NC0022217_Renewal (Application)_20221128

MDTIVA
ENTERPRISES LLC
November 14, 2022 Richard Rogers 1 1 © H " fE
Director, Division of Water Resources II
North Carolina Department of Environmental Quality 1J fl2s2o22j
1617 Mall Service Center
Raleigh, NC 27699-1611 DIVISION OF Vv'ATER RESOURCES
RE: NPDES Minor Industrial Permit Renewal Application
Motiva Enterprises, LLC Apex Terminal
Permit No. NC0022217
Dear Mr. Rogers;
Please find included with this cover letter, Motiva's NPDES minor industrial permit renewal
application for our bulk terminal in Apex, North Carolina. Our current permit expires on April
30, 2023.This application is replacing the October 20, 2022 submittal per the email dated
November 10, 2022 from Emily Richards which informed Motiva that there was an update EPA
form.
• Application Form— Form 1 and 2C
• Attachment I—Topographical Map and Process Flow Diagram
• Attachment II—Detailed Sampling Results August 2019-August 2022
If you have any questions, please contact Megan Boush at [phone] or
[e-mail].
Very truly yours,
r `
Dollnila Slater
General Manager,Terminal & Pipelines
Enclosures
cc: Megan Boush (electronic file 550-03)

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
Form U.S.Environmental Protection Agency
1 %%EPA Application for NPDES Permit to Discharge Wastewater
NPDES Grt1 GENERAL INFORMATION
SECTION 1.ACTIVITIES REQUIRING AN NPDES PERMIT(40 CFR 122.21(f)and(f)(1))
1.1 Applicants Not Required to Submit Form 1
1.1.1 Is the facility a new or existing publicly owned 1 1 2 Is the facility a new or existing treatment works
treatment works? treating domestic sewage?
If yes,STOP. Do NOT complete El No If yes,STOP.Do NOT El No
Form 1.Complete Form 2A. complete Form 1.Complete
Form 2S.
1.2 Applicants Required to Submit Form 1
1.2.1 Is the facility a concentrated animal feeding 1.2.2 Is the facility an existing manufacturing,
operation or a concentrated aquatic animal commercial, mining,or silvicultural facility that is
Zr) production facility? currently discharging process wastewater?
Yes 4 Complete Form 1 D No 0 Yes 4 Complete Form El No
a and Form 2B. 1 and Form 2C.
z —
= 1.2.3 Is the facility a new manufacturing,commercial, 1.2.4 Is the facility a new or existing manufacturing,
C) mining,or silvicultural facility that has not yet commercial,mining,or silvicultural facility that
commenced to discharge? discharges only nonprocess wastewater?
c Yes 4 Complete Form 1 ❑✓ No ❑ Yes 4 Complete Form E✓ No
and Form 2D. 1 and Form 2E.
°1 1.2.5 Is the facility a new or existing facility whose
' discharge is composed entirely of stormwater
a associated with industrial activity or whose
discharge is composed of both stormwater and
non-stormwater?
❑ Yes 4 Complete Form 1 D No
and Form 2F
unless exempted by
40 CFR
122.26(b)(14)(x)or
b 15 .
SECTION 2.NAME, MAILING ADDRESS,AND LOCATION(40 CFR 122.21(f)(2))
2.1 Facility Name
Motiva Enterprises LLC Raleigh Terminal
2.2 EPA Identification Number
-01
0
2.3 Facility Contact
csi
Name(first and last) Title Phone number
Scott Dilling Complex Manager [phone]
Email address
[e-mail]
cis
2.4 Facility Mailing Address
Street or P.O.box
2232 Ten-Ten Road
City or town State ZIP code
Apex NC 27539
EPA Form 3510-1(revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal
OMB No.2040-0004
N d 2.5 Facility Location
a .a Street,route number,or other specific identifier
Q v 2232 Ten-Ten Road
a)
Lc. o County name County code(if known)
Wake
o
City or town State ZIP code
m Apex NC 27539
SECTION 3.SIC AND NAICS CODES(40 CFR 122.21(f)(3))
3.1 SIC Code(s) Description(optional)
5171
N
a)
O
U
n
Z 3.2 NAICS Code(s) Description(optional)
424710
SECTION 4.OPERATOR INFORMATION(40 CFR 122.21(f)(4))
4.1 Name of Operator
Motiva Enterprises LLC
4.2 Is the name you listed in Item 4.1 also the owner?
0 ❑✓ Yes ❑ No
4.3 Operator Status
❑ Public—federal ❑ Public—state ❑ Other public(specify)
o ❑✓ Private ❑ Other(specify)
4.4 Phone Number of Operator
[phone]
4.5 Operator Address
Street or P.O. Box
Ca
E 2232 Ten-Ten Road
City or town State ZIP code
o v Apex NC 27539
is
Email address of operator
Q P
[e-mail]
SECTION 5.INDIAN LAND(40 CFR 122.21(f)(5))
5.1 Is the facility located on Indian Land?
❑Yes ❑✓ No
EPA Form 3510-1(revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 6.EXISTING ENVIRONMENTAL PERMITS(40 CFR 122.21(f)(6))
6.1 Existing Environmental Permits(check all that apply and print or type the corresponding permit number for each)
NPDES(discharges to surface ❑ RCRA(hazardous wastes) ❑ UIC(underground injection of
water) fluids)
• NC0022217
a ❑ PSD(air emissions) ❑ Nonattainment program(CM) ❑ NESHAPs(CM)
a)
❑ Ocean dumping(MPRSA) ❑ Dredge or fill(CWA Section 404) ❑ Other(specify)
SECTION 7.MAP(40 CFR 122.21(f)(7))
7.1 Have you attached a topographic map containing all required information to this application?(See instructions for
0 specific requirements.)
co
❑✓ Yes ❑ No ❑ CAFO—Not Applicable(See requirements in Form 2B.)
SECTION 8.NATURE OF BUSINESS(40 CFR 122.21(f)(8))
8.1 Describe the nature of your business.
The facility is a bulk distribution terminal for gasoline,petroleum distillates and ethanol.It does not
produce,manufacture or consume products or raw materials.Gasoline and distillates are received via
ai pipeline which are then stored in above ground tanks.Ethanol is received via tank truck.All
products are loaded out via tanker truck through the terminal's loading rack.
0
i
R
Z
SECTION 9.COOLING WATER INTAKE STRUCTURES(40 CFR 122.21(f)(9))
9.1 Does your facility use cooling water?
❑ Yes ❑✓ No 4 SKIP to Item 10.1.
9.2 Identify the source of cooling water.(Note that facilities that use a cooling water intake structure as described at
, 40 CFR 125,Subparts I and J may have additional application requirements at 40 CFR 122.21(r).Consult with your
c u' NPDES permitting authority to determine what specific information needs to be submitted and when.)
'
O .
U
c
SECTION 10.VARIANCE REQUESTS(40 CFR 122.21(f)(10))
10.1 Do you intend to request or renew one or more of the variances authorized at 40 CFR 122.21(m)?(Check all that
apply.Consult with your NPDES permitting authority to determine what information needs to be submitted and
when.)
Cr El Fundamentally different factors(CWA ❑ Water quality related effluent limitations(CWA Section
ce Section 301(n)) 302(b)(2))
ro ❑ Non-conventional pollutants(CWA ❑ Thermal discharges(CWA Section 316(a))
Section 301(c)and(g))
❑✓ Not applicable
EPA Form 3510-1(revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 11.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
11.1 In Column 1 below,mark the sections of Form 1 that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority.Note
that not all applicants are required to provide attachments.
Column 1 Column 2
❑✓ Section 1:Activities Requiring an NPDES Permit ❑ w/attachments
❑✓ Section 2:Name, Mailing Address,and Location ❑ w/attachments
❑✓ Section 3:SIC Codes ❑ wl attachments
❑✓ Section 4:Operator Information ❑ w/attachments
❑✓ Section 5: Indian Land ❑ w/attachments
❑✓ Section 6: Existing Environmental Permits ❑ w/attachments
ai
w/topographic
❑✓ Section 7:Map ❑✓ map ❑ w/additional attachments
o ❑✓ Section 8:Nature of Business ❑ wl attachments
..= ❑✓ Section 9:Cooling Water Intake Structures ❑ w/attachments
d
�' ❑✓ Section 10:Variance Requests ❑ wl attachments
co
;n ❑✓ Section 11:Checklist and Certification Statement ❑ wl attachments
d 11.2 Certification Statement
U
I certify under penalty of law that this document and all attachments were prepared under my direction or supervision
in accordance with a system designed to assure that qualified personnel properly gather and evaluate the
information submitted.Based on my inquiry of the person or persons who manage the system,or those persons
directly responsible for gathering the information,the information submitted is,to the best of my knowledge and
belief,true,accurate,and complete. I am aware that there are significant penalties for submitting false information,
including the possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Dollnila Slater General Manager,Terminal&Pipelines
Signature Date signed
11 -- 1-7 -- 2c7s z2
EPA Form 3510-1(revised 3-19) Page 4

Attachment I
Topographical Map around facility

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Motiva Enterprises Raleigh Terminal Outfall 001

Motiva Enterprises LLC
Apex Terminal
NPDES Permit NC0022217
Loading Rack
Stormwater
Recovered ' Tank Farm
Product Sent Offsite Stormwater
SPCC Tank 10,000 gal (Diked Area)
•
Water Tank
Containment Pond '
Outfall 001
Unnamed Tributary to Middle Creek

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
Form U.S.Environmental Protection Agency
2C " EPA Application for NPDES Permit to Discharge Wastewater
NPDES EXISTING MANUFACTURING,COMMERCIAL,MINING,AND SILVICULTURE OPERATIONS
SECTION 1.OUTFALL LOCATION(40 CFR 122.21(g)(1))
1.1 Provide information on each of the facility's outfalls in the table below.
o Numbelr Receiving Water Name Latitude Longitude
.�
001 Unnamed Tributary to Mia 35° 42' 57" N 78° 48' 56" W
R
Q
SECTION 2.LINE DRAWING(40 CFR 122.21(g)(2))
2.1 Have you attached a line drawing to this application that shows the water flow through your facility with a water
3 balance?(See instructions for drawing requirements.See Exhibit 2C-1 at end of instructions for example.)
J Es
o ❑✓ Yes ❑ No
SECTION 3.AVERAGE FLOWS AND TREATMENT(40 CFR 122.21(g)(3))
3.1 For each outfall identified under Item 1.1,provide average flow and treatment information.Add additional sheets if
necessary.
**Outfall Number** 0o1
Operations Contibuting to Flow
Operation Average Flow
Stormwater 0.133 mgd
J
mgd
mgd
mgd
LLTreatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
An oil-water separator(OWS)receives water from the truck Vacuum Truck to offsite treatme
EPA Form 3510-2C(Revised 3-19) Page 1

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
3.1 *"Outfall Number**
cont. Operations Contributing to Flow
Operation Average Flow
mgd
mgd
mgd
mgd
Treatment Units
Description Code from Final Disposal of Solid or
(include size,flow rate through each treatment unit, Table 2C-1 Liquid Wastes Other Than
retention time,etc.) by Discharge
-a
m
0
U
d
E
is
m
F
-0 **Outfall Number**
Operations Contributing to Flow
o Operation Average Flow
a, mgd
a' mgd
mgd
mgd
Description Final Disposal of Solid or
(include size,flow rate through each treatment unit, Code from Liquid Wastes Other Than
Table 2C-1
retention time,etc.) by Discharge
3.2 Are you applying for an NPDES permit to operate a privately owned treatment works?
❑ Yes ❑✓ No 4 SKIP to Section 4.
n 3.3 Have you attached a list that identifies each user of the treatment works?
❑ Yes ❑ No
EPA Form 3510-2C(Revised 3-19) Page 2

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 4.INTERMITTENT FLOWS(40 CFR 122.21(g)(4))
4.1 Except for storm runoff,leaks,or spills,are any discharges described in Sections 1 and 3 intermittent or seasonal?
❑ Yes ❑✓ No 4 SKIP to Section 5.
4.2 Provide information on intermittent or seasonal flows for each applicable outfall.Attach additional pages,if necessary.
Outfall Operation Frec uency Flow Rate
Number (list) Average Average Long-Term Maximum Duration
Days/Week Months/Year Average Daily
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
cu
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
days/week months/year mgd mgd days
SECTION 5.PRODUCTION(40 CFR 122.21(g)(5))
5.1 Do any effluent limitation guidelines(ELGs)promulgated by EPA under Section 304 of the CWA apply to your facility?
❑ Yes ❑✓ No-4 SKIP to Section 6.
5.2 Provide the following information on applicable ELGs.
w ELG Category ELG Subcategory Regulatory Citation
.37
Q
a
5.3 Are any of the applicable ELGs expressed in terms of production(or other measure of operation)?
❑ Yes ❑✓ No 4 SKIP to Section 6.
O
5.4 Provide an actual measure of daily production expressed in terms and units of applicable ELGs.
Outfall Unit of
Operation,Product,or Material Quantity per Day
Number Measure
U)
0
-
U
O
0
EPA Form 3510-2C(Revised 3-19) Page 3

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 6.IMPROVEMENTS(40 CFR 122.21(g)(6))
6.1 Are you presently required by any federal,state,or local authority to meet an implementation schedule for constructing,
upgrading,or operating wastewater treatment equipment or practices or any other environmental programs that could
affect the discharges described in this application?
❑ Yes ❑✓ No 4 SKIP to Item 6.3.
6.2 Briefly identify each applicable project in the table below.
Affected Final Compliance Dates
Brief Identification and Description of Outfalls Source(s)of
oProject (list outfall Discharge Required Projected
number)
i 1=
0
cn
0_
a
6.3 Have you attached sheets describing any additional water pollution control programs(or other environmental projects
that may affect your discharges)that you now have underway or planned?(optional item)
❑ Yes 0 No ❑✓ Not applicable
SECTION 7.EFFLUENT AND INTAKE CHARACTERISTICS(40 CFR 122.21(g)(7))
See the instructions to determine the pollutants and parameters you are required to monitor and,in turn,the tables you must
complete. Not all applicants need to complete each table.
Table A.Conventional and Non-Conventional Pollutants
7.1 Are you requesting a waiver from your NPDES permitting authority for one or more of the Table A pollutants for any of
your outfalls?
❑ Yes ❑✓ No 4 SKIP to Item 7.3.
7.2 If yes,indicate the applicable outfalls below.Attach waiver request and other required information to the application.
Outfall Number Outfall Number Outfall Number
0 7.3 Have you completed monitoring for all Table A pollutants at each of your outfalls for which a waiver has not been
N requested and attached the results to this application package?
❑✓ Yes ❑ No;a waiver has been requested from my NPDES
permitting authority for all pollutants at all outfalls.
5 Table B.Toxic Metals,Cyanide,Total Phenols,and Organic Toxic Pollutants
.i 7.4 Do any of the facility's processes that contribute wastewater fall into one or more of the primary industry categories
listed in Exhibit 2C-3?(See end of instructions for exhibit.)
❑ Yes ❑✓ No 4 SKIP to Item 7.8.
7.5 Have you checked"Testing Required"for all toxic metals,cyanide,and total phenols in Section 1 of Table B?
❑ Yes ❑ No
7.6 List the applicable primary industry categories and check the boxes indicating the required GC/MS fraction(s)identified
in Exhibit 2C-3.
Primary Industry Category Required GC/MS Fraction(s)
(Check applicable boxes.)
❑Volatile ❑Acid ❑ Base/Neutral 0 Pesticide
❑Volatile ❑Acid 0 BaselNeutral ❑Pesticide
❑Volatile ❑Acid ❑Base/Neutral ❑Pesticide
EPA Form 3510-2C(Revised 3-19) Page 4

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
7.7 Have you checked"Testing Required"for all required pollutants in Sections 2 through 5 of Table B for each of the
GC/MS fractions checked in Item 7.6?
❑ Yes ❑ No
7.8 Have you checked"Believed Present"or"Believed Absent"for all pollutants listed in Sections 1 through 5 of Table B
where testing is not required?
ElYes ❑ No
7.9 Have you provided(1)quantitative data for those Section 1,Table B,pollutants for which you have indicated testing is
required or(2)quantitative data or other required information for those Section 1,Table B,pollutants that you have
indicated are"Believed Present"in your discharge?
ElYes ❑ No
7.10 Does the applicant qualify for a small business exemption under the criteria specified in the instructions?
❑ Yes- Note that you qualify at the top of Table B, ❑✓ No
0 then SKIP to Item 7.12.
al
7.11 Have you provided(1)quantitative data for those Sections 2 through 5,Table B,pollutants for which you have
o determined testing is required or(2)quantitative data or an explanation for those Sections 2 through 5,Table B,
y pollutants you have indicated are"Believed Present"in your discharge?
✓❑ Yes ❑ No
;; Table C.Certain Conventional and Non-Conventional Pollutants
7.12 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed on Table C
for all outfalls?
ElYes ❑ No
f0
c 7.13 Have you completed Table C by providing(1)quantitative data for those pollutants that are limited either directly or
indirectly in an ELG and/or(2)quantitative data or an explanation for those pollutants for which you have indicated
"Believed Present"?
d ❑✓ Yes ❑ No
w Table D.Certain Hazardous Substances and Asbestos
7.14 Have you indicated whether pollutants are"Believed Present"or"Believed Absent"for all pollutants listed in Table D for
all outfalls?
El Yes ❑ No
7.15 Have you completed Table D by(1)describing the reasons the applicable pollutants are expected to be discharged
and(2)by providing quantitative data,if available?
ElYes ❑ No
Table E.2,3,7,8-Tetrachlorodibenzo-p-Dioxin(2,3,7,8-TCDD)
7.16 Does the facility use or manufacture one or more of the 2,3,7,8-TCDD congeners listed in the instructions,or do you
know or have reason to believe that TCDD is or may be present in the effluent?
❑ Yes- Complete Table E. ❑✓ No- SKIP to Section 8.
7.17 Have you completed Table E by reporting qualitative data for TCDD?
❑ Yes ❑ No
SECTION 8.USED OR MANUFACTURED TOXICS(40 CFR 122.21(g)(9))
8.1 Is any pollutant listed in Table B a substance or a component of a substance used or manufactured at your facility as
an intermediate or final product or byproduct?
❑ Yes ElNo 4 SKIP to Section 9.
8.2 List the pollutants below.
c
2 0 1. 4. 7.
0
2. 5. 8.
co
3. 6. 9.
EPA Form 3510-2C(Revised 3-19) Page 5

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 9.BIOLOGICAL TOXICITY TESTS(40 CFR 122.21(g)(11))
9.1 Do you have any knowledge or reason to believe that any biological test for acute or chronic toxicity has been made
within the last three years on(1)any of your discharges or(2)on a receiving water in relation to your discharge?
�, ❑ Yes ❑ No 4 SKIP to Section 10.
i 9.2 Identify the tests and their'urnoses below.
Test(s) .. Submitted to NPDES Date Submitted
o Permitting Authority?
o TAE6C-LC50 Static 24hr El Yes ❑ No 06/21/2022
Acute
0
❑ Yes ❑ No
❑ Yes ❑ No
SECTION 10.CONTRACT ANALYSES(40 CFR 122.21(g)(12))
10.1 Were any of the analyses reported in Section 7 performed by a contract laboratory or consulting firm?
ElYes ❑ No 4 SKIP to Section 11.
10.2 Provide information for each contract laboratory or consulting firm below.
Laboratory Number 1 Laboratory Number 2 Laboratory Number 3
Name of laboratory/firm Microbac Fayetteville
Laboratory address 2592 Hope Mills Road
Fayetteville,NC 28306
U
0 Phone number
[phone]
Pollutant(s)analyzed Turbidity,Oil&Grease,
MTBE,Toluene,Benzene,
Ethylbenzene,Naphthalene,
Xylene,TSS
SECTION 11.ADDITIONAL INFORMATION(40 CFR 122.21(g)(13))
11.1 Has the NPDES permitting authority requested additional information?
c ❑ Yes ❑✓ No 4 SKIP to Section 12.
0
E 11.2 List the information requested and attach it to this application.
`0
1. 4.
0
2. 5.
3. 6.
EPA Form 3510-2C(Revised 3-19) Page 6

EPA Identification Number NPDES Permit Number Facility Name Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal OMB No.2040-0004
SECTION 12.CHECKLIST AND CERTIFICATION STATEMENT(40 CFR 122.22(a)and(d))
12.1 In Column 1 below,mark the sections of Form 2C that you have completed and are submitting with your application.
For each section,specify in Column 2 any attachments that you are enclosing to alert the permitting authority. Note
that not all applicants are required to corr,Dlete all sections or provide attachments.
Column 1 Column 2
❑✓ Section 1:Outfall Location ❑ w/attachments
❑✓ Section 2:Line Drawing ❑ w/line drawing ❑ w/additional attachments
171 Section 3:Average Flows and w/list of each user of
Treatment ❑ w/attachments Elprivately owned treatment
works
✓ Section 4: Intermittent Flows 0 w/attachments
❑✓ Section 5:Production ❑ w/attachments
w/optional additional
0Section 6: Improvements ❑ w/attachments ❑ sheets describing any
additional pollution control
plans
❑ w/request for a waiver and ❑ w/explanation for identical
supporting information outfalls
d w/small business exemption❑ request w/other attachments❑
N ❑ Section 7: Effluent and Intake 0 w/Table A ❑ w/Table B
Characteristics
0
❑ w/Table C ❑ w/Table D
d w/Table E ✓ w/analytical results as an
❑ ❑ attachment
= 171 Section 8:Used or Manufactured
�= Toxics ❑ w/attachments
❑✓ Section 9:Biological Toxicity ❑ w/attachments
r Tests
U
❑✓ Section 10:Contract Analyses ❑ wl attachments
❑✓ Section 11:Additional Information 0 w/attachments
Section 12:Checklist and
❑ Certification Statement ❑ w/attachments
12.2 Certification Statement
1 certify under penalty of law that this document and all attachments were prepared under my direction or supervision in
accordance with a system designed to assure that qualified personnel properly gather and evaluate the information
submitted.Based on my inquiry of the person or persons who manage the system,or those persons directly
responsible for gathering the information,the information submitted is,to the best of my knowledge and belief,true,
accurate,and complete.I am aware that there are significant penalties for submitting false information,including the
possibility of fine and imprisonment for knowing violations.
Name(print or type first and last name) Official title
Dollnila Slater General Manager,Terminal&Pipelines
Signature Date signed
li — — 24,,29
EPA Form 3510-2C(Revised 3-19) Page 7

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCOO22217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE A.CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(iii))1
Effluent Intake
Waiver (Optional)
Pollutant Requested Units Maximum Maximum Long-Term
(if apulicab
est (specify) Daily Monthly Average Daily Number of Long-Term Number of
Discharge Discharge Discharge Analyses Average Value Analyses
(required) (if available) (if available)
❑ Check here if you have applied to your NPDES permitting authority for a waiver for all of the pollutants listed on this table for the noted outfall.
1.
Biochemical oxygen demand ❑ Concentration
(BOD5) Mass
2 Chemical oxygen demand ❑ Concentration
(COD) Mass
Concentration
3. Total organic carbon(TOC) ❑✓
Mass
Concentration mg/L 27.2 19
4. Total suspended solids(TSS) ❑
Mass
Concentration
5. Ammonia(as N) ✓❑
Mass
6. Flow ❑ Rate mgd 0.133
Temperature(winter) ❑✓ °C °C
7.
Temperature(summer) ✓❑ °C °C
pH(minimum) ✓❑ Standard units s.u.
8.
pH(maximum) ✓❑ Standard units s.u.
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0. See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 9

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent
(optional) 1
Pollutant/Parameter Testing Units Long•Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Daily
D(req fireischargd a (ifavailablle) Discharge Analyses ischarge AValuee Analyses
(if available)
Check here if you qualify as a small business per the instructions to Form 2C and,therefore,do not need to submit quantitative data for any of the organic toxic pollutants in Sections
2 through 5 of this table.Note,however,that you must still indicate in the appropriate column of this table if you believe any of the pollutants listed are present in your discharge.
Section 1.Toxic Metals,Cyanide,and Total Phenols
Antimony,total Concentration
1.1 El 0 El
(7440-36-0) Mass
Arsenic,total Concentration
1.2 (7440-38-2) Mass
Beryllium,total Concentration
1.3 (7440-41-7) 0 ID Mass
Cadmium,total Concentration
1.4 El 0 El
(7440-43-9) Mass
Chromium,total Concentration
1.5 1:1 El ID
(7440-47-3) Mass
Copper,total Concentration
1.6 (7440 50 8) El 0 0
Mass
Lead,total Concentration
1.7 El 0(7439-92-1) Mass
Mercury,total Concentration
1.8 (7439-97-6) Mass
Nickel,total Concentration
1'9 El ID El
(7440-02-0) Mass
1.10 Selenium,total I:I Concentration
ID
(7782-49-2) Mass
Silver,total Concentration
1.11 1=1 El El
(7440-22-4) Mass
EPA Form 3510-2C(Revised 3-19) Page 11

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v)p
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
Dreq(required) (if available) Discharge Analyses Averageaily of of
ischarge Discharge Value Analyses
(if available)
Thallium,total ✓ Concentration
1.12 (7440-28-0) Mass
1.13 Zinc,total 0Concentration
(7440-66-6) Mass
1.14 Cyanide,total ❑ ❑ Concentration
(57-12-5) Mass
1.15 Phenols,total Concentration
Mass
Section 2.Organic Toxic Pollutants(GC/MS Fraction—Volatile Compounds)
1 Acrolein ✓ Concentration
2.1 (107 02 8) El ❑
Mass
2.2 Acrylonitrile 0 0Concentration
(107-13-1) Mass
Benzene ❑ Concentration
2.3 El 0
(71-43-2) Mass
2 4 Bromoform 0 Concentration
El 0
(75-25-2) Mass
2.5 Carbon tetrachloride ❑ 0Concentration
(56-23-5) Mass
Chlorobenzene ✓ Concentration
2.6 (108-90-7) El ❑
Mass
2.7 Chlorodibromomethane El0Concentration
0
(124-48-1) Mass
2.8 Chloroethane 0Concentration
El 0
(75-00-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 12

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
( of
Drequired)
if available) Discharge Analyses Averageaily of
ischargeValue Analyses
re cared
(if available)
2.9 2-chloroethylvinyl ether Concentration
(110-75-8) Mass
2.10 Chloroform(67-66-3) 0 0 0
Concentration
Mass
2.11 Dichlorobromomethane 0 Concentration
(75-27-4) Mass
1,1-dichloroethane � Concentration
2.12 (75-34-3) Mass
2.13 1,2-dichloroethane 0 0 El Concentration
(107-06-2) Mass
11-dichloroethylene � Concentration
2.14 (75-35-4) Mass
1,2-dichloropropane � � Concentration
2.15 (78-87-5) Mass
2.16 13-dichloropropylene 0 0 Concentration
(542-75-6) Mass
2.17 Ethylbenzene � Concentration
(100-41-4) Mass
Methyl bromide � Concentration
2.18 (74-83-9) Mass
2.19 Methyl chloride Concentration
(74-87-3) Mass
2.20 Methylene chloride El Concentration
(75-09-2) Mass
221 1,1,2,2-tetrachloroethane 0 0 Concentration
CI
(79-34-5) Mass
EPA Form 3510-2C(Revised 3-19) Page 13

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant]Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
aily of of
Discharge
DtaCalablge) Discharge Analyses AValuee Analyses
(if available)
Tetrachloroethylene Concentration
2.22 (127-18-4) Mass
2.23 Toluene Concentration
(108-88-3) Mass
2.24 1,2-trans-dichloroethylene Concentration
El El 0 I
(156-60-5) Mass
2.25 1 1,1-trichloroethane 0 Concentration
0 El
(71-55-6) Mass
2.26 1,1,2-trichloroethane 0 0 Concentration
(79-00-5) Mass
2.27 Trichloroethylene Concentration
(79-01-6) Mass
2.28 Vinyl chloride Concentration
0 0 0
(75-01-4) Mass
Section 3.Organic Toxic Pollutants(GCIMS Fraction—Acid Compounds)
3.1 2-chlorophenol Concentration
(95-57-8) Mass
3.2 2,4-dichlorophenol 0 Concentration
(120-83-2) Mass
3.3 2,4-dimethylphenol 0 Concentration
0 El
(105-67-9) Mass
3.4 4,6-dinitro-o-cresol Concentration
(534-52-1) Mass
3.5 2,4-dinitrophenol Concentration
(51-28-5) I I Mass
EPA Form 3510-2C(Revised 3-19) Page 14

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v)p
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long• Number
Present Absent Daily Monthly Term
(regof
of
Dscharuidge) ifavalabl)ischarge DisDcharge Analyses AValuee Analyses
(if available)
3.6 2-nitrophenol Concentration
El El 0
(88-75-5) Mass
4-nitrophenol Concentration
3.7 (100-02-7) Mass
3.8 p-chloro-m-cresol Concentration
(59-50-7) Mass
3.9 Pentachlorophenol ❑ Concentration
(87-86-5) Mass
3.10 Phenol Concentration
(108-95-2) Mass
3.11 2 4,6-trichlorophenol Concentration
(88-05-2) Mass
Section 4.Organic Toxic Pollutants(GCIMS Fraction—Base/Neutral Compounds)
4.1 Acenaphthene ❑ 0 Concentration
(83-32-9) Mass
4.2 Acenaphthylene ❑ Concentration
(208-96-8) Mass
•
4.3 Anthracene Concentration
ID El 0
(120-12-7) Mass
-
4.4 Benzidine Concentration
(92-87-5) Mass
4,5 Benzo(a)anthracene ElConcentration
(56-55-3) Mass
4.6 Benzo(a)pyrene 0 0 Concentration
(50-32-8) Mass
EPA Form 3510-2C(Revised 3-19) Page 15

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHBJOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
(required)
i Discharge (iischarge f available) Di Daily Discharge Analyses AverageValue Analyses
(if available)
4.7 3,4-benzofluoranthene 0 Concentration
El 0
(205-99-2) Mass
4.8 Benzo(ghi)perylene Concentration
El El 0
(191-24-2) Mass
Benzo(k)fluoranthene 1:1Concentration
4.9 (207-08-9) Mass
4.10 Bis(2-chloroethoxy)methane 0 Concentration
0 El
(111-91-1) Mass
4.11 Bis(2-chloroethyl)ether Concentration
(111-44-4) Mass
4.12 Bis(2-chloroisopropyl)ether Concentration
(102-80-1) Mass
4.13 Bis(2-ethylhexyl)phthalate 1:1Concentration
El El
(117-81-7) Mass
4.14 4-bromophenyl phenyl ether 0 0 Concentration
El
(101-55-3) Mass
4.15 Butyl benzyl phthalate 0 Concentration
0 El
(85-68-7) Mass
4.16 2-chloronaphthalene 0 El Concentration
(91-58-7) Mass
4-chlorophenyl phenyl ether 1=1 Concentration
4.17 El El
(7005-72-3) Mass
Chrysene El Concentration
4.18 (218-01-9) Mass
4.19 Dibenzo(a,h)anthracene 0 0 El Concentration
(53-70-3) Mass
EPA Form 3510-2C(Revised 3-19) Page 16

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EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long Number
Present Absent Daily Monthly Term
Daily
Discharge Discharge Discharge Analyses AverageValue Analyses
(required) (if available)
(if available)
4.33 Hexachlorobenzene Concentration
(118-74-1) Mass
4,34 Hexachlorobutadiene Concentration
(87-68-3) Mass
4.35 Hexachlorocyclopentadiene ❑ ❑ 0Concentration
(77-47-4) Mass
4.36 Hexachloroethane Concentration
(67-72-1) Mass
4.37 Indeno(1,2,3-cd)pyrene 0Concentration
(193-39-5) Mass
4.38 Isophorone Concentration
(78-59-1) Mass
4.39 Naphthalene Concentration
(91-20-3) Mass
4.40 Nitrobenzene Concentration
El El El
(98-95-3) Mass
4.41 N-nitrosodimethylamine ❑ Concentration
(62-75-9) Mass
4.42 N-nitrosodi-n-propylamine Concentration
(621-64-7) Mass
4.43 N-nitrosodiphenylamine Concentration
(86-30-6) Mass
4.44 Phenanthrene Concentration
(85-01-8) Mass
Pyrene Concentration
4.45 (129-00-0) Mass
EPA Form 3510-2C(Revised 3-19) Page 18

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))l
Presence or Absence Intake
(check one) Effluent
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
of of
D(req isch edge Df available) Discharge i D harge aily
Analyses AValuee Analyses
ui ) (if available)
4.46 1 2 4-trichlorobenzene Concentration
(120-82-1) Mass
Section 5.Organic Toxic Pollutants(GC/MS Fraction—Pesticides)
5.1 Aldrin Concentration
(309-00-2) Mass
a-BHC Concentration
5.2 (319-84-6) 0 0 0
Mass
R-BHC Concentration
5.3 (319-85-7) Mass
y-BHC Concentration
5.4 0 El El
(58 89 9) Mass
b-BHC Concentration
5.5 (319-86-8) 0 0 0 Mass
5.6 Chlordane Concentration
(57-74-9) Mass
4 4'-DDT Concentration
5.7 (50-29-3) Mass
5.8 4 4'-DDE Concentration
El 0 El
(72-55-9) Mass
5.9 4 4'-DDD Concentration
El 0 El
(72-54-8) Mass
Dieldrin Concentration
5.10 (60 57 1) 0 0 0
Mass
a-endosulfan Concentration
5.11 El El 0
(115-29-7) Mass
EPA Form 3510-2C(Revised 3-19) Page 19

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v))1
Presence or Absence
(check one) Effluent Intake
(optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long- Number
Present Absent Daily Monthly Term
of
Discharge DtaCalablisharge) Die Daily harge Analyses AValuee Analyses
( ui (if available)
13-endosulfan Concentration
15.12 (115 29 7) 0 0 0 Mass
Endosulfan sulfate Concentration
5.13 (1031-07-8) ❑ ❑ ❑ Mass
Endrin Concentration
5.14 (72 20 8) ❑ El ❑ Mass
Endrin aldehyde � 0 ❑ Concentration
5.15 (7421-93-4) Mass
5.16 Heptachlor ❑ ❑ 0 Concentration
(7644-8) Mass
Heptachlor epoxide Concentration
5.17 (1024-57-3) 0 ❑ ❑✓ Mass
PCB-1242 Concentration
5.18 (53469-21-9) ❑ 0 0 Mass
PCB-1254 Concentration
5.19 (11097-69-1) 0 0 0 Mass
PCB-1221 Concentration
5.20 (11104-28-2) 0 0 ✓❑
Mass
PCB-1232 Concentration
5.21 (11141-16-5) ❑ 0 0 Mass
PCB-1248 Concentration
5.22 (12672-29-6) 0 0 0 Mass
PCB-1260 Concentration
5.23 (11096-82-5) 0 0 0 Mass
PCB-1016 Concentration
5.24 (12674-11-2) ❑ 0 ✓❑ Mass
EPA Form 3510-2C(Revised 3-19) Page 20

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE B.TOXIC METALS,CYANIDE,TOTAL PHENOLS,AND ORGANIC TOXIC POLLUTANTS(40 CFR 122.21(g)(7)(v)p
Presence or Absence Intake
(check one) Effluent (optional)
Pollutant/Parameter Testing Units Long-Term
(and CAS Number,if available) Required Believed Believed (specify) Maximum Maximum Average Number Long• Number
Present Absent Daily Monthly Dail of Term of
Discharge Discharge Discharlge Analyses Average Analyses
(required) (if available) (if avails ge) Value
Toxaphene Concentration
5.25 (8001-35-2) 0 0 0 •
Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 21

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
- (Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
(required) Discharge Discharge Analyses Value Analyses
(if available) (if available)
❑ Check here if you believe all pollutants on Table C to be present in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
1.71
Check here if you believe all pollutants on Table C to be absent in your discharge from the noted outfall.You need not complete the"Presence or Absence"column of Table C for
each pollutant.
1 Bromide ❑ 0 Concentration
(24959-67-9) Mass
Chlorine,total Concentration
2. residual 0 ❑ Mass
Concentration
3. Color 0 0 Mass
Concentration
4. Fecal coliform ❑ 0 Mass
5 Fluoride 0 ❑ Concentration
(16984-48-8) Mass
Concentration
6 Nitrate-nitrite ❑ 0 Mass
Nitrogen,total Concentration
7' organic(as N) 0 ❑ Mass
Concentration
8. Oil and grease ❑ 0 Mass
Phosphorus(as Concentration
9' P),total(7723-14-0) ❑ ❑ Mass
10. Sulfate(as SO4) ❑ 0 Concentration
(14808-79-8) Mass
Concentration
11. Sulfide(as S) 0 0 Mass
EPA Form 3510-2C(Revised 3-19) Page 23

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
(required) Discharge Discharge Analyses Value Analyses
(if available) (if available)
12. Sulfite(as SO3) ❑ 0 Concentration
(14265-45-3) Mass
13. Surfactants ❑ 0
Concentration
Mass
14. Aluminum,total ❑ 0 Concentration
(7429-90-5) Mass
15. Barium,total ❑ 0 Concentration
(7440-39-3) Mass
16. Boron,total ❑ 0 Concentration
(7440-42-8) Mass
17 Cobalt,total ❑ 0 Concentration
(7440-48-4) Mass
18 Iron,total ❑ ❑ Concentration
(7439-89-6) Mass
19 Magnesium,total ❑ 0 Concentration
(7439-95-4) Mass
Molybdenum, _Concentration
20. total 0 0 Mass
(7439-98-7)
21. Manganese,total ❑ 0 Concentration
(7439-96-5) Mass
22. Tin,total ❑ 0 Concentration
(7440-31-5) Mass
Titanium,total Concentration
23. (7440-32-6) El
Mass
EPA Form 3510-2C(Revised 3-19) Page 24

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NCOO22217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE C.CERTAIN CONVENTIONAL AND NON CONVENTIONAL POLLUTANTS(40 CFR 122.21(g)(7)(vi))1
Presence or Absence
(check one) Effluent Intake
(Optional)
Pollutant Units Maximum Long-Term
Believed Believed (specify) Maximum Daily Long-Term
Present Absent Discharge Monthly Average Daily Number of Average Number of
(required) Discharge Discharge Analyses Analyses
(if available) (if available) V21Ue
24. Radioactivity
Concentration
Alpha,total 0 ❑✓
Mass
Concentration
Beta,total ❑ ❑✓
Mass
Concentration
Radium,total 0 0 Mass
Concentration
Radium 226,total 0 0
Mass
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e., methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 25

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
1. Asbestos ❑ ❑✓
2. Acetaldehyde ❑ ❑✓
3. Allyl alcohol ❑ ❑✓
4. Allyl chloride 0 ❑✓
5. Amyl acetate ❑ ❑✓
6. Aniline ❑ ❑✓
7. Benzonitrile ❑ ✓❑
8. Benzyl chloride ❑ ❑✓
9. Butyl acetate ❑ ❑✓
10. Butylamine ❑ ❑✓
11. Captan ❑ ❑✓
12. Carbaryl ❑ ✓❑
13. Carbofuran 0 ✓❑
14. Carbon disulfide 0 ❑✓
15. Chlorpyrifos ❑ ❑✓
16. Coumaphos ❑ ❑✓
17. Cresol ❑ ❑✓
18. Crotonaldehyde ❑ ❑✓
19. Cyclohexane ❑ ❑✓
EPA Form 3510-2C(Revised 3-19) Page 27

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal onOMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
20. 2,4-D(2,4-dichlorophenoxyacetic acid) 0 ❑✓
21. Diazinon ❑ ✓❑
22. Dicamba 0 ❑✓
23. Dichlobenil 0 ❑✓
24. Dichlone ❑ ❑✓
25. 2,2-dichloropropionic acid ❑ ❑✓
26. Dichlorvos ❑ ❑✓
27. Diethyl amine ❑ ❑✓
28. Dimethyl amine 0 ❑✓
29. Dintrobenzene 0 ❑✓
30. Diquat ❑ ✓❑
31. Disulfoton ❑ ❑✓
32. Diuron ❑ ❑✓
33. Epichlorohydrin 0 0
34. Ethion ❑ ❑✓
35. Ethylene diamine 0 0
36. Ethylene dibromide 0 0
37. Formaldehyde 0 0
38. Furfural 0 0
EPA Form 3510-2C(Revised 3-19) Page 28

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motive Raleigh Terminal 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))l
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
39. Guthion ❑ ❑✓
40. Isoprene ❑ ❑✓
41. Isopropanolamine 0 ❑✓
42. Kelthane 0 ✓❑
43. Kepone 0 ❑✓
44. Malathion ❑ ❑✓
45. Mercaptodimethur 0 ❑✓
46. Methoxychlor ❑ ❑✓
47. Methyl mercaptan ❑ ❑✓
48. Methyl methacrylate 0 ❑✓
49. Methyl parathion 0 ❑✓
50. Mevinphos ❑ ✓❑
51. Mexacarbate 0 ❑✓
52. Monoethyl amine 0 ✓❑
53. Monomethyl amine ❑ ❑✓
54. Naled ❑ ❑✓
55. Naphthenic acid 0 ❑✓
56. Nitrotoluene ❑ ✓❑
57. Parathion ❑ ❑✓
EPA Form 3510-2C(Revised 3-19) Page 29

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 122.21(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
58. Phenolsulfonate ❑ ❑✓
59. Phosgene 0 ❑✓
60. Propargite ❑ ❑✓
61. Propylene oxide 0 ❑✓
62. Pyrethrins ❑ 0
63. Quinoline 0 ❑✓
64. Resorcinol ❑ ❑✓
65. Strontium ❑ ❑✓
66. Strychnine 0 ❑✓
67. Styrene 0 ❑✓
68 2,4 5-T(2,4,5-trichlorophenoxyacetic ❑
acid)
69. TDE(tetrachlorodiphenyl ethane) 0 ❑✓
70. 2,4,5-TP[2-(2,4,5-trichlorophenoxy) ❑
propanoic acid]
71. Trichlorofon ❑ 0
72. Triethanolamine ❑ ❑✓
73. Triethylamine ❑ ❑✓
74. Trimethylamine 0 ❑✓
75. Uranium ❑ ❑✓
76. Vanadium 0 ❑✓
EPA Form 3510-2C(Revised 3-19) Page 30

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE D.CERTAIN HAZARDOUS SUBSTANCES AND ASBESTOS(40 CFR 12221(g)(7)(vii))1
Presence or Absence
Pollutant (check one) Available Quantitative Data
Believed Believed Reason Pollutant Believed Present in Discharge (specify units)
Present Absent
77. Vinyl acetate ❑ ❑✓
78. Xylene ❑ ❑✓
79. Xylenol ❑ ❑✓
80. Zirconium 0 ❑✓
1 Sampling shall be conducted according to sufficiently sensitive test procedures(i.e.,methods)approved under 40 CFR 136 for the analysis of pollutants or pollutant parameters or
required under 40 CFR chapter I,subchapter N or 0.See instructions and 40 CFR 122.21(e)(3).
EPA Form 3510-2C(Revised 3-19) Page 31

EPA Identification Number NPDES Permit Number Facility Name Outfall Number Form Approved 03/05/19
NC0022217 Motiva Raleigh Terminal 001 OMB No.2040-0004
TABLE E.2,3,7,8 TETRACHLORODIBENZO P DIOXIN(2,3,7,8 TCDD)(40 CFR 122.21(g)(7)(viii))
TCDD Presence or
Congeners Absence
Pollutant Used or (check one) Results of Screening Procedure
Manufactured Believed Believed
Present Absent
2,3,7,8-TCDD ❑ ❑ ❑✓
EPA Form 3510-2C(Revised 3-19) Page 33

Attachment II
Detailed Sampling Results
August 2019 - August 2022

Detailed Sampling Results
August 2019 -August 2022
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month Day Year Comment Parameter Value Units
8 8 2019 00070-Turbidity 5.6 ntu
11 20 2019 00070-Turbidity 2.3 ntu
12 19 2019 00070-Turbidity 16 ntu
1 10 2020 00070 -Turbidity 11 ntu
2 13 2020 00070 -Turbidity 7 ntu
5 6 2020 00070-Turbidity 5.8 ntu
8 20 2020 00070-Turbidity 12 ntu
9 21 2020 00070-Turbidity 7.7 ntu
10 21 2020 00070- Turbidity 0.15 ntu
1 1 14 2021 00070 -Turbidity 7.3 ntu
2 23 2021 00070 -Turbidity 9.4 ntu
6 8 2021 00070-Turbidity 3.7 ntu
7 12 2021 00070 -Turbidity 24 ntu
11 3 2021 00070 -Turbidity 10 ntu
1 7 2022 00070 -Turbidity 11 ntu
3 18 2022 00070 -Turbidity 8 ntu
4 14 2022 00070-Turbidity 4.7 ntu
6 21 2022 00070 -Turbidity 6 ntu
8 25 2022 00070-Turbidity 4.1 ntu
8 8 2019 00556 - Oil & Grease <5 mg/I
11 20 2019 00556 - Oil & Grease <5 mg/I
12 19 2019 00556-Oil & Grease <5 mg/I
1 10 2020 00556 -Oil & Grease <5 mg/I
2 13 2020 00556 -Oil & Grease <5.6 mg/I
5 6 2020 00556 -Oil & Grease 5.7 mg/I
8 20 _ 2020 00556 -Oil & Grease <5 mg/I
9 21 2020 00556-Oil & Grease <5 mg/I
10 21 2020 00556 - Oil & Grease <5 mg/I
1 14 2021 00556 -Oil & Grease <5 mg/I
2 23 2021 00556 -Oil & Grease <5 mg/I
6 8 2021 00556 -Oil & Grease <5 mg/I
7 12 2021 00556 -Oil& Grease <5 mg/I
11 3 2021 00556 -Oil & Grease <5 mg/I
1 7 2022 00556 - Oil & Grease <5 mg/I
3 18 2022 00556-Oil & Grease <5 mg/I
4 14 2022 00556 - Oil &Grease <4.8 mg/I
6 21 2022 00556 - Oil & Grease <4.9 mg/I
8 25 2022 00556 - Oil & Grease <5 mg/I
11 20 2019 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
12 19 2019 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
1 10 2020 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
2 13 2020 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
5 6 2020 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
8 20 2020 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
9 21 2020 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
10 21 2020 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
1 14 2021 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
2 23 2021 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
Page 1 of 5

1
Detailed Sampling Results
August 2019 -August 2022
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month Day Year Comment Parameter Value Units
6 8 2021 22417- Methyl Tert-Butyl Ether(MTBE) <1 ugh'
7 12 2021 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
11 3 2021 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
1 7 2022 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
3 18 2022 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
4 14 2022 22417- Methyl Tert-Butyl Ether(MTBE) <1 ug/I
6 21 2022 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
8 25 2022 22417 - Methyl Tert-Butyl Ether(MTBE) <1 ug/I
8 8 2019 34010 -Toluene <1 ug/I
11 20 2019 34010 -Toluene <1 ug/I
12 19 2019 34010 -Toluene <1 ug/I
1 10 2020 34010-Toluene <1 ug/I
2 13 2020 34010 -Toluene <1 ug/I
5 6 2020 34010-Toluene <1 ug/I
8 20 2020 34010 -Toluene <1 ug/I
9 21 2020 34010-Toluene <1 ugh!
10 21 2020 34010-Toluene <1 ug/I
1 14 2021 34010-Toluene <1 ug/l
2 23 2021 34010-Toluene <1 ug/I
6 8 2021 34010 -Toluene <1 ug/I
7 12 2021 34010 -Toluene <1 ug/I
11 3 2021 34010 -Toluene <1 ug/I
1 7 2022 34010 -Toluene <1 ug/I
3 18 2022 34010-Toluene <1 ug/I
4 14 2022 34010-Toluene <0.5 ug/I
6 21 2022 34010 -Toluene <0.5 ug/I
1 8 25 2022 34010-Toluene <0.5 ug/I
8 8 2019 34030 - Benzene <1 ug/I
11 20 2019 34030 - Benzene <1 ug/I
12 19 2019 34030- Benzene <1 ug/I
1 10 2020 34030- Benzene <1 ug/I
2 13 2020 34030 - Benzene <1 ug/I
5 6 2020 34030- Benzene <1 ug/I
8 20 2020 34030- Benzene <1 ug/I
9 21 2020 34030 - Benzene <1 ug/I
10 21 2020 34030 - Benzene <1 ug/I
1 14 2021 34030 - Benzene <1 ug/I
2 23 2021 34030- Benzene <1 ug/I
6 8 2021 34030 - Benzene <1 ug/I
7 12 2021 34030-Benzene <1 ug/I
11 3 2021 34030 - Benzene <1 ug/I
1 7 2022 34030 - Benzene <1 ug/I
3 18 2022 34030 -Benzene <1 ug/I
4 14 2022 34030 - Benzene <0.5 ug/I
6 21 2022 _ 34030 -Benzene <0.5 ug/I
8 25 2022 34030-Benzene <0.5 ug/I
8 8 2019 34371 - Ethylbenzene <1 ug/I
11 20 2019 34371 - Ethylbenzene <1 ug/I
Page 2 of 5

Detailed Sampling Results
August 2019 -August 2022
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month Day Year Comment Parameter Value Units
12 19 2019 34371 -Ethylbenzene <1 ug/I
1 10 2020 34371 -Ethylbenzene <1 ug/I
2 13 2020 34371 -Ethylbenzene <1 ug/l
5 6 2020 34371 - Ethylbenzene <1 ug/I 1
8 20 2020 34371 - Ethylbenzene <1 ug/I
9 21 2020 34371 -Ethylbenzene <1 ug/I
10 21 2020 34371 -Ethylbenzene <1 ugh'
1 14 2021 34371 -Ethylbenzene <1 ugh'
2 23 2021 34371 - Ethylbenzene <1 ugh'
6 8 2021 34371 - Ethylbenzene <1 ugh'
7 12 2021 34371 - Ethylbenzene <1 ug/I
11 3 2021 34371 - Ethylbenzene <1 ug/I
1 7 2022 34371 -Ethylbenzene <1 ug/I
3 18 2022 34371 -Ethylbenzene <1 ug/I
4 14 2022 34371 - Ethylbenzene <0.5 ugh'
6 21 2022 34371 -Ethylbenzene <0.5 ug/I
8 25 2022 34371 -Ethylbenzene <0.5 ugh'
8 8 2019 34696-Naphthalene <1 ugh
11 20 2019 34696-Naphthalene <1 ug/I
12 19 2019 34696-Naphthalene <1 ug/I
1 10 2020 34696 - Naphthalene <1 ugh'
2 13 2020 34696 - Naphthalene <1 ug/I
5 6 2020 34696- Naphthalene <1 ugh'
8 20 2020 34696-Naphthalene <1 ug/I
9 21 2020 34696-Naphthalene <1 ug/I
10 21 2020 34696-Naphthalene <1 ug/I
1 14 2021 34696-Naphthalene <1 ug/I
2 23 2021 34696- Naphthalene <1 ug/I
6 8 2021 34696 -Naphthalene <1 ug/l
7 12 2021 34696 -Naphthalene <1 ug/I
11 3 2021 34696- Naphthalene <1 ugh'
1 7 2022 34696- Naphthalene <1 ug/I
3 18 2022 34696- Naphthalene <1 ug/I
4 14 2022 34696-Naphthalene <1 ug/I
6 21 2022 34696-Naphthalene <1 ug/I
8 25 2022 34696-Naphthalene <1 ug/I
8 8 2019 50050- Flow, in conduit or thru treatment plant 0.231 mgd
11 20 2019 50050-Flow, in conduit or thru treatment plant 0.294 mgd '
12 19 2019 50050-Flow, in conduit or thru treatment plant 0.231 mgd
1 10 2020 50050- Flow, in conduit or thru treatment plant 0.168 mgd
2 13 2020 50050-Flow, in conduit or thru treatment plant 0.294 mgd
5 6 2020 50050- Flow, in conduit or thru treatment plant 0.21 mgd
8 20 2020 50050- Flow, in conduit or thru treatment plant 0.168 mgd
9 21 2020 50050- Flow, in conduit or thru treatment plant 0.378 mgd
10 21 2020 50050- Flow, in conduit or thru treatment plant 0.21 mgd
1 14 2021 50050- Flow, in conduit or thru treatment plant 0.252 mgd
2 23 2021 50050- Flow, in conduit or thru treatment plant 0.294 mgd
6 8 2021 50050-Flow, in conduit or thru treatment plant _ 0.273 mgd
Page 3 of 5

Detailed Sampling Results
August 2019 -August 2022
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month Day Year Comment Parameter Value Units
7 12 2021 50050- Flow, in conduit or thru treatment plant 0.21 mgd
11 3 2021 50050- Flow, in conduit or thru treatment plant 0.288 mgd
1 7 2022 50050- Flow, in conduit or thru treatment plant 0.42 mgd
3 18 2022 50050- Flow, in conduit or thru treatment plant 0.126 mgd
4 14 2022 50050- Flow, in conduit or thru treatment plant 0.25 mgd
6 21 2022 50050 - Flow, in conduit or thru treatment plant 0.168 mgd
8 25 2022 50050- Flow, in conduit or thru treatment plant 0.336 mgd
8 8 2019 81551 -Xylene (mix of m+o+p) <1 ug/I
11 20 2019 81551 -Xylene (mix of m+o+p) <1 ug/I
12 19 2019 81551 -Xylene (mix of m+o+p) <1 ug/I
1 10 2020 81551 -Xylene (mix of m+o+p) <1 ug/I I
2 13 2020 81551 -Xylene (mix of m+o+p) <1 ug/I
5 6 2020 81551 -Xylene (mix of m+o+p) <1 ug/I
8 20 2020 81551 -Xylene (mix of m+o+p) <1 ug/I
9 21 2020 81551 -Xylene(mix of m+o+p) <1 ug/I
10 21 2020 81551 -Xylene (mix of m+o+p) <1 ug/I
1 14 2021 81551 -Xylene (mix of m+o+p) <1 ug/I
2 23 2021 81551 -Xylene (mix of m+o+p) <1 ug/I 1
6 8 2021 81551 -Xylene (mix of m+o+p) <1 ug/I
7 12 2021 81551 -Xylene (mix of m+o+p) <1 ug/I�
11 3 2021 81551 -Xylene (mix of m+o+p) <1 ug/I
1 7 2022 81551 -Xylene (mix of m+o+p) <1 ug/I
3 18 2022 81551 -Xylene (mix of m+o+p) <1 ug/I
4 14 2022 81551 -Xylene (mix of m+o+p) <1 ug/I
6 21 2022 81551 -Xylene (mix of m+o+p) <1 ug/I
8 25 2022 81551 -Xylene (mix of m+o+p) <1 ug/I
8 8 2019 C0530 -Solids, Total Suspended - Concentration 5.33 mg/I
11 20 2019 C0530 -Solids, Total Suspended -Concentration <4.17 mg/I
12 19 2019 C0530 -Solids, Total Suspended -Concentration <4.17 mg/I
1 10 2020 C0530 -Solids, Total Suspended -Concentration <4.17 mg/I
2 13 2020 C0530 - Solids, Total Suspended - Concentration 2.56 mg/I
5 6 2020 C0530 -Solids, Total Suspended - Concentration 2.95 mg/I
8 20 2020 C0530 -Solids, Total Suspended - Concentration 7.2 mg/I
9 21 2020 C0530 -Solids, Total Suspended -Concentration 3.67 mg/I
10 21 2020 C0530 - Solids, Total Suspended -Concentration <2.55 mg/I
1 14 2021 C0530 -Solids, Total Suspended -Concentration <2.58 mg/I
2 23 2021 C0530 -Solids, Total Suspended - Concentration 2.66 mg/I
6 8 2021 C0530 -Solids, Total Suspended -Concentration 8.88 mg/I
7 12 2021 C0530 -Solids, Total Suspended - Concentration 18.4 mg/I
11 3 2021 C0530 -Solids, Total Suspended - Concentration 3.74 mg/I
1 7 2022 C0530 - Solids, Total Suspended - Concentration 27.2 mg/I
3 18 2022 C0530 -Solids, Total Suspended -Concentration <2.51 mg/I
4 14 2022 C0530 - Solids, Total Suspended - Concentration <2.5 mg/I
6 21 2022 C0530 -Solids, Total Suspended - Concentration 5.16 mg/I
8 25 2022 C0530 - Solids, Total Suspended - Concentration 6.1 mg/I
5 6 2020 TAE6C- LC50 Static 24hr Acute Pimephales >100% percent
6 22 2021 TAE6C - LC50 Static 24hr Acute Pimephales >100% percent
6 21 2022 TAE6C- LC50 Static 24hr Acute Pimephales >100% percent
Page 4 of 5

Detailed Sampling Results
August 2019 -August 2022
Motiva Enterprises, LLC
Apex, NC
Permit No. NC0022217
Month Day Year Comment Parameter Value Units
Data is shown for all months with recorded flows sufficient for sampling.
Page 5 of 5