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HomeMy WebLinkAboutWQ0031725_Annual Report_20180307t4�� 6P 0 Annual Report Review SOP Class B Land Application Reporting Period: 11% / 1 j, — Permit Details: W'D 0031 -4 2— Is 503? 14-5 Class A orD Maximum Dry Tons Per Year: 9,CD Number of acres permitted: (A, 6 • Number of fields in permit: 10 Counties that land is permitted for. VJ►1 Monitoring Frequency for TCLP: A,," wo-1 Monitoring Frequency for Residuals Analysis: A n ^, Monitoring Frequency for Pathogen & Vector Attraction Reduction: A nr) Groundwater monitoring: . Annual Land Application Certification Form Was a certification form submitted? V Was land application conducted during the reported year? ! 5/J �r,v How many dry tons and dry tons per acre were applied? 14l-> Q 3 D 7- i, S 19 a 9/4 4" 23a o'G? 7 Were the applications within the permitted amount? Verify PAN if more than 10 tons/acre? 1,'N.7 1,518 e), 5,24 VIS7 Did it indicate compliance? Y j ,120 1, 231 ' V,sz)5 I. 84.5 Was it signed by the appropriate people?�/ 2. Monitoring Were the analyses conducted at the required frequency? Was an analyses taken for each source that was land applied?y/ Were the metals analyses reported on the Residual Sampling Summary Form?y Were the results reported in mg/kg?l Were the pH's 6.0 or greater for each residual sample?y told «,4 e � Were the heavy metals within ceiling concentration permit limits? y Were the lab analyses attachedTJ Were all the required parameters tested?w Was TCLP analysis conducted? Were the TLCP contami�n is within regulatory limits? Was a corrosivity, ignitability, and reacti i y analysis conducted? T�&0 (a.4 >'LaC p4 3. Field Summary to Were the land application events recorded on the Field Summary Forms? How many fields were applied on this year?')Q Was a Field Summary Form submitted for each field?y Were all the residuals applied to permitted land? Were all the residuals applied from permitted sources? Were the field loading rates for each metal and PAN calculated (year to date)? Were the cumulative pollutant loading rates calculated? Y Were the calculations correct?I Were the PAN loading rates within permit limits?�I Were the heavy metal cumulative pollutant loading rates within permit limits? Were the residuals applied on a suitable crop?� ®U,( o-.� 4,T Were the applications conducted during the crop's growing season? Were the Field Summary Forms complete? n pq `jl 01) Was lime application on Field Summary Fofm? No lime applied. y pP l -C �ll -► ) D P3 •-cco4 i i—r }) lll�Y Co 1-1 �) 4. Pathogen and Vector Attraction Reduction p P _(At4&S (U -1-7) Was a signed copy of the Path�en and Vector Attraction Re�iction Form sl itted?y Did the form indicate the period of coverage, the residual class, and the pathogen reduction alternative and the vector auction reduction option used? Class B Pathogen Review Alternative 1- Fecal Coliform Density Was the sampling conducted at the required frequency? Were seven samples taken? y . Was the geometric mean calculated and done correctly? y Did the results show compliance (less than either 2,000,000 MPN/gram of total solids or 2,000,000 Colony Forming Units/gram of total solids)?� Alternative 2 - Use of Process to Significantly Reduce Pathogens (one of five) • Was the sampling conducted at the required frequency? 1. Aerobic Digestion Was it an aerobic process (Inspection)? Were logs submitted showing time and temperature? Were temperatures within range for complete time period? Was the time and temperature between 40 days at 20°C (687) and 60 days at 15°C (59°F)? 2. Air Drying Were the residuals on sand beds or pave or unpaved basins for three months? Was the ambient temperature above 0°C (32°F) for two months? Were the residuals partially digested? Were residuals exposed to atmosphere during two months above 0°C (not snow covered)? 3. Anaerobic Digestion • Was it an anaerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? Was the time and temperature between 15 days at 35°C (95T) to 55°C (131T) and 60 days at 20°C (68°F)? 4. Composting (usually will be Class A when composting is used) Was it a composting procedure (not natural decay under uncontrolled conditions)? Were logs submitted showing time and temperature? Was the temperature raised to 40 5. Lime Stabilization Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? Were logs submitted showing time and temperature? Was the pH raised to 12 after two hours of contact? Were logs submitted showing time and pH? Was temperature corrected to 25°C (77°F)? Alternative 3 — Use of Processes Equivalent to RSRP (Not commonly use. See White House Manual page 100-103, tables 11-1 and 11-2.) Vector Attraction Reduction Review Was the sampling conducted at the required frequency? Option 1 — 38% Volatile Solids Reduction Was there 38% reduction? -I ErS��°� Were lab sheets/calculations in report? D Elk Was the reduction on volatile solids (not total solids)? )/ Were the sam les taken at beginning of digestion process and before application (Inspection)? '� • Were calculations correct?�I Option 2 — 40-Day Bench Scale Test Were residuals from anaerobically digested treatment (Inspection)?, Were residuals anaerobically digested in lab? Was the test run for 40 days? Was the test done between 30°C (86°F) and 37°C (99°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 17%? Were lab sheets/calculations in report? Were calculations correct? Option 3 — 30-Day Bench Scale Test Were residuals from aerobically digested treatment (Inspection)? Were residuals aerobically digested in lab? Were residuals 2% or less total solids? If not 2% total solids, was the test ran on a sample diluted to 2% with unchlorinated effluent? Was the test run for 30 days? Was the test done at 20°C (68°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 15%? Were lab sheets/calculations in report? Were calculations correct? Option 4 — Specific Oxygen Uptake Rate(SOUR) Were residuals form aerobically digested treatment (Inspection)? Were residuals 2% or less total solids (dry weight basis) (not diluted)? Was the test done between 10°C (50°F) and 30°C (867)? Was the temperature corrected to 20°C (687)? Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)? Was the sampling holding time two hours? Was the test started within 15 minutes of sampling or aeration maintained? Option 5 —14-Day Aerobic Process Were the residuals from aerobically digested treatment (Inspection)? Were the residuals treated for 14 days? Was the residuals temperature higher than 40°C (104°F) for a 14-day period? Was the average residuals temperature higher than 45°C (113°F)? Option 6 — Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? Did the pH of residuals remain at 12 or higher for two hours without the addition of more alkali? • Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? • Was the pH corrected to 25°C (77 17)? Option 7 — Drying of Stabilized Residuals Does the residuals contain any unstabilized residuals? Were the residuals mixed with any other materials? Were the residuals dried up to 75% total solids? Option 8 — Drying of Unstabilized Residuals Were the residuals mixed with any other materials? Were the residuals dried to 90% total solids? Option 9 —Injection • Was there any significant amount of residuals on land surface one hour after injection (Inspection)? Was injection done on pasture or hay field? Was injection done at time that crop was growing? If Class A with respect to pathogen, were residuals injected with eight hours after discharge from pathogen treatment? • Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? • Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? 5. Soil Tests Was a Standard Soil Fertility Analysis conducted for each application field? Were the soil pH's 6.0 or greater for each application field? (J Q If no, was lime applied to those fields?V Were the copper and zinc indexes in th6 soil less than 2000 for each application field? Was sodium less than 0.5 meq/100 cm^3? Was the exchangeable sodium percentage (ESP) less than 15%? 6.General : Was the report in the proper format?y Was the annual report complete? Y Was the report submitted on time? 1Jo 5P Baxter Healthcare Corporation 2017 Annual Report Land Application Program Permit No. WQ0031725 MAR ®.7 2®,, T LS/yNnil r! /j'tyJ�IV� 1 r j biviSion of Water Resources LIAR 12 2018 Water Quality Regional Operations Asheville R2gienal Office ANNUAL LAND APPLICATiON CERTIFICATION FORM WQ Permit#: WQ0031725 County: McDowell Year: 2017 V, Facility Name (as shown on permit): Land Application Operator: Baxter Healthcare Corporation Soutlicrn Sol] Builders_ inc. Phone: 336-957-7871 Land application of residuals as allowed by the permit occurred during the past calendar year? Yes 0 No - If No, skip Part A, and Part.B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permit: 10 Total number of .fields utilized for land application during the year: 10 Total amount of dry tons applied during the gear for all application sites: 147.03 Total number of acres utilizes for land application during the rear: 69.6 Part B - Annual Comviancc Statement: Facility was compliant during calendar year 2017 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. Yes El No If no please, provide a written description iyhy the facility was not compliant, the (fates, and explain corrective action taken. 1) Only residuals approved for this permit Nvere applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. >) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboraton results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1 I05(a) or the Pollutant Loading Rates in 15A NCAC 02T. I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1.11.1 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and reniediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of lacy, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there arc significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 2 Permittee Name and Title (type or print) Sig 0 lure of Periuittec Date Signature of Prcparer* 1 1 Date Signature of Land Applier Dale (if different from Permittee) �l (if different from Permittee and Preparcr) x Preparcr is defiled in 40 CFR Part 503.9 (r) and 15A NCAC 02T. 1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Facility Name: Residual'Source WQ # or NPDES #: WWTP Name: Residual Analvsis Data Baxter Healthcare WQ0031725 Baxter Healthcare Laboratory: 1) 2) 3) 4) 5) Waypoint Analytical Parameter (mg/kg) Conc. Limit mg/ka k' Sample or Composite Date 1.-9-1.7 Percent Solids (%) NA 10.78 ' Arsenic 75 4.54 Cadmium 85 2 V Copper 4,300 70.7 Chromium NA 32.3'� Lead 840 5.5 ✓ Mercury 57 0.4 Molvbdenum 75 5 Nickel 420 1-.2 Selenium 100 5 Zinc 7,500 87.4 Total Phosphorus NA 8860 TKN NA 84400 Ammonia -Nitrogen NA 9180 Nitrate and Nitrite NA 2.72 '/ For surface disposal facilities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Lily dig Signature of Preparer * Date *Preparer is defined in 40 C1'R Part 50 3.9(r) and 15A NCAC 2'1' .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: WQ00031725 .Facility Name: Residual Source N.PDES # or WQ#: WWTP Name: Residual Analvsis Data Baxter Healthcare WQ00031725 Baxter Healthcare Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Sample or Composite Date 1-9-17 Potassium 2370 Sulfiir 7900 Calcium 7050 Magnesium 2390 Sodium 23 70 Iron 3630 Aluminum 1130 Manganese 36.6 Organic N 75220 14 ; r pH 7.6 V "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer x 7jMrK Date DENR FORM RSSF - B (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ00 31725 Cation Exchange Capacity (non -503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 5.5 Acres Permitted: 5.5 Site #: DPI -A Field #: 11.00 FcC2 DPI. -A Residual Analysis Data (:Heavy Metals and Total Phosphorus use mPA2, %► Solids use Raw :Percent #): Sample or Com- posite Date 1 1/9/17 2 3; 41 51, 6' 7 8 10 11 121, % Solids 10.78 Arsenic 4.54 Cadmium 2 Copper 70.7 hromiun 32.3 Lead 5.5 Mercury 0.4 Mohb- dcnum Nickel 13.2 Selen4uu 5 Zinc 87.4 Total Phos- plionis 8860 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1... 2. 3,s 4.:. 6.. 8 i <.9... 101 11 3 12... DT/Ac./ I _5..: _�J _.._.: _. o App. Event 2.00 Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadrnium 0.008 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.283 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.283 Chroininir 0.1.29 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.129 Lead 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Mcrcun.- 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Mold b- 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Nickel 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.053 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 0.350 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.350 Total Phos- 35.440 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 35.440 horns "l certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier [-11•atiil$ Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 3.23 Permit #: WQ0031725 Cation Exchange Capacity (non -503 only): Operator: Acres Used: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 1.6 Acres Permitted: 1.6 Site #: DP 1-B Field #: DPI-B Residual Analysis Data (}Ieavy Metals and Total Phosphorus use mg/kg, %o Solids use Raw Percent #): Sa.iiple or Com- posite Dale 1 1 1/9/17 21 3 4; 7; 6! 7 8 91 10 ` 17 j 12 j % Solids 10.78 Arsenic 4.54 Cadmium 2 Copper 70.7 hromiun 32.3 Lead Mercury 0.4 Molvb- dgwrn Nickel 13.2 Selenium 5 Zinc 87.4 Total Phos- ho111s 8860 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 2 1 3_ 1 4 5� 7 8 9! 0 1] 11 12 j DT/Ac./ _)..' ... _6.1 _ .. _ _..._.. .._, H o App. Event 2.02 Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.286 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.286 Chroi-niuni 0.131 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.131. Lead 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 M01\=b- 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 dent.1111 Nickel 0.053 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.05 3 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 0.353 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.353 ' Total Phos- 35.812 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 35.812 horns 1 155,Vq "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier 03 -a 0,g Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter- Healthcare Total Dry Tons Applied (Annual): 6.47 WQ0031725 Cation Exchange Capacity (non -03 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: 3 Acres Permitted: 3 Site #: DPI -C Field #: FcC2 DPt-C Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, °/i Solids use Raw Percent #): Sample or Com- posite Date 11 1./9/ l 7 2' � 3i 4; 5; 6 7 8 90 ' � 1 111 12' % Solids 10.78 Arsenic 4.54 Cadmium 2 Copper 70.7 hromiun 32.3 Lead 5.5 Mercury 0.4 Moh-b- denu in Nickel 13.2 Selenium 5 Zinc 87.4 Total Phos- bonus 8860 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total ?._? ?. 3.! 4... 5..1 6' 71 8' ._........ 9, ...__.....! 1 O, 1 i i J 12 DT/Ac./ ....___: App. Event 2.16 Arsenic 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Cadmitun 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.009 Copper 0.305 0.000 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.305 hromiun 0.139 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.139 Lead 0.024 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.024 Mercun, 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 dellllin Nickel 0.057 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.057 Selenium 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Zinc 0.377 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.377 Total Phos- 38.187 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 38.187 horus i certuy, unaer penalty of taw, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sign tore of Land Applier f-as-a fa Date V J J DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non 5503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 9.6 Acres Permitted: 9.6 Site #: DPI-D Field 4: 17.46 FcC2 DPI-D Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2, 0/1 Solids use Raw Percent #): Sample or Coln- posile Date 1 1 U9/17 2 r __3j 51 61 7j 8 j 91 101 11 ' 12 `%, Solids 10.78 Arsenic 4.54 Cadnlllllll 2 Copper 70.7 hro1niun 32.3 Lead 5.5 Mercun 0.4 Molvb- denunl Nickel 13.2 Selenium 5 Zinc 87.4 Total Phos- lhonls 8860 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total �, 2_ 4 5 6s 7 8' 1 9? 10 11' l 12 DT/Ac./ J _3.! ........... o App. Event 1.82 Arsenic 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.017 Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.257 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.257 hromitlrl 0.118 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.118 Lead 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Mercul-y 0.001. j 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 de ntl Ill Nickel 0.048 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.048 Selenium 0.018 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Zinc 0.318 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.318 Total Phos- 32.233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.233 llorus I I I I I I I I I��„'J Sa "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted..) am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier -aa-901A Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 12.06 Permit #: WQ00 3) 1725 Cation Exchange Capacity (non -03 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 5.877 Acres Permitted: 5.877 Site #: DP3-Corn Field #: DP3-Corn Residual Analysis Data (:Heavy Metals and Total Phosphorus use mg/kg, %► Solids use Raw :Percent #): Sample or Com- posite Date 1? 1/9/ 17 2' 3" 4 5; 6 7 8' 9' j0j 1 F 12 % Solids 10.78 Arsenic 4.54 Cadmium 2 Copper 70.7 Chromiuni 3 2. 3 Lead -5.5 Mercury 0.4 Molyb- de nu Im Nickel 13.2 Selenium J Zinc 87.4 Total Phos-- bonus 8860 Annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total w ?..1 4... 6.J 7 ? 8 ! 9...7 1100 I 11 1 12 DT/Ac./ _1 / _3_1 __5..? w ............ H o App. ,/ A Event 2.05 Arsenic 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.290 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.290 hromitu 0.1.33 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.133 Lead 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Mercuryy 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Moh b- 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 denum Nickel 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054 Sclenitun 0.021 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.021 Zinc 0.359 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.359 Total ©,5;8 Phos- 36.361 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 36.361 horns "i certity, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". i� I-aa-aulA Sigma ure of Land Applier Date V i DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ003) 1725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 6.983 Acres Permitted: 6.983 Site #: DP3-Grass Field #: 23.65 FcB2 DP3-Grass Residual Analysis Data (Heavy .M.etals and Total Phosphorus use in2/kg, °/, Solids use Raw Percent 9): Sample or Com- posite Date 1? 1/9/17 2' 3 j 4; 5 6 1 7 I 8! - - 9 i 10 11 121 '%, Solids 10.78 Arsenic 4.54 CadllliUlll 2 Copper 70.7 Cliroiniuni 3 2. 3 Lead 5.5 Mercury 0.4 Molyb- dell a 111 Nickel 13.2 Selenium Zinc 87.4 Total Pllos- 110111 S 8860 Annual Heavv metal new Loadings ic:alculated in lbs/acrel: Tolal a..s _2...1 .__3.. W4.. ....5... _6_ 7_ a._; 9...i. 1._1....i.2._ DT/Ac./ c App. Event 3.39 Arsenic 0.031 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.031 Cadmium 0.014 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.014 Copper 0.479 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.479 hronllun 0.219 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.219 Lead 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Mercin- - 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Mold b- dC (111111 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.034 Nickel 0.089 0.000 0.000 0.000 0.000 0.000 0.000 0.0()0 0.000 0.000 0.000 0.000 0.089 Selenium 0.034 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.034 Zinc 0.592 0.000 0.000 0.000 0.000 0.000 0.000 ().000 0.000 0.000 0.000 0.000 0.592 Total Phos- 60.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 60.018 horns l.CI u,y, u,nlCr NCIlau.y of law, that ups uocument was prepares unser my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". V v V ..0 Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 22.02 Permit #: WQ00 3) 1725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 Acres Used: 8.7 Acres Permitted: 8.7 Site #: DP4 Field #: DP4 Residual Analysis Data (.Heavv Nletals and Total Phosphorus use ing/kg. 0/1 Solids use Raw Percent #l: Sample or Con1- posite Date 1 1/9/17 21 3 1 4 5 6 7! 8- - 9 i 10 11 1 12_ % Solids 10.78 Arsenic 4.54 Cadlniurn 2 Copper 70.7 11ro1111u11 3 2. 3-3 Lcad S.-S Mercul-N 0.4 Molyb- denL1111 Nickel 13.2 Selenium i Zinc 87.4 Total Phos- horus 8860 Annual rleavv lvtetal .rle1Q LOadlilLYs 11-.111culatea In Insmere►: Total 1...._ _3_ 4...; 5... 6 i 7 8..w 9 10 11 12 DT/Ac./ ✓ __...._. c App. y E\•ent 2.5 3 Arsenic 0.0233 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.023 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.0.10 Copper 0.358 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.358 hronliun 0.1.64 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.164 Lead 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Merctin 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- dernirn 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Nickel 0.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.067 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 Zinc 0.442 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.442 Total Phos- 44.849 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 44.849 horns I I I 0. %?, ICI uiy, unuC, penaiLy u1 law, that ups uocument was prepared under my mrectlon or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". w' V Signatu e of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non -03 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 15.9 Acres Permitted: 15.9 Site #: DP5 Field 9: 32.37 FcC2 DP5 Residual Analysis Data (Heavy Metals and Total Phosphorus use m2/k2. 1/0 Solids use Raw Percent 91: Sample or Coin- posite Date 11 1/9/17 21 31 4i 5i 6i 7? 8 jJ 101 M 11 j 12 % Solids 10.78 Arsenic 4.54 CadlnlLlnl 2 Copper 70.7 hroniiuii 32.3 Lead 5.5 Mercuni 0.4 Molyb- denunl Nickel 13.2 SCIC1141111 5 Zinc 87.4 Total Pllos- 11ortis 8860 Annual heavy lvletal rlela Loadln2s (calculated in Ibs/acrel: Total 1.....' ?.. 3 4. ....5. 3 6... a... 11 8.. 9...! 1_. �..�....i 1?...' DT/Ac./ f o App. V �_ Evcnt 2.04 Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadiniuni 0.008 0.000 0.0()0 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 j 0.008 Copper 0.288 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.288 C111-oniiiiiii 0.132 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.132 Lead 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Mercun 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb dciniin 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Nickel 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.054 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 0.356 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.356 Total Plios- 36.078 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 36.078 horus 36,, l q eerily, unuer penalty of law, mat tors aocument was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier -0,2 aotA Date ,€ )9 tl- DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ00 31725 Cation .Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 5.5 Acres Permitted: 5.5 V Site #: DP6 Field #: 10.15 FcC2 DP6 v Residual Analysis Data (Heavy Metals and Total Phosphorus use m-a/kg, 0/0 Solids use Raw Percent #): Sample or Com- posite Date 1' 1/9/17 2 3; 4 5 6 7! 8j 9j 101 111 1211 `%, Solids 10.78 Arsenic 4.4 Cadinhirn 2 Copper" 70.7 Chroiniuni 32.3 Lead 5.5 Mercury 0.4 Molyb- denunl Nickel 13.2 Selenium 5 Zinc 87.4 Total Phos- bonus 8860 Annual Heavy lvletal Pield Loadings (Calculated in lbs/acre): Total 2.. 3 4...i 5_ g 7i 8'':. 9 10j 11 12? DT/Ac./ . .., _.......... o App. Evcnt 1.85 Arsenic 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Cadmium 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Copper 0.261 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.261 c1ii-011141111 0.119 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.119 Lead 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Mercury 0.001. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Mol}?b- 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 denunl Nickel 0.049 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.049 Selenium 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0.18 zinc 0.323 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.323 Total Phos- 32.693 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 32.693 horns 3z?�2 i cercuy, unuer penany or iaw, inat ims aocmnent was preparea unaer my au-ection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Alyplier Vas-aolg Date J v v ;tad V DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM" Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter .Healthcare Total Dry Tons Applied (Annual): 8.62 Permit #: WQ0031725 Cation Exchange Capacity (non 5503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcC2 Acres Used: 4.4 Acres Permitted: 4.4 ✓ Site #: DP7 ✓ Field #: DP7 Residual Analysis Data (.Heavy Metals and Total Phosphorus use m2/Ic2, %► Solids use Raw :Percent #): Salllple or Coin- poslte Date 1 1./9/17 21 3 I 4 j 5 6 7 1 8' 9 j 10 11 12 % Solids 10.78 Arsenic 4.54 Cadnliuni 2 Copper 70.7 hromiun 32.3 Lead 5.5 Mercurn,, 0.4 Molyb- denum Nickel 13.2 ScleniLlIll 5 Zinc 87.4 Total Pllos- bonus 8860 Alltlual Heavv lvletal View Loaclin2s ((Alculated III Ibs/acre): Total _1.... _2_.1 _3... 4 ' ....... 6._! 8_s' 9 10 ' 11 i 12 DT/Ac./ / c App. Event 1.96 " Arsenic 0.018 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.018 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.277 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.277 Chroil-iiiiiii 0.127 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.127 Lead 0.022 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.022 Mercury- 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 MolN b- 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 denum Nickel 0.052 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.052 Selenium 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 0.342 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.342 Total Pllos- 34.71.3 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 34.713 horns 7,51 I ceru,y, uuuer penalty or law, gnat tins aocument was prepares unaer my alrectlon or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I and aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". I V 1/ Signature of Lan Applier Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: ]Baxter Healthcare WQ Permit #: WQ0031725 Field #: DPI -A ✓ Acres Utilized: 1,j Land Owner: IDou�las Poplin Annual Dry Tons Applied: 11.001 5 Site #: DPI -A Acres Permitted: 5.5 Operator: Douglas Poplin Crop 1 Name: Fescue Predominant Soil Series: FCC2 I/ Crop 1 Max. PAN: 158 >,./ Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: `' o QLiquid Volume applied (enter one) Solids,' Cu. Yds Gallons g Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPI:)I S'i_ WQr. Fort._ Animal Waste. etc) Soil Cond. (r.)»;. Wet Moist) Precip. Past 24 Hrs. inches > ^ _ o u o - o - is ° N = = ° TKN m /k 9 9 Z _ qQ c m /k g kgmg/kg Nitrate and Nitrite PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 P Cro P'- Crop I P Crop P 2 8-2017 91.51 10.78 1.511 , WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 82.047 NA Fescue 9-2017 29.67 10.78 0.490 V WQ0031725 dry 0 s 0.5 0.3 84400 9180 2.72 26.602 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS] 121.18 o As Cd Cu Cr Pb Hg Mo Ni Se Zn I P 108.6491 0.000 Lime Applied Annuallbs/acre 0.018 0.008 0.283 0.129 0.022 0.002 0.020 0.053 0.020 0.350 35.440 v Date Ibs/ac Prior Years Cumulative lbs/ac 0.12 0.034 2.076 1.371 0.186 0.005 0.08 0.484 0.064 3.799 Current Cumulative lbs/ac 0.138 0.042 V 2.359 1.500 0.208 0.007✓ 0.100 0.537 ' 0.084 4.149 Permitted C. P. L. R.**** 36 34 1338 NA 267 15 1 NA 374 89 2498 Pen -lilt PAN Limit 1st/2nd Crop 1 1.58 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier I -)a-an Date Application Method: S - Surface, IN - Injection, INC - Incorporation ""Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 " *"C.P.L.R.: Cumulative Pollutant Loading Rate DENR• FORM FSF (1212006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. f Facilitv Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1. Name: Fescue WQ Permit #: WQ003172-5 Field #: DP1-13 Annual Dry Tons Applied: 3.2329 Site #: DPI-13 Predominant Soil Series: FCC2 Crop 1 Max. PAN: 158 J Crop 2 Name: Acres Utilized: 1.6 Acres Permitted: 1.6 Cation Exchange Capacity (non -503): Crop 2 Max. PAN: o w o Q Volume applied (enter one) Solids. Liquid Cu. Yds Gallons % Solids Volume Applied per Acre D Tons/Ac (Dry ) Residual Sources (NPDF-S 4.1 WQ/=. Fert._ Animal Waste, etc) Soil Coed. (DrY, Wet, Moist) Preci p Past 24 Hrs. inches D = o y < ° c - :x ° K. - = ° TKN m /k 9 9 z ° m /k 9 9 Nitrate and Nitrite mg/kg PAN Applied (lbs sere) Name of CropType } Receivin- Residual Application Cro I p Cro p- Crop 1 p Crop 2 1 9-2017 35.61 10.78 2.021 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 109.752 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 (.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOT.US: 35.611 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 109.7521 0.000 Lime Applied Amluallbs/acre 0.018 0.008 0.286 0.131 0.022 0.002 0.020 0.053 0.020 0.353 35.812 Date lbs/ac Prior Years Cumulative lbs/ac 0.118 0.032 1.932 1.244 0.17 0.005 0.074 0.444 0.061 3.48 Current Cumulative lbs/ac 0.136 t/ 0.040 . 1218 1.375 0.192 0.007v 0.094 0.497 - 0.081 3.833 Permitted C. P. L. R.**** 36 34 1338 NA 267 15 NA 374 89 2498 Pemiit PAN Limit 1st/2nd Crop 1 158 "I certif}, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature ol'Land Applier 1 2-a o Date *Application Method: S - Surface, IN - Injection, INC - Incorporation ^''Volatilization Rate: Surface - 0.5, Injection/.Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially di„ested -0.2, aerobically digested -0.3, raw sludhe -0.4 *"C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Baxter Healthcare Land Oivner: Douglas Poplin Operator: Douglas Poplin Crop 1. Name: Fescue ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. C� Acres Utilized: 3 v WQ Permit#: WQ003172i Field #: DPI-C Annual Dry Tons Applied: 6.4658 Site #: DP1-C Acres Permitted: 3 Predominant Soil Series: FCC2 Cation Exchange Capacity (non 503): Crop I Max. PAN: 158 r-/ Crop 2 Name: Crop 2 Max. PAN: o r o Q � Volume applied (enter one) Solids Liquid Cu. Yds Gallons g Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (N1'DI S '" WQ:=. Fert.. Animal _ Wade. etc)Wet. Soil Cond. (Dn: Moisl) Precip. Past 24 I lrs. inches D r 2- = -. o• o - c ?" o. N G = * o I KN mg/kg Z = d m' o = " mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 9-2017 71.22 10.78 2.155 ✓ WQ0031725 dry- 0 S 0.5 0.3 84400 1 9180 2.72 117.069 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 71.22 o As Cd Cu Cr Pb Ho, Mo Ni Se Zn P 1 17.069 0.000 Lime Applied Annuallbs/acre 0.020 0.009 0.305 0.139 0.024 0.002 0.022 0.057 0.022 0377 38.187 ✓ Date lbs/ac Prior Years Cumulative lbs/ac 0.697 0.045 2.584 1.611 0.219 0.007 0.096 0.581 0.078 4.87 1 1-17 1000 Current Cumulative lbs/ac 0.717 v 0.054 2.889 1.750 0.243 0.009 v 0.118 ' 0.638 ' 0.100' 5.247 Permitted C. P. L. R.* * 36 34 1338 1 NA 1 267 15 1 NA 374 89 2498 Permit PAN Limit I st/2nd Crop I.S8 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for ImoNving violations." // Signature of Land Applier •1 Application Method: S - Surface, IN - Injection, INC - Incorporation - 4.101$ ,"-."Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date * * * Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobicalh digested -0.3, raw sludge -0. I "C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. V/ Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: DPI-D Acres Utilized: 9.6 Land Owner: Douglas Poplin Annual Dry Tons Applied: 17.4591 v/ Site #: DPI-D Acres Permitted: 9.6 Operator: Douglas Poplin Predominant Soil Series: FCC2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Crop 2 Name: Crop 2 Max. PAN: O cs o Ca Volume applied one) Solids/ Liquid Cu. Yds Gallons o,� Solids VOIUnIe Applied per Acre (Dry Tons/Ac) Residual Sources (NPD1=S 4WQ:�. Fert.. Animal Waste. etc) Soil Cond (Dry, Wet, Moist) Precip. Past 24 Hrs. inches D J o C O' - x �� _ F = # * o _ TKN mg/kg z mglkg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Na me of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 12-17 1 192.31 10.78 1.819 WQ0031725 dry 0 S 0.5 1 0.3 84400 9180 1 2.72 98.785 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0oo Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 192.311 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 98.785 0.000 Lime Applied Annuallbs/acre 0.017 0.118 0.135 ✓ 36 0.007 0.032 0.039 34 0.257 1.937 2.194 V 1338 0.118 1.26 1.378 NA 0.020 0.194 0.214 If 267 0.001 0.004 0.005 v 15 0.018 0.074 0.092 1 NA 0.048 0.432 0.480 374 0.018 0.048 0.066 ` 89 0.318 3.315 3.633 2498 32.233 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R-**** Permit PAN Limit I st/2nd Crop 1�8 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier I-ad-2 Date "Application Method: S - Surface, IN - Injection, INC - Incorporation Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, rasludge -0.4w ;:*'.,C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM D P 3 --�; - l�',(0'q-c- Q--(. PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: DP3-Corn Acres Utilized: -5,g77 Land O«vner: Douglas Poplin Annual Dry Tons Applied: 12.0610 ✓ Site #: DP3-Corn Acres Permitted: 5.877 Operator: Douglas Poplin Predominant Soil Series: FcB2 Cation Exchange Capacity (non 503): Crop 1. Name: Com-Silage Crop .1 Max. PAN: 214 Crop 2 Name: Crop 2 Max. PAN: o w f Q Volume applied (enter one) Solids," Liquid Cu. Yds Gallons g1 Solids Volume Applied per Acre D Tons/Ac (Dry ) Residual Sources (NPI:)13S i. WQi=, Fert._ Animal Waste. ete) Soil Cond. (Dry. Mold Precip. Past 24 I-Irs. inches C T o _ * ° C-,R # 2 TKN m /k 9 9 fz c = d bo o `-' y m /k 9 9 Nitrate and Nitrite m /k 9 9 PAN Applied PP (lbs%acre) Name or Crop Type Receiving Residual Application Crop I Crop 2 Crop I Crop 2 3-2017 52.72 10.78 0.814 V WQ0031723 dry 0 Inc. 1 0.3 84400 9180 2.72 - 51.713 NA Corn 4-2017 80.13 10.78 1.238 W00031725 dry 0 Ina 1 0.3 84400 9180 2.72 78.599 NA Corn 0.000 0.000 0.000 0.000 0.000 0.0()0 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOT:-U,sl 132.s5 0 As Cd Cu Cr Pb R9, Mo Ni Se Zn P 130.31 1 0.000 Lime Applied Annuallbs/acre 0.019 0.344 0.363 36 0.008 0.105 0.1 13. 34 0.290 0.5893 0.879 1338 0.133 3.957 4.090 NA 0.023 0.523 0.546 X 267 0.002 0.015 0.017 L 15 0.021 0.215 '0.236, NA 0.054 1.214 1.268 374 0.021 0.515 0.536 L, 89 0.359 12.264 12.623 2498 36.361 V Date lbs/ac Prior Years Cumulative lbs/ac 1 1-17 1000 Current Cumulative lbs/ac Permitted C. P. L. R_**** Permit PAN Limit 1 st/2nd Crop 214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Application Method: S - Surface, IN - .Injection, INC - Incorporation "aJ 0t8 `Volatilization Rate: Surface - 0.5,1njection/.Incorporation - 1.0 Date Y"" Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobicalh ditiested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter I lealthcare. Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit#: WQ0031725 Field #: DP3-Grass Annual Dry Tons Applied: 23.6525 J Site 9: DP3-Grass Predominant Soil Series: FcB2 Crop I Max. PAN: 194 Crop 2 Name: Acres Utilized: 6.983 Acres Permitted: 6.983 Cation Exchange Capacity (non -03): Crop 2 Max. PAN: o c� o � Volume a i died 1 1 (enter one) Solids' Liquid 9 Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPi:)ES . \./Q Fert._ Animal Waste. etc ) Soil Cond. (D�y Wet. Moist) Precip. , Fast 24 I1rs. inches D 0 = _ .� o, < _ = �. _ N - Cc x. �• * � ° TKN mglkg Z > _ -- _ 8 ~. -' mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs%acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1-2017 3.6 10.78 0.047 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 2.542 NA Fescue 2-2017 138.23 10.78 1.797 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 97.61 e NA Fescue -2017 118.7 10.78 1.543 WQ0031725 dr. 0 S 0.5 0.3 84400 9180 2.72 83.824 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 260.�3t 0 As Cd Cu Cr Pb H Mo Ni Se Zn P 183,982 0.000 Lime Applied Annual lbs/acre 0.031 ✓ 0.014 0.479 0.219 0.037 0.003 0.034. 0.089 0.034 0.592 60.018 S/ Date lbs/ac Prior Years Cumulative lbs/ac 0.32 0.351 36 0.103 0.1 17 t, 34 5.716 6.195 1 1338 1 3.776 3.995 NA 1 0.499 0.536 267 1 0.014 0.017 15 1 0.208 ` 0.242 NA 1 1.159 - / 1.248 374 0.511 0.545v 8 13498 11.992 12.584 V 1 1-17 1000 Current Cumulative Ibs/ac Permitted C. P. L. R.**** Permit PAN Limit i st/2nd Crop I t94 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." Signature o'f Land Applier Date "Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0-5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost-0.1, anacrobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 •* **C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: DP4 ✓ Acres Utilized: 8 7 Land Otvner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue Annual Dry Tons Applied: 22.0148 Site #: DP4 Predominant Soil Series: FCB2 Crop I Max. PAN: 194 "' Crop 2 Name: Acres Permitted: 8.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Volume applied (enter one) Solids' Liquid Cu. Yds Gallons Solids Volume Applied ier t Acre (Dry Tons/Ac) Residual Sources (NPDES i. WQ/ , Fert.. Animal Wastc. etc) Soil Cond. Wet(Dry. Moist) Preci i , last _-'4 Hrs. inches F. ? �' < � = o' ` � # c' 0 fICN mg/kg Z _ o � (JoQ mg/kg Nitrate and Nitrite mg/kg PAN Applied Name of Cro 1-` e P . P Receiving Residual Application Crop 1 Crop _ Crop I Crop _ 3-2017 1 50.18 10.78 0.524 WQ0031725 do U S 0.5 0.3 84400 9180 2.72 28.443 NA Fescue 5-2017 85.02 10.78 0.887 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 48.190 NA Fescue 6-2017 107.29 10.78 1.120 WQ0031725 dry- 0 S 0.5 0.3 84400 9180 2.72 60.813 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0, oo-- 0.000 0.000 (7,3 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 242.49 0 As Cd Cu Cr Pb H g Mo Ni Se Zn P 137.4471 0.000 Litne Applied A umal lbs/acre 0.023 ✓ 0.245 0.?68 ✓ 36 0.010 0.073 0.083 34 0.358 4.093 ' 4451 1 1338 1 0.164 2.811 2.975 NA 0.028 0.349 0.377 t, 1 267 0.002 (.1.Q1 1 0.013 15 0.025 0.151 0.176 V NA 0.067 0.956 1.02'3 374 0.025 0.098 0.1?3 89 0.442 8.639 9.081� 2498 44.849 ✓ ✓ Date lbs/ac Prior Years Cumulative lbs/ac 11-17 2000 Current Cumulative Ibs/ac Permitted C. P. L. R.**** Penuit PAN Limit 1st/2nd Crop F 194 "I certify under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier NO- 070 Date *Application Method: S - Surface, IN - injection, INC - Incorporation ""Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 * Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, ravv sludge -0.4 **"C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM. PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit 4: WQ0031725 Field #: DPj Acres Utilized: 15.9 Land Ovvner: Douglas Poplin Annual Dry Tons Applied: 32.3717 ✓ Site th DP5 Acres Permitted: 15.9 Operator: Douglas Poplin Predominant Soil Series: FCC2 Cation Exchange Capacity (non 503): Crop I Name: Fescue Crop .1 Max. PAN: 158 V Crop 2 Name: Crop 2 Max. PAN: o cs o V011mle applied (enter one) Solids Liquid Cu. Yds Gallons g, Solids Volume Applied per Acre (Dry Tons/Ac) Residua] Sources (NPI:>L S ft, W(� Fert._ Animal Waste. etc) Cond. (Dry. Moist) Prccip. fast 24 Ilrs. inches > �. c - z n = - � - x• �. ° * �' ° TKN mg/kg Z � _ = 3 =_ mg/kg Nitrate and Nitrite mglkg PAN Applied (lbs/acre) Name of Crop Type Receivma Residual " Application Crop l Crop 2 Crop 1 Crop 2 7-2017 1 215.57 1 10.78 1.231 WQ0031725 dry 0 S 0.5 1 0.3 84400 1 9180 2.72 66.858 NA Fescue 11-2017 141 10.78 0.805 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 43.730L• NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 -U.000 0.000 0.000 2.OV4 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ro'r:v s: 356.571 0 _�As ' Cd Cu Cr Pb Hg Mo Ni Se Zn P 110.588 r 0.000 Lime Applied Annuallbs/acre 0.018 V 0.217 ✓0.235 36 0.008 0.062 0.070 V 34 0.288 3.49 3.778 1 1338 0.132 2.308 2.440 NA 0.022 0.316 0.338 t, 1 267 1 0.002 0.01 0.013 15 0.020 0.13, 0.150V NA 0.054 0.822 0.876" 1 374 0.020 0.075 0.095 89 0.356 7.42 7.776-� 2498 36.078 ✓ Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 158 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier t og�a Date `Application Method: S - Surface, IN - Injection, INC - Incorporation "Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 x x Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, ravv sludge -0.4 "C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. v.- Facility Name: Baxter Healthcare Land Werner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ003172i Field #: Annual Dry Tons Applied: 10.1490 '0"� Site #: Predominant Soil Series: FCC2 Crop I Max. PAN: 158 V, Crop 2 Name: DP6 D P 6 Acres Utilized: 1,j Acres Permitted: 5.5 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: c� p VOIUme a) )lied 1 I (enter one) Solids.;g Liquid Cu. Yds Gallons a Solids Volume Applied per Acre (Dry Tons/Ac)� Residual Sources (NPI:)13S 4. WQ%, Fen - Animal Waste- etc) Soil COed• Wet, Moist) Precip. Past 14rs. inches > T w o- o' o o - x x a %� = = N r 2 TKN mg/kg z _ r ° ^. mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop 7 ypc Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 10-2017 111.79 10.78 1.845 '� WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 100.23&- NA Fescue 0.000 0.006 o.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): Tol"ALS 111.791 o As Cd Cu Cr Pb H- Mo Ni Se Zn P 100.2301 Lime Applied Annuallbs/acre 0.017 0.007 0.261• 0.119 0.020 0.001 0.018 0.049 0.018 0.323 32.693 10 Date Ibs/ac Prior Years Cumulative lbs/ac 0.31 0.09 5.112 3.563 0.477 0.013 0.189 0979 0.094 Current Cumulative lbs/ac 0.327 ✓ 0.097 • 5.373•' 3.682 0.497 " 0.014,- 0 207" 1.028 ` 0.1 12 10.868 Penmitted C. P. L. R.**** 36 34 1 1338 NA 267 15 1 NA 374 89 2498 Pen -nit PAN Limit 1st/2nd Crop 1 158 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations." ignature of Land Applier %-j rd- cl o Date 'Application Method: S - Surface, IN - Injection, INC - Incorporation '."'.`Volatilization Rate: Surface - 0.5,Injection/Incorporation - 1.0 - Mineralization Rates: Compost -0.1, anaerobially digested -0.2, acrobically digested -0.3, raw.sludge -0.4 ""C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLiCATI.ON FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORMTO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" 1N A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter I lealtheare• Land Owner: Dou,las Poplin Operator: Douglas Poplin Crop I Name: Fescue WQ Permit #: WQ0031725 Field #: DP7 Annual Dry Tons Applied: 8.6211 Site #: DP7 �✓` Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503): Crop I Max. PAN: 158 V Crop 2 Name: Crop 2 Max. PAN: Acres Utilized: 4.4 Acres Permitted: 4.4 w o c� Ca VOILmI@ applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per pF t Acre (Dry Tons/Ac) Residual Sources (NPI)];S t, \hQ#. F erL_ Animal Waste, etc Soil Cond. (l:hy, Wet; Moist) Precip. , Past 24 Hrs. inches .y c _ a 2 o , c c - v' * _ c * E- � �' # o TKN mg/kg Z ° = � mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name. of Crop Type Receiving Residual Application Crop 1 Ca•op 2 Crop 1 Crop 2 8-2017 94.96 10.78 1.959 WQ0031725 dry 0 S 0.5 0.3 84400 9180 2.72 106.426r NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 omo 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): rO'r:aLs: 94.961 (T As Cd Cu Cr Pb Hg Mo Ni Se Zn F 106.426 0.000 Lime Applied Amorallbs/acre 0.018 0.008 0.277 0.127 0.022 0.002 0.020 0.052 0.020 0.342 34.713 Date lbs/ac Prior Years Cumulative lbs/ac 0.249 4?67 36 0.067 0.075 34 3.891 4.168 1338 2.613 2.740 NA 0.356 0.378 V 267 0.011 0.013 15 0.146 r 0. 166V NA 0926 0.978 374 0.089 0.1.09. 89 7.97. 8.312 2498 1V 11-17 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 st/2nd Crop 1.58 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier k aq-dol Date "Application Method:- S - Surface, IN - Injection, INC - Incorporation *Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 -***C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) 112U12018 Nutrient Madagement in North Carolina Realistic Yields for FcB2e Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded in !Wilkes County Crop Yiel Barley (Grain) 67 Bush Is Corn (Grain) ...................................................................................................................................................................................................................................... 129 Bushels Corn (Silage) 19.6 To Cotton 637 Pourids Sorghum (Silage) 16,7 Ton Oats (Grain) 83 Bushels Peanuts 0 Pound Rye (Grain) 49 Bushels Small Grain (Silage) 8.8 Tons Sorghum (Grain) ...................................................................................................................................................................................................................................... 49 CWT Soybeans (Double Cropped) ...................................................................................................................................................................................................................................... 33 Bushels Soybeans (Full Season) ...................................................................................................................................................................................................................................... 39 Bushels Soybeans (Double Cropped - Manured) ........................................................................................................................................................................................... 33 Bushels Soybeans (Full Season - Manured) ............................. ................. ............ ................. ............................... ..................... ....................................................... ........................................... ... 39 Bushels Tobacco (Burley) ............................................................................................................................................................................................................................... ................................. .I........... 0 Pound Tobacco (Flue Cured) ..................................................................................................................................................................................................................................... 2548 Po nds Triticale (Grain) ....................................................................................................................................................................................... 69 Bushels Tropical Corn (Silage) .............................................................................................................................................................................................--.............. ........................................... 19.6 Ton Wheat (Grain) .................. ................................................................................................... ....................... .......................... I................... 49 Bushels Bahiagrass (Hay) _............................. ....... 3A Tons ...... Caucasion/Old World Bluestem (Hay) 3A Tons Common Bermudagrass (Hay) 3.4 Tons Dallisgrass (Hay) 3.4 Tons Fescue (Hay) 4.4 Tons Hybrid Bermudagrass (Hay) 4.4 Tons Hybrid Bermudagrass overseeded with Rescuegrass 0 Tons (Hay) Mixed Cool Season Grass (Hay) 3.2 Tons Orchardgrass (Hay) 3.4 Tons Pearl Millet (Hay) 3.7 Tons Rescuegrass (Hay) 0 Tons Sorghum Sudan (Hay) 4.2 Tons Timothv Grass Realistic Nitrogen Rate (Ibs/acre) 99 119 Estimated Phosphorus Removal (Ibs P205/acre) 25 57 10.9 214 67 0.081 52 18 7.6 127 50 1.13 94 21 0 0 0 2.01 98 16 11.1 98 48 1.72 ......................................................................................................................................................... 84 37 0 ......................................................................................................................................................... 0 27 0 ......................................................................................................................................................... 0 31 3.89 ......................................................................................................................................................... 130 27 3.89 ......................................................................................................................................................... 152 31 0.074 ............................................................................................................................................... 0 0 0.029 ................................................................................................................................................. 74 13 1,52 ....................................................................................................................................................... 104 23 6.5 .....-.............. .............. 127 ... ................................................ ................. 67 ............................................ 2.01 ......................................................................................................................................................... 98 25 44 151 39 44 151 41 44 151 42 44 151 45 44 194 69 44 194 54 44 0 0 44 140 44 151 49 180 44 0 49 204 0 Tons 44 0 I:)r. -David Crouse is responsible for the development and mainter}ance of the Realistic Yield reporting tool. 45 50 49 0 58 0 http://yields.sail.ncsu.edulindox.php#county 12/2 "U'LU/Zu1 d Nutrient M4, agement in North Carolina Realistic fields for FcC2a Fairview san moderately eroded in Wilkes County clay loam, 8 to 15 percent slopes, Realistic Estimated Phosphorus Nitrogen Nitrogen Removal Crop Yiel I Factor Rate (Ibs/acre) (Ibs P205/acre) Barley (Grain) . ................................ .............................................. _.................................... ...................................................................... 54 Bush . ............................ Is 1,49 81 21 Corn (Grain) .................................................................................................................................................................................................................................................................................................................................................................................................................................................. 106 Bus .............. ... iels ............. .................... ......... 0.92 ........................................................ ....... 97 ........................................................ :............................................... . 46 Corn (Silage) 16 Tons 10.9 174 54 Cotton 520 Pou ids 0.081 42 15 Sorghum (Silage) 13.6 Tor s 7.6 103 41 Oats (Grain) 68 Bushels 1.13 77 17 Peanuts 0 Pounds 0 0 0 Rye (Grain) 40 Bushels 2.01 80 13 Small Grain (Silage) 7.2 Tons 11.1 80 39 Sorghum (Grain) ........................................................................................................................................................................................................................................................................................................................................................................................................................................................ 40 CWTJ 1.72 69 30 Soybeans (Double Cropped) ................................................................................................................................................................................................................ 27 Bush ds 0 0 22 Soybeans (Full Season) ........................................................................................................................................................................................................................................................................................................................................................................................................................................... 32 Bush Is 0 0 26 Soybeans (Double Cropped - Manured) ................... ..................... ....................................................................................................................... 27 Bush .Is 3.89 106 22 ........... ................. Soybeans(Full Season - Manured) ............................. .............. . ................................... ....... ........... ............................................ :............................................................................................... ...... ............ . ............................................................................................................................................................................................................................................................................................................................. 32 Bush Is 3.89 124 26 Tobacco(Burley) ............................. ............................................ ........... .................. .......................... -........................................................ 0 Pound .............................. ............. .... 0.074 .................. 0 ........................................................... 0 Tobacco (Flue . . .Flue . Cured) ...................................................................................................................................................................... 2080 Po ................................................................................................................................................................................................................................ nds . ................................. 0.029 ..................................... ......... ....................................................... 60 ......................................................... 10 Triticale (Grain) ............................................................................................................................................................................._......................................................................................................................................................................................................................................................................... 56 Bush Is 1.52 85 i9. Tropical Corn (Silage) .......................................................................................................................................................................................................... 16 Tons . 6.5 104 54 Wheat (Grain) 40 Bush .................................. Is 2.01 80 20 Bahiagrass (Hay) 2.8 Tons 44 123 32 Caucasion/Old World Bluestein (Hay) 2.8 Tons 44 123 33 Common Bermudagrass (Hay) 2,8 Tons 44 123 34 Dallisgrass (Hay) 2.8 Tons 44 123 37 Fescue (Hay) 3.6 Tons 44 158 57 Hybrid Bermudagrass (Hay) 3.6 Tons 44 158 44 Hybrid Bermudagrass overseeded with Rescuegrass 0 Tons 44 0 (Hay) 0 Mixed Cool Season Grass (Hay) 2.6 Tons 44 114 37 Orchardgrass (Hay) 2,8 Tons 44 123 41 Pearl Millet (Hay) 3 Tons 49 147 40 Rescuegrass (Hay) 0 Tons 44 0 0 Sorghum Sudan (Hay) ................................................................................................................................................................................................... 3.4 Tons . 49 167 47 Timothy Grass (Hay) 0 Tons 44 0 0 Dr. David Grouse is responsible for the development and maintenance of the Realistic Yield reporting tool. hftp://yields.soil.ncsu.edLVindex.php#county 212 Page: 2 of 2 Report Number: 17-012-0208 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number: 61653 Sample Id : Baxter ,ma's sue. �: Waypoint''. r�rANALYTICAL I Project: Baxter NC Cert #257 REPORT OFANAL-YSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/9/2017 12:30:00 / Date Received: 01/12/2017 00:00 Date Reported: 01/19/2017 Total Cadmium <2.00 2.00 JTR 01/16/2017 20:03 6010C Total Chromium 32.3 5.00 JTR 01/16/2017 20:03 6010C Total Nickel 13.2 5.00 JTR 01/16/2017 20:03 6010C t Total Arsenic 4.54 3.00 JTR 01/16/2017 20:03 6010C Total Mercury <0.400 0.400 JM 01/18/2017 09:00 SW-7471 B Total Selenium <5.00 5.00 JTR 01/1612017.20:03 6010C pH (Standard Units) 7.60 1.00 SJB 1�0312017 09:30 SW-9045D Total Molybdenum <5.00 5.00 JTR 01/16/2017 20:03 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. I 151E'q- ®,k �Wpb All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clienis. and may not be reproduced in whole or part, nor may any reference be made 9&UMM to the work, the results. or the cornpany in any advertising, news release, or oL4er public announcements without obtair;ing our prior v✓r,tten authorization. Debbie Holt Laboratory Supervisor Page: 1 of 2 Report Number: 17-012-0208 Account Number: 46381 Send To: Southern Soil Builders Dennis Key 958 Hoots Road Roaring River, NC 28669 Lab Number: 61653 Sample Id : Baxter Ore Project : Baxter NC Cert #257 REPORT OFANALIYSIS 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com Date Sampled: 1/9/2017 12:30:00 Date Received: 01/12/2017 00:00 Date Reported: 01/19/2017 Total Solids" 10.78 107800 100.0 R D 01/12/2017 15:30 SM-2540G Moisture ` 89.21 100.0 R D 01/12/2017 15:30 SM-254OG Total Kjeldahl Nitrogen 8.44 84400 10.0 SJB 01/16/2017 10:25 SM-4500-NH3C-TKN TdiarPhospITOrus R O tt16/20 r Total Potassium 0.24 2370 1000 JTR 01/16/2017 20:08 6010C Total Sulfur 0.79 7900 100 JTR 01/16/2017 20:03 6010C Total Calcium 0.71 7050 -100 JTR 01/16/2017 20:03 6010C Total Magnesium 0.24 2390 100 JTR 01/16/2017 20:03 6010C Total Sodium 0.24 2370 100 JTR 01/16/2017 20:03 6010C Total Iron 3630 100 JTR 01/16/2017 20:03 6010C Total Aluminum 1130 100 JTR 01/16/2017 20:03 6010C Total Manganese 36.6 5.00 JTR 01/16/2017 20:03 6010C Total Copper 70.7 5.00 JTR 01/16/2017 20:03 6010C Total Zinc 87.4 5.00 JTR 01/16/2017 20:03 6010C Ammonia Nitrogen 0.92 9180 10.0 SJB 01/13/2017 09:30 SM-4500-NI3C Organic N 7.52 75220 10.0 01/13/2017 09:30 CALCULATION Nitrate+Nitrite-N <2.72 2.72 SJB 01/13/201713:45 4500NO3F-2011 All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part, nor .may any reference be made A,m dg to the work, the results. or the company in any advertising, new. s re?ease, or other public announcements without obtaining our prior written authorization. Debbie Holt Laboratory Supervisor Mineralization as decimal JTotal dry JAcres PAN Surface 114.7456libs PAN/acre PAN Injection 134A318311bs PAN/acre mg/kgx.002 =|bs/dryton MR(TKN'NH3)+1(NH3)+NO3+NO2 =mO/kg mg/kg x.002 =Ibs/dry ton Dry Tm sMUOO gal. 20000,4,49526 1st year PAN |ba./acre Surface|bs. Surface 1styear PAN |bs./aonu Injected lbs. Injected ` -` SAR 1'`1-' Vle Sodium Absorption Ratio Na(M Ca'Mc/L MgCMcj/Li Na : Sodium (Mg/L) Equivalent weight: 23 255.486 1 759.99 257.642 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 n' 'mg Cd [Via (ME) 11,10809 7.9995 21.47017 Milli Equivalent = Mg/L / Equivalent weight The amour amount of SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power tI Permitting SAR = 2,0317073 (From, cult;,/i_. entered < bov(:;) SA = 2.037589 (Pro€n ME onterod Naov�) Na ME 1 Ca (ME) Mg (ME) 1 11.11 37.99 21.47 Analytical Re#ults Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/09/2017 Reported: 01 /30/2017 For: Baxter Comments: Sample Number Parameter Sample ID Result 170109-08-01 Corrosivity 170109-08-01 Ignitability 170109-08-01 Reactivity 170109-08-01 TCLP Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Baxter See Baxter See Baxter See Baxter See Unit Method Analyzed Analyst SW-84s 1010M sw-846 as Noted 01/27/2017 PACE 01/27/2017 PACE 01/27/2017 PACE 01/27/2017 PACE PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 1 aceAnalytrcal www.pacelabacom ANAL Project: 170109-08 Pace Project No.; 92325878 RESULTS Pace Analytical Services, LLC 9800 Kincey Ave, Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 170109-08 Lab ID: 92325878001 Collected: 01/09/17 12:30 Received: 01/11/17 08:30 Matrix: Water Parameters Results Units Rellort Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor Heptachlor epoxide Methoxychlor Toxaphene Surrogates ` Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 8082 'G CS PC8 PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) PCB-1232 (Aroclor 1232) PCB-1242 (Aroclor 1242) PCB-1248 (Aroclor 1248) PCB-1254 (Aroclor 1254) PCB-1260 (Aroclor 1260) Surrogates Decachlorobiphenyl (S) 8151 Chlorinate Herbicide TCLP 2,4-D 2,4,5-TP (Silvex) Surrogates 2,4-DCAA (S) 6010 MET ICP, TCLP Arsenic Barium Cadmium Chromium Lead Selenium Silver 7470 Mercury, TCLP Mercury 8270 MSSV TCLP Sep Funnel 1,4-Dichlorobenzene Date: 01/27/2017 06:48 PM Analytical Method: EPA8081 Prep,, Leachate Method/Date: EPA 1311; ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 74 % 61 % Analytical 'Method: -EPA 8082 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 25 % Analytical Method: EPA 8151 ND mg/L ND mg/L 92 % Analytical Method: EPA6010 Preps Leachate Method/Date: EPA 1311; ND mg/L ND mg/L ND mg/L ND mg/L ND mg/L ND mg/L ND mg/L Analytical Method: EPA7470 Preps -Leachate Method/Date: EPA 1311•; f ND mg/L Analytical Method: EPA 8270 Preps Leachate Method/Date: EPA 1311; ND ug/L REPORT OF LABC This report shall not be without the written consent a ration Method: EPA3510 1/21117 14:00 2.5 5 01/23/17 13:11 01/26/17 04:24 58-89-9 , 15:0 5 01/23/17 13:11 01/26/17 04:24 57-74-9 2.5 5 01/23/17 13:11 01/26/17 04:24 72-20-8 2.5 5 01/23/17 13:11 01/26/17 04:24 76-44-8 2.5 5 01/23/17 13:11 01/26/17 04:24 1024-57-3 5000. 5 01/23/17 13:11 01/26/17 04:24 72-43-5 .15..0 5 01/23/17 13:11 01/26/17 04:24 8001-35-2 10-138 5 01/23/17 13:11 01/26/17 04:24 2051-24-3 D3 10-110 5 01/23/17 13:11 01/26/17 04:24 877-09-8 ation -Method: EPA 3510 1 01/13/17 08:48 01/14/17 02:36 12674-11-2 1.0 1 01/13/17 08:48 01/14/17 02:36 11104-28-2 1.0 1 01/13/17 08:48 01/14/17 02:36 11141-16-5 1.0 1 01/13/17 08:48 01/14/17 02:36 53469-21-9 1.0 1 01/13/17 08:48 01/14/17 02:36 12672-29-6 1.0 1 01/13/17 08:48 01/14/17 02:36 11097-69-1 1.0 1 01/13/17 08:48 01/14/17 02:36 11096-82-5 10-132 1 01/13/17 08:48 01/14/17 02:36 2051-24-3 ation Method: EPA3510 0.010 1 01/24/17 22:55 01/27/17 07:34 94-75-7 L3, MO 0.010 1 01/24/17 22:55 01/27/17 07:34 93-72-1 39-139 1 01/24/17 22:55 01/27/17 07:34 19719-28-9 ation Method: EPA3010A /12/17 17:25 Initial pH: 6.9; Final pH: 6.9 0.050 1 01/13/1710:55 01114/1714:44 7440-38-2 0.25 1 01/13/1710:55 01/14/1714:44 7440-39-3 0.0050 1 01/13/1710:55 01/14/1714:44 7440-43-9 0.050 1 01/13/1710:55 01/14/1714:44 7440-47-3 0.025 1 01/13/1710:55 01/14/1714:44 7439-92-1 0.10 1 01/13/1710:55 01114/1714:44 7782-49-2 0.025 1 01/13/1710:55 01/14/1714:44 7440-22-4 ation Method: EPA7470 /12/17 17,25 -Initial pH: 6.9; -Final -pH: 6.5 0.QO020 1 01/13/1712:35 01/16/1711:52 7439-97-6 ation Method: EPA3510 /21/17 14:00 50.0 1 01123/1711:00 01/23/1717:53 106-46-7 TORY ANALYSIS educed, except in full, RAnalytical Services, LLC. Page 5 of 27 aceAnalytical wmpacelabs.com Project: 170109-08 Pace Project No.: 92325878 Sample: 170109-08 Parameters 8270 MSSV TCLP Sep Funnel 2,4-Dinitrotoluene Hexachloro-1, 3-butadiene Hexachlorobenzene Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2,4,5-Trichlorophenol 2,4,6-Trichlorophenol Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol(S) 2,4,6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene ANAL Lab ID: 92325878001 Results Units Rel Analytical Method: EPA 8270 Prep,, Leachate Method/Date: EPA 1311; ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L _ 106. ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 59 % 80 % 94 % 28 % 39 % 113 % Analytical Method: EPA8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L J`I ND ug/L Q� ND ug/L ND ug/L Vinyl chloride Surrogates , 1,2-Dichloroethane-d4 (S) Toluene-d8 S� yy 4=Bromofli%robenzene ) U 1010 Flash point,Closed -up Flashpont 9044, H_ v PH \90 aiaint Filter Liquid Test 1 Free Ligt3i s `\ Date: 01/27/2017 06:48 PM ND ug/L ND ug/L 98 % 106 % 98 % Analytical Method: EPA 1010 >200 deg F Analytical Method: EPA9040 6.7 Std. Units Analytical Method: EPA 9095 FAIL J Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 RESULTS 01/09/17 12:30 Received: 01/11/17 08:30 Matrix: Water )ort Limit DF Prepared Analyzed CAS No. iration Method: EPA3510 11/21/1714:00 50;0 1 01/23/1711:00 01/23/1717:53 121-14-2 60.0 1 01/23/1711:00 01/23/1717:53 87-68-3 50.0 1 01/23/1711:00 01/23/1717:53 118-74-1 50.0 1 01/23/1711:00 01/23/1717:53 67-72-1 50.0 1 01/23/1711:00 01/23/1717:53 95-48-7 50.0 1 01/23/1711:00 01/23/1717:53 50.0 1 01123/1711:00 01/23/1717:53 98-95-3 ,100, 1 01/23/1711:00 01123/1717:53 87-86-5 50.0 1 01123/1711:00 01/23/1717:53 110-86-1 50.0 1 01/23/1711:00 01/23/1717:53 95-95-4 50.0 1 01/23/1711:00 01/23/1717:53 88-06-2 M1 12-102 1 01/23/1711:00 01/23/1717:53 4165-60-0 13-107 1 01/23/1711:00 01/23/1717:53 321-60-8 21-132 1 01/23/1711:00 01/23/1717:53 1718-51-0 10-110 1 01/23/1711:00 01/23/1717:63 13127-88-3 10-110 1 01/23/1711:00 01/23/1717:53 367-12-4 27-108 1 01/23/1711:00 01/23/1717:53 118-79-6 SO ate Method/Date: EPA 1311; 01/12/17 09:30 100, 20 01/24/17 16:05 71-43-2 200 20 01124/1716:05 78-93-3 .100. 20 01/24/1716:05 56-23-5 100 20 01/24/1716:05 108-90-7 100 20 01/24/1716:05 67-66-3 100 20 01/24/1716:05 106-46-7 100 20 01/24/1716:05 107-06-2 100 20 01/24/1716:05 75-35-4 100 20 01/24/1716:05 127-18-4 100 20 01/24/1716:05 79-01-6 100 20 01/24/1716:05 75-01-4 70-130 20 67-135 20 70-130 20 70.0 1 0.10 1 1.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, LLC. 01 /24/17 16: 05 17060-07-0 01/24/1716:05 2037-26-5 01/24/1716:05 460-00-4 Qual 01/12/17 09:27 01/13/1715:09 �H6 01/17/1710:26 mil 6 Page 6 of 27 aceAnaIXieal www.pacelabacam ANAL Project: 170109-08 Pace Project No.: 92325878 RESULTS Pace Analytical Services, LLC 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 170109-08 Lab ID: 92325878001 Colle ed: 01/09/17 12:30 Received: 01/11/17 08:30 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Quaff 733C S Reactive Cyanide Analytical Method: EPA 9014 Pre aration Method: SW-846 7.3.3.2 Cyanide, Reactive ND mglkg 1.0 1 01/17/17 12:46 01/17/17 17:44 734S Reactive Sulfide Analytical' Method: SM4500S2F-0� Preparation Method: SW-846 7.3.4.2 Sulfide, Reactive ND mglkg 10 1 01/17/17 12:46 '01/17/1717:13 Date: 01/27/2017 06:48 PM REPORT OF LAB RATORY ANALYSIS This report shall not b reproduced,• except in full, without the written consent of Pace Analytical Services, LLC. Page 7 of 27 ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTIONFORM (02T Rules) Facility Name: Baxter Healthcare Corporation WQ Permit Number: WQ0031725 WWTP Name: Baxter Healthcare Corporation NPDES Number: NC0006564 Monitoring Period: From I/l/2017 To 12/31/2017 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ( All B (Alk -Treatment) Alt. C (Prior Testing)[1 Alt.D (No Prlor'Fest) EJ Process to Furtlier Redtice Pathooenas If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost El Ileat Dn_ling Heat Treatment 11 4 Thennophilic Beta Ray Gamma Ray Pasteurization L� Class B: lAlt. (1) Fecal Density Ali. (2) Process to Significantly Reduce PathogensLl If applicable to alternative performed (Class B only) uidicate "Process to Significantly Reduce Pathogens": Lillie Stabilization Air Drying 0 Compostin,T 13 Aerobic Digestion Anaerobic Digestion If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o r\ece del ce Trequency oi'Analysis Sample Type Analytical Tech ni ue MAnimurr, Geo..Mean N4axlmum Units Fecal Coliform 2 z 10 to the 6th power Per gram of total solids MPN 1550 1755 1802 MPN/g 0 7 grab sm9221 CPI.I 1000 Illpll per gralll of total solid (dry wveight) Salmonella bacteria (in lieu ol* fecal colilorm) 3 MPN per 4 grails total solid (dry Nveiaht) Vector Attraction Reduction (15A NCAC 02T .1107) -Please indicate alternative performed: Alt.1 (VS reduction) 0 Alt. 2 (40-day bench) Fj Alt. 3 (30-day bencli) El jAlt. 4 (Spec. 0, uptake) Alt. 5 (14-Day Aerobic) 0 Alt. 6 (Alk. Stabilization Alt 7 (Drying - Stable) lAlt. 8 (Drying - Unstable) L3 Alt. 9 (Injection) J Alt. 10 (Incorporation) .No vector attraction reduction alternatives were performed CERTIFICATION STATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in I SA NCAC 02T .1.106 and the vector attraction reduction requirement in :15A NCAC 02T .1107 have been met." tj "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." SZEVoLta 6tArC, E(t S SI r*mjiGNnEaSC Dennis .Key Southern Sol] Builders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Analytical R Southern soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 02/08/2017 Reported: 02/10/2017 For: Baxter Comments: Geometric Mean <1755 MPN/g Sample Number Parameter Sample ID Result 170208-08-01 Fecal Coliforms 1 <1786 170208-08-01 Percent Solids 1 11.2 170208-08-02 Fecal Coliforms 2 <1802 170208-08-02 Percent Solids 2 11.1 170208-08-03 Fecal Coliforms 3 <1802 170208-08-03 Percent Solids 3 11.1 170208-08-04 Fecal Coliforms 4 <1786 170208-08-04 Percent Solids 4 11.2 170208-08-05 Fecal Coliforms 5 <1786 170208-08-05 Percent Solids 5 11.2 170208-08-06 Fecal Coliforms 6 <155&,. 170208-08-06 Percent Solids 6 12.9 170208-08-07 Fecal Coliforms 7 <1786 170208-08-07 Percent Solids 7 11.2 Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 ults Unit Method Analyzed Analyst MPN/g MPN/g MPN/g MPN/g MPN/g MPN/g MPN/g SM92210E-2006 SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM2540B-1997 SM9221 CE-2006 SM25409-1997 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 .I Condition of eceipt Sample Number 170208-08-01 Temp on Arrival: 3 Parameter chedule: Percent Solids Received on Ice Parameter chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-02 Temp on Arrival: 3 Parameter chedule: Percent Solids Received on Ice Parameter chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-03 Temp on Arrival: 3 Parameter chedule: Percent Solids Received on Ice Parameter I chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-04 Temp on Arrival: 3 Parameter chedule: Percent Solids Received on Ice Parameter chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-05 Temp on Arrival: 3 Parameter chedule: Percent Solids Received on Ice Parameter chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-06 Temp on Arrival: 3 PO Box 228 • Statesville, NC 28687 • 704/8 Page 72/4697 ?of 4 S Parameter Parameter Sodium Thiosulfate mber 170208-08-07 Temp on Arrival: 3 Parameter Parameter Sodium Thiosulfate le: Percent Solids Received on Ice edule: Fecal Coliforms Received on Ice le: Percent Solids Received on Ice le: Fecal Coliforms Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 Client: -Ild r L STATESVILLE ANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 28687 (144) 872-4697 Address: s $ t v �; �_ J 1 !� q Q i�Ats .- Contact Person: L Phone # 33C' FAX" 33G _ Q 57 _ 95 y o Chain of Custody Record PO # Requisitioned by: (Time Data) Customer Sample IDn i a"D B one Sampled (GrabOnty) Dale Sampled (Grab Only) ¢ c� s Matrlx w ww Parameters requested for analysis U2 7` k 0 CMG >1 1` Relinquished by: Received by: I Relinquished by: Received by: Composite Samplings #9: Time begin am, pm Date —J_J Time end am, pm Date _/�_ Composite Sampling #2: Time begin am, pm Date / / Time end am, pm Date Time : G am,Date og l d-9 Time : (00 am(r Date � I � Y � Time am, pm Date _0 ! Time am, pm Date _I I Lab Comments: Sampled by: k� Transported by. � K 4) Holding times met: Compliance work: Non-compliance work: n 00 tD tb N v z ai CU to Analytical Re�ults Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/09/2017 Reported; 01/10/2017 For: Comments: Sample Number Parameter sample ID Result 170109-09-01 % Volatile Solids Baxter A 0.24 170109-09-01 Percent Solids Baxter A 0.39 170109-09-02 % Volatile Solids Baxter B 0.69 170109-09-02 Percent Solids Baxter B 1.68 Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Unit Method Analyzed Analyst ova SM254OG 01/09/2017 MD SM254OB-1997 01/09/2017 MID SM2540G 01/09/2017 MD SM254OB-1997 01/09/2017 MD PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 VS in 0.0069 VS out 0.0024 VSFR= 0.653743 VSFR= ,0()() (0.0069-0.0024)/(0.0069-(0.0069*0 r i �, 5-(:7" 24)) 31 `1 Condition of Receipt le Number 170109-09-01 Temp on Arrival: 3 Parameter chedule: Percent Solids I Received on Ice Parameter Schedule: Received on Ice Sample Number 170109-09-02 Temp on Arrival: 3 Parameter chedule: I Received on Ice Parameter chedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 2 Client: cJ'�}.ar tN � �; ,�.,,Ic�N�j T�� r; _ STATESVILLE ANALYTICAL 122 Court Street P.O. Box 228 Statesville, NC 28687 (704) 872-4697 Address: C dj g S �� ci `� f ndi q Contact Person: l Phone # ; 3r - j S) .7 •-�j FAX# Chain of Custody Record PO # Requisitioned by: (Time Date) Customer Sample ID# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only) a 0 a � Matrix Parameters requested for analysis 4 y swaeB w ww Relinquished by: Received by: Y Relinquished by: Received by: Composite Sampling Time begin Time end Composite Samplings Time begin Time end #1: am, pm am, pm #2: am, pm am, pm Date / / Date / / Date Date _/ / Time - �� amJprt)' Date �/ C� /� Sampled by: l _ Time . am,Qate i / / iTransported by: Z Y e e:�: Time am, pm Date _/ / Holding times met: ./ Time am, pm Date _/ Compliance work: Non-compliance work: Lab Comments: Analytical Re�ults 1z—MWI Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 r Receive Date: 02/08/2017 Reported: 02/10/2017 For: Baxter Comments: Geometric Mean <1755 MPN/g Sample Number Parameter Sample ID Result 170208-08-01 Fecal Coliforms 1 <1786 170208-08-01 Percent Solids 1 11.2 170208-08-02 Fecal Coliforms 2 <1802 170208-08-02 Percent Solids 2 11.1 170208-08-03 Fecal Coliforms 3 <1802'� 170208-08-03 Percent Solids 3 11.1 170208-08-04 Fecal Coliforms 4 <1786 170208-08-04 Percent Solids 4 11.2 170208-08-05 Fecal Coliforms 5 <1786 170208-08-05 Percent Solids 5 11.2 170208-08-06 Fecal Coliforms 6 <1550 N 170208-08-06 Percent Solids 6 12.9 170208-08-07 Fecal Coliforms 7 <1786 170208-08-07 Percent Solids 7 11.2 Respectfully submitted, hnP' -ma, J�' X/"" l Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 Unit Method Analyzed Analyst MPN/g MPN/g MPN/g MPN/g MPN/g MPN/g MPN/g SM9221 CE-2006 SM254OB-1997 SM9221 CE-2006 SM254OB-1997 SM9221 CE-2006 SM254OB-1997 SM92210E-2006 SM254OB-1997 SM92210E-2006 SM254OB-1997 SM9221 CE-2006 SM254OB-1997 SM92210E-2006 SM2540B-1997 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC 02/09/2017 WC PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 4 Condition of Receipt Sample Number 170208-08-01 Temp on Arrival: 3 Parameter S hedule: Percent Solids Received on Ice Parameter S hedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-02 Temp on Arrival: 3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-03 Temp on Arrival: 3 Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-04 Temp on Arrival: 3 Parameter Schedule: Percent Solids Received on Ice Parameter chedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-05 Temp on Arrival: 3 Parameter Schedule: Percent Solids Received on Ice ParameterSchedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 170208-08-06 Temp on Arrival: 3 PO Box 228 • Statesville, NC 28687 • 704/8 Page'. 72/4697 >_of4 Parameter Parameter Sodium Thiosulfate Number 170208-08-07 Temp on Arrival: 3 Parameter Parameter Sodium Thiosulfate Percent Solids Received on Ice Fecal Coliforms Received on Ice Percent Solids Received on Ice le: Fecal Coliforms Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 4 Client: C C , STATESVILLEAN.IMICAL 122 Csurt Sttext P.O. Box 226 Statesville, NC 28687 (704)872-4697 Address: Q S g J 1 S� 1 /� u T R.L- �e. ��. a�f��t Contact Person. pC # Phone 0 33c - 9 Requisitioned by: 3 ,7'1)811 FAX# 93 � - 9 $1- 5 y y p (Time vets) Chain Of Custody Record customer Sample 100 Lab 10 ime Sampled (Grab Only) Date Sampled (Grab Only) sg. Matrix w ww Parameters requested far analysis � !J 0-5 07 I Relinquished by. � ` Received by Relinquished by: Received by: Composite Sampling 91: Time begin am, pm Date _I—! Time end am, pm Date _ 1_I_ Composite Sampling #2• Time begin am, pm Date Time end am, pm Date Time J +rJ am, Date O� 1 1� Time ©� am prr Date $ Time am, pm Date s/ / Time am, pm Date _/ ! Lab comments: Sampled by: k� Transported by: Z l'�.a, Holding times met:�-� Compliance work: Non-compllance work: n 00 00 N U z ai Ln N 41 V) to 00 N N X 0 ca NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL007023 Predictive Client: Doug Poplin Advisor: Zach Key �AG��CULTURRµQ ae�� �ZNc 594 Austin Little Mtn Rd Southern Soil Builders, Inc. Soil Report Mehlich-3 Extraction Ronda, NC 28670 958 Hoots Rd Wp A Roaring River, NC 28669 •Fomr��. �� Links to Helpful Information Sampled: 09/28/2017 Sampled County :Wilkes Received: 10/02/2017 Farm: Not Provided Completed: 10/11/2017 Client ID: 160157 Advisor ID: 400594 Sample ID: DP1A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0' 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cO; NO3-N in mg/do]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% S4 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 0.88 19.3 90 2.0 6.2 / 536 423 56 23 58 139 97 802v 802 1768 0.2 1 V Sample ID: DP1B V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 pH$ 0 0 0 Note: 12 Note: $ 2- Test Results [units - W/V in g/cm3; CEC and Na in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral HM% W/V CEC BS% Ac H P-I K_I Ca% Mg% SJ Mn J Mn AL1—Mn-AI2 Zn-�Zfr ^•,.:-6'�;�aE&P—SS-1—N 0.41 0.93 14.3 92 1.1 6.6 t/ 238 222 59 26 52 123 81 747x,'/ 747 966/ 0.2 1/ 1 1% Sample lD: DP1C Recommendations: 'Lime Nutrients'(Ib/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.5 120-200 0. 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - W/V in g/carp; CEC and Na in meq/100 co; NO3-N in mgfdo]: Soil Class: Mineral HM% W/V CEC BS% Ac H P-1 K4 Ca% Mg% S-1 Mn-I Mn-All MnAI2 Zn-1 J Zn-AI Cu-1 Na ,ESP SS4 NO3-N ✓ /. �/ 0.51 0.94 14.0 85 2.1 5.8 281 201 56 22 60 247 165 1256 1256 1278 0.2 1 V North Carolina Tobacco Trust Fund Commission Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY18-SL007023 Doug Poplin Page 2 of 4 Sample ID: DP1 D V Recommendations: Lime Nutrients (lb/acre) Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B More Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 0 0 0 2- 0 Note: 12 Test Results [units - W/V in g/cO; CEC and Na in meq/100 crrP; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH J P-1 K4 V Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.56 0.94 13.7 87 1.8 6.1 361 139 60 21 72 170 118 1224 1224 1574 0.2 1 �� Sample ID: DP2 Recommendations: Lime Nutrients (lb/acre) Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B More Information Lime History: 1- Fescue/OGrassMm, M 1.7 120-200 0 20 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 crn3; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K4 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.66 1.00 7.7 64 2.8 5.1 185 67 44 15 101 113 85 320 320 785 o.2 3 Sample ID: DP3C V Recommendations: Lime Nutrients (lb/acre) Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B More Information Lime History: 1 -Corn, silage 1.5 180-220 0 20 0 0 0 0 0 2- 0 Note: 3 -Iest Results Lunits - VY7V in g c ; CSC and NNa� in meq/100 c ; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac / pH \ �� P-1 K4 Ca% Mg% S-1 Mn-I Mn All Mn AI2 Zn-I / Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.97 7.9 67 2.6 5.2 ,�,� 266 99 39 22 162 101 78 414 ✓ 414 410V 0.3 4 Sample ID: DP3G v Recommendati . Lime Nutrients (lb/acre) Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B More Information Lime History: 1-Fescue/OGrass/Tim, M 0.3 120-200 0 70 0 0 0 0 0 2- 0 Note: 12 Test Results [units - WN in g/cnil; CEC and N�a in meq/100 crrr3; NO3-N in mg/dO]: Soil Class: Mineral % HM% WN CEC BS% Ac (pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-1 Na ESP SS-1 NO3-N 0.51 0.96 9.9 81 1.8 1 5.9 95 36 53 97 as a7 7rZ J - - GUJ U.L L V V NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronorni/ Report No. FY18-SL007023 Doug Poplin Page 3 of 4 Sample ID: DP4 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 1.1 120-200 0 30 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crrP; CEC and Na'in m1eq/100 cO; NO3-N in mg/drr$]: Soil Class: Mineral HM% WN CEC BS% Ac pH y P-1 K-1 i Ca% Mg% S-1 Mn-I Mn-All Mn Al2 Zn-I -Al Cu-I✓ Na ESP SS-1 NO3-N 0.86 0.90 11.7, 76 2.8 5.6 .� 173 55 48 26 70 127 93 1208 1208 845 0.2 2 V Sample ID: DP5 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 0 pH$ 0 0 0 Note: 12 Note: 2- Test Results [units - WN in 9/cm3; CEC and Na in meq/100 crrp; NO3-N in mg/drrr?]: Soil Class: Mineral HM% WN CEC BS% Ac pH V P-1 K4 Ca% Mg% S-1 Mn-I Mn-All MnAl2 Zn-I / Zn-AI Cu-I� Na ESP SS-1 NO3-N 0.60 0.94 12.. 92 1.0 6.5 84 125 57 30 60 122 82 774 v 774 603 0.2 V 2 Sample ID: DP6 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.0 120-200 0 60 0 0 0 0 0 0 Note: 12 2- Its-(units — WNin-gtcm"; CEC anfi a in meq cffP; NO3-N in mg Soil Class: Mineral HM% WN CEC BS% Ac pH ,. / P-1 K4 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 •0.97 12.2 85 1.8 6.0 133 40 60 23 54 116 87 988 988 889 0.2 v 2 V1 Sample ID: DP7 V Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, M 0.6 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cm3; NO3-N in mg/dO]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-I Ca% Mg% S4 Mn-I Mn-All Mn AI2 Zn-I /Zn-AI Cu-IL/ Na iESP SS-1 NO3-N 0.51 0.94 10.4 82 1.9 5.7 23 110 55 21 58 91 72 554 ✓ 554 1014 0.2 ✓ 2 i% v