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HomeMy WebLinkAboutNCG060413_2022 DMR_20220729NCDEQ Division of Energy, Mineral and Land Resources SWo—nvvaier Discharge Monitoring Re)iori. (DiAR) Fofrn fur IVCGO60000 Food and kindred Click here for instructions Complete, sign, scan and submit the DMR via the Stormwater NPDES Permit Data Monitoring Report (DMR) Upload form within 30 days of receiving sampling results. Mail the original, signed hard copy of the DMR to the appropriate DEMLR Regional Office. Certificate of Coverage No, NCG060413 Person Collecting Samples: Parker Cliatt Facility Name: Amazon.com Services LLC - DLT3 Laboratory Name: Eurofins Test America Savannah Facility County: Cabarrus Laboratory Cert. No.: 269 Discharge during this period: ❑✓ Yes ❑ No (if no, skip to signature and date) Has your facility implemented mandatory Tier response actions this sample period for any benchmark exceedances? ❑ Yes El No If so, which Tier (I, II, or III)? A copy of this DMR has been uploaded electronically via iittps://edocs.deg.nc.gov/Forms/SW-DMR ❑✓ Yes ❑ No Date Uploaded: Analytical Monitoring Requirements for Outfalls with Industrial Activities —Benchmarks in (11ed) Parameter Code Parameter Outfall 001 Outfall 002 Outfall 003 Outfall Outfall N/A Receiving Stream Class C C C N/A Date Sample Collected MM/DD/YYYY 6/14/2022 6/14/2022 6/14/2022 46529 24-Hour Rainfall in inches 0.5 0.5 0.5 C0530 TSS in mg/L (1nn nr Sn`) 7.7 11 15 pH in standard units (6.0— 9.0 FW, 00400 7.4 8.11 6.68 Fecal Coliform per 100 ml of 31616 freshwater (if required) (19CC) N/A N / A N /A 61211 Enterococci per 100 ml of saltwater N/A N/A N/A (if required) (500) Chemical Oxygen Demand in mg/L 00340 6.0 29 23 Additional parameters for outfalls in drainage areas that use >S5 gallons per month of new hydraulic oil on average Estimated New Motor/Hydraulic Oil NCOIL Usage in gal/month N/A N/A N/A 00552 Non -Polar Oil & Grease in mg/L 1. ! <0.73 <0.76 <0.77 Outfalls to Outstanding Resource Waters (ORW), High Quality Waters (HQW), Trout Waters (Tr) and Primary Nursery Areas (PNA) have a benchmark TSS limit of 50 mg/L. All other water classifications have a benchmark of 100 mg/L FVJ (Freshwater) SW (Saltwater) Notes (optional): "I certify by my signature below, under penalty of law, that this document and all attachments were prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gather and evaluate the information submitted. Based on my inquiry of the person or persons who manage the system, or those persons directly responsible for gathering the information, the information submitted ' to the best of my k wledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false info r�ir tior�including OiNissibility/4f fines and imprisonment for knowine violations." Signat�/r� of Permittee oV Delegated Authorized Individual mcdbe in@amazon.com Email Address 2d' 2 Z Da e (404) 590-7247 Phone Number urofins Environment j esti ng America ANALYTICAL REPORT Eurofins Savannah 5102 LaRoche Avenue Savannah, GA 31404 Tel: (912)354-7858 Laboratory ,fob ID: 680-217004-4 Client Project/Site: Storm Water - Amazon Warehouses DLT3 For: ERM-West 1920 Main Street Suite 300 Irvine, California 92614 Attn: Doug J Wade Authorized for release by: 6/28/2022 9:22:09 AM Roxanne Cisneros, Senior Project Manager (615)301-5761 rxanne.cisneros(r_et.eurofinsus.com The test results in this report meet all 2003 NELAC, 2009 TNI, and 2016 TNi requirements for accredited parameters, exceptions are noted in this report. This report may not be reproduced except in full, and with written approval from the laboratory. For questions please contact the Project Manager at the e-mail address or telephone number listed on this page. This report has been electronically signed and authorized by the signatory. Electronic signature is intended to be the legally binding equivalent of a traditionally handwritten signature. Results relate only to the items tested and the sample(s) as received by the laboratory. J I Definitions/Glossary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT3 Qualifiers - - - - --- - - - General Chemistry Qualifier Qualifier Description J Result is less than the RL but greater than or equal to the MOIL and the concentration is an approximate value. Glossary Abbreviation These commonly used abbreviations may or may not be present in this report. n Listed under the "D" column to designate that the result is reported on a dry weight basis %R Percent Recovery CFL Contains Free Liquid CFU Colony Forming Unit CNF Contains No Free Liquid DER Duplicate Error Ratio (normalized absolute difference) Dil Fac Dilution Factor DL Detection Limit (DoDIDOE) DL, RA, RE, IN Indicates a Dilution, Re -analysis, Re -extraction, or additional Initial metalslanion analysis of the sample DLC Decision Level Concentration (Radiochemistry) EDL Estimated Detection Limit (Dioxin) LOD Limit of Detection (DoD/DOE) LOQ Limit of Quantitation (DoD/DOE) MCL EPA recommended "Maximum Contaminant Level" MDA Minimum Detectable Activity (Radiochemistry) MDC Minimum Detectable Concentration (Radiochemistry) MDL Method Detection Limit ML Minimum Level (Dioxin) MPN Most Probable Number MQL Method Quantitation Limit NC Not Calculated ND Not Detected at the reporting limit (or MDL or EDL if shown) NEG Negative I Absent POS Positive I Present PQL Practical Quantitation Limit PRIES Presumptive QC Quality Control RER Relative Error Ratio (Radiochemistry) RL Reporting Limit or Requested Limit (Radiochemistry) RPD Relative Percent Difference, a measure of the relative difference between two points TEF Toxicity Equivalent Factor (Dioxin) TEQ Toxicity Equivalent Quotient (Dioxin) TNTC Too Numerous To Count Job ID: 680-217004-4 Eurofins Savannah Page 2 of 13 6/28/2022 Sample Summary Client: ERM-West ProjectlSite: Storm Water - Amazon Warehouses DLT3 Lab Sample ID Client Sample ID 680-217004-9 DLT3_Sample_Point 01_20220614 680-217004-10 DLT3_Sample_Point 02_20220614 680-217004-11 DLT3_Sampie_Point 03_20220614 Matrix Collected Received Water OW14/22 09:15 06/15/22 19:00 Water Water 06/14/22 09:35 06/15/2219:00 06/14/22 09:50 06/15/2219:00 Job ID: 680-217004-4 Page 3 of 13 Eurofins SONOW2 Case Narrative Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT3 Job ID: 680-217004-4 Laboratory: Eurofins Savannah Narrative Job Narrative 680-217004-4 Comments No additional comments. Job ID: 680-217004-4 Receipt The samples were received on 6/15/2022 7:00 PM. Unless otherwise noted below, the samples arrived in good condition, and where required, properly preserved and on ice. The temperatures of the 2 coolers at receipt time were 2.81 C and 3.31 C. General Chemistry Methods 16648: Insufficient sample volume was available to perform a matrix spikelmatrix spike duplicate/sample duplicate (MSIMSD/DUP) associated with preparation batch 680-727836. Methods 1664B: Analysis for Hexane Extractable Material (HEM) was performed for the following samples: DLT3_Sample_Point_01_20220614 (680-217004-9), DLT3_Sample_Point_02_20220614 (680-217004-10) and DLT3_Sample_Point_03_20220614 (680-217004-11). Since the HEM results were below the reporting limit (RL), the results for Silica Gel Treated - Hexane Extractable Material (SGT-HEM) was reported as a non -detect. All HEM quality control criteria were met. No additional analytical or quality issues were noted, other than those described above or in the DefinitionslGlossary page Eurofins Savannah Page 4 of 13 6/28/2022 Client Sample Results Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT3 Client Sample ID: DLT3_Sample_Point_07_20220614 Date Collected: 06114/22 09:15 Date Received: 06/16/22 19:00 General Chemistry Analyte Result Qualifier RL SGT-HEM (TPH) <0.73 Z6 Total Suspended Solids 7.7 2.5 LChemical Oxygen Demand 6.0 J 10 Client Sample ID: DLT3_Sample_Point_02_20220614 Date Collected: 06/14/22 09:35 Date Received: 06/15/22 19:00 FGeneral Chemistry Job ID: 680-217004-4 Lab Sample ID: 680-217004-9 Matrix: Water MDL Unit D Prepared Analyzed Dif Fac 0.73 mg1L 06/27/22 09:06 06/27/22 11:32 1 2.5 mg/L 06/17/2210:11 1 5.0 mg1L 0612712214:41 1 Lab Sample ID: 680-217004-10 Matrix: Water Analyte SGT-HEM (TPH) Total Suspended Solids `Chemical Oxygen Demand Result Qualifier <0.76 11 29 RL 2.7 5.0 10 MDL Unit 0.76 mgIL 5.0 mg1L 5.0 mg/L D Prepared 06/27/22 09:06 Analyzed Dil Fac 06/27/22 11:32 1 06/17/22 10:11 1 06/27/22 14:41 1 Client Sample ID: DLT3_Sample_Point_03_20220614 Lab Sample ID: 680-217004-11 Date Collected: 06/14/22 09:60 Matrix: Water Date Received: 06/15/2219:00 General Chemistry i Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac i SGT-HEM (TPH) <0.77 2.7 0.77 mg/L 06/27/22 09:06 06/27/22 11:32 1 Suspended Solids f 5 5.0 5.0 mg/L 06/17/22 10:11 1 LTotal Chemical Oxygen Demand 23 10 5.0 mg/L 06/27/22 09:45 1 Eurofins Savannah Page 5 of 13 6/28/2022 QC Sample Results Client: ERM-West Project/Site: Storm Water- Amazon Warehouses DLT3 Method: 1664E - HEM and SGT-HEM rLab Sample ID: MB 680-72783611-A Matrix: Water Analysis Batch: 727891 MB MB Analyte Result Qualifier SGT-HEM (TPH) <1.4 Lab Sample ID: LCS 680-72783612-A Matrix: water Analysis Batch. 727891 Analyte LSGT-HEM (TPH) Law Sample !D: LCSD 680-727836/3-A Matrix: Water Analysis Patch: 727891 Analyte LSGT-HEM (TPH) RL MDL Unit 5,0 1.4 mg1L Job ID: 680-217004-4 Client Sample ID: Method Blank Prep Type: Total/NA Prep Batch: 727836 D Prepared Analyzed Dil Fac 06/27122 09:06 06/27/22 11:32 1 Client Sample ID: Lab Control Sample Prep Type; lotaUNA Prep Batch: 727836 Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 200 15.80 mg1L 79 64 - 132 Client Sarn-le !D: Lab Contro! Sample Dup Prep Type: Total/NA Prop Batch: 727836 �r Spike LCSD LCSD %Rec RPD Added Result qualifier Unit D %Rec Limits RPD Limit 20.0 16.40 mg1L 82 64 - 132 4 34 Method: 254OD-2015 - Total Suspended Solids (Dried at 103-105°C) Lab Sample ID: MB 680-72628211 Client Sample 10: Methoct Blank Matrix: Water Prep Type: Total/NA Analysis Batch: 726282 MB M13 Analyte Result Qualifier RL MDL Unit D Prepared Analyzed Dil Fac Total Suspended Solids <2.5 2.5 2.5 mg1L 06/17/22 10:11 1 LLab Sample ID: LCS 680-72628212 Client Sample ID: Lab Control Sample Matrix: U'Vater P-CP T CPC: TOta11N n i cN y Nc. �v�ui i r-i Analysis Batch: 726282 Analyte LTotal Suspended Solids I Lab Sample ID: LCSD 680-72628213 Matrix: Water Analysis Batch: 726282 Analyte Total Suspended Solids Spike LCS LCS %Rec Added Result Qualifier Unit D %Rec Limits 951 850 mglL 89 80 - 120 Client Sample ID: Lab Control Sample Duo Prep Type: Total/NA Spike LCSD LCSD Added Result Qualifier Unit D %Rec 951 848 mglL 89 Method: 6220D-2011 - Chemical Oxygen Demand _ FLab Sample ID: MB 680-727847/3 Matrix: Water Analysis Batch. 727847 MB MB Analyte Result Qualifier RL MOIL Unit Chemical Oxygen Demand <5.0 10 5.0 mglL %Rec Limits 80-120 RPD RPD Limit 0 25 Client Sample it): Method Blank Prep Type: Total/NA D Prepared Analyzed Dil Fac 06/27/22 09:45 1 Eurofins Savannah Page 6 of 13 6/28/2022 QC Sample Results Client: ERM-West Projecl/Site: Storm Water - Amazon Warehouses DLT3 Method: 5220D-2011 - Chemical Oxygen Demand (Continued) Lab Sample ID: LCS 680-72784714 Matrix: Water Analysis Batch: 727847 Job ID:680-217004-4 Client Sample ID: Lab Control Sample Prep Type: Total/NA Spike LCS LCS %Rec Analyte Added Result Qualifier Unit D %Rec Limits Chemical Oxygen Demand 50.0 47.9 mg1L 96 90- 110 FLab Sample ID: MB 680-72792313 Matrix: Water Analysis Batch: 727923 MB MB Analyte Result Qualifier RL MDL Unit L - ' Lab Campla In: LCS 680-72792314 Matrix: Water Analysis hatch: 727923 Analyte Chemical Oxygen Demand <5.0 10 5.0 mg1L Client Sample ID: Method Blank Prep Type: TotaiiNA D Prepared Analyzed Dil Fac 06/27122 14:41 1 !`liana Cwrnlo Ill: L.'..I' rrwntr0l Ear gn!e Prep Type: TotallNA Spike LCS LCS %oRec Added Result Qualifier Unit D %,Rec Limits 50.0 48.2 mglL 96 90 - 11 D Page 7 of 13 Eurofins Savannah 6/28/2022 QC Association Summary Client: ERM-West Job ID: 680-217004-4 Project/Site: Storm Water - Amazon Warehouses DLT3 General Chemi Analysis Batch: 726282 [Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217004-9 DLT3_Sample_Point_01 20220614 Total/NA Water 254OD-2015 680-217004-10 DLT3_S8mple_Point_02_20220614 TotalINA Water 254OD-2015 680-217004-11 DLT3_Sample_Point_03_20220614 Total/NA Water 25400-2015 MB 680-726282/1 Method Blank Total/NA Water 254OD-2015 LCS 680-72628212 Lab Control Sample Total/NA Water 254OD-2015 LCSD 680-72628213 Lab Control Sample Dup TotalINA Water 254OD-2015 Prep Batch: 727836 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217004-9 DLT3 Sample_Point 01y20220614 TotaUNA Water 1664B 680-217004-10 DLT3_Sample-Point TotalINA Water 1664E 680-217004-11 _02_20220614 DLT3_Sample_Point_03_20220614 TotalINA Water 1664B MB 680-727836/1-A Method Blank TotaUNA Water 1664B LCS 680-727836/2-A Lab Control Sample Total/NA Water 1664B LCSD 680-727836/3-A Lab Control Sample Dup Total/NA Water 1664E Analysis Batch: 727847 LLab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217004-11 DLT3_Sample_Point_03_20220614 Total/NA Water 5220D-2011 MB 680-727847/3 Method Blank Total/NA Water 5220D-2011 LLCS 680-727847/4 Lab Control Sample Total/NA Water 5220D-2011 Analysis Batch: 727891 Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217004-9 DLT3_Sample_Point 01_20220614 TotalINA Water 1664E 727836 680-217004-10 DLT3_Sample_Point_02_20220614 Total/NA Water 1664E 727836 680-217004-11 DLT3_Sample_Point03_20220614 Total/NA Water 16648 727836 MB 680-72783611-A Method Blank Total/NA Water 1664B 727836 LCS 680-727836/2-A Lab Control Sample Total/NA Water 1664B 727836 LLCSD 680-72783613-A Lab Control Sample Dup TotalINA Water 1664E 727836 Analysis Batch: 727923 r Lab Sample ID Client Sample ID Prep Type Matrix Method Prep Batch 680-217004-9 DLT3_Sample_Point_01_20220614 Total/NA Water 5220D-2011 680-217004-10 DLT3_Sample_Point_02_20220614 TotalINA Water 5220D-2011 MB 680-72792313 Method Blank Total/NA Water 5220D-2011 LCS 680-72792314 Lab Control Sample TotaI1NA Water 5220D-2011 Eurofins Savannah Page 8 of 13 6/28/2022 Lab Chronicle Client: ERM-West Job ID: 680-2170044 Project/Site: Storm Water - Amazon Warehouses DLT3 Client Sample ID: DLT3_ Sam pie_Point_01_20220614 Lab Sample ID: 680-217004-9 Date Collected: 06114/22 09:16 Matrix: Water Date Received: 06/15/22 19:00 Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab Total/NA Prep 1664B 956 mL 500 mL 727836 06/27/22 09:06 JAS TAL SAV Total/NA Analysis 1664E 1 727891 06/27122 11:32 JAS TAL SAV Instrument ID: NoEquip Total/NA Analysis 254OD-2015 1 1000 mL 1000 mL 726282 06/17/22 10:11 PG TAIL SAV Instrument ID: NOEQUIP LTotolINA Analysis 5220D-2011 1 2 mL 2 mL 727923 06/27/22 14:41 ALG TAL SAV Instrument ID: SPC7 Client Sample ID: DLT3_Sample_Point_02_20220614 Date Collected: 06/14/22 09:35 Date Received: 06/15/22 19:00 r— Batch Batch Dil Initial Prep Type Type Method Run Factor Amount Total/NA Prep 1664B 920 mL TotalINA Analysis 1664B 1 Instrument ID: NoEquip Total/NA Analysis 254OD-2015 1 500 mL Instrument ID: NOEQUIP TotaUNA Analysis 5220D-2011 1 2 mL Instrument ID: SPC7 L Client Sample ID: DLT3 Sam ple_Point_03_20220614 Date Collected: 06/14/22 09:50 Date Received: 06/15122 19:00 Lab Sample ID: 680-217004-1.0 Matrix: Water Final Batch Prepared Amount Number or Analyzed Analyst Lab 500 mL 727836 06/27/22 09:06 JAS TAL SAV 727891 06/27/22 11:32 JAS TAL SAV 1000 mL 726282 06117/22 10:11 PG TAL SAV 2 mL 727923 06/27/22 14:41 ALG TAL SAV Lab Sample ID: 680-217004-11 Matrix: Water Batch Batch Dil Initial Final Batch Prepared Prep Type Type Method Run Factor Amount Amount Number or Analyzed Analyst Lab TotalINA Prep 1664B 914 mL 500 mL 727836 06/27/22 09:06 JAS TAL SAV Total/NA Analysis 1664E 1 727891 06/27/22 11:32 JAS TAL SAV Instrument ID: NoEquip TotalINA Analysis 2540D-2015 1 500 mL 1000 mL 726282 06/17/22 10:11 PG TAL SAV Instrument ID: NOEQUIP TotalINA Analysis 5220D-2011 1 2 mL 2 mL 727847 06/27/22 09:45 ALG TAL SAV Instrument ID: SPC7 Laboratory References: TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 Page 9 of 13 Eurofins Savannah 6/28/2022 Accreditation/Certification Summary Client: ERM-West Project/Site: Storm Water - Amazon Warehouses DLT3 Laboratory: Eurofins Savannah The accreditationstcertifcations listed below are applicable to this report. FAuthority Program Identification Number North Carolina (WW1SW) State 269 Job ID: 680-217004-4 Expiration Date 12-31-22 Eurofins Savannah Page 10 of 13 6/28/2022 Method Summary Client: ERM-West Job ID: 680-217004-4 Project/Site: Storm Water - Amazon Warehouses DLT3 Method Method Description Protocol Laboratory 1664B HEM and SGT-HEM 1664E TAL SAV 2540D-2015 Total Suspended Solids (Dried at 103-105°C) SM TAL SAV 5220D-2011 Chemical Oxygen Demand SM TAL SAV 1664E HEM and SGT-HEM (Aqueous) 1664B TAL SAV Protocol References: 1664E = EPA-821-98-002 SM = "Standard Methods For The Examination Of Water And Wastewater" Laboratory References: TAL SAV = Eurofins Savannah, 5102 LaRoche Avenue, Savannah, GA 31404, TEL (912)354-7858 kffl LtLn Eurofins Savannah Page 11 of 13 6/28/2022 Eurofins Savannah 6102 LaRoche Avenue tit eurofins Savannah GA 31404 Chain of Custody Record E ronment lest 18 Amerce Phone 912-354-76S6 Fax 912-352-0165 Client Information ,. Lob PM taan ores Roxanne Tnaaing "a) CDC Na 240-N104-33341 1 dent cachet /aw ' � yv v Ffwaw b - S 77 -S7,v C-"stow roxanne ctsnerosl�et.eurofinstrs.com OfP Page 1 of 1 CWPWW Pwslo- ERM-Southeast i^c- Analysis Requested jobw. Adcwft T*- T on; at Witdwcod Plata 3200 Wandy Hill Road Suite 154 Due Date itaquested TAT Roque ead {days) *4 4 h t �' '-14 1 @ �$ � o z Preservation Codes u Hexane AN&O N NM 9NaZn AH O-ASNs02 C• e P Na204S D t6lmlA d 0 Na2503 C M �WM _ 0 An=W T ' H-ASWtt2eAdd sp � t_ u MCAAAMOo J DtWater Y PH4 K EDTA Y Tdo" L.EDA v Triodes 2 abrer (sPeofy) Other nta rs= r _ Pndne 12-OWel) r v J a C (� 8 d 6& . w� crrN.G tit Project Nww Storm Water -Amazon Warehouses Ptop,a* 24024260 p m �' rv�arly,corL 4G' OL ssows- — Sam IdertBRcation Sample Time Sample Type (C=Cmp, b Matrix aa Iffr-nawe 1mQ Special lnstnutions/Noto c3' — /t i��wF_ 61— OZZd41 CO&Prea S N 6 `"rater 1 7- 4 oZ—ZaZi feeLrl� 44 Z2 •,vt+fi G Water 1 t z Y 7D rb— /� - b — 74 Z Z ova 1 ,y ZZ 9• s'aA Water V M 2 Water Possible Hazard ldentrlleabon lD Non -Hazard M Flammable E:3 Shin hritant O Pelson a M Unknown Sample Disposal (A tee may be assessed rf samples are retained longer then t month) I C:3 Retunt To Chent M Disposal BY Lab Archive For Months Deliverable Requested 1 II III IV Other (spectly) S petaal MstrudtonstOC Requirements Empty KQ Relm/q�utshed by- Date. Tlnte. Rfathod of shwnent br Oa`e7Thn Zz Gomparty Received 4 a " 11 t dmpany ReiingWsrad r r cO COmpwry Rowvad by sy Rearrquistted by Oa a Compeay Custody Seals Itdact Custody Seal No a Yes a No RMwed by Wartime: con ay COOWTemperaaea(s)'Cand Oaror Remeft. Ver- 0610SP-02I Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217004-4 Login Number: 217004 List Number: 1 Creator: Bissonnette, Ian Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is </= background as measured by a survey N/A meter. The cooler's custody seal, if present, is intact True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COG? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection dateltimes are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. N/A There is sufficient vol. for all requested analyses, incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is N/A <6mm (1/411). Multiphasic samples are not present True Samples do not require splitting or c ompositing. True Residual Chlorine Checked. N/A M Eurofins Savannah Page 13 of 13 6/28/2022 cc M N R w 01 OND N O Eurofins Savannah 5102 LaRoche Avenue Savannah GA 31404 Phone 912-354-7858 Fax 912-52-0165 Chain of Custody Record ,�. eurofins E ronr•,artt Test -18 Arrer•ea Client Information ,- Lab PM Cisneros Roxanne CamerTiad ling NOM COC Na 240 96104 33341 1 CSent ConteG K W Phptx b —,r?7 -S'7'jrj F.Mali iroxanne ctsaeros@et.euroftnsus com State of Odgbx Page: Page 1 of 1 cofflowPWSitr ERM-So" dry Inc. Analysis Requested .loba: TF- * ers at Wildwood Plaza 3200 Wndy Hill Road Suite 150 cue Dau aaRwsud TAT Reque lad (days) Preservation Codes u Hezuu A HCL N NOM cay Atlanta B Ns0H O_ASN.02 C:ZaAeatats P N92043 D-NtdcAeid Sn.. v e N ,Mm, O Ne2S03 P 44"12-0046(TH) C 3 L x M-An I -we hbitAcld U.Acetoone `r Emain � p Otk d d& t s 1 Ol water MCAA ETA yr PH 4-5 I. Tdarera z ovw(Spot* Cow PmjepNDnM: Storm water- Amazon warehouses # 2402426D rly,ge 4LC• OL73 ssa"t I oType m b a Sample Matrm it :s Sample (�mP. e� arena .,! z s Sam to idortiiiwtion Sam a Date Time tab or Tb .rwa M ►° Special Instructions/NoW Pre,SenrallonCode: g N G /ir. f�jwF bl " 7-0=44 Ij GIN water A44 i 1 Z t{ 3— isR R OZ`Z&ZZot¢iY (¢ t¢ 22 •3sh [ water 4AJ ) r 1Z a"—=0i. ly 9•sbA water r.1jq1z? Water Passible Nasard /denbflratron O Non -Hazard M Flammable ElSkin 1mYant 0 pcfson 9 0 Unknown En Raaiobjw4 t le Olsposad (A tee may be assessed of samples are returned longer trim 1 month) �Retum 7'o Chent (1 Daposs( By tab M Archive For Months Deliverable Requested 1 It III N Other (specify) Spectal InshucbmsIOC Requirements Empty Kit Relinquished b)r jDate. Time, seattrod of 9i>mmart by CIr4 Qatemma• ql2pzz company &&&I DttaTmo; Q jmk� 110-- Relhrgrtwwo r OaCompany Rooeind by Dawrimm Company t t 1 r7 CO KOWNUMM by a Company Raeetved try —T DstatTfmo:� Compaq Custody Seals Intact Custody Sect No CoaherTemperame(s) rC and corer Rernaft. a Yes a. No 2. r/z Y Verr 06108R021 Login Sample Receipt Checklist Client: ERM-West Job Number: 680-217004-4 Login Number: 217004 List Number: 1 Creator: Bissonnette, Ian Question List Source: Eurofins Savannah Answer Comment Radioactivity wasn't checked or is <1= background as measured by a survey NIA meter. The cooler's custody seal, if present, is intact. True Sample custody seals, if present, are intact. True The cooler or samples do not appear to have been compromised or True tampered with. Samples were received on ice. True Cooler Temperature is acceptable. True Cooler Temperature is recorded. True COC is present. True COC is filled out in ink and legible. True COC is filled out with all pertinent information. True Is the Field Sampler's name present on COC? True There are no discrepancies between the containers received and the COC. True Samples are received within Holding Time (excluding tests with immediate True HTs) Sample containers have legible labels. True Containers are not broken or leaking. True Sample collection date/times are provided. True Appropriate sample containers are used. True Sample bottles are completely filled. True Sample Preservation Verified. NIA There Is sufficient vol. for all requested analyses, Incl. any requested True MS/MSDs Containers requiring zero headspace have no headspace or bubble is NIA <6mm (114"). Multiphasic samples are not present. True Samples do not require splitting or compositing. True Residual Chlorine Checked. NIA Eurofins Savannah Page 13 of 13 6/28/2022