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WQ0031725_Annual Report_20150223
Annual Report Review SOP Class B Land Application Reporting Period: l �P A01 L /Z/31 lao/y Permit Details: 13OX- e- La.�d DPP_ to Q 00 3 l 7,2 Is 503? . P--S Class A or B? Maximum Dry Tons Per, Year: 200 • Number of acres permitted: l Ito •&),2 Number of fields in permit: I L-[ Counties that land is permitted for: ` lkgf Monitoring Frequency for TCLP: llh Monitoring Frequency for Residuals Analysis: e ay4 ©'' P T Monitoring Frequency for Pathogen & Vector Attraction -Reduction: z,"a-8 - d -' .D T. Groundwater monitoring: N/A:. 1. Annual Land Application Certification Form • Was a certification form submitted? y-P 5 Was land application conducted during the reported year? V -e:.S How many dry tons and dry tons per acre were applied? td to S Were the applications within the permitted amount? Y. —&X Verify PAN if more than 10 tons/acre?: • -Did it indicate compliance? �( Was it signed by the appropriate people? ye-f 2. Monitoring f Were the analyses conducted at the required frequency? y 41r, Was an analyses taken for each source that was land applied? y e-5 Were the metals analyses reported on the Residual Sampling Summary Form? YES Were the results'reported in mg/kg? y Were the pH's 6.0 or greater for each residual sample?,/el}' Were the heavy metals within ceiling concentration permit limits? y.,QS Were the lab analyses attached? Were all the required parameters tested? y e F Was TCLP analysis conducted? Xj Were the TLCP contaminants wn regulatory limits? yes Was a corrosivity, ignitability, and reactivity analysis conducted? y C5 3. Field Summary _Were_the._landapplication events_recorded;on_theF-ieldSummarXForms?it?=.X.--=.-.------ -.------•---,---- How many fields were applied on. this year? Was a Field Summary Form submitted for each field?e.5 . Were all the residuals applied to permitted land?, �' Were all the residuals applied from permitted sources? y-'-5 Were the field loading. rates for each metal and PAN calculated (year to date)? y� Were the cumulative pollutant loading rates calculated? Yle S, Were the calculations correct? 5 Were the PAN loading rates within permit limits? y�r Were the heavy metal cumulative pollutant loading rates within permit limits? ',f S ^ Were the residuals applied on a suitable crop? BAN I 61hIA p P 2 - cor, oc-_ L 0 �_ `C^ C_ U � . (" LOi 0' V 1 4n 3 Were the applications conducted during the crop's growing season? DP. 2 Were the Field Summary Forms complete?�-5 Was lime application on Field Summary Form? No lime applied. OP 2- PP3 (cow., 4_1M5s' bPf C)PC2 DP7 4. Pathogen and Vector Attraction Reduction Was a signed copy of the Patho e and Vector Attractio Reduction Form submitted? x� s Pre�� ` Did the form indicate the perio of�verage; the resi ual class, and the pathogen reduction SN alternative and the vector attraction reduction option used? Was the appropriate documentation to show pathogen and vector attraction reduction included in the report? Was pathogen and vector attraction reduction demonstrated according to 40 CFR Part 503? Class B Pathogen Review Alternative 1 -Fecal Coliform Density Was the sampling conducted at the required frequency? Y'r Were seven samples taken? y ,11f Was the geometric mean calculated and done correctly? S Did the results show compliance (less than either 2,000 00 MPN/gram of total solids or 2,000,000 Colony Forming Units/gram of total solids)? y 2 T Alternative 2 = Use of Process to Significantly -Reduce Pathogens (one of five) Was the sampling conducted at the required frequency? 1. Aerobic Digestion Was it an aerobic process (Inspection)? Were logs submitted showing time. andtemperature? Were temperatures within range for,completetime period? Was the time and temperature between 40 days at 20°C (68T) and 60 days at 15°C (59°F)? 2. Air Drying • Were the residuals on sand beds or pave or unpaved basins -for three months? Was the ambient temperature above 0°C (32T) for two months? Were the residuals partially digested? Were residuals exposed to atmosphere during two months above 0°C (not snow covered)? 3, Anaerobic Digestion • Was it an anaerobic process (Inspection)? • Were logs submitted .showing time and temperature? - - -Were temperatures within range for complete time period? Was the time and temperature between 15 days.at 35°C (95T) to 55°C (131T) and 60 days at 20°C (68°F)? 4. Composting (usually will be; Class'A when composting is used) Was it a composting procedure (riot natural decay under. uncontrolled conditions)? Were logs submitted showing time and temperature? Was the temperature raised to 40 5. Lime Stabilization • Was alkaline material -added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? Were logs submitted showing time and temperature? Was the pH raised to 12 after two hours of contact? Were logs submitted showing time and pH? Was temperature corrected to 25°C (77°F)? Alternative 3 Use of Processes Equivalent to RSRP (Not commonly use. See White House Manual page 100-103, tables 11-1 and 11-2.) Vector Attraction Reduction Review • Was the sampling conducted at the required, frequency? Option 1 — 38% Volatile Solids Reduction Was there 38%o reduction? Ye s Were lab sheets/calculations in report?� s Was the reduction on volatile solids (not total solids)?,I- Were the samples taken at beginning of digestion process and before application (Inspection)? YES • Were calculations correct? j' Option 2 — 40-Day.Bench Scale Test Were residuals from anaerobically digested treatment (Inspection)? Were residuals anaerobically digested in lab'� Was the test run for 40 days? Was the test done between 30°C (86°F) and 37°C (99°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 17%? Were lab sheets/calculations iri report? Were calculations correct? Option 3 — 30-Day Bench Scale Test . Were residuals from aerobically'digested treatment (Inspection)? Were residuals aerobically digested in lab? Were residuals 2% or less total solids? If not 2% total solids, was the test ran on a sample diluted to 2% with unchlorinated effluent? Was the test run for 30 days? Was the test done at 20°C (68°F)? Was the reduction of on volatile solids (not total solids)? Was the reduction less than 15%? Were lab sheets/calculations in report? Were calculations correct? Option 4 — Specific Oxygen Uptake Rate(SOUR) Were residuals form aerobically digested treatment (Inspection)? Were residuals 2% or less total solids (dry weight basis) (not diluted)? • Was the test done between 10°C (50°F) and 300C (86°F)? Was the temperature corrected to 20°C (680F)? Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)? Was thez sampling holding time two hours? Was the test started within 15 minutes of sampling or aeration maintained? Option 5 —14-Day Aerobic Process Were the residuals from aerobically digested treatment (Inspection)? Were the residuals treated for 14 days? Was the residuals temperature higher than 40°C (104°F) for a 14-day period? Was the average residuals temperature higher than 45°C (113°F)? Option 6 — Alkaline Stabilization - Was the pH of the residuals raised to 12 or higher by the "addition of alkali? Did the pH of residuals remain at 12 or higher for two hours without the addition of more alkali? Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? " Was the pH corrected to 25°C (771F)? Option 7 — Drying of Stabilized Residuals Does. the residuals contain any unstabilized residuals? Were the residuals mixed with any other materials? Were the residuals dried up to 75% total solids? Option 8 — Drying of Unstabilized Residuals Were the residuals mixed with any other materials? Were the residuals dried to 90% total solids? Option 9 — Injection Was there any significant amount of residuals on land surface one hour "after injection (Inspection)? : Was injection done on pasture or hay field? Was injection done at time that crop was growing? If Class A with"respect to pathogen, were residuals injected with eight hours after discharge from pathogen treatment? Soil Tests Was a Standard Soil Fertility Analysis conducted for each application field? Y_5 Were the'soil pH's 6.0 or greater for each application field? 1Jo DP2-, 3C, 3CV,'410 6, 7 = a L( 46 If no, was lime applied to those fields? jleS Were the copper and zinc indexes in the soil les§than 2000 for each application.field? y.. S Was sodium less than 0.5 meq/100 cm^3? �-e'S - Was the exchangeable sodium percentage (ESP) less than 15%? 1,65 6.General • Was the report in the proper format? Y14e.,5 • Was the annual report complete?Yl" Was the report submitted on time?� — f : r: JJJ 4 I f I _ f is • �� � Y,�� ��'� + � ss w3, � �+r•. 6?. 'h'�3+. ""+% k k��R W7' �fF'km - m _ M�� E s � ed^ y �? �'6#r'a'.4 2t ,.y ...� xi` .4,y ._.�;� � '��• � . �� �, '�._` - y �V..Jd �iY '2 P' 'r. r< WON l i MA M W` i ii� .0 Baxter Healthcare Baxter Healthcare Corporation 2014 Annual Report Land Application Program NC Permit No. WQ0031725 EOF- it E® FEB 21 '2015 DWR SECTION INFORMATION PROCESSING UNIT RECENED Division of Water Resources MAR - 9 2015 Water Quality Regional Operations Asheville Regional Office ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Permit#: WQ0031725 County: McDowell Year: 2014 Baxter Healthcare Facility Name (as shown on permit): Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909 Land application of residuals as allowed by the permit occurred during the past calendar year? 21"Yes ® No - If No, skip Part A, and Part B and proceed to Part C. Also, If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary. Total number of application fields in thepermit: 14 Total number of fields utilized for land application during the year: 7 Total amount of dry tons applied during the year for all application sites: 108.5 Total number of acres utilizes for land application during the year: 43.81 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2014 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Resources. U1110yes El No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. I ) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T . 1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .1105(b),(applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T . I I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Resources. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 11) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters has occurred. 13) All buffer requirements as specified on the permit were maintained during each application of residuals. Part C - Certification: "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate, and complete. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Permittee Name and Title (type or print) a-y�) Z i 15 'k!knature of Permittee Date 0-.7-IT Signature of Preparer* Date Applier Date (if different from Permittee) (if different from Permittee and Preparer) * Preparer is defined in 40 CFR Part 503.9 (r) and 15A NCAC 02T .l 102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Facility Name: Baxter Healthcare Residual Source WQ # or NPDES #: WWTP Name: Residual Annlvcic data WQ0031725 Baxter Healthcare Laboratory: 1) 2) 3) 4) 5) A&L Eastern Labs. Parameter (mg&g) Cone. Limit m a Sample or Composite Date 1-22-14 Percent Solids (%) NA 9.75✓ Arsenic 75 8 ✓ Cadmium 85 2 Copper 4,300 118 L Chromium NA 74 v Lead 840 12 Mercury 57 0.6 Molybdenum 75 5 Nickel 420 25 Selenium 100 5 s/ Zinc 7,500 305 Total Phosphorus NA 14800 TKN NA 111000 Ammonia -Nitrogen NA 7900 Nitrate and Nitrite NA 18.5 - -1 - -- --- - Wb �� ��•.�..�..,u ..... .."«u iu ulib tv1u1 a1G nun appucame. xeierence ttie mdlvldual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." (1 n 1- of Preparer z /1 7 // 5- Date L *Preparer is defined in 40 CFR Part-503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) r' ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare WQ0031725 Total Dry Tons Applied (Annual): Cation Exchange Capacity (non 503 only): 9.93 Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 5.02 Acres Permitted: 5.02 Site #: DP2 Field #: DP2 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg. % Solids nse Raw PerePnt M- ...a Com- posite Date, © I d Total Phos-�MEEEEEEEEEEE Annual heavy ivletai riela Loadings (Calculated in lbs/acre): Total 121 L3J 4 151 6 L7 8 9 10 11 12 DT/Ac./ App. ✓ a Event 1.98 v.y Arsenic 0.032/ 1 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.032 Cadmium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Copper 0.467 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.467 Chromium 0.293 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.293 Lead 0.047 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.047 Mercury 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Molyb- denum 0.020 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Nickel 0.099 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.099 Selenium 0.020 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.020 Zinc 1.207 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1.207 Total Phos- 58.578 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 58.578 horus I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". /;�I_ A�- Si ature of La Applier ' -)-I S Date nr:klo ar1DKA hACI CC !4nl0nn0\ it, ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 16.05 Permit #: Operator: Acres Used: WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 5.877 Acres Permitted: 5.877 Site #: DP3-Corn Field #: DP3-Corn Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg,mg/kg, % Solids use Raw Percent #): Com- posite Total Phos- phorusMENEEMENEENE Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total LjJ 1 21 3 4 5 6 1 7j 8 9 10 11 12 DT/Ac./ App. 5, W Event 2.73 n Arsenic 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.645 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.645 Chromium 0.404 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0'.404 Lead 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 Nickel 0.137 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.137 Selenium 0.027 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.027 Zinc 1.666 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.666 Total Phos- 80.838 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 80.838 horus "1 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Si ature of Lan pplier a-3�►s Date DENR FORM MFLSF (12/2006) X ANNUAL MKFALS FIELD LOADING SUMMARY FORY1*1' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): 19.25 WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FcB2 6.983 Acres Permitted: 6.983 Site #: DP3-Grass Field #: DP3-Grass Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Date Total Phos- ... .:�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ / App. J Event 2.76 Arsenic 1 0.044 0.000 0.000 1 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.044 Cadmium 0.011 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.011 Copper 0.651 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.651 Chromium0.408 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.408 Lead 0.066 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.066 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 denum Nickel 0.138 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.138 Selenium 0.028 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.028 Zinc 1.682 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.682 Total Phos- 81.607 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .81.607 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Si tore of Land Applier �-j-I S- Date DENR FORM MFLSF (12/2006). b, A1V1VUAL 1V1.NTALN FIELD LVAJ_ENV NUl IMNKY FORM' Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: Acres Used: 6.8 Acres Permitted: 6.8 Site #: DP4 Field #: 15.65 FcB2 DP4 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): posite Date, r�--- o Total h .. �;�� Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 8 9 10 11 12 DT/Ac./ l 0 App. J y Event 2.30 Arsenic 0.037 1 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.037 Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0'00 0.000 0.000 0.000 0.009 Copper 0.543 0.000 0.000 0.000 0.000 '0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.543 Chromium 0.341 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.341 Lead 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.055 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 denum Nickel 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Selenium 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Zinc 1.404 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.404 Total Phos- 68.110 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 68.110 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of LandApplier Date V DENR FORM MFLSF (12/2006) 4k ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): 30.31 WQ0031725 Cation Exchange Capacity (non 503 only): Douglas Poplin Owner: Douglas Poplin Predominant Soil Series: FCB2 11.82 Acres Permitted: 11.82 Site #: DP5 Field #: DP5 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Com- posite Non Total Phos- phorusMENEENEENE00- Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total I 1 1 1 21 3 4 5 6 7 8 9 10 11 12 DT/Ac./ J App. y Event 2.56 Arsenic 0.041 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 1 0.041 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.010 Copper 0.605 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.605 Chromium 0.379 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.379 Lead 0.062 1 0.000 0.000 0.000 0.000 0.000 0.000 0'.000 0.000 0.000 0.000 0.000 0.062 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.026 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.026 denum Nickel 0.128 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.128 Selenium 0.026 1 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.026 Zinc 1.564 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.564 Total Phos- 75.894 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 75.894 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". �- ).- is - Signature of La Applier Date DFNR FORM MFI SF (19/2008) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Permit #: WQ0031725 Operator: Douglas Poplin Owner: Acres Used: 3.97 Acres Permitted: Total pry Tons Applied (Annual): 9.80 Cation Exchange Capacity (non 503 only): Douglas Poplin Predominant Soil Series: FcB2 3.97 Site #: DP6 Field #: DP6 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg,mg/kg, % Solids use Raw Percent #): Com- posite Date Total • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 2 3 4 5 6 7 1819 10 11 112 DT/Ac./ o App. y Event 2.47 Arsenic 0.040 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.040 Cadmium 0.010 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.010 Copper 0.583 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.583 Chromium 0.365 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.365 Lead 0.059 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.059 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- 0.025 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.025 denum denum Nickel 0.123 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.123 Selenium 0.025 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0:000 0.000 0.000 0.025 Zinc 1.506 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.506 Total Phos- 73.082 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 73.082 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Siature of Lan Applier ?-')-I 5, Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare WQ0031725 Douglas Poplin Owner: 3.34 Acres Permitted: Total Dry Tons Applied (Annual): 7.67 Cation Exchange Capacity (non 503 only): Douglas Poplin Predominant Soil Series: FcB2 3.34 Site #: DP7 Field #: DP7 Residual Analysis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): . • • • Com- posite �. a , d 11 100 WIN 11 Total • Annual Heavy Metal Field Loadings (Calculated in lbs/acre): Total 1 1 2 L 3 4 _ 5 61 1 7j L 8 9 10 11 12 DT/Ac./ o App. Event 2.30 Arsenic 0.037 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.037 Cadmium 0.009 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Copper 0.542 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.542 Chromium 0.340 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.340 Lead 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Molyb- denum 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Nickel 0.115 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.115 Selenium 0.023 1 0.000 0.000 0.000 0.000 0.000 0:000 0.000 0.000 0.000 0.000 0.000 0.023 Zinc 1.400V 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.400 Total Phos- 67.932 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 67.932 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land pplier �•3-15 Date DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Corn WQ Permit #: WQ0031725 Annual Dry Tons Applied: 9.9364 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 214 Field #: DP2 Acres Utilized: 5.02 Site #: DP2 Acres Permitted: 5.02 Cation Exchange Capacity (non 503): Crop 2 Name: Crop 2 Max. PAN: S. y Q Volume applied enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ# Fert., Animal Waste, etc) Soil Cond. W Moist) Precip. Past 24 Hrs. inches Y 4 b ,.. o K. � * o 7y # � �, o' 4 � 0 w ., r,' � w- o a TI{N mg/kg Z - o 0° 2 � w• mg/kg Nitrate and Nitrite mg/kg PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual g Application Crop 1 Crop 2 Crop 1 Crop 2 10-2014 121.01 9.75 1.979 WQ0031725 dry 0 Inc 1 0.3 111000 7900 18.5 153.790 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 121.01 01.. . .._.... _..... As Cd Cu Cr Pb H Mo Ni Se Zn P 153.790 0.000 Lime A lied Annuallbs/acre 0.032 0.07 0.102 36 0.008 0.032 0.040 34 0.467 1.626 2.093 1338 0.293 0.892 1.185 NA 0.047 0.136 0.183 267 0.002 0.003 0.005 15 0.020 0.056 0.076 NA 0.099 0.323 0.422 374 0.020 0.029 0.049 89 1.207 3.484 4.691 2498 58.578 Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 2500 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop _ .... _ F_ _.._. 214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Corn WQ Permit #: WQ0031725 Field #: DP3-Corn Annual Dry Tons Applied: 16.0504 Site #: DP3-Corn Predominant Soil Series: FcB2 Crop 1 Max. PAN: 214 Crop 2 Name: Acres Utilized: 5.877 Acres Permitted: 5.877 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 0 Q 0 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons oho Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. We ' Moist) Precip. Past 24 Hrs. inches Y CD a o o CD �: 4 7d � w w * P. � TKN mgfkg Z ct o ac o w• mglkg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 1-2014 57.67 9.75 0.806 WQ0031725 dry 0 INC 1 0.3 111000 7900 18.5 62.604 NA Corn 2-2014 87.13 9.75 1.217 WQ0031725 dry 0 INC 1 0.3 111000 7900 18.5 94.585 NA Com 3-2014 50.67 9.75 0.708 WQ0031725 dry 0 INC 1 0.3 111000 7900 18.5 55.005 NA Corn 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 -0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 195.47 0 AS Cd Cu Cr Pb Hg Mo Ni Se Zn P 212.195 0.000 Lime A lied Annuallbs/acre 0.044 0.011 0.645 0.404 0.066 0.003 0.027 0.137 0.027 1.666 80.838 Date lbs/ac Prior Years Cumulative lbs/ac 0.187 0.071 3.673 2.443 0.305 0.007 0.124 0.692 0.43 8.186 10-2014 1000 Current Cumulative lbs/ac 0.231 0.082 4.318 2.847 0.371 0.010 0.151 0.829 0.457 9.852 Permitted C. P. L. R.**** 36 34 1 1338 1 NA 1 267 1 15 1 NA 1 374 1 89 1 2498 Permit PAN Limit 1 st/2nd Crop 214 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 9- P- )j Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation -1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP3-Grass Annual Dry Tons Applied: 19.2437 Site #: DP3-Grass Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 6.983 Acres Permitted: 6.983 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: �, ° y ° ° Q Volume applied Pp � enter one Solids/ ( ) Liquid Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre . (Dry Tons/Ac) Residual Sources (NPDES # WQ# > > Fert. Animal Waste, etc) Soil Cond. (DrY> We Moist) Precip. Past 24 Hrs. inches y 0 � oc o o w * 5 o �, w �, * �' * ° o 9 � w •t ° ^ * �' * K 0 TKN mg/kg z > .; o 0° ° �• mg/kg Nitrate and Nitrite mg/kg PAN Applied ( lbs/acre) Name of CropType ReceivingResidual Application Crop 1 Crop 2 Crop 1 Crop 2 3-2014 113.84 9.75 1.339 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 93.432 NA Fescue 4-2014 60.52 9.75 0.712 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 49.671 NA Fescue 11-2014 60 9.75 0.706 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 49.244 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 234.36 0 As Cd Cu Cr Pb H Mo Ni Se Zn P 192.346 ro.000 Lime Applied Annuallbs/acre 0.044 0.187 0.231 36 0.011 0.071 0.082 34 0.651 3.673 4.324 1338 0.408 2.443 2.851 NA 0.066 0.305 0.371 267 0.003 0.007 0.010 15 0.028 0.124 0.152 NA 0.138 0.692 0.830 374 0.028 0.43 0.458 89 1.684 8.186 9.870 2498 81.696j Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 2500 Current Cumulative lbs/ac Permitted C. P. L.R.**** Permit AN Limit 1st/2nd Crop 194 641 certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP4 Annual Dry Tons Applied: 15.6563 Site #: DP4 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 6.8 Acres Permitted: 6.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° y o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (D Wet,a Moist Preci . p Past 24 Hrs. inches Y r; b o w c � C c ;� K' t�. ;n � P n ,* w. o TKN mg/kgm Z t Gt o 6 °° 0 E. g/kg Nitrate and Nitrite mg/kg PAN Applied (lbs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 4-2014 25.93 9.75 0.313 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 21.854 A Fescue 5-2014 53.04 9.75 0.640 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 44.703A Fescue 6-2014 29.68 9.75 0.358 W00031725 dry 0 s 0.5 0.3 111000 7900 18.5 25.015 LNA Fescue 7-2014 82.02 9.75 0.990 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 69.128A Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 190.671 0 1 As Cd Cu Cr Pb H Mo Ni Se Zn P 160.700 0.000 u Lime A lied Annuallbs/acre 0.037 0.131 0.168 36 0.009 0.046 0.055 34 1 0.543 2.392 2.935 1338 0.341 1.685 2.026 NA 0.055 0.186 0.241 267 0.003 0.005 0.008 15 0.023 0.081 ' 0.104v NA 1 0.115 0.564 0.679 374 1 0.023 0.031 0.054 89 1 1.404 5.467 6.871 2498 68.110 Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit 1 stJ2nd Crop - "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 9-a-)f Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP5 Annual Dry Tons Applied: 30.3190 Site #: DP5 Predominant Soil Series: Fc1132 Crop i Max. PAN: 194 Crop 2 Name: Acres Utilized: 11.82 Acres Permitted: 11.82 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: o y N o ce A Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. fir', We Moist) Precip. Past 24 Hrs. inches o 0 b o n o• C o %o Iv �, CD C' 01 ��� w CD TKN mg/kg � o °; mg/kg Nitrate and Nitrite mg/kg PAN Applied PP (lbs/acre) Name of Crop Type Receiving Residual Application PP Crop 1 Crop 2 Crop 1 Crop 2 5-2014 59.49 9.75 0.413 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 28.845 NA Fescue 6-2014 53.33 9.75 0.370 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 25.858 NA Fescue 8-2014 140.8 9.75 0.978 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 68.270 1 NA Fescue 9-2014 115.62 9.75 0.803 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 56.061 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 1 0.000 0.000 0.000 1 1 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 369.24 o As Cd Cu Cr Pb Hg Mo Ni Se Zn P 179.033 0.000 Lime Applied - Annual lbs/acre 0.041 0.108 0.149 36 0.010 0.038 0.048 34 0.605 1.93 2.535 1338 0.379 1.26 1.639 NA 0.062 0.162 0.224 267 0.003 0.004 0.007 15 0.026 0.065 0.091 NA 0.128 0.461 0.58 374 0.026 0.014 0.040 89 1.564 4.395 5.959 2498 75.894 Date lbs/ac Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** ,Permit PAN Lnnrt is 2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON Facility Name: Baxter Healthcare Land Owner: Douglas. Poplin Operator: Douglas Poplin PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit #: WQ0031725 Field #: DP6 Annual Dry Tons Applied: 9.8025 Site #• DP6 Predominant Soil Series: FcB2 Crop 1 Name: Fescue Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 3.97 Acres Permitted: 3.97 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Volume applied PP Volume Residual Sources Soil Precip. Y o Z Nitrate Name of CropType 0 o N � (enter one) Solids/ % A hed er PP P �p Q DES #, W #, Cond. Past 24 cg w :v �, w .� w TKN o and PAN Applied Receiving Residual co Liquid Solids Acre Fert., Animal (Dry, Hrs. - a. � w ao o � w. Nitrite lbs/acre ( ) Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste etc ) We Moist) inches mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 11-2014 62.16 9.75 1.286 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 89.735 NA Fescue 12-2014 57.22 9.75 1.183 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 82.604 NA Fescue 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 119.381 01 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 172.3391 0.000 _ Lime Applied Annuallbs/acre 0.040 0.161 0.201 36 0.010 0.059 0.069 34 0.583 3.045 3.628 1338 0.365 2.142 2.507 NA 1 0.059 0.273 0.332 267 0.003 0.005 0.008 15 0.025 0.103 0.128 NA 0.123 0.491 0.614 374 0.025 0.015 0.040A48.272 89 1.506 6.766 2498 73.082 Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 1000 Current Cumulative lbs/ac Permitted C. P. L. R.**** 1 Permit PAN Limit lst/2nd Crop 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier 2-2-1 - Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Douglas Poplin Operator: Douglas Poplin Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: DP7 Annual Dry Tons Applied: 7.6651 Site #: DP7 Predominant Soil Series: FcB2 Crop 1 Max. PAN: 194 Crop 2 Name: Acres Utilized: 3.34 Acres Permitted: 3.34 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: �. ° Y o Q Volume applied PP (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per PP P Acre D Tons/Ac (Dry ) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. D (Dry, Wet, Moist) Precip. Past 24 Hrs. inches a 4 b � o� m c � �; - * O 7y i * w * o TKN mg/kg z ct �o o mg/kg Nitrate and Nitrite mg/kg PAN Applied lbs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 5-2014 32.85 9.75 0.808 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 56.368 NA Fescue 10-2014 60.5 9.75 1.487 WQ0031725 dry 0 s 0.5 0.3 111000 7900 18.5 103.813 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 93.35r o As Cd _ Cu Cr Pb Hg Mo Ni Se Zn P 160.181 0.000 Lime Applied Annuallbs/acre 0.037 0.108 0.145 36 ; 0.009 0.038 0.047 34 0.542 1.93 2.472 1338 0.340 1.26 1.600 NA 1 0.055 0.162 0.217 267 1 0.003 0.004 0.007 15 1 0.023 0.065 0.088 NA 1 0.115 0.461 0.576 374 1 0.023 0.014 0.037 89 1 1.400 4.395 5.795 2498 67.932 _ Date lbs/ac Prior Years Cumulative lbs/ac 10-2014 2500 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit Ist/2nd Crop 194 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier d-a-t Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost-0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) "i""`ii'•"""b"""'u"'-' iI—Ll1 ""Lv U 11LLV.//11UL1 IUULJ.Jl111.ULiJU.GUulylulUJ/ U1UUA.IluPrrwu11L Realistic Yield Expectations for North Carolina Soils The North Carolina Realistic Yield Database is the product of an extensive data gathering and review process conducted by NC State University, the Natural Resource Conservation Service, the North Carolina Department of Agriculture and ConsurmerServices, and the North Carolina Division of Soil and Water Conservation. In 1999, county -based representatives of each of the above -named organizations were asked to collect yield data and make a reasoned judgement of the yields for various crops on each of the soils occurring in their county. These data were collected from 87 responses, representing 93 counties. The data were then compared with available research data and intensively reviewed by a panel of field agronomists, soil scientists and researchers familiar with the soils, crops and climatic conditions in each region. In reviewing the data, the following assumptions were made: 1. Realistic Yield Expectations should be based on the average of the best 3 years in a 5 year period which could be achieved with a high level of management (top 20% of growers) 2. For soils that may be mapped in multiple regions or in slightly different landscapes (for example, flood plains or stream terraces), the Realistic Yields are based on the most common prevailing conditions for that soil rather than the most ideal site for agricultural production. 3. For soils that are Somewhat Poorly, Poorly, or Very Poorly Drained, effective artificial drainage MUST be In place to achieve the yields shown in the RYE tables. 4. For tobacco production in the Piedmont physiographic, irrigation was assumed to be available, whereas no irrigation was assumed in the Coastal Plain physiographic region. This is in accordance with numerous surveys which show less than 15%-20% of tobacco in the Coastal Plain is irrigated, while 70 to 80% of tobacco in the Piedmont receives some Irrigation Citation: North Carolina Nutrient Management Workgroup, 2003. Realistic yields and nitrogen application factors for North Carolina crops. http://nutrients.soil.ncsu edu ieIds North Carolina State University, North Carolina Department of Agriculture and Consumer Services, North Carolina Department of Environment and Natural Resources, Natural Resources Conservation Service. Raleigh NC. To access the database, select a county and at least one crop. Multiple crops may be selected by holding the Ctrl key when selecting crops. A report will be generated showing a summary of currently available data for the county you selected. Select Your County Wilkes EsD: Evard-Cowee complex, 8 to 25 percent slopes, stony Select Your Soil EsE: Evard-Cowee complex, 25 to 60 percent slopes, stony FaD: Fairview sandy loam, 15 to 25 percent slopes FcB2: Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded Use Representative Slope Typical of the Soil Mapunit Correct for Slope Use my slope 0 Submit Reset 1 of 2 1/20/2014 1:56 PN i uLi1V11L 1 1U11UCV Vlll V3141111\Vl Lll �.r U1 V1111U uu.Y.iiuuU icuw.Z)Uii.uusu.UUU/ yiciuZSi uiucx.PujJrtwuiuy Realistic Yields for FcB2: Fairview sandy clay loam, 2 to 8 percent slopes, moderately eroded in Wilkes County Crop Yield Nitrogen Factor Realfistic Nitrogen Rate (lbs/acre) Estimated Phosphorus Removal (lbs PZOs/acre) Barley (Grain) 67 Bushels 1.49 99 25 Corn (Grain) 108 Bushels _ 1.11 _ 120 _ 47 Corn (Silage) 19.6 Tons 10.9 214 67 Cotton _ 637 Pounds 0.081 52 18 Sorghum (Silage) 16.7 Tons _ 7.6 127 50 Oats (Grain) 83 Bushels 1.13 94 21 Peanuts 0 Pounds 0 0 0 Rye (Grain) 49 Bushels _ 2.01 98 16 Small Grain (Silage) 8.8 Tons 11.1 98 48 Sorghum (Grain) 49 CWT 1.72 84 37 Soybeans (Double Cropped) 33 Bushels 0 0 27 Soybeans (Full Season) 39 Bushels 0 _ 0 31 Soybeans (Double Cropped - Manured) 33 Bushels _ 3.89 130 27 Soybeans (Full Season - Manured) 39 Bushels 3.89 152 31 Tobacco (Burley) 0 Pounds 0.074 0 0 Tobacco (Flue Cured) 2548 Pounds 0.029 74 13 Triticale (Grain) 69 Bushels 1.52 104 _ 23 Tropical Corn (Silage) 19.6 Tons 6.5 127 _ 67 Wheat (Grain) 49 Bushels 2.01 98 25 Bahiagrass (Hay) 3.4 Tons 44 _ 151 39 Caucasion/Old World Bluestem (Hay) 3.4 Tons 44 151 41 Common Bermudagrass (Hay) 3.4 Tons 44 151 42 Dallisgrass (Hay) _ 3.4 Tons 44 151 45 Fescue (Hay) 4.4 Tons _ 44 194 69 Hybrid Bermudagrass (Hay) 4.4 Tons 44 194 54 Hybrid Bermudagrass overseeded with Rescuegrass 0 Tons 44 0 0 (Hay) Mixed Cool Season Grass (Hay) 3.2 Tons 44 140 45 Orchardgrass (Hay) _ _ 3.4 Tons_ 44 151 50 Pearl Millet (Hay) 3.7 Tons 49 180 49 Rescuegrass (Hay) _ 0 Tons 44 0 0 Sorghum Sudan (Hay) 4.2 Tons 49 204 58 Timothy Grass (Hay) 0 Tons 44 0 0 Additional Guidance for speciality crops can be found at: http://nutrients.sol1.n(;su.edu/ciuIdance/ 2 of 2 1 /20/2014 1: 5F PM Location of Samples `The Plant process diagram on the flowing page shows the location of where the following samples were taken. The Analysis from A&L Eastern Laboratories, Inc., report number 14-028-0210 was taken from the Belt Filter Press, and is labeled with a red X * on the diagram. The Fecal Coliform Samples from Statesville Analytical Sample IDs 14019-20.1, 14019-20.2, 14019-20.3, 140122-27.1, 140122-27.2, 140122-27.3, 140122-27.4 were taken from Aerobic Digester No. 1 and is labeled with a blue X ( on the diagram. The Volatile Solids In, Sample ID 140122-25.1 was taken from where the solids from the clarifier are pumped to the aerobic digesters and is labeled with a green X V ) on the diagram. The Volatile Solids Out, Sample ID 140122-25.2 was taken from Aerobic Digester No. 1 and is labeled with a blue X (A on the diagram. The TCLP test Sample ID 14019-18was taken from Aerobic Digester No.I and is labeled with a blue X ( on the diagram. 4 co i v D In WASTE WATER TREATMENT' PLANT tVAIWATION BARTER HEALTHCARE CORPORATION McDOWELL COUNTY, NORTH CAROLINA T T I - � I ! CLARIFIER CLARIFIER N N o.3 N o. 4 ) 10" AERATION BASIN fG�e 1T xr--� --xti-- SDIGESTER I 6"C1pQ�%VCIP=JICHLORINEry �ii WICONTACTICHAMBER3.�CLARIFIER I—1 N II No.2 +\ I I i< III -I_ _I — e I I 4.� --12"CIP- -- —4"CIP--- — ---- 4 CIP 150,000 GALLON WATER FILTER SLUDGE BASIN WASHwATER 7 i I I I I I � ' l E UV FILTER -----------n"new__—. I rrfM r � — PUMP II BUILDING I II o AEROBIC DIGESTER I �/ •° �� `—' 1 — — � ---J AERATION BASIN CLARIFIER N I' III SLUDGE �\ No.1 No.1 I j DRYING BEDS � y f � r O O . qc 6 L L i .9Sy�� 4'Pt/ cif FI m T _ of /`�ps LAB & BELT z I I °' FILTER PRESS `" j I A BUILDING IIIZ .000 12"CIP T0� HOLDING BASIN 12"' UNFILTERED & • BACKWASH LINE A S. S Q.. C I. A T E S ENGINEERING PVOi ' - NG• FINANCE �SHEV'ILLE �C (828) 252-0575 11.0 �. ez'=yp.=" .:.< _ . P �'L teM _ ..,.. -. �:•.. .. ;, `;: 1 i_'d"55:� .t . i". �:�-t �. T t I .i - .. � t t 4. I ,. . Page: 1 of 2 /- Report Number: 14-028-0210 r1L A&L EasternLaboratories, Inc. Account Number: 46381 7621 Whitepine Road Richmond, Virginia 23237 (804) 743-9401 Fax (804) 271-6446 Submitted By: ZACH KEY wwwaleastem.com Send To: SOUTHERN SOIL BUILDERS Project: BAXTER DENNIS KEY NC CERT#257 958 HOOTS ROAD ROARING RIVER NC 28669 REPORT OF ANALYSIS Date Sampled: 1/22/2014 12:55`00 Lab Number: 97673 Date Received: 01/28/2014 00:00 Sample Id : BAXTER Date Reported: 02/03/2014 Total Solids * 9.75 97500 100.0 JM 01/28/2014 15:00 SM-2540G Moisture * 90.25 100.0 JM 01/28/2014 15:00 SM-2540G Total Kjeldahl Nitrogen 11.10 111000 10.0 JM 01/29/2014 09:29 SM-4500-NH3C-TKN Total Phosphorus 1.48 14800 100 KM 01/29/2014 13:31 SW 6010C Total Potassium 0.42 4160 100 KM 01/29/2014 13:31 SW 6010C Total Sulfur 1.14 11400 100 KM 01/29/2014 13:31 SW 6010C Total Calcium 0.93 9280 100 KM 01/29/2014 13:31 SW 6010C Total Magnesium 0.40 4010 100 KM 01/29/2014 13:31 SW 6010C Total Sodium 0.48 4780 100 KM 01/29/2014 13:31 SW 6010C Total Iron 9150 100 KM 01/29/2014 13:31 SW 6010C Total Aluminum 1300 100 KM 01/29/2014 13:31 SW 6010C Total Manganese 119 5 KM 01/29/2014 13:31 SW 6010C Total Copper 118 5 KM 01/29/2014 13:31 SW 6010C Total Zinc 305 5 KM 01/29/2014 13:31 SW 6010C Ammonia Nitrogen 0.79 7900 10.0 JM 01/29/2024 00:00 SM-4500-NH3C Organic N 10.31 103100 10.0 01/29/2014 09:29 CALCULATION Nitrate+Nitrite-N 18.5 2.00 JM 01/29/2014 09:30 SM-450ONO3F Total Cadmium 2.'0 2.0 KM 01/29/2014 13:31 SW 6010C All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Ourreports and letters ere.,or-the e ;dash e and conf.deraial use of our clients. and may rot be reproduced m whole orpart. ror may arry: e:erer;ce be made `�`�? to the o"crk. the resu?ts, cr the company ir, any advertising, .news release. or other public anno:nicements without obtain;ng our prior written authonzatior. Debbie Holt Page: 2 of 2 Report Number: 14-028-0210 Account Number: 46381 Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER, NC 28669 Lab Number: 97673 Sample Id: BAXTER v' A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond, Virginia 23237 804 743-9401 Fax 804 271-6446 P 9 ( I ( 1 www.aleastern.coln Project: BAXTER NC CERT#257 REPORT OF ANALYSIS Date Sampled: 1/22/2014 12:55:00 Date Received: 01/28/2014 00:00 Date Reported: 02/03/2014 Total Chromium 74 5 KM 01/29/2014 13:31 SW 6010C Total Nickel 25 5 KM 01/29/2014 13:31 SW 6010C Total Lead 12 5 KM 01/29/2014 13:31 SW 6010C Total Arsenic 8.0 3.0 KM 01/29/2014 13:31 SW 6010C Total Mercury 0.6 0.4 KM 01/29/2014 09:00 SW-7471B Total Selenium <5.0 5.0 KM 01/29/2014 13:31 SW 6010C pH (Standard Units) 7.93 2.00 JM 01/29/2014 09:29 SW-9045D Total Molybdenum 5 5 KM 01/29/2014 13:31 SW 6010C Comments: SULFUR AND ORGANIC NITROGEN NOT FOR COMPLIANCE PURPOSES. QUALIFIER: THE LRB WAS OUT OF LIMITS FOR "Mn". THE MATRIX SPIKE WAS OUT OF LIMITS FOR "Al". ALL OTHER QC DATA IS ACCEPTABLE. All values are on a dry weight basis except as noted by asterisk. Detection limit on all N series is on a wet basis. Our report is and letters are for.1he exclusive and confidential use of our clients, and may not be reproduced in v✓hole or part. nor inay any reference bemade to the work. the results. or the company in any advertising, ne a retaase. or other public announcements Lvithou, oot?inmg our pr for written authorization. Debbie Holt PAN Mineralization as decimal Total dry tons/year Acres Applied on 43.81 —` Rate 0.3 TKM� 111000 IIH3 7900 NO3 18.5 NO2 0 % Solids 0.0975 --' 180.67 PAN Surface 34893.51 mg/kg 69.797 lbsIchry top. -12610.221lbs total PAN 287.83-391lbs PAIIII—acre PAN Injection 38348.5 1 mgfkg 77.697 lbsldry tort 14037.52libs total PAN 320.41311 lbs PANlacre. Dry Tons/1000 gal. 0.406575 1st year PAN Surface lbs. 12610.22399 1st year PAN Iniected lbs. 1 14037.516991 lbs./acre Surface 287.8389407 lbs./acre Iniected 320.4181007 MR(TKN-NH3)+ +.5(NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton MR(TKN-NH3) + I (NH3)+NO3+NO2 =mg/kg mg/kg x.002 =Ibs/dry ton 1000 X 8.34 X %solids X sp. gravity "=dry tons/1 000gal." 2000 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/9/2014 Reported: 1/16/2014 For: Baxter Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 14019-20.1 % Solids 1 1.31 % SM2540B-1997 1/10/14 CL 14019-20.1 Fecal Coliform MTF 1 8397 MPN/g SM92210E-2006 1/10/14 CL 14019-20.2 % Solids 2 1.31 % SM2540B-1997 1/10/14 CL 14019-20.2 Fecal Coliform MTF 2 129,771 MPN/g SM92210E-2006 1/10/14 CL 14019-20.3 % Solids 3 1.34 % SM2540B-1997 1/10/14 CL 14019-20.3 Fecal Coliform MTF 3 82,090 MPN/g SM92210E-2006 1/10/14 CL Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.O. Box 228 9 Statesville, North Carolina 28687 • 704/872/4697 Client: - STATESVII.LEANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 8687 Chain of Custody Record Address ( { v 4E{Q� 0 w wr• .tf ContactPerson`!Gt� ljt Phone #�" ��� FAX# j�;.c�,���/p L �, PO # Requisitioned by: (rme Date) i Customer Sample ID# P Lab ID # Time Sampled Grab On{ t Y) Date Sampled Grab Only) i Y) - n 6 c� o. 0 a Matrix Parameters requested for analysis 1 sludge w ww ! t� � J t- f e7-1' i ) Err-) r��` L.C.'S. t - O �i " � Gi V4 .(CIA - i X Relinquished by: Received by: Y Relinquished by: Received by: Composite Sampling Time begin Time end Composite Sampling Time begin Time end r '1 jz ' I � C.�i�—�-" t- ,., #1: am, pm Date / / am, pm Date / / #2: am, pm Date am, pm Date / / Time -E �� Time 1V Time Time Lab Comments: till, J�M�rF� Ire 01Ae am,®(;;Date am m Date p � , am, pm Date am, pm Date M57 V'4 / 2 / f �� % /� �/ / / Sampled by: � Transported by: iW -L f/- Holding times met: Compliance work: Non-compliance work: Client: :1 E ID � ri — STATESVILLE ANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 28687. (704) 872-4697 Address: ( t (� C't _- O^ _ —fir o a ,-- t T ►�/ rJ1 Contact Person: —',�\l �! Phone # 3 _ z ft { FAX# 3 S tl yu Chain of Custody Record PO # Requisitioned by: (Time Date) Customer Sample ID# Lab ID # Time Sampled (Grab Only) Date Sampled (Grab Only) Matrix Parameters requested for analysis sways y� NN 1,105 Relinquished by: `; /�\`� f% Received by: ° �`_�.. Relinquished by: Received by: Composite Sampling #1: Time begin am, pm Date /_/ Time end am, pm Date _/ / Composite Sampling #2: Time begin am, pm Date Time end am, pm Date / / ' c� Time ��.�i`� am, Date Time G : 7 am,(pm Date Time am, pm Date Time am, pm Date Lab Comments: LW �� M-5)I _rn,rr S 1 /dal Z/ < <"� Sampled by: Transported by: frs L Holding times met: Compliance work: Non-compliance work: Condition of Receipt Sample ID 140122-27.1-27.4 Client Southern Soil Builders Temp on Arrival 1 pH upon Arrival Parameter Schedule Fecal Colifomi WW ❑ HNO3 ❑ HCl ❑ NaOH ❑ 112SO 0 Na2S2O ❑ Dechlorinated ❑ Chemicals in containers, client ❑ Chemicals upon receipt FV1 Received on Ice ❑ Samples chilled upon receipt ❑d Chemicals in containers, lab Page 1 of 1 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/22/2014 Reported: 1/31/2014 For: Baxter Sample ID Parameter' Cust ID Result Units Method Date Analyzed Analyst 140122-25.1 % Total Solids In 1.23 % SM2540B-1997 1/22/14 CL 140122-25.1 % Volatile Solids In 1.04 % SM2540G 1/23/14 CL 140122-25.2 % Total Solids Out 0.57 % SM2540B-1997 1/22/14 CL 140122-25.2 % Volatile Solids Out 0.38 % SM2540G 1/23/14 CL Respectfully submitted, ``- Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 P.U, Box 228 • Statesville, North Carolina 28687 • 704/872/4697 Client: i 0 STATESVILLE ANALYTICAL 122 Court Street • P.O. Box 228 Statesville, NC 28687 (704) 872-4697 Address: _ r a C(; r (�;�� 35 {TC� Contact Person: (J j) // Phone # 7 q FAX# -; t/oChain of PO # U Requisitioned by: (Time Date) Custody Record Customer Sample ID# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only) @ E D Matrix Parameters requested for analysis Sludge W WW J� v — Try r I l'1/� 1. �'` l / s _5. !( e' .C, Relinquished by: Received by: Relinquished by: Received by: Composite Sampling Time begin Time end .. Composite Sampling Time begin Time end A} '� ' r r #1: am, pm Date / / am, pm Date / / #2: am, pm Date / / am, pm Date / / Time `t1 am, p m Date I / `/ f `( Sampled by:�/� Time L11 am m :Date / / Transported by: rl-- , Time am, pm Date / Holding times met: V Time am, pm Date / / Compliance work: Non-compliance work: Lab Comments: <^;>1 t t u'�� I 0�Teri Jc, P o �� c� r� I, ;, �,, �� v� l.,$ $ Condition of Receipt Sample ID 140122-25.1-25.2 Client Southern Soil Builders Temp on Arrival pH upon Arrival Parameter Schedule % volatile solids ❑ HNO3 ❑ HCl ❑ NaOH ❑ 112SO ❑ Na2S2O ❑' Dechlorinated ❑ Chemicals in containers, client ❑ Chemicals upon receipt FV-1 Received on Ice ❑ Samples chilled upon receipt ❑ Chemicals in containers, lab Page 1 of 1 VS in 0.0104 VS out 0.0038 VSFR= 0.637036 VSFR=(IN-OUT)/(IN-(IN*OUT)) ,ol©q- , (Do3R otoq — (.O(O� o IQ �370 ,a�o3CQ Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 1/9/2014 Reported: 1/28/2014 For: Baxter TCLP Sample ID Parameter Cust ID Result Units Method 14019-18 Corrosivity Baxter See Attached SW-846 14019-18 Ignitability Baxter See Attached 1010M 14019-18 Reactivity Baxter See Attached SW-846 14019-18 TCLP Baxter See Attached 1311 Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 Date Analyzed Analyst 1/23/14 PACE 1/23/14 PACE 1/23/14 PACE 1/23/14 PACE P.O. Box 228 • Statesville, North Carolina 28687. 7041872/4697 aceAnalytical www.pacelabs.com Project: 14019-18 Pace Project No.: 92186027 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 14019-18 Lab ID: 92.186027001 Collected: 01/09/14 13:30 Received: 01/10/14 14:55 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared 8081 GCS Pesticides, TCLP gamma-BHC (Lindane) Chlordane (Technical) Endrin Heptachlor epoxide Methoxychlor Toxaphene Surrogates Decachlorobiphenyl (S) Tetrachloro-m-xylene (S) Analytical Method: EPA 8081 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 Analyzed CAS No. Qual ND ug/L 0.50 1 01/21/14 10:40 01/23/14 14:55 58-89-9 ND ug/L 3.0 1 01/21/14 10:40 01/23/14 14:55 57-74-9 ND ug/L 0.50 1 01/21/14 10:40 01/23/14 14:55 72-20-8 ND ug/L 0.50 1 01/21/14 10:40 01/23/14 14:55 1024-57-3 ND ug/L 1000 1 01/2111410:40 01/23/14 14:55 72-43-5 ND ug/L 3.0 1 01/21/14 10:40 01/23/14 14:55 8001-35-2 68 % 10-138 1 01/21/14 10:40 01/23/14 14:55 2051-24-3 59 % 10-110 1 01/21/14 10:40 01/23/14 14:55 877-09-8 8151 Chlorinate Herbicide TCLP Analytical Method: EPA 8151 Preparation Method: EPA 3510 2,4-D ND mg/L 0.010 1 01/16/14 08:00 01/18/14 21:00 94-75-7 2,4,5-TP (Silvex) ND mg/L 0.010 1 01/16/14 08:00 01/18/14 21:00 93-72-1 Surrogates 2,4-DCAA (S) 94 % 70-130 1 01/16/14 08:00 01/18/14 21:00 19719-28-9 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 01/13/14 10:49 Arsenic ND mg/L 0.050 1 01/14/14 11:10 01/14/14 23:13 7440-38-2 Barium 0.74 mg/L 0.25 1 01/14/14 11:10 01/14/14 23:13 7440-39-3 Cadmium ND mg/L 0.0050 1 01/14/14 11:10 01/14/14 23:13 7440-43-9 Chromium ND mg/L 0.025 1 01/14/14 11:10 01/14/14 23:13 7440-47-3 Lead ND mg/L 0.025 1 01/14/14 11:10 01/14/14 23:13 7439-92-1 Selenium ND mg/L 0.10 1 01/14/14 11:10 01/14/14 23:13 7782-49-2 Silver ND mg/L 0.025 1 01/14/14 11:10 01/1411423:13 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 01/13/14 10:49 Mercury ND ug/L 0.20 1 01/14/14 11:45 01/15/1416:02 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 1,4-Dichlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 106-46-7 2,4-Dinitrotoluene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 121-14-2 Hexachloro-1,3-butadiene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 87-68-3 Hexachlorobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 118-74-1 Hexachloroethane ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 67-72-1 2-Methyl phenol (o-Cresol) ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 95-48-7 3&4-Methyl phenol(m&p Cresol) 313 ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 Nitrobenzene ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 98-95-3 Pentachlorophenol ND ug/L 100 1 01/21/14 09:40 01/22/14 16:04 87-86-5 Pyridine ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 110-86-1 2,4,5-Trichlorophenol ND ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 95-95-4 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, Date: 01 /28/2014 11:40 AM without the written consent of Pace Analytical Services, Inc.. Page 4 of 21 aCMnalytical www.pacelabs.com Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2226 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceVAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Project: 14019-18 Pace Project No.: 92186027 Sample: 14019-18 Lab ID: 92186027001 Collected: 01/09/14 13:30 Received: 01/10/14 14:55 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 Leachate Method/Date: EPA 1311; 01/16/14 14:00 2,4,6-Trichlorophenol ND Ug/L 50.0 1 01/21/14 09:40 01/22/14 16:04 88-06-2 Surrogates Nitrobenzene-d5 (S) 56 % 12-102 1 01/21/14 09:40 01/22/14 16:04 4165-60-0 2-Fluorobiphenyl (S) 56 % 13-107 1 01/21/14 09:40 01/22/14 16:04 321-60-8 Terphenyl-d14 (S) 69 % 21-132 1 01/21/14 09:40 01/22/14 16:04 1718-51-0 Phenol-d6 (S) 35 % 10-110 1 01/21/14 09:40 01/22/14 16:04 13127-88-3 2-Fluorophenol (S) 41 % 10-110 1 01/21/14 09:40 01/22/14 16:04 367-12-4 2,4,6-Tribromophenol (S) 77 % 27-108 1 01/21/14 09:40 01/22/14 16:04 118-79-6 8260 MSV TCLP Analytical Method: EPA 8260 Benzene ND ug/L 5.0 1 01/15/14 13:08 71-43-2 2-Butanone (MEK) 52.5 ug/L 10.0 1 01/15/14 13:08 78-93-3 Carbon tetrachloride ND t.ig/L 5.0 1 01/15/14 13:08 56-23-5 Chlorobenzene ND ug/L 5.0 1 01115/1413:08 108-90-7 Chloroform ND ug/L 5.0 1 01/15/14 13:08 67-66-3 1,4-Dichlorobenzene ND ug/L 5.0 1 01/15/14 13:08 106-46-7 1,2-Dichloroethane ND ug/L 5.0 1 01/1511413:08 107-06-2 1,1-Dichloroethene ND ug/L 5.0 1 01/15/14 13:08 75-35-4 Tetrachloroethene ND ug/L 5.0 1 01/15/14 13:08 127-18-4 Trichloroethene ND ug/L 5.0 1 01/15/14 13:08 79-01-6 Vinyl chloride ND ug/L 5.0 1 01/15/14 13:08 75-01-4 Surrogates 1,2-Dichloroethane-d4 (S) 109 % 70-130 1 01/15/14 13:08 17060-07-0 Toluene-d8 (S) 98 % 67-135 1 01/15/14 13:08 2037-26-5 4-Bromofluorobenzene (S) 98 % 70-130 1 01/15/14 13:08 460-00-4 1010 Flash point,Closed Cup Analytical Method: EPA 1010 Flashpoint >200 deg F 70.0 1 01/13/14 00:00 734S Reactive Sulfide Analytical Method: SW-846 7.3.4.2 Modified Sulfide, Reactive ND rrig/L 10.0 1 01/15/14 14:00 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 6.9 Std. Units 0.10 1 01/21/14 15:45 733C Reactive Cyanide Analytical Method: SW-846 7,3.3.2 Modified Cyanide, Reactive ND mg/L 0.0050 1 01/15/14 12:45 Date: 01/28/2014 11:40 AM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 21 Client: Gr ;u�. a. ,� '��� �t'�i'j �+'�C.' �a� _._._. IM �— STATESVILLE ANALYTICAL 122 Court Street • 1'.O. Box 229 Statesville, NC 28687 (704) 872 4697 Chain of Custody Record Address [� f1 s5 ue•C Contact Person: = Phone # �' S - -� FAX" •Z�•���� is PO # / Requisitioned by: (Time Date) Customer Sample ID# Lab -ID # Time Sampled (Grab Only) Date Sampled (Grab Only) a a E 0 Matrix Parameters requested for analysis si�a9a w ww �j C�j TfLP \ ' V Relinquished by: I Time �` Received by: ,lj� '�—�, Time ; Relii squished by. Time Received by: Time Composite Sampling #1: Time begin am, pm Date / / Time end am, pm Date / / Lab Comments: ., .-Composite Sampling #2: ` ? Time begin am, pm Date Time end am, pm Date / _/ am, m ate am, &ate am, pm Date am, pm Date e,� �p f{ / `4 � `� Sampled by: It"A l l l Transported b:: �. t p �� Holding times met: / / Compliance work: Non-compliance work: m .s b d -- AN ANN UAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility Name: Baxter Healthcare WQ Permit Number: WQ0031725 WWTP Name: Baxter Healthcare NPDES Number: NC0006564 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ® Alt. C (Prior Testing) PE-fl I A1t.D (No Prior Test) ❑ Process to Further Reduce If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ElPasteurization El Class B: jAlt. (1) Fecal Density 7 Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ® I composting ❑ Aerobic Digestion ❑ Anaerobic i D estion El g If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge in Pathogen Density Number o Excee- d ces Frequency ofanal sis y Sample Type a ytica Tech - niaue Minim Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN '8397 225,349 1280000 MPN/g 0 7 grab sm9221c CFU 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.1 (VS reduction) Ed Alt. 2 (40-day bench) ® Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ® Alt 7 (Drying - Stable) ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) 53' "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." Dennis Key Southern Soil Builders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signature of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL007224 Client: Southern Soil Builders, Inc. Advisor: Predictive 958 Hoots Rd t- Roaring River, NC 28669 � r Mehlich-3 Extraction ,.:�: �. �}, of Report Sampled County: Wilkes Sampled: Received: 09/3012014 Completed: 10/08/2014 Farm: Links to Helpful Information Sample ID: DP1A Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/l00 cO; NO3-N in mg/drrr3]: Soil Class: Mineral HM% WN CEC BS%t, Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.41 0.93 12.9 86 1.8 6.1 231 185 55 24 36 ill 82 435 _ 435 932 0.1 1 Sample ID: DP1B Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 0.0 120-200 0 10 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cO; CEC and Na in meq/100 cm3; NO3-N in mg/dlm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.46 0.86 12.2 88 1.4 6.1 150 72 62 23 43 65 54 539 539 659 0.1 1 Sample ID: DP1C Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Fescue/OGrass/Tim, 1 0.5 120-200 0_ 10 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in 9/cnr3; CEC and Na in meq/100 cm3; NO3-N in mg/drn3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.51 0.92 11.7 83 2.0 5.8 202 75 60 20 45 131 96 607 607 1003 , 0.2 2 North Carolina 1,,;,a4;;, iur,; I�:r:lt�:•rnaa�t.�t•: Reprogramming of the laboratory -information -management system that makes this report possible is being funded through a grant from the North Carolina Tobacco Trust Fund Commission. Thank you for using agronomic services to manage nutrients and safeguard environmental quality. - Steve Troxler, Commissioner of Agriculture NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL007224 Page 2 of 4 Sample ID: DP1D Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrasslTim, 1 0.9 120-200 0 0 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/crr?; CEC and Na in meq/100 cO; NO3-N in mg/dd]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP' SS-1 NO3-N 0.60 0.90 11.4 81 2.2 5.6 208 116 56 20 49 95 74 697 697 785 0.1 1 Sample ID: DP2 ✓ Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1- Corn, silage 1.3 180-220 0 80 0 0 0 0 0 0 Note: 3 2- Test Results [units - W/V in a/cO; CEC and Na in meq/100 cnT3; NO3-N in mriW.l d-31- Soil Class; "vlincral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-1 Zn-AI Cu-I Na ESP SS-1 NO3-N 0.36 0.96 8.8 72 2.5 5.3 190 59 48 20 60 67 57 666✓ 666 745 L/ 0.1 1 Sample ID: DP3C Recommendations: Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1 -Corn, silage 0.8 180-220 0 100 0 0 0 0 0 0 Note: 3 2- Test Results [units - W/V in g/crn3; CEC and Na in meq/100 cm3; NO3-N in mg/dm3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-1 Mn-All Mn-Al2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N 0.13 0.87 9.3 79 1.9 L56 91 50 46 31 142 61 54 419 ✓ 419 378 LI/ 0.1 1 Sample ID: DP3G ✓ Recommendatio . Lime Nutrients (lb/acre) More Crop (tons/acre) N P205 K20 Mg S Mn Zn Cu B Information Lime History: 1-Fescue/OGrass/Tim, 1 1.4 120-200 0 10 0 0 0 0 0 0 Note: 12 2- Test Results [units - WN in g/cnr3; CEC and Na in meq/100 cnr3; NO3-N in mg/drrr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Cu-1 Na ESP SS-1 NO3-N 0.32 0.85 9.2 73 2.4 5. 95 70 45 24 87 79 64 /Zn-Al 510 ✓ 510 351 0.1 1 NCDA&CS Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY1 F-Ci nm99a Page 3 of 4 Sample ID: DP4 / �/ Lime History: Recommendations: Lime Crop (tons/acre) N P205 1- Fescue/OGrass/Tim, 1 0.6 120-200 0 2- K20 50 Nutrients (lb/acre) Mg S Mn Zn 0 0 0 0 Cu 0 B 0 More Information Note: 12 Test Results [units - WN in g/cO; CEC and Na in meq/100 crn3; NO3-N in mg/dnr3]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 0.60 0.91 11.6 81 2.2 5. 93 44 53 26 45 Sample ID: DP5 / Recommendations:. Lime Crop I (tons/acre) N P205 Lime History: 1- Fescue/OGrass/Tim, 1 0.0 120-200 0 2- Mn-I 87 K20 0 Mn-All Mn-Al2 Zn-1 Zn-AI 69 686/ 686 Nutrients (lb/acre) Mg S Mn Zn 0 0 0 0 Cu-1 63 Cu 0 Na 0.1 ESP SS-1 NO3-N 1 More B Information 0 Note: 12 Test Results [units - W/V in a/crrr3; CEC and Na in meq/100 cm3; NO-%-N in mg/rrrrr3]; $ ;il vla$S: ^ire^c ra^i HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 Mn-I Mn-All Mn-AI2 Zn-I Zn-AI Cu-I Na ESP SS-1 NO3-N " 0.41 0.86 11.8 88 1.4 6.2 95 113 55 28 49 Sample ID: DP6 / Recommendations: Lime I/ Crop (tons/acre) N P205 Lime History: 1- Fescue/OGrass/Tim, 1 0.6 120-200 40 2- 83 K20 50 65 805 805 Nutrients (lb/acre) Mg S Mn Zn 0 0 0 0 532 Cu 0 0.1 1 More B Information 0 Note: 12 Test Results [units - W/V in g/cd; CEC and Na in meq/100 cO; NO3-N in mg/dnr3]: Soil Class: Mineral HM% WN CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 0.41 0.95 7.5 77 1.7 5.7 41 47 54 20 32 Sample ID: DP7 Recommendations: Lime Crop (tons/acre) N P205 Lime History: 1-Fescue/OGrass/Tim, 1 1.4 120-200 0 2- Mn-I 75 K20 10 Mn-All Mn-AI2 Zn-I ✓Zn-AI 62 188 188 Nutrients (lb/acre) Mg S Mn Zn 0 0 0 0 Cu-I 94 `�/ Cu 0 Na 0.1 ESP SS-1 NO3-N 1 More B Information 0 Note: 12 Test Results [units - WN in g/crrr3; CEC and Na in meq/100 cd; NO3-N in mg/drff]: Soil Class: Mineral HM% W/V CEC BS% Ac pH P-1 K-1 Ca% Mg% S-1 I 0.51 0.94 7.4 68 2.4 (5� 99 77 47 16 39 Mn-I 77 Mn All Mn-AI2 63 Zn-I Zn-AI 305 ✓ 305 Cu-I 573 Na 0.1 ESP SS-1 NO3-N 1 NCDA&C&Agronomic Division Phone: (919) 733-2655 Website: www.ncagr.gov/agronomi/ Report No. FY15-SL007224 < r Understanding the Soil Report: explanation of measurements, abbreviations and units Recommendations Lime If testing finds that soil pH is too low for the crop(s) indicated, a lime recommendation will be given in units of either ton/acre or Ib/1000 sq ft. For best results, mix the lime into the top 6 to 8 inches of soil several months before planting. For no -till or established plantings where this is not possible, apply no more than 1 to 1.5 tonlacre (50 Ib/1000 sq ft) at one time, even if the report recommends more. You can apply the rest in similar increments every six months until the full rate is applied. If MG is recommended and lime is needed, use dolomitric lime. Fertilizer. Recommendations for field crops or other large areas are listed separately for each nutrient to be added (in units of lb/acre unless otherwise specified). Recommendations for N (and sometimes for B) are based on researdI/"He ld studies for the crop being grown, not on soil test results. K-1 and P-1 values are based on test results and should be > 50. If they are not, follow the fertilizer recommendations given. If Mg is needed and no lime is recommended, 0-0-22 (11.5% Mg) is an excellent source; 175 to 250 lb per acre alone or in a fertilizer blend will usually satisfy crop needs, SS-1 levels appear only on reports for greenhouse soil or problem samples. Farmers and other commercial producers should pay special attention to micronutrient levels. If $, pH$, $pH, C or Z notations appear on the soil report, refer to $Note: Secondary Nutrients and Micronutrients• In general, homeowners do not need to be concerned about micronutrients. Various crop notes also address lime fertilizer needs; visit ncagr.aovi'agronomi/pubs.htm. Recommendations forsmall areas, such as home lawns/gardens, are listed in units of Ib/1000 sq ft. If you cannot find the exact fertilizer grade recommended on the report, visit V,rww.rc6ar.aov/a4ronomi/obpart4.htm#fs to find information that may help you choose a comparable alternate. For more information, readR Homeownei's Guide to Fer, Test ResuitS The first seven values [soil class, HM%, W/V, CEC, BS%, Ac and pH] describe the soil and its degree of acidity. The remaining 16 [P-I, K-I, Ca%, Mg%, Mn-I, Mn-All, Mn-AI2, Zn-I, Zn AI, Cu-I, S-I, SS -I, Na, ESP, SS -I, NO3-N (not routinely available)] indicate levels of plant nutrients or other fertility measurement. Visit w ww..ncaor.gov/aaronomituvrst_htm for more information. Page 4 of 4 Report Abbreviations Ac exchangeable acidity B boron BS% % CEC occupied by basic cations Ca% % CEC occupied by calcium CEC cation exchange capacity Cu-I copper index ESP exchangeable sodium percent HM% percent humic matter K-1 potassium index K2^v potash Mg% % CEC occupied by magnesium MIN mineral soil class Mn manganese Mn-All Mn-availability index for crop 1 Mn-AI2 Mn-availability index for crop 2 Mn-I manganese index M-O mineral -organic soil class N nitrogen Na sodium NO3-N nitrate nitrogen ORG organic soil class pH current soil pH P-1 phosphorus index P205 phosphate S-1 sulfur index SS -I soluble salt index WN weight per volume Zn-AI zinc availability index Zn-I zinc index k, 9 ANA UAL PAT110GEN ANIV VECTOR ATTRACTION REDUCTION FORM (02T Rules) Fil-ility Name: Baxter Healthcare WWTP Name: Baxter Healthcare WQ Permit Number: . WQ0031725 NPDES Number: NC0006564 Monitoring Period: From 1/1/2014 To 12/31/2014 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative nprfarmPd- Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing) ❑ AID (No Prior Test) ❑ Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ ................... Class B: lAlt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens El If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ Composting ❑ Aerobic Digestion ❑ Anaerobic aero b Digestion g e on If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number o Excee- n s Frequency 9 si of Analysis Sample P Type Analytical Tech - i e inim Geo. Mean axim Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids WN 8397 225,349 1280000 MPN/ g 0 7 grab sm9221 c CFU�F !FfT 1000 mpn per gram of total solid (dry weight) Liwsion of Mate; b n_ 0 resources 1 NNPpR e I DER c 4 015 Salmonella bacteria (in lieu of fecal coliform XT_ 3 WN per 4 grams total solid (dry weight) Water " ^' Qualityai Re ninnar s p RQC� N S/N GUN/% v eciur rAttracnon iceaueTlon tl'A IN AU ul-"4U-4j z_'LlcaSe- sti - e- alternative performed: Alt.l (VS reduction) 5d Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. Oz uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable). ❑ Alt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ l;ER-Hirl(;A ION SIATEMENT (please check the appropriate statement) "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an -explanation why you have not met one or both' of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." HiAv ii ii %Z— Dennis Key Southern Soil Builders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signs of Preparer* Date Signature of Land Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006)