaad I - Ice U -Acetone Email. WO a Z o F c J -OI Water W PN� 4-5 L - EDTTA Y - Tiaras EDA Protect Name. Projact it Storm Water - Amazon Warehouses DRTT 66026743 E it o o 2 - odw (specify) Other: Site: SSOW# Sample Matrix $ E Type Sample (C=comp, o..n.baM O 1o°� as 3 Sample Identification - Client ID (Lab IC ample Date Tim G= tab)er.Ts..., !� r :° F Special Instructions/Note: _ Preservation Cade: DRTT Sample_Point_01 20220617 (68a217189 1) 6/17/22 19:1 Water X 2 ORT7_Sample_Point 03_20220617 (680.217189 2) 6/17/22 20'0 Water X 2 Now. Since laboratory aceredristions am subjed to (hange, Eurorea Erwironmerd Tndng Southeast, LLC places the awnership of method, analyte & accreditation oompbartce upon out subcontract laboratories This sample shipment is forwarded under chain -of -custody. If the laboratory does not currently me ntem accrcditatlon in the Stall of Origin listed above for analysisneals/matrar being analyt:dd, the samples must be shipped back to the Eurotms Environment Testing Southeast, LLC laboratory or other rntr cton will be provided Any changes to accreditation Mat" should be brought to Euranna Enwronmerd Toapng Southeast. LLC aftenhon immediately If ab requested accreditation are current to date, return the signed Chain of Custody attesting to sad compllcance to Eumftns EmAronment Tesmg Southeast. I.I.C. Possible Hazara Identification Sample Disposal (A fee maybe assessed 11'samples are retained longer than 1 month) Unconfirmed I =1 Retum To CWnt 0 Disposal By Lab Archive For Months Deliverable Requested: I, II, III, IV, Other ;specify) Primary Deliverable Rank: 2 Special Instructions/QC Requirements: Empty Kit Relinquished by: Date: Time: Method of Shipment Relinquished by—+07-- Daten'mte• company Received by Datemme: Company 7 1{ )�- Relinquished by Date/Time, Company Reoelved by Daternma: Company Relinquished by Dateirri ns, Company Received by. DaW ime: Company Q M ,02 Custody Seals Intact: Custody Seat No.: Cooler Tomperature(s)°Cand Other Remaft:GLv` I y t} ,`.,� ��� 7 -Ir a Yes d No 4 cK Ver: 06109/2021 Login Sample Receipt Checklist Client: ERM-West Login Number: 217189 List Number: 1 Creator: Sims, Robert D Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection dateltimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Job Number: 680-217189-1 List Source: Eurofins Savannah Eurofins Savannah Page 14 of 15 7/15/2022 Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217189-1 Login Number: 217189 List Number: 2 Creator: Roberts, Alexis J Question Answer List Source: Eurofins Pensacola List Creation: 07/12/22 01:43 PM Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True 1578329,1578330,1578331 Sample custody seals, if present, are intact. NIA The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True 5.6°C, 5.4°C, 4.0°C, 2.4°C IR8 COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection datettimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is NIA <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Savannah Page 15 of 15 7/15/2022 urofins IM Environment resting 1 America ANALYTICAL REPORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-217508-1 Client ProjectlSite: Storm Water - Amazon Warehouses DRT7 Revision: 1 Fnr ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 7/18/2022 1:30:39 PM Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cis neros@et.eurofinsus. corn The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Glossary n Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio {normalized absolute difference) ❑il Fac Dilution Factor DL Detection Limit (DoD/DOE) DL. RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoDIDOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative / Absent POS Positive I Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-217508-1 Eurofins Savannah Page 2 of 15 7/18/2022 (Rev, 1) Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Lab Sample ID Client Sample ID Matrix Collected Received 680-217508-1 5R 77_Sample_Point_02 20220627 Water 06/27/2217:26 06/28/2210:30 Job ID: 680-217508-1 Page 3 of 15 Eura MZWA4RW. 1) Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Job 1D: 680-217508-1 Laboratory: Eurofins Savannah Narrative Job narrative 680-21E 7508-1 Comments Revised Report 7/18/2022 to change sample ID per client email request Job ID: 680-217508-1 Receipt The sample was received on 6/28/2022 10:30 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 0.50 C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Organic Prep Methods 1664B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicate (MSIMSD) associated with preparation batch 400-584672. No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page. Eurofins Savannah Page 4 of 15 7/18/2022 (Rev. 1) Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Client Sample ID: DRT7_Sample_Point_02_20220627 Date Collected: 06/27/22 17:26 Date Received: 06/28/22 10:30 General Chemistry Analyte Result Qualifier RL au i-mr-M Total Suspended Solids Chemical Oxygen Demand <2.7 7.7 23 3.3 20 10 Job ID: 680-217508-1 Lab Sample ID: 680-217508-1 Matrix: Water hADL Unit D Prepared Analyzed Dii Fac 2.7 mglL 07113/2214:47 0711412212:24 1 3.3 mglL 06/3012214:19 1 5.0 mglL 07/1112213:03 1 Eurofins Savannah Page 5 of 15 7/18/2022 (Rev. 1) QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Method: 1664B - HEM and SGT-HEM r Lab Sample ID: MB 400-58467211-A Matrix: Water Analysis Batch: 584793 MB MB Analyte Result Qualifier SGT-HEM <1.4 Lab Sample ID: LCS 400-584672/2-A matrix: water Analysis Batch: 584793 Analyte SGT-HEM rLab Samp!c ID: LCSD 400-58467213-A Matrix: Water Analysis Patch: 584793 Analyte LSGT-HEM Job ID: 680-217508-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 584672 RL MDL Unit D Prepared Analyzed Dil Fac 4.0 1.4 mg/L 07113/2214:47 0711412212:24 � 1 Client Sample ID: Lab Control Sample Prep Type: Total/NA Prep Batch: 584672 Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 20.0 17.40 mg/L 87 64 - 132 f Hent Sample !D: Lab Control Sam-!e Du - Prep Type: TotallNA Gran Batch: 584672 Spike LCSD LCSD %Rec RPD Added Result Qualifier Unit D %Rec Limits RPD Limit 20.0 18.50 m91L 92 64 -132 6 34 Method: 264OD-2016 - Total Suspended Solids (Dried at 103-1050C) F- Lab Sample ID: MB 680-72859311 Client Sample ID: Method Blank Matrix: Water Prep Type: TotallNA Analysis Batch: 728593 MB MB Analyte Result Qualifier Total Suspended Solids <2.5 Lab Sample ID: LCS 680-728593/2 a,- ,X: tier., IG kIA. NYut�r Analysis Batch: 728593 LAnalyte Total Suspended Solids Lab Sample ID: LCSD 680-72859313 Matrix: Water Analvsis Batch: 728593 Analyte LTotal Suspended Solids RL MDL Unit 2.5 2.5 mg/L D Prepared Analyzed Dil Fac 06/30/22 14:19 1 Ciient Sample ID: Lab Control Sample Prep Typc: .-tall".A Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 951 806 mg1L 85 80 -120 Client Sample ID: Lab Control Sample Dur) Prep Type: TotallNA Spike LCSD LCSD Added Result Qualifier Unit 951 798 mg/L %Rec RPD D %Rec Limits RPD Limit 84 80 -120 1 25 Method: 5220D-2011 - Chemical Oxygen Demand W Lab Sarnpie ID: i>TB 680-730044/3 Client Sample ID: Method Bianik Matrix: Water Prep Type: Total/NA Analysis Batch: 73004: MB M8 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Chemical oxygen Demand 5.0 mg1L 07/11 /22 13:03 1 Eurofins Savannah Page 6 of 15 7/18/2022 (Rev. 1) QC Sample Results Client: ERM-West Job ID: 680-217508-1 Project/Site: Storm Water - Amazon Warehouses DRT7 Method: 5220D-2011 - Chemical Oxygen Demand (Continued) r Lab Sample ID: LCS 680-73004414 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 730044 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 48.2 mglL 96 90 -110 Lab Sample ID: 680-217508-1 MS Client Sample ID: DRT7_Sample_Point_02�20220627 Matrix: Water Prep Type: TotaliNA Analysis Batch: 730044 Sample Sample Spike MS MS %Rec Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits LOhemicai Oxygen Demand 20 FLab Sample !D: 680-217508-1 nfcD Matrix: Water Analysis Batch: 730044 S I 5 i Analyte Chemical Oxygen Demand amp amp Result Qualifier 20 50.0 71.9 mg/L 104 90 - 110 CHent Sarnple !D: DRT7_Sample po;-* n�_�n77n677 Prep Type-Total/NA Spike MSD MSD Added Result Qualifier Unit 50.0 71.5 mglL %Rec RPD D %Rec Limits RPD Limit 103 90-110 0 30 Eurofins Savannah Page 7 of 15 7/18/2022 (Rev. 1) QC Association Summary Client: ERM-West Job ID: 680-217508-1 Project/Site: Storm Water - Amazon Warehouses DRT7 General Chemistry Prep Batch: 584672 FLab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217508-1 DRT7_Sample_Point_02_20220627 Total/NA Water 1664E MS 400-584672/1-A Method Blank Total/NA Water 1664E LCS 400-58467212-A Lab Control Sample TotatlNA Water 16646 LCSD 400-58467213-A Lab Control Sample Dup Total/NA Water 16646 Analysis Batch: 584793 j Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217508-1 DRT7_Sample_Point_02_20220627 Total/NA Water 1664E 584672 MB 400-584672/1-A Method Blank TotalINA Water 1664E 564672 LCS 400-584672/2-A Lab Control Sample Total/NA Water 1664E 584672 LCSD 400-58467213-A Lab Control Sample Dup Total/NA Water 1664B 584672 Analysis Batch: 728593 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217508-1 DRT7_Sample—Point_02_20220627 Total/NA Water 254OD-2015 MB 680-72859311 Method Blank Total/NA Water 2540D-2015 LCS 680-72859312 Lab Control Sample Total/NA Water 254OD-2015 LCSD 680-728593/3 Lab Control Sample Dup Total/NA Water 254OD-2015 Analysis Batch: 730044 Lab Sample ID Client Sample ID 680-217508-1 DRT7_Sample_Poini-02_20220627 MB 680-73004413 Method Blank LCS 680-73004414 Lab Control Sample 680-217508-1 MS DRT7_Sample_Point_02_20220627 680-217508-1 MSD DRT7_Sample_Point_02_20220627 Prep Type Matrix Total/NA Water Total/NA Water TotaVNA Water TotalINA Water TotalINA Water Method 5220D-2011 5220 D-2011 5220D-2011 5220D-2011 5220D-2011 Prep Batch Eurofins Savannah Page 8 of 15 7/18/2022 (Rev. 1) Lab Chronicle Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Job ID: 680-217508-1 Client Sample ID: DRT7_ Sample_Point_02_20220827 Lab Sample ID: 680-217508-1 Date Collected: 06/27/22 17:26 Matrix: Water Date Received: 06/28122 10:30 Batch Batch ail Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664E 518 mL 1000 mL 584672 07/13/22 14:47 ARE TAL PEN Total/NA Analysis 1664B 1 584793 07/14/22 12:24 ARE TAL PEN Instrument ID: J.T. Baker 1&2 Total/NA Analysis 2540D-2015 1 750 mL 1000 mL 728593 06/30/22 14:19 PG TAL SAV Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL 2 mL 730G44 07/11/22 13:03 ALG TAL SAV Instrument ID: SPC7 Laboratory References: TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 9 of 15 7/18/2022 (Rev. 1) Accreditation/Certification Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Job ID: 680-217508-1 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date LNorth Carolina (WWISW) State 269 12-31-22 Laboratory: Eurofins Pensacola All accreditationslcertifcations held by this laboratory are listed. Not all accreditationstcertifi cations are applicable to this report. LAuthority Program Identification Number Expiration Date Alabama State 40150 06-30-23 ANAB ISO/IEC 17025 L2471 02-23-23 Arkansas DEQ State 88-0689 09-01-22 California State 2510 06-30-23 Florida NELAP E81010 06-30.23 Georgia State E81010(FL) 06-30-23 Illinois NELAP 200041 10-09-22 Kansas NELAP E-10253 10-31-22 Kentucky (UST) State 53 06-30-23 Kentucky (WW) State KY98030 12-31-22 Louisiana (All) NELAP 30976 06-30-23 Louisiana (DW) State LA017 12-31.22 Maryland State 233 09-30-22 Michigan State 9912 06-30-23 North Carolina (WW/SW) State 314 12-31-22 Oklahoma NELAP 9810 08-31-22 Pennsylvania NELAP 68-00467 01-31-23 South Carolina State 96026 06-30-23 Tennessee State TN02907 06-30-23 Texas NELAP T104704286 09-30-22 US Fish & Wildlife US Federal Programs A22340 06-30-23 USDA US Federal Programs P330-21-00056 05-17-24 Virginia NELAP 460166 06-14-23 West Virginia DEP State 136 03-31-23 Eurofins Savannah Page 10 of 15 7/18/2022 (Rev. 1) Method Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DRT7 Job ID: 680-217508-1 Method Method Description Protocol Laboratory 1664B HEM and SGT-HEM 1664B TAL PEN 2540D-2015 Total Suspended Solids (Dried at 103-105"C) SM TAL SAV 5220D-2011 Chemical Oxygen Demand SM TAL SAV 1664B HEM and SGT-HEM (Aqueous) 1664B TAL PEN Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL PEN = Eurofins Pensacola, 3355 McLemore Drive, Pensacola, FL 32514, TEL (850)474-1001 TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 11 of 15 7/18/2022 (Rev. 1) CD .a N -0 01 Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Chain of Custody Record .;% eurofins 244- • �.. " ® . = IS-NaOH N-Nom •• ED it �•�w. Y ��._ C' •If :'1 r, � ' t arm r t �uetry orawe lceauesorc. � 11 M IV %pum" 1400GIM I �l f` v-,,75�t� bO = KOL(,O IV iu 15@' 1 � ��2� lJ�� �s�'�o✓S_ i Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Phone: 912-354-1858 Fax: 912-352-0165 Chain of Custody Record eurofins cn�u>-rrcm �esftng Sampler Lob PM: CaMerTncksgNola).* COCNo• Client Inform tion Sub Contradt Lab Clsnetos, Roxanne 680-700927.1 Client Contact Phone E-Mail: State of Origin. Psge: Shipp-ing/Recenrtttg roxanne.cisneros@eLeurofinsus.com North Carolina Page 1 of 1 Company Atxreditadons Required (See note) Job # Eurofins Environatent Testing Southeast, State Program - North Carolina (W WISW) 680-217508-1 Address. Due alto Requested: Preservation Codes: 3355 McLemore Drive, 7/12f2022 Analysis Requested A•HCL M-Hexane e - NaOH N - Noire O-AaNa02 Gty. AT Requested (days): Pensacola C-Zn Acetate D - Nitric Acid P • Na2045 O - N82S03 E NaHSO4 State, Zip FL, 32514 x R - Na2S203 F - McOH S - H2SO4 Do Harare Phone Poo. 850.474-1001(Tel) 850-478-2671(Fax) pp g = H-Ascorbic Add u-T�� J Ira V - MCAA -Ol Water Email: WO Ill.Z Z $ o (is 5 W-pl-14-5 A Y . Trims L - EDA Prged Name pct #: Storm Water - Anlazon Warehouses DRT7 68026743 Q O z -other (spacny) Other: Site: BSOWfk. F �r o.t �u m Sample Matrix g Type Sample (C=Comp, 0:..b0A S Sample Identifietltlon - Client ID Lab Itl Sam le Date Time G= rab) ar m..w.,Auu P. ti s° Special InstructlonsfNote: Preservation Code: DRT7_Sample_13oint 20220627 (680-211508-1) 6/27/22 Water X 2 Eastetn Note- Since laboratory accrednadora are subject to ilhangs, Eurorms Environment Testing Southeast. LLC places the ownership of method, ans%rte It accreditation compliance upon out subcontract laboretones This sample shipment is forwarded under chain -of -custody If ttu laboratory does not currently maintain accreditation in the State of Origin dated above for analysisRests/matrix being analyzed, the samples must be shipped back to the Eurofins Environment Testing Southeast. LLC laboratory or other instructions will be provided. Any changes to aareditahon status should be broubht to Eurotlns Environment Testing Southeast LLC attentlot Irnmedtatety. If all requested accretbtaboris are current to date, return the signed Chain of Custody attesting to sob compitcance to Eumfft Emlronment Testirg Southeast. LLC Pid.thle Haza Identification Sample Disposal (A fee may be assessed if samples are retained longer than i month) 0 ED ED For Months Unconfirmed Return To Client Disposal By tab Archive Deliverable Requested: 1, 11, III, IV, Other (specify) Primary Deliverable Rank: 2 Special Instructions/QC Requirements: Empty Kit Relinquished by: Date: Time: Method of shipment RelinqutWad by. DaterTtme: Company RecoNed by Datttlrume: Company ( r,v Relinquished by: ostarrime Company Received by Datefrane: Company Relinciuiahed by Daterrime- Company Received by oatorrme. � Company Custody Seals Intact Custody Seat No.: Cooler Temperature(s) °C and Other Remarks � �� � � ` nvc /% i� U C, "L O e Yes A No ver: uorvm.cvc i Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217508-1 Login Number: 217508 List Source: Eurof;ns Savannah List Number: 1 Creator: Watters, David Question Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent Information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurof ns Savannah Page 14 of 15 7/18/2022 (Rev. 1) Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217508-1 Login Number: 217608 List Number: 2 Creator: Roberts, Alexis J Question Answer List Source: Eurofins Pensacola List Creation: 07/12/22 01:49 PM Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True 1578329,1578330,1578331 Sample custody seals, if present, are intact. N/A The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True 5.6°C, 5.4°C, 4.0°C, 2.4°C IR8 COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspaoe have no headspace or bubble is N/A <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Savannah Page 15 of 15 7/18/2022 (Rev. 1)