HomeMy WebLinkAboutNC0046531_Permit Modification_19980817State: of North Carolina
Department of Environment
and Natural Resources
Division of Water Quality
James B. Hunt, Jr., Governor
Wayne McDevitt, Secretary
A. Preston Howard, Jr., P.E., Director
Mr. John R. Funk
Coordinator Regulatory Compliance & Training
Crown Central Petroleum Corporation
Post Office Box 78
Paw Creek, North Carolina 28130
A7A
NCDENR
August 17, 1998
Subject: NPDES Permit Modification
Paw Creek Terminal
NPDES Permit No. NC0046531
Mecklenburg County
Dear Mr. Funk:
The Division of Water Quality received your request for modification on May 8, 1998 for the above
referenced facility. The permit has been modified per your written request for NPDES permit modification,
supporting information, and modification fee (check #6241, $100). The air stripper may be removed from the
treatment system and the carbon adsorption system modified from six (6) 55 gallon drums to two (2) 500 pound
vessels.
The groundwater pump and treat system was replaced by an air sparging system on July 30, 1997 and is no
longer discharged. Since the discharge is now stormwater and washwater only, monitoring for ethylbenzene, iron,
manganese, phenanthrene, naphthalene and fluorene have been removed.
Please find enclosed an amended supplement to permit cover sheet and an amended effluent sheet which
should be inserted into your permit. The old sheets should be discarded. All other terms and conditions contained in
the original permit remain unchanged and in full effect. This permit modification is issued pursuant to the
requirements of North Carolina General Statutes 143-215.1 and the Memorandum of Agreement between North
Carolina and the U. S. Environmental Protection Agency.
If any parts, measurement frequencies or sampling requirements contained in this permit modification are
unacceptable to you, you have the right to an adjudicatory hearing upon written request within thirty (30) days
following receipt of this letter. This request must be in the form of a written petition, conforming to Chapter 150B of
the North Carolina General Statutes, and filed with the office of Administrative Hearings, Post Office Drawer 27447,
Raleigh, North Carolina 27611-7447. Unless such a demand is made, this permit modification shall be final and
binding.
If you have any questions, please contact Mary Cabe of my staff at (919) 733-5083, extension 518.
Sincerely,
fe,/ Preston Howard, Jr.
Attachment
cc: Mooresville Regional Office, Water Quality Section
NPDES Unit
Central Files
Point Source Compliance Enforcement Unit
Mecklenburg County Environmental Protection
Mr. Matt Einsmann, P.E., S&ME
P.O. Box 29535, Raleigh, North Carolina 27626-0535 Telephone 919-733-5083 FAX 919-733-0719
An Equal Opportunity Affirmative Action Employer 50% recycled/ 10% post -consumer paper
i. 7 ip
Permit No. NC0046531
SUPPLEMENT TO PERMIT COVER SHEET
Crown Central Petroleum Corporation
is hereby authorized to:
1. Continue to operate a 0.0432 MGD system for the treatment of stormwater and washwater
from the loading rackconsisting of an oil/water separator and two 500 pound carbon
adsorption units in series located at the Charlotte Terminal, 7720 Mt. Holly Road, Paw
Creek, Mecklenburg County, (see Part III of this permit), and
2. Discharge from said treatment works at the location specified on the attached map into an
unnamed tributary to Gum Branch which is classified WS-IV waters in the Catawba River
Basin.
A. ( ). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Permit No. NC0046531
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge
stormwater and treated loading rack washwater from outfall serial number 001. Such discharges shall be limited and monitored by the
Permittee as specified below:
Effluent Characteristics
Flow l
Total Suspended Solids
Oil and Grease2
Phenol
Benzene
Toluene
Xylene
Methyl Tert Butyl Ether
EPA Methods 624/6253
Acute Toxicity4
Discharge Limitations
Monthly Avg. Weekly Avg.
Monitoring Requirements
Measurement sample Sample
Daily Max. Frequency Type Location
1 Monthly 1 Effluent
45.0 mg/1 Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Semi-annually Grab Effluent
Annually Grab Effluent
1.19 µg/1
11.0 µg/1
Footnotes:
1 Where no measurable discharge occurs, "no discharge" should be clearly noted on the submitted monthly discharge monitoring report.
Flow may be monitored in one of four ways: a) Measure flow continuously, b) Calculate flow based on the area draining to the outfall, the built upon area, and the total rainfall
(this method of flow measurement should not be used at facilities that have large ponds to collect surface water runoff), c) Estimate by flow measurement at 20 minute
intervals during the entire discharge event, or d) Base flow on pump logs. The flow contribution from the groundwater remdiation system shall not exceed 0.0432 MGD at any
time.
2 Where possible, the grab sample for oil and grease should be skimmed from the surface of a quiescent (calm water) zone.
3 EPA Method 625 includes five (5) chlorophenols. If one or more chlorophenol(s) is detected at concentrations greater than or equal to 50 mil, the permittee will be required to
analyze for the eight chlorophenols (listed below) in addition to EPA Method 625. This additional required monitoring will begin with the permittee's next scheduled monitoring
event, occur on a semi-annual basis, and will last for the duration of the permit. Eight chlorophenols include the following: 3-chlorophenol, 4-chlorophenol, 2,3-dichlorophenol,
2,5-dichlorophenol, 2,6-dichlorophenol, 3,4-dichlorophenol, 2,3,4,6-Tetrachlorophenol, and 3-methyl-6-chlorophenol.
4 Acute Toxicity (Fathead Minnow, 24-hour) Monitoring, Annual, See Part III, Condition E.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
There shall be no direct discharge of tank solids, tank bottom water, or the rag layer.
There shall be no direct discharge of tank contents following hydrostatic testing unless the benzene concentration is less than 1.19 ug/1 and the toluene concentration is less than 11
ug/I.
DIVISION OF WATER QUALITY
July 8, 1998
Memo To: Mary Cabe
From: D. Rex Gleason
Prepared By: Samar Bou-Ghazale 58
Subject: Crown Central Petroleum Corporation
Charlotte Terminal
Permit# NC0046531
Mecklenburg County
The Mooresville Regional Office has no objections to the removal of the air stripper from
the treatment system at Crown Central Petroleum Corporation and the installation of two 500
pound carbon vessels in series prior to the discharge, as per the application. Since the subject
request is for treating stormwater and washdown water only, the monitoring for ethylbenzene,
iron, manganese, phenanthrene, naphthalene and fluorene, which was required for the GW
remediation, can be removed from the permit as requested.
If you have any questions regarding this matter, please advise.
C.)
NC0046531 Crown Central
5/8/98 Received minor mod request and $100 check #6241.
The facility would like to remove the air stripper from the treatment system, and add two
500 pound carbon adsorption units instead of the six 55-gallon drums currently used.
5/28 Tetra-Solv estimated 6.25 E-4 lb C/gall water usage. Design capacity of system 0.0432
MGD -> 8101b C/month.
Called Stanford Lummus, S&ME (864) 574-2360, for the calculations. He will fax info.
Called Samar @ MRO; he would like to see the package so I will send it once I get the
calculations.
5/29 Calcs were faxed.
6/2 Received calcs and sent package to Samar.
Called Matt Einsmann, S&ME
Calculations based on 50 gpm; permit is for 30 gpm (0.0432 MGD).
Flow should be monitored monthly — 7/97 = 0.0097, 12/97 = 0.0013,
1/98 = 0.0054, 2/98 = 0.0101 MGD.
Flow is measured by calculating volume of the spill control basin prior to
episodic discharge.
Volume of oil/water separator? 400 gallons
GKPR has 3 oil/water separator outfalls listed. No data for 2 or 3.
Sent copy to compliance to have other outfalls removed.
Monitoring for ethylbenzene, iron, manganese, phenanthrene, naphthalene and fluorene
was added because the stormwater is mixed with groundwater (see issue letter 8/2/96).
These parameters can be taken out now that the waste streams are not mixed anymore.
Compliance inspection 4/29/97 by Richard Bridgeman. TSS = 3 mg/1, other parameters = BDL
7/13 Received SR. RO has no objections to removing the air stripper and above listed monitoring.
7/21 Drafted modified permit.
To DAG for issue 7/27
A. ( ). EFFLUENT LIMITATIONS AND MONITORING REQUIREMENTS Permit No. NC004653
During the period beginning on the effective date of the permit and lasting until expiration, the Permittee is authorized to discharge stormwater
and treatedwater from outfall(y) serial number 001. Such discharges shall be limited and monitored by the Permittee as specified below:
AA`
lfflu nt Characteristics
Flow I
Total Suspended Solids
Oil and Grease2
Phenol
Benzene
Toluene
Xylene
.hthyibenzene
Phcnanthrcne -
JJuorene
1apthatctte
Methyl Teri Butyl Ether
EPA Methods 624/6253
Acute Toxicity4
(i.,//%/\..chbvc(
Discha ge Limitations Monitoring Requirements
Monthly Avg. Weekly Avg.
Measurement Sample Sample
Daily Max, Frequency Type Location
I Monthly 1 Effluent
45.0 mg/I Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
1.19 µg/I Monthly Grab Effluent
11.0 µg/I Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Monthly Grab Effluent
Semi-annually Grab Effluent
Annually Grab Effluent
Foolnolcs:
I Where no measurable discharge occurs, "no discharge" should be clearly noted on the submitted monthly discharge monitoring report.
Flow may be monitored in one of four ways: a) Measure flow continuously, b) Calculate flow based on the area draining to the outfall, the built upon area, and the total rainfall
(this method of flow measurement should not be used at Facilities that have large ponds to collect surface water runoff), c) Estimate by flow
tneasurement at 20 minute intervals during the entire discharge event, or d) Base flow on pump logs. The flow contribution from the groundwater remdiation system shall not
exceed 0.0432 MGD at any time.
2 Where possible, the grab sample for oil and grease should be skimmed from the surface of a quiescent (calm water) zone.
3 EPA Method 625 includes five (5) chlorophenols. if one or more chlorophenol(s) is detected at concentrations greater than or equal to 50 µg/I, the permittee will be required to
analyze for the eight chlorophenols (listed below) in addition to EPA Method 625. This additional required monitoring will begin with the permittee's next scheduled monitoring
event, occur on a semi-annual basis, and will last for the duration of the permit. Eight chlorophenols include the following: 3-chlorophenol, 4-chlorophenol, 2,3-dichlorophenol,
2,5-dichlorophenol, 2,6-dichlorophenol, 3,4-dichlorophenol, 2,3,4,6-Tetrachlorophenol, and 3-methyl-6-chlorophenol.
4 Acute Toxicity (Fathead Minnow, 24-hour) Monitoring, Annual, See Part III, Condition E.
There shall be no discharge of floating solids or visible foam in other than trace amounts.
There shall be no direct discharge of tank solids, tank bottom water, or the rag layer.
There shall be no direct discharge of tank contents following hydrostatic testing unless the benzene concentration is less than 1.19 ug/I and the toluene concentration is less than I 1
ug/l.
Groundwater Treatment System Design Review 6/4/98
Facility:
NPDES #
[Crown Central - Charlotte Terminal
NC 46531
r
[Air Flow Rate
i 0 I CFM
Air/Water
Ratio = 0
Water Flow Rate
43,200EGPD
163,512 liters/day
30.0 GPM
Oil/Water
Separator
Size:
4
400jgallons
No free product
13.3 minute detention time
Constituent
Concentratior
(ppb)
Removal Eff.
(percent)
Residual
(mg/I)
AC Adsorbed4C
(mg/g)
Absorbed
(g/day)
Benzene
45
99.50
0.000225
16
2.30
Toluene
97
99.50
0.000485
22.5
3.52
Ethyl Benzene
10
99.50
0.00005
24
0.34
Xylene
89
99.50
0.000445
46
1.58
Lead
0
#VALUE!
MTBE
0
85.40
0
7.5
0.00
Dibromoethan
0
98.00
0
1,2 EDC
0
98.80
0
2.5
0.00
IPE
0
98.00
0
162
0.00
Naphthalene
0
68.20
0
68
0.00
Phenol
0
98.00
0
91
0.00
r
1
1,000(total Ibs of GAC in filter) 2 x 500 lb
58,607.64 days to breakthrough
Total usage # 7.75
MAY-29-88 15.45 FROM=S&ME INC SPARTANBURG ID=864 576 8730 PAGE 1/3
FAX TRANSMITTAL
TO:
S&ME
ENVIRONMENTAL SERVICES
ENGINEERING, TESTING
Mary Cabe
FIRM; NCDENR FAX NJ BER: 919 733-0719
LOCATION: Raleigh, NC
FROM: Matt Einsmann
Environmental Engineer
DATE: May 29,1998 Tom: 3:45 pm
RETURN FAX NUMBER: (864) 576-8730
NUMBER OF PAGES INCLUDING COVER SHEET: 3
(If you do not receive all pages, call (864) 574-2360)
PROJECT NUMBER.: 1264-94-288
S&ME, Inc.
155 Tradd Street
Spartanburg, SC 29301
Phone (864) 574-2360
Fax (864) 576-8730
Mary,
As requested, attached find the calculations for the carbon usage rate for the permit modification for
Crown Central Petroleum Corporation at their Charlotte facility. The carbon usage rates were
calculated by Bamebey & Sutcliffe Corp. and are based on EPA isotherms.
Do you foresee any problems with the modification request? and What time frame can we expect for
the modification approval? Call me at (864) 574-2360 with any questions.
Matt Einsmann
NAY-26-88 15:45 FROM:S&ME INC SPARTANBURG ID:864 576 8730
YY•• . •M w I.' Mfg..L.'f 1..LO rM Page 1 of
PAGE 2/ 3
LFAX COVER
Subject : estimated carbon usage
Pages including cover page: 1
MESSAGE
Ap, icadon:50 gm
benzene at 45 ppb: 16.6 IbJday
toluene at 97 ppb: 12 9 IbJday
ethylbenzene at 10 ppb: 5_4IhJday
xylene at 89 ppb: 7.4 lb day
Total estimated carbon usage for saturat o' :
42.27161day
Total estimated carbon usage for nreakthiough:
(42.27 x 1.25 = 53 IbJday
=? (�s
Date : 5/29/1998 Time : 2:41:26 PM
is 4 :- L. 3 / (CIsr%/4 77,e )
MAY-29-98 1S:46 FROM:S&ME INC SPARTANBURG
ID:664 576 8730 PAGE 3/3
JOE NAME
S&ME
a•j.J • Ckf i .o:r
JOB No. /.44 ski. 2.88
SHEET NO. f %
DATE 1/4 ` 8
COMPUTED BY
SUEJECT -^. 4 - s I1 X -Z-, CHECKEC BY
@A1.
N-fPcr S.aF�:Y
?S eo P-•
r
lAc.z
/14c 'sue
�-v grin U 0 u3 /c o a../
.t(rwrvr
• 0.50004s ,[4 Lea,,,,
G-wq E/i O
ro fir A .ar is rd-r) .
C. 4t80., i%s,4af - 0.000623 i( /.j' + 0-do0937�
/moo
PPws4.O 5,)'S -.
c) cy C (xeo� ▪ / G l/, 0 3~3s_ 333 C-4. /4,
O, d)oP37,' [-d C4.¢eb,1
a 7 • C'4o.a /
6- 0009.37s-
1,000 4o C-Ate'B�-' f /
6 - 0 04 9 S is
Cd-•14co.sldJ S
33, 332, 4-44. =/gy O. __
i, 0G4, 64 7 F 4 O
LB SY,1- ,ya,,.4 , CAde..4a .. ..14 Ecj4 7-9 $.ti
/s C r�sA•2G-re 4 . a a 0 dP ! ie
rJ.t•�.t ,
/`rva 8 7S44 SA'S Tom,,/ C *444,i! 111Z12.s 71) 41 a If/F+r4LJ .tlre-4
0/SCkA,:G'74416. �Ot'd oc'o c)di O.
i v ect• d d o L-6 S ySrr [A2.6v,r I""6'.os re) 45 G (6e.0
G��t[.444-e4, 16 / D (�o, 04 {j C_A-r.[o-S e,- 614 ;)—
S&ME
May 4, 1998
North Carolina Department of Environment
and Natural Resources
Division of Environmental Management
NPDES Permits Group
Post Office Box 29535
Raleigh, North Carolina 27626-0535
ATTENTION: David Goodrich
RE0. E
ry f f r't' n f 9r1
`7nrt-n(.:r.ilnrb permitting
Reference: MODIFICATION TO NPDES PERMIT
Crown Central Petroleum Corporation
Charlotte Terminal
7720 Mount Holly Road
Mecklenburg County
Paw Creek, North Carolina
NPDES Permit # NC0046531
S&ME Project No. 1264-94-288
Dear Mr. Goodrich:
S&ME, Inc., on behalf of Crown Central Petroleum Corporation (Crown), herein submits a
modification to the above referenced National Pollutant Discharge Elimination System (NPDES)
Permit. The existing NPDES Permit is for the discharge of stormwater and washwater from the
loading rack and recovered groundwater. The water is treated by an oillwater separator, an 8,000
gallon holding tank, an air stripper, and granular activated carbon filters prior to discharge to an
unnamed tributary to Gum Branch. Figure 1 shows a process and implementation diagram
(P&ID) of the existing treatment system.
Since the groundwater pump and treat system was replaced with an air sparging system on July
30, 1997, the water treatment system has received water from the loading rack only. Crown
continues to operate the treatment system outlined above for all oil/water separator effluent. We
have investigated the option of removing the air stripper from the treatment stream and treating
the discharge water through the activated carbon filters solely.
S&ME, Inc. 155 Tradd Street, Spartanburg, South Carolina 29301, (864) 574-2360, Fax (864) 576-8730
Greenville, South Carolina, (864) 232-8987
J
;. • NPDES Permit Modification
S&ME Project No. 1264-94-288
Crown Central Petroleum Corporation May 1998
On September 9, 1997, we collected a water sample from the discharge of the holding tank. This
sample represents the influent characteristics to the water treatment system. A copy of the
analytical report is included in Appendix A. TetraSolv, Inc. (a carbon manufacturer) estimated
the carbon usage rate (6.25 E —4 pounds of carbon per gallon of water) based on the analytical
results from the influent water and the existing NPDES effluent limitations. From the carbon
usage rate and a safety factor of 1.5, we estimated that approximately 500,000 gallons of water
could be treated by an activated carbon filtration system. The proposed carbon filtration system
consists of two, 500 pound carbon vessels in series. A manufacturer's cut sheet is included in
Appendix B.
The new, proposed water treatment system will include an oil/water separator, an 8,000 gallon
holding tank, and two granular activated carbon filters in series. Figure 2 shows a P&ID of the
proposed treatment system. Per our recent conversation with Ms. Mary Cabe (North Carolina
Division of Environmental Management), we understand that this proposed change constitutes a
minor modification and have enclosed a check for $100.00 for the minor modification permit fee.
Your expedient review of this modification and issuance of an operating permit is appreciated.
Please call us at (864) 574-2360 with any questions.
Sincerely,
Matt Einsmann, P.E.
Environmental Engineer
ME/S L/ld/environ98/npdesmod.doc
cc. Jim Janson
Floyd Reid
John Funk
2
Stanf#d Lummus, P.E.
Senior Environmental Engineer
CAD FILE: K: \DWG\1264\1994\94288\94288PD1.DWG
RECOVERED
GROUNDWATER
STORMWATER
ow -
FROM LOADING RACK
STORMWATER
OIL/WATER
SEPARATOR
8,000
GALLON
HOLDING
TANK
LSH
LOW
PROFILE
AIR
STRIPPER
55-Gallon
Drums (Typ)
a
DISCHARGE
am —
CARBON FILTRA4101t7.
SYSTEM
C>
LT. rt
FROM FACILITY
LEGEND
LEVEL SWITCH -LOW
LEVEL SWITCH -HIGH
au
0
SCALE:
NOT TO SCALE
CHECKED BY:
DRAWN BY: SB
DATE: 05-04-98
E
P & ID - EXISTING
CROWN -CHARLOTTE
CHARLOTTE, NORTH CAROLINA
ENVIRONMENTAL SERVICES
ENGINEERING • TESTING JOB NO:
1264-94-288
FIGURE NO:
1
CAD FILE: K: \DWG\1264\1994\94288\94288PD2.DWG
STORMWATER
FROM LOADING RACK
STORMWATER
OIL/WATER
SEPARATOR
c
8,000
GALLON
HOLDING
TANK
u
500 LB
CARBON
VESSEL
500 LB
CARBON
VESSEL
1
FROM FACILITY
DISCHARGE
SCALE:
NOT TO SCALE
CHECKED BY:
DRAWN BY: SB
DATE: 05-04-98
E
ENVIRONMENTAL SERVICES
ENGINEERING • TESTING
P & ID - PROPOSED
CROWN -CHARLOTTE
CHARLOTTE, NORTH CAROLINA
JOB NO: 1264-94-288
FIGURE NO:
2
SPECIXLIZED ASSAYS, INC.
2960 Foster Creighton Dr.
P.O. Box 40566
Nashville, TN 37204-0566
Phone 1-615-726-0177
S & M E, INC. 6066
ATT. STANrORD LUMMUS
155 TRADD STREET
SPARTANBURGG, SC 29301
Sample ID:
Project: 3168
Project Name: S&ME CROWN CHARLOTTE
Sampler:
State Certification: 94009
Site I.D. :
hiALYT I G AL R TEP R "1"-
Lab Number: 97—A076535
Date Collected: 9/ 9/97
Time Collected: 11:10
Date Received: 9/10/97
Time Received: 9:00
Sample Type: Water
Analyte
1t11RGA1OEC PARA1iETERSr
Benzene
Toluene
Ethylbenzene
Xylenes, total
Result
Report 0uan Dil
Units Unit Unit Factor Date Tine
45.0
97.0
0
89.0
HD = Rot detected at the report linit.
ug/1
ug/1
ug/1
ug/1
1.0 1.0 1
LO 1.0 1
1.0 1.0 1
1.0 1.0 1
9/11/97 17:56
9/14/97 17:56
9/14/97 17:56
9/14/97 17:56
Analyst Method batch
J.Mitchell 602
J.iiitchell SO2
J. li i to hell 602
J.Mitchell 602
4443
4443
4443
4443
Surrogate
AA SURROGATE RECOVERIES Kh
'/, Recovery Target Range
DTEX/CR0 Surr., a,a,a-trifluorotoluene 93. 50. - 150.
Report Approved By: /vtu t Q,nn,wv Report Date:
Theodore •J. Duelio, Ph.D. , D. A. Officer
Michael H. Dunn, M.S. , Technical Director
Danny B. Hale, M.S. , Laboratory Director
SEA 2 2 1997
9/18/97
SPECIALIZED ASSAYS, INC.
2960 Foster Creighton Dr.
P.O. Box 40566
Nashville, TN 37204-0566
Phone 1-615-726-0177
& M E, INC. 6066
ATI'. STANFORD LUMMUS
155 TRADD STREET
SPARTANBURG, SC 29301
I`.I'Pr L.YT I C AL R 1EP QR T
Lab Number : 97—A076536
Sample ID: TRIP BLANK, Date Collected:
Project: 316e Time Collected:
Project Name: S&ME CROWN CHARLOTTE Date Received: 9/10/97
Sampler: Time Received: 9:00
State Certification: 8400E Sample Type: Water
Site I. D. :
Report Pun Dil
Analyse Result Units Limit Limit factor Date Time Analyst Method hatch
*ORGANIC PARAMETERS*
Benzene ND ug/1 1.0 1.0 1 9/13/97 20:30 S. Wani 602 4921
Toluene ND ug/1 1.0 1.0 1 9/13/97 20:30 S. Wani 602 4921
Ethylbenzene ND ug/1 1.0 1.0 1 9/13/97 20:30 S. Wani 602 4921
Xylenes, total ND ug/1 1.0 1.0 1 9/13/97 20:30 S. Mani 602 4921
ND = Not detected at the report limit.
Surrogate
** SURROGATE RECOVERIES Mx
X Recovery Target Range
BTEX/6RO Surr., a,a,a-trifluorotoluene 96. 50. - 150.
Report Approved By:
n LL /
Report Date: 9/18/97
Theodore J. Duello, Ph. D. , Q. A. Officer
Michael H. Dunn, M. S. , Technical Director
Danny B. Hale, N. S. , Laboratory Director
•
SPECIALIZED ASSAYS, INC.
2960 Foster Creighton Dr.
P. O. Box 40566
Nashville, TN 37204-0566
Phone 1-615-726-0177
S & M E, INC. 6066
ATT. STANFORD LUMMUS
155`'TRADD STREET
SPARTANBURG , SC 29301
CHA I I OF �CUSTUL}'Y
Project Number: 3 r 6 g Sampler:
I
Analysis
Requested
I
Project Name: el_a� \ a�p�� SAE Quote:
F
J
Lab No.
Field Number
Date
Time
Matrix
6rab
Como
Bottles
II
lq
ill
97-A076536
7(l2 Mire\
Relin uishe
rg
lIciTi
Received by:
D/T
g(4
Relinquished by:
D/T
Received by.
•
D/T
Relinquished by:
D/T
Received by:
D/T
Relinquished by:
D/T
Received by:
D/T
Cooler Temperature When Recevied:
J� U
Laboratory Project Number:
Cooler Seals Intact?
Fed—X Air Bill Number:
SPECIAL INSTRUCTIONS: