WQ0005763_2001 Annual Report_20020228

Serving Jackson Count
Tuq a ci pigee Chairman, J.C. Alexander
Water- Ind Sewer Authority iNebster
Vice -Chairman, Mickey Luker
Jackson County
Jerry R. King
Executive Director
February 28, 2002
DENR/DWQ/Water Quality Section
Non -Discharge Compliance Unit
1617 Mail Service Unit
Raleigh NC 27699-1617
Gentlemen,
James Cochran
Ann F. Cabe
Keith Ward
Dillsboro
Sylva
Jackson County
Alvin Stiles
Marion Jones
C. J. Carter
Sylva
Sylva
Western Carolina University
MAR 1 9 200Z
RVED
AR
WATER QUALITY SECTION
Non -Discharge Compliance Enf.
Enclosed is the Annual Residuals Report for theTuckaseigee Water and Sewer
Sludge/Compost facility (permit #WQ0005763) for the period of January 1, 2001 December
31, 2001.
Should you have any questions or if I can provide you any additional information, please don't
hesitate to contact me.
5Sincer ly,
��67�'
Stan Bryson
Wastewater Plant Operations Superintendent
Tuckaseigee Water & Sewer Authority
Enc.
32 Asheville Hwy. Post Office Box 1051 Sylva, North Carolina 28779 828/586-5189

C;A
ANNUAL SEWAGE SLUDGE REPORT
OF
TUCKASEIGEE WATER AND SEWER AUTHORITY
PLANT # 1-NPDES # NCO039578 (WQ0005763)
for the period of January 1, 2001-December 31, 2001
as required by
40 CFR, PART 503
STANDARDS FOR THE USE OR DISPOSAL OF SEWAGE SLUDGE

TABLE OF CONTENTS
(1) REPORTING REQUIREMENTS/PERTINENT INFORMATION
(2) CERTIFICATION
(a) 2001 sludge data
(b) 2001 distrubution and marketing summary
(c) 2001 laboratory analysis
(d) 2001 lime stabilization record of operation

REPORTING RE. QUIREMENTS
Facilities responsible for reporting annually are described in the regulations as:
1. Publicly Owned Treatment Works (POTW) with an average design
'influent flow rate equal to or greater than 1.0 MGD.
2. POTW's serving a population of 10,000 or more.
3. Class I (facilities with an approved pretreatment program) sludge management
facilities.
The Tuckaseigee Water and Sewer Authority Wastewater Treatment Plant is a 1.5 MGD
design facility. The facility also treats the sludge from two additional plants owned by the
authority.
Pertinent information includes:
facility name: Tuckaseigee Water & Sewer Authority Plant # 1
NPDES # NCO039578
address: PO Box 1051
1871 North River Rd
Sylva NC 28779
facility operator: Stan Bryson
Wastewater Plant Operations Superintendent
ph. 828-586-9318

0
ANNUAL LAND APPLICATION CERTIFICATION FORM
Permit Number LAU C �' K LZ—) 1 2 County '" � �" Year v� w
Facility Name (as shown on pe ) �' > = ' i-- �i!,v
V.
Land Application Operator phone c3/
Land application of residuals as allowed by the ab ve permit occurred during the past calendar year
YP S _ NO_ If NO, SHIP PART I, AND PART II AND PROCEED TO THE CERTIFICATION. ALSO, IF RESIDUALS %T-RE
GENERATED BUT NOT LAND APPLIED. PLEASE ATTACH AN EXPLANATION ON NOW THE RESIDUALS WERE. HANRLF;D,
Part I
• Total number of application fields in pen -nit.
- Total number of fields land application occurred during the year.
• Total amount of dry tons applied during the year for all application sites. _
Total number of acres land application occurred during the year.
Part 11
:Facility was compliant during calendar year 200_ with all conditions of the land application permit (including but not limited to
items 1-12 below) issued by the Division of Water Quality
}ramS I NO. IF NQ, PLEASE PROVIDE A WRITTEN DESCRIPTION WHY THE FACILITY WAS NOT CONIPLLANT, THE
DATES, ,A D F?\TLAIN CORRECTIVE ACTION TAKEN.
] _ Only residuals approved for this permit were applied to the permitted sites.
2. Soil pTd was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the
limit specified in the permit.
3. Annual soils analysis were performed on each site receiving residua's during the past calendar year and three (3) copies of
laboratory results are attached.
4. Annual'TCLP analysis was performed and tliree (3) copies of certified laboratory results are -
attached.
S. All other monitoring was performed in accordance with the permit and reported during the year as required and three (3)
copies of certified laboratory results are attached.
6. The facility did not exceed any of the Pollutant Concentration Lirrats in Table 1 of 40 CFR Part 503.13 or the Pollutant
Loading Rates in Table 2 of 40 CM part 503.13. (applicable to 40 CFR Part 502 regulated facilities)
7. All general requirements in 40 CFR part 503.12 and management practices in 40 CPR Tart 50114 were complied with.
(applicablc to 40 C,'FR Part 503 regulated facilities)
S. All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior
authorization was received from the Division of Water Quality.
9. No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are
attached to include appropriate actions and remediations.
l0.vegetative cover as specified in the permit was maintained can this site and the crops grown were removed in accordance
with the crop management plan.
11.,No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred.
12.All buffer requirements as specified on the permit were maintained during each application of residuals.
uI CERTWY, UNDEP_ PENAI;fY Of LA't't', THAT THE ABO'�% INFOPtMATIQN IS, To THE BEST OF IMY "OWLEDGE AND BELIEF,
TRUE, ACCVRATE, AND COMPLETE. I AM AWARE THAT THERE ARE SIGNIFICANT PENALTIES)FOR SVBMIT ING F'ALSI
INk OICNIATION, INCLUDING THE POSSIBHdTY OF' F' ES AND MIPRiSONME FOR;KNVING �Rt]LATlom.: r
Perrnfttee blame find Title (typea or print) Signature of Permit ate
Signature of Preparer
(it different from Permittee)
Note: Preparer is defined in 40 CFn Part 503.9(r)
Date
Signature of Land Applier Date
Of different From Permittee and Preparer)
DEM FORM CF (1/2002)
Crnn_6Q 1 _C TC Cr. -cn 7im-,7 /Q.q /�: n

ANNUAL PATHOGEN A+r'D VECTOR ATTRACTION R) DUCTiON F'OPW
Facility Name �l'l - + r✓YY Permit Number 6,
wwTP NAW* .
Mopftoring Period: FrOrn 1_L{Qj TO J jj-/- .%
pathugaq Reductian (40 CFR 503.32) - Please indicate level achieved and alternative perfornled
Class A
Alternativo l
Alternative 4
Alternative 2 _
Alternative 5 X_
Alternative 3
Alternative 6 _
_Composting —Heat Drying _ Meat Treatment _,Thermophilic _Boca Flay
M e �
Alte'stative 1— Alternative 2 Alternative 3 _
_Ganuna Ray YPasteurization
If applicable to alternative performed (Class B only) indicate "Process to Significantly Reducc Pathogens":
Aerobic Digestion _ Air Drying _Anaerobic Digestion _— Composting _ Lime Stabilization
tf applicable to alternative performed (Class A or Class B) complete tite following monitoring data:
Allowable love!
Patho en Deisiity
Number of
Frequency of
Sample
Type
Analytical
Technique
Minimum
GBo. Mean
Maximurn
Units
Parameter
In Sludge
Exceadanca
Analysis
Fecal Colifonn
2 x 106 MPN
par gram of total
solids or 2 x 105
CFU per gram
f total solids
t00oMPN
per gram of
11
/
1 /
(7 I,�
Raal6
total Sore
(dry weight)
C�!rnoneRa
3 NIPN oar 4
bacteria {in
rams total
lieu Of fecal
11:1 (dry
teloht)
colifotm
Vector Attraction Reduction (40 CFR $03.33) - Please indicate option performed
Option I Option 2 Option 3 _ Option 4 Option 5
option 6 option 7 _ Option S Option 9 _ __— Option 10
No victor attraction reduction options v/cre performed —
CERT ATION STATEMENT (please check the appropriate statement)
I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have been met."'
-I certify, under penalty of law, that the pathogen requirements in 40 CFR 503.32 and the vector attraction reduction
requirement in 40 CFR 503.33 have not been met:' (please ante it you check this statement ,attach an explanation why you have not met one
or both of the requirements.)
"This determination has been made under my direction and supervision in accordance with the system designed to ensure that
qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction
reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and
imprisonment" act
o 1 0M �,
;Preparer aand "Title(type orp ntjLand Applier Name and Title (if applicable)(t}Tse or print)
-`nature of Preparer Date Signature of Land Applier (if applicable) Date
DE`I FORM RF (112002)
_ram I .uum'� 6900-EEL-GTG E5t60 Z00Z/90/E0

m
M
w
�7
a
ANNUAL RE-SIDUAI. SAMPLING SUMMARY FORM
Attach this form to the corresponding laboratory analysis.
Please note that yow' permit may contain additional parameters to be analyzed than those required to be surnmar¢ed on this form.
Permit Number
Facility Name
NPDES N
or WO 4
WWTP Name
i
1_
Labowllory 1) f ...
i
13)
Residual Analysils, Data
ate Sampled or I �
3
13%
/
f� /�` � d� � $�a
/
11�3 Vl � �r
[DateCornposited /�
Percent Solids
_
.'
.. ; .�_
......r�r��-
���
:
:
err
■ice
ri�■■�
x.
a1
(SIGNATURE OF PR ARER) ATE
"I cerlify, under penafty, of law, that this document was prepared under my direction or supervision in accordance wiih a system
designed to assure that (tualiled personnel property gathered and evahmted the Inftnmalion submitted. I am aware that there are
significant penalties for, submilf ng take information, including the posftNity of fines and knprisonment for knowing violations."
DEM FORM SSF (112002)

N
m
IL
0
Ca
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0
r
2
C)
In
H
Q
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ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND :SUMMARY FORM
FACILITY NAME )4e- C' t S" PERNi[r#i j /(e 3 COUNii(.�(�11 OPERATOR c'So
�� g
TDV
FACIUTY TYPE (please check one): Surface Dhposal (complete Part A (Sourco(s) and "Residual IN" Volume only) and Part C) PHONE � _��V9 ! 31 lJ
W Disl4button and Marketing (complete Pets A. B. and C)
WAS THE FACILITY IN OPERATION DIKING 7HE PAST CALENDAR YEAR? _X� YES NO. tt NO, skip Parts A, g, and C and cerlily form below.
Part A4
Part B"
Month
Sources(S)
ncludeNPDESYHappfcable'
Volume {dry tons?
Recipient Iigormation
Adrnendmenil
ftftiq A;Tenr IN
Reddual Irr
Product 0Ur
Name(s)
valuma
dryY tuns
Intendeduse (sy
.Januarp
February
March
April
May
Jrne
July
August
Soptembor
_^
October
November
December
Tolots:
Annual (dry torn).
Admenrkneni(s) used: Bulking ent(s) used:
If more space Is required than given, please use the comment space provided below or attach oddmonol J-reet(s). [ Check box If acicklcnol sheets) are attached.
Commends:
Part C
Facility vms compllani duringfcalendcr year ZOOwish aN condNions of the permit (including bul not limited to items 1.3 below) Issued by the
Division of Water Quality i//YES NO. It NO, please provide a wrftn desriplion whV the facility was not compfEani-
1. AN rnontforing was performed In accordance wfth the permit and reported during the year as required and 11yee (3) copies of certtffed loboratory results are attached.
2. AR operailons and maintenance requirements were compiled with or, in the case of a deflation, prior authoTlzartion was received from the Division of WateT Quality.
3, No contravention of Ground Water Quality Standards occurred at a monftoring well,
"I CERTIFY, UNDER PENALTY OF LAW, THAT THE ABOVE INFORMATION IS, TO THE BEST OF MY KNI MREDGE AND BELIEF, TRUE, ACCURATE AND COMPLETE. I AM AWARE THAT
THERE ARE 3 6NIFICAlin PENALTIES FOR SUBMITTIMP FALSE MFORMATION, INCLLMING IM POSSIBUM OF FINES AND IMPRISONMENT FOR KNOWING VIOLATIONS."
O
r9 TLRtE Of
CV
N
NA
LO
a
m
m
(_ --7/zt/P-)�-
SIGNATURE OF PREPARM DATE
Of cilffetent from Permlttee) "Preparer Is defined In 40 CFR Part 503.4(r)
OEM FORM DMSD (1 /MZ

0
2001 SLUDGE DATA
TWSA PLANT # 1 (1.5 mgd)
NPDES # NCO039578
SLUDGE TO DIGESTOR................................................................4,093,500 gallons
totallb s..................................................................... 23 7, 622 lb s
totaltons.......................................................................118.81 tons
total metric tons............................................................107.76 metric tons
TWSA PLANT # 2 (.5 mgd)
NPDES # NCO020214
SLUDGE HAULED TO PLANT # 1....................................................... 274,881 gallons
totaltons........................................................................ 22.95 tons
total metric tons.............................................................20.82 metric tons
TWSA PLANT # 3 (.1 mgd)
NPDES # NCO063321
SLUDGE HAULED TO PLANT # 1......................................................... 262,391 gallons
totaltons............................................................................ 20.00 tons
total metric tons..............................................................18.14 metric tons
A portion of the sludge that was generated at the Tuckaseigee Water and Sewer Authority
a... nni — 1, ,.lA.� h� a ,,, ��, to ��ntra�tnr to a rlPcianntP.d landf ll
Landfill: Macon County Landfill
1448 Lakeside Drive
Franklin NC 28734
A total of 507.83 wet tons were hauled to the landfill during 2001. This does not reflect
residuals that are currently stored onsite.
Copies of haul tickets can be provided if needed.

TWSA PLANT # I
ANNUAL DISTRIBUTION AND MARKETING SUMMARY
2001
PART A
VOLUME IN DRY TONS
MONTH
ADMENDMENT/
BULKING AGENT IN
RESIDUAL
IN
PRODUCT
OUT
January
0
February
0
March
0
April.
25.61
18.82
44.43
May
11.28
13.83
25.11
June
9.01
6.09
15.1
July
0
August
0
September
0
October
13.52
9.34
22.86
November
27.52
19.42
46:94
December
22.57
13.24
35.81
Annual Dry Tons
109.51
80.741
190.25

O
TWSA PLANT # 1
ANNUAL DISTRIBUTION AND MARKETING SUMMARY
2001
PART B
RECIPIENT INFORMATION
DATE
NAMES
VOLUME wet tons
INTENDED USE
2/20/01
Mark Bell
10
pasture
3/29/01
Mark Bell
22
pasture
4/4/01
Mark Bell
22
pasture
4/5/01
Phillip Stephens
18
pasture
4/6/01
Phillip Stephens
6
pasture
4/14/01
Joyce Ridley
6
pasture
4/17/01
Rick Cochran
1
pasture
4/20/01
Rick Cochran
12
pasture
4/21/01
Rick Cochran
12
pasture
4/27/01
Rick Cochran
8
pasture
4/28/01
Everett Deemer
30
Farm and pasture
5/2/01
Rick Cochran
8
pasture
5/7/01
Chester Sorrells
30
silage field
5/18/01
Rick Cochran
12
pasture
6/21/01
Lemuel Norman
1
pasture
9/2V/v 1
ShQiJc CVVk
7
yard
10/3/01
Dickie Gibson
8
hayfield
10/10/01
Chester Sorrells
48
hayfield
10/11/01
Chester Sorrells
32
hayfield
10/24/01
Chester Sorrells
24
hayfield
11/1/01
Chester Sorrells
16
hayfield
11/9/01
Mark Bell
12
hayfield
11/13/01
Chester Sorrells
32
hayfield
11/14/01
Chester Sorrells
48
hayfield
11/16/01
Mark Bell
24
hayfield
11/27/01
Chester Sorrells
48
hayfield
11/27/01
Mark Bell
12
hayfield
11/28/01
Mark Bell
12
hayfield
12/5/01
Mark Bell
12
hayfield
12/6/01
Mark Bell
12
hayfield
12/19/01
Mark Bell
12
hayfield
12/21/01
Mark Bell
12
ha field
Total 1
569 tons

i
aceAnalytical-
www. pacelabs. com
ruIaseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9317865
Client Project ID: TWSA LIME RESIDUAL
Lab Sample No: 93774685 Project Sample Number: 9317865-001 Date Collected: 01/23/01 08:30
Client Sample. ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 01/23/01 13:25
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Wet Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 01/30/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Method: % Moisture
44.8 %
Method: SM 9221B/E
ND 2
01/26/01 JMS
Prep Method: SM 9221B/E
01/23/01 KAS
REP®RT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

aceAnal,yfical
www.pacelabs.com
I
Pace Analytical Services, Inc.
'54 Ravenscrolt Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number: 9318418
Client Project ID: Effluent Analysis 2/20
Lab Sample No: 93797157 Project Sample Number: 9318418-002 Date Collected: 02/20/01 09:00
Client Sample ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 02/20/01 10:00
Parameters Results Units PRL Analyzed Analyst CAS# Ftnote Limit
Wet Chemistry
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 03/05/01
Method: SM 9221B/E Prep Method: SM 92216/E
ND 2 02/21/01 KAS
Page: 2
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

4
a� TceAnalyticalM
www.paceiabs.com
1—,aseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No: 93799815
Client Sample ID: TWSA LIME RESIDUAL
Parameters Results
Wet Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform: Fecal
r
Date: 03/05/01
T„
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9318507
Client Project ID: TWSA LIME RESIDUAL
Project Sample Number: 9318507-001 Date Collected: 02/23/01 09:44
Matrix: Soil Date Received: 02/23/01 12:20
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: % Moisture
46.5 -%
Method: SM 9221B/E
ND 2
02/28/01 AAB
Prep Method: SM 9221B/E
02/23/01 KAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
Page: 1
. Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

11�aceAnalyticafm
www.pacelabs.com
iyckaseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No: 93820009
Client Sample ID: TWSA LIME RESIDUAL
Parameters Results
Wet Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 03/30/01
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone. [phone]
Fax. [phone]
Lab Project Number: 9319068
Client Project ID: TWSA LIME RESIDUAL
Project Sample Number: 9319068-001 Date Collected: 03/21/01 10:00
Matrix: Soil Date Received: 03/21/01 16:37
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: X Moisture
47.7 X
Method: SM 9221B/E
ND 2
03/27/01 TRW
Prep Method: SM 9221B/E
03/22/01 KAS
Page: 1
Laboratory Certification IDs RAP®RT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 02980
without the written consent of Pace Analytical Services, Inc.

ceAnal ical'
www.pacelabs.com
1 ,aseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
4ttn: Mr. Stan Bryson
Phone: [phone]
Solid results are reported on a dry weight basis
Lab Sample No:, "93839439 Project Sample Number: 9315
-lient Sample,.ID: TWSA LIME RESIDUAL Matrix: Soil
Parameters Results Units PRL
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NO 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9319620
Client Project ID: COMPOST
001 Date Collected: 04/11/01 09:00
Date Received: 04/11/01 14:00
Analyzed Analyst CAS# Ftnote Limit
Metals
Metals. ICP, trace -level
Method: EPA 6010
Prep
Method:
EPA 3050
Aluminum
10000 mg/kg
44.
04/23/01
TRW
7429-90-5
Arsenic
1.8 mg/kg
1.7
04/23/01
TRW
7440-38-2
Cadmium
0.99 mg/kg
0.17
04/23/01
TRW
7440-43-9
pn"cium
280000 mg/kg
17.
04/23/01
TRW
7440-70-2
r omium
7.9 mg/kg
0.87
04/23/01
TRW
7440-47-3
pper
91. mg/kg
0.87
04/23/01
TRW
7440-50-8
Lead
7.8 mg/kg
1.7
04/23/01
TRW
7439-92-1,
Magnesium
3000 mg/kg
17.
04/23/01
TRW
7439-95-4
Molybdenum
2.3 mg/kg
0.87
04/23/01
TRW ,
7439-98-7
Nickel
4.0 mg/kg
0.87
04/23/01
TRW
7440-02 0
Potassium
1500 mg/kg
87.
04/23/01
TRW
7440-09-7
Sodium
400 mg/kg
44.
04/23/01
TRW
7440-23-5
Zinc
150 mg/kg
3.5
04/23/01
TRW
7440-66-6
Date Digested
04/17/01
Mercury, CVAAS
Method: EPA 7471
Prep
Method:
EPA 7471
Mercury
0.90 mg/kg
0.035
04/19/01
TRW
7439-97-6
Selenium, AAS Furnace
Method: EPA 7740
Prep
Method:
EPA 3050
Selenium
ND mg/kg
0.87
94/23/01
TRW
7782-49-2 1
Date Digested
04/17/01
Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
42.8 X
04/13/01
AAB
Date: 05/03/01
Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 TN Drinking Water 02980
NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

ikwk M.
ace Analytical u
_i www.pacelabs.com
I
Lab Sample No: 93839439
Client Sample ID: TWSA LIME RESIDUAL.
Parameters .Results
Pace Analytical Services, lnc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax.- 828.254.4618
Lab Project Number: 9319620
Client Project ID: COMPOST
Project Sample Number: 9319620-001 Date Collected: 04/11/01 09:00
Matrix: Soil Date Received: 04/11/01 14:00
Units PRL Analyzed Analyst CAS# Ftnote Limit
Total Percent Solids
Method: EPA
160.3
Percent Sol ids
57.0 1
Ammonia, Soil
Method. EPA
350.3
Nitrogen,.Amffionia
760. mg/kg
Total"Kjeldahl Nitrogen, Soil
Method: EPA
351.2
Nitrogen, Kjeldahl, Total
4370 mg/kg
Nitrogen, Nitrate plus Nitrite
Method: EPA
353.2
Nitrate -Nitrite (as N)
87. mg/kg
Nitrogen, Nitrite, Soil
Method: EPA
354.1
Nitrite as N
NO mg/kg
Phosphorus, Total, Soil
Method: EPA
365-2
:phorus
76.3 mg/kg
Fecal Coliform MPN Solid
Method: SM 9221BIE
8.74
8.74
8.7
0.87
2.19
Coliform. Fecal NO 2
Nitrogen, Totai Method: Standard Methods
Nitrogen 4500 mg/kg 1.0
Plant Available Nitrogen Method:
Nitrogen 960 mg/kg 1.0
Prep Method: EPA 160.3
04/13/01 AAB
Prep Method: EPA 350.3
04/25/01 JDA 7727-37-9
Prep Method: EPA 351.2
04/19/01 JDA
Prep Method: EPA 353.2
04/20/01 JDA 7727-37-9
Prep Method: EPA 354.1
04/30/01 AAB
Prep Method: EPA 365.2
04/13/01 MPS 7723-14-0
Prep Method: SM 92218/E
04/12/01 KAS
04/30/01 JDA 7727-37-9
04/26/01 JDA 7727-37-9
Date: 05/03/01 Page: 2
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NC Drinking Water 37712 This report shall not be reproduced, except in full, SC Environmental 99030
without the written consent of Pace Analytical Services, Inc.

raceAnalical T,
www.pacelahs.com
,seigee Water & Sewer Auth <A"
sox 1051
.5ylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are repo'
Lab Sample No:
Client Sample?
Parameters
on a dry weight basis
TWSA LIME RESIDUAL
Results
Wet Chemistry
Percent Moisture
Percent Moisture
Fecal Coliform MPN Solid
Coliform, Fecal
Date: 07/11/01
aborato[y Certification IN
k Wastewater 40
NC Drinking Water 37712
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab.Project Number: 9321567
Client Project ID: LIME RESIDUAL FECAL
Project Sample Number: 9321567-001 Date Collected: 06/28/01 12:00
Matrix: Soil - Date Received: 06/28/01 15:44
Units PRL Analyzed Analyst CAS# Ftnote Limit
Method: % Moisture
45.6 %
Method: SM 9221B/E
ND 2
07/09/01 AAB
Prep Method: SM 9221B/E
06/29/01 KAS
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N ACCOA\
F
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
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pace Analyticafm
www.pacelabs.com
—aseigee Water & Sewer Auth
PO Box 1051 s
Sylva, NC 28779
Attn: Mr. Stan Bryson
r';;vI,
Phone: [phone]::w"`
Solid results are reported on a dry weight basis
Pace Analytical Services, Inc.
54 Ravenscrott Drive
Asheville, NC 28801
Phone: [phone]
Fax. [phone]
Lab Project Number:.9321807
Client Project ID: TWSA LIME RESIDUAL
Lab Sample No--, 4- 3921765 Project Sample Number: 9321807-001 Date Collected: 07/12/01 08:00
Client SampJ=e''ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 07/12/01 09:08
Paramlt Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
.WetChemi stry
Percent Moisture Method: % Moisture
Percent Moisture 47.7 % 07/16/01 AAB
Fecal Coliform MPN Solid Prep/Method: SM 9221B/E / SM 9221B/E
Coliform, Fecal ND 2 07/12/01 KAS
r
Date: 07/20/01 Page: 1
Laboratory Certification IDs REPORT OF LABORATORY ANALYSIS Laboratory Certification IDs
NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030
\N RCCR
R
a7 n
\f z

w^q
raneAnalyticafm,.:
www.pacelabs.com
ipckaseigee Water & Sewer Auth
PO Box 1051
Syl va , NC 28779 w;
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are reportE
Lab Sample No :VtE s93957645 Project Sample Number: 9322813-001 Date Collected: 08/21/01 07:00
Client Sample ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 08/21/01 12:04
Parameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Wet` Chemistry
Percent Moisture Method: Y. Moisture
Percent Moisture 41.0 % 08/27/01 AAB
Fecal Coliform MPN Solid Prep/Method: SM 9221B/E / SM 9221B/E
Coliform, Fecal ND 2 08/21/01 KAS
Pace Analytical Services, Inc.
54 RavenscroftDrive
Asheville, NC 28801
Phone: 828,254.7176
Fax: [phone]
Lab Project Number: 9322813
Client Project ID: TWSA LIME RESIDUAL
on a dry weight basis
Date: 09/03/01
Laboratory Certification IN REPORT OF LABORATORY ANALYSIS
NC Wastewater 40 This report shall not be reproduced, except in full,
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc.
N ACCpR
Page: 1
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

e Analy ical m
www.pacelabs.com
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
,ckaseigee Water & Sewer Auth Lab Project Number: 9324896
PO Box 1051 Client Project ID: TWLA LIME RESIDUAL
Sylva, NC 28779fi„�
Attn: Mr. Stan Bryson .�
Phone: [phone];y,.
Solid results are4;reported on a dry weight basis
4T�p�
:v
p+a r
Lab Sample�No;;;�� 931043111
Project Sample
Number: 9324896-001
Date Collected: 11/13/01 09:10
Client SAle ID: TWSA LIME
RESIDUAL
Matrix: Soil
Date Received: 11/13/01 13:07
,,,F'arameters
Results Units
Report Limit Analyzed
CAS No. Ftnote Reg Limit
'Wet Chemistry
Percent Moisture
Method: % Moisture
Percent Moisture
47.7 .%
11/14/01
AAB
Fecal Coliform MPN Solid
Prep/Method: SM 9221B/E
/ SM 9221B/E
Coliform, Fecal
ND
2 11/14/01
KAS
t
v
Date: 11/29/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
„ AL�pq
I Ci4
_. ._
Page: 1
Laboratory Certification IDs
TN Drinking Water 02980
SC Environmental 99030

ace Anall �ical
J' `
www.pacelabs.com
fi
Tlckaseigee Water & Sewer Auth.,
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are,...repo
Lab Sample No:,, f931049548 Project Sample Number: 9325053-001 Date Collected: 11/16/01 09:35
Client Sample ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 11/16/01 12:38
.Par-ameters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
"Wet Chemistry
Percent Moisture Method: Moisture
Percent Moisture 47.3 % 11/20/01 AAB
Fecal Coliform MPN Solid Prep/Method: SM 9221B/E / SM 9221B/E
Coliform, Fecal ND 2 11/16/01 KAS
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: 828,254.7176
Fax., 828.254.4618
Lab Project Number: 9325053
Client Project ID: TWSA LIME RESIDUAL
on a dry weight basis
Date: 12/04/01 1 Page: 1
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NC Wastewater 40 This report shall not be reproduced, except in full, TN Drinking Water 02980
NC Drinking Water 37712 without the written consent of Pace Analytical Services, Inc. SC Environmental 99030
\N 1CCOR

ce Analyical m
www.pacelabs.com
Tlckaseigee Water & Sewer Auth
PO Box 1051
Sylva, NC 28779
Attn: Mr. Stan Bryson
Phone: [phone]
Solid results are r1. epo
Lab Sample No 931066880 Project Sample Number: 9325484-001 Date Collected: 12/07/01 09:00
Client SampT'e ID: TWSA LIME RESIDUAL Matrix: Soil Date Received: 12/07/01 10:10
Para meters Results Units Report Limit Analyzed CAS No. Ftnote Reg Limit
Wet Chemistry
Percent Moisture Method: % Moisture
Percent Moisture 47.0 % 12/17/01 AAB
Fecal Coliform MPN Solid Prep/Method: SM 9221B/E / SM 9221B/E
Coliform, Fecal ND 2 12/07/01 KAS
Pace Analytical Services, Inc.
54 Ravenscroft Drive
Asheville, NC 28801
Phone: [phone]
Fax: [phone]
Lab Project Number: 9325484
Client Project ID: TWSA LIME RESIDUAL
R
Date: 12/20/01
Laboratory Certification IDs
NC Wastewater 40
NC Drinking Water 37712
on a dry weight basis
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.
N Al
Page: 1
Laboratory Certification IN
TN Drinking Water 02980
SC Environmental 99030

i 51' r
TWSA LIME STABILIZATION
DAILY RECORD
p
DATE L d I
START STOP TOTAL
RUN TIME, HRS
SLUDGE FEED, GAL L v
LIME FEED, LBS I
SLUDGE FEED % SOLIDS
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TCnADGRATI IRF nF
TIME I
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22 HRS.
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BELT PRESS SPEED, % q , l
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LIME FEED AUGER, % 31' LBS/HR l
POLYMER USAGE
PE USED
TANKS MIXED
LITERS/TANK
M�IIXER SPEED, %- / 06) L
o4

RUNTIME, HRS
SLUDGE FEED, GAL
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TWSA LIME STABILIZATION
DAILY RECORD
DATE ©6
START STOP TOTAL
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[---
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BELT PRESS SPEED, % D
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MIXER SPEED, %
22 HRS. '
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RUN.TIME, HRS
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TWSA LIME STABILIZATION
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DATE
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°at 7-��
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OPERATOR
- POLYMER USAGE
TYPE USEDo
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f
DATE
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TYPE USED
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DATE
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DATE { a
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DATE/s/f7
T
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DATE .1 � �Q
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POLYMER USAGE
TYPE USED - D,3� (::T—.
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LITERS/TANK �� —j

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DATE
START
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RUNTIME, HRS " 1v F`
DRY TON
SLUDGE FEED, GAL L
LIME FEED, LSS
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LITERS/TANK

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DAILY RECORD. 1
DATE D
START STOP TOTAL
RUNTIME, HRS
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MIXER SPEED, %
6
...........................................................,......
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DATE A4,' i
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RUN.TIME, HRS
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..................................................................................................
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DATE C7 /
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DATE Z
d
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