NCG060414_2022 DMR_20220729

NCDEQ Division of Energy, Mineral and Land Resources
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Food and Kindred
Click here for instructions
Complete, sign, scan and submit the DMR via the 5tormwater NPDES Permit Data Monitoring Report. {DMR) Upload form within
30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office.
Certificate of Coverage No. NCG060414
Person Collecting Samples: Duncan Quinn
Facility Name: Amazon.com Services LLC - DRT4
Laboratory Name: Eurofins Test America Savannah
Facility County: Henderson
Laboratory Cert. No.: 269
Discharge during this period: 2] Yes ❑ No (if no, skip to signature and date)
Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes ❑� No
If so, which Tier (I, II, or lli)?
A copy of this DMR has been uploaded electronically via https://edacs.deg.nc.gov/Forms/SW-DMR 0 Yes ❑ No
Date Uploaded:
Analytical Monitoring Requirements for Outfalls with Industrial Activities -- Benchmarks in (Red)
Parameter
Code
Parameter
Outfall002
outfall003
Outfall004
outfall005
Outfall
N/A
Receiving Stream Class
C
C
C
C
N/A
Date Sample Collected MM/DD/YYYY
4/5/2022
4/5/2022
4/5/2022
4/5/2022
46529
24-Hour Rainfall in inches
0.49
0.49
0.49
0.49
C0530
I TSS in mg/L (IODl ,r 5Ct=—
7.1
8.6
3.7
8.2
pH in standard units (6.0 — 9.0 FW,
00400
6.S-3.5SW)
6.71
6.73
6.9
6.67
Fecal Coliform per 100 ml of
31616
freshwater (if required) l+nnnl
N/A
N/A
N/A
N/A
Enterococci per 100 ml of saltwater
61211
(if required) 1,500;
N/A
N/A
N/A
N/A
Chemical Oxygen Demand in mg/L
00340
9.1
<5.0
11
13
Additional parameters for outfalls in drainage areas that use >55 gallons per month of new hydraulic oil on average
Estimated New Motor/Hydraulic Oil
NCOIL
Usage in gal/month
N/A
N/A
N/A
N/A
00552
Non -Polar Oil & Grease in mg/L (15)
<0.69
<0.72
0.73
<0.72
Outfatls to Outstanding Resource Waters (ORW), High QualityWaters (HQW), Trout Waters (Tr) and Primary NurseryAreas (PNA)
have a benchmark TSS limit of So mg/L. All other water classifications have a benchmark of 100 mg/L
RV (Freshwater) S' d (Saltwater)
Notes (optional):
"I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my
inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information
submitt s, he st of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting
false i4rik4ion, i cludin ossibilit o .fi d imprisonment for knowing violations."
Sig ture of Permitte or Delegated Authorized Individual Dfife
[e-mail] [phone]
Email Address Phone Number

urofins
11ar L aa
ANALYTiCAL REPORT
Eurofins Savannah
5102 LaRoche Avenue
Savannah, GA 31404
Tel: [phone]
Laboratory Job ID: 680-213653-1
Client Project/Site: Storm Water - Amazon Warehouses DRT4
For:
ERM-West
1920 Main Street
Suite 300
Irvine, California 92614
Attn: Doug J Wade
RnaAr .. 6"rns
Authorized for release by:
412012022 8:37:55 AM
Roxanne Cisneros, Senior Project Manager
[phone]
roxanne_cisneros(c-Det.eurofinsus.corn
The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNl requirements for
accredited parameters, exceptions are noted in this report. This report may not be reproduced
except in full, and with written approval from the laboratory. For questions please contact the
Project Manager at the e-mail address or telephone number listed on this page.
This report has been electronically signed and authorized by the signatory. Electronic signature is
intended to be the legally binding equivalent of a traditionally handwritten signature.
Results relate only to the items tested and the sample(s) as received by the laboratory.
0

Definitions/Glossary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Qualifiers
Veneral Chemistry
Qualifier Qualifier Description
J
Result is less than the RL but greater than or equal to the MDL and the concentration is an approximate value.
Glossary
Abbreviation These commonly used abbreviations may or may not be present in this report -
a Listed under the "D" column to designate that the result is reported on a dry weight basis
%R Percent Recovery
CFL Contains Free Liquid
CFU Colony Forming Unit
CNF Contains No Free Liquid
DER Duplicate Error Ratio (normalized absolute difference)
Dil Fac Dilution Factor
DL Detection Limit (DoDIDOE)
DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metals/anion analysis of the sample
DLC Decision Level Concentration (Radiochemistry)
EDL Estimated Detection Limit (Dioxin)
LOD Limit of Detection (DQDIDOE)
LOQ Limit of Quantitation (DoD/DOE)
MCL EPA recommended "Maximum Contaminant Level"
MDA Minimum Detectable Activity (Radiochemistry)
MDC Minimum Detectable Concentration (Radiochemistry)
MDL Method Detection Limit
ML Minimum Level (Dioxin)
MPN Most Probable Number
MQL Method Quantitation Limit
NC Not Calculated
ND Not Detected at the reporting limit (or MDL or EDL if shown)
NEG Negative 1 Absent
POS Positive / Present
PQL Practical Quantitation Limit
FIRES Presumptive
QC Quality Control
RER Relative Error Ratio (Radiochemistry)
RL Reporting Limit or Requested Limit (Radiochemistry)
RPD Relative Percent Difference, a measure of the relative difference between two points
TEF Toxicity Equivalent Factor (Dioxin)
TEQ Toxicity Equivalent Quotient (Dioxin)
TNTG Too Numerous To Count
Job ID: 680-213653-1
Eurofins Savannah
Page 2 of 14 4/20/2022

Sample Summary
Client: ERM-West
ProjectlSite: Storm Water - Amazon Warehouses DRT4
Lab Sample ID
Client Sample ID
680-213653-1
DRT4_Sample Point_01_20220405
680-213653-2
DRT4_Sampie_Point_02_20220405
680-213653-3
DRT4 Sample_Point_03 20220405
680-213653-4
DRT4 Sample_Point 04_20220405
Matrix Collected Received
Water 04/05/2215:55 04/07/2210:40
Water
Water
Water
04/05/2216:16 04/07/2210:40
04/05/22 14:31 04/07/22 10:40
04/05/2215:03 04/07/2210:40
Job ID: 680-213653-1
Page 3of14
Eurofins Sa gIOhW2

Case Narrative
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Job ID: 680-213653-1
Laboratory: Eurofins Savannah
Narrative
Job Narrative
680-213653-1
Comments
No additional comments
Job ID: 680-213653-1
Receipt
The samples were received on 4/7/2022 10:40 AM. Unless otherwise noted below, the samples arrived in good condition, and where
required, properly preserved and on ice. The temperature of the cooler at receipt was 4.90 C.
General Chemistry
Methods 16648: Insufficient sample volume was available to perform a matrix spike/matrix spike duplicatels ample duplicate
(MSIMSDIDUP) associated with preparation batch 680-716254.
Method 166413: Analysis for Hexane Extractable Material (HEM) was performed for the following samples:
DRT4_Sample_Point_02 20220405 (680-213653-2) and DRT4_Sample_Point_04_20220405 (680-213653-4). Since the HEM result(s)
was below the reporting limit (RL), the result(s) for Silica Gel Treated - Hexane Extractable Material (SGT-HEM) was reported as a
non -detect. All HEM quality control criteria were met.
No additional analytical or quality issues were noted, other than those described above or in the Definitions/Glossary page
Eurofins Savannah
Page 4 of 14 4/20/2022

Client Sample Results
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Client Sample ID: DRT4_ Sample_Point_01_20220405
Date Collected: 04/05122 15:55
Date Received: 04/07/22 10:40
r
General Chemistry
Analyte Result Qualifier
RL
SGT-HEM (TPH) <0.69
2.5
Chemical Oxygen Demand 9.1 J
10
LTotal Suspended Solids 7.1
2.5
Client Sample ID: DRT4_ Sample_ Point _02_20220405
Date Collected: 04/05/22 16:15
Date Received: 04/07/22 10:40
rGeneral Chemistry
Analyte
SGT-HEM (TPH)
[Chemical Oxygen Demand
Total Suspended Solids
MDL Unit
0.69 mg1L
5.0 mg1L
2.5 mg1L
Job ID: 680-213653-1
Lab Sample ID: 680-213653-1
Matrix: Water
D Prepared Analyzed DII Fac
04/18/22 09:29 04/18/22 11:52 1
04/18/22 10:19 1
04/11/22 08:48 1
Lab Sample ID: 680-213653-2
Matrix: Water
Result Qualifier
RL
MDL Unit
D Prepared Analyzed
DII Fac
<0.72
2.6
0.72 mg1L
04/18/22 09:29 04/18/22 11:52
1
<5.0
10
5.0 mg1L
0411812210:19
1
8.6
2.5
2.5 mglL
04/11/22 08:48
1
Client Sample ID: DRT4_ Sample_Point_03_20220405
Lab Sample ID: 680-213653-3
Date Collected: 04/05122 14:31
Matrix: Water
Date Received: 04/07/22 10:40
General Chemistry
Analyte Result Qualifier
RL
MDL Unit
D Prepared Analyzed Dil Fac
SGT-HEM (TPH) 0.73 J
2.6
0.73 mg1L
04/18/22 09:29 04/18/22 11:52 1
Chemical Oxygen Demand 11
10
5.0 mg1L
04/19/22 10:12 1
Total Suspended Solids 3.7
2.5
2.5 mg1L
04/11122 08:48 1
Client Sample ID: ❑RT4_Sam pie -Poi nt_04_20220405
Date Collected: 04/05122 15:03
Date Received: 04/07/22 10.40
General Chemistry
Analyte Result Qualifier RL MDL Unit
SGT-HEM (TPH) <0.72 2.6 0.72 mglL
Chemical Oxygen Demand 13 10 5.0 mglL
L Total Suspended Solids 8.2 2.5 2.5 mg1L
Lab Sample ID: 680-213653-4
Matrix: Water
D Prepared Analyzed DII Fac
04/18/22 09:29 04/18/22 11:52 1
04/19/22 10:12 1
04/11/22 08:48 1
Eurofins Savannah
Page 5 of 14 4/20/2022

QC Sample Results
Client: ERM-West Job ID: 680-213653-1
Project/Site: Storm Water - Amazon Warehouses DRT4
Method: 1664B - HEM and SGT-HEM
} Lab Sample ID: MB 680-71625411-A
Client Sample ID. Method Blank
f Matrix: Water
Prep Type: TotallNA
Analysis Batch: 716290
Prep Batch: 716254
MB MB
Analyte Result Qualifier
RL VIDL Unit D Prepared Analyzed Dil Fac
SGT-HEM (TPH) <1.a
5.0 1.4 mg1L 04/18/22 09:29 04/18122 11:52 1
LLab Sample ID: LCS 680-71625412-A
Client Sample ID: Lab Control Sample
Matrix: water
Prep Type: TotaiiNA
Analysis Batch: 716290
Prep Batch: 716254
Spike LCS LCS %Rec
Analyte
Added Result Qualifier Unit D %Rec Limits
LSGT-HEM (TPH)
20.0 17.20 mg/L 86 64 - 132
FL-ah 'Sample !D: LCSD 680-71625413-A
Client S2rnrle Ill_ Lab Control Sµmrla D----
Matrix: Water
Prep Type: Total/NA
Anal,sis Batch: 716290
Pre- Ra+C3i: 716254
Spike LCSD LCSD %Rec RPD
Analyte
Added Result Qualifier Unit D %Rec Limits RPD Limit
LSGT-HEM (TPH)
20.0 16.40 mgJL 82 64 - 132 5 34
Method: 6220D-2011 - Chemical Oxygen Demand
I—
Lab Sample ID: MB 680-71626613
T
Client Sample la: Method Blank
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 716266
]VIa Ma
Analyte Result Qualifier
Chemical Oxygen Demand a5.0
LLab Sample ID: LCS 680-71626614
i i�uii in: �Arutc.r
Analysis Batch: 716266
Analyte
Chemical Oxygen Demand
FLab Sample ID: MB 680-71644813
Matrix: Water
Analv_ sis Batch. 716448
MB MB
Analyte Result Qualifier
LChemical oxygen Demand <5.0
F
Lab Sample ID: LCS 680-71644814
Matrix: Water
Analysis Batch: 716448
1 Analyte
Chemical Oxygen Demand
RL MDL Unit D Prepared Analyzed Oil Fac
10 5.0 mg1L 0411812210:19 1
Client Sample ID: Lab Control Sample
Prep Typc: T.:tul1"ern,
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
50.0 47.8 mg/L 96 90 -110
Client Sample ID: Method Blank
Prep Type: Total/NA
RL MDL Unit D Prepared Analyzed Oil Fac
10 5.0 mg/L 04119/2210:12 1
Client Sample ID: Lab Control Sample
Prep Type: Total/NA
Spike LCS LCS %Rec
Added Result Qualifier Unit D %Rec Limits
50.0 49.4 mg1L 99 90 - 110
Eurofins Savannah
Page 6 of 14 4/20/2022

QC Sample Results
Client: ERM-West Job ID: 680-213653-1
Project/Site: Storm Water -/amazon Warehouses DRT4
Method: 5220D-2011 - Chemical Oxygen Demand (Continued)
Lab Sample ID: 680-213653-3 MS Client Sample ID: DRT4_Sample_Point_03_20220406
Matrix: Water Prep Type: Total/NA
Analysis Batch: 716448
Sample Sample Spike MS MS %Rea
Analyte Result Qualifier Added Result Qualifier Unit D %Rec Limits
Chemical oxygen Demand 11 50.0 66A mg1L 110 90 - 110
FLab Sample ID: 680-213653-3 MSD Client Sample ID: DRT4_Sample_Point_03_20220405
Matrix. Water Prep Type: TotaiiNA
Analysis Batch: 716448
Sample
Sample
Spike
MSD MSD
%Rec
RPD
Analyte
Result
Qualifier
Added
Result Qualifier
Unit D
%Rec
Limits
RPD Limit
LChemical Oxygen Demand
11
50.5
65.1
mg1L
107
90 - 110
2 30
rLab Samp!e ID: 680-213C-S3-4
MS
Chent Sample Ill: IDRT4_C-mrnle_Pc;-*_04-20220405
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 716411
Sample
Sample
Spike
MS MS
%Rec
Analyte
Result
Qualifier
Added
Result Qualltler
Unit D
%Rec
Limits
Chemical Oxygen Demand
13
50.0
62A
mglL
99
90 -110
Lab Sample ID: 680-213653-4
MSD
Client Sample ID: DRT4_Sample_Point_04_20220405
Matrix: Water
Prep Type: Total/NA
Analysis Batch: 716448
Sample
Sample
Spike
MSD MSD
%Rec
RPD
Analyte
Result
Qualifier
Added
Result Qualifier
Unit D
%Rec
Limits
RPD Limit
Chemical Oxygen Demand
13
50.0
62.8
mglL
100
90- 110
1 30
Method: SM 2540D - Solids, Total Suspended (TSS)
FLalb Sample ID: MB 680-715136/1
Matrix: 'Natc.,
Analysis Batch: 715136
MB M8
Analyte Result Qualifier RL
LTotai Suspended Solids <2.5 2.5
rLab Sample ID: LCS. 680-71513612
Matrix: Water
AnalV_ sis Batch: 715136
Spike
Analyte Added
LT01al Suspended Solids 951
r—
Lab Sample ID: LCSD 680-715136/3
Matrix: Water
Analysis Batch: 715136
Client Sample ID: Method Blank
Prep Type: 'r—faiIl111 A
IV% 11r
MDL Unit D Prepared Analyzed Dil Fac
2.5 mg/L 04/11/22 08:48 1
Client Sample ID: Lab Control Sample
Prep Type: Total]NA
LCS LCS %Rec
Result Qualliier Unit D %Rec Limits
844 i;g L 89 80 -120
Client Sample 11D: Lab Control Sample Dup
Prep Type: Total/NA
Spike LCSD LCSD
Analyte Added Result Qualifier Unit
Total Suspended Solids 951 934 mg1L
%Rec RPD
D %Rec Limits RPD Limit
98 80-120 10 25
Eurofins Savannah
Page 7 of 14 4/20/2022

QC Association Summary
Client: ERM-West
ProjectISite: Storm Water - Amazon Warehouses DRT4
General Chem
Analysis Batch: 716136
Job ID: 680-213653-1
F-Lab Sample ID
client Sample ID
Prep Type
Matrix
Method Prep Batch
680-213653-1
DRT4_Sample_Point_01_20220405
TotallNA
Water
SM 2540D
680-213653-2
❑RT4_Sample_Point_02 20220405
TotalINA
Water
SM 2540D
680-213653-3
DRT4_Sample_Point_03_20220405
Total/NA
Water
SM 2540D
680-213653-4
DRT4_Sample_Point_04_20220405
TotallNA
Water
SM 2540D
MB 680-715136/1
Method Blank
TotallNA
Water
SM 2540D
LCS 680-71513612
Lab Control Sample
TotallNA
Water
SM 2540D
L LCSD 680-715136/3
Lab Control Sample Dup
Total/NA
Water
SM 2540D
Prep Batch: 716264
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
BBO-213653-1
DRT4_Sample_Point _01_20220405
Total/NA
Water
1664E
680-213653-2
DRT4_Sample_Point_02_20220405
TotaliNA
Water
1664E
680-213653-3
DRT4_Sample_Point_03_20220405
Total/NA
Water
16648
680.213653-4
DRT4_Sample_Point 04_20220405
TbtaUNA
Water
1664E
MB 6BO-716254/1-A
Method Blank
TbtallNA
Water
1664B
LCS 680-716254/2-A
Lab Control Sample
TotaUNA
Water
1664B
LLCSD 680-71625413-A
Lab Control Sample Dup
Total[NA
Water
1664B
Analysis Batch: 716266
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
6BO-213653-1
DRT4_Sample_Point_01_20220405
Total/NA
Water
5220D-2011
680-213653-2
DRT4_Sample_Point_02_20220405
TotaUNA
Water
5220D-2011
MB 6BO-716266/3
Method Blank
Total[NA
Water
5220D-2011
LCS 680-71626614
Lab Control Sample
TotaUNA
Water
5220D-2011
Analysis Batch: 716290
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method
Prep Batch
680-213653-1
DRT4_Sample_Point_01_20220405
Total/NA
Water
1664E
716254
6BO-213653-2
DRT4_Sample_Point 02_20220405
Total/NA
Water
1664E
716254
680-213653-3
DRT4_Sample Point_03_20220405
Total/NA
Water
1664B
716254
680-213653-4
DRT4_Sample_Point_04_20220405
TotallNA
Water
1664B
716254
MB 680-7162541i-A
Method Blank
Total/NA
Water
1664B
716254
680-716254/2-A
Lab Control Sample
TotaUNA
Water
1664E
716254
LLCS
LCSD 680-716254/3-A
Lab Control Sample Dup
TotallNA
Water
1664B
716254
Analysis Batch: 716448
Lab Sample ID
Client Sample ID
Prep Type
Matrix
Method Prep Batch
680-213653-3
DRT4_Sample_Point_03_20220405
Total/NA
Water
5220D-2011
680-213653-4
DRT4_Sample_Point_04_20220405
Total/NA
Water
5220D-2011
MB 680-71644813
Method Blank
Total/NA
Water
52200-2011
LCS 680-716448/4
Lab Control Sample
Total/NA
Water
5220D-2011
680-213653-3 MS
DRT4_Sample_Point_03_20220405
Total/NA
Water
5220D-2011
680-213653-3 MSD
DRT4_Sample_Point_03_20220405
Total/NA
Water
5220D-2011
680-213653-4 MS
DRT4_Sample_Point_04_20220405
Total/NA
Water
5220D-2011
680-213653-4 MSD
DRT4_Sample_Point_04_20220405
Total/NA
Water
5220D-2011
Eurofins Savannah
Page 8 of 14 4/20/2022

Lab Chronicle
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Client Sample ID: DRT4 Sample_Point_01_20220405
Date Collected. 04/05/22 15:55
Date Received: 04/07122 10:40
Batch Batch
Dil
Initial
Prep Type Type Method
Run
Factor
Amount
Total/NA Prep 1664B
1016 mL
Total/NA Analysis 1664B
1
Instrument ID: NoEquip
TotaVNA Analysis 5220D-2011
1
2 mL
Instrument ID: SPC7
TotaVNA Analysis SM 2540D
1
1000 mL
Instrument ID: NOEQUIP
Client Sample ID: DRT4_ Sample_Point_02_20220405
Date Collected: 04105/22 16:15
Date Received: 04107/22 10:40
Batch Batch
Dil
Initial
Prep Type Type Method
Run
Factor
Amount
Total/NA Prep 1664B
966 mL
TotaIINA Analysis 1664E
1
Instrument ID: NoEquip
Total/NA Analysis 5220D-2011
1
2 mL
Instrument ID: SPC7
Total/NA Analysis SM 2540D
1
1000 mL
Instrument ID: NOEQUIP
Client Sample ID: DRT4_ Sample_Point_03_20220405
Date Collected: 04105/22 14:31
Date Received: 04107/22 10:40
Batch Batch
Dil
Initial
Prep Type Type Method
Run
Factor
Amount
Total/NA Prep 1664E
464 mL
Total/NA Analysis 1664B
1
Instrument ID: NoEquip
Total/NA Analysis 5220D-2011
1
2 mL
Instrument ID: SPC7
Total/NA Analysis SM 2540D
1
1000 mL
Instrument ID: NOEQUIP
Client Sample ID: DRT4_Sample_Point
04_20220405
Date Collected: 04/05/22 15:03
Date Received: 04/07122 i0:40
F-
Batch Batch
Dil
Initial
Prep Type Type Method
Run Factor
Amount
Total/NA Prep 1664B
966 mL
Total/NA Analysis 16648
1
Instrument ID: NoEquip
Total/NA Analysis 522OD-2011
1
2 mL
Instrument ID: SPC7
Total/NA Analysis SM 2540D
1
1000 mL
Instrument ID: NOEQUIP
Job ID: 680-213653-1
Lab Sample ID: 680-213663-1
Matrix: Water
Final Batch
Prepared
Amount Number
or Analyzed Analyst Lab
500 mL 716254
04/18/22 09:29 JAS TAL SAV
716290
04/18/22 11:52 JAS TAL SAV
2 mL 716266 04/18/22 10:19 ALG TAL SAV
1000 mL 715136 04/11/22 08:48 PG TAL SAV •
Lab Sample 1D: 680-213653-2
Matrix: Water
Final Batch
Prepared
Amount Number
or Analyzed Analyst Lab
500 mL 716254
04/18/22 09:29 JAS TAL SAV
716290
04118/22 11:52 JAS TAL SAV
2 mL 716266 04/18/22 10:19 ALG TAL SAV
1000 mL 715136 04/11/22 08:48 PG TAL SAV
Lab Sample ID: 680-213653-3
Matrix: Water
Final
Batch
Prepared
Amount
Number
or Analyzed
Analyst
Lab
500 mL
716254
04/18/22 09:29
JAS
TAL SAV
716290
04/18/22 11:52
JAS
TAL SAV
2 mL
716448
04/19/22 10:12
ALG
TAL SAV
1000 mL
715136
04111/22 08:48
PG
TAL SAV
Lab Sample ID: 680-213653-4
Matrix: Water
Final Batch
Prepared
Amount Number
or Analyzed Analyst Lab
500 mL 716254
04/18/22 09:29 JAS TAL SAV
716290
04/18/22 11:52 JAS TAL SAV
2 mL 716448 04/19/22 10:12 ALG TAL SAV
1000 mL 715136 04/11122 08:48 PG TAL SAV
Eurofins Savannah
Page 9 of 14
4/20/2022

Lab Chronicle
Client: ERM-West Job ID: 680-213653-1
Project/Site: Storm Water - Amazon Warehouses DRT4
Laboratory References:
TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Eurofins Savannah
Page 10 of 14 4/20/2022

Accreditation/Certification Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Laboratory: Eurofins Savannah
The accreditationslcertiFcations listed below are applicable to this report.
Authority Program Identification Number
LNorth Carolina (WW15W) State 269
Job ID: 680-213653-1
Expiration hate
12-31-22
*1
Eurofins Savannah
Page 11 of 14 4/20/2022

Method Summary
Client: ERM-West
Project/Site: Storm Water - Amazon Warehouses DRT4
Job ID: 680-213653-1
Method
Method Description
Protocol
1664E
HEM and SGT-HEM
1664E
5220D-2011
Chemical Oxygen Demand
SM
SM 2540D
Solids, Total Suspended (TSS)
SM
1664B
HEM and SGT-HEM (Aqueous)
1664B
Protocol References:
16648 = EPA-821-98-002
SM = "Standard Methods For The Examination Of Water And Wastewater"
Laboratory References:
TAL SAV = Eurolins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL [phone]
Laboratory
TAL SAV
TAL SAV
TAL SAV
TAL SAV
Eurofins Savannah
Page 12 of 14 4/20/2022

Eurolins Savannah
5102 LaRoche Avenue
Savannah GA 31404
Phone [phone] Fax: [phone]
Chain of Custody Record
tie eurofins
Client Information
Sampler
�i �t F1l �1 r'`i 11.Yt
Lab PM
Cisneros Roxanne
Carrier p
Q- o
2 -9 34006 1
Client Contact
Doug Wade
Phoney
919 - %-t i O ZC� S
E-Mail �•� state 0n 'a:
[e-mail] AliC
Pa
Page 1 of 1
Company
P WSI D
Jab t
ERM-west
Analysis Requested
Addrpsc.
Due Date Requested.'
Preservation Codes.
1920 Main Street Suite 300
A -HCL M-Hexane
f3 - NaOH N -None
City
FAT Requested (days),
Irvine
[''�;�
C-Zn Acetate O-AsNa02
D - Nitric Add P - Na20AS
Stare Tip
CA, 92614
Compliance Project: a Yes A No
»..
E - NeHSO4 Q - Na2S03
F-Me0H R Na2S203
Phone:
PO
443-612-0046(Tel)
DRT4
o
w
H- AscorbicAaq T TSPDodecahytimte
1 - Ice U - Acetone
water V MCAA
Err+ail
WO
`o
doug wade@erm com
y
rd,
_
�
J - DI -
K -EDTA W-pH 4-5So+ecl
L-EDA Z- Other(cpeafy)
Name'
Project
Storm Water -Amazon Warehouses
24024260
m
�
''',
e
o
Other
Ste:
SSO'rva:
E
°a
w
tll
0
E
Sample
Matrix,
TYPE
(w-.ra.
�
�'
L)
r
o
x
2
Sample
(C=comp,
s..olie.
w.a.won,
o
ry
�
Sample Identtfication
Sample Date
Time
G=grab)
ax-liww.�•u,
w
:'p .
e
W
S ecial InstructionslNote:
Preservation Code:
S
N
S
0AT`f-le_fanf_0i-e7C2af-iss
441-�t;�
i5' S.a
Cr-
Water
N
1
1
2
q
P,KT4-5a k_ PC,kt 02- :�O-zk"Yc5
Lf_5r-.2;Z
16- f 5
Cr
Water
V
N
D'R i 't 03 o2' 0 fc
' - - �.2
i=i', 3 i
G
Water
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q-] `?2.
ja. M3
G
water
Jul
1
1
660-213653 Chain of Custody
Possible Hazard Identifcadorr
Sample Disposal (A fee may be assessed if samples are retained longer than 1 month)
© = = M
© 0 Disposal By Lab © Archive For Months
Non -Hazard Flammable Sktn Irritant Poison 6 Unknown Radiologicaf
Retum To Client
IDeliverable Requested 1 II 111 IV Other (soecrfv)
'elirLjm,Shzi b('
J,
SSDecial InstruLilOnSJQC Reoulrements
? - �=7 z le�5 yo
C .'-'- _ y
Cue*,dy Sz-i: 13$313E

Login Sample Receipt Checklist
Client: ERM-West Job Number: 680-213653-1
Login Number: 213653
List Source: Eurofins Savannah
List Number: 1
Creator: Sims, Robert D
Question
Answer Comment
Radioactivity wasn't checked or is </= background as measured by a survey
NIA
meter.
The cooler's custody seal, if present, is intact.
True
Sample custody seals, if present, are intact.
True
The cooler or samples do not appear to have been compromised or
True
tampered with.
Samples were received on ice.
True
Cooler Temperature is acceptable.
True
Cooler Temperature is recorded.
True
COC is present.
True
COC is filled out in ink and legible.
True
COC is filled out with all pertinent information.
True
Is the Field Sampler's name present on COC?
True
There are no discrepancies between the containers received and the COC.
True
Samples are received within Holding Time (excluding tests with immediate
True
HTs)
Sample containers have legible labels.
True
Containers are not broken or leaking.
True
Sample collection date/times are provided.
True
Appropriate sample containers are used.
True
Sample bottles are completely filled.
True
Sample Preservation Verified.
NIA
There is sufficient vol. for all requested analyses, incl. any requested
True
MS/MSDs
Containers requiring zero headspace have no headspace or bubble is
NIA
<6mm (1/4").
Multiphasic samples are not present.
True
Samples do not require splitting or compositing.
True
Residual Chlorine Checked.
N/A
Mi
Eurofins Savannah
Page 14 of 14 4/20/2022