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HomeMy WebLinkAboutNC0006351_Wasteload Allocation_19941018NPDES WASTE L OAD ALLOCATION PERMIT NO.: NC0006351 PERMI 1'1'EE NAME: FACILITY NAME: Chemical Specialties, Inc. Mineral Research & Development Facility Status: Existing Permit Status: Renewal Major Minor �l Pipe No.: 001 Design Capacity: 0.025 MGD Domestic (% of Flow): Industrial (% of Flow): 100 % Comments: Inorganic chemical manufacturing, 40 CFR 415.360 applies to Copper Nitrate. 455.10 applies to pesticides. No other guidlines. Discharge includes cooling water, process water, boiler blowdown, etc. See attached schematic. RECEIVING STREAM: the Rocky River Class: C Sub -Basin: 03-07-11 Reference USGS Quad: F 16 SE & F 16 SW (please attach) County: Cabarrus Regional Office: Mooresville Regional Office Previous Exp. Date: 9/30/94 Treatment Plant Class: Class II Classification changes within three miles: Requested by: Prepared by: Reviewed by: Dana Bolden f' Date: 9/29/94 Date: /0/J7/ 4 Date: l a Modeler Date Rec. # Drainage Area (mil ) J.36 Avg. Streamflow (cfs): 7Q10 (cfs) .4 ' Winter 7Q: Toxicity Limits: IWC 0, % Instream Monitoring: Parameters ki I k Upstream Ai II: Location Downstream Location Flow (MGD): TSS (lbs/day): NH3-N (mg/1): Copper (#/day): Nickel (#/day): Selenium (mg/I) Selenium (#/day): pH (SU): Zinc (#/day): Chromium (#/day): Arsenic (ug/1): Cadmium (#/day): monitor Manganese (ug/1): monitor Oil and Grease (mg/1) monitor Pesticides include guideline language/ definition "L''`back of page Special monitoring requirements: Limited parameters mllst be monitored for 30 consecutive days at least once a year per 40 CFR 415.363. The month chosen should be either Jan, Apr, Jul, 0 The rest of the 11 months POC's should be monitored monthly. Toxicants which have monitoring requirements should be monitored quarterly (Jan, Apr, Jul, Oct) to conicide with the WET test. Acu hronic (jf/966 L 700 -fYAr faHg-d Monthly Avg. Daily Max. 0.025 0.025 2.2g • 6.83 BAT 2 /`back of pages 3 IA. 1' BPJ 0.099 10.30 BAT 0.198 0.60 BAT 0.240 0.521 corresponding concentrations 0.050 0.108 WQ limited need #/day & mg/1 6-9 6-9 BAT 0.313 0.626 . BPJ 0.104 0.200 BPJ 0.208 0.416 BPJ monitor Qrtly monitor Qrtly Comments: 3 **See staff report for further detail. Region, P&E and facility met (2/8/94) about interim limits for NH3N and Zinc while facility is upgrading 1. Begin construction of proposed wastewater treatment plant modifications (necessary to achieve compliance with final effluent limitations) on or before May 15,1994 (Facility met this requirement). 2. Complete construction of proposed wastewater treatment plant modifications (necessary to achieve compliance with final effluent limitations) on or before August 1, 1995 3. Achieve compliance with final effluent limitations on or before October 1, 1995. Interim Limts should apply until September 30, 1995. Monthly Avg. Daily Max. NH3N (#/day): 4.0 5.0 Zinc (#/day): 0.70 1.40 County Water Supply 74,400 GPD 4,200 GPD 1,400 GPD m r Water Softeners 4,200 GPD r Boilers `200 GPD Evap. 4,000 GPD A 400 GPD 2,100 GPD Evap. Rain Scrubber 1,000 GPD 8,500 GPD Rain 1-,000 GPD Lime 200 GPD Waste to Landfills 48,600 GPD 17,600 GPD Chemical Manufacturing 44,500 GPD in Products 6,000 GPD 16,000 GPD Evap. Cooling Towers r r rr Waste Treatment < Plant 6,900 GPD Rain r f11,600 GPD Evap. 2 Acre Storage Lagoon 1,700 GPD Rain 1,600 GPD 2,900 GPD Evap. 1 1/2 Acre Storage 144,000 GPD Lagoon Max. 144,000 GPD Max. Recycle Settling Tank 16,200 GPD Discharge 001 2,600 GPD Sanitary Water 100 GPD Consumed Septic Tank 2,500 GPD Drain Field Schematic of Water Flow Chemical Specialies, Inc. Harrisburg, Cabarrus, NC March 1, 1994 P. 1 of 1 Zinc Nitrate -Acetic Zinc Nitrate -Citric Arsenic Acid Chromated Copper Arsenate Sodium Bichromate (sold but not produced on site) I / Ultrawood -- War piNd for - in1�Te40f-0d �� 4 Weed- v ' ,or S4'9 1 CSI Products - The following are taken from CSI's Pretreatment permit application. Aluminum Nitrate Calcium Chelate Calcium Nitrate - Copper Ammonia Carbonate % Copper Count-N Ce : r^fr" onie ,fcr.f fe Copper Nitrate Tar? - 1--- Hydrogen Peroxide blends (hydrogen peroxide is not produced on site) Magnesium Acetate Magnesium Chloride or Zacure MG-60 Magnesium Chloride - Buffered Magnesium Dihydrogen Phosphate or Zacure M-33 Magnesium Nitrate Manganese Chloride Manganese Nitrate Micro-Nite Citrus Special e� — A/W ,' g , 1 f ni c Gc" • Mold Guard Products 1 Ora -Cop — �j f' fn►c. 4 oat 4/9 r 1�,Irtoc Prod, flag /i//.o,4 ,h 417` y r. 4// . yD ire 7%req° si4ce Ayo'/ .e4 (0)/ ped .f,, r ; Ltd Preact 7-;4c 11/no4a ACT4 /;de Gy1,/gnT Zinc Acetate Zinc Ammonia Carbonate Zinc Chloride (Zinc Chloride is not produced on site [packaged and diluted-djb]) Cr4per ✓t ez) / iiZel D-Blaze P 11 n c arc; d. evw bor,' ati'4 6.76,„c44 c ,f47 7441 fvf5p47te) Vod In444 % ACQ-Q (not presently produced on site, but raw materials are stored and shipped from Harrisburg) :'9 K,'�Qlj4P4 cry/l' qr 4l/' �Cl ./�711C0fe cry/ c Sow e �� •��9� cC He Pelf: r-r• oe5 Cder,P of Me deO1 i7 opePi*c,1t 7 GS z ifid s 741-✓o ,1v Citecy ram lle3s , 7e ,‘,..ev (/ a. -i,%% 4 '4) , 2 A6e,t mer elteeP qnt . 4 44f e�ff f q� II' --/P5 c%r 'd /7t, - t/ GrivT1) • /Q/% e�l/pv. is (oleiinPd 4 e fie. ee5$ e 1rri,%7/4C- M18 3.S A-04, cis, rec c.ce ��sre. , qo c`, Ad- -1/� 544,(1- fr .1kies %s 44 e - _-74-- 54Ca/I 6e .x.71"-r7f--- o 4)(` D roe9YPf1 /ef c - ° W �.•/�`d f-de 4 Enos A/so cO 41.—r; yf e C.t - 1 v✓'s/I ez,t7rP i. s'. gorr'7 5- ;4 cl,'c4 47/- tie o7iif1` fires ler ke a /yIGI_ %-9Pe /rn/t c✓ucf o„ 7441. tie Cl -g f•- / 74111 or c� /../mY )�1"P i CV% e77) -�a. IA five t✓Qu /9' 7 -TAN` Ab )9,--:-..- pm 9 o c. , V47, 36 &aO PL 4 /�. s-,r) Vihr TSS : C7.067 . o. a3 PC�%� °-D0030E c70,9/D q'// ra /6,r /1/sPo '74: 5411'1A'(.o.4a1S. 0.1 04DS0 9 0 ° c_ 00 ,_2•95-r.,,,w.v <d (-4)Vvi jor&7,./...1)) P-cf., a 6e TS, I 3;454g Cr? WQ o o*7 0. 325 4%47 iqsg. 0 zs z ( a o2v-) ,(7-x' qq71-1. nle ccoriii.pefdl• rooterer9d /iitcf )71- fie /9ePrt/cf(le 0/1-4. /0 cco Op)ZZYe ;446 Je Cerro( .get -71/1 se,vtr d 15-.41s /g44-, disetfif e or _preerf,i,erzt...v Zf; r %pear (7.740 elitmC. siewe/1 te d %/1 74e ?to r•71,7. 4 nology available, energy re - and costs) which can affect ry s'abcategorization and ef- ls established. It is, however, lat data which would affect Cations have not been avail- t,s a result, these limitations ldjusted for certain plants in ,ry. An individual discharger lterested person may submit to the Regional Adminis- to the State, if the State has •ity to issue NPDES permits) rs relating to the equipment es involved, the process ap- )ther such factors related to .arger are fundamentally dif- m the factors considered in ishment of the guidelines. On of such evidence or other information, the Regional atur ('or the State) will make finding that such factors are fundamentally different for .ty compared to those speci- e Development Document. If iamentally different factors to exist, the Regional Admin- • the State shall establish for trger effluent limitations in S permit either more or less than the limitations estab- ein, to the extent dictated by amentally different factors. tations must be approved by inistrator of the Environ- otection Agency. The Admin- nay approve or disapprove rations, specify other limita- nitiate proceedings to revise ilations. following limitations estab- uantity or quality of pollut- Ilutant properties, controlled 3ragraph, which may be dis- om the manufacture of essen- )y a point source subject to lions of this paragraph after n of the best practicable con- ology currently available: rghckg of product; English units, Ib/1,000 Ib of product) racteristic Effluent limitations Maximum for any 1 day Average of daily values to 30 consecutive days shall not exceed- 22.7 9.01 12.0 3.11 [Metric units, kg/kkg of product; English units, lb/1,000 Ib of product }---Co n li n u ed Effluent characteristic Effluent limitations Maximum for any 1 day Average of daily values for 30 consecutive days shall not exc ed pH Within the range 6.0 to 9.0. (') (' ) Subpart F—Rosin-Based Derivatives Subcategory § 454.60 Applicability; description of manufacture of rosin -based deriva- tives subcategory. The provisions of this subpart are ap- plicable to discharges resulting from the manufacture of rosin -based deriva- tives. § 454.61 Specialized definitions. For the purpose of this subpart: (a) Except as provided below, the gen- eral definitions. abbreviations and methods of analysis set forth in 40 CFR Part 901 shall apply to this subpart. (b) The term "product" shall mean rosin -based derivatives. § 454.62 Effluent limitations and guide- lines representing the degree of ef- fluent reduction attainable by the application of the best practicable control technology currently avail- able. In establishing the limitations set forth in this section, EPA took into ac- count all information it was able to collect, develop and solicit with re- spect to factors (such as age and size of plant, raw materials, manufacturing processes, products produced, treat- ment technology available, energy re- quirements and costs) which can affect the industry subcategorization and ef- fluent levels established. It is, however, possible that data which would affect these limitations have not been avail- able and, as a result, these limitations should be adjusted for certain plants in this industry. An individual discharger or other interested person may submit evidence to the Regional Adminis- trator (or to the State, if the State has the authority to issue NPDES permits) that factors relating to the equipment or facilities involved, the process ap- plied, or other such factors related to such discharger are fundamentall ferent from the factors considere the establishment of the guideline the basis of such evidence or o available information,4 the Regi Administrator (or the State) will a written finding that such factors or are not fundamentally differen that facility compared to those s fied in the Development Document. such fundamentally different factors are found to exist, the Regional Admin- istrator or the State shall establish for the discharger effluent limitations in the NPDES permit either more or less stringent than the limitations estab- lished herein, to the extent dictated by such fundamentally different factors. Such limitations must be approved by the Administrator of the Environ- mental Protection Agency. The Admin- istrator may approve or disapprove such limitations, specify other limita- tions, or initiate proceedings to revise these regulations. (a) The following limitations estab- lish the quantity or quality of pollut- ants or pollutant properties, controlled by this paragraph, which may be dis- charged from the manufacture of rosin - based derivatives by a point source subject to the provisions of this para- graph after application of the best practicable control technology cur- rently available: (Metric units, kg/kkg of product; English units. bl1,000 Ib of product( Effluent characteristic Effluent limitations Maximum for any 1 day Average of daily values tor 30 consecutive days shall not exceed-- BOD5 TSS pH 1.41 0.045 (') 0.748 0.015 (1) t Within the PART 455—PESTICIDE CHEMICALS Sec. 455.10 General definitions. Subpart A —Organic Pesticide Chemicals Manufacturing Subcategory 455.20 Applicability; description of the or- ganic pesticide chemicals manufacturing subcategory. 455.21 Specialized definitions. .22 Effluent limitations guidelines rep- resenting the degree of effluent reduction attainable by the application of th9 best practicable control technology currently available. Subpart B—Metalio-Organic Pesticide Chemicals Manufacturing Subcategory 455.30 Applicability; description of the metallo-organic pesticide chemicals manufacturing subcategory. 455.31 Specialized definitions. 455.32 Effluent limitations guidelines rep- resenting the degree of effluent reduction attainable by the application of the hest practicable control technology currently available. Subpart C—Pesticide Chemicals Formulating and Packaging Subcategory 455.40 Applicability; description of the pes- ticide chemicals formulating and pack- aging subcategory. 455.42 Effluent limitations guidelines rep- resenting the degree of effluent reduction attainable by the application of the best practicable control technology currently available. AUTHORITY: Secs. 301, 304, 306. 307, and 501, Pub. L. 92-500, 86 Stat. 816, Pub. L. 95-217, 91 Stat. 156 (33 U.S.C. 1311, 1314, 1316, 1317, and 1361). SOURCE: 43 FR 17776, Apr. 25, 1978, unless otherwise noted. *455.10 General definitions. As used ' s his .. rt: (a)(1) " gt8.1iee or tended for pelling, or ' ` t. (b) "Active ingredient" means an in- gredient of a pesticide which is in- tended to prevent, destroy, repel, or mitigate any pest. (c) "Pesticide chemicals" means the sum of all active ingredients manufac- tured at each facility covered by this part. (d) 1) Any insect, ro- dent, nematode, , weed, or (2) any other form of terrestrial or aquatic plant or animal life or virus, bacteria, or other micro-organism (except virusus, bacteria, or other micro-orga- nisms on or in living man or other liv- ing animals) which the Administrator declares to be a pest under section 25(c)(1) of Pub. L. 94-140, Federal Insec- ticide, Fungicide and Rodenticide Act. 338 339 ,• -V r' (e) Except as provided in this regula- ,,ion, the general definitions, abbrevia- ns and methods of analysis set forth n Part 401 of this chapter shall apply o this part. '3 FR 17776, Apr. 25, 1978, as amended at 50 40701, Oct. 4, 1985; 51 FR 44911, Dec. 15, 6] ;ubpart A —Organic Pesticide: Chemicals Manufacturing Subcategory Seugc : 43 FR 44846, Sept. 29, 1978, unless -herw•ise noted. - ...455.20 Applicability; description of the organic pesticide chemicals manufacturing subcategory. a) For the purpose of calculating ef- r_nt limitations for COD, BOD5, and S, the provisions of this stibpart are oplicable to discharges resulting from ,,ne manufacture of organic active in- redients, excluding the following: ]ethrin, Benzyl Benzoate, Biphenyl, sethylxanthogen, Chlorophacinone, umafuryl, Dimethyl Phthalate, .phacinone, Endothall Acid, EXD :=lerbisan), Gibberellic Acid, lyphosate, Methoprene, Naphthalene -etic Acid, Phenylphenol, Piperonyl toxide, Propargite, 1,8 Naphthalic Ihydride, Quinomethionate, .;;smethrin, Rotenone, Sulfoxide, So- iium Phenylphenate, Triazine com- :'ands (both symmetrical and asym- trical), and Warfarin and similar i coagulants. o) For the purpose of calculating .'T effluent limitations for organic 'esticide chemicals, the provisions of his subpart are applicable to dis- 1-arges resulting from the manufac- :'e of the following organic active in- -dients: Aldrin, BHC, Captan, .lordane, DDD, DDE, DDT, Dichloran, ieldrin, Endosulfan, Endrin, Hepta- hlor, Lindane, Methoxychlor, Mirex, 'CND. Toxaphene, Trifluralin, ,zinphos Methyl, Demeton-O, lemeton-S, Diazinon, Disulfoton, Mal - 'lion, Parathion Methyl, Parathion ). Aminocarh, Carbary], hiocarb, Mexacarbate, Propoxur, ..:.ban, Chlorpropham, Diuron, nuron, Fenuron-TCA, Linuron, -:uron, . Monuron-TCA, Neubron, tam, Swep, 2,4-D, Dicamba, 40 CFR Ch. I (7-1-93 Edition) ex, 2,4,5-T, Siduron, Perthane,,and fol. ) The intermediates used to manu- ure the active' ingredients and ac- ingredients used solely in experl- ntal pesticides are excluded from - coverage in this subpart. Insecticidal pathogenic organisms such as Bacillus thuringicnsis, insect growth horrnones,, plant extracts such as pyrethrins;.sex attractants and botanicals such•as Ro- tenone are also excluded from BPT coverage in this subpart. [43 FR 44846, Sept. 29, 1978, as amended at 50 FR 40702, Oct. 4, 1985; 51 FR 44911, Dec..15, 1986] § 455.21 Specialized definitions. (a) "Organic active ingredients" means carbon -containing active ingre- dients used in pesticides, excluding metalloorganic active ingredients. (b) "Total organic active ingredi:: ents" means the sum of all organic ac tive ingredients covered by §455.20(a) which are manufactured at a facility._; subject to this subpart. , (c) "Organic pesticide chemicals' means the sum of all organic active in- gredients listed in §455.20(b) which:are manufactured at a facility subject to this subpart. §455.22 Effluent limitations guidelines.- representing the degree of effluent': reduction attainable by the applica- ' tion of the best practicable control technology currently available. In establishing the limitation set forth in this section, EPA took into ac- count all information it was able to collect, develop, and solicit withre- spect to factors (such as age and size of plant, raw materials, manufacturing processes, products produced, treat- ment technology available, energy re- quirements, and costs) which can affect the industry subcategorization and ef- fluent levels established. It is possible, however, that data which would affect these limitations have not been avail- able and, as a result, these limitations should be adjusted for certain plants in this industry. An individual discharger or other interested person may submit evidence to the Regional Adminis- trator (or to the State, if the State has the authority to issue NPDES permits) that factors relating to the equipment Environmental Protection Agency or facilities involved, the process ap- plied, or other such factors related to such discharger are fundamentally dif- ferent from the factors considered in the establishment of the guidelines. On the basis of such evidence or other available - information, the Regional Administrator (or the State) will make a written finding that such factors are or are not fundamentally different for that facility compared to those speci- fied in the Development Document. If such fundamentally different factors are found to exist, the Regional Admin- istrator or the State shall establish for the discharger effluent limitations in the NPDES permit either more or less stringent than the limitations estab- lished herein, to the extent dictated by such fundamentally different factors. Such limitations must be approved by the Administrator of the Environ- mental Protection Agency. The Admin- istrator may approve or disapprove such limitations, specify other limita- tions, or initiate proceedings to revise these regulations. The following limitations establish the quantity or quality of pollutants or pollutant properties controlled by this paragraph which may be discharged from the manufacture of organic active ingredient by a point source subject to the provisions of this paragraph after application of the best practicable con- trol technology currently available. Effluent characteristics Effluent limitations Maximum for any 1 day Average of daffy values for 30 consecutive days shall not exceed — COD B00 TSS Organic pesticide chemicals pH 13.000 7.400 6.100 .010 (') 9.0003 1.6000 1.E000 .0018 () Within the range of 6.0 10 9.0. ' NOTE: For COD, BOD5, and TSS, metric units: iGl gram/ 1.000 kg of Iota/ organic active ingredients. English units: Pound/.1,030 lb of total organic active ingredients. For organic pesticide chemicals —metric units: Kilogram/1.000 kg of or- ganic pesticide chemicals. English units: Pound/1.000 b of or- ganic pesticide chemicals. Subpart B—Metallo-Organie, Pes- ticide Chemicals Manufactur- ing Subcategory § 455.30 Applicability; description of the metallo-organic pesticide chemicals manufacturing sub- category. The provisions of this subpart, are ap- plicable to discharges resulting from the manufacture of metallo-organic ac- tive ingredients containing mercury, cadmium, arsenic, or copper. The man- ufacture of intermediates used to man- ufacture the active ingredients are ex- cluded from coverage by this subpart. § 455-31 Specialized definitions. (a) "Metallo-organic active ingredi- ents" means carbon containing active ingredients containing one or more me- tallic atoms in the structure. § 455.32 Effluent limitations guidelines representing the degree of effluent reduction attainable by the applica- ' tion of the best practicable control technology currently available. In establishing the limitations set forth in this section, EPA took into ac- count all information it was able to collect, develop and solicit with re- spect to factors (such as age and size of plant, raw materials, manufacturing processes, products produced, treat- ment technology available, energy re- quirements and costs) which can affect the industry subcategorization and ef- fluent levels established. It is possible, however, that -data which would affect these limitations have not been'avail- able and, as a result, these limitations should be adjusted for certain plants in this industry. An individual discharger or other interested person may submit evidence to the Regional Adminis- trator (or to the State, if the State has the authority to issue NPDES permits) that factors. relating to the equipment or facilities involved, • the process ap- plied, or other such factors related to such discharger are fundamentally dif- ferent from the factors considered in the establishment of the guidelines. On the basis of such evidence or other available information, the Regional • Administrator (or the State) will make a written finding that such factors are or are not fundamentally different. for 4U 1,-tK l,.I1. r ./—r--YJ talrla(1) Environmental Protection Agency §447. tlt facility compared to those speci- fied in the Development Document. If such fundamentally different factors are found to exist. the Regional Admin- istrator or the State shall establish for the discharger effluent limitations in the NP'D1 S permit either more or less stringent than the limitations estab- lished herein, to the extent dictated by such fundamentally different factors. Such limitations must be approved by the Administrator of the Environ- mental Protection Agency. The Admin- istrator may approve or disapprove such limitations. specify other limita- tions, Or initiate proceedings to revise these regulations. The following limitations establish the Quantity or quality of pollutants or pollutant properties controlled by this paragraph which may be discharged from the manufacture of metallo-or- ganic active ingredients by a point source subject to the provisions of this paragrah after application of the best practicable control technology cur- rently- available: There shall be no dis- charge of process waste water pollut- ants to navigable waters. Subpart C—Pariciar. Cher Formulating and Pack g Subcategory § 455.40 Applicability; description of the pesticide chemicals formulating and packaging subcategory. The provisions of this subpart are ap- plicable to discharges resulting from all pesticide formulating and packag- ing operations. (51 FR 44911, Dec. 15, 1986) 455.42 Effluent limitations guidelines representing the degree of effluent reduction attainable by the applica- tion of the best practicable control technology currently available. In establishing the limitations set forth in this section, EPA took into ac- count, all information it was able to collect, develop and solicit with re- spect to factors (such as age and size of plant, raw materials, manufacturing processes, products produced. treat- ment technology available, energy re- quirements and costs) which can affect the industry subcategorization and ef- fluent Levels established. It is possible, however, that data which would affect these limitations have not been avail- able and, iLti a result.. these limitations should be adjusted for certain plants in this industry. An individual discharger or other interested person nra,v submit, evidence to the Regional Adminis- trator (or to the State. if the State has the authority to issue NPDES permits) that factors relating to the equipment or facilities involved. the process ap- plied. or other such factors related to such discharger are fundamentally dif- ferent from the factors considered in the Establishment of the guidelines. On the basis of such evidence or other available information. the Regional Administrator (or the State) will make a written finding that such factors are or are not fundamentally different for that facility compared to those speci- fied in the Development Document. If such fundamentally- different, factors are found to exist, the Regional Admin- istrator or the State shall establish for the discharger effluent limitations in the NPDES permit either more or less stringent than the limitations estab- lished herein. to the extent dictated by such fundamentally different factors. Such limitations roust he approved by the Administrator of the Environ- mental Protection Agency. The Admin- istrator may approve or disapprove such limitations, specify other limita- tions, or initiate proceedings to revise these regulations. The following limitations establish the quantity or quality of,, pollutants or pollutant properties coftrolled by this paragraph from the formulation and packaging of pesticides by a point source subject to the provisions of this paragraph after application of the best practicable control technology cur- rently available: PART 457—EXPLOSIVES MANUFAC- TURING POINT SOURCE CAT- EGORY Subpart A —Manufacture of Explosives Subcategory Sec. 457.10 Applicability; description of the com- mercial manufacture of explosives sub- category. 4;;7.11 specialized definitions. 957.12 Effluent limitations and guidelines representing the degree of effluent reduc- tion attainable by the application of the best practicable control technology cur- rently available. Subpart B—(Reserved) Subpart C—Explosives Load, Assemble, and Pock Plants Subcategory 457.30 457.31 457.32 Efflu^r:[ represents;..! lion atlas;;, best prael rent.ly ava: ,:bib''. `on- :311. 1::90.6 and i . 86 Stat. 816 et .seq.. !'`ub. L. 92- sou0cE: 41 FR. 10184. Mar. theru•ise note'.. Subpart A —Manufacture of Explosives Subcategory .457.10 Applicability; description of the commercial manufacture of ex- plosives subcategory. The provisions of this subpart are alr plicable to discharges resulting from the production of explosives. § 457.11 Specialized definitions. For the purpose of this subpart: (a) Except as provided below. the gen- eral definitions. abbreviations and methods of analysis set forth in 40 CFR Part 401 shall apply to this subpart. (b) The term "product. shall mean dynamite, nitroglycerin. cyclotrimethylene trinitramine ;RDX). cyclotetramethylene tetranitramine (HMX), and trinitrotoluene (TNT). § 457.12 Effluent limitations and guide- lines representing the degree of ef- fluent reduction attainable by the application of the best practicable control technology currently avail- able. In establishing the limitations set. forth in this section, FPA took into ac- count all information it was able collect, develop and solicit with spect to factors (such as age and size plant„ MIN nraterirLis, ilia 111 firl'tll t'l processes, products, produced, -tre. rnclit technology available, cnert'y quirements and costs) which can affc the industry subcategorization and fluent levels establishes . It is, howev possible t.ha.t (lava which would af' these lirnita.tir,ns have not. been ,t,, able and, 0- . ill., these lu, htt!cl l,c• :v: . ...I for e'..'.;i ; h indutr . . indi', r ut 11(1. Ind 11.1N. evidence tc• Region),: Admil trator (or t:n r'.. state. if St. the author'i'.ssue l:I':'ii that factor_, to '.1. flied. or fever t1Y.• F'Sl.cf.Uh . can 11)011,i ; of the guidelines. basis .:.:i; evidence or ot: liable information. the Regio :ninistrat.or'or the State) will nu .L written finding that such factors or are not fundamentally,different that facility c-ompared to those sp fled in the Development Document such fundamentally different fact are found to exist. the Regional Adn. istrator or the State shall establish, the discharger effluent limitations the NPDES permit either more or stringent than the limitations est fished herein, to the extent dictated such fundamentally different fact, Such limitations must be approved the Administrator of the Envii mental Protection Agency. The Adn istrator may approve or disappr such limit:' ,: ns. specify other lim t-ions, or it,. , proceedings to re' these regui..O: :. . (a) The toll .v ng limitations esl lish the quanr.il;; or quality of poi ants or pollutant properties. cont.ro by this paragraph, which may be charged from the manufacture of plosives by a point source subject the provisions of this paragraph a application of the best practical trol technology currently available: 342 343 §415.350 itations are the same for TSS and pH as specified in § 415.342. [47 FR 55227, Dec. 8, 1982] Subpart AI —Chromic Acid Production Subcategory § 415.350 Applicability; description of the chromic acid production sub- category. The provisions of this subpart are ap- plicable to discharges resulting from the production of chromic acid in fa- cilities which also manufacture sodium dichromate. § 415.351 Specialized definitions. [Re- served] § 415.352 Effluent limitations guide- lines representing the degree of ef- fluent reduction attainable by the application of the best practicable control technology currently avail- able (BPT). Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart must achieve the following effluent limita- tions representing the degree of efflu- ent reduction attainable by the appli- cation of the best practicable control technology currently available (BPT): There shall be no discharge of process wastewater pollutants to navigable wa- ters, except as provided for in § 415.172. §§ 415.353--415.355 [Reserved] § 415.356 Pretreatment standards for new sources (PSNS). Except as provided in 40 CFR 403.7, any new source subject to this subpart which introduces pollutants into a pub- licly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources (PSNS): The limitations are the same as specified in § 415.352. [49 FR 33421, Aug. 22, 1984] Subpart AJ—Copper Salts Production Subcategory 40 CFR Ch. I (7-1-93 Edition) § 415.360 Applicability; description of the copper salts production sub- category. The provisions of this subpart are ap- plicable to discharges and to the intro- duction of pollutants into treatment works which are publicly owned result- ing from the production of copper salts, including (a) copper sulfate, copper chloride, copper iodide, and copper ni- trate, and (b) copper carbonate. § 415.361 Specialized definitions. For the purpose of this subpart: (a) Except as provided below, the gen- eral definitions, abbreviations, and methods of analysis set forth in part 401 of this chapter shall apply to this subpart. (b) The term product shall mean cop- per salts. (c) The term copper shall mean the total copper present in the process wastewater stream exiting the wastewater treatment system. (d) The term selenium shall mean the total selenium present in the process wastewater stream e..iting the wastewater treatment system. (e) The term nickel shall mean the total nickel present in the process wastewater stream exiting the wastewater treatment system. § 415.362 Effluent limitations guide- lines representing the degree of ef- fluent reduction attainable by the application of the best practicable control technology currently avail- able (BPT). (a) Except as provided in 40 CFR 125.30 through 125.32 any existing point source subject to this subpart and pro- ducing copper sulfate, copper chloride, copper iodide, or copper nitrate must achieve the following effluent limita- tions representing the degree of efflu- ent reduction attainable by the appli- cation of the best practicable control technology currently available (BPT). Environmental Protection Agency SUBPART AJ—COPPER SULFATE, COPPER CHLORIDE, COPPER IODIDE, COPPER NITRATE Pollutant or pollutant property BPT effluent limitations Maximum for any 1 day Average of daily values for 30 con- secutive days TSS copper m Nickel m Selenium (T) PH Kg/kkg (or pounds per/1,000 lb) of product 0.069 0.0030 0.0060 0.0015 (') 0.023 0.0010 0.0020 0.00050 t Within the range 6.0 to 9.0. (b) Except as provided in 40 CFR 125.30 through 125.32 any existing point source subject to this subpart and pro- ducing copper carbonate must achieve the following effluent limitations rep- resenting the degree of effluent reduc- tion attainable by the application of the best practicable control technology currently available (BPT): SUBPART kJ —COPPER CARBONATE Pollutant or pollutant property BPT effluent limitations Maximum for any 1 day Average of day values for 30 con- secutive days TSS Copper m Nickel (T) Selenium (T) pH Kykkg (or pounds per/1,000 lb) of product 4.2 0.19 0.37 0.093 (') 1.4 0.064 0.12 0.031 ' Within the range 6.0 to 9.0. §415.363 Effluent limitations guide- lines representing the degree of ef- fluent reduction attainable by the application of the best available technology economically achievable (BAT). (a) Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart and pro- ducing copper sulfate, copper chloride, copper iodide, or copper nitrate must achieve the following effluent limita- tions representing the degree of efflu- ent reduction attainable by the appli- cation of the best available technology economically achievable (BAT): The limitations for copper (T), nickel (T), § 415.364 and selenium (T) are the same as speci- fied in §415.362(a). - (b) Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart and pro- ducing copper carbonate must achieve the following effluent limitations rep- resenting the degree of effluent reduc- tion attainable by the application of the best available technology economi- cally achievable (BAT): The limita- tions for copper (T), nickel (T) and se- lenium (T) are the same as specified in § 415.362(b). § 415.364 Pretreatment standards for existing sources (PSES). (a) Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart and producing copper sulfate, copper chloride, copper iodide, or copper nitrate which introduces pol- lutants into a publicly owned treat- ment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for existing sources (PSES): SUBPART AJ—COPPER SULFATE, COPPER CHLORIDE, COPPER IODIDE, COPPER NITRATE Pollutant or pollutant property PSES effluent limitations Maximum for any 1 day Average of daily values for 30 con- secutive days Copper(T) Nicketm Selenium(7) Milligrams per liter (mg/l) 3.2 6.4 1.6 1.1 2.1 0.53 In cases where POTWs find it necessary to impose mass limitations, the follow- ing equivalent mass limitations are provided as an alternate: The limita- tions for copper (T), nickel (T), and se- lenium (T) are the same as specified in § 415.362(a). (b) Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart and producing copper carbonate which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for existing sources (PSES): SOURCE: 49 FR 33421, Aug. 22, 1984, unless otherwise noted. §415.365 SUBPART AJ--COPPER CARBONATE Pollutant or pollutant property PSES effluent limitations Maximum for any 1 day Average of daily values for 30 con- secutive days Copper Nic el(T) Selenium (T) Milligrams per liter (mg/1) 3.2 6.4 1.6 1.1 2.1 0.53 In cases where POTWs find it necessary to impose mass limitations, the follow- ing equivalent mass limitations are provided as an alternate: The limita- tions for copper (T), nickel (T), and se- lenium (T) are the same as specified in § 415.362(b). § 415.365 New source performance standards (NSPS). (a) Any new source subject to this subpart and producing copper sulfate, copper chloride, copper iodide, or cop- per nitrate must achieve the following new source performance standards (NSPS): The limitations for pH, TSS, copper (T), nickel (T), and selenium (T), are the same as specified in § 415.362(a). (b) Any new source subject to this subpart and producing copper carbon- ate must achieve the following new source performance standards (NSPS): The limitations for pH, TSS, copper (T), nickel (T), and selenium (T) are the same as specified in §415.362(b). § 415.366 Pretreatment standards for new sources (PSNS). (a) Except as provided in 40 CFR 403.7, any new source subject to this subpart and producing copper sulfate, copper chloride, copper iodide, or cop- per nitrate which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources (PSNS): The limitations for copper (T), nickel (T), and selenium (T) are the same as speci- fied in §415.364(a). (b) Except as provided in 40 CFR 403.7, any new source subject to this subpart and producing copper carbon- ate which introduces pollutants into a publicly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment 40 CFR Ch. I (7-1-93 Edition) standards for new sources (PSNS): The limitations for copper (T), nickel (T), and selenium (T) are the same as speci- fied in §415.364(b). § 415.367 Effluent limitations guide- lines representing the degree of ef- fluent reduction attainable by the application of the best conventional pollutant control technology (BCT). (a) Except as provided in 40 CFR 125.30 through 125.32 any existing point source subject to this subpart and pro- ducing copper sulfate, copper chloride, copper iodide, or copper nitrate must achieve the following effluent limita- tions representing the degree of efflu- ent reduction attainable by the appli- cation of the best conventional pollut- ant control technology (BCT): The lim- itations are the same for TSS and pH as specified in §415.362(a). (b) Except as provided in 40 CFR 125.30 through 125.32 any existing point source subject to this subpart and pro- ducing copper carbonate must achieve the following effluent limitations rep- resenting the degree of effluent reduc- tion attainable by the application of the best conventional pollutant control technology (BCT): The limitations are the same for TSS and pH as specified in § 415.362(b). Subpart AK—Cuprous Oxide Pro- duction Subcategory (Re- served) Subpart AL —Ferric Chloride Production Subcategory § 415.380 Applicability; description of the ferric chloride production sub- category. The provisions of this subpart are ap- plicable to discharges and to the intro- duction of pollutants into treatment works which are publicly owned result- ing from the production of ferric chlo- ride from pickle liquor. § 415.381 Specialized definitions. (a) Except as provided below, the gen- eral definitions, abbreviations and methods of analysis set forth in 40 CFR part 401 shall apply to this subpart. (b) The term process wastewater means any water which, during manu- facturing or processing, comes into di - Environmental Protection Agency rect contact with or results from the production or use of any raw material, intermediate product, finished product, by-product, or waste product. The term "process wastewater" does not include contaminated nonprocess wastewater, as defined below. (c) The term process wastewater pollut- ants means pollutants present in proc- ess wastewater. (d) The term contaminated nonprocess wastewater shall mean any water which, during manufacturing or proc- essing, comes into incidental contact with any raw material, intermediate product, finished product, by-product or waste product by means of (1) rain- fall runoff; (2) accidental spills; (3) ac- cidental leaks caused by the failure of process equipment, which are repaired within the shortest reasonable time not to exceed 24 hours after discovery; and (4) discharges from safety showers and related personal safety equipment: Provided, that all reasonable measures have been taken (i) to prevent, reduce and control such contact to the maxi- mum extent feasible; and (ii) to miti- gate the effects of such contact once it has occurred. § 415.382 Effluent limitations guide- lines representing the degree of ef- fluent reduction attainable by the application of the best practicable control technology currently avail- able (BPT). Except as provided in 40 CFR 125.30 through 125.32, any existing point source subject to this subpart must achieve the following effluent limita- tions representing the degree of efflu- ent reduction attainable by the appli- cation of the best practicable control technology currently available (BPT): There shall be no discharge of process wastewater pollutants to navigable wa- ters. § 415.383 [Reserved] § 415.384 Pretreatment standards for existing sources (PSES). Except as provided in 40 CFR 403.7 and 403.13, any existing source subject to this subpart which introduces pol- lutants into a publicly owned treat- ment works must comply with 40 CFR part 403 and achieve the following §415.401 pretreatment standards for existing sources (PSES): SUBPART AL —FERRIC CHLORIDE Pollutant or pollutant property PSES limitations Maximum for any 1 day Average of daily values for 30 con- secutive days Total Chromium Hexavalent Chromium Copper (T) Nickel (n Zinc (T) Milligrams per liter (mg/1) 3.0 0.25 1.0 2.0 5.0 1.0 0.09 0.50 1.0 2.5 § 415.385 [Reserved] § 415.386 Pretreatment standards for new sources (PSNS). Except as provided in 40 CFR 403.7, any new source subject to this subpart which introduces pollutants into a pub- licly owned treatment works must comply with 40 CFR part 403 and achieve the following pretreatment standards for new sources (PSNS): The limitations are the same as specified in §415.382. [99 FR 33423, Aug. 22, 19841 Subpart AM —Ferrous Sulfate Pro- duction Subcategory (Re- served) Subpart AN —Fluorine Production Subcategory § 415.400 Applicability; description of the fluorine production sub- category. The provisions of this subpart are ap- plicable to discharges resulting from the production of fluorine by the liquid hydrofluoric acid electrolysis process. § 415.401 Specialized definitions. (a) Except as provided below, the gen- eral definitions, abbreviations and methods of analysis set forth in 40 CFR part 401 shall apply to this subpart. (b) The term process wastewater means any water which, during manu- facturing or processing, comes into di- rect contact with or results from the production or use of any raw material, intermediate product, finished product, by-product, or waste product. The term 010 319 ® r, TS f CBI CHEMICAL SPECIALTIES, INC. March 18, 1994 CERTIFIED MAID RETURN RECEIPT REQUESTED North Carolina Department of Environment, Health and Natural Resources Division of Environmental Management Water Quality Section Permits and Engineering Unit Archdale Building P.O. Box 27687 Raleigh, NC 27611 Subject: NPDES Permit No. NC 0006351 Chemical Specialties, Inc. (formerly Mineral Research and Development Corp.) Permit Renewal Application Gentlemen: Attached please find a copy of our NPDES permit renewal application, three (3) copies and a check for $400. The current permit expires on September 30, 1994 and the renewal 180 day period begins April 3, 1994. We have been in contact with Mr. Michael Parker, of the Mooresville Regional Office, concerning several upgrades and modifications we intend to make to our system. He, along with Raleigh personnel, have determined that these mods will not require an "Authorization to Construct" and that we can begin making the modifications once capital money is approved. The proposed modifications and upgrades were%outlined to Mr. Parker in a letter dated 3/25/94 and are duplicated below for your review. In short, the proposed system utilizes the exact same treatment technology as previously utilized. The existing solids mixing. tank, pH adjusting tanks and various system pumps will be replaced with new equipment. The' number of pH adjusting tanks will be increased to provide more residence time. More instrumentation has been provided to improve pH control and several interlocks have been incorporated. The storage lagoon's volume will be increased. A detailed listing of the specific modifications is listed below: PO Box 640.5910 Pharr Mill Road • Harrisburg, NC 28075.704-455-5181 • FAX 704-455-6507 • LAB FAX 704-455-1123 Permits and Engineering Unit March 18, 1994 Page 2 1. Remove all the existing equipment from the Waste Water Treatment Area, decontaminate and dispose of. This equipment includes the pH adjustment tanks, and the solids mixing tank. 2. This area will be cleaned and the area inspected for cracks or evidence of leakage. This inspection shall be performed by site personnel and Dames & Moore personnel who will verify the integrity for State/EPA purposes. This sump pit is designated as Solid Waste Management Unit, under our site RCRA Part A/B permit. This area will be re -lined with an appropriate concrete lining material after any required repairs are made. 3. A new sludge hopper (solids mixing tank), of similar design shall be installed, and overflow into the first treatment tank. 4. The residence time for neutralization will be improved by increasing the number of pH adjusting tanks to four. New 1,000 gallon pH adjustment tanks with agitators will be installed. Each tank will overflow into the next tank. 5. A new pump will be provided to transfer the neutralized wastes to the 2 acre unlined storage lagoon. This pump will have instrumentation to stop pumping if the pH adjustment tanks have not been able to adequately neutralize the incoming wastes. It will start back up when the pH reaches the correct level. It will have a manual override. 6. The capacity of the unlined storage lagoon will be increased by a combination of embankment raising and solids dredging. A new decanting pump will also be installed at the unlined storage lagoon. This pump will increase recirculation between the storage lagoon and the pH adjustment tanks. 7. The final effluent shall be a slip stream from the returned decanting pump. It shall be introduced to the existing settling tank. Previously I had mentioned the use of a polishing filter however, in talking further with Dames & Moore they have recommended upgrading the flocculent system and relying on the settling in the lagoon and settling tank in lieu of using cartridge filters. Thus, a new flocculent mixing and addition tank will be added. A pH probe will be installed in the existing weir box. This final effluent pH probe will shutdown discharge if the pH is below or above preset values. 8. 1, Permits and Engineering Unit March 18, 1994 Page 3 9. Increase the pumping rate from the 1/2 acre lined storage lagoon to 100 gpm from approximately 50 gpm. This lagoon is used for stormwater and spill collection. If you have any questions please feel free to contact me. Thank you for your time and consideration in this matter. Sincerely, Sylvester 7. Bartos Compliance Manager Chemical Specialties, Inc. Attachments: 1-original 3-copies Check for $400 - cc: D.W. Moon w/o attachments Mr. Rex Gleason, MRO w/o attachments E. Harmon (D&M) w/ attachments MEMO DATE• TO:PGu�,ull�J., W�At,� SUBJECT: l/J6I )-1-41-66//o74)- eZe ICE/77 -� W FP. From /6// 7 /12S/red_61-1 J7J'jf 4)/202/Z135* North Carolina Department of Environment, Health, and Natural Resources c) Printed on Recycled Paper • .rI 547-12-1994 15:13 FROM DEM WATER QUALITY SECTION TO MRO F.15:'19 Facility Name: NPDES No.: Type of Waste: Facility Status: Permit Status: Receiving Stream: Stream Classification: Subbasin: County: Regional Office: Requestor; Date of Request: Topo Quad: FACT' SHEET FOR WASTELOAD ALLOCATION Request # 8019 Mineral Research & Development Chemical Specialities NC0006351 100% Industrial Existing Renewal Rocky River C 030711 Cabarr'us MooresvillC Dana Bolde 9/29/'94 F16SE&F16SW Stream Charamnsticz USGS # Date: Drainage Area (mi2): Summer 7Q10 (cfs): Winter 7Q10 (cfs): Average Flow (cfs): 30Q2 (cfs): IWC (%): 0212418300 6/85 *10/94 136 136 8.6 21 177 34 0.45% 0.9r Wasteload Allocation Summary (approach taken, correspondence with region, EPA, etc.) 40 CFR 455.10 & .42, 415.363 & 415.367 guidelines apply to this facility and rec limits for Se, Cu, Ni, TSS, pH. Guidelines require 30 consecutive day effluent moni'to: !latch process. Toxicant anaylsis was performed and reviewed with Joe Pearce front Pretrwil limits for Zn, Cr, Ar, and NH3N will remain in permit per existing BPJ. Recommend monit for manganese due to production. The existing flows were calculated in 1985; I updated tloN using current USGS low -flow procedure (*see above). New 7Q10 was used to determine �4 limits and toxicity requirement ( new IWC = 0.96%). Faciltty is present" upgrading and no A tQ C is being requested_ They have groundwater contamination and the 2 arce storage lagoon is unlined; steps should be taken to find an alternative or to line the lagoon. Special Schedule Requirements and additional comments from Reviewers: /./4Recommended by: .. ��� /! Reviewed by Instream Assessment Regional Supervisor Permits & Engineering: Date:-24/a* l ; aLL,ctrut 3 Tate: l0] ! a%' « Cl,� Date: /Vi9� yDate: RETURN TO TECIHNICAL SUPS °- 2 TOXICS/METALS/CONVENTIONAL PARAMETERS Recommended Limit: Acute toxicity P/F at 90% Existing Limit: Acute toxicity P/F @ 45 % Fathead minnow 48 hr (TAA6C) Monitoring Schedule: Jan„Apr, Jul, Oct New limit based on updated flows, necessary to protect water qualtiy. Existing Limits Flow (MGD): TSS (lbs/day): NH3-N (mg/1): pH (SU): Arsenic (#/day): Cadmium (#/day): Chromium (#/day) Copper (#/day): Selenium (#/day): Zinc (#/day): Lead (#/day) BPJ and WQ limits calculated limits. Recommended Limits Flow (MGD): TSS (lbs/day): NH3-N (mg/1): Copper (#/day): Nickel (#/day): Selenium (#/day): pH (SU): Zinc (#/day): Chromium (#/day): Arsenic (ug/1): Cadmium (#/day): Manganese (ug/l): Oil and Grease (mg/1) Pesticides **next page Special monitoring requirements: Limited parameters most be monitored for 30 consecutive days at least once a year per 40 CFR 415.363. The month chosen should be either Jan, Apr, Jul, Oct. The rest of the 11 months POes should be monitored monthly. Toxicants which have monitoring requirements should be monitored quarterly (Jan, Apr, Jul, Oct) to conicide with the WET test. Monthly 0.025 2 2 6-9 0.208 0.092 0.104 0.06 0.208 0.313 monitor were given as Avg. Daily Max. EL or WQ 0.025 3 BPJ 3 BPJ 6-9 BPJ 0.416 BPJ 0.184 WQ 0.200 BPJ 0.12 BPJ 0.416 BPJ 0.626 BPJ monitor monthly average and daily max is 2X the corresponding concentrations Monthly Avg Daily Max. Monthly Avg. 0.025 --c7.a8 2 ** 0.099 0.198 0.050 BAT 6-9 0.313 0.104 0.208 monitor monitor monitor include guideline language/ definition ** Daily Max. 0.025 -2-:-28- L•8-5 BAT 3 ** BPJ 0.30 BAT 0.60 BAT 0.108 WQ BAT/WQ 0.240 mg/1 0.521 mg/1 6-9 BAT 0.626 ** BPJ 0.200 BPJ 0.416 BPJ monitor Qrtly monitor Qrtly Limit changes due to Effluent guidelines and toxicant anaylsis. Oil and Grease due to maintenance area wasteflow source. X_ No parameters are water quality limited, but this discharge may affect future allocations. 3 **See staff report for further detail. Region, P&E and facility met (2/8/94) about interim limits for NH3N and Zinc while facility is upgrading 1. Begin construction of proposed wastewater treatment plant modifications (necessary to achieve. compliance with final effluent limitations) on or before May 15,1994 (Facility met this requirement). 2. Complete construction of proposed wastewater treatment plant modifications (necessary to achieve compliance withfinal effluent limitations) on or before August 1, 1995 3. Achieve compliance with final effluent limitations on or before October 1, 1995. Interim Limts should apply until September 30, 1995. NH3N (#/day): Zinc (#/day): Monthly Avg. Daily Max. 4.0 5.0 0.70 1.40 4 INSTREAM MONITORING REQUIREMENTS Upstream Location: N/A Downstream Location: N/A Parameters: N/A Special instream monitoring locations or monitoring frequencies: MISCELLANEOUS INFORMATION & SPECIAL CONDITIONS Adequacy of Existing Treatment Has the facility demonstrated the ability to meet the proposed new limits with existing treatment facilities? Yes No If no, which parameters cannot be met? Would a "phasing in" of the new limits be appropriate? Yes No If yes, please provide a schedule (and basis for that schedule) with the regional office recommendations: If no, why not? Special Instructions or Conditions Wasteload sent to EPA? (Major) _N (Y or N) (If yes, then attach updated evaluation of facility, including to)tics analysis, modeling analysis if modeled at renewal, and description of how it fits into basinwide plan) Additional Information attached? N (Y or N) If yes, explain with attachments. Facility Name G emi(4/ ,S Pria4r Permit # NC0O) 635) Pipe # /Hera ! Oe &wit N Ve/op nefr/ ACUTE TOXICITY PERMIT LIMIT (QRTRLY) The permittee shall conduct acute toxicity tests on a quarterly basis using protocols defined as definitive in E.P.A. Document 600/4-85/013 entitled "The Acute Toxicity of Effluents to Freshwater and Marine Organisms." The monitoring shall be performed as a Fathead Minnow (Pimephales promelas) 48 hour static test, using effluent collected as a 24 hour composite. The LC50 of this effluent using the previously stated methodology may at no time in any toxicity test be less than $ %. Effluent samples for self -monitoring purposes must be obtained during representative effluent discharge below all waste treatment. The first test will be performed cft'ter thirty days from the effective date of this permit during the months of ,TAN , ,q»), J UL, of,r The parameter code for this test is TAA6C. All toxicity testing results required as part of this permit condition will be entered on the Effluent Discharge Monitoring Form (MR-1) for the month in which it was performed, using the appropriate parameter code. Additionally, DEM Form AT-1 (original) is to be sent to the following address: Attention: Environmental Sciences Branch North Carolina Division of Environmental Management 4401 Reedy Creek Road Raleigh, N.C. 27607 Test data shall be complete and accurate and include all supporting chemical/physical measurements performed in association with the toxicity tests, as well as all dose/response data. Total residual chlorine of the effluent toxicity sample must be measured and reported if chlorine is employed for disinfection of the waste stream. Should any single quarterly monitoring indicate a failure to meet specified limits, then monthly monitoring will begin immediately until such time that a single test is passed. Upon passing, this monthly test requirement will revert to quarterly in the months specified above. Should any test data from either these monitoring requirements or tests performed by the North Carolina Division of Environmental Management indicate potential impacts to the receiving stream, this permit may be re -opened and modified to include alternate monitoring requirements or limits. NOTE: Failure to achieve test conditions as specified in the cited document, such as minimum control organism survival and appropriate environmental controls, shall constitute an invalid test and will require immediate retesting(within 30 days of initial monitoring event). Failure to submit suitable test results will constitute noncompliance with monitoring requirements. 7Q10 4, 0 cfs Permitted Flow d . 025 MGD 1WC D. n. % Basin & Sub -basin ,VA' D 0 307/ Receiving Stream ,Po rty M UP r County L4 h a r✓u5 J QAL Fathead 48 Version 10/91 Recommended by: Date ( ( sr,„ 41/are.( /4,..ceavt4 A,ve��,, 10070 (yw O. Oz6.1760 h/� J / i /9Uq tM OM if t/ese _ o 2/_244/J30d 410 001 c cligiff4/(Llf point._. sairct,__(.449.Q7 nc e . 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Zz/o a 2 flak/ b O14A�}-i1-.. ,,i&v = Q._0..?7 al. 0, 0/44 Q 2- TS.S vlob,kok,f »''aX /Z 2• a 2 Ch"-onlvii, Yid IYr Y= O. z' 4 v O..OS/ ti u faith( Floz&-4 �v WelkiLd CLutk *Dr) 13( - 7f10= 6_5q V / 0 10 13,0 .- Q = l `f7 leit_ t.)14fr., . _ tr. zr 2g351-00 019 = 2 : r. 4 eta (?fit -allo gin w 102 , ("<e., &Hy: "frafx., cam^ 2X. 4 csv = 3S,_4 7/93 35'7._ /4;fietj citt, &Lai E. , �.. -ace) xr% 7(5,3 A - 7Y/ 7 t, -rf - . iil 14t , S$ 7 tia# u G 40// - 8"4f co 7 6P3" altz,z4-4 14,1, 20-7 ( der co- ,6.414: r BPr 61-1, sP5 1N %J C;t tvJ-.?.e) A t, un c ek % b w {vr✓e r, r7 yy �,� u.I I SS (i» 4 c_a go„,„, J TOXICANT ANALYSIS A Facility Name Chemical Specialities NPDES # NC0006351 Ow (MGD) 7Q10s (cfs) .,_.._.._.._.._.._.._. 8.6 !WC (%) Rec ving Stream Yadkin River Stream Class C FINAL RESULTS Cadmium Max. Pred Cw 214.14 Allowable Cw 445.9 Chromium Max. Pred Cw 558.6 Allowable Cw 11146.8 Copper Max. Pred Cw 367.22 Allowable Cw 1560.5 Zinc Max. Pred Cw 266425.5 Allowable Cw 11146.8 Arsenic Max. Pred Cw 4845 Allowable Cw 11146.8 Selenium Max. Pred Cw 229.08 Allowable Cw 1114.7 Lead Max. Pred Cw 187.88 Allowable Cw 5573.4 Nickel Max. Pred Cw 0 Allowable Cw 19618.3 /004- eztr 6. 0 73 4%17 2,32 4`/d1, 6 3 25 lq'4'`3 2 32' a cI1 2.32 * 0,23Z (1"' 9z5- 10/10/94 PAGE • TOXICANT ANALYSIS uutAt Facility Name Chemical Specialities NC0006351 NPDES # Qw (MGD) 7Q10s (cfs) n IWC (%) Rec'ving Stream Yadkin River Stream Class C FINAL RESULTS Cadmium Max. Pred Cw 214.14 Allowable Cw 208.5 Chromium Max. Pred Cw 558.6 Allowable Cw 5211.3 Copper Max. Pred Cw 367.22 Allowable Cw 729.6 Zinc Max. Pred Cw 266425.5 Allowable Cw 5211.3 Arsenic Max. Pred Cw 4845 Allowable Cw 5211.3 Selenium Max. Pred Cw 229.08 Allowable Cw 521.1 Lead Max. Pred Cw 187.88 Allowable Cw 2605.6 0 Max. Pred Cw 0 Allowable Cw 0.0 0 Max. Pred Cw 0 L L M gw Gdwir44/94 (),6431q 1,04#/11 1, ogp tr/oli og' *16'7 o to 4/✓i. 0,543#/4 afir 10/10/94 PAGE' cdtto Jaeles/ Gies- 4-1 I1,at) - Sa 1; t f "t1 -ia Q xi 6 o TOXICANT ANALYSIS Ii ICJ Parameter = Cadmium Parameter = Chromium Standard = 2 µg/1 Standard = 50 Aily,,PoWi o l.e #/day MGD adv./ n BDL=1Y2DL Actual Data FLOW RESULTS n BDL=1/2DL 1 5 0.00092 0.022 Std Dev. 8.425721631 1 8.6 2 5 0.0005 0.012 Mean 4.194166667 2 13.4 3 5 <0.0005 0.011 C.V. 2.008914357 3 4.3 4 5.3 <0.0006 0.013 4 52.8 5 49.8 <0.0444 0.107 5 213 6 10 <0.0019 0.023 Mult Factor = 4.3 6 202 7 10 <0.002 0.024 Max. Value 49.8 µg/I 7 224 8 5.3 <0.0008 0.018 Max. Pred Cw 214.14 µg/I 8 70 9 9.6 <0.0012 0.015 Allowable Cw 208.5 µg/I 9 155 10 4.8 <0.0006 0.015 10 67 11 4.7 <0.0007 0.018 11 50 12 0.92 <0.0001 0.013 12 46 13 0.98 <0.00009 0.011 13 54 14 0.98 <0.00009 0.011 14 95 15 0.98 <0.00009 0.011 15 65 16 1 <0.00006 0.007 16 71 17 0.66 <0.0001 0.018 17 189 18 0.85 <0.0001 0.014 18 116 19 1.26 <0.0002 0.019 19 56.6 20 0.75 <0.0001 0.016 20 146 21 1.16 <0.0003 0.031 21 26 22 1.33 <0.0002 0.018 22 142 23 12 <0.0004 0.004 23 47 24 1.1 <0.0002 0.022 24 104 25 0.96 <0.0002 0.025 25 149 26 0.96 <0.0002 0.025 26 75 27 0.96 <0.0002 0.025 27 165 28 1 <0.0002 0.024 28 294 29 1 <0.0004 0.048 29 145 30 1 <0.0004 0.047 30 94.5 31 1 <0.0002 0.024 31 84 32 1 <0.0002 0.024 32 65 33 1.2 <0.0002 0.02 33 148 34 1.2 <0.0002 0.02 34 85 35 1.1 <0.0002 0.022 35 36 1.14 <0.0002 0.021 36 37 37 38 38 39 39 /1 10/10/94 PAGE' TOXICANT ANALYSIS L arameter = Standard = Copper 7 µg/I Actual Data RESULTS 8.6 13.4 Std Dev. Mean 68.13 103.6 4.3 C.V. 0.658 52.8 213 202 224 70 155 67 50 Mult Factor = 1.9• Max. Value 294 Max. Pred Cw 558.6 Allowable Cw 05211 46 54 95 65 71 189 116 56.6 146 26 142 47 104 149 75 165 294 145 94.5 84 65 148 85 n 1 2 3 4 5 BDL=1/2DL 8.6 4.8 4.3 5.3 85.4 Actual D 8.6 4.8 4.3 5.3 85.4 RESULTS Std Dev. Mean C.V. 13.83 6.766 2.044 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 9.1 9.6 7.2 5.8 5.8 7.2 10.1 0.43 4.3 1.9 4.8 6.2 0.96 0.96 4.3 6.2 0.96 0.46 4.3 2.9 12 2.9 2.9 1.9 1.9 9.6 1.9 0.96 0.96 4.3 2.4 9.1 9.6 7.2 5.8 5.8 7.2 10.1 0.43 4.3 1.9 4.8 6.2 0.96 0.96 4.3 6.2 0.96 0.46 4.3 2.9 12 2.9 2.9 1.9 1.9 9.6 1.9 0.96 0.96 4.3 2.4 Mult Factor = 4.3 Max. Value 85.4 Max. Pred Cw 367.2 Allowable Cw 0730 µg/I µg/I 38 39 10/10/94 PAGE TOXICANT ANALYSIS n BDL=1/2DL 1 2196 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 1400 680 473 49.8 17516 17186 3838 1098 649 148 664 2332 1127 303 221 57.3 57.4 48.6 1829 594 409 48441 1237 141 510 299 109 748 722 245 2465 2285 2871 Actual Data 0.403 0.14 0.0623 0.0513 0.0444 3.36 3.44 0.5761 0.1374 0.0975 0.016 0.0609 0.2139 0.1034 0.0278 0.0129 0.0086 0.0067 0.0077 0.2441 0.1536 0.0614 1.616 0.2269 0.0293 0.1064 0.0623 0.0218 0.2995 0.2831 0.049 0.4934 0.4002 0.5029 RESULTS Std Dev. Mean C.V. Mu/t Factor = Max. Value Max. Pred Cw Allowable Cw 2.6879 5.5 48441 µg/I 266426 µg/I 5211.3 µg/I • n 1 2 3 4 5 6 7 8 9 10 11 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 39 BDL=1/2DL 8.6 6.7 4.3 5.3 213 9.1 96 7.2 5.75 5.76 7.2 0.48 0.43 15.3 15.8 1.4 2.9 2.9 5.3 2.4 1.4 0.33 1.9 6.7 8.6 1.9 0.96 7.7 13 0.96 0.96 750 61 3.4 3.4 µg/I 1 1 1 Actual Datal 0.0018 0.0014 0.0009 0.0011 0.0444 0.0019 0.002 0.0015 0.0012 0.0012 0.0015 0.0001 0.00009 0.0032 0.0033 0.0003 0.0006 0.0006 0.0011 0.0005 0.0003 0.00007 0.0004 0.0014 0.0018 0.0004 0.0002 0.0016 0.0027 0.0002 0.0002 0.1564 0.0127 0.0007 0.0007 10/10/94 PAGE TOXICANT ANALYSIS Parameter Selenium rsutir(, RESULTS Std Dev. Mean C.V. 130.099 36.5151 3.56288 Mult Factor = Max. Value Max. Pred Cw Allowable Cw 6.46. 750 µg/I 4845 µg/I 5211.3 µg/I Standard = n 1 2 3 4 5 6 7 8 9 10 11 5 at B /2DL 5 5 5.5 5.5 49.8 4.7 5 5.3 5.3 5.3 4.7 µg/1 Actual b to 0.00092 0.0005 0.0005 0.0006 0.0444 0.0009 0.001 0.0008 0.0006 0.0006 0.0007 RESULTS Std Dev. Mean C.V. Mult Factor = Max. Value Max. Pred Cw Allowable Cw 7.99782 3.63105 2.20262 4.6 49.8 µg/I 229.08 µg/INg 521.1 µg/IiiN 12 13 14 15 16 17 18 19 20 21 22 23 24 25 26 27 28 29 30 31 32 33 34 35 36 37 38 39 0.92 2.2 0.98 0.98 1 0.24 0.96 0.96 0.96 0.96 0.96 1.2 1.92 0.96 0.96 0.96 0.96 0.96 0.96 0.96 0.96 1.2 1.2 1 1 9.6 0.96 0.0001 0.0002 0.00009 0.00009 0.00006 0.0001 0.0001 0.0002 0.0001 0.0003 0.0002 0.00004 0.0002 0.0002 0.0002 0.0002 0.0002 0.0004 0.0004 0.0002 0.0002 0.0002 0.0002 0.0002 0.0002 0.002 0.0002 10/10/94 PAGE TOXICANT ANALYSIS arameter = Lead Standard = 25 µg/I n BDL=1/2DL Actual Data RESULTS 1 8.6 0.0018 Std Dev. 7.29553 2 4.8 0.001 Mean 3.53171 3 4.3 0.0009 C.V. 2.06572 4 5.3 0.0011 - -- --5:." r._.._42.7 0.0089 6 9.1 0.0019 Mult Factor = 4.4 - 7 7.2 0.0015 Max. Value 42.7 µg/I 8 5.76 0.0012 Max. Pred Cw 187.88 µg/I 9 5.76 0.0012 Allowable Cw 2605.6 µg/I 10 7.2 0.0015 11 0.48 0.0001 12 0.43 0.00009 13 0.43 0.00009 14 0.43 0.00009 15 0.29 0.00006 16 0.48 0.0001 17 0.48 0.0001 18 0.96 0.0002 19 1.92 0.0004 20 1.44 0.0003 21 0.96 0.0002 22 0.19 0.00004 23 0.96. 0.0002 24 0.96 0.0002 25 0.96 0.0002 26 0.96 0.0002 27 0.96 0.0002 28 1.92 0.0004 29 1.92 0.0004 30 0.96 0.0002 31 0.96 0.0002 32 0.96 0.0002 33 0.96 0.0002 34 0.96 0.0002 35 0.96 0.0002 36 37 38 39 10/10/94 PAGE'. Page 1 i Note for Michelle Wilson From: Joe Pearce Date: Thu, Oct 6, 1994 12:33 PM Subject: Chemical Specialties. To: Michelle Wilson cc: Carla Sanderson I have the following comments concerning Chem Spec. I would recommend limits for any of the typical toxicants they use in their production process. The limits would either be the previously used limits or the water quality based limits which ever is most stringent. The Copper salts (copper nitrate) category requires 30 consecutive day sampling. Would you want to consider 30 cons days for all POCs during each quarter? These are batch processes where they can control their discharge. Several pesticides which cannot be discharged are produced. Cabarrus county said it would be several months before they developed their speculative limits. They did ask for a copy of our draft limits as soon as they are available. Chemical Specilaities Rocky River Residual Chlorine 7Q10 (CFS) DESIGN FLOW (MGD) DESIGN FLOW (CFS) STREAM STD (UG/L) UPS BACKGROUND LEVEL (UG/L) IWC (%) Allowable Concentration (ug/I) Fecal Limit Ratio of 221.9 :1 tuJf{Ovos 2aiia o4 f63.2; NC0006351 Ammonia as NH3 (summer) 8.6 4,0 7Q10 (CFS) 0.025 DESIGN FLOW (MGD) 0.03875 DESIGN FLOW (CFS) 17.0 STREAM STD (MG/L) 0 UPS BACKGROUND LEVEL (MG/L) 0.45% IWC(%) 3790 )in. Allowable Concentration (mg/I) Ammonia as NH3 (winter) 7Q10 (CFS) 200/100m1 DESIGN FLOW (MGD) DESIGN FLOW (CFS) STREAM STD (MG/L) UPS BACKGROUND LEVEL (MG/L) IWC (%) Allowable Concentration (mg/I) 8.6 0.025 0.03875 1.0 0.22 0.45 % 174 21 0.025 0.03875 1.8 0.22 0.2 % 858 4,0 82 12,3 520 USGS weighted low flow estimate procedure ro/D6/74 FacilitylChemical Specialities Region DA_LFPR s7Q10_LFPR DA_new MAR QA_eq HA9 277 NPDES # LNC0006351 I sq mile 14 cfs 136 1.08 146.88 sq mile cfs/sq mile cfs STEP 1 calculate drainage area ratio Stream' RockyRiver J NOTE: procedure applies for regions HA3, HA5, HA9, and HA10, else see flow SOP MFIL RATIO = new drainage area = drainage area at gage IF 0.25 < RATIO < 4, CONTINUE to STEP 2, ELSE too far from gage OK, do STEP 2 now! STEP 2 determine weight of gage (weight_LFPR) A. RATIO < 1 B. RATIO > 1 weight ratio weight ratio 0 1 0 1 0.32 f 0.49 I #VALUE! 1 see A 1 0.25 1 4 STEP 3 HA3 HA5 HA9 HA10 STEP 4 weight = 0.32 calculate 7010_EQ using regional equation 34.14 2.65 2.65 23.93 cfs cfs cfs cfs 7010_EQ = calculate 7Q10 yield using weighted equation 2.65 7Q10yield = [weight_LFPR * 7Q10_LFPR] + [weight_EQ * 7Q10_EQ] cfs DA_LFPR DA_new yield = 0.02 + 0.01 STEP 5 calculate s7Q10 7010 = 7Q10yield * DA_new summer 7010 = 4.01 cfs 10.490974731 0.03 cfs/sq mile USGS weighted low flow estimate procedure 1 FacilitylChemicalSpecialities NPDES # LNC0006351 I Stream'Rockt River Region DA_LFPR w7Q10_LFPR DA_new MAR QA_eq .._.._..HA9._.._... 277 sq mile 24 cfs 136 146.88 sq mile cfs/sq mile cfs STEP 1 calculate drainage area ratio NOTE: procedure applies for regions HA3, HA5, HA9, and HA10, else see flow SOP RATIO = new drainage area drainage area at gage IF 0.25 < RATIO < 4, CONTINUE to STEP 2, ELSE too far from gage OK, doSTEP2now! STEP 2 determine weight of gage (weight_LFPR) A. RATIO < 1 weight ratio r 0 _..-0.32 1 STEP 3 HA3 HA5 HA9 HAI 0 STEP 4 1 1 0.49 0.25 weight = B. RATIO > 1 weight r lig 0• 1 r.. #VALUE! 1 see A 1 4 0.32 calculate 7Q10_EQ using regional equation 65.65 13.09 13.09 35.21 cfs cfs cfs cfs 7Q10 EQ 13.09 cfs/sq mile calculate 7Q10 yield using weighted equation 7Q10yield = [weight_LFPR * 7Q10_LFPR] + [weight_EQ * 7Q10_EQ] DA_LFPR DA_new yield = 0.03 + 0.07 STEP 5 calculate w7Q10 7Q10 = 7Q10yield * DA_new winter 7Q10 = 12.67 cfs I.0.49097473. 0.09 cfs/mile USGS weighted low flow estimate procedure FacilityChemical Specialities NPDES # fNC0006351 Region DA_LFPR 30Q2_LFPR DA_new MAR QA_eq HA9 277 sq mile 34 cfs 136 1.08 146.88 sq mile cfs/sq mile cfs STEP 1 calculate drainage area ratio Stream': Rockt River NOTE: procedure applies for regions HA3, HA5, HA9, and HA10, else see flow SOP RATIO = new drainage area drainage area at gage IF 025 < RATIO < 4, CONTINUE to STEP 2, ELSE too far from gage OK, do STEP 2 now! STEP 2 determine weight of gage (weight_LFPR) A. RATIO < 1 weight ratio 0 1 F 0.32_ I 0.49 1 0.25 weight = I 0.32 B. RATIO > 1 weight Lag 0 1 #VALUE! see A 1 4 STEP 3 calculate 30Q2_EQ using regional equation HA3 HA5 HA9 HA10 74.29 18.64 18.64 50.53 cfs cfs cfs cfs 30Q2_EQ = STEP 4 calculate 30Q2 yield using weighted equation 18.64 cfs/sq mile 30Q2yield = [weight_LFPR * 30Q2_LFPR] + [weight_EQ * 30Q2_EQ] DA_LFPR DA_new yield = 0.04 + 0.09 STEP 5 calculate 30Q2 30Q2 = 30Q2yield * DA_new 30Q2 = 18.02 cfs L Q9.0974731 0.13 cfs/sq mile WHOLE EFFLUENT TOXICITY TESTING 0{SELF-MONITORING SUMMARY] Mull, Sep 19. 1994 FACILITY 5.FQIIIRFMFN'r YI/AI2 JAN FEB MAR APR MAY Jl1N JUL Al Ill SF.P OCT MIDDLESEX WWTP PERM C11R LIM:90% 90 27.8' 40.7' <I' Nil MI 5.0' 1.4' NONE' 4.8' NONE' NC002I563/001 Bcgin:4/1/94 Frequency: Q P/F A 1E13 MAY AUG NOV NonComp:SINGLE o1 •-- 324' --- Ni 13.87' 7.86' --- County:NASII Region: RRO Subbasin: N1,1107 92 --- Nl --- _. >100' PASS FAIL FAIL FAIL PF:0.08 Special SOC: 4126/94-4/1/97 CI IR NI' Q MONrr 90% A(1E13 MAY 93 -- PASS FAIL FAIT. PASS NR/FAIL FAIL. FAIL 7010: 0.0 TWC(%):100.0 Ocdcr: AUG NOV) 94 --- FAIL FAIL FAIL FAIL LATE FAIL MII..liiI3 URI:WING CO. PERM ('III( LIM. 2.'10. - 00 ,-- NC00299801001 Begin:6/1/93 Frequency: Q P/F A AUG NOV 1.5B MAY NonComp: --- County:ROCKINGHAM Region: WSRO Subbasin: ROA03 PF:5.2 Special 93 -- -- - - -- PASS 7.10: 313 IWC(%):2.51 Order: 94 -- PASS PASS PASS NONE' NONE' NII --- S; Ni PASS 1' NFVFAIL PASS /MINERAL RESEARCH &15EVELOPMENT PERM: 4811R LC50 AC LIM 45% FrITD - Y 90 >1001 --- 84.51 - N3 >1001 >100f NC0006351/001 Begin:9/1/91 Eminency: Q A JAN APR JUL OCT NonComp: 91 >1001 >1001 599 63.2f 581 County:CABARRUS Region: MRO Subbasin: YAD11 92 >1001 - >1001 1001 >100f S ecial 93 >1001 •-- - NR/>1001 35.7f,lATE >100f 72.0f PE': 0.025 P 7Q10:8.6 IWC(%):0.45 Order 94 >1001 38.41 66.21 H MOCKS'rILLE WWTP BEAR CREEK PERM CHR LIM:32%, 37% @ EXPANSION (NEW PERM 9/1 Y 90 PASS PA PASS NC0050903/001 Begin:7/1/92 Frequency: Q P/F A AUG NOV FEB MAY NonComp:SINGLE 91 --- PASS -- PASS --- PASS County:DAVIE Region: WSRO Subbasin: YAD06 92 -- PASS --- -- PASS PASS PF: 0.192 Special 93 - DA PASS -- 1'R PASS PASS 7Q10:0.c3 1\VC(%):32.00 Omer: 94 PASS --- PASS PASS MOCKSVILLE WWTP DUTCHMAN'S CRK PERM C13R L.IM:6.6% Y 90 PASS - PASS --- LATE PASS Nil PASS NCOC21491/001 Begin:3/1/88 Frequency: Q P/F APR JUL. OCT JAN NonComp: 91 PASS -- --- PASS -- -- PASS -- PASS County:DAVIE Region: WSRO Subbasin:YAD05 92 PASS --- --- PASS --- - PASS PASS 93 PASS - NT --- --- PASS - - --- PASS PP:0.63 Special -- - 7Q1U: 15.0 IWC(%):6.57 Order: 94 PASS --- PASS -- - PASS }' 90 --- --- PASSI -- PASSI -. PASSI FAILI 91 --- - FAILI - -- - PASSI --- --- PASSI --- -- PASSI -- - I'A551 PASSI -.- PASSI --- --- FAILI.FAIII -- __ --� --- PASSf -- -- PASSI --- -- PASSI --- FAILI PASS PASS PASS PASS 7 MONARCII HOSIERY PERM. 241112 AC' I'/1: LIM '>d',5' (F1'3ID) M.:000I210/001 Begin:10/1/93 P mitts cy: Q A MAR 11IN SEP I)G(' NnnGnnpSINGI.I. County:ALAMANCE Region: WSRO Subbasin: Cl'1,02 PF: 0.05 Special 7Q10: 47.8 IWC(%):0.16 Order: MONROE WWTP PERM CI112 1.IM:96%, 97% (d, 9.0, 98% es > 9.0 90 Nfl FAIL bt FAIL --- FAIL FAIL FAIL PASS --- -- LATE NC0024333/001 Begin:7/I/89 Frequency: Q P/F A MAR JIIN Sill' D1i(' NonComp: 91 FAIL PASS -- PASS P,PASS P,PASS PASS PASS PASS PASS PAS 3 PASS County:UNION Region: MRO Subbasin: YADI4 92 PASS PASS LATE/PASS PASS PASS PASS PASS PASS PASS - FAIL PF: 7.00 Special SOC:1/18/91-4/30/94 Q LIM @ 97% 93 PASS -- PASS --- -- FAIL PASS PASS PASS 7Q10: 0.43 I\VC(%):96.18 Order: - 94 --- --- PASS PASS - MONSAN'I'O/001,002 PERM: 241112 AC NI' LIM 909(PIPP_S 00I& 002) Y 90 NONE --• N,NONEI --- >90 --- --- >100,bt NC0003719/002 Bcgin:4/1/94 Fnequency: Q A 1.13B MAY AUG NOV NonComp:SINGLE 91 NONE --- --- N,>100I --- - N,>1001 NONE --- --- County-:CUMBERLAND Region: FRO Subbasin: CPFI5 92 N,NONEI -- -- >90' -- - >100',>1001 ---71.0' 1'F:0,73 Special - - 93 >1001,>100' >100' >100',>1001 -->100' - 7Q10: 791.0 IWC(%):0.14 Order: 94 >100',>1001 --- - -- PASSI PASSI MOORE COUNTY WWTP PERM CIiR L1M:41% Y 90 N'3 PASS PASS FAIL FAIL PASS PASS PASS PASS PASS PASS PASS NC0037508/001 Begin: 12/1/92 Frequency: Q P/F A TUN SEP DEC MAR NonComp:SINGLE 91 PASSREV PASS PASS PASS PASS PASS PASS PASS PASS PASS PASS PASS PASS County:MOORE Region: FRO Subbasin: LUMSO 92 PASS PASS PASS PASS PASS PASS PASS - PASS Special 93 --- - PASS PASS PASS PASS PASS 7Q10: 15.2 I\VC(%):40.54 Order. 94 PASS FAIL,PASS -- - PASS MOORESVILLE WWTP PERM CIIR LIM:94% Y 90 -- PASS - - PASS --- FAIL PASS - PASS NC0046728/001 Begin:7/1/90 Frequency: Q P/F A FEB MAY AUG NOV NonComp: 91 -- FAIL PASS --- FAILSIG PASSSIG - PASS - PASS County:IREDELL Region:MRO Subbasin: YADI I 92 --- -- FAIL PASS PASS,FAIL PASS - PASS Special 93 ... Pfi -- PASS PASS PASS 0 7Q 7QI0: 0.0.5 IWC(%):94.15 Order: 94 --- FAIL PASS -•- FAIL PASS --- 0 2 consecutive failures = significant noncompliance Y Pre 1990 Data Available 94 Btl,Btt FART FAILI,FAILI PASSI --- PASSI LEGEND: PERM = Permit Requirement LE1' = Administrative Letter - Target Frequency = Monitoring frequency: Q- Quarterly; M- Monody: BM- Bimonthly; SA- Semiannually; A- Annually; OWD- Only when discharging: D- Discontinued monitoring requirement; IS- Conducting independent stud; Begin = First month reouircd 7Q10 = Receiving stream low flow criterion (efs) A = quarterly monitoring increases to monthly upon single failure Months that testing must occur - ex. JAN,APR,JULOC F • NonComp = Current Compliance Requirement PF = Permitted flow (MGD) IWC% = lnstrnam waste concentration 3 /1 I >s/Foil chronic text AC: = Acme CI II2 =Chronic Data Notation: f - Fathead Minnow: • - Ceriodanlmia so.: my - Mvsid shrimp: CAN - Chronic value, I' - Mortality of stated percentage at I,iclast concentration: at - Performed by DI Tnx lived (rout,. bt - Bad test Reporting Notation: --- = Data not required; NR - Not rcponed; ( ) - Beginning of Quarter Facility Activity Status: 1 - Inactive, N • Newly lssued(Io construct); 11 - Active but not discharging; 7-More data available for month in question SIG = ORC signature needed 3.1 Page 1 Note for Marcia Toler-McCullen From: Joe Pearce Date: Thu, Sep 15, 1994 10:20 AM Subject: RE: NC0006351 To: Marcia Toler-McCullen cc: Dana Bolden Chemical Specialties/Mineral Research is proposing to tie on to Cabarrus County Sewer. Cab. Co. is reviewing to see if they will accept. From: Marcia Toler-McCullen on Thu, Sep 15, 1994 9:39 AM Subject: RE: NC0006351 To: Dana Bolden; Joe Pearce Can either of you help me with the active/inactive status with this facility? Thanks, I would really appreciate it. From: Susan Wilson on Thu, Sep 15, 1994 9:37 AM Subject: RE: NC0006351 To: Marcia Toler-McCullen i have a chemical specialties under that number (could have changed names) that came in march and has not been issued. bolden is handling so you may want to talk to him. or joe i think knows what is going on with them. From: Marcia Toler-McCullen on Thu, Sep 15, 1994 9:29 AM Subject: NC0006351 To: Susan Wilson Can you help me on figuring out this facility? Chemical Specialties, Inc Formerly: Mineral Research and Development Corporation NC0006351 Rocky River Cabarrus County 03-07-11 I have a return letter dated April 29, 1994 stating an NPDES Permit Application Return. Therefore, I closed out our files. Then in July 14, 1994, I received a new staff report. I am thoroughly confused. Is this facility active or inactive? Is there anyway you can check and assist me in this mess? If you can, I will be eternally grateful. I have not forgotten your staff reports either! ! ! Thanks.