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WQ0031725_Annual Report_20100218
S S B Southern Soil Builders, Inc. Wednesday, June 16, 2010 Beverly Price NCDENR-DWQ Information Processing Unit 1617 Mail Service Center Raleigh, NC 27699-1617 Subject: Baxter Healthcare WQ0031725 958 Hoots Road Roaring River, NC 28669 (336) 957-8909 9 Fax (336) 957-8940 RECENED N 2 2 2510 .Si1 viiie Regional OfficS Enclosed you will find the undated PAN and SAR calculations as requested. The three field summary forms have been corrected where the mineralization rates and the volatilization rates got reversed. If you have any further questions or concerns, please contact me at zkey@southersoilbuilders.com or at 336-957-7871. P"�. Zach Key Southern Soil Builders, Inc. RECEIVED JUN 17 2010 Information Processing knit DWQ/BOG SAR & ESP Sodium Absorption Ratio Na: Sodium (Mg/L) Equivalent weight: 23 Ca: Calcium (Mg/L) Equivalent weight: 20 Mg.: Magnesium (Mg/L) Equivalent weight: 12 Milli Equivalent = Mg/L / Equivalent weight Na M /L Ca M /L Mg M /L 407.4 1 1955.52 1 512.16 Na ME 17.71304 Ca ME 97.776 M ME 42.68 SAR= Na Milli Equivalent/[0.5 X (Ca Milli Equivalent + Mg Milli equivalent)]0.5 power SAR = 2.113674 (From Mg/L entered above) SAR= 2.11313 (From ME entered below) Na (ME) Ca (ME) MEl17.71 12.68 97.8 Exchangeable Sodium Percentage ESP = Na (Milli Equivalents) / CEC X 100 The percentage of sodium ions occupying the Na ME CEC 0.869565 7.1 ESP = 112.24739 Na on NC soil test is expressed as meq. ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Trilby Setzer WQ Permit #: WQ0031725 Field #: S-01 Annual Dry Tons Applied: 7.8227 Site #: S-01 Operator: Derek Teague Predominant Soil Series: CmB2 Crop I Name: Fescue Crop I Max. PAN: 216 Crop 2 Name: Acres Utilized: 19.8 Acres Permitted: 19.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: `' s .� 0 Q Volume applied pp (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) Soil Cond. (Dry' MisWett) Precip. Past 24 Hrs. inches Y 3 2 co b o raw, ' < o w °' N > � coo p7 CD w �,' > TKN mg/kg _z Y -; � o 00 o w mg/kg Nitrate and Nitrite mg/kg PAN Applied Ibs/acre ( ) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop 1 Crop 2 8-09 j 79.8 11.64 0.395 WQ0031725 dry 0 s 0.5 0.3 81200 8200 1 20.545 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 79.8 - 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 20.545 1 0.000 Lime Applied Annuallbs/acre 0.010 0.003 0.232 0.084 0.023 0.001 0.006 0.034 0.002 0.255 15.600 1 Date I lbs/ac Prior Years Cumulative lbs/ac 0.11 0.05 9.146 0.634 1.47 0.043 0.182 0.465 0.079 12.396 8-09 1000 Current Cumulative lbs/ac 0.120 0.053 .9.378 0.718 1.493 0.044 0.188 0.499 0.081 12.651 Permitted C. P. L. R.**** 36 34 1338 NA 267 15 1 NA 1 374 89 2498 Permit PAN Limit Ist/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure tnat qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signatffre of Land Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface -0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Larry Teague Operator: Derek Teague Crop 1 Name: Fescue WQ Permit #: WQ0031725 Field #: T-02 Annual Dry Tons Applied: 18.4000 Site #: T-02 Predominant Soil Series: MgC2 Crop I Max. PAN: 162 Crop 2 Name: Acres Utilized: 10 Acres Permitted: 10 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: `- t ° �? o Volume applied (enter one) Solids/ Liquid Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES # WQ# Fert., Animal Waste, etc) SOil Cond. (Dry, WetCu. Moist) Precip. Past 24 Hrs. inches a K co �'- r o' o0 w o w R co _ * K X c1 w °' w * a TKN mg/kg z 3 � o 3 mg/kg Nitrate and Nitrite mg/kg PAN Applied pp (Ibs/acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 8-09 1 24 11.64 0.235 W00031725 dry 0 s 0.5 0.3 81200 8200 1 12.234 NA Fescue 9-09 44.7 11.64 0.438 WQ0031725 dry 0 s 0.5 0.3 81200 8200 1 22.787 NA Fescue 10-09 45.3 11.64 0.444 W00031725 dry 0 s 0.5 0.3 81200 8200 1 23.093 NA Fescue 11-09 73.7 11.64 0.722 W00031725 dry 0 s 0.5 0.3 81200 8200 1 37.570 NA Fescue 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 187.71 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 95.684 1 0.000 Lime Applied Annuallbs/acre 0.044 0.015 1.067 0.386 0.107 0.004 0.029 0.155 0.008 1.174 71.760 Date lbs/ac Prior Years Cumulative lbs/ac 0 0 0.371 0.132 0 0.003 0 0.055 0 0.417 8-09 1000 Current Cumulative lbs/ac 0.044 0.015 1.438 0.518 0.107 0.007 0.029 0.210 0.008 1.591 Permitted C. P. L. R.**** 36 1 34 1 1338 1 NA 1 267 1 15 1 NA 1 374 1 89 1 2498 Permit PAN Limit Ist/2nd Crop 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of rand Applier Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Larry Teague Operator: Derek Teague CrOD 1 Name: Fescue WQ Permit #• WQ0031725 Field #: T-01 Acres Utilized: 26 Annual Dry Tons Applied: 43.7690 Site #: T-01 Acres Permitted: 26 Predominant Soil Series: HsB2 Cation Exchange Capacity (non 503): Crop 1 Max. PAN: 216 Crop 2 Name: Crop 2 Max. PAN: Volume applied Volume Residual Sources Soil Cond. precip. > F o w CD z Nitrate PAN Applied Name of Crop Type Receiving Residual o - (enter one) Solids/ % Applied per (NPDES #, WQ#, Past 24 - m ? - �, w TKN o 3 00 0 and ( Ibs/acre) ca o Liquid Solids Acre Fert., Animal D ( ry' Hrs. E' F 0 w 0 * * N' 0 0 w Nitrite Application Q Cu. Yds Gallons (Dry Tons/Ac) Waste, etc) Wet, Moist) Inches n 0. o * * �, 0 mg/kg mg/kg mg/kg Crop 1 Crop 2 Crop 1 Crop 2 2-09 107.29 11.64 0.405 W00031725 dry 0 s 0.5 0.3 81200 8200 1 21.036 NA Fescue 3-09 108.8 11.64 0.410 W00031725 dry 0 s 0.5 0.3 81200 8200 1 21.332 NA Fescue 4-09 108. 11.64 0.407 W00031725 dry 0 s 0.5 0.3 81200 8200 1 21.175 1 NA Fescue 5-09 72.6 11.64 0.274 WQ0031725 dry 0 s 0.5 0.3 81200 8200 1 14.234 NA Fescue 6-09 49.8 11.64 0.188 W00031725 dry 0 s 0.5 0.3 81200 8200 1 9.764 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 446.491 0 ' : As Cd Cu Cr Pb H Mo Ni Se Zn P 87.541 0.000 Lime Applied Annuallbs/acre 0.040 0.013 0.974 0.353 0.097 0.004 0.027 0.141 0.007 1.072 65.520 Date lbs/ac Prior Years Cumulative lbs/ac 0.108 0.01 1.86 0 0.157 0.0066 0.145 0.1178 0.0158 1.704 8-09 1000 Current Cumulative lbs/ac 0.148 1 0.023 2.834 0.353 0.254 0.011 0.172 0.259 0.023 2.776 Permitted C. P. L. R.**** 36 34 1.338 1 NA 1 267 1 15 NA 374 89 2498 Permit PAN Limit 1st/2nd Crop 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signatre of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) kph � Annual Report Review SOP Class B Land Application 1. Annual Land Application Certification Form .• Was a certification form submitted? Y65. • Was land application conducted during the reported year? ® How many dry tons and dry tons per acre were applied? • Were the applications within the permitted amount? y,es • Verify PAN if more than 10 tons/acre . • Did it indicate compliance? Yes • Was it signed by the appropriate people? 2. Monitoring • Were the analyses conducted at the required frequency? y.P—s • Were the metals analyses reported on the Residual Sampling Summary Form? y z s • Were the results reported in mg/kg? YES • Were the metals within ceiling concentration permit limits? Ines • If no, were the lab. analyses attached? [„�o . respti o • Were all the required parameters tested? y e. s s p �'— ca l ewla Rc�d • Was TCLP analysis conducted? y ej. Co,-ros 5�' Y • Were the TCLP contaminants within regulatory l�M, its? ye�y 6os�d 4L 3. Field Summary Ga �� c ©�€ �1= �'� be P o Were the land application events recorded on the Field Summary Forms? ye _5 ® Was a Field Summary Form submitted for each field applied on? )re-,5 • Were all the residuals applied to permitted land? YES O Were all the residuals applied from permitted sources? yS5 • Were the field loading rates for each metal and PAN calculated (year to date)? yes :KO Were the cumulative pollutant loading rates calculated?yams F2 too pQl0 R ci,},,+ ��v ve 4 ,E • Were. the'ealculations correct? PA m. --> Na 3 R'cvd , in Ate- k. o , response. Pb MG) se. • Were the. PAN loading rates within permit limits? y-e-S • Were the heavy metal cumulative pollutant loading rates within permit limits? y-I- 14e • Were the residuals applied on a suitable crop? IDS A -Sic 7"ji • Were the applications conducted during the crop's growing season? .y e,S ® Were the Field Summary Forms complete? e.5 • Was lime application on Field Summary Form? T I 3/0q i000 16s . Ae T?_ 7 9r3 Y►e Urt o, 4: Pathogen and Vector Attraction Reduction s Was a signed copy of. the Pathn and Vector Attraction eduction Form submitted? kpS l,tn Wln G� • Did the forwndicate the period of coverage, the residual class, and the pathogen reduction alternative and the mil. vector attraction reduction' option used? �n�—� A • Was the appropriate documen�- -ion to show patho�en s and vector attractin�reduction included in the report? a e Was pathogen and vector,6' action reduction demonstrated according to 40 CFR Part 503 or 2T? Don t �zsd ro ��« /}el �j J -S �"� 5. Soil Tests p • Was a Standard Soil Fertility Analysis conducted for each field applied on? • Were the soil pH's 6.0 or greater for each application field? N9 a . ® Were the copper and zinc indexes in the soil less than 3000 for eaLh application field (state soils lab)? w�S 6. General a o • Was the report in the proper format? YtS �• �� Q u�' �� • Were any parts of the annual report missing? e Was the report submitted on time? Y �S V�r4 SK �j f �Icwla � Shk PAN�t- �C S" pJc-1.,t.cl� Va„ dQ T+5 no+ 55 Class B Pathoizen Review Alternative 1 - Fecal Coliform Density • Was the sampling conducted at the required frequency? • Were seven samples taken? bN� %k' LEA be- w P • Was the geometric mean calculated and done correctly? .4-00 • Did the results show compliance (less than either 2,000,000 MPN/gram of total solids or 2,000,000 Colony Forming Units/gram of total solids) y,k5 Alternative 2 - Use of Process to Significantly Reduce Pathogens (one of five) • Was the sampling conducted at the required frequency? Aerobic Digestion ® Was it an aerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? • Was the time and temperature betweeri 40 days at 20°C (68T) and 60 days at 15°C (59T)? Air Drying • Were residuals on sand beds or pave or unpaved basins for three months? • Was the ambient temperature above 0°C (32T) for two months? o Were the residuals partially digested? • Were residuals exposed to atmosphere during two months above 0°C (riot snow covered)? Anaerobic Di e� stion a 'Was it an anaerobic process (Inspection)? • Were logs submitted showing time and temperature? • Were temperatures within range for complete time period? ® Was the time and temperature.between 15 days at 35°C (95T) to 55°C (131T) and 60 days at 20°C (68-F)? Composting • Was it a. composting procedure (not natural decay under uncontrolled conditions)? Were logs submitted showing time and temperature? © Was the temperature raised to 40°C (104°F) or higher and remained at 40°C (104T) for five days? • Did the temperature exceed 55°C (13IT) for four hours during the five-day period? Lime Stabilization • Was alkaline material added to residuals a form of lime (hydrated lime, quicklime, lime containing kiln dust or fly ash)? • Were logs submitted showing time and temperature? • Was the pH raised to 12 after two hours of contact? • Were logs submitted showing time and pH? • Was the temperature corrected to 25°C (77T)? Vector Attraction Reduction Review '• r; ''''�~ ® Was the sampling conducted at the required frequency? 38% Volatile Solids Reduction • Was there 3 8 % reduction? 10, ® Were lab sheets/calculations in report? ® Was the reduction on volatile solids (not total solids)? �S ® Was the samples taken at beginning of digestion process and before application y�e y (Inspection)? Were calculations correct? 01 40-Day Bench Scale Test ® Were residuals from anaerobically digested treatment (Inspection)? o Were residuals anaerobically digested in lab? ® Was the test run for 4.0 days? Was the test done between 30°C (86T) and 37°C (99°F)? ® Was the reduction on volatile solids (not total solids)? ® Was the reduction less than 17%? ® Were lab sheets/calculations in report?. ® Were calculations correct? 30-Day Bench Scale Test ® Were residuals from aerobically digested treatment (Inspection)? ® Were residuals aerobically digested in lab? ® Were residuals 2% or less total solids? ® Was the test run for 30 days? ® Was the test done at 200C (680F)? ® Was the reduction on volatile solids (not total solids)? ® Was the reduction less than 15%? Q Were lab'sheets/calculations in report? ® Were calculations correct? Specific Oxygen Uptake Rate (SOURR) Were residuals from aerobically digested treatment (Inspection)? ® Were residuals 2% or less total solids (dry weight basis) (not diluted)? ® Was the test done between 10°C (50°F) and 300C (860F)? ® Was the temperature corrected to 20°C (68°F)? ® Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)? Was the sample holding time under two hours? Was the test started within15 minutes of sampling or aeration maintained? 14-Dav Aerobic Process Were residuals from aerobically digested treatment (Inspection)? ® Were the residuals treated for 14 days? ® Was the residuals temperature higher than 400C (104T) for the 14-day period? ® Was the average residuals temperature higher than.45°C (113T)? Alkaline Stabilization Was the pH of the residuals raised to 12 or higher by the addition of alkali? ® Did the pH of residuals remain at 12 or higher for two hours without the addition of more alkali? ® Did the pH of residuals remain at 11.5 or higher for an additional twenty-two hours without the addition of more alkali? a Was the pH corrected to 250C (770F)? Dr�jng of Stabilized Residuals • Does the residuals contain any unstabilized residuals? ® Were the residuals mixed with any other materials? Were the residuals dried to 75% total solids? Drying of Unstabilized Residuals Were the residuals mixed with any other materials? ® Were the residuals dried to, 90% total solids? . Infection ® Was there any significant. amount of residuals on land surface one hour after injection (Inspection)? ® Was injection done on pasture or hay field? ® Was injection.done at time that crop was growing? ® If Class A with respect to pathogen, were residuals inj ected within eight hours after discharge from pathogen treatment? Incorporation ® Were the residuals incorporated into the soil within six hours after application? Q Was incorporation done on pasture or hay field? ® Was incorporation done at time that crop was growing? ® If Class A with respect to pathogen, were residuals incorporated within eight _................. _.. _. _.. -_hours- after- discharge- from- pathogen. treatment?.._...___....... _....__.........._ ....._ ... _.__. __._ 7 233.� CLIENT'S COPY r i . F`B 22 2t;:� Asheville Regional Office BAXTER HEALTHCARE CORPORATION 2009 ANNUAL REPORT LAND APPLICATION PROGRAM NC PERMIT NO. WQ0031725 E CEV'J .0 FEa s zolo ANNUAL LAND APPLICATION CERTIFICATION FORM WQ Fermit4: WQ0031725 County: McDowell r; Year: 2.009 Facility Name (as shown on permit): Baxter Healthcare Land Application Operator: Southern Soil Builders, Inc. Phone: 336-957-8909 Land application of residuals as allowed by the permit occurred during the past calendar year? R Yes ❑ No - If No, skip Part A, and Part B and proceed to Part C. Also; If residuals were generated but not land applied, please attach an explanation on how the residuals were handled. Part A - Residuals Application Summary: Total number of application fields in the permst: 4 Total number of fields utilized for land application during the year; 3 Total amount of dry tons applied during the year for all application sitW 69.9 Total number of acres utilizes for land application during the year: 55.8 Part B - Annual Compiance Statement: Facility was compliant during calendar year 2009 with all conditions of the land application permit (including but not limited to items 1-13 below) issued by the Division of Water Quality. 0 Yes ❑ No If no please, provide a written description why the facility was not compliant, the dates, and explain corrective action taken. 1) Only residuals approved for this permit were applied to the permitted sites. 2) Soil pH was adjusted as specified in the permit and lime was applied (if needed) to achieve a soil pH of at least 6.0 or the limit specified in the permit. 3) Annual soils analysis were performed on each site receiving residuals during the past calendar year and three (3) copies of laboratory results are attached. 4) Annual TCLP analysis (if required) was performed and three (3) copies of certified laboratory results are attached. 5) All other monitoring -was performed in accordance with the permit and reported during the year as required and three (3) copies of certified laboratory results are attached. 6) The facility did not exceed any of the Pollutant Concentration Limits in 15A NCAC 02T .1105(a) or the Pollutant Loading Rates in 15A NCAC 02T .I 105(b) (applicable to 40 CFR Part 503 regulated facilities). 7) All general requirements in as specified in the. Land Application Permit were complied with (applicable to 40 CFR Part 503 regulated facilities). 8) All monitoring and reporting requirements in 15A NCAC 02T .1 I I I were complied with (applicable to 40 CFR Part 503 regulated facilities). 9) All operations and maintenance requirements in the permit were complied with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 10) No contravention of Ground Water Quality Standards occurred at a monitoring well or explanations of violations are attached to include appropriate actions and remediations. 1 1) Vegetative cover was maintained and proper crop management was performed on each site receing residuals, as specified in the permit. 12) No runoff of residuals from the application sites onto adjacent property or nearby surface waters`a v oc�urrec 13) All buffer requirements as specified on the permit were maintained during each application of residdy s., 2010 Part C - Certification: ttttSS ,LL�,� "I certify, under penalty of law, that the above information is, to the best of my knowledge aad,belief'tr,ue;°ae�'u4'�,�e, V.and complete. I am aware that there are significant penalties for submitting false information;` ncluding the possibility of fines and imprisonment for knowing violations." �S-Kl E-N 61, 6-C 1P Mk-zzgy �v�Ss r• Permittee Name and Title (type or print) 7 JJ 110 Signature of Permittee Date I`A- Signature of Preparer* (if different from Permittee) * Preparer is defined in 40 CFR Part 503.9 (r) and Date ture of Applier Date (if different from Permittee and Preparer) 15A NCAC 02T .1102 (26) DENR FORM ACF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0031725 Facility Name: Residual Source WQ # or NPDES #: WWTP Name: Residual Analvsis Data Baxter Healthcare NC0006564 Laboratory: 1) 2) 3) 4) 5) A&L Eastern Laboratories. Inc. Parameter .Limit Conc. Chromium Nitrate and Nitrite ror surrace uisposai racemes me ceiling concentration limits listed in this torm are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant p?"Ities for submitting false information, including the possibility of fines and imprisonment for knowing violations:" Signaturelof Preparer' _7jIsl16 Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1 102 (26) DEN'R FORM RSSF (12/2006) SAR r PAN= 26,001 Mg/Kg vl' cc-o, �7— g00 o, s ANNUAL METALS FIELD LOADING SUMMARY FORM* 'Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 43.68 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Derek Teague Owner: Larry Teague Predominant Soil Series: 9 HSB2 Acres Used: 26 Acres Permitted: 26 Site #: T-01 Field #: T-01 Residual Analvsis Data (Heavv Metals and Total Phosphorus use m2/kg, % Solids use Raw Percent #): Com- posite Date - Total Phos phorusMENEENEENEEN Annual Heavv Metal l+ield LoadmLirs (Calculated in Ws/acre): I Total 1 2 3j 5j 6 7 8j 9 10 ill 12 DT/Ac./ ° App. Event 1.68 Arsenic 0.040 1 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 •0.000 1 0.040 Cadmium 0.013 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.013 Copper 0.974 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.974 Chromium 0.353 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 O.00Q �.0.000 0.353 Lead 0.097 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 ' 0.000 0.000 0.000 0.097 Mercury 0.004 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 1 0.004 Molyb- 0.027 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.027 denum Nickel 0.141 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.141 Selenium 0.007 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 '0.000 0.007 Zinc 1.072 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 "0.000 1.072 Total Phos- 65.520 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 65.520 horus "I certify, under .penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date J N5% 12 n .002 -,ul` lalbl A 1.6%> : o,ou \SAG DENR FORM MFLSI= (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual I !Port Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 18.39 Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Derek Teague Owner: Larry Teague Predominant Soil Series: MgC2 Acres Used: 10 Acres Permitted: 10 Site #: T-02 Field #: T-02 Residual Analvsis Data (Heavv Metals and Total Phosphorus use me/kg, % Solids use Raw Percent Com- posite Date. �. Total P .. �� Annual Henw Metal Field Loadings it:alculatea In ins/acre): Total 1 121 3 4 v _5j 6 1 7 8 9 10 "1 12 y DT/Ac./ 0 App. r Event 1.84 Arsenic 0.044 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.044 Cadmium 0.015 0.000 0.000 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.01 Copper 1.067 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.067 Chromium 0.386 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.386 Lead 0.107 0.000 0.000 0.000 0.600 0.000 0.000 0.000 0.000 0.000 0.000 .0.000 0.107 Mercury 0.004 0.000 0.000 0.000 0.'000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.004 Molyb- 0.029 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.029 denum Nickel 0.154 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.154 Selenium 0.008 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.008 Zinc 1.173 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0;000 1.173 Total Phos- 71.721 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 71.721 horus "I certify, under penalty of law, that this document was prepared under my airection or supervision In accoruance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Date DENR FORM MFLSF (12/2006) o/ Signature of Land Applier ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 7.82 , Permit #: WQ0031725 Cation Exchange Capacity (non 503 only): Operator: Derek Teague Owner: Trilby Setzer Predominant Soil Series: CmB2` Acres Used: 19.8 Acres Permitted: 19.8 Site #: S-01 Field #: S-01 Residual Analysis Data (Heave Metals and Total Phosphorus use nfe/k2. % Solids use Raw Percent #1: Com- posite Date. �. Total • .• Annual Heavv Metal Meld Loadines (Calculated in Ibs/acre): Total 1 2 4 1 jj 6 7 9 J i2i 11 12 DT/Ac./ _3j _Bj o App. y Event 0.40 " Arsenic 0.009 0.000 0.000 1 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.009 Cadmium 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 Copper 0.229 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.229 Chromium 0.083 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.083 Lead 0.023 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.023 Mercury 0.001 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.001 Molyb- 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 denum Nickel 0.033 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.033 Selenium 0.002 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.002 Zinc 0.252 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.252 Total Phos- 15.405 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 15.405 horus "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". Signature of Land Applier Date DENR FORM MFLSF (12/2006) `---\_ I-- ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: T-01 Acres Utilized: 26 Land Owner: Larry Teague Annual Dry Tons Applied: 43.7690 Site #: T-01 Acres Permitted: 26 Operator: Derek Teague Predominant Soil Series: HsB2 Cation Exchange Capacity (non 503): Crop I Name: Fescue Crop 1 Max. PAN: 216 Crop 2 Name: Crop 2 Max. PAN: ` t o Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#, Fert., Animal Waste, etc) SOLI Cond. (Dry, t. vest) Precip. Past 24 Hrs. inches D a 3 �• o w a * ' o w °=, - N' * w 0 a N c 3 TKN mg/kg z D �' E3 c oo c g a mg/kg Nitrate and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application Cro 1 Crop 2 Crop 1 Crop 2 2-09 107.29 1'•5 PT 11.64 0.405 W00031725 dry 0 s 0.3 0.5 81200 8200 1 ,31.521 NA Fescue 3-09 108.8 io,W 0-r 11.64 0A10 W00031725 dry 0 s 0.3 0.5 81200 8200 1 31.965 NA Fescue 4-09 108 11.64 0.407 ✓ W00031725 dry 0 s 0.3 0.5 81200 8200 1 31.730 NA Fescue 5-09 72.6 11 p"( 11.64 0.274 / W00031725 dry 0 s 0.3 0.5 81200 8200 1 21.329 NA Fescue 6-09 49.8 y, 11.64 0.188 ✓ W00031725 dry 0 s 0.3 0.5 81200 8200 1 14.631 NA Fescue 0.000 0.000 0.000 0.000 0 , 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 446.49 o As Cd Cu Cr Pb H g Mo Ni Se Zn P 131.176 0.000 Lime Applied , Annuallbs/acre 0.040 0.013 0.974 0.353 0.097 0.004 0.027 0.141 0.007 1.072 65.520 Date I lbs/act Prior Years Cumulative lbs/ac 0.108 0.01 1.86 0 0.157 0.0066 0.145 0.1178 0.0158 1.704 - Oq lOoO Current Cumulative lbs/ac 0.148 ✓ 0.021 2.834 0.353 0.254 0.011 0.172 V, 0.259 0.023 2.776 Permitted C. P. L. R.***'* 36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit lst/2nd Crop F 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false - information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation (.2.4- **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested, -0.3, raw sludge -0.4 a• ****C.P:L.R.: Cumulative Pollutant Loading Rate F5� DENR FORM FSF (1212006) nn 00 0 7 AN, A (49 ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Larry Teague Operator: Derek Teague Crop I Name: Fescue WQ Permit #: WQ0031725 Field #: T-02 Annual Dry Tons Applied: 18.4000 Site #: T-02 Predominant Soil Series: MgC2 Crop 1 Max. PAN: 162 Crop 2 Name: Acres Utilized: 10 Acres Permitted: 10 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: ° Y ° M ° Volume applied enter one Solids/ ( ) Liquid 9 Cu. Yds Gallons o /o Solids Volume Applied per PP P Acre (Dry Tons/Ac) Residual Sources (NPDES #, \N Q#, Fert., Animal Waste, etc) Soil Cond. (Dry, Wet Moist) Preci P Past 24 Hrs. inches D � 0 o < X a a _ = N # w' 0 TKN mg/kg z ➢ 0 o o g �'-• mg/kg Nitrate and Nitrite mg/kg PAN Applied PP (Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 8-19 24 11.64 0.235 W00031725 dry 0 s 0.3 1 0.5 81200 8200 1 18.333 NA Fescue 9-09 44.7 11.64 0.438 WQ0031725 dry 0 s 0.3 0.5 81200 8200 1 34.145 NA Fescue 10-09 45.3 11.64 0.444 WQ0031725 dry 0 s 0.3 0.5 81200 8200 1 34.603 NA Fescue 11-09 73.7 11.64 0.722 WQ0031725 dry 0 s 0.3 0.5 81200 8200 1 56.297 NA Fescue 0.000 1 0.000 0.000 0.000. 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 1877F 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 143.371 0.000 Lime Applied Annuallbs/acre 0.044 0 0.044 36 0.015 0 0.015 34 1.067 0.371 1.438 1338 -'. 0.386 0.132 0.518 NA 0.107 0 0.107 267 0.004 0.003 0.007 15 0.029 0 0.029G NA 0.154 0.055 0.209v 37.4 0.008 0 0.0081, 89 1.173 0.417 1.590 1 2498 71.721 6 Date- -114&4ap Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop I 1 162 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment -for knowing violations." '7 *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Signature of Land Applier Date *** Mineralization Rates: Compost-0.1,'anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare WQ Permit #: WQ0031725 Field #: S-01 Acres Utilized: Land Owner: Trilby Setzer Annual Dry Tons Applied: 7.8227 Site #: S-01 Acres Permitted: Operator: Derek Teague Crop I Name: Fescue Predominant Soil Series: CmB2 Crop 1 Max. PAN: 216 Crop 2 Name: Cation Exchange Capacity (non 503): Crop 2 Max. PAN: 19.8 19.8 a s C p Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons % Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES #, WQ#. Fert., Animal Waste, etc) Soil Cond. (Dry, (D Wet, Moist) Precip. Past 24 Hrs. inches > K a c a -• o ; _ N' . w a " w TKN mg/kg z > c 9 °; c g w mg/kg Nitrate and Nitrite mg/kg ( Ibs/acre) Name of Crop Type Receiving Residual Application Crop 1 Crop 2 Crop I Crop 2 1-2009 79.8 11.64 0.395 W00031725 dry 0 s 0.3 0.5 81200 8200 1 30.786 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 79.81 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P ( 30.186 ) 0.000 Lime Applied Annual lbs/acre 0.009 0.003 0.229 0.083 0.023 0.001 0.006 0.033 0.002 0.252 15.405 � Date lbs/ac Prior Years Cumulative Ibs/ac 0.11 0.119 - 36 0.05 0.053„ 34 9.146 9.375,, 1 1338 0.634 0.717v NA 1.47 IA93 267 0.043 0.044v 15 0.182 0.188 J NA 0.465 0.498 374 0.079 0.081 89 12.396 12.648v 2498 Current Cumulative lbs/ac Permitted C. P. L. R.**** Permit PAN Limit lst/2nd Crop F 216 "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." �j *Application Method: S - Surface, IN - Injection, INC - Incorporation /G **Volatilization Rate: Surface -0.5, Injection/incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate. DENR FORM FSF (12/2006) Report Number: R09126-8005 Account Number: 46381 To: SOUTHERN SOIL BUILDERS 958 HOOTS ROAD ROARING RIVER, NC 28669 ATTN: DENNIS KEY LAB NUMBER: 42762 SAMPLE ID: BAXTER A&L EASTERN LABORATORIES, INC. 7621 Whitepine Road • Richmond, Virginia 23237 (804) 743-9401 • Fax No. (804) 271-6446 FOR: BAXTER li•L�Z�I�:i�I3�k'f/ REPORT OF ANALYSIS copy: ZACH KEY DATE SAMPLED: 5/4/2009 1245 DATE RECEIVED: 5/6/2009 1230 DATE REPORTED: 5/1 1/2009 PAGE: 1 Solids, Total (As is) 11.64 116400 100 JM 05/06/09 16:00 SM 2540G Nitrogen, Total Kjeldahl 8.12 81200 10 JM 05/07/09 16:00 SM 4500 (NorgB+NH3C) Phosphorus 1.95 19500 100 KM 05/07/09 16:00 SW 846-3051/6010B Potassium 0.55 5500 100 KM 05/07/09 16:00 SW 846-3051/6010B Sulfur 1.58 15800 100 KM 05/07/09 16:00 SW 846-3051/6010B Calcium 1.68 16800 �q% 1L 100 KM 05/07/09 16:00 SW 846-3051/6010B Magnesium 0.44 4400 512•Z 100 KM 05/07/09 16:00 SW 846-3051/6010B .Sodium 0.35 35004olN-5P- 100 KM 05/07/09 16:00 SW 846-3051/6010B Iron 11800 1 KM 05/07/09 16:00 SW 846-3051/6010B Aluminum 2350 10 KM 05/07/09 16:00 SW 846-3051/6010B Manganese 153 1 KM 05/07/09 16:00 SW 846-3051/6010B Copper - 290 1 KM Q5/07/09 15:00 SW 846-3051/6010B Zinc 319 1 KM 05/07/09 16:00 SW 846-3051/6010B Nitrogen, Ammonia (as N) 0.82 8200 10 JM 05/07/09 14:00 SM 4500(NH3B+NH3C) Nitrogen, Organic (N) 7.30 73000 100 DCH CALCULATION Nitrogen, NO3+NO2 < 1 1 KS 05/07/09 1.5:00 SM 4500-NO3F Cadmium 4.0 1 KM 05/07/09 16:00 SW 846-3051/6010B Chromium 105 5 KM 05/07/09 16:00 SW 846-3051/6010B All values are on a dry weight basis except as noted. Detection Limit on all N series is on a wet basis. BDL' - Below Detection Limit Our reports and letters are for the exclusive and confidential use of our clients. and ma.r.not be reproduced in whole or ,n part, nor may any reference be made to the work, the results.. or the company ,n any advernsinq.,news release or other public announcements without obtaining our prior written authorization --li'CI `n � PAUL C. H. CHU • Report Number: R09126-8005 A&L EASTERN LABORATORIES, INC. y Account Number: 7621 Whitepine Road •Richmond, Virginia 23237 AFL 46381 (804) 743-9401 • Fax No. (804) 271-6446 TO: SOUTHERN SOIL BUILDERS 958 HOOTS ROAD ROARING RIVER, NC 28669 ATTN: DENNIS KEY LAB NUMBER: 42762 SAMPLE ID: BAXTER FOR: BAXTER NC CERT #257 REPORT OF ANALYSIS copy: ZACH KEY DATE SAMPLED: 5/4/2009 1245 DATE RECEIVED: 5/6/2009 1230 DATE REPORTED: 5/11/2009 PAGE: 2 Nickel 42 5 KM 05/07/09 16:00 SW 846-3051/601OB Lead 29 5 KM 05/07/09 16:00 SW 846-3051/601OB Arsenic 12.0 1.0 KM 05/07/09 15:00 SW 846-601 OB Mercury 1.2 0.4 KM 05/08/09 15:00 SW 846-7471A Selenium 2.1 1.0 KM 05/07/09 15:00 SW 846-601OB pH (Std. Unit, As is) 7.29 0.01 RD 05/07/09 12:30 SW 846-9045D Molybdenum 8 5 KM 05/07/09 16:00 SW 846-3051/601OB All values are on a dry weight basis except as noted. Detection Limit on all N series is on a wet basis. BDL' - Below Detection Limit Our reports and letters are for the exclusive and confidential use of our clients, and may not be reproduced in whole or in part, nor may any reference be made - to the work. the results, or the company in any advertising, news release. or other public announcements without obtaining our prior written authorization �y• PAUL C. H. CHU •;S Analytical Results Southern Soil Builders For: Baxter 958 Hoots Road Roaring River NC 28669 Entered 5/4/2009 Reported: 7/8/2009 Sample Remark Sample ID Parameter Cust ID Result Units Method 'Date Analyzed Analyst 09054-9.1 % Solids 1 1.7 % SM2540B 5/5/09 CL 09054-9.1 Fecal Coliform MTF 1 7,647 MPN/g SM92210E 5/5/09 CL 09054-9.10 Corrosivity TCLP See Attached SW-846 5/21/09 PACE 09054-9.10 Ignitability TCLP See Attached 1010M 5/21/09 PACE 09054-9.10 Reactivity TCLP See Attached SW-846 : 5/21/09 CL 09054-9.10 TCLP TCLP See Attached 1311 t 5/21/09 PACE 09054-9.2 % Solids 2 1.76 % SM2540B 5/5/09 CL 09054-9.2 Fecal Coliform MTF 2 7,955 MPN/g SM92210E. 5/5/09 CL 09054-9.3 % Solids 3 1.75 % SM2540B 5/5/09 CL 09054-9.3 Fecal Coliform MTF 3 9,714. MPN/g SM92210E 5/5/09 CL 09054-9.4 %.Solids 4 1.67 % SM2540B 5/5/09 CL 09054-9.4 Fecal Coliform MTF 4 29,940 MPN/g SM92210E 5/5/09, CL 09054-9.5 % Solids 5 1.67 % SM2540B 5/5/09 CL 09054-9.5 Fecal Coliform MTF 5 6,587- MPN/g SM92210E 5/5/Q9 CL 09054-9.6 % Solids 6 1.64 % SM2540B 5/5/09 CL 09054-9.6 Fecal Coliform MTF 6 4,878 MPN/g SM9221 CE ' 5/5/09 CL. 09054-9.7 % Solids 7 1.7 % SM2540B 5/5/09 CL 09054-9.7 Fecal Coliform MTF 7 10,000 MPN/g SM92210E' 5/5/09 CL 09054-9.7 Geometric Mean 7 9,225 ✓ MPN/g dry wt. basis 5/5/09 CL 09054-9.8 VSS Baxter A, 11,900 mg/L SM2540G 5/6/09 CL 09054-9.9 VSS Baxter B 350 mg/L SM2540G 5/6/09 CL W. T VS --3 P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697 Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 5/4/2009 Reported: 7/8/2009 Sample Remark Sample ID Parameter Cust ID Respectfully submitted, 1 Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 For: Result Units Method Date P.O. Box 228 • Statesville, North Carolina 28687. 704/872/4697 Analytical Environmental Services, Inc Date: 15-May-09 Client: Pace Analytical Services, Inc. Client Sample ID: 09054-9.10 Project: 9243664 Collection Date: .5/4/2009 12:50:00 PM Lab ID: 0905561-001 Matrix: Aqueous Analyses Reporting Dilution , Y Result Limit Qual Units BatchID 4 Factor Date Analyzed Analyst HERBICIDES, TCLP SW1311/8151A 2,4,5-TP (Silvex) BRL 0.20 2,4-D BRL 0.20 Surr: DCAA 100 36.6-149 Qualifien: Value exceeds maximum contaminant level BRL Below reporting limit H Holding times for preparation or analysis exceeded N Amlyte not NELAC certified B Analyte detected in the associated method blank > Greater than Result value (SW3510B) m8/L i'13188 1 05/13/2009 13:36' El , m8/L 113188 1 05/13/2009 13:36 El %REC 113188' 1 05/13/200913:36 El E Estimated (value above quantization range) S Spike Recovery outside limos due to matrix Narr See case narrative NC Not confirmed < Less than Result value Page 3 of 5 Analytical Environmental Services, Inc. CLIENT: Pace Analytical Services, Inc. Work Order: 0905561 Project: 9243664 Sample ID: MB-113188 Client ID: Analyte 2,4,5-TP (Silvex) 2.4-D Surr: DCAA Sample ID: LCS-113188 Client ID: Analyte 2,4.5-TP (Silvex) 2,4-D Surr: DCAA Date: 15-May-09 ANALYTICAL QC SUMMARY REPORT TestCode: HERBICIDES, TCLP SW1311/8151A camp i ype: MBLK Batch ID: 113188 Units: mg/L TestCode: HERBICIDES, TCLP SW131118151A Result RPT Limit SPK value SPK Ref Val BRL 0.20 0 0 BRL 0.20 0 0 0.4379 0 0.5 0 SampType: LCS Batch ID:113188 Units: mg/L TestCode: HERBICIDES, TCLP SW131118161A Result RPT Limit SPK value SPK Ref Val 0.4525 0.20 0.5 0 0.4238 0.20 0.5 0 0.5144 0 0.5 0 Sample ID: 0905428-001AMS SampType: MS Batch ID:113188 Units: mg/L Client ID: TestCode: HERBICIDES, TCLP SW1311181SIA Analyte Result RPT Limit SPK value SPK Ref Val 2,4,5-TP (Silvex) 0.3733 0.20 0.5 0 2,4-D 0.3462 0.20 0.5 0 Surr: DCAA 0.4369 0 0.5 0 Prep Date: 6/12/2009 Analysis Date: 6/1312009 %REC Lowl-imit Highlimit RPD Ref Val 0 0 0 0 0 0 0 0 87.6 36.6 149 0 Prep Date: 5/12/2009 Analysis Date: 5/13/2009 %REC Lowl-imit Highlimit RPD Ref Val 90.5 73.3 120 0 84.8 57.9 120 0 103 36.6 149 0 Prep Date: 5/12/2009 Analysis Date: 5/13/2009 %REC Lowl-imit Highlimit RPD Ref Vat 74.7 63.4 133 0 69.2 44.5 128 0 87.4 36.6 149 0 RunNo: 147867 SegNo: 3037980 %RPD RPDLimit Qual 0 0 0 RunNo: 147867 SegNo: 3037981 %RPD RPDLimit Qual 0 0 0 RunNo: 147867 SegNo: 3037983 %RPD RPDLimit Qual 0 0 0 .' Qualifiers: < Less than Result value > Greater than Result value ' B Analyte detected in the associated Method Blank ` BRL Below Reporting Limit E Estimated value above quantitation range H Holding times for preparation or analysis exceeded 1 Estimated value detected below Reporting Limit N Analyte, not NELAC certified . R. . • RPD outside limits due.to.matrix �.• Rpt Lim Reporting Limit S Spike Recovery outside limits due to matrix ` Page I of l Page 5 of 5 7 a/� ,, ^ a' Pace analytical Services, Ina Pace Analytical Services, Inc. G ceA alytic.al . 2225 Riverside Dr. 98W KncryAve. Suite 1pp wwwPacerabsr= Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Project: 09054-9 Pace Project No.: 9243664 Sample: 09054-9.10 lab ID: 9243664001 Collected: 05/04/09 12:50 Received: 05/07/09 10:25 Matrix: Other Re& is reported on a "dry -weight' basis Parameters Results Units Report Limit OF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP SPE Analytical Method: EPA 8081 Preparation Method: EPA 3535 Leachate Method/Date: EPA 1311; 05/15/09 00:00 gamma-BHC (Lindane) Chlordane (Technical) NO ug/L 0.50 1 05/20/09 17:45 05/21/09 11:22 58-89-9 Endrin NO ug/L 3,0 1 05/20/09 17:45 05/21/09 11:22 57-74-9 Heptachlor epoxide ND ug/L NO ug/L 0.50 1 05/20/09 17:45 05/21/09 11:22 72-20-8 ' Methoxychlor NO ug/L 0.50 1 05/20/09 17:45 05/21/09 11:22 1024-57-3 Toxaphene NO ug/L 1,000 1 05/20/09 17:45 05/21/09 11:22 72-43-5 Decachlorobiphenyl (S) 66 % 3.0 1 0520169 17:45 05/21/09 11:22 8001-35-2 Tetrachloro-m-xy(ene (S) 31 % 10-138 1 0520/09 17:45 0521/09 11:22 2051-24-3 10-110 1 0520/09 17:45 0521109 11:22 87.7-09-8 9010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Me#wWDate: EPA 1311; 0520/09 17:30 Arsenic Barium NO mg/L 0.025 1 0521/09 12:30 0521/09 17:09 7440-W2 Cadmium 0.043 mg/L 0.025 1 05/21/09 12:30 0521/09 17:09 7440-39-3 Chromium NO mg/L 0.0050 1 0521/0912:30 0521/09 17:09 7440-43-9 Lead NO mg/L 0.025 1 0521/09 12:30 0521/09 17:09 7440- 47-3 Selenium NO mg/L 0.025 1 0521/09 12:30 05/21/09 17:0 ' 7439-92-1 NO mg/L 0.050 1 0521/09 12:30 0521/09 17:09 7782-49-2 Silver NO mg/L 0.025 1 0521/09 12:30 0521/09 17:09 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 05/20/09 17:30 Mercury NO uWL 020 1 0521109 12:30 0521109 15:57 7439-97-6 , 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 t• Leachate Method/Date: EPA 1311; 05115/09 00:00 ,1,4-Dichlorobenzene 2,4-Dinitrotoluene NO ug/L 50.0 1 05/21/09 10:00 0522109 02:46 106-46-7 Hexachloro-1,3-butadiene NO ug/L NO ug/L 50.0 1 0521/09 10:00 0522/09 02:46` 12-1-14-2 Hexachlorobenzene NO ug/L 50.0 1 05/21/09 10:00 0522/09 02:46 '87.68-3 Hexachloroethane NO ug/L 50.0 1 05/21/09 10:00 05122/09 02:46 118-74-1 2-Methylphenol(o-Cresol) NO ug/L 50.0 1 0521/09 10:00 0522/09 02:46 67-72-1 3&4-Methylphenol(m&p Cresol) NO ug/L 50.0 1 50.0 0521/09 10:00 0522/09 02:46 95-48-7 Nitrobenzene NO ug/L 1 0521/09 10:00 051WO9 02:46 Pentachlorophenol NO ug/L 50.0 1 50.0 0521/09 10:00 0522109 02:46 98-95-3 Pyridine 1 0521/09 10:00 0522/09 02:46 87-86-5 2,4,5-Trichlorophenol NO ug/L NO ug/L 50.0 1 0521/09 10:00 0522109 02:46 110-86-1 2,4,6-Tdchlorophenol NO ug/L 50.0 1 0521/09 10:00 05rM09 02:46 95-la5-4 Nitrobenzene-d5 (S) 56 % 50.0 1 0521/09 10:00 0522/09 02:46 88-06-2 2-Fluorobiphenyl (S) 62 % 30-150 1 05/21/09 10:00 0522/09 02:46. •4165-60-0 TerphenyW 14 (S) 30-150 1 05/21/09 10:00 05/22/09 02:46 321-60-8 Phenol-d6 (S) 64 % 30-150 1 05/21/09 10:00 0522/09 02:46 1718-01-0 ' - 2-Fluorophenol (S) 34 % 46 % 25-150 1 0521/09 10:00 0522/09 02:46 13127-88.3 2,4,6-Tribromophenol (S) 42 % 25-150 1 05/21/09 10:00 0522/09 02:46 367-124 25-150 1 0521/09 10:00 0522/09 02:46 118-79-6 Date: 06/092009 03:31 PM REPORT OF LABORATORY ANALYSIS Page 4 of 11 This report shell not be reproduced, except in full, without fhe written consent of Pace Ana"ml Services, Inc.. PiceAnalytical wwwyacelabscw Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical t W00 iGrw;Ave: H-lie�. Project: 09054-9 •. Pace Project No.: 9243664 Sample: 09054-9.10 Lab ID: 9243664001 Collected: 05/04/09 12:50 Received: 06/07/09 10:25 Matrix: Other Resuks reported on a "d7-weight, bases Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1,4-Dichlorobenzene 1,2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Trichloroethene Vinyl chloride 12-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) W45 pH Soil PH at 25 Degrees C 733C Reactive Cyanide Cyanide, Reactive 734S Reactive Sulfide Sulfide, Reactive Date: 06/09/2009 03:31 PM Analytical Method: EPA 8260 _ NO ug/L NO 125 25 s Ci° 05/20/09 01:4 71-43-2 ug/L 250 2t5 05/20/09 01:43, 78-93-3 ND ug/L 125 25 OSR0109 01:43 56-23-5 ND ug/L 125_ 25 `/ 05/20/09 01:43 108-90-7 - NO ug/L 125 25 Lot OW" 01:43 67-6&3 ND ug/L 125 25 YNA-) 05/20/09 01:43. 106-46-7 NO ug/L 125 25 05/20/09 01:43 1074)6-2 ' NO ug/L 125 25 ��5ixk 0520/09 01:43 75-35-4 ND ug/L 125 25 0520/09 01:43 127-18-4 NO ug/L 125 25 tipcD ' 05/20/09 01:43' 79-01-6 NO ug/L 125 25 4-1- 0520/09 01:43. 75-01-4 114 % 79-120 25 05/20/0905/20/09 01:43 17060-07-0 122 % 70-120 25 /,',"!`�- 0520/09 01:43 2037-26-5 94 % 87-109 25 1 0520/09 01:43 460-00-4 117 % 85-115 25 //l G/�` 0520/09 01.43 1868,53-7 Analytical Method: EPA 9045 5.4 Std.. Units 0.10 1 Analytical Method: SW-846 7.3.3.2 Modified NO mg/L 0.0050 1 Analytical Method: SW-846 7.3.4.2 NO mg/L 1.0 1 0511210911:2;. Vo t&( f 05/11/09 14:32 . REPORT OF LABORATORY ANALYSIS This report shall not be reproduoed, except in full, without the written consent of Pace Analytical Services, Inc.. Page 5 of 11 Analytical Results Southern Soil Builders 958 Hoots Road Roaring River NC 28669 Entered 7/31/2009 Reported: 8/14/2009 Sample Remark Sample ID Parameter Cust ID For Result Units Method Date Analyzed Analyst 090731-5 Ignitability Baxter <0.8 1010M 8/11/09 Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NCO0909 PACE P.O. Box 228 9 Statesville, North Carolina 28687 • 704/872/4697 • ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FOR14 (02T Rules) Facility Name: Baxter Healthcare WWTP Name: Baxter Healthcare WQ Permit Number: WQ0031725 NPDES Number: NC0006564 Monitoring Period: From 1/1/2009 To 12/31/2009 Pathogen Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: Class A: Alt. A (time/temp) ❑ Alt B (Alk Treatment) ❑ Alt. C (Prior Testing)❑ AILD (No Prior Test) I Process to Further Reduce Pathogengs ❑ If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ❑ Heat Drying ❑ Heat Treatment ❑ I Thermophilic ❑ Beta Ray ❑ Gamma Ray ❑ Pasteurization ❑ 1 - Class B: JAIt. (1) Fecal Density Alt. (2) Process to Significantly Reduce Pathogens ❑ If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ❑ Air Drying ❑ 1 Composting ❑ jAerobic Digestion 0 Anaerobic Digestion ❑ If applicable to alternative performed (Class A or Class B) complete the following monitoring data: Parameter Allowable Level in Sludge Pathogen Density Number ot Excee- dene Frequency of Analysis Sample Type Analytical Tech - woue Minimu Geo. Mean Maximum Units Fecal Coliform 2 x 10 to the 6th power per gram of total solids MPN 4878 9225 29940 MPN/g 0 7 grab sm9221 e CFU • 1000 mpn per gram of total solid (dry weight) Salmonella bacteria (in lieu of fecal coliform) 3 MPN per 4 grams total solid (dry weight) • Vector Attraction Reduction (15A NCAC 02T .1107) - Please indicate alternative performed: Alt.I (VS reduction) Alt. 2 (40-day bench) ❑ Alt. 3 (30-day bench) ❑ Alt. 4 (Spec. OZ uptake) ❑ Alt. 5 (14-Day Aerobic) ❑ Alt. 6 (Alk. Stabilization ❑ Alt 7 (Drying - Stable) jAlt. 8 (Drying - Unstable) ❑ Alt. 9 (Injection) ❑ Alt. 10 (Incorporation) ❑ No vector attraction reduction alternatives were performed ❑ CERTIFICATION STATEMENT (please check the appropriate statement) +❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance,with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." S-(uuCN r�t,•�E �,J S7EUG1-C�K Y Dennis Key President Southern Soil Huilders, Inc. Preparer Name and Title (type or print) Land Applier Name and Title (if applicable)(type or print) Signatu e of Preparer* tlDate Signature of and Applier (if applicable) Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM PVRF 02T (12/2006) Page 1 of 5 A &L Eastern Laboratories, Inc. Report Number: 09-351-0538 ®� L Account Number: 46381 r77621 wh¢epine Road Richmond. Virginia 23277 (804) 743-9401 Fax (804) 27t-gaa6 www.allabscomJ Submitted By: ZACH KEY Send To: SOUTHERN SOIL BUILDERS Grower: SOUTHERN SOIL BUILDERS Farm ID: DENNIS KEY 958 HOOTS ROAD ROARING RIVER NC 28669 SOIL ANALYSIS REPORT Analytical Method(s): Date Received: 12/17/2009 Date Of Analysis: 12/18/2009 Date Of Report: 12/21/2009 MEHLICH 3 Organic Matter Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Field ID Number % Rate Ca Na Rate m Rate Soil pH Buffer H Index meq/100g meq/1009 lbs/A ppm Rate ppm Rate ppm. Rate ppm Rate ppm pp BT9-1 125 VH 37 VL 151 M 1745 H 19 VL 6.9 6.92 0.1 10.3 17851 2.9 M 93 NC=104 NC=19 BT6-1 72 H 31 VL 158 H 1287 H 72 L 6.7 6.89 0.4 8.5 17852 2.8 M 94 NC=60 NC=16 77 H 30 VL 11B M 1515 H 21 VL 71 0.0 8.7 BT6-3 17853 3.0 M 98 NC=64 NC=15 50 VL 221 H 607 M 12 VL 6.3 6.87 0.6 5.7 54 2.1 L 84 NC=19 NC=26 F��lL 21 L 43 VL 132 H 744 M 11 VL 6.80 1.3 6.3 T1 F1755 2.5 L 91 = NC = 22 NC 17 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NO3N S Zn Mn Fe Cu B Ss CI AI Field ID /a /o o % % % ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ms/cm Rate ppm Rate ppm 9 VL 23.7 VH 82 VH 77 VH 7.4 VH 0.7 M 0.16 VL BT9 1 0.9 12.2 84.7 0.8 1.4 NC=23 NC=592.5 NC=513 NC=370.0 9 VL 10.6 VH 28 H 77 VH 5.6 VH 0.5 L 0.16 VL BT6-1 0.9 15.5 75.7 3 7 4.5 NC = 23 NC = 265.0 NC = 175 NC = 280.0 7 VL 14.5 VH 92 VH 65 VH 5.3 .VH 0.5 L 0.13 r VL BT6-3 0.9 11.3 j 87.1 1.0 0.0 ., NC =•18• NC = 362.5• Nr- = 57.5 NC = 265.0. 10 L 1.7 L 18 M 60 VH 1 A M 0 1 VL 0.1 1 VL I S1 2.2 32.3 53.2 0 9 10.5 NC = 25 NC = 42.5 NC = 113 NC = 70.0 7 VL 5.7 H B L 137 VH 1.9 H 01 VL 0.12 VL T1 TT81:775HE E211 NC=18 NC=1425 NC=50 NC=950 , Values on this report represent the plant available nutrients ,n the Explanation of symbols % (percent). ppm tparts per million) Ibs/A tms,enon appd.es to samoteisi testeo Samples �n�m d th-rty (lays attw tesnnq afe ,eta,neo a soil. Rating alter each value VL (Very Low). L (Low) M (Medium). (pounds per acre). ms/cm (milli -mhos per centimeter) meq/ t00g ma. t7 y H (High) VH (Very High). ENR - Estimated Nitrogen Release (mill-e(1uivalent per 100 grams) Convers,ons ppm x 2 = Ibs/A Anatvs.s n,eparen oy Axt Eastw^ i ono, ato, es i^,: ' C E C - Canon Exchange Capacity Soluble Salts ms/cm x 640 = ppm Oscar Rwz Page 2 of 5 Report Number: 09-351-0538 Account Number: 46381 r7Y� Y www allabs.com Send To: SOUTHERN SOIL BUILDERS DENNIS KEY 958 HOOTS ROAD ROARING RIVER NC 28669 A&L Eastern Laboratories, Inc. 7621 Whitepine Road Richmond Virginia 23237 (804) 743-9401 Par (804) 271 b146 Grower: Submitted By: ZACH KEY SOUTHERN SOIL BUILDERS Farm ID: SOIL ANALYSIS REPORT Analytical Method(s): n.to r)f Ronnnt- 19/71/?nnq MEHLICH 3 vp" `cyy yV _ Organic Matter' Phosphorus Potassium Magnesium Calcium Sodium pH Acidity C.E.0 Sample ID Lab ENR Mehlich 3 Reserve K Mg Ca Na Soil Buffer H Field ID Number % Rate lbs/A ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate ppm Rate PH Index meq/100g megH00g F1 159 VH 28 VL 109 M 800 M 17 VL 5.8 6.81 1.2 6.2 17856 3.2 M 105 NC = 132 NC = 14 T2 25 L 70 L 145 H 668 M 11 VL 6.82 1.1 5.9 17857 2.2 L 86 NC=21 NC=36 -] 1 -] 64 H 26 VL 124 H 649 M 17 VL 6.0 6.85 0.8 �71 FP-0 17858 2 2 L 87 I NC=53 NC=13 - - NW11 VH 123 M 184 H 1216 M 16 VL 5.9 6.76 1.7 9.7 17859 3.2 M 100 I307 NC = 256 NC = 63 NW13 344 VH 197 H 225 H 1414 M 15 VL 5.9 6.73 2.0 11.5 17860 4.2 M 118 1 1 NC = 287 NC = 101 Percent Base Saturation Nitrate Sulfur Zinc Manganese Iron Copper Boron Soluble Salts Chloride Aluminum Sample ID K Mg Ca Na H NOON S Zn Mn Fe Cu B SS CI Al Field ID , /a % o /o o /o % PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate PP m Rate ms/cm Rate PP m Rate PP m F1 12 L 5.9 H 8 L 106 VH 9.7 VH 0.3 VL 0.13 VL 1.2 14.7 64.5 1.2 19.2 NC = 30 NC = 147.5 NC = 50 NC = 485.0 T2 8 VL 3.0 M 7 L 70 VH 2.0 H 0.1 VL 0.137VL 3.0 20.5 56.6 0.8 19.0 NC = 20 NC = 75 0 NC = 44 NC = 100.0 JP-01 7 VL 7.1 H 7 L 99 VH 4.9 VH 0.2 VL 0.11 VL 1.3 19.9 „ 62.4 , 1.4 F15 5 NC=18 NC=1775 NC=44 NC=245.0 NW11 9 VLrNC VH M VH 6.0 VH 0.4 L 0.14 VL 3 3 15.8 62.7 0.7 17 1 NC = 23 = 342 S �1ONC = 63 1238 NC = 300.0 NW13 12 L VH M VH VH 0.6 M. 0 32 VL 44 163 61.5 06 171 1153 NC = 30 NC = 382 5 �12 NC = 75 1229 16.6 NC = 330.0 Values on this report represent the plant available nutrients in the Explanation of symbols °i, (percent) ppm (parts per million) Ibs/A th's reoon to wslea sanWes are reranect a sal Rating after each Value VL (Very Low) L (Low) M (Medium), (pounds per acre) msrcm (milli -mhos per centimeter) megr 100g tit ln"n, oars Atte, tesang H IHigh) VH (Very Fligh) ENR - Estimated Nitrogen Release (mill -equivalent per 100 grams) COnvers�ons pp^r + 2 = Ibs/A AIVsis oqe.nare,i n.. 4Sl Faster^ ano, aiurs ❑n C E C - Canon Exchange Capacity Soluble Salts ms/cm . 640 = poni by Oscar Rutz Below are the calculations for Vector Attraction Reduction requirement per 15A NCAC 02T.1107 (Alt 1). Statesville Analytical shows a VSS on 5/6/09, Sample ID 09054-9.8 (also identified as "Baxter A") of 11900 mg/L. This sample was pulled at the beginning of the digestor process. Statesville Analytical shows a VSS on 5/6/09, Sample ID 09054-9.9 (also identified as "Baxter B") of 350 mg/L. This sample was pulled at the end of the dewatering process. ((VSS In (mg/L) — VSS Out (mg/L)) _ VSS In (mg/L)) x 100 = % Solids Reduction ((11900 mg/L — 350 mg/L) _ 11900 mg/L) x 100 = 97.06 % Solids Reduction d This meets the 15A.NCAC 02T.1107 (Alt 1) requirement of minimum 38% Solids Reduction. Stephen Gouge Wastewater TreatrrYent Supervisor Baxter Healthcare Corp. 11,9, oo i - 310 Il�6'J -(119(�,p7, v, 6(5, S-A