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HomeMy WebLinkAboutNCG060423_2022 DMR_20220729NCDEQ Division of Energy, Mineral and Land Resources Storitiwater Discharge Monitor rig Report (DPAR) Forth for NCU-000000 Food and Kindred Click here for instructions Complete, sign, scan and submit the DMR via the Stormvrater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No. NCG060423 Person Collecting Samples: John Speed Facility Name: Amazon.com Services LLC - DLT8 Laboratory Name: Eurofins Test America Savannah Facility County: Mecklenburg Laboratory Cert. No.:269 Discharge during this period: ❑ Yes ❑✓ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes El No If so, which Tier (I, II, or ill)? A copy of this DMR has been uploaded electronically via stps://edocs.cieg.nc.goy/Forms/SW-DMR 0 Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in 4Red) Parameter Code Parameter Outfall 001 Outfall Outfall Outfall O utfa II N/A Receiving Stream Class C N/A Date Sample Collected MM/DDIWYY 06/29/2022 46529 24-Hour Rainfall in inches 01 C0530 TSS in mg/L f100 or 50*) 7.6 pH in standard units (6.0— 9.0 FW, 00400 6.3-3.5SL.') 5.61 Fecal Coliform per 100 ml of 31616 freshwater (if required) I_000) N/A Enterococci per 100 ml of saltwater 61211 (if required) (500) N/A Chemical Oxygen Demand in mg/L 00340 18 Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A 00552 Non -Polar Oil & Grease in mg/L (15) 1.3 " Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 nI,/!. rtw (Freshwater) SW (saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted i to thg bes of my knpFvledge a d belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false info m dtj incl ing o sibility o fines�a d imprisonment for knowing violations." Signa#jle of Permittee o elegated Authorized Individual Date mcdMlin@amazon.com (404) 590-7247 Email Address Phone Number urofins Environment Testing America ANALYTICAL REPUORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory Job ID: 680-217710-1 Client Project/Site, Storm Water - Amazon Warehouses DLT8 For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 711812022 9:12.05 AM Roxanne Cisneros, Senior Project Manager (615)301-5761 roxanne.cisneros(Cr et.eUfOfinSU5.COrn The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNl requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent at a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. Definitions/Glossary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Qualifiers General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value. Glossary _ Abbreviation These commonly used abbreviations may or may not be present in this report. a Listed under the " D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoDIDOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample DLC Decision Level Concentration (Radiochemis(ry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoDIDOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative I Absent POS Positive 1 Present PQL Practical Quantitation Limit PRES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-217710-1 -- - Eurofins Savannah Page 2 of 12 7/18/2022 Sample Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Lab Sample ID Client Sample ID Matrix Collected Received 680-217710-1 DLT8_Sampie_Point 01_20220629 Water 06129l22 09:07 07/01/22 11:00 Job ID: 680-217710-1 Page 3 of 12 Eurofins Sai ANW2 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 .fob ID: 680-217710-1 Laboratory: Eurofins Savannah Narrative Job ID: 680-217710-1 Ed Job Narrative 680-217710-1 Comments No additional comments. Receipt The sample was received on 7/1/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 2.1 ° C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. Eurofins Savannah Page 4 of 12 7/18/2022 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Client Sample ID: DLT8_Sample_Point_01_20220629 Date Collected: 06/29/22 09:07 Date Received: 07/01/22 11:00 General Chemistry Analyte Result Qualifier RL MDL Unit Oil 8 Grease (HEM) 1.3 J 2.8 0.77 mgil Total Suspended Solids 7.6 2.5 2.5 mg/L Chemical Oxygen Demand 18 10 5.0 mg/L Job ID: 680-217710-1 Lab Sample ID: 680-217710-1 Matrix: Water D Prepared Analyzed Dil Fac 07/12/22 08:59 07/12/22 13:33 1 07/05/22 15:02 1 07/16/22 11:16 1 Eurofins Savannah Page 5 of 12 7/18/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Method: 1664E - HEM and SGT-HEM r Lab Sample ID: MB 680-73020311-A Matrix: Water Analysis Batch: 730293 Jab ID: 680-217710-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 730203 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Oil & Grease (HEM) - <1.4 5.0 1.4 mg/L 07/12/22 08:59 07/12/22 13:33 1 FLab Sample ID: LCS 680-73020312-A Client Sample 1D: Lab Control Sample Matrix: Water Prep —type: TotaiiNA Analysis Batch: 730293 Prep Batch: 730203 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits I Oil & Grease (HEM) 40.0 36.40 mg/L v 91 78- 114 Method. 254OD-2015 - Total Suspended Solids (Dried at 103-105°C) [Lab Sample ID: MB 680-72913611 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 729136 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Suspended Solids <2.5 2.5 2.5 mglL 07/05/22 15:02 1 Lab Sample ID: LCS 680-729136/2 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total/NA Analysis Batch: 729136 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 908 mg/L 95 80-120 F Lab Sample ID: LCSD 680-72913613 Client Sample ID: Lab Control Sample Dup Matrix. •iIutcr Prop yrc. Iv alli�ra Analysis Batch: 729136 Spike LCSD LCSD %Rec RPD Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit LTotal Suspended Solids 951 932 mglL 98 80-120 3 25 Method: 5220D-2011 - Chemical Oxygen Demand Lab Sample ID: MB 680-73100913 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 731009 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac LChemical Oxygen Demand <5.0 10 5.0 mg1L 07/10/22 11:16 1 F-Lab Sample ID: LCS 680-7 3100914 Client Sample ID: Lab Control Saiiipie Matrix: Water Prep Type: Total/NA Analysis Batch: 731009 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 60.0 45.9 mg1L 92 90 -110 Eurofins Savannah Page 6 of 12 7/18/2022 QC Association Summary Client: ERM-West Job ID: 680-217710-1 Project/Site: Storm Water - Amazon Warehouses DLT8 General Chemistry Analysis Batch: 729136 I Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8_Sample_Point_01_20220629 Total/NA Water 254OD-2015 MB 680-729136tl Method Blank TotalINA Water 2540D-2015 LCS 680-729136/2 Lab Control Sample Total1NA Water 2540D-2015 LCSD 680-72913613 Lab Control Sample Dup Total/NA Water 25400-2015 Prep Batch: 730203 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8_Sample_Point_01_20220629 Total/NA Water 1664E i MB 680-730203/1-A Method Blank TotallNA Water 1664B LCS 680-73020312-A Lab Control Sample Total/NA Water 1664B Analysis Batch: 730293 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8_ Sample_Point_01_20220629 Total/NA Water 1664E 73D203 MB 680-73020311-A Method Blank TotaVNA Water 16646 730203 V LCS 680-730203/2-A Lab Control Sample Total1NA Water 1664B 730203 Analysis Batch: 731009 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8_Sample_Point_01 20220629 Total/NA Water 5220D-2011 MB 680-731009/3 Method Blank Total/NA Water 5220D-2011 LCS 680-73100914 Lab Control Sample Total/NA Water 5220D-2011 Eurofins Savannah Page 7 of 12 7/18/2022 Lab Chronicle Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Client Sample ID: DLT8_Sample_Poinf_01_20220629 Date Collected: 06129122 09:07 Date Received: 07101122 11:00 Batch Batch oil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 906 mL Total/NA Analysis 16646 1 instrument ID: NoEquip Total/NA Analysis 254OD-2015 1 1000 mL Instrument ID: NOEQUIP Total/NA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 Job ID: 680-217710-1 Lab Sample ID: 680-217710-1 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 730203 07l12122 08:59 YR TAL SAV 730293 07/12/22 13:33 YR TAL SAV 1000 mL 729136 07/05/22 15:02 PG TAL SAV 2 mL 731009 07/16/22 11:16 ALG TAL SAV 13 Laboratory References: TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 8 of 12 7/18/2022 Accreditation[Certification Summary Client: ERM-West Job ID: 680-217710-1 Project/Site: Storm Water - Amazon Warehouses ❑LT8 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date North Carolina (WWlSW) Stale 269 12-31-22 VM f Eurofins Savannah Page 9 of 12 7/18/2022 Method Summary Client: ERM-West ProjectlSite: Storm Water - Amazon Warehouses DLTB Job ID: 680-217710-1 Method Method Description Protocol 1664E HEM and SGT-HEM 1664E 2540D-2015 Total Suspended Solids (Dried at 103-105°C) SM 5220D-2011 Chemical Oxygen Demand SM 1664E HEM and SGT-HEM (Aqueous) 16648 Protocol References: 1664B = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurotins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Laboratory TAL SAV TAL SAV TAL SAV TAL SAV Eurof[ns Savannah Page 10 of 12 7/18/2022 Address Chain of Custody Record Regulatory Program: ❑Dw ZNPDES ❑RMA ❑Odter 585062 O urofins Environment Testing TestAmerica TAL-92to Client Contact Project Manager. Site Contact: Date: COC No Company Name 6 Tel/Email: Lab Contact: Carrier. of COCs Address q fS I ti., TZ-Act Analysis Turnaround Time Z „ E W w = U. 2 'C a rt [r/j' p IJ ri y� 9 ' :t r � _..N V► t Sampler CdylState2ip a:( G ❑ CALENDAR DAYS WOWNG DAYS For Lab Use Only. Walk-in Client: Lab Sampling Phone ^a— 2s —2-2 g I TAT if dbferent from Below ❑ 2 weeks ❑ 1 week ❑ 2 days ❑ 1 day Fax. Project Name S t.aes _ —, �,.� Site rf Job J SDO NO P O # Sample Identification Sample Data Sample Time Sample (Type c G-b) Matrix trof Cont Sample Specific Notes ,_.LT13—SPo! Y 4<1 I. 680-217710 Chain of Custody L Preservation Used: i=Ice, 2=HCI, 3=H28 k 4--HNO3; S=NaOH;6=Other 1 11 Possible Hazard Identification: Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the; sample Sample Disposal (A fee may be assessed rf samples are retalne ❑ P:etum to Cient ❑ Disposal by Lab ❑ kd*e for d longer than 1 month) MWft ❑ Pion -Hazard ❑ Rammable ❑ Skin Udtint ❑ PobOn a ❑ unknown Special InstructionslOC Requirements & Comments: Custody Seals Intact: ❑ Yes ❑ No Custody Seal No ICoolerTemp (C) O s rr d erm ID No Relinquished by Company �vn. DateTme rocZ�fu- to Is,vt Reoeiv b Company Dat ime as as o Relinquished b .( �� Company at a Recery by- Compan� Date , t 1 k/ Relinquished by Company D e Received in Laboratory bj Company DateM N Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217710-1 Login Number: 217710 List Number: 1 Creator: Padayao, Abigail Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection dateltimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, ind. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is True <6mm (114"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A Eurofins Savannah Page 12 of 12 7/18/2022 Sample Summary Client: ERM-West ProjectlSite: Storm Water - Amazon Warehouses DLT8 Job ID: 680-217710-1 Lab Sample ID Client Sample ID Matrix Collected Received Lt 680-217710-1 DLT8_Sample Point 01_20220629 Water 06129/22 09:07 07/01/22 11:00 Page 3 of42 Eurofins Sa7i&Oh% 2 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Job ID: 680-217710-1 Laboratory: Eurofins Savannah Narrative Job Narrative 680-217710-1 Comments No additional comments. Job ID: 680-217710-1 Receipt The sample was received on 7/1/2022 11:00 AM. Unless otherwise noted below, the sample arrived in good condition, and where required, properly preserved and on ice. The temperature of the cooler at receipt was 2.10 C. General Chemistry No analytical or quality issues were noted, other than those described in the Definitions/Glossary page. h��(p�1,� d1.?�l Eurofins Savannah Page 4 of 12 7/18/2022 Client Sample Results Client: ERM-West Project/Site. Storm Water - Amazon Warehouses DLT8 Client Sample ID: DLT8_Sample_Point_01_20220629 Date Collected: 06/29/22 09;07 Date Received: 07/01/2211:00 [General' Chemistry General Result Qualifier RL Oil & Grease (HEM) 1.3 J 2.8 Total Suspended Solids 7.6 2.5 LChemical Oxygen Demand 18 10 Job ID: 680-217710-1 Lab Sample ID: 680-217710-1 Matrix: Water MDL Unit 0 Prepared Analyzed 0.77 mg/L 07/12/22 08:59 07/12/22 13:33 2.5 mg1L 07/0512215:02 5.0 mg/L 07/16/22 11 :1 6 Dil Fac 1 1 1 Eurofins Savannah Page 5 of 12 7118/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Method: 1664E - HEM and SGT-HEM r Lab Sample ID: MB 680-73020311-A Matrix: Water Analysis Batch: 730293 MB MB Job ID: 680-217710-1 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 730203 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac LOil & Grease (HEM) <1.4 5.0 1.4 mg -IL 07112/22 08:59 07/12/22 13:33 1 FLab Sample ID: LCS 680-73020312-A Client Sample ID: Lab Control Sample Matrix: Water Prep Type. TotaiiNA Analysis Batch: 730293 Prep Batch: 730203 Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits LOil & Grease (HEM) 40.0 36.40 mgIL 91 78 - 114 Method: 254OD-2015 - Total Suspended Solids (Dried at 103-105°C) _ FLab Sample ID: MB 680-72913611 Client Sample ID: Method Blank Matrix: Water Prep Type: TotalINA Analysis Batch: 729136 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac L-Total Suspended Solids <2.5 2.5 2.5 mg/L 07/05/22 15:02 1 i Lab Sample ID: LCS 680-72913612 Client Sample ID: Lab Control Sample Matrix: Water Prep Type: Total]NA j Analysis Batch: 729136 Spike LCS LCS %Rec i Analyte Added Result Qualifier Unit D %Rec Limits Total Suspended Solids 951 908 mglL 95 80 - 120 FLab Sample ID: LCSD 680-729136/3 Client Sample ID: Lab Control Sample Dup 19114t11x: 'A'ater P c p Type: Tata!,'N'A Analysis Batch: 729136 Spike LCSD LCSD %Rec RPD i Analyte Added Result Qualifier Unit D %Rec Limits RPD Limit Total Suspended Solids 951 932 mg/L 98 $D 120 3 25 Method: 5220D-2011 - Chemical Oxygen Demand LLab Sample ID: MB 680-731009/3 Client Sample ID: Method Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 731009 1 MB MB Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac LChemical Oxygen Demand <5.0 10 5.0 mg/L 07/16/22 11:16 1 Lab Sample ID: LCS 680-73100914 Matrix: Water Analysis Batch: 731009 Spike Analyte Added Chemical Oxygen Demand 50.0 Client Sample ID: Lab Control San-, pie Prep Type: Total/NA LCS LCS Result Qualifier Unit 45.9 mg/L %Rec D %Rec Limits 92 90-110 Eurofins Savannah Page 6 of 12 7/18/2022 QC Association Summary Client: ERM-West Job ID: 680-217710-1 Project/Site: Storm Water - Amazon Warehouses DLT8 General Chemist Analysis Batch: 729136 F Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLTB_Sample _Point_01_20220629 TotalINA Water 2540D-2015 MB 680-729136/1 Method Blank Total/NA Water 254OD-2015 LCS 680-72913612 Lab Control Sample Total/NA Water 254OD-2015 LCSD 680-72913613 Lab Control Sample Dup TotalINA Water 254OD-2015 Prep Batch: 730203 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLTB_Sarnple_Point_01_20220629 TotaI1NA Water 1664B MB 680-730203/1-A Method Blank Total/NA Water 1664B LCS 680-73020312-A Lab Control Sample Total/NA Water 1664E Analysis Batch: 730293 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8_Samplo_Point_01_20220629 Total/NA Water 1664B 730203 MB 680-730203/1-A Method Blank Total/NA Water 1664B 730203 LCS 660-73020312-A Lab Control Sample Total/NA Water 1664E 730203 Analysis Batch: 731009 r Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217710-1 DLT8 Sample_Point_01_20220629 Total/NA Water 5220D-2011 MB 680-731009/3 Method Blank Total/NA Water 522OD-2011 LLCS 680-731009/4 Lab Control Sample Total/NA Water 5220D-2011 Eurofins Savannah Page 7 of 12 7/18/2022 Lab Chronicle Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT8 Client Sample ID: DLT8_Sample_Point_01_20220629 Date Collected: 06/29/22 09:07 Date Received: 07101122 11:00 r Batch Batch Dil Initial Prep Type Type Method stun Factor Amount Total/NA Prep 1664B 906 mL Total/NA Analysis 1664B 1 Instrument ID: NoEquip Total/NA Analysis 254OD-2015 1 1000 mL Instrument ID: NOEQUIP Jab ID: 680-217710-1 Lab Sample ID: 680-217710-1 Matrix: Water Final Batch Prepared Amount Number orAnaiyzed Analyst Lab 500 mL 730203 07112f22 08:59 YR TAL SAV 730293 07112/22 13:33 YR TAL SAV 1000 mL 729136 07/05/22 15:02 PG TAL SAV Total/NA Analysis 5220D-2011 1 2 mL 2 mL 731009 07/16/22 11:16 ALG TAL SAV Instrument ID: SPC7 Laboratory References; TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Page 8 of 12 Eurofins Savannah 7/18/2022 13 Accreditation/Certification Summary Client: ERM-West Job ID: 680-217710-1 Project/Site: Storm Water - Amazon Warehouses DLT8 Laboratory: Eurofins Savannah The accreditations/certifications listed below are applicable to this report. Authority Program Identification Number Expiration Date LNorth Carolina (WWISW) State 269 12-31-22 Eurofins Savannah Page 9 of 12 7/18/2022 Method Summary Client: ERM-West Job ID: 680-217710-1 Project/Site: Storm Water - Amazon Warehouses XT8 Method Method Description Protocol Laboratory 1664E HEM and SGT-HEM 1664B TAL SAV 254OD-2015 Total Suspended Solids (Dried at 103-105'C) SM TAL SAV 522OD-2011 Chemical Oxygen Demand SM TAL SAV 1664E HEM and SGT-HEM (Aqueous) 1664B TAL SAV Protocol References: 1664E = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurotins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Eurofins Savannah Page 10 of 12 7/18/2022 Address Chain of Custody Record Regulatory Program: ❑Dw IrJNPDES ❑RCRA ❑other 585062 tiff urofins Environment Testing TestAmerica TAL-CIO Client Contact Project Manager. Site Contact: Date: COC No Company Name W',a it TeUEmail: Lab Contact: Carrier. of COCS Address qatV Analysis Turnaround Time z y o 0 U= z o 0 w 2 € a° /Z i� I D N N d �r Z r 3 Vt i D H Sampler CityiStateMp ❑ cALENDAR oAYs ❑ WORKING DAYS For Lab Use Only. Walk-in Client: Lab Sampling Phone 30— Z$q —7-2 4 t TAT if dttremitt from Below ❑ 2 heels ❑ I week ❑ 2 days ❑ I day Fax Project Name LJr�4es _ p v►.� w Site t �(' Job I SDG No P O # Sample identification Sample Data Sample Time Sample (Type (;=Gmb)P, Matrix o of Cool Sample Specific Notes LAY$ - Sfla 1 2g3uKt Z�z2.. 4.►t�z 9 Sc r 680-217710 Chain of Custody Preservation Used: 4-1taB, 2= HCI; 3= H S=NaOH; G= Other Possible Hazard Identifcation: Are any samples from a listed EPA Hazardous Waste? Please List any EPA Waste Codes for the sample in the Comments Section if the lab is to dispose of the; sample Sample Disposal (A fee may be assessed d samples are retain ❑ Return to C lent ❑ Disposal by Lab ❑ Ardtive for longer than 1 month) Months ❑ Non -Hazard ❑ Rammable ❑ Skin Irritant ❑ Poison a ❑ Unknown Special InstructionsIOC Requirements & Comments: Custody Seals Intact: ❑ yes ❑ No Custody Seal No Coo er emp (Cj orr'd Tfierm 10 No Relinquished by % J to N 5 z e- Company DateTme �?rzW2L•,o /S Rece b V kk Company D me ,r•� c a V Relinquished b .' "Aj Company *De Rece by Compar> Da i 1 t t elmquished by Company Received in Laboratory bA Company DatelTi Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217710-1 Login Number: 217710 List Number: 1 Creator: Padayao, Abigail Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. True There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspac a have no headspace or bubble is True <6mm (1/4"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. N/A M ,rZj,-' an Eurofins Savannah Page 12 of 12 7/18/2022