NCG550941_Response to Notice_20221031

NC Dept of Environmental Quality
Patricia McKenna, Owner
3610 Gooch Road Raleigh Regional Office
Durham, NC 27704-3927
919-682-0325 (Home)
919-280-2071 (Mobile)
[e-mail] (Patricia's Email)
[e-mail] (Frank McKenna — Husband)
Jane Bernard
Raleigh RO Surface Water Protection
NC Division of Environmental Quality
1628 MSC
Raleigh, NC 27699-1628
RE: McKenna Property, 3610 Gooch Road, Durham, NC 277704
NPDES General Permit NCG550941
Dear Ms. Bernard,
OCT 31 2022
I collected the water sample from the septic system at the above address on October 4,
2022. Jim Frei could not do the test till after November so he told me I could collect the
water sample from the septic system. I hand delivered the water sample to Pace
Analytical on Oct 4, 2022. I finally heard from them yesterday, October 26, 2022 even
though the report date was Oct 11, 2022 they never sent me the final report even though
they had my mailing address and my email address. I called them on Oct. 26, 2022 to
find out what the delay in getting the report because I did not know how long it would
take to receive the report from Pace Analytical Labs and he immediately emailed it to me
at my husband's email address.
I did not understand the report created by Jonathan Biddix of Carolina Labs and Pace
Labs so asked Jonathan to give me the results in layman's terms. He said the sample
tested at 31.00 mg/L. I am hoping that since the limits are for 45.0 mg/L that the sample
passed the test. Please advise if I am incorrect. I am enclosing a complete copy of
Jonathan's Biddix's test results.
I want to thank you for helping me during my initial phone call to find out what I should
do when the test Jim Frei took did not pass the test. Please let me know if there is
anything more I need to do.
Thank you again for all the assistance and advice you provided me to get the testing
completed.
Sincerely,
Ali z�
Patricia McKenna. Owner

From: Jonathan Biddix
Sent: Wednesday, October 26, 2022 11:29 AM
To: [e-mail]
Subject: Final Results
Importance: High
NC Dept of Environmental Quality
OCT 3 1 2022
Raleigh Regional Office
Good morning,
I have attached your final report. Please let me know if you have any questions.
Thanks,
Jonathan Biddix
Project Manager 1 Carolina Labs
9800 Kincey Ave, Suite 100, Hvntersville NC 28078
Direct: 704.977.0978 { :celabs. c'm
NEW: PROCESS PAYMENTS ONLINE — click on the link below
Online Bin I'u\
//Pace
NOTICE-- The contents of this email and any attachments may contain confidential, privileged, and/or
legally protected information and are for the sole use of the addressee(s). Any review or distribution by
others is strictly prohibited. If you are not the intended recipient, please contact the sender immediately
and delete any copies.
Please . t.hMiH,vircinment. before printing this email

From: Jonathan Biddix
Sent: Wednesday, October 26, 2022 12:13 PM
To: Frank McKenna
Subject: RE: Final Results
Good afternoon,
NC Dept of Environmental Quality
OCT 31 2022
Raleigh Regional Office
Your results are 31.00 Milligrams per liter verses a reporting limit of 2 milligrams per Liter.
I unfortunately I cannot say whether this will pass or fail that is up to the body you are reporting the
results to. Please let me know if you need anything else.
Thanks,
From: Frank McKenna <[e-mail]>
Sent: Wednesday, October 26, 2022 11:57 AM
To: Jonathan Biddix <Jonathan.Biddixt7a pacelabs.com>
Subject: RE: Final Results
CAUTION: This email originated from outside Pace Analytical. Do not click links or open attachments
unless you recognize the sender and know the content is safe.
I am so sorry but I cannot tell from the report —The first test done by Jim Frei did not pass because we
had just had the system cleaned out so it did not pass. The report does not look like Jim's report so I
really cannot tell if it passed or if it failed the test. When he reported it was 64.0 with a limit of
45.0. Since I am the one who took the sample I don't know if I took the sample incorrectly or if it passed
the test with an amount of less than 45.0. I need to make a report to NC Division of Environmental
Quality and I cannot read the report well enough to give them a report. I apologize because I am
probably not reading the report correctly so could you please explain in layman's terms. Did we pass
the test or was it another failure. I hope I am making sense in this explanation. Thank you for any
assistance you may give with this.
Patricia McKenna you may text my Cell 919-280-2071
Or email at above address
Again thank you for your assistance.
Sent from Mail for Windows
From: Jonathan Biddix
Sent: Wednesday, October 26, 2022 11:29 AM
To: [e-mail]
Subject: Final Results
Importance: High
Good morning,

I have attached your final report. Please let me know if you have any questions.
Thanks,
Jonathan Biddix
Project Manager I Carolina Labs
9800 Kincey Ave, Suite 100, Huntersyiile, NC 28078
Direct: 704.977.0978 I pacelabs com
NEW: PROCESS PAYMENTS ONLINE — click on the link below
Online Bill Yak
(Pace
NC Dept of Environmental Quality
OCT 3 1 2022
Raleigh Regional Office
NOTICE-- The contents of this email and any attachments may contain confidential, privileged, and/or
legally protected information and are for the sole use of the addressee(s). Any review or distribution by
others is strictly prohibited. if you are not the intended recipient, please contact the sender immediately
and delete any copies.
Please consider the environment before printing this email
NOTICE-- The contents of this email and any attachments may contain confidential, privileged, and/or
legally protected information and are for the sole use of the addressee(s). Any review or distribution by
others is strictly prohibited. If you are not the intended recipient, please contact the sender immediately
and delete any copies.
Please consider the environment before printing this email

aceAnalytrcal
www.paaelabs cam
October 11, 2022
One Time Client
Private Small Jobs
Huntersville, NC 28078
RE: Project: MCKEVNA PROPERTY
Pace Project No.: 92629009
Dear One Client:
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
l-tuntersville, NC 28078
[phone]
NC Dept of Environmental Quality
OCT 3 12022
Raleigh Regional Office
Enclosed are the analytical results for sample(s) received by the laboratory on October 04, 2022. The results relate only to
the samples included in this report. Results reported herein conform to the applicable TNI/NELAC Standards and the
laboratory's Quality Manual, where applicable. unless otherwise noted in the body of the report.
The test results provided in this final report were generated by each of the following laboratories within the Pace Network:
• Pace Analytical Services - Eden
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
Jonathan W Biddix
[e-mail]
[phone]
Project Manager
Enclosures
=�yPQ PC RHO/��G
TN-,8000
!;
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 1 of 9

liC
aceAnalytrcal
www.pacelabs corn
CERTIFICATIONS
Project: MCKEVNA PROPERTY
Pace Project No, 92629009
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Pace Analytical Services Eden
205 East Meadow Road Suite A, Eden, NC 27288
North Carolina Drinking Water Certification #: 37738
North Carolina Wastewater Certification #: 633
VirginiaNELAP Certification #: 460025
REPORT OF LABORATORY ANALYSIS
This report Shall not be reproduced. except in fuil,
without the written consent of Pace Analytical Services, LLC.
NC Dept of Environmental Quality
OCT 31 2022
Raleigh Regional Office
Page 2 of 9

?2eAnalytical
www.pacelabs.con
SAMPLE ANALYTE COUNT
Project: MCKEVNA PROPERTY
Pace Project No.: 92629009
Pace Analytical Services, LLC
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID
Method
Analytes
Analysts Reported Laboratory
92629009001 SEPTIC SYSTEM
PASI-E = Pace Analytical Services - Eden
SM 5210B-2016
REPORT OF LABORATORY ANALYSES
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
MWF 1 PASI-E
NC Dept of Environmental Quality
OCT 3 12022
Raleigh Regional Office
Page 3 of 9

aceAnalytical
www.pacelabs tom
ANALYTICAL RESULTS
Project: MCKEVNA PROPERTY
Pace Project No.: 92629009
Pace Analytical Services, LLC
9800 KinceyAve, Suite 100
Huntersville, NC 28078
[phone]
Sample: SEPTIC SYSTEM Lab ID: 92629009001 Collected: 10/04/22 11:05 Received: 10/04/22 12:23 Matrix: Water
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
5210B BOD, 5 day EDN Analytical Method: SM 5210B-2016 Preparation Method: SM 5210B-2016
Pace Analytical Services - Eden
BOD, 5 day 31.0 mg/L
Date' 10/11/2022 04:14 PM
2.0 1 10/05/22 23:26 10/10/22 19:36
NC Dept of Environmental Quality
OCT 31 2022
Raleigh Regional Office
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC, Page 4 of 9

ace Analytical
www.pacelabs.com
QUALITY CONTROL DATA
Project: MCKEVNA PROPERTY
Pace Project No,: 92629009
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
NC Dept of Environme'{' lie, NC 28078
(0,-sosz
OCT 31 2022
Raleigh Regional Office
QC Batch: 728028 Analysis Method: SM 5210B-2016
QC Batch Method: SM 5210B-2016 Analysis Description: 5210E BOD, 5 day Final EDN
Laboratory' Pace Analytical Services - Eden
Associated Lab Samples: 92629009001
METHOD BLANK: 3791188 Matrix: Water
Associated Lab Samples: 92629009001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
BOO, 5 day mg/L ND 2.0 10/10/22 10:11
LABORATORY CONTROL SAMPLE. 3791189
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
BOD, 5 day mg/L 198 196 99 84.6-115
SAMPLE DUPLICATE: 3791191
92629031001 Dup
Parameter Units Result Result RPD Qualifiers
BOD, 5 day
mg/L 177 171 3 R6
Results presented on this page are in the units indicated by the "Units` column except where en altemate unit Is presented to the right of the resuI.
Date: 10/11/2022 04:14 PM
REPORT OF LABORATORY ANALYSIS
This report shay not be reproduced, except in full,
without the written consent of Pace Analytical Services. LLC. Page 5 of 9

aceAnalytical
www.pacelabs.com
QUALIFIERS
Project: MCKEVNA PROPERTY
Pace Project No.: 92629009
Pace Analytical Services, LLC
NC Dept of Environrnen ?y�r�,JincerAve., Suite 100
r1Un4fe, NC 28078
[phone]
OCT 31 2022
Raleigh Regional Office
DEFINITIONS
DF - Dilution Factor. if reported, represents the factor applied to the reported data due to dilution of the sample aliquot.
ND - Not Detected at or above adjusted reporting limit.
TNTC - Too Numerous To Count
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
POL - Practical Quantitation Limit.
RL - Reporting Limit - The lowest concentration value that meets project requirements for quantitative data with known precision and
bias for a specific analyte in a specific matrix.
S - Surrogate
1,2-Diphenylhydrazine decomposes to and cannot be separated from Azobenzene using Method 8270. The result for each analyte is
a combined concentration.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
Acid preservation may not be appropriate for 2 Chloroethylvinyl ether.
A separate vial preserved to a pH of 4-5 is recommended in SW846 Chapter 4 for the analysis of Acrolein and Acrylonitrile by EPA
Method 8260.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Reported results are not rounded until the final step prior to reporting. Therefore, calculated parameters that are typically reported as
"Total" may vary slightly from the sum of the reported component parameters.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
ANALYTE QUALIFIERS
R6 The RPD between valid sample dilutions exceeded 30%.
Date: 10/11/2022 04:14 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC,
Page 6 of 9

NC Dept of Environmental Quality
PaceArialyticai
www-pacelabs coin
OCT 3 1 2022
Raleigh Regional Office
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Project MCKEVNA PROPERTY
Pace Project No.. 92629009
Pace Analytical Services, LLC
9800 Kincey Ave. Suite 100
Huntersvilie, NC 28078
[phone]
Lab ID Sample ID
Analytical
QC Batch Method QC Batch Analytical Method Batch
92629009001 SEPTIC SYSTEM
Date: 10/11/2022 04:14 PM
SM 5210B-2016
728028 SM 5210B-2016 728553
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, LLC.
Page 7 of 9

NC Dept of Environmental Quality
Oa
CHAIN -OF -CUSTODY Analytical Request Document
FaceAnalyticaf'
COm ny:
Chain -of -Custody is a LEGAL DOCUMENT- Complete all relevent fields
360.0 rr-t'3 Qf cdl4!
Pe,prt�o •,�r/. 4..i�
Copy To:
Customeetr Project NameiNumber'
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Phonel � 2"e3 25/
Email: ��
Collected
By (print(:
Billing Information:
Email T
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Site Collection In o/ dpliress:
1 `1 c) G-to et —PonR 43 kfi..10117
State: County/City: Time Zone Collected:
]PT[ )MT[ ]CrejET
Site/Facility ID #:
f3, Ne _N� 6-rsa ? �Y!
Purchase Order 11:
Quote d:
WOlF:92629009
Raiei
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I' .1 t I [ [ r ].,
" Preservative Types: (1) nitric acid, (2) sulfuric acid, (3) hydrochloric acid, (4) sodium hydroxide, (5) tiro acetate,
(6) methanol, (7) sodium blsuifate, (8) sodium thiesulfate, (9) hexane, (A) ascorbic acid, (e) ammonium sulfate,
(C) ammonium hydroxide, (D) TSP, (U) Unpreserved, (0) Other
Co Tplianee Monitoring?
IA Yes 1 ] No
DW PW5 ID is
OW Location Code:
lectedBy(5gr, rtrA
Sample Disposal:
[ 1 Dispose m. appropriate [ [ Return
[ ( Archive:
[ S Hold
Turnaround Date Required:
Rush:
( J Same Day [ ] Next Day
( (2Day [ J3Day [ ]4Day [ I5Day
{Expedite Gnarges Apply)
immediately Packed on ice:
[ ) Yes 1 ) No
Field Filtered (if applicable):
Pei Yes [ ] No
Analysis:
Matrix Codes (Insert in Matrix box below)' Drinking Water (DW), Ground Water [GW(, Wastewater (WW),
Product (P), Soil/Solid (St), 011 (OLJ, Wipe (W P), Air (AR), Tissue ITS), Bioassay (B), Vapor (V), Other (OT)
Customer Sample ID
5 e 4c, SIsipiyt
Matrix
Comp /
Grab
Collected [or
Composite Start)
Campo ite End
Date
10/6
Time
16
Date
Time
Res
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Ctns
Ana yses
Lab :- u1.
.- Lab Sample Receipt Checklist:
Custody, Seams Present/Intact 4
.Custody -.Signatures Present •Y .rya
Collector -Signature Free en �V iii a
•9r4tics intact t
Correct Bottles -tom ra
Sufficient volume - ti
Sampleu Received on1eo
VOA''- xaadrpacee AcCrptabin
aSpa BcguJ.ates
-Sample .in r?ol'diag Tine
Residual Chlorine Pr -pent Y 11 l-
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Sulfide Present
Lead Acetate. Strips:
LAB USt: gpLY--'
Lab Sample # / Comments:�..
4t 7(' ai4( V;t
Customer Remarks / Special Conditions / Possible I iazards:
Refirxtuished by/Company: (Signature)
eiinquished by/Company: (Signature)
Relinquished by/Company: (Signature)
Typeo(lccUsed:/ wee) Blue-. Dry '1r,ne
Parkiri4 Material Usc
SHORT HOLDS f ESENT (r?_ 'pour
Lab Tractcing
2653936
Radchem samples) ,creened (<sOU cpm): Y N
Gate/time: �ZZj
Date/Time:
Received oy/Company: (Signature,
Received by/Cum... •' : [ ,nature)
Samples received v
FEDE)C - U. Client
Date/Tlme:
e
Date/Time:
Courier Pace Coiner
MT( L LAB USE 05 LY
Table p:
Date/Time:
Received by/Company: (Signature}
Date/T i me:
Acctnunt:
Template:
Prelogin:
PM; '
P8:."
Lab Sample Temperatureln(n. /�1f
Temp BlaOtt:
Retre : _ Y trr Aa
Therm IDk(j,
Cooler 1 Temp Upon Receipt
C_ooicr t Therm Carr. Factor. oC
Cooler 1 Corrected Temp -
Comments:
Comments:
Trip Blank Received: y N(5
-ICL McOH TSP Othe
Non Cgnformir7RQ(S):
YES' L. O/)
Page: 1
of:

Qualtrax Document ID: 70677
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ACLU-1Bter Amber Unpreaerved (N/A) (0-)
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AG3U-250 mL Amber Unpreserved (N/A) (O-)
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DG94-250 mL Amber NH4O (N/A)(CI-)
OG9H-00 mL VOA HO (N/A)
VG9T-40 inLVOA Na25203 (N/A)
VG9U-40 mL VOA Unpreserved (N/A)
0G9V-4O mL VOA H3PO4 (N/A)
DG9S-10 mL VOA 112504 (N/A)
V/OK (3 vials per Wt)-VPWGas kit (N/A)
SPST-125 mL Sterile Plastic (N/A -lab)
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