NCG060408_2022 DMR_20220729

NCDEQ Division of Energy, Mineral and Land Resources
Stormwater Discharge Monitoring Report (DMR) Form for NCG060000
Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG060408
Person Collecting Samples: Linda Cortes
Facility Name: Amazon.com Services LLC - DRT9
Laboratory Name: Eurofins Test America Savannah
Facility County: Wake
Laboratory Cert. No.: 269
Discharge during this period: ❑J Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ❑r No
If so, which Tier (I, II, or III)?
A copy of this DMR has been uploaded electronically via https://edocs.deq.nc.gov/Forms/SW-DMR❑ Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities — Benchmarks in (Red)
Parameter
Parameter
Outfall001
Outfall002
Outfall
Outfall
Outfall
Code
N/A
Receiving Stream Class
C;NSW
C;NSW
N/A
Date Sample Collected MM/DD/YYYY
6/16/2022
6/16/2022
46529
24-Hour Rainfall in inches
0.75
0.75
C0530
TSS in mg/L (100 or 50•)
10
12
pH in standard units (6.0-9.0 FW,
00400
6.8-8.5SW)
7.87
7.97
Fecal Coliform per 100 ml of
31616
freshwater (if required) (1000)
N/ A
N/ A
Enterococci per 100 ml of saltwater
61211
(if required) (500)
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
(120)
52
73
Additional parameters for outfalls in drainage areas that use >S5 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
N/A
00552
Non -Polar Oil & Grease in mg/L (15)
<0.80
1.5
Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA)
have a benchmark TS5 limit of 50 mg/L. Ail other water classifications have a benchmark of I00 rng/l.
FIN (Freshwater) SiV (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitted,is, to hp best -my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false inf r at' n, incj�u ng the pos lity fines an imprisonment for knowing violations."
Sig ture of Permittee or Delegate Authorized Individual Da e
[e-mail] [phone]
Email Address Phone Number

urofins
F.
America
ANALYTICAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-217154-1
Client Project/Site: Storm Water - Amazon Warehouses DRT9
For.
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
R"a"L . Cistvcros
Authorized for release by:
6/29/2022 4:49:51 PM
Roxanne Cisneros, Senior Project Manager
[phone]
roxarine.cis [e-mail]
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNI
requirements for accredited parameters, exceptions are noted in this report. This
report may not be reproduced except in full, and with written approval from the
laboratory. For questions please contact the Project Manager at the e-mail address or
telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic
signature is intended to be the legally binding equivalent of a traditionally handwritten
signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
0

Definitions/Glossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Qualifiers
General Chemistry
Qualifier Qualifier Description
J Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation
a
%R
CFL
CFU
CNF
DER
Dil Fac
DL
DL, RA. RE, IN
DLC
EDL
LOD
LOQ
MCL
M DA
MDC
MDL
ML
MPN
MQL
NC
ND
NEG
POS
PQL
PRES
QC
RER
RL
RPD
TEF
TEQ
TNTC
These commonly used abbreviations may or may not be present in this report.
Listed under the "D" column to designate that the result is reported on a dry weight basis
Percent Recovery
Contains Free Liquid
Colony Forming Unit
Contains No Free Liquid
Duplicate Error Ratio (normalized absolute difference)
Dilution Factor
Detection Limit (DoDIDOE)
Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metaislanion analysis of the sample
Decision Level Concentration (Radiochemistry)
Estimated Detection Limit (Dioxin)
Limit of Detection (DoD/DOE)
Limit of Quanlitation (DoDIDOE)
EPA recommended "Maximum Contaminant Level'
Minimum Detectable Activity (Radiochemistry)
Minimum Detectable Concentration (Radiochemistry)
Method Detection Limit
Minimum Level (Dioxin)
Most Probable Number
Method Quantitabon Limit
Not Calculated
Not Detected at the reporting limit (or MDL or EDL if shown)
Negative 1 Absent
Positive ! Present
Practical Quantitation Limit
Presumptive
Quality Control
Relative Error Ratio (Radiochemistry)
Reporting Limit or Requested Limit (Radiochemistry)
Relative Percent Difference, a measure of the relative difference between two points
Toxicity Equivalent Factor (Dioxin)
Toxicity Equivalent Quotient (Dioxin)
Too Numerous To Count
Job ID: 680-217154-1
Eurofins Savannah
Page 2 of 13 6/29/2022

Sample Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Lab Sample ID Client Sample ID Matrix Collected Received
680-217154-1 DRT9_Sample Point_01_20220616 Water 06/16/22 18:40 06/18/22 09:45
680-217154-2 DRT9_Sample_Point_02_20220616 Water 06/16/22 18:50 06/18/22 09:45
Job ID: 680-217154-1
Page 3 of 13 Eurofins Spa NOW2

Case Narrative
Client: ERM-West Job ID: 680-217154-1
Project/Site: Storrs Water - Amazon Warehouses DRT9
Job ID: 680-217154-1Laboratory:Eurofins Savannah
Narrative
Job Narrative
680-217154-1
Comments
No additional comments.
Receipt
The samples were received on 6/18/2022 9:45 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 4.20 C.
General Chemistry
Methods 1664B: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicateisample duplicate
(MSIMSDIDUP) associated with preparation batch 680-727836,
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page.
Eurofins Savannah
Page 4 of 13 6/29/2022

Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Client Sample ID: DRT9_Sample_Point_01_20220616
Date Collected: 06/16/22 18:40
Date Received: 06/18/22 09:45
General Chemistry
Analyte Result Qualifier RL MDL Unit
SGT-HEM (TPH)
<0.80
2.9
0.80 mg/L
Total Suspended Solids
10
2.5
2.5 mglL
Chemical Oxygen Demand
52
10
5.0 mg/L
Client Sample ID: DRT9—Sample_Point_02_20220616
Date Collected: 06116/22 18:50
Date Received: 06/18/22 09:45
General Chemistry
Analyte
Result Qualifier
RL
MDL Unit
SGT-HEM (TPH)
1.5 J
2.6
0.74 mg/L
Total Suspended Solids
12
5.0
5.0 mglL
Chemical Oxygen Demand
73
10
5.0 mg/L
Job ID: 680-217154-1
Lab Sample ID: 680-217154-1
Matrix: Water
D Prepared Analyzed Dil Fac
06/27/22 09:06 06/27/22 11:32 1
08/22/22 11:13 1
06/29/22 12:04 1
Lab Sample ID: 680-217154-2
Matrix: Water
D Prepared Analyzed Dil Fac
06/27/22 09:06 06/27/22 11:32 1
06/22/22 11:13 1
06/29/22 12:04 1
Eurofins Savannah
Page 5 of 13 6/29/2022

QC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Method: 1664E - HEM and SGT-HEM
Lab Sample ID: MB 680-72783611-A
Matrix: Water
Analysis Batch: 727891
Analyte
SGT-HEM (TPH)
Lab Sample ID: LCS 680-72783612-A
Matrix: Water
Analysis Batch: 727891
Analyte
SGT-HEM (TPH)
Lab Sample ID: LCSD 680-72783613-A
Matrix: Water
Analysis Batch: 727891
I ne *751IK'eI-T$VJVAl6Sffl
Client Sample ID: Method Blank
Prep Type: Total/NA
Prep Batch: 727836
RL MDL Unit D Prepared Analyzed oil Fac
5.0 1.4 mglL 06/27/22 09:06 06/27/22 11:32 1
Client Sample ID: Lab Control Sample
Prep Type: TotalINA
Prep Batch: 727836
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
20, 0 15.80 mglL 79 64 -132
Client Sample ID: Lab Control Sample Dup
Prep Type: TotalINA
Prep Batch: 727836
Spike LCSD LCSD
Analyte Added Result Qualifier Unit
SGT-HEM (TPH) 20.0 16.40 mglL
Method: 254OD-2015 - Total Suspended Solids (Dried at 103-1060C)
Lab Sample ID: MB 680-72709711
Matrix: Water
Analysis Batch: 727097
Analyte
Total Suspended Solids
Lab Sample ID: LCS 680-727097/2
Matrix: Water
Analysis Batch: 727097
Analyte
Total Suspended Solids
Lab Sample ID: LCSD 680-72709713
Matrix: Water
Analysis Batch: 727097
Analyte
Total Suspended Solids
IVI B M B
Result oualifier
<1.4
IVIB MB
Result Qualifier
Q.5
%Rea RPD
D %Rec Limits RPD Limit
- — 82 64 -132 4 34
Client Sample ID: Method Blank
Prep Type: TotalINA
RL MDL Unit D Prepared Analyzed Dil Fac
2.5 2.5 mglL 06/2212211:13 1
Client Sample ID: Lab Control Sample
Prep Type: TotalINA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
951 814 mglL a6 80-12D
Client Sample ID: Lab Control Sample Dup
Prep Type: TotalINA
Spike
LCSD LCSD
%Rec
RPD
Added
Result Qualifier
Unit
D %Rec Limits
RPD Limit
951
804
mglL
85 80 -120
1 25
Method: 5220D-2011 - Chemical Oxygen Demand
Lab Sample ID: MB 680-728340/3
Matrix: Water
Analysis Batch: 728340
MB MB
Analyte Result Qualifier
Chemical Oxygen Demand <5.0
RL
10
Client Sample ID: Method Blank
Prep Type: Total/NA
MDL Unit D Prepared Analyzed Oil Fac
5.0 mglL 06129/2212:04 1
Eurofins Savannah
Page 6 of 13
6/29/2022

OC Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Job ID: 680-217154-1
Method: 5220D-2011 - Chemical Oxygen Demand (Continued)
i Lab Sample ID: LCS 680-72834014 Client Sample ID: Lab Control Sample
Matrix: Water Prep Type: Total/NA
Analysis Batch: 728340
Spike LCS LCS %Rec
Analyte Added Result Qualifier Unit n % Rec Limits
Chemical Oxygen Demand 50.0 48.9 mg/L 98 90-110
Eurofins Savannah
Page 7 of 13 6/29/2022

QC Association Summary
Client: ERM-West Job ID: 680-217154-1
Project/Site: Storm Water - Amazon Warehouses DRT9
General Chemist
Analysis Batch: 727097
Lab Sample ID
Client Sample I❑
Prep Type
Matrix
Method
Prep Batch
680-217154-1
DRT9_Sample_Point_01_20220616
Total/NA
Water
2540D-2015
680-217154-2
DRT9_Sample_Point_02_20220616
TotaUNA
Water
254OD-2015
MB 680-72709711
Method Blank
Total/NA
Water
254OD-2015
LCS 680-727097/2
Lab Control Sample
Total/NA
Water
254OD-2015
LCSD 680-727097/3
Lab Control Sample Dup
Total/NA
Water
2540D-2015
Prep Batch: 727836
Lair Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217154-1
DRT9_Sample_Point_01_20220616
TotaUNA
Water
1664B
680-217154-2
DRT9_Sample_Point_02_20220616
Total/NA
Water
1664B
MB 680-727836/1-A
Method Blank
Total/NA
Water
1664B
LCS 680-72783612-A
Lab Control Sample
TotalINA
Water
1664B
LCSD 680-72783613-A
Lab Control Sample Dup
Total/NA
Water
1664B
Analysis Batch: 727891
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-217154-1
DRT9_Sample_Point_01_20220616
TotalINA
Water
1664E
727836
680-217154-2
DRT9_Sample_Point_02_20220616
Total/NA
Water
1664B
727836
MB 6BO-727836/1-A
Method Blank
Total/NA
Water
1664B
727836
LCS 680-72783612-A
Lab Control Sample
Total/NA
Water
1664B
727836
LCSD 680-727836/3-A
Lab Control Sample Dup
TotalINA
Water
1664E
727836
Analysis Batch: 728340
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-217154-1
DRT9_Sample_Point_01_20220616
Total/NA
Water
5220D-2011
680-217154-2
DRT9_Sample_Point_02_20220616
Total/NA
Water
5220D-2011
MB 680-72834013
Method Blank
Total/NA
Water
5220D-2011
LCS 680-728340/4
Lab Control Sample
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 8 of 13 6/29/2022

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Client Sample ID: DRT9_Sample_Point_01_20220616
Date Collected: 06/16/22 18:40
Date Received: 06/18/22 09:45
Batch Batch
Dil Initial
Prep Type Type Method
Run Factor Amount
Total/NA Prep 1664B
876 mL
Tota11NA Analysis 16648
1
Instrument ID: NoEquip
Total/NA Analysis 254OD-2015
1 1000 mL
Instrument ID: NOEQUIP
Total/NA Analysis 5220D-2011
1 2 mL
Instrument ID: SPC7
Client Sample ID: DRT9_Sample_Point_02_20220616
Date Collected: 06/16/22 18:50
Date Received: 06/18122 09:45
Job ID: 680-217154-1
Lab Sample ID: 680-217154-1
Matrix: Water
Final Batch
Prepared
Amount Number
or Analyzed Analyst Lab
500 mL 727836
06127/22 09:06 JAS TAL SAV
727891
06/27/22 11:32 JAS TAL SAV
1000mL 727097 0612212211A3 PG
2 mL 728340 06/29/22 12:04 ALG
TAL SAV
TAL SAV •
Lab Sample ID: 680-217154-2
Matrix: Water
Batch Batch
Dil Initial
Final
Batch
Prepared
Prep Type
Type Method
Run Factor Amount
Amount
Number
or Analyzed
Analyst
Lab
Total/NA
Prep 16648
947 mL
500 mL
727836
06127/22 09:06
JAS
TAL SAV
Total/NA
Analysis 1664B
1
727891
06/27/22 11:32
JAS
TAL SAV
Instrument ID: NoEquip
Total/NA
Analysis 254OD-2015
1 500 mL
1000 mL
727097
06/22/22 11:13
PG
TAIL SAV
Instrument ID: NOEQUIP
Tolal/NA
Analysis 5220D-2011
1 2 mL
2 mL
728340
06/29/22 12:04
ALG
TAL SAV
Instrument ID: SPC7
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Page 9 of 13
Eurofins Savannah
6/29/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT9
Laboratory: Eurofins Savannah
The accreditationsloertifications listed below are applicable to this report.
CAutharity Program Identification Number
North Carolina (WW/SW) State 269
Job ID: 680-217154-1
Expiration Date
12-31-22
Eurofins Savannah
Page 10 of 13 6/29/2022

Method Summary
Client: ERM-West Job ID: 680-217154-1
Project/Site: Storm Water - Amazon Warehouses DRT9
Method Method Description Protocol Laboratory
1664E HEM and SGT-HEM 1664E TAL SAV
2540D-2015 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV
5220D-2011 Chemical Oxygen Demand SM TAL SAV
1664B HEM and SGT-HEM (Aqueous) 1664E TAL SAV
Protocol References:
1664E = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 11 of 13 6/29/2022

R
i
CO
tJ
O
N
tV
Eurofins Savannah
5102 LaRoche Avenue
Savannah GA 31404
Phone [phone] Fax:[phone]
Chain of Custody Record
tiz eurofins
Er cnre� r5. n�
'"en
Client Infottrlation
Sam r_ (�,� s�r/
ClJy+�
tab PM.
Cisneros Roxanne
Carrier Tracking No(s)
COG No:
240-93305-33339 1
Mient Contact:
Doug Wade
Phon
tq` �{Qo3—p ✓0�
E-Mail.
[e-mail]
Slate of Origm: t /.
lv(�
Page:
Page 1 of 1
company,
ERM-West
PWSID
Analysis Requested
Job #:
Address,
1920 Main Street Suite 300
Due Date Requested. ry, _}
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Preservation Codes
A HCl. M Hexane
e NaOH N None
C -Zn Acelale 0 AsNaO2
D Nitric Add P Na204S
E - NaHSO4 Q - Na2SO3
P Me OH R Na2S203
G Amchlor s H2SO4
H- Ascorbic Acid T TSP Dedeahydrate
I Ice LI- Acetone
-1 - DI Wale, V - MCAA
K EDTA W pH4-5
L EQA Z- olher(spedfy)
Other
City.
Irvine
TAT Requested (days)
�1%
State Zip.;.
CA, 92614
Compliance Project 4 Yes ❑ No
Phone.
443-012-0046(Tel
PO#:
Di
Email.
doug wade@erm corn
WO #:
Project Name
Storm Water• Amazon Warehouses
Site ,r1 /
Prejed#:
24024260
ssowb:
Sample Identification
Sample Date
Sample
Time
Sample
Type
10-w:awaL
G= rab)
Matrix
(w.—
BT.T:qu..-)
Special Instructions/Note
j
Preservation Code:
S
S
N
nl- ^ nu.
/1 U
yy
i� �i7i
�$-_l
Water
e}
io41 �i u`lQ �t17
�lQ �!fi
�1 ' t"3[�
Water
684-217t 5A Chain of Custody
Pos ible Hazard lden0ficatron
Non -Hazard © Flammabie Skin Irritant Poison 0 Unknown © Radiological
Sample Disposal (A fee may be assessed ifsamples are retained longer than 1 month)
= Retum To Client = Disposal By Lab © Archive For Months
Deliverable Requested I II II( N Other {specify)
Special Instf-uctiori Requirements
Empty Kit Relinquished by' Date. Time. Methcd of Siupment
Re4nquahed b
Daum : t r
Compa
Received by
Daternme: I
company
Relinquished by'
Dalelr'i e
Company
Received by
Daterr:me:
company
Relinquished by
OalerRme:
Company
Received by
DatefTme:
Company
Custody Seats Intact
A Yes A No
Custody Seal No
Cooi Temperature(s) °C and Other Remarks --
( 7 L
ver- uoluS12u-,I

Login Sample Receipt Checklist
Client: ERM-West
Login Number: 217154
List Number: 1
Creator: Sims, Robert D
Question Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
N/A
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
N/A
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
N/A
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
List Source: Eurofins Savannah
Eurofins Savannah
Page 13 of 13 6/29/2022