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WQ0031725_Annual Report_20170306
Annual Report Review SOP Class B Land Application Reporting Period: ti'31 �% Detaffs:W 003119 5 64 uj-A--y r2Ae_We8.., Is 503?. V-e--S. q_ Class A 0ro?av 6�j, Maximum Dry Tons Per Year: 1-600 &q" 10 • M40 S • Number of acres perm -Z itted: 114 0 - Number of fields in permit:-.� 007 -,901/ Counties that land is permitted for: 2c67- Monitoring Frequency.for TCLP: AA ---- Monitoring Frequency for.Residuals Analysis:,44,7 "'Od -Monitoring Frequency for.Pathogen &Vector Attraction Reduction:, Groundwater monitoring: N/A: L. Annual.Land Application bertificatioi Fornif, Was a certification form submitted? Was landapplication conducted, durkg the reported year? , I - S/57 1. -17/ How many y tons and dry tons per acre were applied? 1-36 A 40'r dry Were the licationsithin within IV73 applications thp.-permitt6d amoun0y.' 41147 Verify PAN if more than 10 tons/acre.? Did it indicate compliance? 6.29 Was it signed by the appropriate people? 2. Monitoring W6relhe analyses conducted at,thl exequired frequency?; (ile4?, Was. an analyses taken for.each source that. was. I/ -metals analyses reported on.the Residual Saj?kplin9 Summary Were the Form? T Were the results reported in mg/kg? Were the pH's 6.0 or greater for each residual sample? Were the heavy metals within --ceiling concentration permit limits? Were the lab analyses attached7y, Were all the required parameters tested? Was TCLP analysis conducted? Were the TLCP contaminants within regulatory limits? I Was a corrosivity, ignitability, and reactivity analysis conducted? 3. Field Summar'y ....-....-...................--Were-the.-land.applicafionev.ents.re' ded-on-the-Field-Summat�LF-orms'? cor How many fields were applied on, this year? Was a Field Summary Form submitted for each field? Were- all the residuals applied to permitted land? Were all the residuals applied from permitted sources? Were the field loading rates for each metal and PAN calculated (year to date)? Were the cumulative.pollutant loading rates calculated? Were the calculations correct? \1 Were the PAN loading rates within permit limits? Were the heavy metal cumulative pollutant loading rates within permit limits?,.) Were the residuals applied on a suitable crop? Were the applications conducted during thecirop's growing season? Were the Field Summary Forms complete? Was lime application on Field Summary Form? No lime applied. 4. Pathogen and Vector Attraction Reduction - Was a signed copy of the Pathogen and Ve� Attraction Reduction Form Omitted? K/ -Did the form indicate the perio of coverage, the residual class, and the,pathog'en reduction alternative' and the vector attraclion. reduction optioned?- Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? Was pathogen and vector attraclif -reduction demonstrated according to 40 CFR Part 503 ? Class B Pathogen Review Alternative I — Fecal Coliform Density Was the sampling conducted at the required frequdncy9 Were seven samples taiken? Was the geometric, mean ca. l6ulated and done correctly?' - Did the results show compliance (less than either 2,000,000 WN/gram'of total solid , s or 2,000,000 Colony Forming Units/gram of total- solids)?. Alternative 2 —Use of Process to Significantly -Reduce -Pathogens (one of five) Was the sampling conducted at the required frequency? 1. Aerobic Digestion Was it an aerobic process (Inspection)? 'Were logs submitted showing time.and'tempeiatur 9 e Were temperatures within iange'iforcompletelime:period? Was the time and temperaturebetween 40 days at 20°C (68T) and 60 days at 156C 2. Air Drying - Were the residuals on sand beds or pave or unDayed basins for three months? Was the ambient temperature above VC (32T) for two months? Were the residuals partially digested? Were residuals exposed to atmosphere during two months above 0°C (not snow covered)? 3. Anaerobic Digestion. -Was it an anaerobic process (Inspection)? -Were logs submitted -.showihg:tune and tompeiAture?. - Were temperatures within time period? erature ith complete -Was the time and temperature bdfween15 day's.at 359C (95T) to 55T (13 IT) and 60 days at 20°C (68T)? 4. Composting (usually will bb,.Class A."when composting is used) Was itacompostin procedure (fiot:tlatutal decay under uncontrolled conditions)? . 9 pro Were logs submitted showing time and temperature? Was the temperature raised to 40 5. Lime Stabilization Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? Were logs submitted showing time and temperature? Was the pHraised to 12 after two hours of contact? Were logs submitted showing time and. pH? . • Was temperature corrected to'25°C (770F)? Alternative 3 - Use of Processes Equivalent to RSRP ° . (Not commonly use. See White House Manual page 100.103, tables 11-1 and 11-2.) Vector Attraction Reduction Review Was the sampling conducted at the requiredfirequency?� Option 1— 38% Volatile Solids Reduction Was there 38%o reduction? CP _ iti • Were lab sheets/calculations in r6port?l 15. Was the reduction on volatile solids (not total solids)? Were the samples taken at beginning of digestion process and before application (Inspection)? Were calculations correct? c Option 2 — 40-Day Bench Scale Test Were residuals from anaerobically digested treatment (Inspection)? I Were residuals anaerobically digested in lab?. Was the test run for 40 days? . Was the test done between 30°C (86°F) and 379C (999F)? Was the reduction of on volatile solids (not total solids)? • Was the reduction less.than 17%? Were lab sheets/calculationsin. report? Were calculations correct? Option 3 — 30-Day Bench Scale Test Were residuals from aerobically`digested treatment (Inspection)?. - Were residuals aerobically digested in lab? Were residuals 2% or less total solids? • If not 2% total solids, was the test ran on a sample diluted to 2% with unchlorinated effluent? Was the test run for 30 days?> Was the test done 'at 20°C (68°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 15%? Were lab sheets/calculations in. report? Were calculations correct? Option 4 — Specific Oxygen Uptake Rate(SOUR) Were residuals form aerobically digested treatment (Inspection)? Were residuals 2% or less total solids (dry weight basis) (not diluted)? • Was the test done between 10°C (50°F) and 30°C (86°F)? . Was the temperature corrected to 20°C (68°17)? Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)? Was the sampling holding time two hours? . Was the test started within 15 minutes of sampling or aeration, maintained? Option 5 14-Day Aerobic Process ..Were the residuals from aerobically digested treatment (Inspection)? Were the residuals treated for 14 .day s? Was the residuals temperature higher than 40°C (I 040F) for a 14-day period? Was the average residuals temperature higher than 45T (I 13T)? Option 6 — Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? Did the pH of residuals remain at 12 or higher f6r two hours wi , thoutthe addition of more alkali? Did the pH of re * siduals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? Was the pH corrected to.25°C (77-F)? Option 7 — Prying of Stabilized Residuals * Does.the residuals contain any unsfabilized residuals? Were the residuals mixed with.any other materials? -Were the residuals dried up to 75% total solids? Option .8 — Drying. of . Unstabilized Residuals Were the residuals mixed with any other.mat.prials? Were the residuals dried to 90% total solids?. Option 9 — Injection Was there any significant amount of residuals on land surface one hour after injection (Iiispectiion)? Was injection done on pasture or hay field? Was injection done at time that crop was growing? If Class A with respect to pathogen, -were . s re iduals injected With eight hours after discharge from pathogen treatment? 5. Soil Tests Was a, Standard Soil Fertility'Analysis conducted nducted for each application field? __4 LIN yrit — y,e,5 -Were the soil pH's 6.0 or, greater for each application field? -No 0P1B.=r54r3/ UPI-L Z S, � qr b LP ev -If no, was lime applied to those fields? 13c, DP 3 - Were the copper and zinc indexes in the soil less -than 2000 for each application. field?Y4-v (> ^ 0 -Was sodium less than 0.5 meq/100 cm.1\3? E)PiN ---) Na% 0,9' Was 'the exchangeable sodium percentage (ESP) less than 15%? UrG 6.General Was the report in the proper format? Was the annual report co-mplet6? I Was the report submitted on time? MAR -- 6 2017 r, . Water Quaty Baxter Healthcare Baxter Healthcare Corporation 2016 Annual Report Land Application Program NC Permit No. WQ0031725 F �;h 91- r3P RECEIVED FEB 2 8 2017 (11 InfvFination-processing Unit DWi? Ssction C-� AININ UAL 1,ANI) APPLICATION CERTIFICATION FORM WQ Permit#: WQ0031725 County: McDowell Year: 2016 Facility Name (as shown on permit): Baxter Healthcare Corporation Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-7871 Land application of residuals as allowed by the permit occurred during the past calendar year? R1 Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Racirl—la A... i otall number ofapplicatio Total number of fields utilized for land applic Total amount of dry tons applied during the year fo Total number of acres utilizes for land applic Part B - Annual Comniance Statement: n fields in the ermit: r ation 10 ation during the year: g all application sites: 136.19 during the year: 67.06 Facility was compliant during calendar year 2016 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. R1 Yes 11 No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1111 were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Name and Title (type or print) % T" n ature of Permittee Date Signature of Preparer* Date Signature of Land Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC. MT 1 1 n) i1)�, M, .. ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Facility Name: Baxter Healtcare Residual Source WQ # or NPDES #: WWTP Name: Residual Annlvcic Data WQ0031725 Baxter Healtcare Laboratory: 1) Waypoint Analytical 2) 3) 4) 5) Parameter (mg/kg) Conc. Limit m a Sample or Composite Date ✓ 2-2-16 Percent Solids (%) NA 11.87 Arsenic 75 7 Cadmium 85 2 Copper 4,300 128 Chromium NA 79 V Lead 840 11 Mercury 57 0.4 Molybdenum 75 5 ✓ Nickel 420 29 Selenium 100 5 Zinc 7,500 194; Total Phosphorus NA 19900 TKN NA 82300 Ammonia -Nitrogen Nitrate and Nitrite I a For surface disposal facilities NA NA the rP;l;nv 6490 28.1 nnnePrf—+;,,,, r,.,,;+.. 1;-+ a :_ ..L:_ c — _ uYY.,..---- jo-1 1-C uie mulvmaua permit Tor metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * Date L *Preparer k defined in 40 CFR PCULi ✓V�.94'r) and 13A'1VCAl 21 .1102 (26) DENR FORM RSSF (12/2006) to'41'MUH1, IV lAL6 rILI U LUAVnU SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Popin Predominant Soil Series: 5.5 Acres Permitted: 5.5 Site #: DP1-A Field #: Residual Analvsis Data fFfenvv Metalc and T,,t.,l Vik-L /L- a/ [7 ,• , 2.83 FcC2 DP1-A Com- posite Date, Total DT/Ac./ App. Event Total DT/Ac./ App. Event 0.52 121 3 141 5 J L6 7 8 9 10 11 12 y 0 W Arsenic Cadmium 0.007 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 0.000 0.002 Copper 0.132 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.132 " Chromium 0.081 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0;000 0.000 0.000 0.081 0.011, Lead Mercury Molyb- denum 0.011 0.000 0.005 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000, 0.000 ' •0.000 ; ;0,.000 0.000 0.000 0.000 0.000 0.005 Nickel Selenium Zinc Total Phos- horus "I eertifv. 0.030 0.005 0.200 20.497 under 0:000 0.000 0.000 0.000 nenalty of 0.000 0.000 0.000 0.000 law that 0.000 0.000 0.000 0.000 th;o a,,,,,,,.. 0.000 0.000 0.000 0.000 ---I 0.000 0.000 0.000 0.000 -.-- _ 0.000 0. 000 0.000 0.000 _ � __ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.000 0.000 0.000 0.000 0.030 0.000 0.005 0.000 0.200 l 0.000 20.497 20'H�iia Ir , F"A - . ""%,. „ly .,11 ccuuL ur supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 7 f �-Z� - Sign61re of Land Applier Date 2 2 npKip Pr)PIIA hAM c� /1710nnc� 1-11"N UAL 1VIE ALl FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 2.83 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: FcC2 Acres Used: 1.6 Acres Permitted: 1.6 Site #: DPI-B Field #: DPI-B Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #1: Samnle org 11 121,11 M e Com- posite Date 2/2/16 % Solids 11.87 Arsenic 7 Cadmium 2 Copper 128 Chromi 79 Lead 11 Mercury 0.4 Molyb- denum 5 Nickel 29 Selenium 5 Zinc 194 Total Phos- 19900 - ----- ==tea• r 1.1Gtal ri-eiu Loaumgs (Ualculated in lbs/acre): Total 1 2 3 4 DT/Ac./ 5 6 8 9 10 11 12 App. Event 1.77 Arsenic 0.025 0:000 0.0000.000 0.007 0:000 0.000 0.000 0.000 0.000 0:000_ 0.000 : 0000 0.Cadmium 40-'v', 0.000:. 0.000 0.453 0.000 00000.0000.0000.0000.0000.0000.0000.000 0-!- 0.000 0.000 0.000 . 0.000 0.000i 0 000 0.Copper 0.280 0.000 0.000 0.000 0.0000.000 , ; 0000 0.Chromi Lead 0.039 0.000 0.000 0.000 0.000 0.000 0.0000.0000.0000.000 0.000 0000 0.00 0.280 ✓ Mercury 0.001 0.000 0 0 00 : 0. 000 0: 000' 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.039 ✓ Molyb- 0.018 0.000 0.000 0:000 denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 o01 ✓ Nickel O. L03 0.000 0.000 0:000 0.000 0.000' -0.000 0.000 0.000 0.000 0.000 0.018 V Selenium 0.018 .0.000 0.000 , 0:000 O:Q00 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 0.103 Zinc 0.487 0.000 0.0.00 0:000 0:000 . - . 0.000 0.000 0.000 0.000 0.000 0.000 ?0:000 0.000 ; b.000 0.000 0.018 Total ; . 0.000 0.687 Phos- 70.486 0.000 0.00o 0.000 horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 70.486 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly I am aware that there are significant for gathered and evaluated the information submitted. penalties submitting imprisonment for knowing violations". false information, including the possibility of fines and Signature of Land Applier Date Aviv uAL 1V1E'1A1.S FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual R Facility Name: Beport Baxter Healthcare Total Dry Tons Applied (Annual): 5.67 Permit #: WQ0031725 Operator: Douglas Poplin Owner: Cation Exchange Capacity (non 503 only): • Acres Used: Douglas Popin Predominant Soil Series: 3 Acres Permitted: 3 FcC2 Site #: DPI-C Field #: DPI-C Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent Sample or 1 2 3 4 5 s � #). Com- $ 9 10 11 12 posite Date 2/2/16 % Solids 11.87 Arsenic 7 Cadmium 2 Copper 128 Mromi 79 Lead 11 Mercury 0.4 1 5 29 gden' 5 194 Total Phos- 1 19900 Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 DT/Ac./ I 3 4 5 g 8 9 10 11 12 App. t1 0 Event 1.89 Arsenic 0.026 0.000- Cadmium 0:008 -. 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 . 0000 0.000 y 0.026 V Copper 0.484 0.000 .0.000 0.000 0.000 0.000 0.000 0:000 0:000 0.000 0.000 0.000 0.000 ;0:000 0.000 0 008 Chromi 0.298 0.000 . 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 '0.000 0 " Lead 0.042 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.298 298 ✓ Mercury 0.002 0.000 0.000 0.000 0..000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.042 Molyb- denum 0.019 0.000 0.000 . 0.000 0.000 0.000 0.000 0.000 0.000 ; 0:000 0.000 0.002 Nickel 0.110 0.000 0:600 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.019 Selenium 0.733 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 `'0.000 0.0 00 0.110 Zinc 0.733 0.000 .0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.019 ✓ Total 0.000 0.000 0.000 0.000 0.000 0.733 Phos- 75.182 0.000 horus 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 "I certify, under penalty of law, that this document was 75.182 tiati with a system designed to assure that qualified personnel prepared under my direction or supervision in accordance I am aware that there are significant penalties for submitting properly evaluated the itted. imprisonment for knowing violations". false nformationlincluding the pos litylon ibi of finessub and ILA ail' Signature of Land Applier )- 3 �` Date tfIIUIIUt1L 1rlrIitiL.7 r1GLL LVL-1Lllvl= OUIV11VIAKI V kJIUV1'' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: Acres Used: 9.6 Acres Permitted: 9.6 Site #: DPI-D Field #: 16.42 FcC2 DPI-D Residual Analvsis Data (Heave Metals and Total Phosnhorus use mu/ku- % Rnlidq nee Raw Percent JA- Com- posite Date Total h ••�� tX11uUM 11e2LVV 1V1GLUI rlelU LuilulnY-s Il..alcalaiea In InwnerP.1_ Total 1 1 L2 1 31 4 L5 6 171 L 8j 19110 11 12 DT/Ac./ APP. Event 1.71 y Arsenic 0.024 0.000 0.000- 0.000 . 0:000 0.000 0.000 0.000 0:000 0.000. 0 000 0.000 0.024 Cadmium 0.007 0.00.0 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000. 0.000 0.007 Copper 0.438 0.000 0.000 0.000 Oi00.0 0.000 -0.000 0.000 0.000 0.000 1.0 000 0.000 0.438 Chromium 0.270 0.000 0.000 0.000 -0.000 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.000 0.270 Lead 0.038 .0.000 0.006 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.038 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 , 0.000 0.000 0.000 0.000. ! 0.000 04000 0.001 Molyb- denum 0.017 0.000 0.000 0.000 0".000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.017 Nickel 0.099 0.000 0-.000 . '0.000 0.000 0.000 0.000 0.000 0 000 0.000 ' 0:000 0.000 0.099 Selenium 0.017 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 U:000 0:000 0.000 0.017 Zinc 0.663 0:000" 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0,000 0.000 0.663 Total Phos- 68.058 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.058 horus T .n - -.71 ..,...... r..ua.%7 .,X ,a.., L""t LULa UU%;U■uG„L was prep2lreu unuer my uireciion or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier ,9 3+3 Date J DENR FORM MFLSF (12/2008) ti1111 U 111- lY JV, 11i.LC r I-V LL L VALln I T L-3 U IV11V1AK Y V' VKiVI- Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 25.71 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: Fc:B2 Acres Used: 6.983 Acres Permitted: 6.983 Site #: DP-3 Grass Field #: DP-3 Grass Residual Analvsis Data (Heave Metals and Tntal.Phncnhnr„c nae ma/ka o/ Ralifle „ao D.- ID----4- u1. Com- posite Date, ®m� Total . ..�� .. cXuaauai iivav r iVXVLai rioiu L.rauium� . L,Rucuiateu .n In\/aa, r " Total Ill L2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ rt App. �. Event 3.68 y Arsenic 0.052 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 -' 0.000 0.000 0.052 Cadmium 0.015 :0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0:000 0:000 0.000 0.015 Copper 0.943 UK 0.000 0.000 0.000 0.000 0.000 0.000 0:000 . 0.000. A-000 0.000 0.943 Chromium 0.592 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 I.0:000 0.000 0.582 Lead 0.081 0.000 0.000 0.000 0,000 0.000 0.000 0.000 0:000 0.000 A000 0.000 0.081 Mercury 0.003 0.000 0.000 0.000 0.00.0 0.000. 0.000 0.000 0.000 0.000. 0.000 0.000 0.003 Molyb- denum 0.037 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 :0.000 0.000 0.037 Nickel 0.214 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.214 Selenium 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.000 0.037 Zinc 1.429 0.000 0.000 0.000 0.000 0.006 0.000 0.000 0.000 0.000 , D-000 0.000 1.429 Total Phos- 146.544 0.000 0.000. 0.0.00 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 146.544 horus .....xy, UJUL"V. Fullaa.y UI ,av►, wat iu,N uvUu,ueuL was prepareu unuer my mrection or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 0-1-- 1 , � - Y- 1-7 Signature of Land Applier Date I DENR FORM MFI SF r1,?»nnFN tallqlllut1L 1TiL' 1tiLO r1LJJLJ" LVt'iVll\lT Oulv11v1ti1mZ rVltivl' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: Acres Used: 5.877 Acres Permitted: 5.877 Site #: DP3-Corn Field #: 14.53 FcC2 DP3-Corn Residual Analysis Data (Heave Metals and Total Phosphorus use mg/kg. % Solids uce Raw Percent ii)- Com- posite Date, in10lM Total . ... ..�o tinnuai neavv iviLmai rieia i,oaainis (uaicuiaten in insiacrei: Total 1 121 L3]4 5 6 7 J S 9 10 IIJ 12 DT/Ac./ c App. i� Event 2.4 y Arsenic 0.03 0.000 0.-000 0.000 0:000 0.000 0.000 0.000 '0.000 0.000, 1-0.000 0.000 0.035 Cadmium 0.010 0.000 0.000 0.000 0.000 0.6100 0.000 0.000 0.000 0.000 0:000 0.000 0.010 Copper 0.633 0.0.00 0.000 0.006 0.000 0.000 0.000 0.000 0.000 0.000 j 0.000 0.000 0.633 Chromium 0.301 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 1 0.000 0.000 0.391 Lead 0.054 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.054 Mercury 0.002 0.000 , 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 , 10.000 0.000 0.002 Molyb- denum 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1-.0.000 0.000 0.025 Nickel 0.143 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 i 0.000 0.000 0.143 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 .' i 0.000 0.000 0.025 Zinc 0.960 - 0.060 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 0.960 Total ! l Phos- 98.425 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 98.425 horus f 1 l:Ci -Lily, u..uC.- Pumilay Ul i'dw, 6IlaL tuis uucument was preparea unaer my alrectlon or supervision In accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Sign Lure of Land Applier Date J J J I DENR FORM MFLSF (12/2006) fuviv uAL METALS HELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Baxter Healthcare Total Dry Tons Applied (Annual): 23.12 WQ0031725 Cation Exchange Capacity ty (non 503 only):O Operator: Acres Used: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: FcB2 8.7 Acres Permitted: 8.7 Site #: DP-4 Field #: DP-4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 3 4 5 6 7 8 9 10 11 12 Com- posite Date 2/2/16 % Solids 11.87 Arsenic 7 Cadmium 2 Copper 128 Chromi 79 Lead 11 Mercury 0.4 Molyb- 5 denum Nickel 29 Selenium 5 Zinc 194 Total Phos- 19900 Total 1 DT/Ac./ App. Event 2.66 Arsenic 0.037 Cadmium 0.011: Copper 0.680 ' Chrommir 0.420 Lead 0.058 Mercury 0.002 Molyb- denum 0.027 Nickel 0.154 -, Selenium 0.027 Zinc 1.031 Total 0.0.0.0 0 000 0.000 0 0'.Q00. 0.000 0.000 '0 0.000 0.000. 0.000 0 0.000 ' -0.000j 0:000 0 0.000 0.000 0.000 0.000 0.000 0.000 0:000 6.000 0.000 0.000 0.000 0.000 0.000 0.000 0 000 0.000 0.000 -66 6 000 0.000 0.000 0.000 0.000 lbs/acre): 7 0.000 ,0.000 0.600 O000 0.000 0.000 0.000 0.000 0.000 0.000 Phos- 105.749 0.000 10:000 10.000 10.000 10.000 1 0 8 9 10 LIJ 12 0 a WOO 0.000 0.1000 0.00.0 0.000 0.000 0.037 1.000 0.000 0.000 0.000 0.000 0:000 0.011 .000 0.000 0:000 0:000 0.000 0.000 0.680 .000 0.000 0:000 0.000 "0''.000 0.000 0.420 000 0.000 0.000 0.000' 0.000 0.000 0.058 .000 0.000 0.000 0.000' , '0.000 0.000 0.002 .000 0.000 0.000 0.000 :0.000 0.000 0.027 .000 0.000 0:000 0.000 0.000 0.000 0.154 � 000 0.000 0.000 0.000 0.000 0.000 0.027 r 000 0.000 0.000 0.000 '-0.000 0.000 1.031 000 0.000 0.000 0.000 0.000 0.000 105.749 f i cemly, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date a Cf111114Ur...1V1L' JL11kU711L`Lll LVttIl11\V aUA'livillk<I 1'1J111Y1' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 25.57 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: FcC2 Acres Used: 15.9 Acres Permitted: 15.9 Site #: DP-5 Field #: DP-5 Residual Analvsis Data (Heave Metals and Tatal Phnenhnrm nee mallro o/ 441. "MIN Com- posite Date in non a MI. TotalVA . .�. ..�� Auuual AXUaV V 1V1GLal i`1G111 L9211LUMP1 It.d ICnINYVII In In4aimprP1- Total 11 1213j L4 5 6 7 8 9 J 110111 12 DT/Ac./R. o App. E Event 1.61 y Arsenic 0.023 0.000 0.000 0.-000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Cadmium 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Copper 0.412 0.000 0.060 6.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.412 Chromium 0.254 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0:000 0.000 -0.000 0.000 0.254 Lead 0.035 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.035 Mercury 0.001 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.001 Molyb- denum 0.016 0.000 0.000 0.000 .0.000 0.000 0.000 0.000 01.000 0.000 FA000 0.000 0.016 Nickel 0.093 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.093 Selenium 0.016 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 1 0.016 Zinc 0.624 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1, 0.000 0.000 0.624 Total Phos- 63.998 0.000 0.00.0 0.000 0.000 0.000 0.000 0.000 0.'000 0:000. 0.000 0.000 63.998 horus vex �1 t 1 L.GA L11J', UIlUVl PVL1iCl1LY V1 law, LUUL tum umumenl was preparea under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (1212006) to\1� VAL IVMIEiLk-5 VI IA) LUADIAU aUNIMARY k'U)EiM- Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 11.31 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: FcC2 Acres Used: 5.5 Acres Permitted: 5.5 Site #: DP-6 Field #: DP-6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or 1 2 3' L4 5 L6J 171L8J 19110 11 12 Com- posite Date 2/2/16 % Solids 1 L87 Arsenic 7 Cadmium 2 Copper 128 Chromium 79 Lead. 11 Mercury 0.4 Molyb- 5 denum Nickel 29 Selenium 5 Zinc 194 Total Phos- 19900 Annual DT/Ac./ App. Event 1 2.06 Arsenic 0.029 1 0.000 0.000 Cadmium 0 0.08 0:000 0.00.0 Copper 0.527 0.000 0.000 "hromium 0.325 0.006 0.000 Lead 0.045 0.000 ` 0.000 denum 0.021 Nickel 0.119 Selenium 0.021 Zinc 0.798 Total 0.000 .'1 0.000 1 101 11l1 mgs (Calculated in lbs/acre): 4j 1516 7 0" 000 : 0.000. 0.000 0.000 `0.000 0.000 '0.000. 0.000 0.000 0.000 0.006 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 (Y.0.00. '-0.000 0:000 0.000 0.000 .0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000: 0.000 0.000 y 0 y t/ ✓ ✓ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 0.000 ' 0.000 0.000 0.000 0.000 0.000 0.000 0.008 0.527 0.325 0.000 0.000 0.000 ,: 0.006 , 0.000 0.000 0.000 . 0.000 0.0001 ` .0.000 : 0,000 0:000 0.000 0.00.0 0.000 0.045 0..002 0.021 0.000 0.000 0. O0 0.000 0.000 ' 0.00,0; 4 0.000 0:000 0.000: 0.000 0.000 0.000 0.000 0.000 0.000 0.119 0.021 0.798 0.000 0.000 0.000 ; 0.000 0.000 0.000 Phos- 81.869 0.000 0000 1 0.000 1 0.000 1 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 81.869 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier a-3-- Ig Date nr-hip s=r)phA RAG{ CC f47/7nnc� ru�l��rylvi�it>,1,J r1L+LL LVAIJll�ili 6U1V11VjI KY FUKMV Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Popin Predominant Soil Series: Acres Used: 4.4 Acres Permitted: 4.4 Site #: DP-7 Field #: Residual Analvsis Data (Neavv 1VMetnle ana Tn+ol ,, _ W_n__ al n , 8.20 FcC2 DP-7 .. . � © i© � !QJ Com- posite NONE on Date . ..�i ... Total DT/Ac./ App. Event 1 1.86� 2 3 4 --------__._---,- L5J L6J7 8 9 10 11 12 y y Arsenic 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0'000 0.000 , 0,000 0.000 0.026 Cadmium Copper Chromium Lead Mercury Molyb- denum 0.007 0.477 0.294 0.041 0.001 0.019 0.000 0.000 0.000 0.000 0.000 0.000 0.000 : - 0.006 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 . 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 . 0.000 0.000 0.000 0.000 0.000 �•0 000 6.0.00 0.000 0.006 0 000 0.000 0.000 0.007 ; 0.000 0.477 0.000 0.294 0.000 0.041 0.000 0.001 0.000 0.019 Nickel Selenium Zinc Total Phos- horus "I certifv- 0.108 0.019 0.723 74.147 jI"dPW Fia..alty 0.000 0.000 0.000 0.000 of 6.000 -0.000 0.000 0.000 l.aa. fkn4 "0..000 0.000 0.000 0.000 4t„� a 0.000 . 0.000 0.000 0.000 _..<_u� 0.000 0.000 0.000 0.000 ._. _ . ,_ ____ 0.000 0.000 0.000 0.000 . 0.000 0.000 0.000 0.000 - -- 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 lbhoo 0.000 0.000 0.108 0.000 0.019 0.000 0.000 0.723 0.000 0.000 74.147 _ -a 1„ vpai cu uuucr my ulrecilon or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �-� 2 9-3- Ir Signatur of Land A plier Date nF-NR F()RAA mm CF tior)nna� ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue/ PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0031725 Field #: DPI -A Annual Dry Tons Applied: 2.8340 Site #: DPI -A Predominant Soil Series: FcC2 Crop 1 Max. PAN: 158 l/ Crop 2 Name: Acres Utilized: 5.5 Acres Permitted: 5.5 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° Volume applied PP Volume Residual Sources Soil Precip. y o Z Nitrate Name of CropType 0 >~ o (enter one) Solids/ % Applied per PP P DES # W #, Q Cond. Past 24 cu b w w � w , TKN o and PAN Applied Receiving Residual A Liquid Solids Acre Fert. Animal (DiY, Hrs. o o w K' * - 04 ° CD Z. o Nitrite ( lbs/acre) Application Cu Yds Gallons (Dry Tons/Ac) Waste etc ) Wet Moist) inches ¢ # ] * mg/kg �• mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 12-2016 28.35 11.87 0:515 WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 26.811 NA Fescue 0.000 0.000 0.000 0.000 0.000 0:000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TA-LS 3s 0 As Cd Cu Cr Pb H Mo Ni Se Zn P 26 811; 0.000 Lime Applied ► lbs/a28 cre 0.007 ✓ 0.1127 0.120 36 ✓ 0:002 0.032 0.034 34 0 132 1.944 2.076 1338 0.081 1.29 1.371 NA 0.011 v 0.175 0.186' 267 0.000k/ 0.005 0.005%1 15 V 0.005 0.075 0.080 NA 0.030 0.454 0.484 374 0.005 0.059 0.064 89 ✓ 0.200 3.599 3.799 2498 20.497 ...._........ Date lbs/ac 'rior Years Cumulative lbs/ac )urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** ermit PAN Limit l st/2nd Crop _.. i cernry, unaer penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false iformation, including the possibility of fines and imprisonment for knowing violations." AIL;' Signature of Land Applier 9- 3 -1r7 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate r)FNR FORM FSF (19/9nnAi ANNUAL LAND APPLICATION FIELD S RY PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED ,AND SU�BMMITTED FORREACH FIELD Facility Name: Baxter Healthcare PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. APPLIED ON Land Owner: Douglas Poplin WQ Permit #: WQ0031725 Field #: DPl-B Annual Dry Tons Applied: 2.8340 Acres Utilized: 1.6 Operator: Douglas poplin Predominant Soil Series: FcC2 Site #: DPl-B Acres Permitted: 1.6 Crop 1 Name: Fescue Crop 1 Max. PAN: 158 Cation Exchange Capacity (non 503): -�� Crop 2 Name: Crop 2 Max. PAN: Volume applied (enter one) Solids/ o Volume Residual Sources Soil precip, y c /o Applied per (NPDES #, W # Cond. Z Nitrate ° Liquid Solids Acre Q ' Past 24 cu a w, w R, q PAN Name of crop T Q Fert., Animal (Dry, �' �' ; cow TKN ° and Applied P Type Cu. Yds Gallons Waste etc) wet, ems' a * � * ( lbs/acre Receiving Residual' (Dry Tons/Ac) o * �'* p .�, Nitrite ) .2-2016 28.35 Moist) inches Application 11.87 1.771 WQ0031725 0 mg/k9 mg/kg mg/kg Crop1 0 s 0.5 0.3 82300 6490 Crop 2 Crop 1 Crop 2 0.000 28.1 92.163 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0:000 0.0000.000 0.000 0.000 --- • ...a■�-ppucations totals on FORM FSF su attach FO u•uuu 0.000 TALS: 28.- - 0 pp ( RM FSF supp to this form): As Cd Cu Cr Pb H .nnuallbs/acre MO NiSe Zn P 92.163 0:025 000 Lime A lie V 0.007 0.453 0.280 0.039 0.001 0.018 0.103t- 0. 18� nor Years Cumulative lbs/ac 0.093 0.025 1.479 0.964 0.131 0.004 0.056 0.341 - 0.043 2.793 0.687 0.486 - -- urrent Cumulative lbs/ac Date lbs/a 0.118 0.032 1.932 1.244 0.170 0.005 0.074 0.444' 0.061• 3.480 ermitted C. P. L. R.**** 36 ' 'rmit PAN Limit lst/2nd Crop 34 1338 NA 267 15 374 _ .. NA 89 2498 ........... certify,_. _ :.. _ -..._ 158 under penalty _.,_ p ty of law, that this document was prepared under my direction or supervision in accordance with a system designed t ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false iformation, including the possibility of fines and imprisonment for knowing violations." g o assure that *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization, Rate: Surface -0.5, Injection/Incorporation- 1.0 Signature of Land Applier *** Mineralization Rates: Compost -0.1, anaerobially digested - Date aerobically digested -0.3, raw sludge -0.4 g 0.2, ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ` ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0031725 Field 0: DPI-C Acres Utilized: 3 Annual Dry Tons Applied: 5.6681 Site #: DPI-C Acres Permitted: 3 Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 158 [,�-- Crop 2 Name: Crop 2 Max. PAN: o ° A 12-2016 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons 56.7 % Solids 11.87 Volume Applied per Acre (Dry Tons/Ac) 1.889 Residual Sources (NPDES # WQ#, Fert., Animal Waste, etc) QQO031725 Soil Cond. (Dry, We Moist) dry Preci . p Past 24 Hrs. inches 0 y b a o' o a..... '� s c � -- * N' * o 0 0.5 ��. w ; + * m. * � 0.3 TKN mg/kg 1 82300 Z q co o e w mg/kg 6490 Nitrate and Nitrite mg/kg 28.1 PAN Applied (Ibs/acre) Name of CropType Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 98.307 NA Fescue 0.000 0.000 0.000 -0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 -0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 OTALS: 56.7 0 ►nnual lbs/acre Tior Years Cumulative lbs/ac As 0.026 ,/ 0.671. 0.697 36 Residuals Applications totals Cd Cu Cr 0.008. 0.484 0.298 0.037 2.1 1.313 0.045 2.584. 1.611 34 1 1338 NA on FORM FSF supp ( attach FORM FSF supp to this form): Pb H Mo Ni Se Zn P 98.307 0.000 0.042, 0.002 0.019 0.110 0.019 0.733 75.182 0.177 0.005 0.077 0.471 0.059 4.137• 0.219 0.007 0.096 0.581 kf 0.078 V 4.8 00 267 15 NA 374 89 2498 ' Lime Applied Date lbs/ac 11-2016 2000 :urrent Cumulative lbs/ac ermitted C. P. L. R.**** ermit PAN Limit l st/2nd Crop T _ _ «1.71 uuu�l Fcuaiiy V.L law, Mai Luis document was prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false iformation, including the possibility of Lines and imprisonment for knowing violations." Signature of Land Applier 3-1 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725Field #: DPI-D Annual Dry Tons Applied: 16.4144 Site #: DP1-D Acres Permitted: 9.6 Predominant Soil Series: FcC2 Cation Exchange Ca acity (non 503)• Crop 1 Max. PAN: Acres Utilized: 9.6 p _ 158 Crop 2 Name: Crop 2 Max. PAN: ° ° 11�° Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons u /o Solids Volume Applied per Acre (Dry Tons/AC) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc ) Soil Cond. wry. Wet, Moist) Precip. Past 24 Hrs. inches Y � 10 a 12, 0 o A P * o w * t o .» ; * == *0 TKN mg/kg Z o � mgikg Nitrate and Nitrite mg/kg PAN Applied pp ( lbs/acre) Name of CropT Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1-2016 58.5 11.87 0.609 ✓ WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 31.696 NA Fescue 7-2016 29.2 11.87 0.304 WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 15.8211 NA Fescue :0-2016 76.5 11.87 0.797 WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 41.449b NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 J 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 t e Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): OTALS: 164.21 Or As Cd Cu Cr Pb Hg Mo Ni Se Zn P 88.966 1 0.000 Lime Applied-' mnual lbs/acre 0.024 ,v 0.094 0.118 .,/ 36 0.007 0.025 0.032 34 0.438 1.499 1.937 1338 0.270 0.99 7 1.260 NA 0.038 0.156 0.194 267 0.001 0.003 0.00 15 0.017 0.057 0.074 . NA 0.099 0.333 0.432 374 0.017 L, 0.031 0.048 89 0.661 2.652 3.31.5 2498 68.058 ................. Date lbs/ac rior Years Cumulative lbs/ac !urrent Cumulative lbs/ac ermitted C. P. L. R.**** ermit PAN Limit 1st/2nd Crop _. 158 I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false kformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate npmp Fnphii FCG 117i7nnrn ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: DP-3 Grass Acres Utilized: 6.983 Land Owner: Douglas Poplin Annual Dry Tons Applied: '25.7112 Site #: DP-3 Grass Acres Permitted: 6.983 Operator: Douglas Poplin Predominant Soil Series: FcB2 Cation Exchange Capacity (non 503): Crop 1 Name: Fescue Crop 1 Max. PAN: 194 4_- Crop 2 Name: Crop 2 Max. PAN - Volume 1" d S '1 . o s~ _ Q o 3-2016 5-2016 )-2016 0-2016 app ie (enter one) Solids/ Liquid Cu. Yds Gallons 59.9 30.7 82.4 84.2 ova Solids 11.87 11.87 11.87 11.87 Volume A lied er PP P Acre D Tons/Ac t ry 1 0.858 0.439 v 1.180 v 1.205./ Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) WQ0031725 WQ0031725 WQ0031725 WQ0031725 O1 Cond. (Dry, We t' Moist) dry dry dry dry Precip. Past 24 Hrs. inches 0 0 0 0 y 4 b a o w ia. s s s s o � 0 w * M o 0.5 0.5 0.5 0.5 ;d = w * w" 0 0.3 0.3 0.3 0.3 T1 mg/kg 82300 Z � o �; o mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type P YP ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 6490 28.1 44.618 NA Fescue 82300 82300 6490 28.1 22.868 NA Fescue 6490 28.1 61.3-78w NA Fescue 82300 6490 28.1 62.718 NA Fescue 0.000 )TALSI V 257, nnual lb /acre for Years Cumulative lbs/ac irrent Cumulative lbs/ac :rmitted C. P. L. R_**** 0.000 0.000 0.000 0.000 0.000 (17b Residuals Applications totals on FORM FS As Cd Cu Cr Pb I H 0.051 0.015 0.943 0.582 0.081 0.003j 0.268 0.088 ' 4.773 3.194 0.418 0.011 0.320 V 0.103 5.716. 3.776 0.499, 0.014. 36 34 1338 NA 267 15 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ipp ( attach FORM FSF supp to this form): Mo Ni Se Zn P 191.581 0.000 146.544 Lime Applied Date lbs/ac 0.037., 0.214 0.037. 1.429 0.17t 0.945 0.474 10.563 11-2016 2506 0.208 1.159 0.511 11.992 NA 374 89 2498 rmit PAN Limit lst/2nd Crop _ certify, under penalty of law; that this document was prepared under my direction or supervision in accordance with a system designed to assure that ialified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false formation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation r I lJ 3-�1 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Corn WQ Permit #: WQ0031725 Field #: DP3-Corn Acres Utilized: 5.877 Annual Dry Tons Applied: 14.5351 Site #: DP3-Corn Acres Permitted: 5.877 Predominant Soil Series.-ce-2- Cation Exchange Capacity (non 503): Crop 1 Max. PAN: -2-14 Crop 2 Name: Crop 2 Max. PAN: ° N Q Volume applied enter one Solids/ ( ) Liquid q Cu. Yds Gallons o /a Solids Volume Applied per Acre D Tons/Ac �' ) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) Soil Cond. (Drys Wet, Moist) Precip, Past 24 Hrs. inches > II 5 'S a p o o o 7y w - # o o TKN mglkg Z q o ° mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4-2016 145.4 11.87 2.473 `V. WQ0031725 dry 0 Inc 1 0.3 1 82300 6490 28.1 144.738 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 01.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): OTALS: 145.41 0 . As Cd Cu Cr Pb Hg Mo Ni Se Zn P 144.73 0.000 : Lime Applied annuallbs/acre 0.035 I✓ 0.309 0.344 ✓ 36 0.010 0.095 0.105 34 0.633,1 5.26 5.893 1338 0.391 3.566 3.957 NA 0.054 0.469 0.523 267 1 0.002 0.013 0.015 15 1 0.0251 0.19 0.215 NA 0.143 1.071' 1.214' 374 0.025A 0.49 0.515 89 6.960 11.304 12:264. 2498 98.425 Date lbs/ac `rior Years Cumulative lbs/ac 11-2016 2500 .urrent Cumulative lbs/ac ermitted C. P. L. R.**** ermit PAN Limit lst/2nd Crop 214 I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false iformation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation -z 3-11 Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP-4 Annual Dry Tons Applied: 23.1121 V Site #: DP-4 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 c_-,/ Crop 2 Name: Acres Utilized: 8.7 Acres Permitted: 8.7 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: $-. o y o Q Volume applied (enter one) Solids/ Liquid Cu. Yds G811onS % Solids Volume Applied r pP per Acre D Tons/Ac (ry ) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) Soil Cond. D Wei' Moist) Precip. Past 24 His. inches y b b a � C o �' * PM o p 7y :Z F o' o TKN mglkg Z cE o �, o mg/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 2-2016 56.3 11.87 0.647 ,/ WQ0031725 dry 0 s 0.5 1 0.3 82300 6490 28.1 33.660t1 NA Fescue 3-2016 149 11.87 1.712 WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 89.082V NA Fescue 4-2016 25.9 11.87 0.298 WQ0031725 dry 0 s 0.5 0.3 82300 6490 28.1 15.48.5v.NA Fescue 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0':000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): OTALS: 231.21 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 138.227 0.000 Lime Applied �rmual lbs/acre 0.037 0.208, 0.245 ✓ 36 0.01 1,f, 0.062 0.07.3 34 0.680 3.413• 4.093 1338 0.420 2.391 2.811 NA 0.058 0.291. 6.349 267 0.002 v 0.009 0.011 15 0..027 0.124 0.151 NA 0.154 0.802 0.950 374 0.027 V 0.071 0.098 89 1.931. 7.608 8.639,E 2498 105.749 Date lbs/ac Tior Years Cumulative lbs/ac 11-2016 2000 ;urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** ertnit PAN Limit lst/2nd Crop 194..... •I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ivalified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false nformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier a- 3 •-1'1 Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 * * * Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit W #• • Q0031725 Field.. #: Dp_g AcresUtilized:_ 15.9 Land Owner: Douglas Poplin Annual Dry Tons Applied: 25.5713 V Site #• DP-5 Acres Permitted: 15.9 Operator: Douglas Poplin Predominant Soil Series: FcC2 Cation Exchange Capacity (non 503):. Crop 1 Name: Fescue Crop 1 Max PAN• 158 C ° ° 4-20 66 :-2016 1-2016 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons 574 $7.2 77.9 33.3 oho Solids 11.87 11.87 11.87 11.87 Volume Applied per Acre (Dry Tons/Ac) 0.361 v 0.548 V 0.490 V 0.209 • Soil Residual. Sources DES #, W # Cond. Q ' Fert., AnimalWe'Hrs. etc) Moist )0 WQ0031725 dry WQ0031725 dry WQ0031125 dry WQ0031725 dry 4--- rop 2 Name: Crop 2 Max. PAN: Precip. y Past 24 b o s ¢ o* inchesoi-2016 0 s 0 s 0 s 0 s C 7y 2 p; * C' ��. ;n ?» w 1XN m9/k9 Z Nitrate o andkPANppliedReceivin w Nitrite coo cre)gWaste, mg�kg mg/kg Crop 2 Name of Crop Type Residual Application Crop 1 Crop 2 0.5 0.3 82300 6490 28.1 18.778 NA Fescue 0.5 0.3 82300 6490 28.1 28.526 NA Fescue 0.5 0:3 82300 6490. 28.1 25.484 NA Fescue 0.5 0.3 82300 6490 28.1 10.894 NA Fescue 0.000 0:000 0.000 0.000 0000 0:000 0.000 0.000 0:000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0 000 0:000 Residuals Applications totals on FORM FSF supp ( attach FORM TALS: 0.000 FSF supp to this form): 255.8o As Cd I mual lbs/acre 0.023 V'0.006. Cu 0.412 Cr 0.254 Pb I H Mo Ni, Se Zn P 83.681 0.000 Lime A lies for Years Cumulative lbs/ac 0.194 0.056 3.078 2.054 0.035 O:OOI 0:016 0.093 0:016 0.624 0.281 0.009 63.998 Date lbs/ai irrent Cumulative lbs/ac 0.21.7 ✓ 0.062 3.490 2.3 88 0.114 0.729 0.059 6.796. 0.316 0.010 0.130 0.822 0.075 11-2016 1000 emitted C. P. L. R.**** 36 34 1338 NA 7.420 267 15 NA 374 89 _ mit PAN Limit lst/2nd Crop 2498 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to alified personnel properly gathered and evaluated assure that the information submitted. I am aware that there are significant for false penalties submitting brmation, including the possibility of fines and imprisonment for knowing violations." _ *Application Method: S - Surface, IN - Injection, INC - Incorporation h **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization, Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin WQ Permit #: WQ0031725 Field #: DP-6 Annual Dry Tons Applied: 11.3161 Site #: DP-6 Predominant Soil Series: FcC2 Crop 1 Name: Fescue Crop 1 Max. PAN: 158 _� Crop 2 Name: Acres Utilized: 5.5 Acres Permitted: 5.5 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° ° ° Q Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources tNPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet, Moist) Precip. Past 24 Hrs. inches y K b o' a * � C o ;h �; w � ; *MM 0 w •, CD E. * r * TKN mglkg Z q o °; o w mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5-2016 113.2 11.87 2057 WQ0031725 dry 0 s 0.5 0.3 1 82300 6490 28.1 107.055 NA Fescue 0000 0.000 0.000 0:000 0.000 1 0.0.00 0.000 0.000 0.000 0.000 0:000 0.000 0:000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): OTALS: 113.21 0 _ ........_. As Cd Cu Cr Pb H Mo Ni Se Zn P 107.055 0.000 ... Lime A lied umual lbs/acre 0.029.v 0.281. 0.310 36 0.008 p 0.082 0.090 v 34 0.527 v 4.585 5.112 v 1338 0.325' 3.238 3.563 NA _ 0.04$ 0.432 0.477 267 0.002 0.011• 0.0131 15 0.021 0.168 0.189 NA 0.119 0.86 0.979. 374 0.021 0.073. 0.094 89 0.798^' 9.747 10.545 2498 81.869 Date lbs/ac 'rior Years Cumulative lbs/ac 11-2016 2000� :urrent Cumulative lbs/ac 'ermitted C. P. L. R.**** ermit PAN Limit l st/2nd Crop 158 _. I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that ualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false iformation, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD :APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE Facility Name: Baxter Healthcare WQ Permit #: W00031725 Field #: DP-7 . Land Owner: Douglas Poplin Acres Utilized: 4.4 g P Annual Dry Tons Applied: 8.1972 Site #: DP-7 Acres Permitted: 4.4 Cation Exchange Capacity (non 503) Operator: Douglas Poplin Predominant Soil Series: FcC2 : - : Crop 1 Name: Fescue Crop 1 Max. PAN: 158 `- Crop2 Name: Crop 2 Max. PAN: Volume applied Vol -Soil - o a; o e (enter one) Solids/ o /o Applied per ieridual Sources DES #, WQ#, cip. 24 a zs n %c4 oa0.382300 Z Nitrate PAN Applied Name of Crop Type a Liquid Solids Acre ., Animals. L(D Jet o m w # K'c°4c o and (lbs/acre) Receivin Residual g Cu.. Yds G811ons (Dry Tons/Ac) Waste, etc)a o* 0 o �, Nitrite Application i-2016 82 11.87 1.863 WQ0031725 dry es 0 o og mg/kg mg/kg Crop 1 Crop:2 Crop 1 Crop 2 0.000 s 0.5 6490 28.1 96.936 NA Fescue 0.000 0.000 0.000 TALS:1 821 - inual lbs/acre or Years Cumulative lbs/ac rrent Cumulative lbs/ac mitted C. P. L. R.**** mit PAN Limit 1 st/2nd ( 0.000 0,000 0.000 0.000 0.000 0.000 0.000 OA00 . 0.000 0.000 0.000 Oe000 0:000 0;000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM'FSF supp to this form): 0.000 0.000 As 0.026 ✓ Cd I 0.007, Cu 0.477•1. Cr 0.294 I Pb I H2 Mo I Ni Se Zn P 96.936 0.000 Lime A lied 0.223. 0.06 O.Q41, 0.001 4 0.019 0.108- 0.01.9 0.723 74.147 Date lbs/ac 0.249 3414 2.319 0.315 0.01 0.127 0.818 0.07 ........... ........ 7.2.47, 11-2016 2000 • ✓ 0.067 3.891 2.613 0.356 0.011 0.146 0.926 0.089 7.970 36 34 1338 NA 267 15 NA 374 89 2498 158 certify, under penalty -of flaw, that this document was prepared under my direction or supervision in accordance' with a system designed to assure that ilified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false ormation, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate -cuiviuia http://yields.soil.ncsu.edu/index.php#count) Realistic Yields for FcB2r Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded in Wilkes County Realistic Estimated Phosphorus Crop Nitrogen Nitrogen Removal Yield Factor hate (Ibs/acre) (Ibs P205/acre) Barley (Grain) 67 Bushels 1.49 99 Corn (Grain) 129 Bushels 0.92 119 25 57 Corn (Silage) 19.6 Tons 10.9 214 67 — Cotton 637 Pounds 0.081 52 18 Sorghum (Silage) 16.7 Tons 7.6 127 Oats (Grain) 83 Bushels 1.13 50 94 21 Peanuts 0 Pounds 0 0 Rye (Grain) 49 Bushels 2.01 98 0 16 Small Grain (Silage) 8.8 Tons 11.1 98 Sorghum (Grain) 49 CWT 1.72 84 48 Soybeans (Double Cropped) 33 Bushels 0 0 37 Soybeans (Full Season) 39 Bushels 0 _ 0 27 / Soybeans (Double Cropped - Manured) 33 Bushels 3.89 130 31 Soybeans (Full Season - Manured) 39 Bushels 3.89 152 27 Tobacco (Burley) 0 Pounds 0.074 0 31 Tobacco (Flue Cured) 2548 Pounds 0.029 74 0 Triticale (Grain) 69 Bushels 1.52 104 13 Tropical Corn (Silage) 19.6 Tons 6.5 127 23 Wheat (Grain) 49 Bushels 2.01 98 67 Bahiagrass (Hay) 3.4 Tons 44 151 25 Caucasion/Old World Bluestein (Hay) 3.4 Tons 44 39 Common Bermudagrass (Hay) 3.4 Tons _ 44 151 151 41 Dallisgrass (Hay) 3.4 Tons 44 151 42 Fescue (Hay) 4.4 Tons 44 194 45 Hybrid Bermudagrass (Hay) 4.4 Tons 44 194 69 Hybrid Bermudagrass overseeded with Rescuegrass 0 Tons 44 54 (Hay) 0 0 Mixed Cool Season Grass (Hay) 3.2 Tons 44 140 Orchardgrass(Hay) 3.4 Tons 44 151 45 Pearl Millet (Hay) 3.7 Tons _ 49 50 180 49 Rescuegrass(Hay) 0 Tons 44 0 0 Sorghum Sudan (Hay) 4.2 Tons 49 204 58 Timothy Grass (Hay) 0 Tons 44 0 0 Dr. David Crouse is responsible for the development and maintenance of the Realistic Yield reporting tool. of 2 http://yields.soil.ncsu.edu/index.php#count Realistic Yields for FcC2: Fairview sandy clay loam, a to ZS percent slopes, moderately eroded in Wilkes County Realistic Estimated Phosphorus Crop Nitrogen Nitrogen Removal Yield Factor Rate (Ibs/acre) (Ibs PZOs/acre) Barley (Grain) 54 Bushels 1.49 81 Corn (Grain) 106 Bushels 0.92 97, 21,/' 4� Corn (Silage) 16 Tons 10.9 174 - 54 Cotton 520 Pounds 0.081 42 15 Sorghum (Silage) 13.6 Tons 7.6 103 Oats (Grain) 68 Bushels 1.13 77 41 Peanuts 0 Pounds 0 0 17 Rye (Grain) 40 Bushels 2.01 80 0 Small Grain (Silage) 7.2 Tons 11.1 8p 13 Sorghum (Grain) 40 CWT 1.72 69 39 Soybeans (Double Cropped) 27 Bushels 0 0 30 Soybeans (Full Season) 32 Bushels 0 0 22 Soybeans (Double Cropped - Manured) 27 Bushels 3.89 106 26 Soybeans (Full Season - Manured) 32 Bushels 3.89 124 22 Tobacco (Burley) 0 Pounds 0.074 0 26 Tobacco (Flue Cured) 2080 Pounds 0.029 60 0 Triticale (Grain) 56 Bushels 1.52 85 10 Tropical Corn (Silage) 16 Tons 6.5 104 19 Wheat (Grain) 40 Bushels 2.01 80 54 Bahiagrass(Hay) 2.8 Tons 44 123 20 Caucasion/Old World Bluestem (Hay) 2.8 Tons 44 32 Common Bermudagrass (Hay) 2.8 Tons 44 123 33 Dallisgrass (Hay) 2.8 Tons 44 123 123 34 Fescue (Hay) 3.6 Tons 44 158 37 Hybrid Bermudagrass (Hay) 3.6 Tons 44 158 57 Hybrid Bermudagrass overseeded with Rescuegrass 0 Tons _ 44 (Hay) 44 0 0 Mixed Cool Season Grass (Hay) 2.6 Tons 44 114 Orchardgrass (Hay) 2.8 Tons 44 123 37 Pearl Millet (Hay) 3 Tons 49 147 41 Rescuegrass (Hay) 0 Tons 44 0 40 Sorghum Sudan (Hay) 3.4 Tons 49 _ 167 0 Timothy Grass (Hay) 0 Tons 44 0 47 — 0 Dr. David Crouse is responsible for the development and maintenance of the Realistic Yield reporting tool. 2 of 2 Location of Samples The Plant process diagram on the flowing page shows the location of where the following samples were taken. The Analysis from Waypoint Analytical report number 16-036-0202 was taken from the Belt Filter Press, and is labeled with a red X (X on the diagram. The Fecal Coliform Samples from Statesville Analytical Sample IDs 160113-22-01, 160113-22- 02, 160113-22-03, 160113-22-04, 160127-15-01, 160127-15-02, 160127-15-02 were taken from Aerobic Digester No. 1 and is labeled with a blue X (* on the diagram. The Volatile Solids In, Sample ID Baxter A 160133-22-09 was taken from where the solids from the clarifier are pumped to the aerobic digesters and is labeled with a green X W on the diagram. The Volatile Solids Out, Sample ID Baxter B 160113-22-1.0 was taken from Aerobic Digester No. 1 and is labeled. with a blue X (* on the diagram. The TCLP test Sample ID 160113-22-08 was taken from Aerobic Digester No.1 and is labeled with a blue X on the diagram. PLAN_ WASTEWATER TREATMENT scams, j•_ aa' PLANT EVALUATION BARTER HEALTHCARE CORPORATION McDoIIE-�co�rr, NORTH CAROLMA T T Il I y,` I � I. 1 I i CLARIFIER CLARIFIER zn No.3 No.4 I I_ IV I ♦ /7` �o\P•�/ 6"CPS— — %�Q��� s"CIP—Jou' CHLORINE I CONTACT i D I CHAMBER 150,000 GALLON FILTER SLUDGE BASIN WATER FILTER WASHWATER T I I I I I _.1 I I I f I JB 12"CIP TO HOLDING BASIN Page: 1 of 2 Report Number: ° 16-036-0202 Account Number: 46381 Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 Wa Yp®intao ANALYTICAL Project: BAXTER NC CERT#257 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 2/2/2016 14:15:00 Lab Number: 66665 Date. Received: 02/05/2016 00:00 Sample Id: BAXTER Date Reported: 02/17/2016 Total Solids * 11.87 118700 100.0 JM 02/05/2016 16:00 SM-2540G Moisture * 88.13 100.0 JM 02/05/2016 16:00 SM-2540G Total Kjeldahl Nitrogen 8.23 82300 10.0 JM 02/09/2016 09:20 SM-4500-NH3C-TKN Total Phosphorus 1.99 19900 100 KM 02/17/2016 14:38 SW 6010C Total Potassium 0.86 8570 100 KM 02/17/2016 14:38 SW 6010C Total Sulfur 1.20 12000 100 KM 02/17/2016 14:38 SW 6010C Total Calcium 1.33 13300 100 KM 02/17/2016 14:38 SW 6010C Total Magnesium 0.48 4760 100 KM 02/17/2016 14:38 SW 6010C Total Sodium 0.52 5160 100 KM 02/17/2016 14:38 SW 6010C Total Iron 9860 100 KM 02/17/2016 14:38 SW 6010C Total Aluminum 2000 100 _ KM 02/17/2016 14:38 SW 6010C Total Manganese 122 5 KM 02/17/2016 14:38 SW 6010C Total Copper 128 5 KM 02/17/2016 14:38 SW 6010C Total Zinc 194 5 KM 02/17/2016 14:38 SW 6010C Ammonia Nitrogen 0.65 6490 10.0 JM 02/09/2016 09:20 SM-4500-NI3C Organic N 7.58 75810 10.0 02/09/2016 09:20 CALCULATION Nitrate+Nitrite-N 28.1 2.00 JM 02/08/2016 09:00 SM-450ONO3F Total Cadmium 2.0 2.0 KM 02/17/2016 14:38 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our p: for written authorization. Debbie Holt Page: 2 of 2 Report Number: 16-036-0202 Account Number: 46381 Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 Waypoint ANALYTICAL Project: BAXTER NC CERT#257 7621 Whitepine Road, Richmond, VA 23237 Main 804-743-9401 ° Fax 804-271-6446 www.waypointanalytical.com REPORT OF ANALYSIS Date Sampled: 2/2/2016 14:15:00 Lab Number: 66665 Date Received: 02/05/2016 00:00 Sample Id: BAXTER Date Reported: 02/17/2016 roiai Unromiurn 19 5 KM 02/17/2016 14:38 SW 6010C Total Nickel 29 5 KM 02/17/2016 14:38 SW 6010C Total Lead 11 5 KM 02/17/2016 14:38 SW 6010C Total Arsenic 7.0 3.0 KM 02/17/2016 14:38 SW 6010C Total Mercury <0.4 0.4 KM 02/08/2016 09:00 SW-7471 B Total Selenium <5.0 5.0 KM 02/17/2016 14:38 SW 6010C pH (Standard Units) * 7.97 ' 2.00 JM 02/08/2016 09:00 SW-9045D Total Molybdenum 5 5 KM 02/17/2016 14:38 SW 6010C Comments: QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al" AND "Se". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our reports and letters are for the exclusive and confidential use of our clients. and may not be reproduced in whole or part. nor may any reference be made to the work, the results, or the company in any advertising, news release, or other public announcements without obtaining our prior written authorization. Debbie Holt PAN Mineralization v v I as decimal ITotal dry tons/year IAcres Applied on 67.06 Rate 0.3 TKN 82300 NH3 64.90 NO3 28.1 NO2 0 %Solids 0.1187 136.19 PAN Surface ✓ 26016.1 I mg/kg 52.0322 lbs/dry ton 7086.265 1 lbs total PAN 105.6705 Ibs PAN/acre PAN Injection 29261.1 imglkg 58.5222 lbs/dry ton 7970.138 1 lbs total PAN 118.8509 1 lbs PAN/acre Dry Tons/1000 ual. 0.494979 1st year PAN Surface lbs. 7086265318 1st year PAN Injected lbs. 7970.138418 lbs./acre Surface 105.6705237 lbs./acre Injected 118.8508562 MR(TKN-NH3)+ + .5(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =Ibs/dry ton MR(TKN-NH3) + l(NH3)+NO3+NO2 =mg/kg mg/kg x .002 =Ibs/dry ton 1000 X 8.34 X %solids X sp. gravity 2000 "=dry tons/1 000gal. 11 SAR Sodium Absorption Ratio Na: Sodium (Mg/L) Equivalent weight: 23 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg : Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight ✓ ✓ ✓ Na M /L Ca M /L M M /L 612.49 L 1578.71 1 565.01 Na ME Ca ME 1 Ma lME) 26.63 78.9355 47.08417 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power SAR = 3.354803 (From Mg/L entered above) V SAR= 3 354932 (From ME entered below) Na (ME) Ca ME 78.93 M ME 26.63 1 47.08 The amour amount of E Permitting Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/27/2016 Reported: 01/29/2016 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 160127-15-01 Fecal Coliforms 1 �30 am) MPN/g SM92210E-2006 01/28/2016 CL 160127-15-01 Percent Solids 1 1.65 % SM2540B-1997 01/28/2016 CL 160127-15-02 Fecal Coliforms 2 31 � D MPN/g SM92210E-2006 01/28/2016 CL 160127-15-02 Percent Solids 2 1.58 % - SM2540B-1997 01/28/2016 CL 160127-15-03 Fecal Coliforms' 3 18,9.87 MPN/g SM92210E-2006 01/28/2016 CL 160127-15-03 Percent Solids 3 1.58 % SM254OB-1997 01/28/2016 CL Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 Client: s , 11 Address. Contact Person: " Via• �. � ��/ PO # Customer Sample ID# Lab -ID # Time Sampled (Grab Only) �xf�,- `7-1 V. 1Jn���r V �.9j � / • 3�j` �Tn Relinquished by: Received by: Relinquished by: Received by: Composite.Samplina #1: Tiime•begin am, pm Date Time end am, pm .Date Composite Sampling #'2: rme begin am, pm Date. Tige,end am, pm Date / / STATESVILLE ANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 28687 —' (704) 872-4697 Phone # � G s '73 .i FAX# J�6 - i a r I = �+ p Chain of Requisitioned by: (-rime Date) Custody Record Date Sampled a Matrix (Grab Only) o Slu a Parameters requested for C7 (J W WW - / d' Time ! - I V. am, r6 Date l /�' / j6 Sampled by: 7 Y� Time i f (� am, �' Date �j f 1 Transported by: z Time am, pm Date Holding times met: Time.- am, pm Date Compliance work: Non-compliance work: Lab Comments: Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/13/2016 Reported: 02/15/2016 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed Analyst 160113-22-01 Fecal Coliforms 1 28;90 MPN/g SM92210E-2006 01/13/2016 WL 160113 -22-01 Percent Solids 1 1.73 % SM254OB-1997 01/13/2016 WL 160113-22-02 Fecal Coliforms 2 150943� MPN/g SM92210E-2006 01/13/2016 WL 160113-22-02 Percent Solids 2 1.59 % SM254OB-1997 01/13/2016 WL 160113-22-03 Fecal Coliforms 3 149 068 MPN/g SM9221 CE-2006 01/13/2016 WL 160113-22-03 Percent Solids 3 1.61 % SM254OB-1997 01/13/2016 WL 160113-22-04 Fecal Coliforms 4 �8,97 MPN/g SM9221 CE-2006 01/13/2016 WL 160113-22-04 Percent Solids 4 1.75 % SM254OB-1997 01/13/2016 WL Respectfully submitted, "Op'-WVV ` ,6)t I Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 3 Condition of Receipt s ample Number 160113-22-01 Tem on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 160113-22-02 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 160113-22-03 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 160113-22-04 Temp on Arrival - Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Fecal Coliforms Sodium Thiosulfate Received on Ice Sample Number 160113-22-08 Temp on Arrival: Parameter Schedule: Reactivity Received on Ice Parameter Schedule: Corrosivity Received on Ice Parameter Schedule: Ignitability Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 3 Client: 6,n: Address: L�ID v1y-tlContact Persrei.., C PO # 17 Customer Sample ID# Lab-lD # o2. 8�rV C Relinquished by: - il-, Received by: I��� �✓V' Relinquished by. - Received by: Composite Sampling #1 Time begin am, pm Date_J_/_ Time end am, pm Date Composite Sampling #2- Time begin am, pm Date Time end am, pm Date STATESVILLE ANALYTICAL - 122 Court Street • P.O. Box 228 Statesville, NC 28687 • ('164) 872- 697 a Phone # 336 _ S _ �, ,� FAx# 33� 61 Li p Chain of Requisitioned by: (rime Date) Custody Record Date Sampled a. Matrix (Grab Only) o �� a TP.aramet�ersrequested for analysis 9 W +-1�3-1 �ta.) :. Time 3 , am, Jm Date / 3/( )� Sampled by: Time 3. j am,60 Date '. /� J_&" Transported by: Y_f, /_ tr Time -am, pm Date Holding times met: Time am, pm Date _/_/_ / Compliance work: ✓ Non-compliance work: Lab Comments: VS in 0.0133 VS out 0.0054 VSFR= 0.59721 Do UO-71"J ,E�133" o o -7 d c.3 2T Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/13/2016 Reported: 02/03/2017 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed 01/94/2016 01/14/2016 Analyst WL WL 160113-22-09 160113-22-09 % Volatile Solids Percent Solids Baxter A Baxter A 1.33 1.60 % SM254OG % sM254os-1997 Respectfully submitted, �QP.-w ,j"'It , Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 1 of 2 Condition of Receipt Sample Number 160113-22-09 Temp on Arrival: Parameter Schedule: Percent Solids Parameter Schedule: Received on Ice Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 2 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River, NC 28669 Receive Date: 01/13/2016 Reported: 02103/2017 For: Baxter Comments: Sample Number Parameter Sample ID Result Unit Method Analyzed 01/14/2016 01/14/2016 Analyst WL WL 160113-22-10 160113-22-10 % Volatile Solids Percent Solids Baxter B Baxter B 0.54 0.81 % SM2540G % SM2540B-1997 Respectfully submitted, ,Op - a, J'n t Dena Myers NC Cert #440, NCDW Cert #37755, EPA #NC00909 PO Box 228 • Statesville, NC 28687 i 704/872/4697 Page 1 of 2 Condition of Receipt _Sample Number 160113-22-10 Temp on Arrival: Parameter Schedule: Received on Ice Parameter Schedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 2 of 2 Client: (J tt� T Y\ = 'Address- ( l ftj STATESVII.LE ANALYTICAL 122 Court Street • P.O. Box 228, lJ N r . ,n Statesville, NC 28687 , c704) 872- 697 .... o 'Contact Person: r Phone # . `` !, 36- A S� - �S'�1 FAX# 3 3 ' gs-1 `ty0 Chain of PO # Requisitioned by: (rime Date) Custody Record '4 Customer Sample ID# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only) a a Matrix Parameters requested for analysis Sludge W WW 1 %3 „.,. 3- Relinquished by:j Received by; Relinquished by: Received by: Composite Sampling #1: Time begin am, pm Date _/_/_ Time end am, pm Date_/_/_ Composite Sampling #2- Time begin am, pm Date time end am, pm Date / - I I F- X V/d VS . • Time ` I S am, pm Date 1 / 13/ 1 � Sampled by: Z !Ar . Time �� . �� am, pi Date / Transported by: Time am, pm Date Holding times met: f Time am, pm Date Compliance work: Non-compliance work: Lab Comments: aceAnalytical WWW,pacalabs.cm ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 160113-22-08 Pace Project No.: 92283107 Sample: 160113-22-08 Lab ID: 92283107001 Collected: 01/13/16 13:47 Received: 01/14/16 10:45 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions, Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/25/16 14:30 gamma-BHC (Lindane) Chlordane (Technical) ND ug/L 0.50 1 01/26/16 11:30 01/26/16 16:25 58-89-9 Endrin ND ug/L 3.0 1 01/26/16 11:30 01/26/16 16:25 57-74-9 Heptachlor epoxide ND ND ug/L 0.50 1 01/26/16 11:30 01/26/16 16:25 72-20-8 Methoxychlor ug/L 0.50 1 01/26/16 11:30 01/26/16 16:25 1024-57-3 Toxaphene ND ug/L 1000 1 01/26/16 11:30 01126/1616:25 72-43-5 Surrogates ND ug/L 3.0 1 01/26/16 11:30 01/26/16 16:25 8001-35-2 Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) 74 % 10-138 1 01/26/16 11:30 01/26/16 16:25 2051-24-3 70 % 10-110 1 01/26/16 11:30 01/26/16 16:25 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-D 2,4,5-TP (Silvex) ND mg/L 0.010 1 01/22/16 08:20 01/23/16 04:58 94-75-7 Surrogates ND • mg/L 0.010 1 01/22/16 08:20 01/23/16 04:58 93-72-1 2,4-DCAA (S) 93 % 42-142 1 01/22/16 08:20 01/23/16 04:58 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010A Leachate Method/Date: EPA 1311; 01/15/16 20:10 Initial pH: 7; Final pH: 5 Arsenic Barium ND mg/L 0.060 1 01/20/16 00:20 01/20/16 11:47 7440-38-2 Cadmium ND mg/L 0.25 1 01/20/16 00:20 01/20/16 11:47 7440-39-3 Chromium ND mg/L 0.0050 1 01/20/16 00:20 01/20/16 11:47 7440-43-9 Lead ND mg/L 0.025 1 01/20/16 00:20 01/20/16 11:47 7440-47-3 Selenium ND mg/L 0.025 1 01/20/16 00:20 01/20/16 11:47 7439-92-1 Silver ND mg/L 0.10 1 01/20/16 00:20 01/20/16 11:47 7782-49-2 ND mg/L 0.025 1 01/20/16 00:20 01/20/16 11:47 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/15/16 20:10 Initial pH: 7; Final pH: 5 Mercury ND r mg/L 0.00020 1 01/25/16 11:45 01/25/16 15:09 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01125/1614:30 1,4-Dichlorobenzene 2,4-Dinitrotoluene ND ug/L 50.0 1 01/26/1613:15 01/27/1616:15 106-46-7 Hexachloro-1,3-butadiene ND ND ug/L ug/L 50.0 1 01/26/1613:15 01/27/1616:15 121-14-2 Hexachlorobenzene ND ug/L 50.0 1 50.0 01/2611613:15 01/27/1616:15 87-68-3 Hexachloroethane ND ug/L 1 01/26/1613:15 01127/1616:15 118-74-1 2-Methyl phenol(o-Cresol) ND ug/L 50.0 1 01126/1613:15 01/27/1616:15 67-72-1 3&4-Methylphenol(m&p Cresol) ND ug/L 50.0 1 50.0 01/26/1613:15 01/2711616:15 95-48-7 Nitrobenzene ND 1 01/26/16 13:15 01/27/16 16:15 Pentachlorophenol ND ug/L 50.0 1 01/26/1613:15 01/27/1616:15 98-95-3 Pyridine ug/L 100 1 01/26/1613:15 01/27/1616:15 87-86-5 2,4,5-Trichlorophenol ND ND ug/L 50.0 1 01/26/1613:15 01/27/1616:15 110-86-1 2,4,6-Trichlorophenol ND ug/L 50.0 1 01/26/1613:15 01/27/1616:15 95-95-4 ug/L 50.0 1 01/26/1613:15 01127/1616:15 88-06-2 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 02/12/2016 04:24 PM without the written consent of Pace Analytical Services, Inc.. Page 4 of 23 aceAnalytical wwx!pacelabs.com ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 160113-22-08 Pace Project No.: 92283107 Sample: 160113-22-08 Lab ID: 92283107001 Collected: 01/13/16 13:47 Received: 01/14/16 10:45 Matrix: Solid Results reported on a "dry weight" basis and are adjusted for percent moisture, sample size and any dilutions. Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/25/16 14:30 Surrogates Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) 33 % 12-102 1 01/26/16 13:15 01/27/16 16:15 4165-60-0 Terphenyl-d14 (S) 37 % 78 13-107 1 01/26/16 13:15 01/27/16 16:15 321-60-8 Phenol-d6 (S) 16 % 21-132 1 01/26/16 13:15 01/27/16 16:15 1718-51-0 2-Fluorophenol (S) 24 % 10-110 1 01/26/16 13:15 01/27/16 16:15 13127-88-3 2,4,6-Tribromophenol (S) 36 % 10-110 1 01/26/16 13:15 01/27/16 16:15 367-12-4 27-108 1 01/26/16 13:15 01/27/16 16:15 118-79-6 8260 MSV TCLP Analytical Method: EPA 8260 Leachate Method/Date: EPA 1311; 01117/16 10:43 Benzene 2-Butanone (MEK) ND ug/L ND 100 20 01/21/16 14:48 71-43-2 Carbon tetrachloride u /L 9 ND ug/L 200 20 01/21/16 14:48 78-93-3 Carbonenzene ND ug/L 100 20 01/21/16 14:48 56-23-5 Chloroform ND ug/L 100 20 01/21/16 14:48 108-90-7 1,4-Dichlorobenzene ND ug/L 100 20 01/21/16 14:48 67-66-3 1,2-Dichloroethane ND ug/L 100 20 01/21/1614:48 106-46-7 1,1-Dichloroethene ND ug/L 100 20 01/21/16 14:48 107-06-2 Tetrachloroethene ND ug/L 100 20 01/21/16 14:48 75-35-4 Trichloroethene ND ug/L 100 20 01/21/16 14:48 127-18-4 Vinyl chloride ND ug/L 100 20 01/21/16 14:48 79-01-6 Surrogates 100 20 01/21/16 14:48 75-01-4 1,2-Dichloroethane-d4 (S) 100 % 70-130 20 Toluene-d8 (S) 111 ° /° 01/21/16 14:48 17060-07-0 4-Bromofluorobenzene (S) 99 % 67-135 20 01/21/16 14:48 2037-26-5 70-130 20 01/21/16 14:48 460-00-4 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 98.3 % 0.10 1 01/15/16 07:04 1010 Flashpolnt,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 01/27/16 11:20 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 6.9 Sid. Units 0.10 1 . 01/18/16 14:50 733C S Reactive Cyanide Analytical Method: SW-846 7.3.3.2 Cyanide, Reactive ND mg/kg 60.1 1 01/19/16 23:47 735S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Sulfide, Reactive ND mg/kg 601 1 01/19/16 16:25 Date: 02/12/2016 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 23 auuftlytical WW1V./J8CBi8t18.COrn ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 160113-22-08 Pace Project No.: 92283107 Sample: 160113-22-08 Lab ID: 92283107002 Collected: 01/13/16 13:47 Received: 01/14/16 10:45 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8082 GCS PCB Analytical Method: EPA 8082 Preparation Method: EPAL3510 PCB-1016 (Aroclor 1016) PCB-1221 (Aroclor 1221) ND ug/L 5.0 1 02/11/16 16:30 02/12/16 12:32 12674-11-2 PCB-1232 (Aroclor 1232) ND ND ug/L ug/L 5.0 1 02/11/16 16:30 02/12/16 12:32 11104-28-2 PCB-1242 (Aroclor 1242) ND ug/L 5.0 1 02/11/16 16:30 02/12/16 12:32 11141-16-5 PCB-1248 (Aroclor 1248) ND ug/L 6.0 1 02/11/16 16:30 02/12/16 12:32 53469-21-9 PCB-1254 (Aroclor 1254) ND ug/L 5.0 1 02/11/16 16:30 02/12/16 12:32 12672-29-6 PCB-1260 (Aroclor 1260) ND ug/L 5.0 1 02/11/16 16:30 02/12/16 12:32 11097-69-1 Surrogates 5.0 1 02/11/16 16:30 02/12/16 12:32 11096-82-5 Decachlorobiphenyl (S) 37 % 10-132 1 02/11/16 16:30 02/12/16 12:32 2051-24-3 9095 Paint Filter Liquid Test Analytical Method: EPA 9095 Free Liquids FAIL 1.0 1 02/11/16 12:55 Date: 02/12/2016 04:24 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 6 of 23 Parameter Schedule: TCLP Received on Ice Parameter Schedule: Received on Ice Sample Number 160113-22-09 Temp on Arrival: Parameter Schedule: Percent Solids Received on Ice Parameter Schedule: Received on Ice Sample Number 160113-22-10 Temp on Arrival: Parameter Schedule: Received on Ice Parameter Schedule: Percent Solids Received on Ice PO Box 228 • Statesville, NC 28687 • 704/872/4697 Page 3 of 3 Client: 0 v 1 l2 r t, S m .' v; rs 'S ,t , Address: 9 S STATES VILLE ANALYTICAL 122 CourtStreet % P.O. Box 228 roar: srr � no ai {. N L �� k Statesville, NC 28687 �...q (704) 8724697 . Contact Person: Phone # q G�13r FAX# t Chain of Requisitioned by: Crime Date) Custody Record Customer Sample ID# Lab -ID # Time Sampled . (Grab Only) Date Sampled a a (Grab Only) CU Matrix Sludgew VJw Parameters requested for analysis jj ° re. 1 ' , s s s s i i t S Relinquished by: Time 1 am;jPmDate%/3/ Sampled by: Received by: �'{ l�J� ��' Time 1 am,ate� I? _ l/' t� Transported by: Z 1� ' J — — — Relinquished by: Time am, pm Date —/_/ ✓� Holding times met: Received by: Time am, pm Date Composite Sampling #1: Compliance work: Time begin am, pm Date _/ / Non-compliance work: Time end am, pm Date Lab Comments: Composite Sampling #2: Time begin am, pm Date _I / Time end am, pm Date _/ /_ ► riiiutu, rt�ltivhLlr A1VL VrUTUH A TRACTION REDUCTION FORM (02T Rules) Facility Name: Baxter Healtcare Corporation WQ Permit Number: WQ0031725 WWTP Name: Baxter Healtcare Corporation NPDES Number: NC0006564 Monitoring Period: From 1/1/2016 ,% To 12/31/2016 }/ Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testis A1t.D (No Prior Test) ❑ Process to Further Reduce Pathoae ble to alternative performed (Cl 111 Heat Drying ❑ ❑ 1 Gamma Ray ❑ Class B: I Alt. (1) Fecal Density If applicable to alternative performed (Cl, Lime Stabilization ❑ Air Anaerobic Digestion ❑ ble to alternative Parameter Fecal Coliform (in lieu of fecal Vector Allowable Level in Sludge 2 x 10 to the MPN 6th power per gam of total solids CFU 1000 mpn per gram of total solid (dry 3 MPN per 4 grams total solid (dry iss A only) indicate "Process to Further Reduce Pathog Heat Treatment ❑ ThermopY Pasteurization ❑ Process to Significantly Reduce Pathoge iss B only) indicate "Process to Significantly Reduce Pa Drying ❑ I Composting ❑ Aerobic A or Class B) complete the Geo. MeanjMaximunr Units gs �J ,estion ❑ wowing monitoring data: umber ot Frequency Sample a ytic Excee- Tech- dences of Analysis Type 18987 44229.7 150943 MPN/g 0 NVAC mT 1111171 _ 'Di.,...,,._i --- 7 1 grab I sm9221 Alt.1 (VS reduction) 21 -- • i Alt. 2 (40-day bench) ❑ ------.---..+.vww saswaasauvG "U'l1VI- III Cui Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ C'FR TTFTC' A Truly CT A TlWl%XVIrm 1 -i... _ _L - _,_ �.- . - W .."%AI,. 11,.c Appi upi-,ate statement) R1 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T 1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an .explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." � A 4 h, 9-4L r- `ng/ Dennis Key Southern Soil Builders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* � '�--` p Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) r)Gnlp Crnone ONIMC nn+ .� ,,...,... NCDA&CS Agronomic Division Phone: (919) 733-2655 hV Predictive Soil Report `'t •.tk.vur.5, Website: wmw.ncagr.gov/agronomi/ Client: Doug Poplin 594 Austin Little Mtn Rd Ronda NC 28670 Mehlich-3 Extraction Sampled County: Wilkes Sampled: 10/31/2016 Received: 11/03/2016 Completed: 11/18/2016 Farm: Sam=History: Recommendations: Lime - Nutrients (Ib/acre) Crop (tons/acre) N P2O5 K2O Mg S Mn Zn Cu Lim1_ Fescue/OGrass/Tim, M 0.0 120-200 0 0 0 2_ 0 0 0 0 Test Results [units - WN in g/cnf; CEC and Na in men/100 crrA NO N • —1 Report No. FY17-SL012128 3r: Zach Key Southern Soil Builders, Inc. 958 Hoots Rd Roaring River, NC 28669 Links to Helpful Information More B Information 0 Note: 12 3- m mg/d j: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn Al2 J Zn-1 Zn-AI 0.27 0.94 19.5 94. 1.1 6.5 ✓ 483 580 50 29 319 256 Cu-fl Na S Sample ID: DPI Recommendations: Lime 164 772 772 965 0?g 4 Crop (tons/acre) N Nutrients (lb/acre) Lime History: 1=Fescue/OGrassrrim, M 0.0 P2O5 K2O 120-200 Mg S M° Zn Cu B 2- 0 0 0 0 0 0 0 0 Test Results [units - WN in g/cnr ; CEC and Na in MOO cO- NO3-N . ldrrr� HM% WN CEC \ BS% In mg ]. Soil Class: Mineral 0.36 Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI Cu-I 0.89 15.0 Sample ID: DP1C V 90 1.6 5.9 304 308 Recommendati 53 26 227 147 105 969 969 700• Lime Crop (tons/acre) Nutrients (lb/acre) Lime History: 1 - Fescue/OGrass/Tim, M 1.0 - N P2O5 120-200 K2O M g S Zn Cu 2- 0 0 0 0 0 p 0 0 Test Results [units - WN in glcrrP; CEC and Na in meq/100 crrP; NO3-N in mg/dd]: HM% WN CEC BS% Ac P-1 K-1 Soil Class: Mineral 0.36 0.94 13.3 /pH Ca% Mg% S-1 Mn-I Mn-All Mn AI2 Zn4 Zn-AI Cu-1 84 2.2 5.5 243 188 55 21 73 147 105 927 927 1164 North Carolina [A, hacc+, ?Icnt Fm;d Cuaam+�l.�r+ SS-1 NO3-N More Information Note: 12 Na ESP SS-1 NO3-N 0.5 3 More B Information 0 Note: 12 Na ESP SS-1 NO3-N 0.1 1 Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Trox NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ i Report No. FY17-SL012128 Doug Poplin - Sample ID: DP1 D Recommendations: Lime Page 2 of 4 � Nutrients (lb/acre) Lime History: Crop (tons/acre) 1- Fescue/OGrass/Tim, M 0.0 N P2O5 120-200 K2O Mg S Mn Zn ' Cu B More Information 2- 0 0 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cO; CEC and Na in meq/100 cnr3; NO3-N in mg/d0]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-I Zn-AI ' Cu-I Na ESP 0.32 0.97 12.9 89 1.4 6.3 189 130 57 27 50 93 69 SS-1 NO3-N Sample ID: DP2 ,� .Recommendations: Lime 696 696 733 0:1, 1 Nutrients (lb/acre) Lime History: Crop (tons/acre) 1 -Corn, silage 1.1 N PzOS K20 Mg S Mn Zn Cu More B Information 2- 180-220 0 40 0 0 0 0. 0 0 Note:3 Test Results [units - WN in g/cO; CEC and Na in meq/100 crrr3; NO3-N in mg/dnP]: Soil Class: Mineral HM% WN CEC BS% Ac H P P-1 K-1 o o Ca /o Mg /o S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na 0.51 0.98 9.7 78 2.1 5.3 152 81 50 24 99 ESP -'SS-I NO3-N Sample ID: DP3C Recommendati Lime 78 64 590 590 671 0.1 1 / Crop (tons/acre) Nutrients (Ib/acre) More N P2O5 K2O Mg S Lime History: 1-Fescue/OGrasslrim, M 1.5 120-200 0 0 Mn Zn Cu B T Information 2- 0 0 0 0 0 01 Note: 12 Test Results [units - W/V in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/deft Soil Class: Mineral HM% W/V; CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP 0.46 1.11 7.3 70 2.2 4. 163 91 44 20 57 103 79 SS-1 NO3-N Sample ID: DP3G / Recommendatis:_ Lime 297 297 192 0.1 1 '✓ Crop (tons/acre) Nutrients (lb/acre) More N P2O5 K2O Mg S Lime History: 1 -Corn, silage 1.7 180-220 0 120 Mn Zn 0 0 Cu B Information 2_ 0 0 0 0 Note: 3 Test Results [units - W/V in g/crrP; CEC and Na in meq/100 cO; NO3-N in mg/dO]: Soil Class: Mineral HM% W/V CEC BS% Ac p P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP 0.46 0.97 8.8 69 2.7 4.9 102 40 47 19 55 110 83 SS -I NO3-N 463 463 198 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: vwvw:ncagr.gov/agronomi/ + Report No. FY17-SLO12128 Doug Poplin Page 3 of 4 Sample ID: DP4 / V Recommendations: Lime Nutrients (Ib/acre) Lime History: Crop (tons/acre) N P205 1- Fescue/OGrass/Tim, M 1.0 120-200 0 K20 Mg S Mn Zn Cu B More Information 2- 30 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dnP]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.97 12.0 82 2.2 .5 173 57 55 25 57 111 84 835 835 697 0.1 1 Sample ID: DP5 Recommendatio : Lime Nutrients (lb/acre) Lime History: Crop (tons/acre) N P205 1-Fescue/OGrass/Tim, M 0.3 120-200 K20 Mg S Mn Zn Cu B More Information 0 2- 10 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/cO; CEC and Na in meq/100 crn3; NO3-N in mg/do]: Soil Class: Mineral - HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.60 0.92 12.5 85 1.9 r. ° 123 70 55 27 53 97 75 102 1028 687 0.1, 1 Sample ID: DP6 V Recommendati§9: Lime Nutrients (lb/a e) Lime History: Crop (tons/acre) N P205 1-Fescue/OGrassfFim, M 1.2 120-200 K20 Mg S Mn, --Zn Cu B More Information 0 2- 0 0 0 0- 0 0 0 Note: 12 Test Results [units - WN in g/crrP; CEC and Na in meg1100 cmP; NO3-N in mg/drr?]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 1.14 0.92 11.2 79 2.4 F5 4 70 156 45 27 59 108 82 757 757 456 0.1 1 Sample ID: DP7 Recommendation '. Lime Nutrients (lb/acre) I Lime History: Crop (tons/acre) N P205 1- Fescue/OGrass/Tim, M 0.7 120-200 K20 Mg S Mn Zn Cu B More Information 0 2- 20 0 0 0 0 0 0 Note: 12 Test Results [units - WN in g/crap; CEC and Na in meq/100 co; NO3-N in mg/dni]` Soil Class: Mineral HM% WN CEC BS% Ac H P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.97 11.4 82 2.0 (5,".9 173 65 56 24 52 87 69 764 764 624 0.1 1