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WQ0039924_Renewal (Application)_20221201
Initial Review Reviewer Thornburg, Nathaniel D Is this submittal an application? (Excluding additional information.)* Yes No Permit Number (IR) * WQ0039924 Applicant/Permittee von Drehle Corporation Applicant/Permittee Address 126 First Street Cordova, NC 28330 Is the owner in BIMS? Yes No Is the facility in BIMS? Owner Type Facility Name County Fee Category Is this a complete application?* Yes No Signature Authority Signature Authority Title Signature Authority Email Document Type (if non -application) Email Notifications Organization von Drehle Corporation Class A Residuals Program Richmond Does this need review by the hydrogeologist? * Yes No Regional Office CO Reviewer Admin Reviewer Yes No Fee Amount $0 Complete App Date 12/05/2022 Below list any additional email address that need notification about a new project. ... ... .. Email Address Comments to be added to email notfication Comments for Admin Comments for RO Comments for Reviewer Comments for Applicant Submittal Form Project Contact Information Please provide information on the person to be contacted by NDB Staff regarding electronic submittal, confirmation of receipt, and other correspondence. ............................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................................ Name* Robert T. Branch Email Address* bbranch@branchrs.com Project Information Application/Document Type* New (Fee Required) Modification - Major (Fee Required) Renewal with Major Modification (Fee Required) Annual Report Additional Information Other Phone Number* 3363129007 Modification - Minor Renewal GW-59, NDMR, NDMLR, NDAR-1, N DAR-2 Residual Annual Report Change of Ownership We no longer accept these monitoring reports through this portal. Please click on the link below and it will take you to the correct form. hftps://edocs.deq.nc.gov/Forms/NonDischarge_Monitoring_Report Perm it Type:* Wastewater Irrigation High -Rate Infiltration Other Wastewater Reclaimed Water Closed -Loop Recycle Residuals Single -Family Residence Wastewater Other Irrigation Permit Number: * WQ0039924 Has Current Existing permit number Applicant/Permittee* von Drehle Corporation Applicant/Permittee Address* 126 First Street Cordova, NC 28330 Facility Name* von Drehle Corporation Class A Residuals Program Please provide comments/notes on your current submittal below. Renewal with no modifications At this time, paper copies are no longer required. If you have any questions about what is required, please contact Nathaniel Thornburg at nathaniel.thornburg@ncdenr.gov. Please attach all information required or requested for this submittal to be reviewed here. (Application Form, Engineering Plans, Specifications, Calculations, Etc.) 2022 vd final renewal.pdf 3.15MB Upload only 1 PDF document (less than 250 MB). Multiple documents must be combined into one PDF file unless file is larger than upload limit. * By checking this box, I acknowledge that I understand the application will not be accepted for pre -review until the fee (if required) has been received by the Non - Discharge Branch. Application fees must be submitted by check or money order and made payable to the North Carolina Department of Environmental Quality (NCDEQ). I also confirm that the uploaded document is a single PDF with all parts of the application in correct order (as specified by the application). Mail payment to: NCDEQ — Division of Water Resources Attn: Non -Discharge Branch 1617 Mail Service Center Raleigh, NC 27699-1617 Signaturej• Submission Date 12/1/2022 PERMIT RENEWAL FOR THE DISTRIBUTION OF RESIDUAL SOLIDS WQ0039924 VON DREHLE CORPORATION CORDOVA, NC FACILITY FIBER CLAY CORDOVA, NORTH CAROLINA Prepared For: von Drehle Corporation 126 First Street Cordova, NC 28330 Prepared By: Branch Residuals & Soils, LLC 1735 Heckle Blvd. — Suite 103-291 Rock Hill, SC 29732 November 2022 BRANCH RESIDUALS & SOILS, LLC 1735 Heckle Blvd. Suite 103-291, Rock Hill, SC 29732 PHONE (336) 510-0340 • Cell (336) 312-9007 November 30, 2022 NCDEQ -Division of Water Resources Non -Discharge Branch Mail Service Center 1617 Raleigh, North Carolina 27699-1617 Attention: Mr. Nathaniel Thornburg Reference: PERMIT RENEWAL WQ0039924 von Drehle Corporation — Cordova Facility Cordova, North Carolina BR&S Job No. 2022-141 Dear Mr. Thornburg: Branch Residuals & Soils, LLC is under contract with the von Drehle Corporation to prepare to renew the current Class A distribution permit. von Drehle has transferred land that they own to Bio-Nomics so that applications can continue to be made and a potential nitrogen source that will aid in the breakdown of the fiber clay. The generated Fiber Clay has no domestic input but is derived from woody sources that are known to have interference with fecal coliform values (Klebsiella sp.). Based on the false positive interferences with the fecal coliform testing procedures, von Drehle will be performing Salmonella testing. Distribution avenues will include application in accordance with soil lime requirements, distribution as a soil amendment (either alone or in concert with other products), distributed to facilities that may blend soil amendments and mulch, and as a daily landfill cover. Please contact me immediately if you require additional information or have questions in the review of the permit application. Si ely, r Robert T. Branch, L. S. S. Project Manager cc: Mr. Mitchell Luckie— von Drehle Corporation— Cordova Facility TABLE OF CONTENTS Section No. Title I DISTRIBUTION OF RESIDUAL SOLIDS APPLICATION FORM Copy of Existing Permit II RESIDUALS SOURCE CERTIFICATION ATTACHMENT — FIBER CLAY Vicinity Map Process Flow Diagram and Narrative Justification of Residuals Production Rate Sampling Plan Residual Analytical Reports III MANAGEMENT PLAN Overview of Process and Residual Solids Handling Distribution Methods for Reuse Transportation and Logistics Monitoring and Recordkeeping Leachate Collection IV VON DREHLE CORDOVA FIBER CLAY LABEL AND PRODUCT INFORMATION SHEET V VON DREHLE CORDOVA FIBER CLAY RESIDUALS RECEIPT FORM VI SPILL CONTROL PLAN VII APPLICATION RATES ;3 01 fl Col 1 DISTRIBUTION OF RESIDUAL SOLIDS APPLCIATION FORM State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS INSTRUCTIONS FOR FORM: DCAR 06-16 & SUPPORTING DOCUMENTATION Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website General — This application is for treatment, storage, transport, distribution, land application, and/or marketing of Class A (or Equivalent) residuals under 15A NCAC 02T .1100. Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Distribution of Class A Residuals (FORM: DCAR 06-16): ® Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR 06-16) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® The project name should be consistent on the plans, specifications, etc. ® The Applicant's Certification on Page 3 of this form shall be signed in accordance with 15A NCAC 02T .0106(b). An alternate person may be designated as the signing official if a delegation letter is provided from a person who meets the criteria in 15A NCAC 02T .0106(b). ❑ If this project is for a modification of an existing permit, submit one copy of the existing permit. ❑ Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to operation of proposed facility(ies) for application packages involving new or changes to treatment and storage units. B. Application Fee (New and Major Modification Application Packages) ® Submit a check, money order or electronic funds transfer made payable to: North Carolina Department of Environmental Quality (NCDEQ). Facility Classification New Permit Major Modification Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 $395 Minor (residuals permitted for distribution < 3,000 dry tons/year) $810 $245 - A major modification shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage; adds additional residuals sources; or includes the addition of new treatment or storage units/processes not previously permitted. There is no fee for minor permit modifications. C. Cover Letter (All Application Packages) ® List all items included in the application package, as well as a brief description of the requested permitting action. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 1 of 3 D. Program Information (All Application Packages) ® Provide a narrative explaining the following: ® How the materials will be handled and transported from where the residuals were produced to where it will be treated. ® How the residuals will be processed/treated (attach process flow diagram). ® How leachate collection will be handled. ® Where the residuals will be stored until processed. ® How the final product will be distributed (packaging, bulk, etc.) ® What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality. ® Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed. ® Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following information: ® Name and address of the person who prepared the residual that is sold or given away. ® A statement that application of the residuals to the land shall be in accordance with the instructions on the label or information sheet. ® A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered. ® A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored residuals into any surface waters. ® Information on all applicable setbacks in accordance with 15A NCAC 02T. I 108(b). ® A statement that the residuals shall be applied at agronomic or recommended rates for intended uses. E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard specifications, but use of the standard specifications must be noted on each sheet of the plans. ❑ Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T A 108(a) on the plans. ❑ Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units: description of materials to be used, methods of construction, quality of construction testing procedures to ensure the integrity of the final product in accordance with 15A NCAC 02T A 104(a)(2)(B), including leakage and pressure testing as appropriate. ❑ Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION. F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units) ❑ Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T .1 104a . G. Environmental Assessments (Maybe Required— See 15A NCAC 1C .0300) ❑ Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands are used for the construction of the subject facilities. INSTRUCTIONS FOR FORM: DCAR 06-16 Page 2 of 3 H. Operation and Maintenance Plan (New and Renewal Application Packages) ® For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan. ® Submit the O&M Plan in accordance with 15A NCAC 02T .1110 and include at a minimum: ® Operational functions; describe the operation of the program to show what operations are necessary for the program to function and by whom the functions are to be conducted. ® Maintenance schedules; may include equipments calibration, maintenance of signs, etc. ® Safety measures; may include safety training program, manuals, signs, etc. ® Spill response plan; including control, containment, remediation, emergency contact information, etc. ® Inspection plan including the following information; ® Names and titles of personnel responsible for conducting the inspections. ® Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program. ® Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed. ® Sampling and monitoring plan including the following information; ® Names and titles of personnel responsible for conducting the sampling and monitoring. ® Detailed description of monitoring procedures including parameters to be monitored. ® Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures. ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS: NORTH CAROLINA DEPARTMENT OF ENVIRONMENTAL QUALITY DIVISION OF WATER RESOURCES WATER QUALITY PERMITTING SECTION NON -DISCHARGE PERMITTING UNIT By U.S. Postal Service: 1617 MAIL SERVICE CENTER RALEIGH, NORTH CAROLINA 27699-1617 TELEPHONE NUMBER: (919) 807-6464 By Courier/Special Delivery: 512 N. SALISBURY STREET RALEIGH, NORTH CAROLINA 27604 FAX NUMBER: (919) 807-6496 INSTRUCTIONS FOR FORM: DCAR 06-16 Page 3 of 3 State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS FORM: DCAR 06-16 I. APPLICANT INFORMATION: 1. Applicant's name: von Drehle Corporation Applicant type: ❑ Individual ® Corporation ❑ General Partnership ❑ Privately -Owned Public Utility ❑ Federal ❑ State ❑ Municipal ❑ County Signature authority's name per 15A NCAC 02T .0106: Michael Mennin¢ Title: Mill Manager Applicant's mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (2jQ) 410-1327 Email Address: michael.menning@vondrehle.com 2. Consultant's name: Branch Residuals & Soils, LLC License Number (for P.E.): Affiliation: ❑ On Staff ® Retained (Firm: ) Consultant's mailing address: 1735 Heckle Blvd. - Suite 103-291 City: Rock Hill State: SC Zip: 29732- Telephone number: (336) 312-9007 Email Address: bbranchAbranchrs.com 3. Fee submitted: 0.00 (See Instruction B) II. PERMIT INFORMATION: 1. Application is for (check all that apply): ❑ new, ❑ modified, ® renewed permit 2. If this application is being submitted to renew or modify an existing permit, provide the following: Permit number: W00039924 Date of most -recently issued permit: June 28, 2018 Date of most -recently certified Attachment A (if different than the permit): April 8, 2021 III. FACILITY INFORMATION: 1. Name of residuals processing facility: von Drehle Corporation - Cordova City: Cordova State: NC Zip: 28330- Coordinates: Latitude: 34' 55' 2." Longitude: 79. 49' 42" Datum: NAD 83 Level of accuracy: V Method of measurement: Map County where facility is located: Richmond 2. Facility contact (person familiar with residuals preparation): Name: Mitchell Luckie Title: Process Engineer Mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (256) 496-6530 E-mail address: mitchell.luckie(a-,vondrehle.com FORM: DCAR 06-16 Pagel of 3 3. Is the residual process facility also the generator? ® Yes; ❑ No If No, please specify delivery frequency and quantity of residual to be processed: 4. Length of residuals storage at facility: 5 days (Note: the Division requires minimum 30 days storage in units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.) IV. RESIDUALS QUALITY INFORMATION: 1. Specify how these residuals will be distributed: ❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk); ® other (explain); See Attached Management Plan Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a load capacity of one metric ton or less. 2. Complete the following if residuals are to be mixed with other materials: Type of Materials Amounts to be added er 1.0 dry ton of residuals (dry ton None None 3. Approximate amounts of the residuals received and processed at the facility: 28,500 dry tons per year. 4. Approximate amounts of the final product (processed residuals) to be distributed: 35,000 dry tons per year. 5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and maximum storage times prior to distribution): Residuals are kept on small storage pad prior to loading onto trucks 6. Does the facility have a stormwater management plan? ® Yes; ❑ No Explain whether the treatment and storage areas are under roof or how stormwater runoff will be handled: Due to % solids, free water is not generated, rainwater rewets solids. V. RESIDUALS SOURCE INFORMATION: (Required for all new, renewed, or modified residuals source) Complete and submit the attached Residuals Source Certification and all associated documentation. If `r-� Residuals Source Certification FORM: DCAR 06-16 Page 2 of 3 Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units) attest that this application for has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have reviewed this material and have judged it to be consistent with the proposed design. North Carolina Professional Engincer's Seal, Signature, and Date: Applicant's Certification: The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105. ® Yes ❑ No, Explain; I, Michael Menning Mill Manager (Signature Authority's Name — PLEASE PRINT) (Title) attest that this application for von Drehle Corporation — Cordova. NC Facility _ (Facility Name) has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this application are not completed and that if all required supporting information and attachments are not included, this application package will be returned to me as incomplete. Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine not to exceed $10,000 as well as civil penalties up^to $25,000 per violation. i n /! c Signature: Y Date: FORM: DCAR 06-16 Page 3 of 3 Copy of Existing Permit Water Resources ENVIRONMENTAL QUALITY June 28, 2018 JUSTrN DAWKINS — PLANT MANAGER vON DREHLE CORPORATION 126 FIRST STREET CORDOVA, NORTH CAROLINA 28330 Dear Mr. Dawkins: ROY COOPER Governor MICHAEL S. REGAN .Secretory I INDA CULPEPPER Interim Director Subject: Permit No. WQ0039924 von Drehle Corporation DCAR Distribution of Class A Industrial Byproduct Residuals Richmond County In accordance with your permit application request received April 16, 2018, we are forwarding herewith Permit No. WQ0039924 dated June 28, 2018, to the von Drehle Corporation for the start-up and operation of the subject residuals management program. This permit shall be effective from the date of issuance until May 31, 2023, and shall be subject to the conditions and limitations as specified therein. Please pay particular attention to the monitoring requirements listed in Attachment A. Failure to establish an adequate system for collecting and maintaining the required operational information shall result in future compliance problems. In response to questions raised during the review of the permit, the following responses were given: 1. Q: Condition 11.2. How will the damages be assessed in the event of a "third" party or a contractor? A: Condition III.12 comes into play for part of the answer to this question. If the Permittee knew of the overapplication and did not report it, the Permittee would bear part of the responsibility. If the Permittee knew of the overapplication and did report it, the Permittee would bear none of the responsibility. If the Permittee did not know, then it will become a matter of demonstrating lack of knowledge with a presumption that the Permittee did not know. 2. Q: Condition 11.5. Since von Drehle will have both a Class A and a Class B permit, can Class A pathogen testing be utilized to meet Class B requirements for the Class B permit? A: Yes, as long as they are less than a year old and it passes the Class A requirements. - IP " 1' ot3 big Coinpare State of North Carolina I Environmental Quality Water Resources I Water Quality Permitting Non -Discharge Permitting 1617 Mail Service Center I Raleigh, North Carolina 27699-1617 919-807-6332 Mr. Justin Dawkins June 28, 2018 Page 2 of 2 3. Q: Condition 11.6. Are these setbacks applicable to temporary 60 days' storage and if not are there any additional requirements? Spelling treatment instead of reatment. A: Yes the setbacks would apply to the temporary storage as well. The 60 days' storage would be considered a temporary facility. And thanks for catching spelling error. 4. Q: Condition IV.6f. Application of this material will not be made based on the Agronomic RYE rates. Use of these rates could provide a false justification of over -application. A: This is a very valid point. Condition IV.6.f has been modified to account for a non -limiting nutrient other than nitrogen. If any parts, requirements or limitations contained in this permit are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Unless such demands are made, this permit shall be final and binding. If you need additional information concerning this permit, please contact Troy Doby at (919) 807- 6336 or trov.doby ,ncdenr.goov. Sinc//e--re��l��y,,,,,cc :;?Linda Culpepper, Interim Director Division of Water Resources cc: Richmond County Health Department (Electronic Copy) Fayetteville Regional Office, Water Quality Regional Operations Section (Electronic Copy) Bob Branch, LSS — Branch Residuals & Soils, LLC (Electronic Copy) Laserfiche File (Electronic Copy) Digital Permit Archive (Electronic Copy) Central Files NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION DEPARTMENT OF ENVIRONMENTAL QUALITY RALEIGH DISTRIBUTION OF CLASS A INDUSTRIAL BYPRODUCT RESIDUALS PERMIT In accordance with the provisions of Article 21 of Chapter 143, General Statutes of North Carolina as amended, and other applicable Laws, Rules, and Regulations PERMISSION IS HEREBY GRANTED TO von Drehle Corporation Richmond County FOR THE operation of a residuals management program for von Drehle Corporation and consisting of the distribution of Class A industrial byproduct residuals generated by the approved facility listed in Attachment A with no discharge of wastes to surface waters, pursuant to the application received April 16, 2018, and in conformity with other supporting data subsequently filed and approved by the Department of Environmental Quality and considered a part of this permit. The use and disposal of residuals are regulated under Title 40 Code of Federal Regulations Part 257. This permit does not exempt the Permittee from complying with the federal regulations. This permit shall be effective from the date of issuance until May 31, 2023, and shall be subject to the following specified conditions and limitations: I. SCHEDULES No later than six months prior to the expiration of this permit, the Permittee shall request renewal of this permit on official Division forms. Upon receipt of the request, the Division will review the adequacy of the facilities described therein, and if warranted, will renew the permit for such period of time and under such conditions and limitations as it may deem appropriate. Please note Rule 15A NCAC 02T .0105(d) requires an updated site map to be submitted with the permit renewal application. [15A NCAC 02T .0108(b)(2), 02T .0105(d), 02T .0109] H. PERFORMANCE STANDARDS The subject residuals management program shall be effectively maintained and operated at all times so there is no discharge to surface waters, nor any contravention of groundwater or surface water standards. In the event the facilities fail to perform satisfactorily, including the creation of prolonged nuisance conditions due to improper operation and maintenance, the Permittee shall immediately cease distribution of residuals, contact the Fayetteville Regional Office supervisor, and take any immediate corrective actions. [G.S. 143-215.1] 2. This permit shall not relieve the Permittee of responsibility for damages to groundwater or surface water resulting from the operation of this residuals management program. [15A NCAC 02B .0200, 02L .0100] WQ0039924 Version 1.0 Shell Version 171.103 Page 1 of 10 3. Only residuals generated by the facility listed in Attachment A are approved for distribution in accordance with this permit. [G.S. 143-215.1] 4. Pollutant concentrations in residuals distributed or applied to any land application site shall not exceed the following Ceiling Concentrations or Monthly Average Concentrations (i.e., dry weight basis): Parameter Arsenic Ceiling Concentration (milligrams per kilogram) Monthly Average Concentration (milligrams per kilogram) 75 41 Cadmium 85 39 Copper 4,300 1,500 Lead 840 300 Mercury 57 17 Molybdenum 75 n/a Nickel 420 420 Selenium 100 100 Zinc 7,500 I 27800 [15A NCAC 02T .1105] 5. Residuals that are distributed shall meet Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2). Exceptions to this requirement shall be specified in Attachment A. [ 15A NCAC 02T .1106] 6. Setbacks for treatment and storage facilities shall be as follows: Setback Description Setback _ (feet Habitable residence or place of public assembly under separate ownership or not to 100 be maintained as part of the project site Property lines 50 Private or public water supply 100 Surface waters (streams — intermittent and perennial, perennial waterbodies, and 50 -----1--- 1-• Wells with exception to monitoring wells [15A NCAC 02T. 1108] 100 WQ0039924 Version 1.0 Shell Version 171103 Page 2 of 10 7. Setbacks for Class A land applied bulk residuals shall be as follows: Setback by residual type Setback Description (feet) Liquid Cake' Private or public water supply 100 100 Surface waters (streams — intermittent and perennial, 100 25 erennial waterbodies, and wetlands) Surface water diversions (ephemeral streams, _ T 25 0 waterways, ditches) 25 0 Groundwater lowering ditches (where the bottom of the ditch intersects the SHW Wells with exception to monitoring wells 100 100 Bedrock outcrops 25 0 Unless otherwise noted in Attachment A, "cake" residuals are those that have greater than 15% solids by weight and can be stacked without flowing, as well as can be handled, transported and spread as a solid (e.g., using a backhoe, front end loader, stinger spreader, broadcast spreader or other equipment designed for handling solid materials) without leaving any significant liquid fraction behind. [15A NCAC 02T .l 108] 8. Bulk residuals and other sources of Plant Available Nitrogen (PAN) shall not be applied in exceedance of agronomic rates. Appropriate agronomic rates shall be calculated using expected nitrogen requirements based on the determined Realistic Yield Expectations (RYE) using any of the following methods: a. Division's pre -approved site specific historical data for specific crop or soil types by calculating the mean of the best three yields of the last five consecutive crop harvests for each field. b. North Carolina Historical Data for specific crop and soil types as provided by North Carolina State University Department of Soil Science (Lti.:,Ii'nuti-ients.soil.nesu.edu/vields/index.t)hp). A copy shall be kept on file and reprinted every five years in accordance with Condition IV.6. c. If the RYE cannot be determined using methods (a) or (b) above, the Permittee may use the RYE and appropriate nutrient application rates reported in any of the following documents: i. Crop management plan as outlined by the local Cooperative Extension Office, the North Carolina Department of Agriculture. and Consumer Services, the Natural Resource Conservation Service, or other agronomist. ii. Waste Utilization Plan as outlined by the Senate Bill 1217 Interagency Group - Guidance Document: Chapter 1 (littn://www.nea2r.i;ov/SWC/tecli/doctimetits/9th Guidance Doc 100109.Rt). iii. Certified Nutrient Management Plan as outlined by the Natural Resources Conservation Services (NRCS). These plans must meet the USDA-NRCS 590 Nutrient Management Standards (ftp://ftp-fc.sc.eeov.usda.aovNl10 practice-standardslstandards/590.pdfZ d. If the RYE and appropriate nutrient application rates cannot be determined, the Permittee shall contact the Division to determine necessary action. [I 5A NCAC 02T . 1109(b)(1)(k)] WQ0039924 Version 1.0 Shell Version 171103 Page 3 of 10 The Permittee shall not distribute Class A industrial byproduct residuals that have a sodium adsorption ratio (SAR) of 10 or higher without prior written Division approval. The Permittee may seek approval by demonstrating that the entity accepting the residuals is: aware of the effects of a high SAR content; has agreed on proper residual application rates; and has agreed to operational considerations to ensure that the high SAR content will not adversely impact the receiving sites. Recommendations regarding sodium application rate, soil amendments (e.g., gypsum, etc.) or a mechanism for maintaining site integrity and conditions conducive to crop growth, can be obtained from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist. [15A NCAC 02T .0108(b)(1)] III. OPERATION AND MAINTENANCE REQUIREMENTS 1. The residuals management program shall be properly maintained and operated at all times. The program shall be effectively maintained and operated as a non -discharge system to prevent any contravention of surface water or groundwater standards. [15A NCAC 02T .1110] 2. The Permittee shall maintain an approved Operation and Maintenance Plan (O&M Plan) Modifications to the O&M Plan shall be approved by the Division prior to utilization of the new plan. The O&M Plan, at the minimum, shall include: a. Operational functions; b. Maintenance schedules; c. Safety measures; d. Spill response plan; e. Inspection plan including the following information: i. Names and/or titles of personnel responsible for conducting the inspections; ii. Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the selected location(s) and inspection frequency are representative of the residuals management program; iii. Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event that noncompliance is observed pursuant to the noncompliance notification requirements under the monitoring and reporting section of the permit; f. Sampling and monitoring plan including the following information: i. Names and/or titles of personnel responsible for conducting the sampling and monitoring; ii. Detailed description of monitoring procedures including parameters to be monitored; iii. Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature, flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for residuals to meet pathogen reduction requirements (e.g. facilities that distribute multiple times per year but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to be negatively affected by cold temperatures). [ 15A NCAC 02T .1100] WQ0039924 Version 1.0 Shell Version 171103 Page 4 of 10 3. Upon the Water Pollution Control System Operators Certification Commission's (WPCSOCC) classification of the facility, the Permittee shall designate and employ a certified operator in responsible charge (ORC) and one or more certified operators as back-up ORCs in accordance with 15A NCAC 08G .0201. The ORC or his back-up shall visit the facilities in accordance with 15A NCAC 08G. 0204, or as specified in the most recently approved O&M plan (i.e., see Condition 111.2.), and shall comply with all other conditions of 15A NCAC 08G. 0204. For more information regarding classification and designation requirements, please contact the Division of Water Resources' Protection and Enforcement Branch at (919) 707-9105. At the time of this permit issuance, a certified ORC is not required for the subject Distribution of Class A Residuals program. [15A NCAC 02T .0117] 4. When the Permittee land applies bulk residuals. a copy of this permit and a copy of O&M Plan shall be maintained at the land application sites during land application activities. [15A NCAC 02T .0108(b)(1)] 5. When the Permittee transports or land applies bulk residuals, the spill control provisions shall be maintained in all residuals transport and application vehicles. [15A NCAC 02T .l 110] 6. When the Pennittee land applies bulk residuals, adequate measures shall be taken to prevent wind erosion and surface runoff from conveying residuals from the land application sites onto adjacent properties or into surface waters. [G.S. 143-215.1 ] 7. When the Permittee land applies bulk residuals, a suitable vegetative cover shall be maintained on land application sites onto which residuals are applied, or application shall be in accordance with the crop management plan outlined by the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, or an agronomist and as approved bythe Division. [15ANCAC 02T .1109(b)(1)] 8. Bulk residuals shall not be land applied under the following conditions: a. If the residuals are likely to adversely affect a threatened or endangered species listed under section 4 of the Endangered Species Act or its designated critical habitat; b. If the application causes prolonged nuisance conditions; c. If the land fails to assimilate the bulk residuals or the application causes the contravention of surface water or groundwater standards; d. If the land is flooded, frozen or snow-covered, or is otherwise in a condition such that runoff of the residuals would. occur: e. Within the 100-year flood elevation, unless the bulk residuals are injected or incorporated within a 24-hour period following a residuals land application event; f. During a measurable precipitation event (i.e., greater than 0.01 inch per hour), or within 24 hours following a rainfall event of 0.5 inches or greater in a 24-hour period; g. If the slope is greater than 10% for surface applied liquid residuals, or if the slope is greater than 18% for injected or incorporated bulk liquid residuals; h. If the land does not have an established vegetative cover unless the residuals are incorporated or injected within a 24-hour period following a residuals land application event. Any field that is in a USDA no -till program shall be exempted from meeting this vegetative cover requirement; i. If the vertical separation between the seasonal high water table and the depth of residuals application is less than one foot; j. If the vertical separation of bedrock and the depth of residuals application is less than one foot, k. Application exceeds agronomic rates. [I 5A NCAC 02T. 1109] WQ0039924 Version 1.0 Shell Version 171103 Page 5 of 10 The Permittee shall notify all third -party entities receiving bulk distributed Class A industrial byproduct residuals that land application activities occurring on the third-party's property shall meet the requirements in 15A NCAC 02T .1108(b)(1) and 02T .1109(b) (i.e., Conditions II.8. and III.8., respectively). [15A NCAC 02T .1103(5)] 10. All residuals shall be adequately stored to prevent untreated leachate runoff. The finished product may be placed on a concrete pad, placed under shelter or physically covered until it is distributed to a third - party entity. If bulk residuals are to be applied, the residuals may be staged at the application site for up to 30 days for biological residuals, and 60 days for non -biological residuals. If an alternate storage site is used, approval must be obtained from the Division. [15A NCAC 02T .0108(b)(1)] 11. A label shall be affixed to the bag or other container in which residuals are sold or given away for land application, or an information sheet shall be provided to the person who receives Class A residuals. At a minimum, the label or information sheet shall contain the following: a. The name and address of the person who prepared the residuals; b. A statement that residual land application is prohibited except in accordance with the instructions on the label or information sheet; c. A statement identifying that this material shall be prevented from entering any public or private water supply source (including wells) and any surface water (e.g., stream, lake, river, wetland, etc.); d. A statement that the residuals shall be applied at agronomic rates and recommended rates for its intended use. [ 15A NCAC 02T. I 109(a)] 12. The Permittee shall not distribute bulk residuals to any person or entity known to be applying residuals contrary to the conditions of this permit. The Permittee shall report to the Fayetteville Regional Office as per reporting conditions under Condition IV.8. any person or entity known to be applying residuals contrary to the condition of this permit. [15A NCAC 02T.] 103(a)] WQ0039924 Version 1.0 Shell Version 171103 Page 6 of 10 IV. MONITORING AND REPORTING REQUIREMENTS Any Division -required monitoring (including groundwater, plant tissue, soil and surface water analyses) necessary to ensure groundwater and surface water protection shall be established, and an acceptable sample reporting schedule shall be followed. [15A NCAC 02T .0108(c)] Residuals shall be analyzed to demonstrate they are non -hazardous under the Resource Conservation and Recovery Act (RCRA). Residuals that tests or is classified as a hazardous or toxic waste under 40 CFR Part 261 shall not be used or disposed under this permit. The analyses [corrosivity, ignitability, reactivity, and toxicity characteristic leaching procedure (TCLP)J shall be performed at the frequency specified in Attachment A, and the Permittee shall maintain these results for a minimum of five years. Any exceptions .from the requirements in this condition shall be specified in Attachment A. The TCLP analysis shall include the following parameters (the regulatory level in milligrams per liter is in parentheses): Arsenic (5.0) 1.4-Dichlorobenzene (7.5) Nitrobenzene (2.0) Barium (100.0) 1,2-Dichloroethane (0.5) Pentachlorophenol (100.0) Benzene (0.5) 1,1-Dichloroethylene (0.7) Pyridine (5.0) Cadmium (1.0) 2,4-Dinitrotoluene (0.13) Selenium (1.0) Carbon tetrachloride (0.5) Endrin (0.02) Silver (5.0) Chlordane (0.03) Hexachlorobenzene (0.13) Heptachlor (and its hydroxide) (0.008 Tetrachloroethylene (0.7) Chlorobenzene (100.0) Toxaphene (0.5) Chloroform (6.0) Hexachloro-1,3-butadiene (0.5) Trichloroethylene (0.5) Chromium (5.0) Hexachloroethane (3.0) 2,4,5-Trichlorophenol (400.0) m-Cresol (200.0) • Lead (5.0) 2,4,6-Trichlorophenol (2.0) o-Cresol (200.0) Lindane (0.4) 2,4,5-TP (Silvex) (1.0) p-Cresol (200.0) Mercury (0.2) I Methoxychlor (10.0) Methyl ethyl ketone (200.0) Vinyl chloride (0.2) Cresol (200.0) 2,4-D (10.0) Once the residuals have been monitored for two years at the frequency specified in Attachment A, the Permittee may submit a permit modification request to reduce the frequency of this monitoring requirement. In no case shall the monitoring frequency be less than once per permit cycle. [15A NCAC 13A .0102(b), 02T .1101, 02T .1105] WQ0039924 Version 1.0 Shell Version 171103 Page 7 of 10 3. An analysis shall be conducted on the residuals from each source generating facility at the frequency specified in Attachment A, and the Permittee shall maintain the results for a minimum of five years. The analysis shall include the following parameters: Aluminum Mercury Potassium Selenium Ammonia -Nitrogen Molybdenum Arsenic Nickel Sodium Cadmium Nitrate -Nitrite Nitrogen Sodium Adsorption Ratio (SAR) Calcium Copper Lead Percent Total Solids TKN i pH Zinc W — Phosphorus Magnesium � Plant Available Nitrogen (by calculation) [15A NCAC 02T .1101] 4. Residuals shall be monitored for compliance with pathogen reduction requirements at the frequency specified in Attachment A, and at the time indicated in the sampling and monitoring sections of the approved O&M plan. The required data shall be specific to the stabilization process utilized, and sufficient to demonstrate compliance with the Class A pathogen reduction requirements in 15A NCAC 02T .1106 (a) and (b)(2) shall be met. Any exceptions from the requirements in this condition shall be specified in Attachment A. [15A NCAC 02T .1106, 02T .l 107, 02T .l l 11(c)j 5. Laboratory parameter analyses shall be performed on the residuals as they are distributed, and shall be in accordance with the monitoring requirements in 15A NCAC 02B .0505. [15A NCAC 02B .0505] 6. The Permittee shall maintain records tracking all bulk residual distribution or land application events performed by the Permittee. At a minimum, these records shall include the following: a. Source of residuals; b. Date of distribution/land application; c. Name and address of recipient of residuals; d. Volume of residuals distributed to each recipient; e. Intended use of residuals; f. If land application events performed by the Permittee: i. When the agronomic rate is on the basis of Nitrogen, then the Nitrogen Application Rate based on RYES (if using data obtained from the North Carolina State University Department of Soil Science Website, the printout page shall be kept on file and reprinted every five years). ii. When the agronomic rate is on the basis of some other nutrient than Nitrogen, then this shall be included as part of the Operations & Maintenance Plan required in Condition HI.2. A set of calculations shall be performed to show that the residuals are being applied at an agronomic rate on the basis of this limiting nutrient. These records shall be kept for a minimum of five years and shall be available for inspection. [15A NCAC 02T .0108(a)] WQ0039924 Version 1.0 Shell Version 171103 Page 8 of 10 7. Three copies of an annual report shall be submitted on or before March 11. The annual report shall meet the requirements described in the Instructions for Residuals Application Annual Reporting Forms. Instructions for reporting and annual report forms are available at http://'deL.nc.L,ov/about/divisions/water-resourcess/�ater-resources-perm its!wastewater-branch/non- discharue-termitting-unit/reporting-forms, or can be obtained by contacting the Non -Discharge Permitting Unit directly. The annual report shall be submitted to the following address: Division of Water Resources Information Processing Unit 1617 Mail Service Center Raleigh, North Carolina 27699-1617 [15A NCAC 02T .I I I l(a)] 8. Noncompliance Notification The Pennittee shall report by telephone to the Fayetteville Regional Office, telephone number (910) 433-3300, as soon as possible, but in no case more than 24 hours or on the next working day following the occurrence or first knowledge of the occurrence of any of the following: a. Distribution of residuals abnormal in quantity or characteristic. b. Any failure of the distribution program resulting in a release of material to surface waters. c. Any time self -monitoring indicates the facility has gone out of compliance with its permit limitations. d. Any process unit failure, due to known or unknown reasons, rendering the facility incapable of adequate residual treatment. e. Any spill or discharge from a vehicle or piping system during residuals transportation. Any emergency requiring immediate reporting (e.g., discharges to surface waters, imminent failure of a storage structure, etc.) outside normal business hours shall be reported to the Division's Emergency Response personnel at telephone number (800) 662-7956, (800) 858-0368, or (919) 733-3300.Persons reporting such occurrences by telephone shall also file a written report in letter form within five days following first knowledge of the occurrence. This report shall outline the actions taken or proposed to betaken to ensure that the problem does not recur. [15A NCAC 02T .0105(1), 02T .0108(b)(1)] V. INSPECTIONS 1. The Permittee shall provide adequate inspection and maintenance to ensure proper operation of the subject facilities and shall be in accordance with the approved O&M Plan. [ 15A NCAC 02T .0l 08(b)] 2. Prior to each bulk residuals distribution event, the Pennittee or his designee shall inspect the residuals storage, transport and distribution facilities to identify malfunctions, facility deterioration and operator errors that could result in discharges to the environment, a threat to human health or a public nuisance. The Pennittee shall maintain an inspection log that includes, at a minimum, the date and time of inspection, observations made, and any maintenance, repairs, or corrective actions taken. The Pennittee shall maintain this inspection log for a period of five years from the date of inspection, and this log shall be made available to the Division upon request. [15A NCAC 02T .0108(b)] 3. Any duly authorized Division representative may, upon presentation of credentials, enter and inspect any property, premises or place on or related to the distribution sites or facilities permitted herein at any reasonable time for the purpose of determining compliance with this permit; may inspect or copy any records required to be maintained under the terms and conditions of this permit; and may collect groundwater, surface water or leachate samples. [G.S. 143-215.3(a)(2)] WQ0039924 Version 1.0 Shell Version 171103 Page 9 of 10 VI. GENERAL CONDITIONS 1. Failure to comply with the conditions and limitations contained herein may subject the Permittee to an enforcement action by the Division in accordance with North Carolina General Statutes 143-215.6A to 143-215.6C. [G.S. 143-215.6A to 143-215.6C] 2. This permit shall become voidable if the residuals distribution events are not carried out in accordance with the conditions of this permit. [15A NCAC 02T .0110] 3. This permit is effective only with respect to the nature and volume of residuals described in the permit application and other supporting documentation. [G.S. 143-215.1] 4. The issuance of this permit does not exempt the Permittee from complying with any and all statutes, rules, regulations, or ordinances, which may be imposed by other jurisdictional government agencies (e.g., local, state, and federal). Of particular concern to the Division are applicable river buffer rules in 15A NCAC 02B .0200; erosion and sedimentation control requirements in 15A NCAC Chapter 4 and under the Division's General Permit NCGO10000; any requirements pertaining to wetlands under 15A NCAC 02B .0200 and 02H .0500; and documentation of compliance with Article 21 Part 6 of Chapter 143 of the General Statutes. [ 15A NCAC 02T .0105(c)(6)] In the event the residuals program changes ownership or the Permittee changes his name, a formal permit modification request shall be submitted to the Division. This request shall be made on official Division forms, and shall include appropriate documentation from the parties involved and other supporting documentation as necessary. The Permittee of record shall remain fully responsible for maintaining and operating the residuals program permitted herein until a permit is issued to the new owner. [15A NCAC 02T .0104] 6. This permit is subject to revocation or unilateral modification upon 60-day notice from the Division Director, in whole or part for the requirements listed in 15A NCAC 02T .0 l 10. [15A NCAC 02T .0110] 7. Unless the Division Director grants a variance, expansion of the permitted residuals program contained herein shall not be granted if the Permittee exemplifies any of the criteria in 15A NCAC 02T .0120(b). [15A NCAC 02T .0120] 8. The Permittee shall pay the annual fee within 30 days after being billed by the Division. Failure to pay the annual fee accordingly shall be cause for the Division to revoke this permit. [15A NCAC 02T .0105(e)(3)] Permit issued this the 28" day of June 2018 NORTH CAROLINA ENVIRONMENTAL MANAGEMENT COMMISSION ?Linda Culpepper, Interim Director Division of Water Resources By Authority of the Environmental Mt"hagi n ent Commission Permit Number WQ0039924 WQ0039924 Version 1.0 Shell Version 171103 Page 10 of 10 0 C 0 d E a z Fv5 u a O z •.-; N cl; 4 vi E 11 o 95 U ti 1.6 ca 2 c 9 o. d E d N � O T C a a E w a .:w Len Q. 0 N C• L i e � _ 0 cc 03 o � E w a r. y C O v 3 •� y L T y � 0 L � C 1 a a on 'o = on •L e c 9 E L W 7 y O E y �N a y a E fl {. 40. O O R 03 O O Ir. � L .a a ea • re T.� m •o d C � O ob u w g+ E • L a. t m u E w a o a •v = w W L 6i .1 r QF W L _ e0 > a+ C V N a L O G C O L y d L y d � L E •� a w e ea r O ROY COOPER Governor DIONNE DELLPGATTI Secretory S. DANIEL SMITH Director JUSTIN DAIWKINS — PLANT MANAGER VON DREHLE CORPORATION 126 FIRST STREET CORDOVA, NORTH CAROLINA 28330 Dear Mr. Dawkins NORTH CAROLINA Environmental Quality April 8, 2021 Subject: Permit No. WQ0039924 von Drehle Corporation DCAR Attachment A Certification Richmond County In accordance with your pen -nit major modification request received February 1, 2021, we are forwarding herewith a modified Attachment A certified April 8, 2021, to the von Drehle Corporation for the subject residuals management program. Modifications to the subject Attachment are as follows: Increasing the permitted dry tonnage of residuals from the von Drehle Corporation WWTP from 16,499 dry tons per year (DT/yr) to 35,000 DT/yr. The modified Attachment A shall be effective from the date of certification until May 31, 2023 (i.e., expiration date of the current permit), shall void Attachment A of Pen -nit No. WQ0039924 issued June 28, 2018, and shall be subject to the conditions and limitations as specified therein, as well as those specified in the above -referenced pennit. Please replace Attachment A of Permit No. WQ0039924 that was issued June 28, 2018 with the modified Attachment A. Please note that the Permittee shall submit a renewal application no later than December 2, 2022. If any parts, requirements or limitations contained in this certification are unacceptable, the Permittee has the right to request an adjudicatory hearing upon written request within 30 days following receipt of this permit. This request shall be in the form of a written petition, conforming to Chapter 150B of the North Carolina General Statutes, and filed with the Office of Administrative Hearings at 6714 Mail Service Center, Raleigh, NC 27699-6714. Otherwise, this certification shall be final and binding. If you need any additional infonriation concerning this matter, please contact Erick Saunders at (919) 707-3659 or erickson.saunders umcdenr.lrov. Sincerely, S. Daniel Smith, Director Division of Water Resources 1 cc: Richmond County Health Department (Electronic Copy) Fayetteville Regional Office, Water Quality Regional Operations Section (Electronic Copy) North Carolina Department of Envkronmental Quality I Division of Water Resources 512 North Salisbury Street 1617 Mail Service Center I Raleigh, North Carolina 27699 1611 919.707,9000 Mr. Justin Dawkins April 8, 2021 Page 2 of 2 Bob Branch, LSS — Branch Residuals & Soils, LLC (Electronic Copy) Laserfiche File (Electronic Copy) Digital Permit Archive (Electronic Copy) A C L •Q � `r Q y •O.r � � ^ p Q u a 7 .o n yt p u u z k. U i � v c p a y u � u .o ai a a i O L i p Qp Y v; tn M �Q c ci ci pq AG v N s � c H c 5 C U v z fs, L1 C �x. C L O F, f`1 2i E■ N x x x •� a., � c c � O c L v O O O kn G i O Q G v �/ O r nl o M � A v Al n C = o d o 0 v v o a CA G v CD nl d v Al H A� a 7 a C O C � 7 > c p "C v CJ .�• v. 61 1= 7 .O C C {u C14 .0 o u E s• ;� c Q � F•+ a v U = z c a o a U tz g a a ca 3 x e Q o an e U on C G p > c7 O O >3 .yam. C u u C a u s ^c a� 6 } G aj N u R y •C" � v �0. C F •� i 7 Z' L c N 2 .yam.. ecj2 c S ac v a-9 c c ON M •� Ol C L La 3 SECTION II RESIDUALS SOURCE CERTIFICATION ATTACHMENT - FIBER CLAY State of North Carolina DWR Department of Environmental Quality Division of Water Resources Division of Water Resources RESIDUALS SOURCE CERTIFICATION INSTRUCTIONS FOR FORM: RSC 06-16 Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional information requested. Failure to submit all of the required items will lead to additional processing and review time for the permit application. Unless otherwise noted. the Applicant shall submit one original and two copies of the application and supporting documentation For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit General — This certification provides detailed information of residuals source generating facility and its residuals quality for land application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without a corresponding application form (FORM: RLAP 11-15, FORM: DCAR 11-15, or FORM: SDR 11-15). Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed below. A. Residuals Source Certification (FORM: RSC 11-15): ® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-15) form. Please do not make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer. ® For new or renewed permits, submit a separate certification for each source facility. ❑ For modified permits, submit a separate certification for only those facilities that are affected by the proposed modification. ® Complete the residuals source facility summary page. List all new, renewed, or modified facilities. B. Residuals Source -Generating Facility Information: ® For each source facility, attach the following: ® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for Residuals Land Application Permits". ® Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals are to be generated, treated, processed, and stored at the facility. ® Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item I. 8. Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of the permit. In addition, ensure that this amount is equivalent to that which is actually to be land applied, distributed, and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during processing. ® Sampling plan - A detailed sampling plan for the residuals source -generating facility. Ensure that the plan identifies sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to be used. In addition, ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as they are to be land applied, distributed, and/or disposed. C. Residuals Quality Information: ® For each source facility, attach the following: ® Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification. ® Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector attraction reduction requirements. ❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please attach analytical results of residuals generated from a similar facility along with the description of similarities of the two facilities. INSTRUCTIONS FOR FORM: RSC 06-16 Page 1 of 1 v o �+ a v a a y O F sue. A � a O O C3 L Vj L 6� .0 z y v a b aa O pO O U U R z � o b U � o b x0 v � �+ L Q u C f7i � y a v� U nWR Division of Water Resources State of North Carolina Department of Environmental Quality Division of Water Resources RESIDUALS SOURCE CERTIFICATION FORM: RSC 06-16 I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.): 1. Facility Name: von Drehle Corporation 2. Facility permit holder is: ❑ Federal, ❑ State, ❑ Local Government, or ® Private. Facility permit issued by: ❑ Div. of Water Resources, ❑ Div. of Environmental Health, or ❑ Other (explain: �. 3. Facility contact person and title: Mitchell Luckie, ORC Complete mailing address: 126 First Street City: Cordova State: NC Zip: 28330- Telephone number: (910) 410-9131 E-mail address: mitchell.luckie@,vondrehle.com 4. Facility physical address: 126 First Street. City: Cordova State: NC Zip: 28330- Coordinates: Latitude: 34° 55' 2.73" Longitude: 79' 49' 42.77" Datum: NAD 83 Level of accuracy: F Method of measurement: Mai) 5. Purpose of the facility: ❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater, ❑ treatment of potable water, ® treatment of 100% industrial wastewater, ❑ treatment of industrial wastewater mixed with domestic wastewater, (approximate percentages: % industrial and _ % domestic) ❑ other (explain: ). 6. Does the facility have an approved pretreatment program: ❑ Yes ® No 7. Facility permitted/design flow: 0.395 MGD and facility average daily flow: 0.272 MGD 8. Average amount of residuals being generated at this facility 35,000 dry tons per year. 9. Specify the following regarding treatment and storage volumes available at the facility: Type and volume of residuals treatment: Separation and Belt Press Type and volume of residuals storage (i.e., outside of residuals treatment units): Storage pad 150 cubic yards II. RESIDUALS QUALITY INFORMATION (See Instruction C.): 1. Specify if residuals are regulated under: ❑ 40 CFR Part 503 or ® 40 CFR Part 257. Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are regulated under 40 CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257. 2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as: ❑ Biological ® Non -Biological FORM: RSC 06-16 Page 1 of 5 Note: Biological residuals are residuals that have been generated during the treatment of domestic wastewater, animal processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems). 3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non -hazardous under RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat 100% non -municipal, domestic wastewater only) a. Are the residuals listed in 40 CFR §261.31-§261.33: ❑ yes ® no. If yes, list the number(s): b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21- 261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and reactivity: Laboratory: Environmental Chemists Inc. and Date of analysis: Feb 09, 2022 Passed corrosivity test: ® yes ❑ no. pH: s.u. (2 < pH < 12.5) Passed ignitability test: ® yes ❑ no. Flashpoint: <0.8 mm/sec (> 140°F) Passed reactivity test: ® yes ❑no. HCN: 1.36 mg/kg (<250) & H2S: 0.56 mg/kg (<500) TCLP Parameter Limit (mg/1) Result (mg/1) TCLP Parameter Limit (mg/1) Result (mg/1) Arsenic 5.0 <1.00 Hexachlorobenzene 0.13 <0.05 Barium 100.0 <1.00 Hexachloro-1,3-Butadiene 0.5 <0.05 Benzene 0.5 <0.01 Hexachloroethane 3.0 <0.05 Cadmium 1.0 <1.00 Lead 5.0 <1.00 Carbon Tetrachloride 0.5 <0.01 Lindane 0.4 <0.0005 Chlordane 0.03 <0.02 Mercury 0.2 <0.0002 Chlorobenzene 100.0 <0.01 Methoxychlor 10.0 <0.0005 Chloroform 6.0 <0.01 Methyl Ethyl Ketone 200.0 <0.05 Chromium 5.0 <1.00 Nitrobenzene 2.0 <0.05 m-Cresol 200.0 <0.05 Pentachlorophenol 100.0 <0.05 o-Cresol 200.0 <0.05 Pyridine 5.0 <0.05 p-Cresol 200.0 <0.05 Selenium 1.0 <1.00 Cresol 200.0 <0.05 Silver 5.0 <1.00 2,4-D 10.0 <0.003 Tetrachloroethylene 0.7 <0.01 1,4-Dichlorobenzene 7.5 <0.05 Toxaphene 0.5 <0.05 1,2-Dichloroethane 0.5 <0.01 Trichloroethylene 0.5 <0.01 l,l-Dichloroethylene 0.7 <0.01 2,4,5-Trichlorophenol 400.0 <0.05 2,4-Dinitrotoluene 0.13 <0.05 2,4,6-Trichlorophenol 2.0 <0.05 Endrin 0.02 <0.0005 2,4,5-TP (Silvex) 1.0 <0.003 Heptachlor and its Hydroxide 0.008 <0.0005 Vinyl Chloride 0.2 <0.01 FORM: RSC 06-16 Page 2 of 5 4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105. a. For Distrihution/Land Application: Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: Waypoint Analytical and Date of analysis: July 26, 2022 Parameter Ceiling Concentration Limits (ClassA & C1assB) (mglkg) Monthly Average Concentration Limits (Class A Only) (mglkg) Result (mglkg) Arsenic 75 41 <1.56 Cadmium 85 39 <0.312 Copper 4,300 1,500 27.0 Lead 840 300 2.08 Mercury 57 17 <0.452 Molybdenum 75 n/a 3.64 Nickel 420 420 2.08 Selenium 100 100 <1.56 Zinc 7,500 2,800 93.8 b. For Surface Disposal Unit (landrll): Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following metal parameters: Laboratory: and Date of analysis: Distance from Disposal Unit to Boundary to Closest Property Line (meters, check one) Arsenic (mg/k-g) Chromium (mg/kg) Nickel (mg/kg) ❑ > 0 but < 25 30 200 210 ❑ > 25 but < 50 34 220 240 ❑ > 50 but < 75 39 260 270 ❑ > 75 but < 100 46 300 320 ❑ > 100 but < 125 53 360 390 ❑ > 125 62 450 420 Result (mg/kg) FORM: RSC 06-16 Page 3 of FORM: RSC 06-16 Page 4 of 5. Nutrient/Micronutrient Determination: Complete the following: a. Total solids: 32.1 %. b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and micronutrient parameters: Laboratory: Waypoint Analytical and Date of analysis: July 26, 2022 Parameter Result (mg/k-9) Aluminum 1680.00 Ammonia -Nitrogen 330.00 Calcium 110,000.00 Magnesium 1,400.00 Nitrate -Nitrite Nitrogen <3.12 pH (Standard Unit) 7.80 Phosphorus 127.00 Potassium 66.70 Sodium 595.00 Total Kjeldahl Nitrogen 2,830.00 c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.28 [Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity and conditions conducive to crop growth]. d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals: 0.40 %. This rate is a (check one): ® default value, or ❑ actually established. If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical justification as to why the selected default value is appropriate to be applied to these residuals: N/A e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table: Application Method First (15`) Year PAN Five -Year Maximum Adjusted PAN (mg1kg) (mg/kg) Surface 1,168 1,668 Injection/Incorporation 1,333 1,833 6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide the results of the latest analyses: FORM: RSC 06-16 Page 5 of 7. Pathogen Reduction: Per 15A NCAC 02T.11061 specify how residuals will meet the pathogen reduction requirements: a. For Distribution/Land Application of Class A or Equivalent: ® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids, or ® A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids. AND one of the followings (except for non -biological residuals): ❑ Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance. ❑ Alternative 2 [15A NCAC 02T.I 106(b)(3)(B)] - Alkaline Treatment. ❑ Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova. ❑ Alternative 5 [15A NCAC 02T.I 106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP). Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ thermophilic aerobic digestion, ❑ beta ray irradiation, ❑ gamma ray irradiation, or ❑ pasteurization. b. For Land Application of Class B: ❑ Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration. ❑ Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP). Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion, ❑ composting, or ❑ lime stabilization. c. For Surface Disposal: ❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above. ❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above. ❑ Exempt -If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.1106(a)(2)]. ❑ Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. 8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements: ❑ Alternative 1 [15A NCAC 02T. I 107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion). ❑ Alternative 2 [15A NCAC 02T.I 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion). ❑ Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion). ❑ Alternative 4 [15A NCAC 02T.I 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion). ❑ Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes. ❑ Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization. ❑ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals. ❑ Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals. ❑ Alternative 9 [15A NCAC 02T.I 107(a)(9)] - Injection. ❑ Alternative 10 [15A NCAC 02T.I 107(a)(10)] - Incorporation. ❑ Alternative for Surface Disposal Units Only - Soil/Other Material Cover [ 15A NCAC 02T. 1107(b)(2)]. ® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution. Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically occur when these residuals are applied and left on the land surface. FORM: RSC 06-16 Page 6 of Vicinity Map .... A7�� V-a w� r � r � 1c 6G s t 3 0 q ,m 1 Von Drehle Corporation �a Cordova ti e s� y�r 95 r OV %*V 04 CIO °4 s, 'bs <1 as s o n 3 r 4 O� omen Cir � H tz i "tli U Carla C` Trent S t G,cc ca t Sources: Esri, HERE, Del-orrx USGS Intermap INCREMENT P, t NRCan, Esri Japan, METI, Esri China (Hong Kong), Esn Korea Esr t (Thailand). Mapmylndia, NGCC, © OpenStreetMap contributors and the t GIS User Community Q' SCALE: 1 "= 1,500 ft Triple S Farms Facility CHECKED BY: RTB Land Application Program pp g Vicinity DR -AWN BY: RTB BRANCH von Drehle Corporation Map RE+ SIDUAS DATE: 1 8, 2021 SOLILS, LLC Project No. 2014-110 Process Flow Diagram and Narrative FIBER CLAY PROCESS NARRATIVE Recycled paper in bales is released and placed in the pulping process. There, mixed with water, the recycled paper is reduced to pulp. The pulp is sent through a de -trashing system, where large metals and plastics such as plastic bags or soda cans are removed. These large rejects are deposited in an indoor pit to be removed to landfill. From here, the accepted material is sent to a holding chest where it is fed into the pulp cleaning and screening system. The first stage of the cleaning and screening system is responsible for the removal of dense contaminants such as glass and small metal pieces such as staples. The next stage is the coarse screening stage which removes smaller plastics that are slightly larger than .06 inches in diameter; these plastics, as well as the glass and small metals, are ultimately deposited in the previously mentioned indoor pit. Following this stage is the centrifugal forward cleaning stage. In this stage, lighter, but still relatively dense particles, such as sand and dirt, are separated by centrifugal force from pulp and ultimately rejected to the mill sump. The final stage of cleaning and screening is the fine screening stage. In the fine screening stage, very small (slightly larger than. 005 inches), light contaminants s u c h a s s t i c k i e s, ink particles and smaller dirt particles are removed and ultimately sent to the mill sump as well. From the mill sump, these rejected solids are sent to a Krofta DAF clarifier where they are coagulated, floated and skimmed off the surface and sent to a belt press where it is dewatered to approximately 40% solids and deposited onto the fiber clay pad outside. The accepted material from the fine screening stage is sent to a Variosplit washing system where through a dewatering process of the pulp, very fine ash and fiber fines are removed. These rejects are sent to a Tauro DAF clarifier where they are removed in a similar fashion as with the Krofta and sent to the belt press to be dewatered and deposited on the fiber clay pad. Accepted pulp from the washing stage is sent to a screw press for further dewatering, and the pulp is then fed into a high temperature dispersion system, where any remaining small contaminants such as dirt and stickies are pulverized to a size smaller than what can be seen with the human eye. The pulp is also mixed with a bleaching agent at high temperature and is sent to a bleaching tower to allow the bleaching process to take place and increase pulp brightness. The pulp is then mixed with water and diluted to 5% solids and sent to the paper machines. At the paper machines, the pulp is applied to a press felt, while simultaneously being dewatered with a poly wire belt; a sheet of paper is formed, which is pressed, dried, and rolled up to be shipped. In this process, more ash and fines are removed and are ultimately sent to a Megacell DAF clarifier where, as with the other DAF units, a fiber clay blanket is formed, sent to the belt press and then the fiber clay pad. The water from each of these DAF units is generally re -used in the process, with the excess being discharged to the City of Rockingham wastewater treatment system. Following is the process flow schematic diagram for the water and solids in von Drehle Corporation Cordova's Paper Process. Von Drehle Paper Process Flowchart aste Paperl_J Pulper Bails in Dump L accepts I Detrasher Tank Scavenger accepts rejects Coarse Screen creene accepts Ho Cleaner accepts :Coarsereen accepts Cleaners accepts Fine Screens accepts Washer accepts Screw Press accepts �ate� accepts Drum Screen rejects Tailings reje� Pit Landfill accepts rejects Mill Krofta rejects Sludge 'um OAF Press accepts Water to City or return to Process IBleach Tower egacel OAF rejects Paper Machine Product Belt Press Fiber Clay to Land Application or Landfill Justification of Residuals Production Rate h1il. I�T1 M�C�7TI ����►[�] ai : � .�1i1:11[.�7��J7i���[��i:7:11�1 � von Drehle Corporation produces approximately 28,500 dry tons of the Fiber Clay annually. In order to account for variability, the dry ton permit limit will be set at 35,000 dry tons. Sampling Plan FIBER CLAY SAMPLING PLAN von Drehle Fiber Clay is transported by conveyor from the belt presses to the storage pad in the back at von Drehle's facility in Cordova. Fiber Clay will be distributed by placement onto sealed trailers that will be routed to one of several marketing sites, non-specific receiver sites or to the landfill as daily cover. Based on the amount of residual to be distributed, von Drehle Fiber Clay will be sampled monthly from the belt presses. Representative samples of von Drehle Fiber Clay will be collected and composited prior to the beginning of the preceding monthly cycle so that data will be made available prior to that distribution period. Seven independent grab samples will be collected monthly for Salmonella analysis. These samples will be immediately placed on ice and delivered to a lab certified in the testing protocol. Since there are no labs that are certified for the state of North Carolina for the Salmonella testing, at a minimum this lab has certification such as Nation Environmental Laboratory Accreditation Conference (NELAC). If at an any point, North Carolina has a lab that becomes accredited and is close enough to meet the necessary hold times, they will be used. All samples will be sent to qualified laboratories that are familiar with the environmental sample preparation and standards required. Annually, a residuals solid sample will be analyzed for toxicity characteristics leaching procedure (TCLP). TCLP parameters are listed below: Arsenic Cadmium Chlorobenzene o-Cresol Cresol 1,2-Dichloroethane Endrin Hexachloroethane Lindane Methyl ethyl ketone Pyridine Tetrachloroethylene 2,4,5-Trichlorophenol Vinyl chloride Barium Benzene Carbon tetrachloride Chlordane Chloroform Chromium m-Cresol p-Cresol 2, 4-D 1,4-Dichlorobenzene 1, 1 -Dichloroethylene 2,4-Dinitrotoluene Hexachlorobenzene Heptachlor (and its hydroxide) Lead Hexachloro-1,3-butadiene Mercury Methoxychlor Nitrobenzene Pentachlorophenol Selenium Silver Toxaphene Trichloroethylene 2,4,6-Trichlorophenol 2,4,5-TP (Silvex) Monthly (prior to the end of the preceding monthly period,) a composite Fiber Clay residual solid sample will be collected and analyzed for: Cadmium, Copper, Lead, Nickel, Zinc, Aluminum, Ammonia — Nitrogen, Nitrate -Nitrite, Nitrogen, % Total Solids, pH, Phosphorus, Potassium, TKN, and Calcium Carbonate Equivalency (CCE). From this information, the Plant Available Nitrogen (PAN) and Agricultural Lime Equivalency (ALE) will be calculated. This will be the basis for the application rates that will be used in the next monitoring period and changes will be made to the - product label to reflect the most recent analytical data. Residual Analytical Reports Facility: Source: Location: Contractor: Type of Analysis: Report No: Date Sampled: Date Reported: Reporting Period: von Drehle Corporation Fiber Clay Cordova, NC Bio-Nomic Services Industrial Residual Solids 22-195-0047 7/13/2022 7/26/2022 July -Aug 2022 Parameter % PPM Dry Weight EPA Monthly Limits Solids 32.10 Nitrogen (TKN) 0.283 2,830.000 Phosphorus 0.01270 127.000 Potassium 0.007 66.700 Sulfate Calcium 11.000 110,000.000 Magnesium 0.144 1,440.000 Sodium 0.060 595.000 Iron --- 1,140.000 Aluminum --- 1,680.000 Manganese --- Copper --- 27.000 1,500 Zinc --- 93.800 2,800 Ammonia Nitrogen 0.033 330.000 Nitrate N / Nitrite N --- 3.120 Cadmium --- 0.312 39 Chromium --- 1,200 Nickel --- 2.080 420 Lead --- 2.080 300 Arsenic --- 1.560 41 Mercury --- 0.452 17 Selenium --- 1.560 100 pH 7.800 Calcium Carbonate Eq. 28.100 281,000.000 Organic Nitrogen 0.250 Molybdenum 3.640 75 Volatile Solids Boron TOC 0.000 Industrial Residual Solids Fiber Clay Cordova, NC Bio-Nomic Services July -Aug 2022 Date Reported: 7/26/2022 Report No: 22-195-0047 Note All Units in Pounds Per Dry Ton Macro Nutrients Physical Characteristics PAN Surf. 2.336 PAN Inj. 2.666 P 0.254 K 0.133 Lime 562.000 Secondary Nutrients Calcium 220.000 Magnesium 2.880 Sodium 1.190 SAR 0.276 Chloride 0.000 Iron 2.280 Alumium 3.360 Manganese 0.000 Boron 0.000 Sulfur 0.000 % Solids 32.10 pH 7.800 Min Rate 0.400 C:N Ratio 0.000 N Needed for 30:1 0.000 Metals Arsenic 0.003 Cadmium 0.001 Chromium 0.000 Copper 0.054 Lead 0.004 Mercury 0.001 Molybdenum 0.007 Nickel 0.004 Seleniun 0.003 Zinc 0.188 Waypointo ANALYTICAL 7/26/2022 Branch Residuals and Soils LLC Mr. Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill, SC, 29732 Ref: Analytical Testing Lab Report Number: 22-195-0047 Client Project Description: Von Dizehle Cordova, NC Project #2014-110 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Dear Mr. Bob Branch: Waypoint Analytical, LLC. received sample(s) on 7/14/2022 for the analyses presented in the following report. The above referenced project has been analyzed per your instructions. The analyses were performed in accordance with the applicable analytical method. Where the laboratory was not responsible for the sampling stage (refer to the chain of custody) results apply to the sample as received. The analytical data has been validated using standard quality control measures performed as required by the analytical method. Quality Assurance, method validations, instrumentation maintenance and calibration for all parameters (NELAP and non-NELAP) were performed in accordance with guidelines established by the USEPA (including 40 CFR 136 Method Update Rule May 2021) and NELAC unless otherwise indicated. Any parameter for which the laboratory is not officially NELAP accredited is indicated by a'—' symbol. These are not included in the scope because NELAP accreditation is either not available or has not been applied for. Additional certifications may be held/are available for parameters, where NELAP accreditation is not required or applicable. A full list of certifications is available upon request. Certain parameters (chlorine, pH, dissolved oxygen, sulfite...) are required to be analyzed within 15 minutes of sampling. Usually, but not always, any field parameter analyzed at the laboratory is outside of this holding time. Refer to sample analysis time for confirmation of holding time compliance. The results are shown on the attached Report of Analysis(s). Results for solid matrices are reported on an as - received basis unless otherwise indicated. This report shall not be reproduced except in full and relates only to the samples included in this report. Please do not hesitate to contact me or client services if you have any questions or need additional information. Sincerely, 4rjo P. A~ Randy Thomas Project Manager Laboratory's liability in any claim relating to analyses performed shall be limited to, at laboratory's option, repeating the analysis in question at laboratory's expense, or the refund of the charges paid for performance of said analysis. Page 1 of 8 Waypoint . N ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 www.waypointanalytical.com Certification Summary Laboratory ID: WP MTN: Waypoint Analytical, LLC., Memphis, TN State Program Lab ID Expiration Date Alabama State Program 40750 02/28/2023 Arkansas State Program 88-0650 02/07/2023 California State Program 2904 06/30/2023 Florida State Program - NELAP E871157 06/30/2023 Georgia State Program C044 02/18/2023 Georgia State Program 04015 06/30/2023 Illinois State Program - NELAP 200078 10/10/2022 Kentucky State Program 80215 06/30/2022 Kentucky State Program KY90047 12/31/2022 Louisiana State Program - NELAP LA037 12/31/2022 Louisiana State Program - NELAP 04015 06/30/2023 Mississippi State Program MS 02/11/2023 North Carolina State Program 415 12/31/2022 Pennsylvania State Program - NELAP 68-03195 05/31/2023 South Carolina State Program 84002 06/30/2022 Tennessee State Program 02027 02/11/2023 Texas State Program - NELAP T104704180 09/30/2022 Virginia State Program 00106 06/30/2023 Virginia State Program - NELAP 460181 09/14/2022 Page 1 of 1 00001 /22-195-0047 Page 2 of 8 ry � ,f Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Sample Summary Table Report Number: 22-195-0047 Client Project Description: Von Dizehle Cordova, NC Project #2014-110 Lab No Client Sample ID 99086 VD Matrix Date Collected Date Received Solids 07/13/202213:00 07/14/2022 Page 3 of 8 Wa y p dio n t CR ANALYTICAL 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 www.waypointanalytical.com Client: Branch Residuals and Soils LLC CASE NARRATIVE Project: Von Dizehle Lab Report Number: 22-195-0047 Date: 7/25/2022 Metals Analysis Method 6010D Sample 86731 (SB27-2-4) Analyte: Aluminum QC Batch No: 1-628020/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Arsenic QC Batch No: 1-627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A post digestion spike was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Iron QC Batch No: 1-627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Sample 86731 (SB27-2-4) Analyte: Potassium QC Batch No: 1-627787/1-627265 The matrix spike and/or the matrix spike duplicate was outside quality control acceptance ranges. A dilution test was performed and passed quality control acceptance ranges. No matrix interference is suspected. Page 4 of 8 0 Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Dizehle Mr. Bob Branch Report Date : 07/26/2022 1735 Heckle Blvd Information : Cordova, NC Received : 07/14/2022 Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-195-0047 REPORTOFANALYSIS Lab No : 99086 Matrix: Solids Sample ID: VD Sampled: 7/13/2022 13:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Neutralizing Value (%CCE) 28.1 % 0.1 1 07/20/22 16:34 DXT AOAC 955.01 Moisture 67.9 % 0.010 1 07/20/2216:09 FMM 254OG-2011 Ammonia Nitrogen 330 mg/Kg - dry 312 1 07/25/22 12:30 JPJ 4500NH3C-2011 Nitrate (NC3-N) <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 JCA 9056A Nitrite (NO2-N) <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 JCA 9056A Nitrate+Nitrite-N <3.12 mg/Kg - dry 3.12 1 07/15/22 19:40 9056A pH 7.8 s.u. 1 07/21/2216:06 DRS 9045D Total Solids 32.1 % 0.010 1 07/20/22 16:09 FMM 2540G-2011 Total Kjeldahl Nitrogen 2830 mg/Kg - dry 458 1 07/19/22 12:36 CLP 4500NORGD-2011 Phosphorus 127 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Aluminum 1680 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Arsenic <1.56 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Cadmium <0.312 mg/Kg - dry 0.312 1 07/20/22 22:30 EAL 6010D Calcium 110000 mg/Kg - dry 779 5 07/21/22 13:21 EAL 6010D Copper 27.0 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Iron 1140 mg/Kg - dry 31.2 1 07/20/22 22:30 EAL 6010D Lead 2.08 mg/Kg - dry 0.934 1 07/20/22 22:30 EAL 6010D Magnesium 1440 mg/Kg - dry 15.6 1 07/20/22 22:30 EAL 6010D Mercury <0.452 mg/Kg - dry 0.452 1 07/21/22 16:32 JTR 7471A Molybdenum 3.64 mg/Kg - dry 0.778 1 07/20/22 22:30 EAL 6010D Nickel 2.08 mg/Kg - dry 0.778 1 07/20/22 22:30 EAL 6010D Potassium 66.7 mg/Kg - dry 31.2 1 07/20/22 22:30 EAL 6010D Selenium <1.56 mg/Kg - dry 1.56 1 07/20/22 22:30 EAL 6010D Qualifiers/ DF Dilution Factor MQL Method Quantitation Limit Definitions Page 5 of 8 0 Waypoint. 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 0 Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com 22972 Branch Residuals and Soils LLC Project Von Dizehle Mr. Bob Branch Report Date : 07/26/2022 1735 Heckle Blvd Information : Cordova, NC Received : 07/14/2022 Suite 103-291 Project #2014-110 Rock Hill , SC 29732 Report Number: 22-195-0047 REPORT OPANALYSIS Lab No : 99086 Matrix: Solids Sample ID : VD Sampled: 7/13/2022 13:00 Test Results Units MQL DF Date / Time By Analytical Analyzed Method Sodium 595 mg/Kg - dry 77.9 1 07/20/22 22:30 EAL 6010D Zinc 93.8 mg/Kg - dry 3.89 1 07/20/22 22:30 FAL 6010D Qualifiers/ DF Dilution Factor Definitions MQL Method Quantitation Limit Page 6 of 8 r'�W Waypoint 2790 Whitten Road, Memphis, TN 38133 Main 901.213.2400 ° Fax 901.213.2440 ANALYTICAL www.waypointanalytical.com Shipment Receipt Form Customer Number: 22972 Customer Name: Branch Residuals and Soils LLC Report Number: 22-195-0047 Shipping Method 0 Fed Ex 0 US Postal 0 Lab UPS - 0 Client 0 Courier Other: Thermometer ID: r102� Shipping container/cooler uncompromised? 0 Yes No Number of coolers/boxes received 1 Custody seals intact on shipping container/cooler? 0 Yes 0 No 0 Not Present Custody seals intact on sample bottles? 0 Yes 0 No 0 Not Present Chain of Custody (COC) present? # Yes 0 No COC agrees with sample label(s)? (# Yes 0 No COC properly completed (# Yes 0 No Samples in proper containers? # Yes 0 No Sample containers intact? (# Yes 0 No Sufficient sample volume for indicated test(s)? Yes 0 No All samples received within holding time? Yes 0 No Cooler temperature in compliance? Yes 0 No Cooler/Samples arrived at the laboratory on ice. Samples were considered acceptable as cooling process had begun. Yes 0 No Water - Sample containers properly preserved 0 Yes 0 No N/A Water - VOA vials free of headspace 0 Yes 0 No N/A Trip Blanks received with VOAs 0 Yes 0 No N/A Soil VOA method 5035 — compliance criteria met 0 Yes 0 No # N/A High concentration container (48 hr) [_ Low concentration EnCore samplers (48 hr) j High concentration pre -weighed (methanol -14 d) F_ Low conc pre -weighed vials (Sod Bis -14 d) Special precautions or instructions included? Comments: 0 Yes (# No Signature: IMakayla Weaver Date & Time: 7/14/2022 11:18:53 Page 7 of 8 O O _ c ycu E E E �_ a, ? .1 , j T T O 0 0 O 1A N �vo= axx� n� E 0 c x 0 0. $ u m �S C O o o a O O N O n Z V r6n p u u x z Z x S S V o m v O a Vf Q m U O W LL V' S_ W W F- � Q Q ai 'A W1 5 2 N m 9 Q _ G' c c 40 0 > " v a E a v E cc a°'c 2 m L C✓ -' A ILI N Y 1 N % IL O W 0 E E `� CJ E 9 E 3 L_ o u o vd i m d a` d at F f�l ❑� .. G a > n V G'"'� C G a L E � u � �� b•N��1'V � � c o -0 lE `` JV-`�ry'Zty c rJ 0 Z W W lY 'Tt njtv`N Il. E T.lx v o N G A ~ — W > W cc > W cc > f� c�S 1 �y� . ctj m apsodwo(�) jo gej(g)i ,a aU r-c (Aa)l o3 ja1aH) xljleyy aE a \ t t ti c n Cr c c svauleluoi jo jagwnN m'- 1 m m 1 t <r �� p: ,a 0-4 O r = LL v u 0 _cud c0 C -(j pi d •~ b � � u ?•.. p { iV a % �...J � Y �V�l C. Q a � �, e U a a` a E E O u -0+ � � '^ o 00 Y �, 9 J p. c — 41 E `y " N E v A E �-0 r d o 3 .;, z z u a` c Page 8 or 8 inc. BIOLOGICAL CONSULTING SERVICES OF NORTH FLORIDA, INC. July 19, 2022 Robert Branch Branch Residuals and Soils 1735 Heckle Blvd. Suite 103-291 Rockhill SC 29732 336-312-9007 bbranch@branchrs.com Client ID: VD 1, VD 2, VD 3, VD 4, VD 5, VD 6, VD 7 BCS ID: 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 Dear Robert Branch, We have completed the analysis of the submitted samples as outlined below. Project Name: Von Drehle Cordova NC Analysis Method Salmonella EPA 1682; BCS SOP M-4 (ISO17025 and TNI Accredited) Following, you will find our report on the results of the analysis conducted on the referenced samples. Should you have any questions, please do not hesitate to contact me. Sincerely, Bonnie Mull, MPH Laboratory Operations Manager Page 1 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES IGMEAAAAB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 1 Sample Date/Time: July 13, 2022 12:44 BCS Sample ID: 2207109 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 33.0 Amount Analyzed: 29.98 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 2 BCS Sample ID: 2207110 Sample Date/Time: July 13, 2022 12:46 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 38.0 Amount Analyzed: 30.03 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: 150.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.7 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 2 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 6&03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES r.rn Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 3 Sample Date/Time: July 13, 2022 12:48 BCS Sample ID: 2207111 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 28.7 Amount Analyzed: 30.10 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 4 Sample Date/Time: July 13, 2022 12:51 BCS Sample ID: 2207112 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 31.4 Amount Analyzed: 30.00 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.8 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 3 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 6&03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Mac- AAMB Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 5 Sample Date/Time: July 13, 2022 12:53 BCS Sample ID: 2207113 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 29.1 Amount Analyzed: 30.00 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: 50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 6 Sample Date/Time: July 13, 2022 12:55 BCS Sample ID: 2207114 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 27.1 Amount Analyzed: 30.00 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: _<1.0 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 4 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. - GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:201 7 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHJUT THE WRITTEN CONSENT OF BCS LABORATORIES J18G:h7RAA&B "oa Client: Branch Residuals and Soils Analysis: Salmonella Project Name: Von Drehle Cordova NC Client Sample ID: VD 7 Sample Date/Time: July 13, 2022 12:57 BCS Sample ID: 2207115 Sample Description: Biosolid Date Received: July 14, 2022 9:52 Amount Submitted:100 mL Bottle % Solids: 29.1 Amount Analyzed: 30.01 g Receipt Temperature: 3.0 deg C Preserved: Yes Analysis Start: July 14, 2022 10:20 Analysis Stop Date: July 19, 2022 10:40 Analyst: Erika DiPasquale, B.S. Qualifier: U Primary Value: :50.07 Salmonella MPN/mL sample analyzed Secondary Value: :50.9 Salmonella MPN/4 dry grams Analysis Notes: Undetected: Analyte was not detected in the sample analyzed; Value represents the method's detection limit for the amount of sample analyzed as per the method's standard reporting units Page 5 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 68-03950, AZDHS:AZ0820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES ac-luA&B Client: Branch Residuals and Soils Project: Von Drehle Cordova NC Method Detection Limit: 1 microorganism/ unit weight or volume analyzed Practical Qua ntitation Limit: 1 microorganism/ unit weight or volume analyzed Report Notes: Custody Seal Condition: Not Present Sample(s) were received well preserved and in excellent condition. Sample(s) were analyzed following receipt as per the described analytical methodology. End of report notes. Page 6 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-563C WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO 17025:2017 L2422, PADEP: 6&03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES Aac r AA19M I certify that I have examined and I am familiar with the information submitted herein. The results pertain only to sample(s) identified and their condition at time of receipt. Based on my inquiry of the individuals responsible for the analysis, I believe the data to be true, accurate, and complete. Sampling and field data was obtained from submitted documents. The analysis was authorized and commissioned by the client. The resulting data are representative of the analysis conducted on the material/samples/articles provided by the client (or client's representative) and it's/their condition at the time of analysis. The sample(s) were analyzed in accordance with the appropriate method , however due to the inherent limitations of the methods, microorganisms may avoid detection. BCS Laboratories offers no express or implied warranties concerning the quality, safety, and/or purity of any sample, batch, source, or the process they are derived from. Quality assurance controls were performed as outlined in the method and as per Good Laboratory Practices. The analysis and results presented in this report meet the requirements of the standards of The NELAC Institute (TNI), ISO 17025, and the FL DOH Environmental Laboratory Certification Program, as applicable unless otherwise noted. Signature of Laboratory Director/Authorized Rep. Date: July 19, 2022 Page 7 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAX. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 6&03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES A I�Y� B qpww ;� DATA QUALIFIER CODES SYMBOL MEANING B Results based on counts outside the acceptable range. X Sample received without prior notification ordelayed delivery. Analysis performed outside of associated method required QC data set (1 QC data set per 20 samples per 168 hours). I Value is between the laboratory method detection limit &the practical quantitation limit. J1 The sample matrix interfered with the abilityto make any accurate determination. J2 No Quality Control criteria exist forthe component. J3 The data are questionable because of improper laboratory orfield protocols. L Off scale high. Actual value is known to be greaterthan value given. N Presumptive evidence forthe presence of material. There is an indication that the analyte is present, but the confirmation requirement was not met. O Sampled, but analysis not performed. Q Sample held beyond the accepted holding time. U Indicates that the compound was analyzed for but not detected. The specified component was not detected. The reported value is the method detection limit. V Analyte was detected in both sample and the method blank. Data may not be accurate. Y Laboratory analysis was from an improperly preserved -sample; the data may not be accurate Z Too many colonies present (TNTC); the numeric value given represents the upper end of the value that can be determined based on the volume. 7 Data are rejected and should not be used. QC data for analyte did not meet acceptance criteria. Presence or absence of analyte could not be confirmed. ** Not reported due to interference. A Sampling container supplied by client. Sterility can not be confirmed by BCS. # BCS Lab specific qualifier. See laboratory analysis notes. Page 8 of 8 Final Report BCS ID 2207109, 2207110, 2207111, 2207112, 2207113, 2207114, 2207115 BCS LABORATORIES, INC. — GAINESVILLE 4609 NW 6TH STREET, STE. A, GAINESVILLE, FLORIDA 32609 TEL. (352) 377-9272, FAx. (352) 377-5630 WWW.MICROBIOSERVICES.COM FLDOH E82924, ISO17025:2017 L2422, PADEP: 68-03950, AZDHS:AZO820, EPA FLO 1 147 THIS REPORT SHALL NOT BE REPRODUCED, EXCEPT IN FULL, WITHOUT THE WRITTEN CONSENT OF BCS LABORATORIES O z M a r II ti U m Q3 N M `/ d d M ti ° O N J t- i N h` m •� M E O J z ,� U T( 4 CD U W O U LL O z S U Z8:6 ZZOZ11,WL0 Z4:6 ZZOZ/VL/LO MLOZZ SUL= L aA _ 9 CIA sllOS Pue slenPlsab youeJg sOOS Pue slenplsaa yz)uej 8 aay10 ualnno, ••, N I N N O h OLn In G N R cm In m N N Oi N H C N • H ^ Q1 ) m n r- N _= y N CD - 7 p h O g! N NCY �' Er'! N 1 y, N N ems- c C C •m - p 0 o _ o II- •ro F u t E d ?� o w 9 (L a: c m u. �t .l T \� tL w 0 N r� z d00 U w _ X tL d p ; O v o L. 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Chemists, Inc. envirochem 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax sM 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.5843 Lab/Fax ANALYTICAL & CONSULTING CHEMISTS info`t environmentalcllemists.com Branch Residuals/Bob Branch 1735 Heckle Blvd Suite 103-291 Rock Hill SC 29732 Attention: Bob Branch Date of Report: Feb 09, 2022 Customer PO #: Customer ID: 15060009 Report #: 2022-00648 Project ID: Sludge -von Drehle Lab ID Sample ID: Collect Date/Time Matrix Sampled by 22-01588 Site: Sludge 1/11/2022 11:30 AM Solid/Sludge Bob Branch Test Method Results Date Analyzed Chlordane (TCLP) SW-846 8081 8 <0.02 mg/L 01/26/2022 Endrin (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Heptachlor (TCLP) SW-646 8051 B <0.0005 mg/L 01/26/2022 Heptachlor epoxide (TCLP) SW-846 8081 8 <0.0005 mg/L 01/26/2022 Lindane (TCLP) SW446 8081 B <0.0005 mg/L 01/26/2022 Methoxychlor (TCLP) SW-846 8081 B <0.0005 mg/L 01/26/2022 Toxaphene (TCLP) SW-846 8081 B <0.05 mg/L 01/26/2022 2,4,5-TP (TCLP) SW-8468151 A <0.003mg/L 01/27/2022 2,4-D (TCLP) SW-846 8151 A <0.003 mg/L 01/27/2022 1,4-Dichlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 2,4,5-Trichlorophenol (TCLP) 5W-846 8270 E <0.050 mg/L 01/28/2022 2,4,6-Trichlorophenol(TCLP) SW8468270E <0.050mg/L 01/28/2022 2,4-Dinitrotoluene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Cresol (TCLP) SW-8468270E <0.050mg/L 01/28/2022 Hexachlorc-1,3-butadiene (TCLP) SW-848 8270 E <0.050 mg/L 01/28/2022 Hexachlorobenzene (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 Hexachloroethane(TCLP) SW-8468270E <0.050mg/L 01/28/2022 m + p-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 01128/2022 Nitrobenzene (TCLP) SW-8468270E <0.050mg/L 01/28/2022 o-Cresol (TCLP) SW-846 8270 E <0.050 mg/L 01 /28/2022 Pentachlorophenol(TCLP) SW-8466270E <0.050mg/L 01/28/2022 Pyridine (TCLP) SW-846 8270 E <0.050 mg/L 01/28/2022 1,1-Dichloroethylene (TCLP) SW-84B Method 8260D <0.01 mg/L 01/19/2022 1,2-Dichloroethane (TCLP) SW-846 Method8250D <0.01 mg/L 01/19/2022 Benzene (TCLP) SW-845Method 8260D <0.01 mg/L 01/19/2022 Carbon Tetrachloride (TCLP) SW-846 Method8260D <0.01 mg/L 01/19/2022 Report # 2022-00648 Page 1 of 2 envirochem M ANALYTICAL 8 CONSULTING CHEMISTS Environmental Chemists, Inc. 6602 Windmill Way, Wilmington, NC 28405 - 910.392.0223 Lab - 910.392.4424 Fax 710 Bowsertown Road, Manteo, NC 27954 - 252.473.5702 Lab/Fax 255-A Wilmington Highway, Jacksonville, NC 28540 - 910.347.58-13 Lab/Fax info cc environmentalchemists.com Branch Residuals/Bob Branch Date of Report: Feb 09, 2022 1735 Heckle Blvd Suite 103-291 Customer PO #: Rock Hill SC 29732 Customer ID: 15060009 Attention: Bob Branch Report #: 2022-00648 Project ID: Sludge -von Drehle Chlorobenzene (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Chloroform (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 Methyl ethyl ketone (TCLP) SW-846 Method 0250D <0.05 mg/L 01/19/2022 Tetrachloroethylene (TCLP) SW-B46 Method 8280D <0.01 mg/L 01/19/2022 Trichloroethylene (TCLP) SW-846 Method 8250D <0.01 mg/L 01/19/2022 Vinyl Chloride (TCLP) SW-846 Method 8260D <0.01 mg/L 01/19/2022 RCI Ignitability EPA 1030 <0.8 mm/sec 01/17/2022 Cyanide SM 4500 CN D 1.36 mg/kg 01/20/2022 Sulfide SM 4500 S D 0.56 mg/kg 01121 /2022 pH SW 846 Method 9045D 7,87 units 01/24/2022 Result estimated. Analyzed out of 15 minutes hold time. TCLP Metals Arsenic EPA 200.7, Rev. 4.4, 1994 <1.Omg/L 01/26/2022 Barium EPA 200.7, Rev. 4.4, 1994 <1.0 mg/L 01/26/2022 Cadmium EPA 200.7. Rev. 4.4, 1994 <1.Omg/L 01/26/2022 Chromium EPA 2007, Rev. 4.4, 1994 <1.0 mg/L 01/26/2022 Lead EPA 200.7, Rev. 4.4. 1994 <1.0 mg/L 01/26/2022 Selenium EPA 200.7,Rev. 4.4,1994 <1.Omg/L 01/26/2022 Silver EPA 200.7, Rev. 4.4, 1094 <1.0 mg/L 01/26/2022 Mercury EPA 245.1 <0.0002 mg/L 01/28/2022 Comment: Reviewed by: Report #:: 2022-00648 Page 2 of 2 Environmental Chemist, Inc., Wilmington, NC Lab #94 6502 Windmill Way Wilmington, NC 28405 910.392.0223 ,, Sample Receipt Checklist Client:ELUISA 4 S I DU rI.S Date: 1 Report Number..Qo, — bO �o q s Receipt of sample: ECHEM Pickup Cq Client Delivery O UPS ❑ FedEx ❑ Other ❑ ❑ YES 113 NO Off N/A Il. Were custody seals present on the cooler? ❑ YES 10 NO W N/A 12. If custody seals were present, were they intact/unbroken? Original temperature upon receipt °C Corrected temperature upon receipt eC How temperature taken: ❑ Temperature Blank V Against Bottles IR Gun ID: Thomas Traceable S/N 192511657 IR Gun Correction Factor'C: 0.0 D YES ❑ NO 3. If temperature of cooler exceeded 6°C, was Project Mgr./QA notified? Dr YES ❑ NO 4. Were proper custody procedures (relinquished/received) followed? YES ❑ NO 5. Were sample ID's listed on the COC? JV YES ❑ NO 6. Were samples ID's listed on sample containers? $1 YES ❑ NO 7. Were collection date and time listed on the COC? YES ❑ NO 8. Were tests to be performed listed on the COC? YES ❑ NO 9. Did samples arrive in proper containers for each test? YES ❑ NO 10. Did samples arrive in good condition for each test? YES ❑ NO 11. Was adequate sample volume available?' YES ❑ NO 12. Were samples received within proper holding time for requested tests? ❑ YES Ill NO 13. Were acid preserved samples received at a pH of <2? ❑ YES ❑ NO 14. Were cyanide samples received at a pH >12? ❑ YES I ❑ NO 15. Were sulfide samples received at a pH >9? ❑ YES O NO 16. Were NH3/TKN/Phenol received at a chlorine residual of <0.5 m/L? ** ❑ YES ❑ NO 117. Were Sulfide/Cyanide received at a chlorine residual of <0.5 m/L? ❑ YES ❑ NO 118. Were orthophosphate samples filtered in the field within 15 minutes? * TOC/volatiles are pH checked at time of analysis and recorded on the benchsheet. ** Bacteria samples are checked for Chlorine at time of analysis and recorded on the benchsheet. Sample Preservation: (Must be completed for any sample(s) incorrectly preserved or with headspace) Sample(s) were received incorrectly preserved and were adjusted accordingly by adding (circle one): H2SO4 HNO3 HCI NaOH Time of preservation: If more than one preservative is needed, notate in comments below Note: Notify customer service immediately for incorrectly preserved samples. Obtain a new sample or notify the state lab if directed to analyzed by the customer. Who was notified, date and time: Volatiles Sample(s) were received with headspace COMMENTS: DOC. QA.002 Rev 1 `-J Z, P //��n 41 c Z C a N LL F lz W WU t!; i J a ZO f- W LL I4R w w 0 Z" z W tl1 t� LL O Z a U 0 z Q z O U w J J O V z H Q' O 0. cc 0) .4 Q z (i W 7 O a a s c cc m 0 m ed z p 0 a 0 >- L) w L) i I J • ul E1- W i u 0 i m J � I ( Z I � o. I I w i MaHlo I a m Z OIHl O d HOVN CONH R� uj IL 4OSZH dl7H MON x aasmN al 8Vl ouliol4c G (9JGd) a. I1 U` IL (9 Il 0 n. (9 d (D d U m (9 IL U' Jaulejuo3 Vis Jo U U (D L) (D c.) C7 U (D L) (9 c.) CD U CD C) U ailsodwon adR aldwsg 1 m E o o � , ri �N 0 c i 0 d to N a E CD to e- N F d O. 7 a i I SECTION III MANAGEMENT PLAN MANAGEMENT PLAN von Drehle Corporation produces Fiber Clay from its Cordova, North Carolina facility as a bi-product of paper towel production using recycled paper. These residual solids are produced by non -biological processes that separate clay non -suitable fibers out during the production processes. Plastics are also separated and are sent to the land fill and are not to be considered as part of this Class A permit application. These residuals have no domestic contribution. Based on the pathogen testing and the no -biological nature of the treatment process, vector attraction reduction testing is not required. von Drehle wishes to distribute their Fiber Clay in the following ways: • Use as a landfill daily cover, • Admixture for composts, soil amendments, and potting soils, and • As a replacement for commercial lime (or most limiting application factor) on nonspecific agricultural receiver sites. For direct application, von Drehle Corporation or it's assigned representative will identify local landowners and/or other property as receiver sites. Application made to all sites will be based on the ability of the crop and the land to properly assimilate the residual solids. Application thickness of the application rate, percent solids of the residuals applied, the type, whether the field can or will be incorporated, thickness of the vegetative cover, and the lime requirement of the soil will be predominant application factors. The nitrogen needs of the crop will be secondary since it is expected that additional nitrogen will need to be applied to correct the carbon -nitrogen ratio to all the proper growth of the crop. von Drehle, plans to take all of these into account to be conservative and will distribute these residuals based on the most restrictive of these application rates. For uses of these residuals in other processes other than direct application, von Drehle makes no claim for their consistency or properties. Use by other entities will be without their responsibility to determine and accept as is, with no liability or other implication to von Drehle Corporation. Overview of Process and Residual Solids Handling Overview of Process and Residual Solids Handling von Drehle Corporation Cordova facility is located at 126 First Street in Richmond County, North Carolina. This facility produces, approximately 28,500 dry tons of Fiber Clay annually through separation and fractionation processes from their feed stock recycled paper. The processes remove all plastics which are sent to the landfill. The majority of the recycled paper is repulped for von Drehle's paper making process. The clay and short fibers that are separated out in the various screening and fractionation processes are run through a belt press and Fiber Clay is made. Fiber Clay is a product of non -biological processes and has no domestic contribution. Fiber Clay can be placed in sealed trucks have three potential types of destinations: • To a landfill for use as daily cover, • To an offsite blending operation for the inclusion in composts, soil amendments, and potting soils or • As a replacement for commercial lime (or most limiting application factor) on nonspecific agricultural receiver sites. Distribution Methods for Reuse Distribution Methods for Reuse The Fiber Clay may be distributed in the following manner: • Use as a landfill daily cover, • Admixture for composts, soil amendments, and potting soils, and • As a replacement for commercial lime on nonspecific agricultural receiver sites. For direct application to nonspecific receiver sites, von Drehle Corporation or its assigned representative will identify local landowners and/or other property as receiver sites. Application made to all sites will be based on the ability of the crop and the land to properly assimilate the residual solids. Application thickness of the application rate, percent solids of the residuals applied, and the type and thickness of the vegetative cover will be the determining factors. These materials have very little nitrogen value so application will be based on: • application thickness or • lime needs of the soil. whichever of these accounts for the most restrictive application rate. Application thickness of the application rate, percent solids of the residuals applied, the type, whether the field can or will be incorporated, thickness of the vegetative cover, and the lime requirement of the soil will be predominant application factors. The nitrogen needs of the crop will be secondary since it is expected that additional nitrogen (above what is required for crop growth) will need to be applied to correct the carbon -nitrogen ratio to all the proper growth of the crop. von Drehle, plans to take all of these into account to be conservative and will distribute these residuals based on the most restrictive of these application rates. For other distribution points regarding the use of this residual in other processes or as admixtures, von Drehle makes no claim for their consistency or properties. Use by other entities will be without their responsibility to determine and accept as is with no implication to von Drehle. Transportation and Logistics Transportation and Logistics von Drehle Corporation Fiber Clay will be loaded into sealed sludge trailers. These trailers will be routed to various points for distribution, land application to nonspecific receiver sites, or sent a landfill as daily cover. Trucks will travel on major traffic routes to the application and or distribution sites. Individuals, agencies, or companies wishing to receive either of the von Drehle Fiber Clay will be issued a product information sheet, the most recent copy of the analytical information, and Product Receipt Form. The product information sheet will specify the buffer requirements for von Drehle's Fiber Clay as well as application restrictions. Each Product Receipt Form will document: • Amount of Fiber Clay received, • The name, address and telephone number of the person who prepared the Fiber Clay, • The name, address and telephone number of the person distributing/land applying the residuals, • A description of the processes that generated the residuals, • A summary of the results from the most recent residuals sampling event, • A summary of the type and volume of residuals distributed/land applied per acre, • A summary of the nutrients land applied per acre, and • A list of recommendations to the recipient of the residual regarding field use, soil testing, pH adjustment, and other relevant agronomic information. Both the Product Label and the Product Receipt Form will be required to ensure receipt of this information and for the removal volume. Copies of this information will be retained by the von Drehle Cordova and will be available for review upon request The distribution receiver, the land applier, and the site receiver will be instructed as to the proper use of this material as listed below: • Applications should be made in accordance with approved application standards. • Application shall not be made to land that is flooded, frozen, or snow covered. • Application and storage must be performed to prevent runoff from the application or storage site to any surface water. Buffer or "no application" zones as described in the approved permit and Product Information Sheet. • Applications must not be applied so thick as to cover existing vegetation. • Additional nitrogen may need to be applied to offset nitrogen deficient symptoms due to improper carbon to nitrogen ratio. Monitoring and Recordkeeping Monitoring and Recordkeeping The von Drehle Corporation Cordova facility requests that the Fiber Clay (Fiber Clay) be monitored monthly for residuals analysis based on the amount of these residuals expected to be distributed. A set of seven (7) Salmonella analyses will be performed prior to the end of the preceding month. A TCLP analysis will be performed annually. Fiber Clay samples will be collected and delivered to a laboratory qualified to analyze residual solids and that is familiar with routine environmental sample preparation and standards. Records pertinent to the successful management of the land applications program will be maintained for the benefit of the farm operator, DWR, land applicator, and permittee. These records will contain at a minimum: • Source of the residuals, • Type of the residuals, • Date of the residual application/ distribution receiver, • Information regarding the location of the residual application / distribution receiver (i.e. field owner name, address, and telephone number, approximate field location, and field number) • Method of application / intended distribution, • Weather conditions (if applicable), • Soil conditions (if applicable), • Type of crop or crops to be grown on the field or type of distribution receiver and intended use, • Volume or weight of residuals applied to the field or provided to distribution receiver, • Annual totals of dry tons per acre of residuals, annual pounds of plant available nitrogen, and annual pounds of phosphorus applied to the field or annual total of dry tons given to distribution receiver if distributed as a non -land application alternative. Each year an annual summary of the activities of the program will be prepared and delivered to the appropriate agencies and participants on or before the 1 st of March. The Fiber Clay annual summary will include: A) Summary of the Fiber Clay, B) Volume/Weight of the distributed amount of Fiber Clay, C) Name of the receiver of the distributed Fiber Clay, D) Intended use(s) of the Fiber Clay, E) Volume/Weight of other Amendments or Bulking Agents, F) Annual totals of dry tons/acre of the Fiber Clay, G) pounds of plant available nitrogen (PAN), phosphorus, and lime applied from the Fiber Clay, if distributed to non-specific receiver sites and H) pounds of nitrogen needed to offset organic carbon applied through Fiber Clay. 2. Monthly - nutrients and metals will be analyzed of: Aluminum, Ammonia, Arsenic, Cadmium, Calcium, Copper, Lead, Magnesium, Mercury, Molybdenum, Nickel, Nitrate -Nitrite, Zinc, % Total Solids, CCE, pH, Phosphorus, Potassium, TKN, Selenium, and Sodium will be collected and analyzed by a qualified laboratory. From this information, the Plant Available Nitrogen (PAN) will be calculated. If land application occurs at a frequency of less than monthly, nutrient and metal analyses will be required for each distribution event. 3. Once a permit cycle a Toxicity Characteristics Leaching Procedure (TCLP) analysis with ignitability, reactivity, and corrosivity of the von Drehle Fiber Clay will be collected and analyzed by a qualified laboratory. Leachate Collection Leachate Collection No provision is made for leachate collection since the residuals are not designed to undergo any mixing with other productions on -site. The storage pad at the facility is sloped to the back to the drainage feature. Below the drainage feature is a screen to capture any solids that are washed to the drain. Once these residuals have been transported to the potential application sites or for other uses, the fiber clay can be stockpiled in a covered facility or covered on the ground similar to other Class A products. Once covered this material will remain covered until the time of application. No provision is made for leachate collection since the residuals are not designed to undergo any mixing with other productions on -site. The storage pad at the facility is sloped to the back to the drainage feature. Below the drainage feature is a screen to capture any solids that are washed to the drain. It will be the responsibility of the distribution sites that receive these residuals. These residuals that are to be land applied, either to permitted or unspecified sites, can be stockpiled in a covered facility similar to what is provided with chicken litter and not be removed until the time of application. Below are Solvita tests for von Drehle Fiber Clay for ammonia and carbon dioxide. These tests have been used in the past for stockpile use and as a measure of product stability. These tests were performed over a 4-hour period on November 1, 2022. Solvita Test for CO2 evolution for Fiber Clay — low CO2 (values of 7/8 for all six jars). Solvita Test for NH4 evolution for Fiber Clay — low NH4 (values of 5, 5, 5, 5, 5, and 5) Based on Solvita's brochure, Fiber Clay has a Maturity Index of 5, one below the maturity level of 6 that is considered "Mature Compost". Fiber Clay has no ammonia and at a level that is between Mature compost and compost that has a low carbon to nitrogen ratio. These values were rechecked after 2 additional days incubation. At that time CO2 evolution for Fiber Clay —after 2 days had values of 2, 2 2, 3, 3, and 2. The ammonia values of before remained unchanged. In light of the values after 2 days, the Fiber Clay is a characterized by the Solvita tests as a very active compost with a maturity level of 3. Both of these levels of maturity indicate that high respiration rates will continue to occur and significant turning made be necessary as respiration occurs. Onsite stockpiling is recommended to remain at no more than 60 days for these non -biological residuals. SECTION IV VON DRHLE CORDOVA FIBER CLAY LABEL AND PRODUCT INFORMATION SHEET The von Drehle Corporation Cordova Fiber Clay Label Produced By Preparer von Drehle Corporation Mitchell Luckie (256) 496-6530 Wastewater Treatment Plant 126 First Street Cordova, North Carolina 28330 Cordova, North Carolina 28330 For information on this product contact von Drehle Corporation Cordova, NC facility at (910) 410-9131 Fiber Clay from the von Drehle Corporation Cordova NC are the clay and short fibers excluded from the repulping process of recycled paper production. The generated residuals have no domestic source percentage and are an exceptional quality residual solid that is permitted for bulk distribution. Approved used for von Drehle Fiber Clay: • Amendment for creation of soil mixture to be further distributed to the public, • Amendment for compost to be further distributed to the public, • Use as a daily landfill cover, • Application to potential receiver sites for use as a soil amendment or replacement for agricultural lime. Provisions for application are listed below. Provisions for Application Application of von Drehle Fiber Clay are prohibited except in accordance with the provisions specified in the Application Information Sheet. Application must conform to standards identified in Permit No. WQ0039924 and include but are not limited to: Maximum slope for the land application of these residuals is 10 % for surface applications and 18% for subsurface applications Distance Buffer Items (feet) Public or private water supply source, waters classified as SA or SB, and any Class 1 or Class 11 impounded reservoir used as a source of drinking water for both surface and subsurface methods 100 Surface waters (intermittent streams, perennial streams, perennial surface water bodies and wetlands) 100 Surface water diversions (ephemeral streams, ditches, groundwater lowering ditches, or waterways) 0 Application can not occur to: • adversely affect a threatened or endangered species or it's critical habitat, • within the 100-year flood plain unless solids are incorporated within a 24-hour period, • cause prolonged nuisance conditions, • create conditions where runoff will occur, • within the 100-year flood plain unless solids are incorporated within a 24-hour period, or • during a measurable rainfall event or 24-hours following a 0.5 inch cumulative rainfall event (over 24-hours). Application Information Sheet von Drehle Fiber Clay 1. von Drehle Fiber Clay shall not be applied to flooded, frozen, or snow-covered areas. 2. Application and storage of von Drehle Fiber Clay must be conducted in such a way as to prevent runoff or erosion from the application or storage site to any surface water. 3. Applications of von Drehle Fiber Clay must not be applied so thick as to cover existing vegetation. Application that is made to sites with less than 50 percent ground cover should be incorporated unless incorporation will result in violation of other federal program. 4. Applications of von Drehle Fiber Clay shall be applied uniformly at a rate equal to amount that can be adequately assimilated into the soil through incorporation, will not smother any current living crop on the surface of the soil if material will not be incorporated, or the agronomic rate of the crop as specified by the permit and the most recent residual analysis, or the lime requirement of the soil and most recent residuals analysis; whichever is most limiting. 5. An acceptable soil pH (greater than 6.0) see appropriate state extension service for crop specific optimal soil pH on individual receiver sites. The soil pH should be verified annually with a soil sample with recommendations. These recommendations should be followed as they relate to optimal crop growth, monitoring and adjustment of the exchangeable sodium percentage, potential for calcium and magnesium deficiency, as well as other relevant agronomic information. Additional fertilizer, lime, or other nutrients may need to be added as directed by the soil sample results. 6. Applications and loading rates of von Drehle Fiber Clay shall be applied at rates that comply with realistic yield expectations based on the soil series and crops found at: http://nutrients.soil.nesu.edu/yields:' von Drehle Corporation Cordova Fiber Clay Approximately Contain: 32.10 Percent Solids 2.34 Plant Available Nitrogen surface land applied) pounds per dry ton 2.67 Plant Available Nitrogen (incorporated or injected pounds per dry ton 0..6 Phosphate 205pounds per dry ton 0.16 Potash K2Opounds per dry ton 180 Lining agent pounds per dry ton 7.8 pH of Fiber Clay See von Drehle Corporation Cordova WWTP for a copy of the most recent residuals analysis and loading rates. SECTION V VON DREHLE FIBER CLAY RECEIPT FORM VON DREHLE CORPORATION CORDOVA I , (printed name) have received wet tons of von Drehle Corporation Cordova Fiber Clay, a von Drehle Fiber Clay product label, and a copy of the most recent analysis of the product. I have read these documents and agree to adhere to the directions specified on the Application Information Sheet and the Product Label. My intended use of this product is Contact Information: Name Address City, State, Zipcode Phone Number Email Address Signature of Receiver Date of Receipt SECTION VI SPILL CONTROL PLAN SPILL CONTROL PLAN VON DREHLE CORPORATION CORDOVA FIBER CLAY CORDOVA, NORTH CAROLINA In the case of a spill, the following actions shall be taken immediately: l . Halt the source of the spill: Damaged truck or trailer tank unit. 2. Contain spill: Use straw bales to form a barrier. Straw hay bales can be obtained from several sources for this purpose. Soil near the site can also be used to form a barrier for containment. Clean up: Use residual solids application equipment to recover as much of the material as possible. After the application equipment has recovered as much material as possible, it will be land applied as per operation plan. 4. Final Clean up: Any unrecoverable material will be scraped and swept from the road surface and incorporated into an adjacent tillable area. Notification: As soon as possible after a spill occurs notify: A. von Drehle Corporation - (910) 410-9131 B. Department of Environment and Natural Resources Fayetteville Regional Office at (910) 433-3300 or appropriate regional office C. The appropriate County Sheriffs Department D. Fire Department if assistance is required for washdown Management of clean-up efforts: The ORC or applicator shall take immediate charge of the clean-up activities. Additional labor will be requested from the treatment plant and other departments as needed. Reporting: Within 5 days of notifications, a written report will be prepared detailing the cause of the spill, all actions taken in response to the spill, and proposed actions to be taken to ensure spill does not recur.. SECTION VII APPLICATION RATES APPLICATION RATES Prior to a distribution event, a private land owner will contact von Drehle Corporation Cordova to initiate an application. This land owner will indicate the type of crop to be grown and the size of the field to have the residuals distributed. A recent soil sample will be needed to determine lime requirements. A recent sample of Fiber Clay generated from von Drehle Corporation Cordova will be used to calculate the application rates for the crop based on the soil liming needs and the crop and soil assimilation characteristics. Prior to the distribution event, the potential receiver sites will be reviewed to insure the crop has been identified correctly and the field size is correct. Soils data will be checked at that time. Application rates will be determined based on the solids content of the residuals, the height of the crop on the receiver site, smothering potential of the crop, the lime requirement of the soil, lime requirements of the soils analysis, and nitrogen needs of the crop to be grown. Application rates will be limited based on either: application thickness, lime needs of the soil, or nitrogen needs of the crop; whichever of the three accounts for the most restrictive application rate. Based on my knowledge of potential receiver sites, application thickness should be no more than 10 wet tons per acre if it is to be spread on the surface of the soil with an actively growing crop, depending on the percent solids of the residuals. The incorporated amount will be reduced if the incorporation equipment fail to properly turn the residual under depending on slope, cover, soil assimilation. Application should not occur at a rate that the residuals may experience runoff or erosion from the receiver site. Re -application of sites will be based on these same factors. If there are questions concerning an individual application rate for a receiver site, consult a licensed soil scientist. Application of Fiber Clay has been shown to create an imbalance in the soil carbon to nitrogen ratio. This is particularly important as it relates to specific time periods in a crop's growth cycle. It may be necessary to apply additional nitrogen to achieve the crop results. The application rates listed below outline the lime -added values from the following applications. At this point application rates should be limited to lime needs of the soil. Wet Tons/ Acre Dry Tons/ Acre PAN #/Acre Lime Tons/Acre 1 0.32 0.75 0.09 2 0.64 1.50 0.18 3 0.96 2.25 0.27 4 1.28 3.00 0.36 5 1.61 3.75 0.45 6 1.93 4.50 0.54 7 2.25 5.25 0.63 8 2.57 6.00 0.72 9 2.89 6.75 0.81 10 3.21 7.50 0.90 11 3.53 8.25 0.99 12 3.85 9.00 1.08 13 4.17 9.75 1.17 14 4.49 10.50 1.26 15 4.82 11.25 1.35 16 5.14 12.00 1.44 17 5.46 12.75 1.53 18 5.78 13.50 1.62 19 6.10 14.25 1.71 20 6.42 15.00 1.80