HomeMy WebLinkAboutNCG060423_2022 DMR_20220729NCDEQ Division of Energy, Mineral and Land Resources
Storitiwater Discharge Monitor rig Report (DPAR) Forth for NCU-000000
Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormvrater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG060423
Person Collecting Samples: John Speed
Facility Name: Amazon.com Services LLC - DLT8
Laboratory Name: Eurofins Test America Savannah
Facility County: Mecklenburg
Laboratory Cert. No.:269
Discharge during this period: ❑ Yes ❑✓ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes El No
If so, which Tier (I, II, or ill)?
A copy of this DMR has been uploaded electronically via stps://edocs.cieg.nc.goy/Forms/SW-DMR 0 Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in 4Red)
Parameter
Code
Parameter
Outfall 001
Outfall
Outfall
Outfall
O utfa II
N/A
Receiving Stream Class
C
N/A
Date Sample Collected MM/DDIWYY
06/29/2022
46529
24-Hour Rainfall in inches
01
C0530
TSS in mg/L f100 or 50*)
7.6
pH in standard units (6.0— 9.0 FW,
00400
6.3-3.5SL.')
5.61
Fecal Coliform per 100 ml of
31616
freshwater (if required) I_000)
N/A
Enterococci per 100 ml of saltwater
61211
(if required) (500)
N/A
Chemical Oxygen Demand in mg/L
00340
18
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
00552
Non -Polar Oil & Grease in mg/L (15)
1.3
" Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 nI,/!.
rtw (Freshwater) SW (saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted i to thg bes of my knpFvledge a d belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false info m dtj
incl ing o sibility o fines�a d imprisonment for knowing violations."
Signa#jle of Permittee o elegated Authorized Individual Date
mcdMlin@amazon.com (404) 590-7247
Email Address
Phone Number
urofins
Environment Testing
America
ANALYTICAL REPUORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: (912)354-7858
Laboratory Job ID: 680-217710-1
Client Project/Site, Storm Water - Amazon Warehouses DLT8
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
Authorized for release by:
711812022 9:12.05 AM
Roxanne Cisneros, Senior Project Manager
(615)301-5761
roxanne.cisneros(Cr et.eUfOfinSU5.COrn
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNl
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent at a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
Definitions/Glossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary _
Abbreviation These commonly used abbreviations may or may not be present in this report.
a Listed under the " D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample
DLC Decision Level Concentration (Radiochemis(ry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DoDIDOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative I Absent
POS Positive 1 Present
PQL Practical Quantitation Limit
PRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTC Too Numerous To Count
Job ID: 680-217710-1 -- -
Eurofins Savannah
Page 2 of 12 7/18/2022
Sample Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Lab Sample ID Client Sample ID Matrix Collected Received
680-217710-1 DLT8_Sampie_Point 01_20220629 Water 06129l22 09:07 07/01/22 11:00
Job ID: 680-217710-1
Page 3 of 12 Eurofins Sai ANW2
Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
.fob ID: 680-217710-1
Laboratory: Eurofins Savannah
Narrative
Job ID: 680-217710-1
Ed
Job Narrative
680-217710-1
Comments
No additional comments.
Receipt
The sample was received on 7/1/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.1 ° C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 12 7/18/2022
Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Client Sample ID: DLT8_Sample_Point_01_20220629
Date Collected: 06/29/22 09:07
Date Received: 07/01/22 11:00
General Chemistry
Analyte Result
Qualifier
RL
MDL Unit
Oil 8 Grease (HEM)
1.3 J
2.8
0.77 mgil
Total Suspended Solids
7.6
2.5
2.5 mg/L
Chemical Oxygen Demand
18
10
5.0 mg/L
Job ID: 680-217710-1
Lab Sample ID: 680-217710-1
Matrix: Water
D Prepared Analyzed Dil Fac
07/12/22 08:59 07/12/22 13:33 1
07/05/22 15:02 1
07/16/22 11:16 1
Eurofins Savannah
Page 5 of 12 7/18/2022
QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Method: 1664E - HEM and SGT-HEM
r
Lab Sample ID: MB 680-73020311-A
Matrix: Water
Analysis Batch: 730293
Jab ID: 680-217710-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 730203
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Oil & Grease (HEM) - <1.4 5.0 1.4 mg/L 07/12/22 08:59 07/12/22 13:33 1
FLab Sample ID: LCS 680-73020312-A Client Sample 1D: Lab Control Sample
Matrix: Water Prep —type: TotaiiNA
Analysis Batch: 730293 Prep Batch: 730203
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
I Oil & Grease (HEM) 40.0 36.40 mg/L v 91 78- 114
Method. 254OD-2015 - Total Suspended Solids (Dried at 103-105°C)
[Lab Sample ID: MB 680-72913611 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729136
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
Total Suspended Solids <2.5 2.5 2.5 mglL 07/05/22 15:02 1
Lab Sample ID: LCS 680-729136/2 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 729136
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 951 908 mg/L 95 80-120
F
Lab Sample ID: LCSD 680-72913613 Client Sample ID: Lab Control Sample Dup
Matrix. •iIutcr Prop yrc. Iv alli�ra
Analysis Batch: 729136
Spike LCSD LCSD %Rec RPD
Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
LTotal Suspended Solids 951 932 mglL 98 80-120 3 25
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-73100913 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 731009
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
LChemical Oxygen Demand <5.0 10 5.0 mg1L 07/10/22 11:16 1
F-Lab Sample ID: LCS 680-7 3100914 Client Sample ID: Lab Control Saiiipie
Matrix: Water Prep Type: Total/NA
Analysis Batch: 731009
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
Chemical Oxygen Demand 60.0 45.9 mg1L 92 90 -110
Eurofins Savannah
Page 6 of 12 7/18/2022
QC Association Summary
Client: ERM-West Job ID: 680-217710-1
Project/Site: Storm Water - Amazon Warehouses DLT8
General Chemistry
Analysis Batch: 729136
I Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217710-1
DLT8_Sample_Point_01_20220629
Total/NA
Water
254OD-2015
MB 680-729136tl
Method Blank
TotalINA
Water
2540D-2015
LCS 680-729136/2
Lab Control Sample
Total1NA
Water
2540D-2015
LCSD 680-72913613
Lab Control Sample Dup
Total/NA
Water
25400-2015
Prep Batch: 730203
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217710-1
DLT8_Sample_Point_01_20220629
Total/NA
Water
1664E
i MB 680-730203/1-A
Method Blank
TotallNA
Water
1664B
LCS 680-73020312-A
Lab Control Sample
Total/NA
Water
1664B
Analysis Batch: 730293
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLT8_ Sample_Point_01_20220629
Total/NA
Water
1664E
73D203
MB 680-73020311-A
Method Blank
TotaVNA
Water
16646
730203
V LCS 680-730203/2-A
Lab Control Sample
Total1NA
Water
1664B
730203
Analysis Batch: 731009
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLT8_Sample_Point_01 20220629
Total/NA
Water
5220D-2011
MB 680-731009/3
Method Blank
Total/NA
Water
5220D-2011
LCS 680-73100914
Lab Control Sample
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 7 of 12 7/18/2022
Lab Chronicle
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Client Sample ID: DLT8_Sample_Poinf_01_20220629
Date Collected: 06129122 09:07
Date Received: 07101122 11:00
Batch Batch
oil
Initial
Prep Type Type Method
Run Factor
Amount
Total/NA Prep 1664B
906 mL
Total/NA Analysis 16646
1
instrument ID: NoEquip
Total/NA Analysis 254OD-2015
1
1000 mL
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1
2 mL
Instrument ID: SPC7
Job ID: 680-217710-1
Lab Sample ID: 680-217710-1
Matrix: Water
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
500 mL
730203
07l12122 08:59
YR
TAL SAV
730293
07/12/22 13:33
YR
TAL SAV
1000 mL
729136
07/05/22 15:02
PG
TAL SAV
2 mL 731009 07/16/22 11:16 ALG TAL SAV
13
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
Eurofins Savannah
Page 8 of 12 7/18/2022
Accreditation[Certification Summary
Client: ERM-West Job ID: 680-217710-1
Project/Site: Storm Water - Amazon Warehouses ❑LT8
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
North Carolina (WWlSW) Stale 269 12-31-22
VM
f
Eurofins Savannah
Page 9 of 12 7/18/2022
Method Summary
Client: ERM-West
ProjectlSite: Storm Water - Amazon Warehouses DLTB
Job ID: 680-217710-1
Method
Method Description
Protocol
1664E
HEM and SGT-HEM
1664E
2540D-2015
Total Suspended Solids (Dried at 103-105°C)
SM
5220D-2011
Chemical Oxygen Demand
SM
1664E
HEM and SGT-HEM (Aqueous)
16648
Protocol References:
1664B = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurotins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
Laboratory
TAL SAV
TAL SAV
TAL SAV
TAL SAV
Eurof[ns Savannah
Page 10 of 12 7/18/2022
Address
Chain of Custody Record
Regulatory Program: ❑Dw ZNPDES ❑RMA ❑Odter
585062 O urofins
Environment Testing
TestAmerica
TAL-92to
Client Contact
Project Manager.
Site Contact:
Date:
COC No
Company Name 6
Tel/Email:
Lab Contact:
Carrier.
of COCs
Address q fS I ti., TZ-Act
Analysis Turnaround Time
Z
„
E
W
w
=
U.
2
'C
a
rt
[r/j'
p
IJ
ri
y�
9 '
:t
r
�
_..N
V►
t
Sampler
CdylState2ip a:( G
❑ CALENDAR DAYS WOWNG DAYS
For Lab Use Only.
Walk-in Client:
Lab Sampling
Phone ^a— 2s —2-2 g I
TAT if dbferent from Below
❑ 2 weeks
❑ 1 week
❑ 2 days
❑ 1 day
Fax.
Project Name S t.aes _ —, �,.�
Site rf
Job J SDO NO
P O #
Sample Identification
Sample
Data
Sample
Time
Sample
(Type
c G-b)
Matrix
trof
Cont
Sample Specific Notes
,_.LT13—SPo!
Y
4<1
I.
680-217710 Chain of Custody
L
Preservation Used: i=Ice, 2=HCI, 3=H28 k 4--HNO3;
S=NaOH;6=Other
1
11
Possible Hazard Identification:
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the
Comments Section if the lab is to dispose of the; sample
Sample Disposal (A fee may be assessed rf samples are retalne
❑ P:etum to Cient ❑ Disposal by Lab ❑ kd*e for
d longer than 1 month)
MWft
❑ Pion -Hazard ❑ Rammable ❑ Skin Udtint ❑ PobOn a ❑ unknown
Special InstructionslOC Requirements & Comments:
Custody Seals Intact: ❑ Yes ❑ No
Custody Seal No ICoolerTemp (C) O s rr d
erm ID No
Relinquished by
Company
�vn.
DateTme
rocZ�fu- to Is,vt
Reoeiv b
Company
Dat ime
as as o
Relinquished b .( ��
Company
at a
Recery by-
Compan�
Date , t
1 k/
Relinquished by
Company
D e
Received in Laboratory bj
Company
DateM
N
Login Sample Receipt Checklist
Client: ERM-West Job Number: 680-217710-1
Login Number: 217710
List Number: 1
Creator: Padayao, Abigail
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection dateltimes are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, ind. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
True
<6mm (114").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Eurofins Savannah
Page 12 of 12 7/18/2022
Sample Summary
Client: ERM-West
ProjectlSite: Storm Water - Amazon Warehouses DLT8
Job ID: 680-217710-1
Lab Sample ID Client Sample ID Matrix Collected Received Lt
680-217710-1 DLT8_Sample Point 01_20220629 Water 06129/22 09:07 07/01/22 11:00
Page 3 of42 Eurofins Sa7i&Oh% 2
Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Job ID: 680-217710-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-217710-1
Comments
No additional comments.
Job ID: 680-217710-1
Receipt
The sample was received on 7/1/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 2.10 C.
General Chemistry
No analytical or quality issues were noted, other than those described in the Definitions/Glossary page.
h��(p�1,�
d1.?�l
Eurofins Savannah
Page 4 of 12 7/18/2022
Client Sample Results
Client: ERM-West
Project/Site. Storm Water - Amazon Warehouses DLT8
Client Sample ID: DLT8_Sample_Point_01_20220629
Date Collected: 06/29/22 09;07
Date Received: 07/01/2211:00
[General' Chemistry
General
Result Qualifier RL
Oil & Grease (HEM) 1.3 J 2.8
Total Suspended Solids 7.6 2.5
LChemical Oxygen Demand 18 10
Job ID: 680-217710-1
Lab Sample ID: 680-217710-1
Matrix: Water
MDL
Unit
0 Prepared Analyzed
0.77
mg/L
07/12/22 08:59 07/12/22 13:33
2.5
mg1L
07/0512215:02
5.0
mg/L
07/16/22 11 :1 6
Dil Fac
1
1
1
Eurofins Savannah
Page 5 of 12
7118/2022
QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Method: 1664E - HEM and SGT-HEM
r
Lab Sample ID: MB 680-73020311-A
Matrix: Water
Analysis Batch: 730293
MB MB
Job ID: 680-217710-1
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 730203
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
LOil & Grease (HEM) <1.4 5.0 1.4 mg -IL 07112/22 08:59 07/12/22 13:33 1
FLab Sample ID: LCS 680-73020312-A Client Sample ID: Lab Control Sample
Matrix: Water Prep Type. TotaiiNA
Analysis Batch: 730293 Prep Batch: 730203
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit D %Rec Limits
LOil & Grease (HEM) 40.0 36.40 mgIL 91 78 - 114
Method: 254OD-2015 - Total Suspended Solids (Dried at 103-105°C) _
FLab Sample ID: MB 680-72913611 Client Sample ID: Method Blank
Matrix: Water Prep Type: TotalINA
Analysis Batch: 729136
MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
L-Total Suspended Solids <2.5 2.5 2.5 mg/L 07/05/22 15:02 1
i
Lab Sample ID: LCS 680-72913612 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total]NA
j Analysis Batch: 729136
Spike LCS LCS %Rec
i Analyte Added Result Qualifier Unit D %Rec Limits
Total Suspended Solids 951 908 mglL 95 80 - 120
FLab Sample ID: LCSD 680-729136/3 Client Sample ID: Lab Control Sample Dup
19114t11x: 'A'ater P c p Type: Tata!,'N'A
Analysis Batch: 729136
Spike LCSD LCSD %Rec RPD
i Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit
Total Suspended Solids 951 932 mg/L 98 $D 120 3 25
Method: 5220D-2011 - Chemical Oxygen Demand
LLab Sample ID: MB 680-731009/3 Client Sample ID: Method Blank
Matrix: Water Prep Type: Total/NA
Analysis Batch: 731009
1 MB MB
Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac
LChemical Oxygen Demand <5.0 10 5.0 mg/L 07/16/22 11:16 1
Lab Sample ID: LCS 680-73100914
Matrix: Water
Analysis Batch: 731009
Spike
Analyte Added
Chemical Oxygen Demand 50.0
Client Sample ID: Lab Control San-, pie
Prep Type: Total/NA
LCS LCS
Result Qualifier Unit
45.9 mg/L
%Rec
D %Rec Limits
92 90-110
Eurofins Savannah
Page 6 of 12 7/18/2022
QC Association Summary
Client: ERM-West Job ID: 680-217710-1
Project/Site: Storm Water - Amazon Warehouses DLT8
General Chemist
Analysis Batch: 729136
F Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLTB_Sample _Point_01_20220629
TotalINA
Water
2540D-2015
MB 680-729136/1
Method Blank
Total/NA
Water
254OD-2015
LCS 680-72913612
Lab Control Sample
Total/NA
Water
254OD-2015
LCSD 680-72913613
Lab Control Sample Dup
TotalINA
Water
254OD-2015
Prep Batch: 730203
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLTB_Sarnple_Point_01_20220629
TotaI1NA
Water
1664B
MB 680-730203/1-A
Method Blank
Total/NA
Water
1664B
LCS 680-73020312-A
Lab Control Sample
Total/NA
Water
1664E
Analysis Batch: 730293
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLT8_Samplo_Point_01_20220629
Total/NA
Water
1664B
730203
MB 680-730203/1-A
Method Blank
Total/NA
Water
1664B
730203
LCS 660-73020312-A
Lab Control Sample
Total/NA
Water
1664E
730203
Analysis Batch: 731009
r
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217710-1
DLT8 Sample_Point_01_20220629
Total/NA
Water
5220D-2011
MB 680-731009/3
Method Blank
Total/NA
Water
522OD-2011
LLCS 680-731009/4
Lab Control Sample
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 7 of 12 7/18/2022
Lab Chronicle
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DLT8
Client Sample ID: DLT8_Sample_Point_01_20220629
Date Collected: 06/29/22 09:07
Date Received: 07101122 11:00
r
Batch Batch
Dil Initial
Prep Type Type Method
stun Factor Amount
Total/NA Prep 1664B
906 mL
Total/NA Analysis 1664B
1
Instrument ID: NoEquip
Total/NA Analysis 254OD-2015
1 1000 mL
Instrument ID: NOEQUIP
Jab ID: 680-217710-1
Lab Sample ID: 680-217710-1
Matrix: Water
Final Batch Prepared
Amount Number orAnaiyzed Analyst Lab
500 mL 730203 07112f22 08:59 YR TAL SAV
730293 07112/22 13:33 YR TAL SAV
1000 mL 729136 07/05/22 15:02 PG TAL SAV
Total/NA Analysis 5220D-2011 1 2 mL 2 mL 731009 07/16/22 11:16 ALG TAL SAV
Instrument ID: SPC7
Laboratory References;
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
Page 8 of 12
Eurofins Savannah
7/18/2022
13
Accreditation/Certification Summary
Client: ERM-West Job ID: 680-217710-1
Project/Site: Storm Water - Amazon Warehouses DLT8
Laboratory: Eurofins Savannah
The accreditations/certifications listed below are applicable to this report.
Authority Program Identification Number Expiration Date
LNorth Carolina (WWISW) State 269 12-31-22
Eurofins Savannah
Page 9 of 12 7/18/2022
Method Summary
Client: ERM-West Job ID: 680-217710-1
Project/Site: Storm Water - Amazon Warehouses XT8
Method Method Description Protocol Laboratory
1664E HEM and SGT-HEM 1664B TAL SAV
254OD-2015 Total Suspended Solids (Dried at 103-105'C) SM TAL SAV
522OD-2011 Chemical Oxygen Demand SM TAL SAV
1664E HEM and SGT-HEM (Aqueous) 1664B TAL SAV
Protocol References:
1664E = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurotins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858
Eurofins Savannah
Page 10 of 12 7/18/2022
Address
Chain of Custody Record
Regulatory Program: ❑Dw IrJNPDES ❑RCRA ❑other
585062 tiff urofins
Environment Testing
TestAmerica
TAL-CIO
Client Contact
Project Manager.
Site Contact:
Date:
COC No
Company Name W',a it
TeUEmail:
Lab Contact:
Carrier.
of COCS
Address qatV
Analysis Turnaround Time
z
y
o
0
U=
z
o
0
w
2
€
a°
/Z
i�
I
D
N
N
d
�r
Z
r
3
Vt
i
D
H
Sampler
CityiStateMp
❑ cALENDAR oAYs ❑ WORKING DAYS
For Lab Use Only.
Walk-in Client:
Lab Sampling
Phone 30— Z$q —7-2 4 t
TAT if dttremitt from Below
❑ 2 heels
❑ I week
❑ 2 days
❑ I day
Fax
Project Name LJr�4es _ p v►.� w
Site t �('
Job I SDG No
P O #
Sample identification
Sample
Data
Sample
Time
Sample
(Type
(;=Gmb)P,
Matrix
o of
Cool
Sample Specific Notes
LAY$ - Sfla 1 2g3uKt Z�z2..
4.►t�z
9
Sc
r
680-217710 Chain of Custody
Preservation Used: 4-1taB, 2= HCI; 3= H
S=NaOH; G=
Other
Possible Hazard Identifcation:
Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the
Comments Section if the lab is to dispose of the; sample
Sample Disposal (A fee may be assessed d samples are retain
❑ Return to C lent ❑ Disposal by Lab ❑ Ardtive for
longer than 1 month)
Months
❑ Non -Hazard ❑ Rammable ❑ Skin Irritant ❑ Poison a ❑ Unknown
Special InstructionsIOC Requirements & Comments:
Custody Seals Intact: ❑ yes ❑ No
Custody Seal No Coo er emp (Cj orr'd
Tfierm 10 No
Relinquished by %
J to N 5 z e-
Company
DateTme
�?rzW2L•,o /S
Rece b
V
kk
Company
D
me ,r•�
c a V
Relinquished b .' "Aj
Company
*De
Rece by
Compar>
Da i 1 t
t
elmquished by
Company
Received in Laboratory bA
Company
DatelTi
Login Sample Receipt Checklist
Client: ERM-West Job Number: 680-217710-1
Login Number: 217710
List Number: 1
Creator: Padayao, Abigail
Question
List Source: Eurofins Savannah
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
True
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspac a have no headspace or bubble is
True
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
M ,rZj,-'
an
Eurofins Savannah
Page 12 of 12 7/18/2022