HomeMy WebLinkAboutWQ0035207_Application_20110203AQUIFER PROTECTION SEI
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LPPLICATION REVIEW RE(
Date: February 3, 2011 Asheville Regional Office
To: ®Landon Davidson, ARO-APS ❑ David M ®lO�,sAl. P �t ��1f��
❑ Art Barnhardt, FRO-APS ❑ Charlie Stehin-a WiRO= S}-----
❑ Andrew Pitner, MRO-APS ❑ Sherri Knight, WSRO-APS
❑ Jay Zimmerman, RRO-APS
From: Chonticha McDaniel ❑AFO❑GW Protection❑GW Planning ®LAU
E-Mail: chonticha.mcdaniel iincdenr.gov
Telephone: (919) 715-6188 Fax:(919) 715-0588
A. Permit Number: WQ0035207
C. Facility/Operation: Town of Franklin WTP
® Proposed ❑ Existing
D. Application:
B. Owner: Synagro Central
❑ Facility ® Operation
1. Permit Type: ❑ Animal ❑ Surface Irrigation ❑ Reclaimed ❑ H-R Infiltration
❑ Recycle ❑ FE Lagoon ❑ GW Remediation (ND)
❑ UIC - (5A7) open loop geothermal ❑ Single Family Residence
® Residuals
2. Project Type: ® New ❑ Major Mod. ❑ Minor Mod. , ❑ Renewal ❑ Renewal w/ Mod.
E. Comments/Other Information: ❑ I would like to accompany you on a site visit.
Attached, you will find all information submitted in support of the above -referenced application for your
review, comment, and/or action. Within 30 calendar days, please take the following actions:
® Return a Completed APSARR Form.
❑ BIMS indicates monitoring wells locations are not complete. Please update monitoring well
locations not currently in BIMS.
❑ BIMS indicates ongoing ❑ NDMR ❑NDAR ❑ GW monitoring violations. Please investigate
reoccurring compliance issues and summarize results in staff report.
❑ Attach Well Construction Data Sheet.
❑ Process Attachment B for Certification by the Land Application Unit (LAU).
❑ Issue an Attachment B Certification from the RO.*
*coordinating site visits and reviews, as well as additional information requests with other RO-APS
representatives in order to prepare a complete Attachment B for certification. Refer to the RPP SOP for
additional detail.
Please indicate the name and date assigned in the spaces below, make a copy of this sheet, and return it to
the appropriate Central Office -Aquifer Protection Section contact person listed above.
RO-APS Reviewer:
Date:
FORM: APSARR 03/10 Page 1 of 1
A M,
,-TT4
HCDEHR
North Carolina Department of Environment and Natura
Division of Water Quality
Beverly Eaves Perdue Coleen H. Sullins
Governor Director
January 27, 2011
Marshall Puryear, Technical Services Director
Synagro Central, LLC
284 Boger Road
Mocksville, NC 27028
Subject: Acknowledgement of Application No. WQ0035207
Town of Franklin WTP
Distribution of Residual Solids (503)
Macon
Dear Mr. Puryear:
Resources
Dee Freeman
Secretary
The Aquifer Protection Section of the Division of Water Quality (Division) acknowledges receipt of your permit application and
supporting materials on January 7, 2011. This application package has been assigned the number listed above and will be reviewed by
Chonticha McDaniel.
The reviewer will perform a detailed review and contact you with a request for additional information if necessary. To ensure the
maximum efficiency in processing permit applications, the Division requests your assistance in providing a timely and complete
response to any additional information requests.
Please be.aware that the Division's Regional Office, copied below, must provide recommendations prior to final action by the
Division. Please also note at this time, processing permit applications can take as long as 60 - 90 days after receipt of a complete
application.
If you have any questions, please contact Chonticha McDaniel at 919-715-6188715-6188, or via e-mail at
chonticha.mcDaniel@ncdenr.gov. If the reviewer is unavailable, you may leave a message, and they will respond promptly.
PLEASE REFER TO THE ABOVE APPLICATION NUMBER WHEN MAKING INQUIRIES ON THIS PROJECT.
Sincerely,
for Jon Risgaard
LAU Supervisor
cc:
2ishewiileional Office Aqutfei_Ptoiecfion Section
Permit Application File WQ0035207
AQUIFER PROTECTION SECTION
1636 Mail Service Center, Raleigh, North Carolina 27699-1636
Location: 2728 Capital Boulevard, Raleigh, North Carolina 27604
Phone: 919-733-3221 \ FAX 1: 919-715-0588: FAX 2: 919-715-6048 \ Customer Service: 1-877-623-6748
Internet: mm.nmateroualitv.ora
,an Equal Opportunity i ynirmarive.Action Employer
One
o1-ffiCarolinp-
�1 i 1, - 4
s
M
.V0 SYNAGR.O
A Residuals Management Company
January 5, 2011
N.C. Department of Environment and Natural Resources
Water Quality Section
Non -Discharge Permitting Unit — Aquifer Protection Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
ATTENTION: Mr. John Risgaard
REFERENCE: APPLICATION FOR NEW DISTRIBUTION OF RESIDUAL
SOLIDS PERMIT FOR SYNAGRO CENTRAL, LLC
Mr. Risgaard:
Synagro Central, LLC is submitting a new permit application to be able to distribute the
residual solids from the Town of Franklin North Carolina's water treatment plant. Synagro is
planning on distributing these solids to agricultural fields in Macon County North Carolina.
These residuals will be applied at agronomic rates based on the most recent nutrient and metals
analysis.
Synagro is enclosing the new permit fee of $810 as well as one original and two copies of the
permit application as required on form DRS.
This application package contains the information necessary to complete the modification of
this permit. However, if you require any additional information or have further questions about
the information presented herein, please contact me at mpuryeargsyna roxom or at phone
number (336) 998-7150 ext 17. I look forward to working with you to ensure a timely and
efficient review of this application.
Sincerely, _ ., A
Marshall Puryear
Technical Services Director = '
Synagro Central, LLC a_
c-�
284 Boger Road • Mocksville, NC 27028-7619 • Ph: (336) 998-7150 • Fax: (336) 998-8450 e Toll Free: (877) 267-2687
Table of Contents
Section # Title
Section 1 Attachment Order 1: Distribution of Residual Solids
Attachment Order l a: Signing Official Delegation Letter
Section 2 Attachment Order 2: Residuals Source Certification Attachment
Attachment Order.2-a: Vicinity Map
Attachment Order 2-b: Process Flow Diagram
Attachment Order 2-c: Quantitative Justification for Residuals Production
Attachment Order 2-d: Sampling Plan
Attachment Order 2-e Laboratory Analytical Reports (where applicable)
Attachment Order 1:
Distribution of Residual Solids
(DRS form)
State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
DISTRIBUTION OF RESIDUAL SOLIDS
(FORM: DRS 070807)
(THIS FORM MAY BE PHOTOCOPIED FOR USE AS AN ORIGINAL)
Application Number:
I. OWNERSHIP INFORMATION:
1. Specify whether the process facility is owned by:
❑ County; ❑ Federal; ❑ Municipal; ❑ State; ® Non -Government.
2. Owner's name (please specify the name of the municipality, corporation, individual, etc.):
Synagro
(to be completed by DWQ)
r
{ '
-
Mailing address: 284 Boger Road
=
City: Mocksville State: NC Zip:
27028
Physical address: same
City: State:
Zip:
Telephone number: ( 336 ) 998-7150 ext 17 Facsimile number:( 336
) 998-8450
E-mail address: mpurvearAsynagro.com
3. Signing official's name and title: (See Instruction A)
Marshall Purvear Technical Services Director
Mailing address: 284 Boger Road
City: Mocksville State: NC
Zip: 27028
Physical address: Same
City: State:
Zip:
Telephone number: ( 336 ) 998-7150 Ext 17 Facsimile number: ( 336 )
998-8450
E-mail address: mpuryearAsynagro com
II. PERMIT INFORMATION:
1. Application is for: ® new; ❑ modified; ❑ renewed permit (check all that apply).
2. Fee Submitted: $ 810 (See Instruction B)
3. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number:
Most recent issuance date:
(please attach a copy of the existing permit).
and the expiration date:
FORM: DRS 070807 Page 3 of 6. Attachment Order 1
III. FACILITY INFORMATION:
1. Name of facility where residuals are processed:
Town of Franklin WTP
Physical address: 437 Industrial Park Road
City: Franklin State: NC Zip: 28744
Telephone number: ( 828-369-8998) Facsimile number: ( )
County where facility is located:
Latitude: 35 09'36.73" N Longitude: 83 26' 14.75" W of residual process facility.
2. Facility contact (person familiar with residuals preparation):
Robert Hartzel Water Treatment Plant Superintendent
Mailing address: 437 Industrial Park Road
City: Franklin State: NC Zip: 28744
Physical address:
City:
Telephone number: ( 828-369-8998 )
E-mail address:
State:
Facsimile number: (
Zip:
3. Program contact person and/or consulting firm who prepared application (If different from the above):
Marshall Purvear
Mailing address: 284 Bojzer Road
City: Mocksville State: NC Zip: 27028
Physical address:
City:
State:
Zip:
Telephone number: ( 336 ) 998-7150 ext. 17 Facsimile number: ( 336 ) 998-8450
E-mail address: mDurvear(@,synaizro.com
4. Is the residual process facility also the generator? ® Yes; ❑ No
5. If the residual process facility is not the same as the generator, please specify delivery frequency and quantity of residual to
be processed:
6. Length of residuals storage at facility: 180 days days (the Division requires a minimum 30 days storage in
units that are separate from treatment system, i.e. not in clarifiers, aeration basins, etc.).
IV. RESIDUALS QUALITY INFORMATION:
1. Specify if residuals are regulated under (check one): ❑ 40 CFR Part 503 or
40 CFR Part 257.
'FORM: DRS 070807 Page 4 of 6 Attachment Order 1
2. Specify how these residuals will be distributed:
❑ sold or given away in bags or other containers; ❑ lawn (bulk); ❑ home garden (bulk);
® other; Land applied to agricultural fields
3. Complete the following if residuals are to be mixed with other materials:
Type of Materials I Amounts to be added
per 1.0 dry ton of residuals (dry ton)
4. Approximate amounts of the final product to be distributed
300
dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): The residuals are stored in a half acre lagoon prior to being land applied
which gives the town over 180 days storage time based on the amount of solids that they are currently producing
V. ADDITIONAL REQUIRED INFORMATION:
1. Provide a narrative explaining the following: -
a. How will. the materials be handled and transported from where the residuals were produced to where it will be
treated?
b. How will the residuals be processed/treated (attach process flow diagram).
c. How will leachate collection be handled?
d. Where will the residuals be stored until processed?
e. How will the final product be distributed (packaging)?
2. Attach a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
3. Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to
the person who receives the processed residual. The label or information sheet shall contain, at a minimum, the following
information:
a. The name and address of the person who prepared the residual that is sold or given away in a bag or other container for
application to the land.
b. A statement that application of the residual to the land is prohibited except in accordance with the instructions on the
label or information sheet.
c. A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
d. A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
e. Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
f. A statement that the residuals shall be applied at agronomic rates and recommended rates for intended uses.
FORM: DRS 070807 Page 5 of 6 Attachment Order 1
Professional Engineer's Certification: (Application Packages Involving New or Changes to Treatment and Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal
package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I have
reviewed this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
t J J
J
Applicant's Certification;' _
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without
proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with any
active compliance schedule, and do not have any overdue annual fees under Rule 2T .0105.
® Yes F-J_ No, Explain;
I, Marshall Purvear , attest that this application for Synagro
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that if all required parts of this
application are not completed and that if all required supporting information and attachments are not included, this application package
will be returned to me as incomplete.
Signature
Date 0V C,51 /
THE COMPLETED APPLICATION PACKAGE,
INCLUDING ALL SUPPORTING INFORMATION AND MATERIALS,
SHOULD BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER QUALITY
AQUIFER PROTECTION SECTION
LAND APPLICATION UNIT
By U.S. Postal Service:
1636 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1636
By Courier/Special Delivery:
2728 CAPITAL BOULEVARD
RALEIGH, NORTH CAROLINA 27604
TELEPHONE NUMBER: (919) 733-3221
FORM: DRS 070807 Page 6 of 6 Attachment Order 1
FARM REPORT
HARNETT CO. UTILITIES, NC Synagro Field#:
Month & Year: April 2010
Landowner: County: HARNETT
Operator: Latitude: 35.16'56"
Crop: FESCUE Longitude: 78.41'53"
Acres: 25 (10.13 ha )
Operator Address:
Last Date Applied This Month: April 30, 2010
Month To Date
Year To Date Cumulative
Applied Amounts As Hauled
Gallons Applied-
440,200.00
440,200.00 0.00
Applied Amounts Converted To Dry Weight
Dry Tons/Acre Applied:
1.44
1.44 0.00 13.40
**************** POUNDS PER ACRE APPLIED
(Kilograms Per Hectare Applied)
MONTH
YEAR
PARAMETER
TO DATE
TO DATE CUMULATIVE
MACRO NUTRIENTS
Est. Avail Nitrogen
6.74
6.74
Est. Avail Phosphate
6.16
6.16
Total Phosphorus (P)
5.35
5.35
Total Potassium (K)
2.99
2.99
Total Potash (K20)
3.59
3.59
Calcium
8.00
8.00
Magnesium
3.94
3.94
Sulfur
19.66
19.66
MICRO NUTRIENTS
Manganese
2.85
(3.19)
2.85
(3.19)
44.01 (49.29)
Zinc
0.20
(0.22)
0.20
(0.22)
1.95 (2.18)
Copper
1.18
(1.32)
1.18
(1.32)
25.14 (28.16)
Molybdenum
0.01
(0.01)
0.01
(0.01)
0.25 (0.28)
Iron
89.51
(100.25)
89.51
(100.25)
TRACE METALS
Arsenic
0.02
(0.02)
0.02
(0.02)
0.41 (0.46)
Cadmium
<.01
(<.01)
<.01
(<.01)
0.03 (0.03)
Chromium
0.16
(0.18)
0.16
(0.18)
1.73 (1.94)
Lead
0.04
(0.04)
0.04
(0.04)
0.30 (0.34)
Mercury
<.01
(<.01)
<.01
(<.01)
0.01 (0.01)
Nickel
0.05
(0.06)
0.05
(0.06)
0.44 (0.49)
Selenium
<.01
(<.01)
<.01
(<.01)
0.13 (0.15)
* Note: Parameters are given in pounds per acre unless otherwise noted.
NR = Data not reported to Synagro Technologies, Inc. or Data not required.
Town of Franklin NC
Water Treatment Plant
Narrative for Class A Residuals
This project involves the removal of alum residuals from the Town of Franklin's
Water treatment plant. These residuals are produced by adding aluminum sulfate
to raw water drawn from Cartoogechaye Creek. The water alum mixture is then
allowed to settle in 3 settlement basins for a volume of about 150,000 gallons in
order to allow the water and solids (mainly mud and silt) to separate. The solids
are then moved by gravity to the holding ponds in order to settle out further.
When the lagoons start to get full the lagoons will be mixed up and the solids
pumped out as a liquid. The residuals will then be land applied to agricultural
fields at rates well below the agronomic rate due to the low nitrogen content of
the material. The residuals receive no further treatment after they are placed in
the lagoon. The residuals will be transported in sealed tankers to the land
application site that will be used for that event. No leachate will be collected from
this process since the residuals are going to be land applied as a liquid.
Attachment Order la:
Signing Official Delegation Letter
December 15, 2010
Division of Water Quality
Land. Application Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
Subject: Permitting Signature Authority
To Whom It May Concern:
As an appropriate signing official for Synagro Central, LLC., as designated by .15A NCAC 2T .0106(c), I
hereby delegate authority to sign and certify all permit applications, reports or other permit related
documents to the following staff for the following permit types (sewer, spray, land application) and/or
permit numbers:
Position
Person Currently in Position
Permit Type or Permit Number
Technical Services Director
Marshall Puryear
New .Distribution of Residual
Solids (Synagro Central LLC)
Regional Operations Director
Bill Cotter
New Distribution of Residual.
Solids (Synagro Central .LLC)
If you have any questions, please contact we at the following:
PermtteelApplicant name (please print): Mark Miller
Title: General Manager Services Division
Complete mailing address: 7014 East Baltimore Street
City: Baltimore State: MD Zip: 11224
Telephone number: (410) 284-4120 Facsimile number: (410) 2842-7466
Sincerely,
Attachment Order. 2:
Residuals Source Certification Attachment
(RS CA form)
State of North Carolina
Department of Environment and Natural Resources
Division of Water Quality
RESIDUALS SOURCE CERTIFICATION ATTACHMENT
(FORM: RSCA 070807)
(THIS FORM MAYBE PHOTOCOPIED FOR USE AS AN ORIGINAL)
Applicant's name: Smagro
Check all that apply: ® NEW RESIDUALS PROGRAM ❑ RENEWED RESIDUALS PROGRAM
❑ INCREASE ❑ DECREASE the maximum permitted annual dry tonnage for this residuals source -
generating facility certified for this residuals program.
Current: 0 Dry Tons/yr. and proposed: 300 Dry Tons/yr.
❑ ADD ❑ DELETE this residuals source -generating facility to/from those certified for this
residuals program.
❑ OTHER Explain:
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction B.):
1. Name of facility: Town of Franklin Water Treatment Plant
2. Facility permit holder: Town of Franklin NC
Facility permit holder is (check one): ❑ federal, ❑ state, ® local government, or ❑ private.
Facility permit number: PWS 01-57-010
Facility permit issued by (check one): ❑ Div. of Water Quality, ® Div. of Environmental Health, or
❑ other (explain: ).
3. If the facility permit is not issued by the Div. of Water Quality, complete the following:
a. Facility contact person and title: Robert Hartzel Water Treatment Plant Superintendent
Facility complete mailing address: 437 Industrial Park Road
City: Franklin State: NC Zip: 28744
Telephone number: ( 828-369-8998) Facsimile number: ( )
E-mail address:
b. Facility complete location address: Same as above
City:
State:
Latitude: 35 09' 36.73"N and longitude: 83 26' 14.75" w
4. County where facility is located:
Zip:
5. Purpose of the facility (check one):
❑ treatment of municipal wastewater, ❑ treatment of 100% domestic wastewater,
® treatment of potable water, ❑ treatment of 100% industrial wastewater,
❑ treatment of industrial wastewater mixed with domestic wastewater, or
(approximate percentages: % industrial and % domestic)
❑ other (explain:
FORM: RSCA 070807 Page 2 of 8 Attachment Order 2
6. Does the facility have an approved pretreatment program: ❑ yes ® no
7. Facility permitted/design flow: 2.2 MGD and facility average daily flow: 1.5 MGD.
8. Average amount of residuals being generated at this facility 300 dry tons per year.
9. Specify the following regarding treatment and storage volumes available at the facility:
Type and volume of residuals treatment: The residuals are stored in a concrete storage system before
being transferred to the lagoon. The concrete storage is capable of holding approximately 275,000 gallons
Type and volume of residuals storage (i.e., outside of residuals treatment units): The plant has 2 lagoons
with a capacity of approximately 500,000 gallons each
H. RESIDUALS QUALITY INFORMATION (See Instruction C.):
1. Specify if residuals are regulated under (check one): ❑ 40 CFR Part 503 or ® 40 CFR Part 257.
2. Specify if residuals are intended for (check one):
® Land Application/Distribution (Class A or Equivalent).
Complete all items EXCEPT Items II.4b., 7b., and 7c.
❑ Land Application (Class B or Equivalent).
Complete all items EXCEPT Items II.4b., 7a., and 7c.
❑ Surface Disposal.
Complete all items EXCEPT Items II.4a., 5., 7a., 7b., and 8.
***FORM: RSCA CONTINUES ON NEXT PAGE***
FORM: RSCA 070807 Page 3 of 8 Attachment Order 2
3. Hazardous Waste Determination: Complete the following to demonstrate that the residuals are non-
hazardous under RCRA:
a. Are the residuals are listed in 40 CFR §261.31-§261.33: ❑ yes ® no.
If yes, list the number(s):
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21-
§261.24: ❑ yes ® no. Fill in the following tables with the results of the latest toxicity
characteristic leaching procedure (TCLP) analysis as well as those for corrosivity, ignitability, and
reactivity: laboratory: Summit Environmental Technologies and date of analysis: 10/12/2010
Passed corrosivity test: ® yes ❑ no. pH: 6.73 s.u. (2 < pH < 12.5).
Passed ignitability test: ® yes ❑ no. Flashpoint: >140 OF (> 1400F).
Passed reactivity test: ® yes ❑ no. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500).
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
TCLP Parameter
Limit
(mg/L)
Result
(mg/L)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
<0.1
Barium
100.0
ND
Hexachloro-1,3-Butadiene
0.5
<0.1
Benzene
0.5
<0.1
Hexachloroethane
3.0
<0.1
Cadmium
1.0
ND
Lead
5.0
ND
Carbon Tetrachloride
0.5
<0.1
Lindane
0.4
<0.002
Chlordane
0.03
<0.01
Mercury
0.2
ND
Chlorobenzene
100.0
<0.1
Methoxychlor
10.0
<0.002
Chloroform
6.0
<0.1
Methyl Ethyl Ketone
200.0
<2.0
Chromium
5.0
ND
Nitrobenzene
2.0
<0.1
m-Cresol
200.0
<5.0
Pentachlorophenol
100.0
<0.25
o-Cresol
200.0
<5.0
Pyridine
5.0
<0.25
p-Cresol
200.0
<5.0
Selenium
1.0
ND
Cresol
200.0
<5.0
Silver
5.0
ND
2,4-D
10.0
<5.0
Tetrachloroethylene
0.7
<0.1
1,4-Dichlorobenzene
7.5
<0.1
Toxaphene
0.5
<0.1
1,2-Dichloroethane
0.5
<0.1
Trichloroethylene
0.5
<0.1
1,1-Dichloroethylene
0.7
<0.1
2,4,5-Trichlorophenol
400.0
<0.25
2,4-Dinitrotoluene
0.13
<0.1
2,4,6-Trichlorophenol
2.0
<0.25
Endrin
0.02
<0.002
2,4,5-TP (Silvex)
1.0
<0.5
Heptachlor and its Hydroxide
0.008
<0.002
Vinyl Chloride
0.2
<0.2
FORM: RSCA 070807 Page 4 of 8 Attachment Order 2
4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the
residuals do not violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Class A or Class B: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory: A&L Eastern Labs and date of analysis: 10/04/2010
Parameter
Ceiling
Concentration Limits
(ClassA & ClassB) -
(mg/kg)
Monthly Average
Concentration Limits
(For Class A Only)
(mg/kg)
Result
(mg/kg)
Arsenic
75
41
4.0 mg/kg
Cadmium
85
39
<1.0 mg/kg
Copper
4,300
1,500
61 mg/kg
Lead
840
300
10 mg/kg
'Mercury
57
17
<0.4 mg/kg
Molybdenum
75
n/a
<5 mg/kg
Nickel
420
420
22 mg/kg
Selenium
100
100
<1.0 mg/kg
Zinc
7,500
2,800
84 mg/kg
b. For Surface Disposal: Fill in the following table with the results of the latest analyses (i.e., on a dry
weight basis) for the following metal parameters:
Laboratory:
and date of analysis:
Closest Distance
to Property Lines
(meters)
Arsenic
(mg/kg)
Chromium
(mg/kg)
Nickel
> 0 but < 25
30
200
210
�t25 but < 50
34
220
240
>50 but < 75
39
260
270
>_75 but < 100
46
300
320
>_100 but < 125
53
360
390
>_125 but < 150
62
450
420
>_150
73
600
420
FORM: RSCA 070807 Page 5 of 8 Attachment Order 2
5. , Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 4.71 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the
following nutrient and micronutrient parameters: laboratory: A&L Eastern Labs
and date of analysis: 10/04/2010
Parameter
Result
(mg/kg, dry weight)
Aluminum
21700 mg/kg
Ammonia -Nitrogen
1700 mg/kg
Calcium
1130 mg/kg ,
Magnesium
2300 mg/kg
Nitrate -Nitrite Nitrogen
23.4 mg/kg
pH (Standard Unit)
6.47
Phosphorus
854 mg/kg
Potassium
1260 mg/kg
Sodium
185 mg/kg
Total Kjeldahl Nitrogen
6790 mg/kg
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR): 0.16
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the
residuals: 40 %. This rate is a ® default value or ❑ actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or
provide technical justification as to why the selected default value is appropriate to be applied to these
residuals:
Calculate the PAN for the residuals (i.e., on a dry weight basis) and list the results in the following table:
Application Method
First Year
Five -Year
PAN
Maximum Adjusted
PAN
(mg/kg)
(mg/kg)
Surface
2909 mg/kg
4005 mg/kg
Injection/Incorporation
3759 mg/kg
4855 mg/kg
e. Are the residuals a registered fertilizer with the NC Department of Agriculture and Consumer Services:
❑ yes ® no. If yes, provide date of registration approval:
the current registration number:
and the fertilizer equivalent: %, %, and %.
FORM: RSCA 070807 Page 6 of 8 Attachment Order 2
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the
residuals and list the results of the latest analyses: There are no pollutants of concern in the residuals from
7. Pathogen Reduction Determination: Specify which alternative(s) will be used to meet the pathogen
reduction requirements:
a. For Class A or Equivalent:
® A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids.
OR
❑ A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the following (except for residuals regulated under 40 CFR Part 257 that are to be distributed):
❑ Alternative 1 [40 CFR §50132 (a)(3)] - Time/Temperature Compliance.
❑ Alternative 2 [40 CFR §503.32 (a)(4)] - Alkaline Treatment.
❑ Alternative 3 [40 CFR §503.32 (a)(5)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
❑ Alternative 4.[40 CFR §503.32.(a)(6)] - No Prior Testing for Enteric. Virus/Viable Helminth Ova.
❑ Alternative 5.[40 CFR §503.32 (a)(7)] - Process to Further Reduce Pathogens (PFRP).
Specify one: ❑ composting, ❑ heat drying, ❑ heat treatment, ❑ pasteurization,
❑ thermophilic aerobic digestion, ❑ beta ray irradiation, or ❑ gamma ray irradiation.
❑ Alternative 6 [40 CFR §503.32 (a)(8)] - PFRP-Equivalent Process.
Explain:
b. For Class B or Equivalent:
❑ Alternative 1 [40 CFR §503.32. (b)(2)] - Fecal Coliform Density Demonstration.
❑ Alternative 2 [40 CFR §503.32 (b)(3)] -Process to Significantly Reduce Pathogens (PFRP).
Specify one: ❑ aerobic digestion, ❑ air drying, ❑ anaerobic digestion,
❑ composting, or ❑ lime stabilization.
❑ Alternative 3 [40 CFR §503.32 (b)(4)] - PSRP-Equivalent Process.
Explain:
® Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
c. For Surfaee Disposal:
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
❑ Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item II. 7b. above.
® Not Applicable - Regulated under 40 CFR Part 257 with NO Domestic Wastewater Contribution.
FORM: RSCA 070807 Page 7 of 8 Attachment Order 2
8. Vector Attraction Reduction Determination: Specify which alternatives) will be used to meet the vector
attraction reduction requirements:
❑ Alternative 1 [40 CFR §503.33 (b)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
❑ Alternative 2 [40 CFR §503.33 (b)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
❑ Alternative 3 [40 CFR §503.33 (b)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
❑ Alternative 4 [40 CFR §503.33 (b)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
❑ Alternative 5 [40 CFR §503.33 (b)(5)] - 14-Day Aerobic Processes.
❑ Alternative 6 [40 CFR §503.33 (b)(6)] - Alkaline Stabilization.
❑ Alternative 7 [40 CFR §503.33 (b)(7)] - Drying of Stabilized Residuals.
❑ Alternative 8 [40 CFR §503.33 (b)(8)] - Drying of Unstabilized Residuals.
❑ Alternative 9 [40 CFR §503.33 (b)(9)] - Injection.
❑ Alternative 10 [40 CFR §503.33 (b)(10)] - Incorporation.
❑ Alternative for Surface Disposal Units Only [40 CFR §503.33 (b)(11)] - Soil/Other Material Cover.
❑ Alternatives for Animal Processing Residuals Only:
Specify one: ❑ injection, ❑ incorporation, or ❑ lime addition to raise pH to 10.
® Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
FORM: RSCA 070807 Page 8 of 8 Attachment Order 2
Attachment Order 2-a:
Vicinity Map
SYNAGIRO
LOCATION NIAP A Residuals Management Company
N�
ct,
4a� I Q Y1 `� Ali, 1 Lenka t
iz eyf Ip 1 Any 0 , 1 — I `r ��.� � p tc °;P
FRNeed
IL
° 7T
peck I 0Rp H'A A G� I:
..-
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ve, I R ; c f ,`Knob
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.Q• BI9 yMl R o o a J{ m 'teatherma
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f ♦ A W p2n, t \ A ` 00WOLE RD fru.66
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91'•.. 7 ��1 t SKEENAR ♦� —'tFl111
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W OLD YURPNY PD^=C1� ^ 1 \ :� H.V.
COUNTY (i ,4 G o N OWNER o w N 4- FM o I L l l)
Attachment Order 2-b:
Process Flow Diagram
�f 4:
M/x
TOWN OF FRANKLIN WATER TREATMENT PLANT
w4Q pmW
b.
;/ooal,F Z,,.?�s 00,65
Attachment Order 2-c:
Quantitative Justification for Residuals Production
Quantitative Justification for Residuals Production Rate
Facility:
Town of Franklin WTP
Requested Permitted Rate:
300 dry tons/year
Justification:
The Town of Franklin currently produces and stores it's water plant residuals in a
settling basin that it cleans out every 2-3 years. It is at this time that the volume of solids
is calculated based on the percent solids of the lagoon and the depth of the solids.
Calculations:
The lagoons at this plant hold approximately 500,000 gallons each the percent solids are
4-5% solids. The requested dry tonnage should provide adequate volume to do a thorough
cleaning of these lagoons without exceeding the permitted dry tonnage.
Attachment Order 2-d:
Sampling Plan
Residuals Sampling Plan
Town of Franklin WTP Land Application Class A Program
Nutrients and Metals Analysis
Sampling Point: Lagoon
Sampling Frequency: Annually
Sample Type: Composite
Lab: A&L Eastern Agricultural Laboratories, Inc.
Pathogen (Fecal Coliform Density Demonstration)
Sampling.Point: Lagoon
Sampling Frequency: Annually
Sample Type: Composite
Lab: Statesville Analytical
Vector Attraction Reduction
Not required due to being residuals being generated from the treatment of potable
water with no domestic wastewater contribution.
Sampling Points:
Sampling Frequency:
Sample Type
Lab:
TCLP + RCI
Sampling Point: Lagoon
Sampling Frequency: Annually
Sample Type: Composite
Lab: Summit Environmental Technologies; Inc
Attachment Order 2-e:
Laboratory Analytical Reports
SUMMIT
ENVIRONMENTAL TECHNOLOGIES, INC.
Analytical Laboratories
LABORATORY REPORT
Client
Synagro Southeast
284 Boger Rd.
Mocksville, NC 27028
Order Number
1015564
Project Number
Franklin WTP
Issued
Tuesday, October 12, 2010
Total Number of Pages
5 (excluding C.O.C. and cooler receipt form)
Approved By : Q it4-i
QA Manager
NELAC Accreditation #E87688
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489
Web Site: www.settek.com
SU M-MIT'...
ENVIRONMENTAL TECHNOLOGIES, INC.
October 12, 2010
Analytical Laboratories
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville,
NC 27028
Received: 9/24/2010
Project #: Franklin WTP
TCLP
Metals
Client ID# Lab ID#
Collected Anal tc
Rep Lmt
Result
Units
Mahia Method
DF
Re Lvl
Run Analyst
Frankling NC WTP 1015564-01
16-Sep-10 Selenium
0.5
ND
mg/I
SL
1311
1
1
05-Oct-10 VVK
Frankling NC WTP 1015564-01
16-Sep-10 Barium
5
ND
mg/I
SL
1311
1
100
05-Oct-10 VVK
Frankling NC WTP 1015564-01
16-Sep-10 Arsenic
0.5
ND
mg/I
SL
1311
1
5
05-Oct-10 WK
Frankling NC WTP 1015564-01
16-Sep-10 Chromium
0.2
ND
mg/I
SL
1311
1
5
05-Oct-10 VVK
Frankling NC WTP 1015564-01
16-Sep-10 Silver
0.5
ND
mg/I
SL
1311
1
5
05-Oct-10 VVK
Frankling NC WTP 1015564-01
16-Sep-10 Mercury
0.002
ND
mg/1
SL
1311
1
0.2
05-Oct-10 WK
Frankling NC WTP 1015564-01
16-Sep-10 Cadmium
0.1
ND
mg/1
SL
1311
1
1
05-Oct-10 VVK
Frankling NC WTP 1015564-01
16-Sep-10 Lead
0.5
ND
mg/I
SL
1311
1
5
05-Oct-10 VVK
TCLP Volatiles
Client ID# Lab ID#
Collected Anal tc
Rep Lmt
Result
tinits
Mahix Method
DF
RegLvl
Run Analyst
Frankling NC WTP 1015564-01
16-Sep-10 Benzene
0.1
<0.1
mg/L
SL _
1311
1
0.5
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 2-Butanone (MEK)
2
<2.0
mg/L
SL
1311
1
200
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Vinyl Chloride
0.2
<0.2
mg/L
SL
1311 _
1
0.2
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Chloroform
0.1
<0.1
mg/L
SL
1311
1
6
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Chlorobenzene
0.1
<0.1
mg/L
SL
1311
1
100
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Tetrachloroethene
0.1
<0.1
mg/L
SL
1311
1
0.7
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 1,1-Dichloroethene
0.1
<0.1
mg/L
SL
1311
1
0.7
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Carbon tetrachloride
0.1
<0.1
mg/L
SL
1311
1
0.5
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 1,2-Dichloroethane
0.1
<0.1
mg/L
SL
1311
1
0.5.
05-Oct-10 MS
Frankling NC WTP 1015564-01
16-Sep-10 Tdchloroethene
0.1
<0.1
mg/L
SL
1311
1
0.5
05-Oct-10 MS
TCLP BNA
Client 1D# Lab ID#
Collected Anale
Rep Lmt
Result
Units
Matrix Method
DP
RegLvl
Run Analyst
Frankling NC WTP 1015564-01
16-Sep-10 Hexachloro-1,3-butadiene
0.1
<0.1
mg/I
SL
1311
1
0.5
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Nitrobenzene
0.1
<0.1
mg/1
SL
1311
1
2
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-1,0 2,4-Dinitrotoluene
0.1
<0.1
mg/I
SL
1311
1
0.13
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Hexachloroethane
0.1
<0.1
mg/1
SL
.1311
1
3
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 1,4-Dichlorobenzene
0.1
<0.1
mg/1
SL
1311
1
7.5
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Pentachlorophenol
0.25
<0.25
mg/I
SL
1311
1
100
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 2,4,6--Trichlorophenol
0.25
<0.25
mg/1
SL
1311
1
2
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 2,4,5-Trichlorophenol
0.25
<0.25
mg/1
SL
1311
1
400
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Pyridine
0.25
<0.25
mg/I
SL
1311
1
5
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Cresols
5
<5.0
mg/1
SL
1311
1
200
05-Oct-10 AE
Frankling NC WTP 1015564-01
16-Sep-10 Hexachlorobenzene
0.1
<0.1
mg/l
SL
1311
1
0.13
05-Oct-10 AE
Page 4
"Analytical Integrity" - EPA Certified • NELAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 - Fax: 330-253-4489
Web Site: www.settek.com
TCLP Pesticides
Client [DO Lab I #
('ollLcted Anal yte
Rep Lmt
Result
Frankling NC WTP 1015564-01
16-Sep-10 Heptachlor Epoxide
0.002
<0.002
Frankling NC WTP 1015564-01
16-Sep-10 Toxaphene
0.1
<0.1
Frankling NC WTP 1015564-01
16-Sep-10 Chlordane
0.01
<0.01
Frankling NC WTP 1015564-01
16-Sep-10 Methoxychlor
0.002
<0.002
Frankling NC WTP 1015564-01
16-Sep-10 Endrin
0.002
<0.002
Frankling NC WTP 1015564-01
16-Sep-10 Heptachlor
0.002
<0.002
Frankling NC WTP 1015564-01
16-Sep-10 Gamma-BHC
0.002
<0.002
Client ID# Lab ID# Colleted Analyte
Frankling NC V fP 1015564-01 16-Sep-10 2,4,5-TP(Silvex)
Frankling NC WTP 1015564-01 16-Sep-10 2,4,D
Clime ID# lab 11)# Colleeted Analyte
Frankling NC WTP 1015564-01 16-Sep-10 Flash Point
Client ID# Lab ID# Collected Analyze
Frankling NC WTP . 1015564-01 16-Sep-10 pH
TCLP Herbicides
Rep Lmt Result
0.5 <0.5
5 <5.0
Result
>140F
October 12, 2010
Client: Synagro Southeast
Address: 284 Boger Rd.
Mocksville. NC 27028
Received: 9/24/2010
Project #: Franklin WTP
Units Matrix Method 2F RegLyl Run Analyst
mg/I
SL
1311
1
0.008
06-Oct-10 KMG
mg/I
SL
1311
1
0.5
06-Oct-10 KMG
mg/1
SL
1311
1
0.03
06-Oct-10 KMG
mg/I
SL
1311
1
10
06-Oct-10 KMG
mg/I
SL
1311
1
0.02
06-Oct-10 KMG
mg/I
SL
1311
1
0.008
06-Oct-10 KMG
mg/I
SL
1311
1
0.4
06-Oct-10 KMG
Units
Matrix
Method
llF
RggLvi
Run Analyst
mg/I
SL
1311
1
1
06-Oct-10 KMG
mg/I
SL
1311
1
10
06-Oct-10 KMG
Units
Matrix
Method
DF
LOQ
Run Analyst
SL
1010
1
12-Oct-10 DVW
Result Units Matrix Method DF LOQ Run Analyst
6.73 su@23.9C SL 9010 1 0.01 29-Sep-10 DHC
Client ID# Lab ID# Collected Analvtc Result
Frankling NC WTP 1015564-01 16-Sep-10 Reactive Cyanide ND
Client ID# Lab ID# Collected Analvie Result
Frankling NC WTP 1015564-01 16-Sep-10 Reactive Sulfide ND
Ihlits Matrix Method N. LOQ Run Analyst
mg/kg SL 7.3.3.2 1 0.5 27-Sep-10 TIR
Units Matrix Method DF LOQ Run Analyst
mg/kg SL 7.3.4.2 1 25 27-Sep-10 TIR
Page 5
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 - Phone: 330-253-8211 - Fax: 330-253-4489
Web Site: www.settek.com
Report Narrative
Client: Synagro Southeast
Order Number: 1015564
3
No problems were encountered during analysis of this order number, except as noted.
Data Qualifiers:
B = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
DF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request.
Matrices:
A=Air
C = Cream
DW = Drinking Water
L = Liquid
O = Oil
SL = Sludge
SO = Soil
S = Solid
T = Tablet
TC = TCLP Extract
WW = Waste Water
W = Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which
this report was issued. The results contained in this report are only representative of the samples received.
Conditions can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc.
is not responsible for use or interpretation of the data included herein.
"Analytical Integrity" - EPA Certified • iVELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 m Phone: 330-253-8211 - Fax: 330-253-4489
Web Site: www.settek.com
MIN
, I` 1 1 • , •
Sample Summary
Client: Synagro Southeast
Order Number: 1015564
Laboratory ID Client ID
1015564-01 Frankling NC WTP
2
Matrix Sampling Date
Sludge 9/16/2010
"Analytical Integrity" - EPA Certified • NELAP Certified
3310 Win Street - Cuyahoga Falls, Ohio 44223 o Phone: 330-253-8211 • Fax: 330-253-4489
Web Site: www.settek.com
Summit Environmental Ti �jologles, Inc.
Cooler Receipt -
Client:
Order Number;
Date Received:
Time Received: '3
Number otoxes:
N/A
Shipper:UPS
DHL Airborne US Postal Walk-in Pickup Other:
Packaging: Peanuts Bu ble Paper Foam None Other:
Tape on cooledbox:
(YDN WA
Custody Seals intact
Y N !A
C-O-C in plastic /
N NIA
IceBlue ice t//
I absent / melted N/A
Sample Temperature
°C
NIA
C-O-C filled out property
O` N
N/A
Samples in separate bags
Y
(ZN:_�) N/A
Sample containers intact`
CID N N/A
*If no, list broken sample(s):
Sample label(s) complete (ID, date, etc.) N N/A
Label(s) agree with C-O-C Of ) N N/A
Correct containers used (10 N N/A
Suffrclent sample received 1 Y� N NIA
Bubbles absent from 40 mL vials-
►l
** Samples with bubbles less than the size of a pea are acceptable.
N /A
Was client contacted about samples Y N
Will client send new samples Y N
Client contact:
Date/Time:
Logged in by:
Comments:
Rev. 6
Summit Environmental Technologies, Inc. Analysis Request/Chain of Custody
3310 Win Street
n.... t, .. n..yt., r,>,: AAI)I)o rr 1. "I , 1C— '10n n« Anon For Summit Environmental Technologies, Inc. use only
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Page of
SET No.
Company Name (Please Print)
�
Project Name
Analytical Parameters and Methods
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Company Address
Project Address
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Client Phone No.
Report to
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Client Fax No. 2 lee Fax Result ✓
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Quote No.
Con Pers
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Sample/ram by / ,„ P
Check if Ohio VAP samples ✓
rig
#
Sample Identification
ate
Timea
Collected
Collected
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lit
Please Check Analytical Box
MENNEN
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Date , manager
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�'' White and yellow pages should accompany samples to the laboratory. The client retains the pink page. t r c n n
Page: 1 of 2
Report Number: 10-273-0201
Account Number: 46622
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAUTECHNICAL
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 78750
Sample Id: FRANKLIN WTP
AFL Eastern Laboratories, Inc.
7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
www.al-labs-east6rn.com
Project: FRANKLIN WTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/29/2010 10:13:00
Date Received: 09/30/2010 00:00
Date Reported: 10/04/2010
Total Solids *
4.71
47100
100.0
JM
09/30/2010 15:00
SM-2540G
Moisture *
95.29
100.0
JM
09/30/2010 15:00
SM-254OG
Total Kjeldahl Nitrogen
0.68
6790
10.0
JM
10/01/2010 08:05
SM-4500-NH3C-TKN
Total Phosphorus
0.09
854
100
KM
10/01/2010 08:00
SW 6010C
Total Potassium
0.13
1260
100
KM
10/01/2010 08:00
SW 6010C
Total Sulfur
0.33
3340
100
KM
10/01/2010 08:00
SW 6010C
Total Calcium
0.11
1130
100
KM
10/01/2010 08:00
SW 6010C
Total Magnesium
0.23
2300
100
KM
10/01/2010 08:00
SW 6010C
Total Sodium
0.02
185
100
KM
10/01/2010 08:00
SW 6010C
Total Iron
29600
1
KM
10/01/2010 08:00
SW 6010C
Total Aluminum
217000
10
KM
10/01/2010 08:00
SW 6010C
Total Manganese
544
1
KM
10/01/2010 08:00
SW 6010C
Total Copper
61
1
KM
10/01/2010 08:00
SW 6010C
Total Zinc
84
1
KM
10/01/2010 08:00
SW 6010C
Ammonia Nitrogen
0.17
1700
10.0
JM
10/01/2010 08:05
SM-4500-NH3C
Organic N
0.51
5090
10.0
10/01/2010 08:05
CALCULATION
Nitrate+Nitrite-N
23.4
1.00
JM
10/01/2010 08:05
SM-450ONO3F
Total Cadmium
<1.0
1.0
KM
10/01/2010 08:00
SW 6010C
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis.
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole orpart, nor may any reference be made Pof�
C.to the work. the results, or the company in any advertising, news release, or otherpublic announcements without obtaining our prior written authorization.
Pauric McGroary
Page: 2 of 2
Report Number: 10-273-0201
Account Number: 46622
Submitted By: MARSHALL PURYEAR
Send To: SYNAGRO CENTRAL/TECHNICAL
MARY BREWER
284 BOGER RD
MOCKSVILLE , NC 27028
Lab Number: 78750
Sample Id: FRANKLIN WTP
Y A&L Eastern Laboratories, Inc.
7621 Whitepine. Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446
www.al-labs-eastem.com
Project: FRANKLIN WTP
NC CERT#257
REPORT OF ANALYSIS
Date Sampled: 9/29/2010 10:13:00
Date Received: 09/30/2010 00:00
Date Reported: 10/04/2010
Total Chromium
79
5
KM
10/01/2010 08:00
SW 6010C
Total Nickel
22
5
KM
10/01/2010 08:00
SW 6010C
Total Lead
10
5
KM
10/01/2010 08:60
SW 6010C
Total Arsenic
4.0
1.0
KM
10/01/2010 08:00
SW 6010C
Total Mercury
<0.4
0.4
KM
10/01/2010 09:00
SW-7471B
Total Selenium
<1.0
1.0
KM
10/01/2010 08:00
SW 6010C
pH (Standard Units) *
6.47
JM
10/01/2010 08:30
SW-9045D
Total Volatile Solids
25.65 256500
100.0
JM
09/30/2010 15:00
SM-2540G
Total Molybdenum
<5
5
KM
10/01/2010 08:00
SW 6010C
Comments:
IE LRB WAS SLIGHTLY OUT OF LIMITS FOR "Cu" AND Mn". ALL OTHER QC IS ACCEPTABLE.
-IE MATRIX SPIKE RESULTS FOR "AI", "Cr", "Fe", AND "Se" ARE OUT OF LIMITS. ALL OTHER QC DATA IS ACCEPTABLE.
All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. /
Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or part, nor may any reference be made ?Wi
1 Vto the work. the results, or the company in any advertising, news release, or other public announcements withoutobtaining our prior written authorization. a
Pauric McGroary
Analy deal Results
Synagro Central
284 Boger Rd.
Mocksville NC 27028
Entered 11123/2010
Reported: 1212/2010
For:
-Sample ID
Parameter Cust 1,13
Result
Units -
Method
Date Analyzed
Analyst
1001 123-5:4
% Soli.ds F4
5.1
%
SM2540B
11/23/10
MID
1001123"5.4
Fecal Collform, MTF F4
<4
MPN/g
SM92210E,
11/23/10
MID
Respectfully submitted,
Dena Myers
N.CQert #440,
N6-DW Cert #37756,
EPA NCOG9,09 -
I
P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697
Client:
0"
STATESVILLE ANALYTICAL
122Court Street - P.O.Box 228
Statesville, NC 28687
(704) 872-4697
Address: '> e."
'o
Contact Person:
Phone #
IlDe-
FAX#
Chain of
PO #
Requisitioned
by: Crime
Date)
Custody Record
Customer
Lab -ID #
Time Sampled
Date Sampled
E
0
Matrix
Parameters requested
for analysis
Sludge l
W 1
VVW
Sample 1D#
(Grab Only)
(Grab Only)
0
Q X12 '5'
X
5W) 2/ 6E
'2L
61V 17- If
it
f;
4
Relinquished
Time 1Gi
am, pm Date," /0-3/ /0
Sampled by:
Received by:
Time
am, pm Date
Transported by:
Relinquished by:
Time
am, pm Date
Holding times met:
'eM,�PM
Received by:
Time
JID at
Compliance work:
Composite Sampling
#11:
Time begin-
am, pm Date
Non-compliance work:
Time end
am, pm Date
Lab Comments:
Composite Sampling
#2:
6
1
Time begin-
am, pm Date
Time end
am, pm Date