Loading...
HomeMy WebLinkAboutWQ0007026_Monitoring - 09-2022_20221026Monitoring Report Submittal Permit Number #* Name of Facility:* Month: * September Report Information Type * GW-59 WQ0007026 Sanford Health & Rehabilitation Confirmation Email Address:* Biowater@aol.com Name of Submitter: * Randall Jarrell Signature: Year:* 2022 Upload Document* SHR MW's 9-8-22.pdf PDF Only 6.93M B Please upload one PDF containing all applicable monitoring reports (i.e., NDMR, NDAR-1, NDAR-2, NDMLR, GW-59). Date of submittal: 10/26/2022 This will be filled in automatically Initial Review Reviewer: Gerald, Wanda Is the project number correct?* WQ0007026 Is the monitoring report accepted?* Yes No Regional Office* Raleigh Reviewer: _anonymous Review Date: 11/14/2022 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: OF ENVIRONMENT & NATURAL RESOURCES IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM qfr.EPARTMENT 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 7333221 FACILITY INFORMATION Please Print Clearly or Type ERMIT Number: Expiration Date: Facility Name: Sanford Health & Rehabiitation on -Discharge WQ0007026 UIC NPDES Other Permit Name (if different): W00007026 Facility Address: 4400 Ferrell Road TYPE OF PERMITTED OPERATION BEING MONITORED anford NC 27330 County Lee El Lagoon ❑ Remediation: Infiltration Gallery ® Spray Field ❑ Remediation: ontact Person: Randall Jarrell I Telephone#: 919-210-2500 ❑ Rotary Distributor El Land Application of Sludge ell Location/Site Name: Lee County No. of wells to be sampled: 3 ElWater Source Heat Pump ElOther: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-1 Date sample collected: 9-8-22 FIELD ANALYSES: WAS Well Depth: 100 ft. Well Diameter:2 in. pH 5.28 units Temp. 18.4 °C DRY at Depth to Water Level: 13.5ft. below measuring point Screened Interval: ft. to ft. Spec. Cond. µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor sampling,check Volume of water pumped/bailed before sampling: 25 gallons Appearance here: Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO ❑ LABORATORY INFORMATION Date sample analyzed: 9/8/22 - 9/22/22 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N <0.017 mg/I Pb - Lead mg/I Coliform: MF Fecal 1.0 /100ml Nitrate (NO3) as N 3.2 mg/I Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.058 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 56 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC 31 rng/I Ca - Calcium mg/I Chloride 6.4 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen; NH3 as N; Ammonia Nitrogen, Total) Mn -Manganese mgll method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Randall Jarrell - ORC Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or 1-0 1,(. 1 z-2- ;Date) GW-59 Rev.1/2007 (9 �(7;.(P www.encolabs.com AN L YTICAL RESULTS .... -...,. mremmc ..... ...,-_ ��mrm Description: MW-1 Lab Sample ID:CF11320-01 Received: 09/08/22 12:45 Matrix: Ground Water Sampled:09/08/22 11:00 Work Order: CF11320 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analvte rCAS Numberl Results Flao Units DF MDL PQL Batch Method Analyzed gy Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,1,1-Trichloroethane [71-55-6]^ < 0,15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,1,2-Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0,050 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0,25 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.S0 2119029 EPA 8260D 09/20/22 10:12 RKY 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2,4-Trimethyl benzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2-Dichlorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2-Dichloroethane [107-06-2]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,2-Dichloropropane [78-87-5]^ < 0.098 ug/L 1 0.098 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,3-Dichlorobenzene[541-73-I]^ < 0.092 ug/L 1 0.092 0,50 2119029 EPA 8260D 09/20/22 10:12 RKY 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 1,4-Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 2,2-Dichloropropane [594-20-7]^ < 0.12 ug/L 1 0.12 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY 4-Chlorotoluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY 4-Isopropyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Benzene[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Bromobenzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Bromochloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Bromodichloromethane [75-27-4]^ < 0,010 ug/L 1 0.010 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Bromomethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Carbon Tetrachloride[56-23-5]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Chlorobenzene [108-90-7]^ < 0.069 ug/L 1 0.069 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Chloroethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Chloroform [67-66-3]A 0.27 JB ug/L 1 0.083 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY J-01 Chloromethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY cis- 1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY cis-1,3-Dichloropropene[10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Dichlorodifluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Ethylbenzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Isopropyl Ether[108-20-3]^ < 0.20 ug/L 1 0.20 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Isopropyl benzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Methyl-tert-Butyl Ether[1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. Page 4 o 1 9 uuiwumuuu iVNuuuu W (S=a uumwi�tlmmmwmomm www.encolabs.com ANALYTICAL RESULTS �I�HM�NmI XMMf�ItlmmMBMm�IM1� Description: MW-1� Lab Sample ID: CF11320-01 Received: 09/08/22 12:45 Matrix: Ground Water Sampled: 09/08/22 11:00 Work Order: CFI 1320 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte (NC 5911 Analyte rCAS Numberl Results Flag Units OF MDL POLL Batch Method Analyzed gy Notes Naphthalene[91-20-3]^ < 0.086 ug/L 1 0.086 0,50 2I19029 EPA 8260D 09/20/22 10:12 RKY n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY n-PropylBenzene [103-65-I]^ < 0.073 ug/L 1 0.073 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY sec -Butyl benzene [135-98-8]^ < 0.053 ug/L 1 0.053 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Toluene [108-88-3]^ < 0.053 ug/L 1 0.053 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY trans- 1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY trans-1,3-Dichloropropene[10061-02-6]1 < 0.080 ug/L 1 0.080 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Trichlorofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 2119029 EPA 8260D 09/20/22 10:12 RKY Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Xylenes (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 2I19029 EPA 8260D 09/20/22 10:12 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Analyzed By Notes 4-8romofluorobenzene 54 1 50.0 108 % 53-136 2119029 EPA 8260D 09120122 10:12 RKY Dibromofluoromethane 43 1 50.0 87 % 67-129 2119029 EPA 8260D 09120122 10:12 RKY Toluene-d8 44 1 50.0 89 % 59-134 2119029 EPA 8260D 09120122 10:12 RKY Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units DF MDL POL Batch Method Analyzed My Notes Ammonia as N [7664-41-7]^ < 0.045 mg/L 1 0.045 0.10 2I09020 EPA 350.1 09/09/22 14:10 MSE Chloride [16887-00-6]^ 7.7 mg/L 1 1.9 5.0 2I13012 SM 4500CIE-2011 09/13/22 12:06 MSE Nitrate as N [14797-55-8] 3.2 D mg/L 2 0.082 0.20 [CALC] EPA 353.2 09/12/22 13:55 MSE Nitrate/Nitrite as N ^ 3.2 D mg/L 2 0.082 0.20 2I12010 EPA 353.2 09/12/22 13:55 MSE Nitrite as N [14797-65-0]^ < 0,017 mg/L 1 0.017 0.10 2108026 EPA 353.2 09/08/22 16:32 MSE Phosphorus [7723-14-0]^ 0.058 J mg/L 1 0.025 0.10 2I15018 EPA 365.4 09/16/22 17:20 MSE Total Dissolved Solids^ 56 mg/L 1 50 50 2I15028 SM 2540C-2011 09/15/22 17:00 DMJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 77 Analyte rCAS Numberl Results Flag Units OF MDL POL Batch Method Analyzed ffy Notes Coliform, Fecal^ 1.0 MPN/100 1 1.0 2I12021 Colilert 18 09/09/22 11:34 MJY mL Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analyte rCAS Number] Results Flag Units DF MDL POL Batch Method Analyzed By Notes Total Organic Carbon^ 31 mg/L 1 0.90 1.0 2I22009 SM 531OB-2011 09/22/22 21:38 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 5 Of 19 SUBMIT FORM ON YELLOW PAPER ONLY GROUNDWATER QUALITY MONITORING: "gDEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES IVISION OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM 617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 7333221 FACILITY INFORMATION Please Print Clearly or Type ERMIT Number: Expiration Date: Facility Name: Sanford Health & Rehabiitation on -Discharge WQ0007026 UIC NPDES Other Permit Name (if different): WQ0007026 Facility Address: 4400 Ferrell Road TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Sanford NC 27330 County Lee ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#: 919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Lee County No. of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-4 Date sample collected: 9-8-22 FIELD ANALYSES: WAS Well Depth: 32.85ft. Well Diameter:2 in. H 6.96 p units Temp. 18.1 °C DRY at Depth to Water Level: 11.Oft. below measuring point Screened Interval: ft. to ft. Spec. Cond. µMhos time of Measuring Point is 3 ft. above land surface Relative M.P. Elevation: ft. Odor sampling, check Volume of water pumped/bailed before sampling: 15 gallons Appearance here: ❑ Samples for metals were collected unfiltered: ❑YES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/8/22 - 9/22/22 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N <0.017 mg/I Pb - Lead mg/1 Coliform: MF Fecal <1.0 /100ml Nitrate (NO3) as N 0.13 mg/1 Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 0.23 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/1 Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 300 mg/I Al - Aluminum mg/I pH (when analyzed) units Ba - Barium mg/I TOC <0.90 mg/1 Ca - Calcium mg/1 Chloride 23 mg/I Cd - Cadmium mg/I Arsenic mg/1 Chromium: Total mg/1 Grease and Oils mg/1 Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/1 Report Attached? ® Yes (1) ® No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen: NH3 as N; Ammonia Nitrogen, Total) Mn - Manganese mg/1 , method # TKN as N mg/I Ni - Nickel mg/1 method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% rerrmuee for .vumorizeo Agent) ivame ana i iue - mease print or type Siqnature of Permittee (or Authorized Agent) ;Date) GW-59 Rev.1/2007 iuuuuumu911uvuuuu I�OIP VIVVIVIIV� cm," www.encolabs.com ANALYTICAL RESULTS Description: MW-4 Lab Sample ID: CF11320-02 Received: 09/08/22 12:45 Matrix: Ground Water Sampled:09/08/22 10:15 Work Order: CF11320 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell (Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte FCAS Numberl Results Flag Units DF MDL PDL Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,1,1-Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,1,2-Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,1-Dichloroethene [75-35-4]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2,4-Trimethylbenzene [95-63-6]^ < 0,067 ug/L 1 0.067 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2-Dichlorobenzene [95-50-1]^ < 0.062 ug/L 1 0.062 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2-Dichloroethane [107-06-2]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,2-Dichloropropane [78-87-5]^ < 0.098 ug/L 1 0.098 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,3,5-Trimethylbenzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY 1,3-Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 1,4-Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 2,2-Dichloropropane [594-20-71^ < 0.12 ug/L 1 0.12 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 4-Chlorotoluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY 4-Isopropyltoluene [99-87-6]^ < 0.066 ug/L 1 0,066 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Benzene[71-43-2]^ < 0.050 ug/L 1 0.050 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Bromobenzene[108-86-11^ < 0.13 ug/L 1 0.13 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Bromochloromethane [74-97-5]^ < 0.11 ug/L 1 0.11 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Bromoform [75-25-21^ < 0.20 ug/L 1 0.20 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Bromomethane [74-83-9]^ < 0.28 ug/L 1 0.28 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Carbon Tetrachloride [56-23-5]^ < 0.082 ug/L 1 0.082 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Chloroethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Chloroform [67-66-3]^ < 0.083 ug/L 1 0,083 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY QB-02 Chloromethane[74-87-3]^ < 0.050 ug/L 1 0.050 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY cis- 1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY cis-1,3-Dichloropropene [10061-01-5]^ < 0,073 ug/L 1 0.073 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Dichlorodifluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Ethylbenzene [100-41-4]^ < 0.10 ug/L 1 0.10 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Isopropyl Ether[108-20-3]^ < 0.20 ug/L 1 0.20 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Isopropylbenzene[98-82-8]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY m,p-Xylenes [108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Methyl-tert-Butyl Ether[1634-04-41^ < 0.12 ug/L 1 0.12 0,50 2119029 EPA 8260D 09/20/22 10:45 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 6 Of 1� @L]V'mm� ,.�(DD www.encolabs.com ANALYTICAL RESULTS gram nn� nnm W-m- Description: MW-4 Lab Sample ID: CF11320-02 Received: 09/08/22 12:45 Matrix: Ground Water Sampled: 09/08/22 10:15 Work Order: CF11320 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag uniLs DF MDL IQ Batch Method Analyzed By Notes Naphthalene [91-20-3]^ < 0.086 ug/L 1 0.086 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY n-PropylBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY sec -Butyl benzene [135-98-8]^ < 0.053 ug/L 1 0.053 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Styrene[100-42-5]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 2119029 EPA 8260D 09/20/22 10:45 RKY Tetrachloroethene[127-18-4]^ < 0.099 ug/L 1 0.099 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Toluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY trans- 1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY trans-1,3-Dichloropropene[10061-02-6]^ < 0,080 ug/L 1 0.080 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Trichlorofluoromethane [75-69-4]1 < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Xylenes (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 2I19029 EPA 8260D 09/20/22 10:45 RKY Surrogates Results DF Spike Lv/ % Rec % Rec Limits Batch Method Ana/vied Bar Notes 4-Bromofluorobenzene 56 1 50.0 112 % 53-136 M9029 EPA 8260D 0912012210:45 RKY Dlbromofluoromethane 41 1 50.0 8291, 67-129 2119029 EPA 6260D 0912012210:45 RKY Toluene-d8 47 1 50.0 95 % 59-134 2119029 EPA 8260D 0912012210:45 RKY Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analvte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed Iy Notes Ammonia as N [7664-41-7]^ < 0.045 mg/L 1 0.045 0.10 2109020 EPA 350.1 09/09/22 14:37 MSE Chloride [16887-00-6]^ 23 mg/L 1 1.9 5.0 2I13012 SM 4500CIE-2011 09/13/22 12:08 MSE Nitrate as N (14797-55-8] 0.13 ing/L 1 0.041 0.10 [CALC] EPA 353.2 09/12/22 14:01 MSE Nitrate/Nitrite as N ^ 0.13 mg/L 1 0.041 0.10 2I12010 EPA 353.2 09/12/22 14:01 MSE Nitrite as N [14797-65-0]^ < 0.017 mg/L 1 0.017 0.10 2108026 EPA 353.2 09/08/22 16:37 MSE Phosphorus [7723-14-0]^ 0.23 mg/L 1 0.025 0.10 2113020 EPA 365.4 09/14/22 14:26 MSE Total Dissolved Solids^ 300 mg/L 1 50 50 2I08027 SM 254OC-2011 09/08/22 17:45 DMJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analvte fCAS Numberl Results Flag Units DF MDL PQL Batch Method Analyzed By Notes Coliform, Fecal^ < 1.0 MPN/100 1 1.0 2I12021 Colilert 18 09/09/22 11:34 MJY mL Classical Chemistry Parameters ENCO Orlando certified analyte [NC 424] Analvte [CAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed By Notes Total Organic Carbon^ < 0.90 mg/L 1 0.90 1.0 2I22009 SM 531OB-2011 09/22/22 21:59 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 7 Of 19 1 SUBMIT FORM ON YELLOW PAPER ONLY £6DIVISION DEPARTMENT OF ENVIRONMENT & NATURAL RESOURCES GROUNDWATER QUALITY MONITORING: OF WATER QUALITY -INFORMATION PROCESSING UNIT COMPLIANCE REPORT FORM £$ 1617 MAIL SERVICE CENTER, RALEIGH, NC 27699-1617 Phone: (919) 7333221 FACILITY INFORMATION Please Print Clearly or Type PERMIT Number: Expiration Date: Facility Name: Sanford Health & Rehabiitation Non -Discharge W00007026 UIC NPDES Other Permit Name (if different): WQ0007026 Facility Address: 4400 Ferrell Road TYPE OF PERMITTED OPERATION BEING MONITORED ❑ Lagoon ❑ Remediation: Infiltration Gallery Sanford NC 27330 County Lee ® Spray Field ❑ Remediation: Contact Person: Randall Jarrell Telephone#: 919-210-2500 ❑ Rotary Distributor ❑ Land Application of Sludge Well Location/Site Name: Lee County No, of wells to be sampled: 3 ❑ Water Source Heat Pump ❑ Other: (from Permit SAMPLING INFORMATION If WELL WELL ID NUMBER (from Permit): MW-5 Date sample collected: 9-8-22 FIELD ANALYSES: WAS Well Depth: 29.5ft. Well Diameter:2 in. pH 6.54 units Temp. 18.6 °C DRY at Depth to Water Level: 13.0ft. below measuring point Screened Interval: ft. to ft. Spec. Cond, µMhos time of 3 sampling, Measuring Point is ft. above land surface Relative M.P. Elevation: ft. Odor check Volume of water pumped/bailed before sampling: 16 gallons Appearance here: ❑ Samples for metals were collected unfiltered: DYES ❑ NO and field acidified: ❑ YES ❑ NO LABORATORY INFORMATION Date sample analyzed: 9/8/22 - 9/22/22 Laboratory Name: ENCO Certification No. 591 PARAMETERS NOTE: Values should reflect dissolved and colloidal concentrations. COD mg/I Nitrite (NO2) as N <0.017 mg/I Pb - Lead mg/I Coliform: MF Fecal <1.0 /100ml Nitrate (NO3) as N <0.041 mg/l Zn - Zinc mg/I Coliform: MF Total /100ml Phosphorus: Total as P 1.8 mg/I (Note: Use MPN method for highly turbid samples) Orthophosphate mg/I Other (Specify Compounds and Concentration Units): Dissolved Solids: Total 410 mg/I Al - Aluminum mg/1 pH (when analyzed) units Ba - Barium mg/I TOC 1.2 mg/I Ca - Calcium mg/I Chloride 62 mg/I Cd - Cadmium mg/I Arsenic mg/I Chromium: Total mg/I Grease and Oils mg/I Cu - Copper mg/I ORGANICS: (by GC, GC/MS, HPLC) Phenol mg/I Fe - Iron mg/I (Specify test and method #. ATTACH LAB REPORT.) Sulfate mg/I Hg - Mercury mg/I Report Attached? ® Yes (1) ❑ No (0) Specific Conductance µMhos K - Potassium mg/I VOC method # Total Ammonia <0.045 mg/I Mg - Magnesium mg/I method # (Ammonia Nitrogen: NH3as N: Ammonia Nitrogen, Total) Mn -Manganese mg/I ,method # TKN as N mg/I Ni - Nickel mg/I method # For Remediation Systems Only (Attach Lab Reports): Influent Total VOCs: mg/L Effluent Total VOCs: mg/L VOC Removal% Permittee (or Authorized Agent) Name and Title - Please print or type Signature of Permittee (or Authorized Agent) ;Date) GW-59 Rev.1/2007 su 911-liN7""M um�m www.encolabs.com ANALYTICAL RESULTS �a nm mumm vamnreeream Description: MW-5 Lab Sample ID:CF11320-03 Received: 09/08/22 12:45 Matrix: Ground Water Sampled:09/08/22 10:35 Work Order: CF11320 Project: Groundwater Monitoring(Sep) Sampled By: Randall Jarrell IVolatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte ANC 591] Analyte rCAS Numberl Results Flag Units DF MDL RgLL Batch Method Analyzed By Notes 1,1,1,2-Tetrachloroethane [630-20-6]^ < 0.091 ug/L 1 0.091 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1,1-Trichloroethane [71-55-6]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1,2,2-Tetrachloroethane [79-34-5]^ < 0.085 ug/L 1 0.085 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1,2-Trichloroethane [79-00-5]^ < 0.068 ug/L 1 0.068 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1-Dichloroethane [75-34-3]^ < 0.050 ug/L 1 0.050 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1-Dichloroethene [75-35-4]^ < O.1S ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,1-Dichloropropene [563-58-6]^ < 0.063 ug/L 1 0.063 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY 1,2,3-Trichlorobenzene [87-61-6]^ < 0.25 ug/L 1 0.25 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2,3-Trichloropropane [96-18-4]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2,4-Trichlorobenzene [120-82-1]^ < 0.097 ug/L 1 0.097 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2,4-Trimethyl benzene [95-63-6]^ < 0.067 ug/L 1 0.067 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY 1,2-Dibromo-3-chloropropane [96-12-8]^ < 0.48 ug/L 1 0.48 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2-Dibromoethane [106-93-4]^ < 0.27 ug/L 1 0.27 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2-Dichlorobenzene [95-50-1]^ < 0,062 ug/L 1 0.062 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2-Dichloroethane [107-06-2]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,2-Dichloropropane [78-87-S]^ < 0.098 ug/L 1 0.098 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,3,5-Trimethyl benzene [108-67-8]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,3-Dichlorobenzene [541-73-1]^ < 0.092 ug/L 1 0.092 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,3-Dichloropropane [142-28-9]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 1,4-Dichlorobenzene [106-46-7]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 2,2-Dichloropropane [594-20-7]^ < 012 ug/L 1 0.12 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 2-Chlorotoluene [95-49-8]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 4-Chlorotoluene[106-43-4]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY 4-Isopropyltoluene[99-87-6]^ < 0.066 ug/L 1 0.066 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Benzene[71-43-2]^ < 0.050 ug/L 1 0,050 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Bromobenzene[108-86-1]^ < 0.13 ug/L 1 0.13 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Bromochloromethane [74-97-5]^ < 0,11 ug/L 1 0.11 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Bromodichloromethane [75-27-4]^ < 0.010 ug/L 1 0.010 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Bromoform [75-25-2]^ < 0.20 ug/L 1 0.20 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Bromomethane[74-83-9]^ < 0.28 ug/L 1 0.28 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Carbon Tetrachloride[56-23-5]^ < 0.082 ug/L 1 0.082 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Chlorobenzene[108-90-7]^ < 0.069 ug/L 1 0.069 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Chloroethane[75-00-3]^ < 0.18 ug/L 1 0.18 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Chloroform (67-66-3]^ 0.32 JB ug/L 1 0.083 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY J-01 Chloromethane [74-87-3]^ < 0,050 ug/L I 0.050 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY cis- 1,2-Dichloroethene [156-59-2]^ < 0.075 ug/L 1 0.075 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY cis-1,3-Dichloropropene [10061-01-5]^ < 0.073 ug/L 1 0.073 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Dibromochloromethane [124-48-1]^ < 0.067 ug/L 1 0.067 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Dibromomethane [74-95-3]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Dichlorodifluoromethane [75-71-8]^ < 0.091 ug/L 1 0.091 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Ethylbenzene[100-41-4]^ < 0.10 ug/L 1 0.10 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Hexachlorobutadiene[87-68-3]^ < 0.15 ug/L 1 0.15 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Isopropyl Ether[108-20-3]A < 0.20 ug/L 1 0.20 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Isopropyl benzene [98-82-8]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY m,p-Xylenes[108-38-3/106-42-3]^ < 0.18 ug/L 1 0.18 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Methylene Chloride [75-09-2]^ < 0.070 ug/L 1 0.070 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Methyl -tent -Butyl Ether[1634-04-4]^ < 0.12 ug/L 1 0.12 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 8 Of 19 CGE","N oAKB 00 u u Volatile Organic Compounds by GCMS ^ - ENCO Cary certified analyte [NC 591] Analyte rCAS Numberl Results Flag Units OF MDL Q Batch Method Analyzed By Notes Naphthalene[91-20-3]^ < 0,086 ug/L 1 0.086 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY n-Butyl Benzene[104-51-8]^ < 0.074 ug/L 1 0.074 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY n-PropylBenzene [103-65-1]^ < 0.073 ug/L 1 0.073 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY o-Xylene[95-47-6]^ < 0.088 ug/L 1 0.088 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY sec-Butylbenzene[135-98-8]^ < 0.053 ug/L 1 0.053 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Styrene[100-42-5]^ < 0.082 ug/L 1 0,082 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY tert-Butylbenzene[98-06-6]^ < 0.094 ug/L 1 0.094 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Tetrachloroethene[127-18-4]^ < 0,099 ug/L 1 0.099 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Toluene[108-88-3]^ < 0.053 ug/L 1 0.053 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY trans-1,2-Dichloroethene [156-60-5]^ < 0.11 ug/L 1 0.11 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY trans- l,3-Dichloropropene[10061-02-6]^ < 0.080 ug/L 1 0.080 0.50 2119029 EPA 8260D 09/20/22 11:18 RKY Trichloroethene [79-01-6]^ < 0.13 ug/L 1 0.13 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Trichlorofluoromethane [75-69-4]^ < 0.15 ug/L 1 0.15 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Vinyl chloride [75-01-4]^ < 0.083 ug/L 1 0.083 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Xylenes (Total) [1330-20-7]^ < 0.22 ug/L 1 0.22 0.50 2I19029 EPA 8260D 09/20/22 11:18 RKY Surrogates Results DF Spike Lv/ % Rec a/a Rec Limits Batch Method Ana/vzed BLr Notes 4-Bromofluorobenzene 56 1 50.0 112 96 53-136 2119029 EPA 8260D 0912012211:18 RKY Dibromofluoromethane 44 1 50.0 89 % 67-129 2119029 EPA 6260D 0912012211:18 RKY Toluene-d8 46 1 50.0 93 % 59-134 2119029 EPA 8260D 09120122 11:18 RKY Classical Chemistry Parameters ^ - ENCO Cary certified analyte [NC 591] Analvte ]CAS Number] Results Flag Units DF MDL PPL Batch Method Analyzed ft Notes Ammonia as N [7664-41-7]^ < 0.045 mg/L 1 0.045 0.10 2109020 EPA 350.1 09/09/22 14:40 MSE Chloride [16887-00-6]^ 62 mg/L 1 1.9 5.0 2I13012 SM 4500CIE-2011 09/13/22 12:08 MSE Nitrate as N [14797-55-8] < 0.041 mg/L 1 0.041 0.10 [CALC] EPA 353.2 09/12/22 14:04 MSE Nitrate/Nitrite as N^ < 0.041 mg/L 1 0.041 0.10 2I12010 EPA 353.2 09/12/22 14:04 MSE Nitrite as N [14797-65-0]^ < 0.017 mg/L 1 0.017 0.10 2I08026 EPA 353.2 09/08/22 16:37 MSE Phosphorus [7723-14-0]^ 1.8 mg/L 1 0.025 0.10 2I15018 EPA 365.4 09/16/22 17:22 MSE Total Dissolved Solids^ 410 mg/L 1 50 50 2I08027 SM 2540C-2011 09/08/22 17:45 DMJ Microbiological Parameters ^ - ENCO Cary certified analyte [NC 591] Analvte rCAS Number] Results Flag Units DF MDL tQ Batch Method Analyzed By Notes Coliform, Fecal^ < 1.0 MPN/100 1 1.0 2I12021 Colilert 18 09/09/22 11:34 MJY mL ]Classical Chemistry Parameters ^ - ENCO Orlando certified analyte [NC 424] Analvte rCAS Numberl Results Flag Units DF MDL POLL Batch Method Analyzed By Notes Total Organic Carbon^ 1.2 mg/L 1 0.90 1.0 2I22009 SM 531OB-2011 09/22/22 22:17 KG FINAL This report relates only to the sample as received by the laboratory, and may only be reproduced in full. I Page 9 OP 19