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HomeMy WebLinkAboutWQ0031725_Annual Report_20090224Annual Report Review SOP Class B Land Application 1. Annual Land Application Certification Form • Was a certification form submitted? y S. • Was land application conducted during the reported year? NHS © How many dry tons and dry tons per acre were applied? 151. 7l • Were the applications within the permitted amount? y.eS • Verify PAN if more than 10 tons/acre . • Did it indicate compliance? veS • Was it signed by the appropriate people? N65 2. Monitoring 1 • Were the analyses conducted at the required frequency?y. 5 • Were the metals analyses reported on the Residual Sampling Summary Form? ..es a Were the results reported in mg/kg? yf5 B Were the metals within ceiling concentration permit limits? yes • If no, were the lab analyses attached? • Were all the required parameters tested?t 'r• Was TCLP analysis conducted?-' & . "�5 / P tcec..: — NO • Were the TCLP contaminants within regulatory limits? y42S' 3. Field Summary a Were the land application events recorded on the Field Summary Forms?/e., o Was a Field Summary Form submitted for each field applied on?eS • Were all the residuals applied to permitted land?1 ,5 • Were all the residuals applied from permitted sources? y &Y • Were the field loading rates for each metal and PAN calculated (year to date)?1 L S' • iWere the cumulative pollutant loading rates calculated?v,5 • Were the calculations correct? ey � OZ PAN �„it �! NEef Caf°"e�� ®�• • © Were the PAN loading rates w°e.5 J7 within permit limits?�a ,ieU . 5- J 4rcli ii/Aloe- i-S' /ow SO * Were the heavy metal cumulative pollutant loading rates within permit limits? fi€ic1 5-"" kV VP" • Were the residuals applied on a suitable crop . t(-S r T • Were the applications conducted during the crop's growing season?j e5 • Were the Field Summary Forms complete?'-9-5 • Was lime application on Field Summary Form? -C a ° two ' arAker2r 4: Pathogen and Vector Attraction Reduction • Was a signed copy of. the Pathogen and Vector Attraction UT ©. / Z f0 D. S'z .b T/4c fir Lv4�� q N� - u�gr1yJ' 'T.�arr�� eduction Form submit ed?'jeS • Did the f indicate the period of coverage, the residual class, and the pathogrn reduction alternative and the vector attraction reduction option used? • Was the. app priate documentation to show pathogeand vector attraction reduction included in the report? ® Was path gen and vector attraction reduction demonstrated according to 40 CFR Part 503 or 2T? .14® 5. Soil Tests • Was a Standard Soil Fertility Analysis conducted for each field applied on?J • Were the soil pH's 6.0 or greater for each application field? J0 TI = S. T2. 5. 5) ,SZ 5.3 • Were the copper and zinc indexes in the soil less than 3000 for each application field (state soils lab)? rtef 6. General • Was the report in the proper format?'45 • Were any parts of the annual report missing?y°es .7)004.4,--e- 4to>^ -Or VAR - Was• the report submitted on time?1 p_5 �iav- zoo9- PG-0($7 Vector Attraction Reduction Review ' "�� `4✓� • Was the sampling conducted at the required frequency? y eJ 38% Volatile Solids Reduction ® Was there 38% reduction? Do,±a nab' Su-br i -i • Were lab sheets/calculations in report? 64 no+ Subw% • Was the reduction on volatile solids (not total solids)? '/ S • Was the samples taken at beginning of digestion process and before application (Inspection)? Doc+a Ant sab.a.i • Were calculations correct? po-4A J 4 SLAILYh^►4e$::1_ 40-Day Bench Scale Test • Were residuals from anaerobically digested treatment (Inspection)? • Were residuals anaerobically digested in lab? • Was the test run for 40 days? • Was the test done between 30°C (86°F) and 37°C (99°F)? • Was the reduction on volatile solids (not total solids)? a Was the reduction less than 17%? • Were lab sheets/calculations in report? • Were calculations correct? 30-Day Bench Scale Test © Were residuals from aerobically digested treatment (Inspection)? ® Were residuals aerobically digested in lab? • Were residuals 2% or less total solids? • Was thetest run for 30 days? • Was the test done at 20°C (68°F)? a Was the reduction on volatile solids (not total solids)? o Was the reduction less than 15%?. © Were lab sheets/calculationsin report? • Were calculations correct? Specific Oxygen Uptake Rate (SOUR) • Were residuals from aerobically digested treatment (Inspection)? o Were residuals 2% or less total solids (dry weight basis) (not diluted)? • Was the test done between 10°C (50°F) and 30°C (86°F)? • Was the temperature corrected to 20°C (68°F)? a Was the SOUR equal to or less than 1.5 mg of oxygen per hour per gram of total residual solids (dry weight basis)? a Was the sample holding time under two hours? O Was the test started withinl5 minutes of sampling or aeration maintained? ANNUAL RESIDUAL SAMPLING SUMMARY FORM Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: W00031725 Facility Name:, Residual Source WQ # or NPDES #: WWTP Name: Residual Analysis Data Parameter (mg/kg) Percent Solids (%) Arsenic Baxter Healthcare NC0006564 Laboratory: 1) 2) 3) 4) 5) Pace Analytical Ceiling Conc. Limit NA 8-26-08 1.8 Sample or Composite Date 75 ND Cadmium Copper 85 ND -Chromium Lead 4,300 NA 245 87 840 ND Mercury 57 2.1 Molybdenum Nickel 75 ND 420 36.2. Selenium Zinc Total Phosphorus TKN , 100 7,500 NA NA ND 275 9230 18700 Ammonia -Nitrogen NA 1660 ND a For surface disposal fac'lities the ceiling concentration limits listed in this form are not applicable. Reference the individual permi for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant pen ies for submitting false information, including the possibility of fines and imprisonment for knowing violations." 212.o 1601 Nitrate and Nitrite Signature of Preparer *Preparer is defined in 40 CFR Part 503.9(r) and I5A NCAC 2T .1 102 (26) NA Date DENR FORM RSSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Baxter Healthcare Total Dry Tons Applied (Annual): 28.90 Permit #: Operator: .Acres Used: WQ0031725 Cation Exchange Capacity (non 503 only): Derek Teague Owner: Trilby Setzer Predominant Soil Series: CmB2 19.8 Acres Permitted: 19.8 Site #: S-01 Field #: S-0I Is and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posue Date 8/26/08 ? 3 6 6 8 9 10 11 12 "o Solids 1.8 Arsenic 0 Cadmium '0 Copper 245 Chromium 87 Lead 0 Mercury 2.1 Molvh- den um 0 Nickel 36.2 Selenium 0 Zinc 275 Total Phos- phorus 9230 , IDs/acre ): Total DT Ac.: App. Event 1 1.46 2 ± 6 7 6 9 1.0 11 12 Totals: Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 0.716 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.716 Chromium 0.254 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.254 1.ead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.006 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.006 Molvb- denum 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - Nickel 0.106 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.106 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Zinc 0.804 0.0Q0 0.000 0.000 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.804 Total Phos- phorus 26.989 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 d 26.989 "I certify, under penalty of law, that this document was prepared under my d�rect�on or supervision to aecor ance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". I,1.JLc �! Signature of Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: .Acres Used: Baxter Healthcare WQ0031725 Total Dry Tons Applied (Annual): 40.50 Cation Exchange Capacity (non 503 only): Derek Teague Owner: Trilby Setzer Predominant Soil Series: HsB2 25 Acres Permitted: 25 Site #: S-02 Field #: S-02 d st al Anal sis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample ort� Com- posite Date 8:26/08 ? 3 5 6 7 8] 9 10 11 12 % Solids I .8 Arsenic 0 Cadmium 0 Copper 245 Chromium 87 I.ead 0 Mercury 2.1 Molvb- denum 0 Nickel 36.2 Selenium 0 Zinc 275 Total Phos- phorus 9230 I Hea Metal Field Loadings (C alculated to Ibsiacre): :,lgII„a vy Total I)I Ac. App. Lent 1 I.62 2 3 4 5 6 7 8 9 10 11 12 Totals: Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 0.000 Copper 0.794 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.794 Chromium 0.282 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.282 I.ead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.007 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.007 Mol• b denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Nickel 0.117 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.117 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,000 Y.inc 0.891 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.891 I otal Phos- phorus 29.905 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 29.905 "I certify, under penalty of law, that this document was prepared under my airection or supervtston to accor ance v, ith a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". 7%. (3- 1)•) .") Signature or Land Applier Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: • Acres Used: Baxter Healthcare Total Dry Tons Applied (Annual): WQ0031725 Cation Exchange Capacity (non 503 only): 74.72 Derek Teague Owner: Larry Teague Predominant Soil Series: HsB2 26 Acres Permitted: 26 Site #: T-01 Field #: T-01 sis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or_LI Com- posite Dale 8n6/08 2 4 5 6 7 SJ 9 10 11 12' °'o Solids 1.8 Arsenic 0 Cadmium 0 Copper 245 Chromium 87 I.cad 0 Mercury 2.1 Molyb- denum 0 Nickel 36.2 Selenium 0 Zinc 275 I otal t'hos- phorus 9230 annual Heavy Metal Field Loadings (Calculated in Ibs/acre): Total Dt'Ac. A PP. .rent 1 2.87 2 3 4 6 7 8 9 10 11 12 c f Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Copper 1.406 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.406 Chromium 0.499 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.499 I.cad 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.012 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.012 v101} b denum 0.000 0.000 • 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Nickel 0.208 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.208 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Linc 1.579 0,000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 1.579 Total Phos- phorus 52.980 • 0.000 0.000 _ 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 - 0.000 52.980 "I certify, under penalty of law, that this document was prepared under my tree ion or supervision to accordance rs ith a system designed tp assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of tines and imprisonment for knowing violations". a? •1,7-dc�`1 Signature of 1.and Applier �. PP • Date DENR FORM MFLSF (12/2006) ANNUAL METALS FIELD LOADING SUMMARY FORM* Attach this form to the corresponding Field Loading Summary Form to be submitted in Annual Report Facility Name: Permit #: Operator: Acres Used: Baxter Healthcare WQ0031725 Derek Teague Owner: Larry Teague Predominant Soil Series: MgC2 10 Acres Permitted: 10 Site #: T-02 Field #: T-02 Total Dry Tons Applied (Annual): 7.60 Cation Exchange Capacity (non 503 only): al Anal sis Data (Heavy Metals and Total Phosphorus use mg/kg, % Solids use Raw Percent #): Sample or Com- posite Date J 8/26/08 2 1_3_ ji 5 6 8 9 10 11 12 % Solids I.8 Arsenic 0 Cadmium 0 Copper 245 Chromium 87 I.ead 0 Mercury 2.1 Molyb- denum 0 Nickel 36..2 Selenium 0 Zinc 275 Total Phos- phorus 9230 \11IIUAI Ilcllr� i.■a.■a■ ■�.■.. uvw.....b� ��...._�.�-_� ---------- , Total 1)T Ac. APP. Event 1 0.76 2 3 b 6 7 8 9 10 11 12 Totals: Arsenic 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Cadmium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.0.00 0.000 0.000 Copper 0.371 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.37I Chromium 0.132 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.132 Lead 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Mercury 0.003 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.003 b1c lyh denum 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Nickel 0.055 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.055 Selenium 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Zinc 0.417 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0,417 1 oral Phos- phorus 13.993 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000, 0.000 0.000 13.993 on in accordance "1 certify, under penalty of law, that this document was prepared direction or supervise with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations". a' Date Land Signa Applier re of DENR FORM MFLSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE,. Facility Name: Baxter Healthcare Land Owner: Trilby Setzer Operator Derek Teague Croa I Name: Fescue WQ Permit 11: WQ0031725 Annual Dry Tons Applied: 28.9388 Predominant Soil Series: CmB2 Crop 1 Max. PAN: 216 Field #: S-01 Site 14: S-01 Crop 2 Name: Acres Utilized: 19.8 Acres Permitted: 19.8 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: O Y(enter ?; Volume one)Solids/ Liquid Cu. Yds applied Gallons % Solids Volume Applied per PP Acre (Dry Tons/Ac) Residual Sources NPDES f<, W #, ( 0 Fen., Animal Waste, etc) Soil Cond. (Dry Wet. Moist) Precip.Nitrate Past 24 Hrs. inches Application 'Method' o m a a _ _.z. ^ = Mineralization Rates* TKN mg/kg Ammonia Y' Nitrogen E and Nitrite mg/kg PAN Applied ( Ibs/acre) Name of Crop Type Receiving Residual Application PP Crop 1 Crop 2 Crop I Crop 2 11-2008 168.6 11.5 0.825 WQ0031725 dry 0 s 0.5 0.3 18700 1660 0 9.801 NA Fescue 12-2008 130.2 11.5 0.637 WQ0031725 dry 0 1 s 0.5 0.3 18700 1660 0 7.568 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): ' TOTALS: 298.8 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 17.369 0.000 Lime Applied Annual lbs/acre 0.000 0.000 0.716 0.254 0.000 0.006 0.000 0.106 0.000 0.804 26.989 Date lbs/ac Prior Years Cumulative lbs/ac 0.11 0.05 8.43 0.38 1.47 0.037 0.182 0.465 0.079 12.396 6-2008 2000 Current Cumulative lbs/ac 0.110 v 0.050 v 9.146v 0.6341/ 1.470v 0.043v 0.182v 0.571,E 0.079v 13.200✓ Permitted C. P. L. R.**** 36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit lstl2nd Crop 216 h "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure ta qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Land Applier *Application Method: S - Surface, IN - Injection, INC - Incorporation 2 - 11-,a(Jo y **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 Date *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE: A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter llealthcare Land Owner: Trilby Selzer Operator: Derek Teague Fescue WQ Permit n: WQ0031725 Annual Dry Tons Applied: 40.5026 Predominant Soil Series: HsB2 Field tt: S-02 Site 14: S-02 Crop 1 Max. PAN: 216 Crop 2 Name: Acres Utilized: 25 Acres Permitted: 25 Cation Exchange Capacity (non 503): Crop 2 Max. PAN: Precip.-0 Past 24 Hrs. nches 3 - 3 ^ a « o' > < --• z - _ ' a > z 5 w P w •-N" * w > TKN mg/kg Ammonia m rn Nitrogen E Nitrate and Nitrite PAN Applied (Ibs/acre) Name of Crop Type Receiving Residual Application o 0 = Q Volume (enter one) Liquid Cu. Yds applied Solids/ Gallons % Solids Volume Applied per Acre (DryTons/Ac) Residual Sources (NPDES #_ WQ#. Fen., Animal Waste, etc) Soil Cont (Dry. Wet. Moist) mg/kg Crop 1 Crop 2 Crop 1 Crop 2 0 s 0.5 0.3 18700 1660 0 5.350 NA Fescue 7-2008 116.2 11.5 0.450 WQ0031725 dry t 0 s 0.5 0.3 18700 1660 0 1.441 NA Fescue 8-2008 31.3 11.5 0.121 WQ0031725 dry 0 s 0.5 0.3 18700 1660 0 3.540 NA Fescue 9-2008 76.9 11.5 0.298 WQ0031725 dry 0 s 0.5 0.3 18700 16600 0 13.409 NA Fescue 10-2008 193.8 11.5 0.751 WQ0031725 dry 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 FORM FSF supp to this form): Residuals Applications totals on FORM FSF supp ( attach TOTALS: 4182 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 23.740 0.000 Lime Applied Annual lbs/acre 0.000 0.000 0.794 0.282 0.000 0.007 0.000 0.117 0.000 0.891 29.905 le Date lbs/ac 6-2008 2000 Prior Years Cumulative lbs/ac 0 0 0 0 0 0 0 0 0 0 19"23 3 Current Cumulative lbs/ac 0.000 t/ 0.000✓ 0.794 t/ 0.282✓ 0.000v 0.007 ✓ 0.000'1 0.117✓ 0.000;/ 0.891'/ 36 34 1338 NA 267 15 NA 374 89 2498 Permitted C. P. L. R.**** Permit PAN Limit 1st/2nd Crop 216 • d d to assure that "I certify, under penalty of law, that this document was prepared under my direction or supervision ►n accordance with a system estgne qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." 7*Application Method: S - Surface, IN - Injection, INC - Incorporation ,G,.--;,, 222- /a- `uvel **Volatilization Rate: Surface-0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, // Si na ure of Land Applier Date calldigested -0.3, raw sludge-0.4 g aerobically ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Facility Name: Baxter Healthcare Land Owner: Larry Teague Qperator: Derek Teague Crop 1 Name: Fescue Crop 1 Max. PAN: 216 Volume applied (enter one) Solids/ Liquid Cu. Yds Gallons Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES WQ#. Fen.. Animal Waste. etc) 1-2008 2-2008 3-2008 4-2008 6-2008 87.1 11.5 0.324 213.3 11.5 0.795 WQ0031725 Soil Cond. (Dry.' Wet. Moist) WQ0031725 194.6 199.2 11.5 11.5 0.725 0.742 WQ0031725 WQ0031725 77.2 11.5 0.288 WQ0031725 0.000 dry Precip. Past 24 Hrs. inches ANNIUAI. LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. WQ Permit /t: WQ0031725 Field i : T-01 Acres Utilized: 26 Site #: T-01 Acres Permitted: 26 Annual Dry Tons Applied: 74.7100 Predominant Soil Series: HsB2 Cation Exchange Capacity (non 503): • Crop•.2 Max. PAN: Crop 2 Name: UO! T'Lw1PiOn 1KN mg/kg fi mg/kg Nitrate and N itrite mg/kg PAN Applied ( Ibs acre) Name of Crop Type Receiving Residual Application Crop I Crop 2 Crop 1 Crop 2 0 s 0.5 0.3 18700 1660 0 3.856 NA Fescue dry dry dry 0 0 0 s s s 0.5 0.5 0.5 0.3 0.3 0.3 18700 18700 18700 1660 1660 1660 0 0 0 9.442 8.615 8.818 NA NA NA Fescue Fescue Fescue dry 0 s 0.5 0.3 18700 1660 0 3.417 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 TOTALS: 771.4 0 Annual lbs/acre Prior Years Cumulative lbs/ac Current Cumulative lbs/ac Permitted C. P. L. R.**** 0.000 As 0.000 0.108 0.108 ✓ 36 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): P Cd 0.000 0.01 0.010 / 34 Cu 1.406 1.86 3.266 ✓ 1338 Cr 0.499 0 0.499 ✓ NA Pb 0.000 0.157 0.157� 267 Hg 0.012 0.0066 0.019 ✓ 15 Mo 0.000 0.145 0.1451-- NA Ni 0.208 0.1178 374 Se 0.000 0.0158 0.016✓ 89 Zn 1.579 1.704 3.283 ✓ 2498 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 52.980 34.1484- 0.000 Lime Applied Date lbs/ac 6-2008 2000 216 Permit PAN Limit 1 st/2nd Crop "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." *Application Method: S - Surface, IN - Injection, INC - Incorporation � 2- 1 ) --3(.• C 5 **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, Signature of Land Applier Date aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) ANNUAL LAND APPLICATION FIELD SUMMARY FORM PLEASE MAKE A COPY OF THIS BLANK FORM TO BE COMPLETED AND SUBMITTED FOR EACH FIELD APPLIED ON PLACE A "N/A" IN A BLANK OR BOX WHEN NOT APPLICABLE. Facility Name: Baxter Healthcare Land Owner: Larry Teague Operator: Derek Teague Crop 1 Name: Fescue Crop I Max. PAN: 162 WQ Permit #: WQ0031725 .Annual Dry Tons Applied: 7.5833 Field #: T-02 Site #: T-02 Acres Utilized: 10 Acres Permitted: 10 Predominant Soil Series: MgC2 Cation Exchange Capacity (non 503): Crop 2 Name: • Crop 2 Max. PAN: a) c( Q Volume (enier one) Liquid Cu. Yds applied. Solids/ Gallons 0/0. Solids Volume Applied per Acre (Dry Tons/Ac) Residual Sources (NPDES p. WQ4, Fen., Animal Waste, etc) Soil Cond. Wet. (i)r�' Moist) preci p. past 24 Hrs. inches > > K ? - Volatilization Rate** Mineralization Rate*** TKN mg/kg Ammonia g rn Nitrogen E Nitrate and Nitrite PAN Applied lbs acre) Name of Crop Type Receiving Residual Application mg/kg Crop I Crop 2 Crop 1 Crop 2 5-2008 78.3 11.5 0.758 WQ0031725 dry 0 s 0.5 0.3 18700 1660 0 9.012 NA Fescue 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 0.000 Residuals Applications totals on FORM FSF supp ( attach FORM FSF supp to this form): TOTALS: 78.3 0 As Cd Cu Cr Pb Hg Mo Ni Se Zn P 9.0121 0.000 Lime Applied lbs/acre 0.000 0.000 0.371 0.132 0.000 0.003 0.000 0.055 0.000 0.417 13.993 Date lbs/ac Annual Cumulative Ibs/ac 0 0 0 0 0 0 0 0 0 0 6-2008 2000 Prior Years Cumulative lbs/ac 0.000 d 0.000✓ 0.371 " 0.132 V 0.000.- 0.003 y 0.0001,- 0.055 v 0.000 i. 0.417✓ Current Permitted C. P. L. R.**** 36 34 1338 NA 267 15 NA 374 89 2498 Permit PAN Limit lst/2nd Crop 162 h "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure ta qualified personnel properly gathered and evaluated the information submitted. 1 am aware that there are significant penalties for submitting false information, including the ossibility of fines and imprisonment for knowing violations." Signature of Land Applier 9- /2•2LG ? Date *Application Method: S - Surface, IN - Injection, INC - Incorporation **Volatilization Rate: Surface - 0.5, Injection/Incorporation - 1.0 *** Mineralization Rates: Compost -0.1, anaerobially digested -0.2, aerobically digested -0.3, raw sludge -0.4 ****C.P.L.R.: Cumulative Pollutant Loading Rate DENR FORM FSF (12/2006) Analytical Results Southern Soil Builders 958 Hoots Road Roaring River Entered 11/20/2008 Reported: 11/25/2008 Sample Remark NC 28669 For: Baxter STATESVILLE ANALYTICAL Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 081120-3 % Solids Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NC00909 11.5 0/0 SM2540B 11/24/08 CL P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/469 7 ace Analytical www.pacelabs.com Project SLUDGE ANALYSIS Pace Project No. 9226439 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 Asheville, NC 28804 Huntersville, NC 28078 (828)254-7176 (704)875-9092 ANALYTICAL RESULTS Sample: DIGESTER SLUDGE Lab ID: 9226439001 Collected: 08/26/08 12:30 Received: 08/26/08 15:15 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 8081 GCS Pesticides, TCLP SPE Analytical Method: EPA 8081 Preparation Method: EPA 3535 gamma-BHC (Lindane) ND ug/L 0.50 1 09/03/08 00:00 09/04/08 21:24 58-89-9 Chlordane (Technical) ND ug/L 3.0 1 09/03/08 00:00 09/04/08 21:24 57-74-9 Endrin ND ug/L 0.50 1 09/03/08 00:00 09/04/08 21:24 72-20-8 Heptachlor epoxide ND ug/L 0.50 1 09/03/08 00:00 09/04/08 21:24 1024-57-3 Methoxychlor ND ug/L 1000 1 09/03/08 00:00 09/04/08 21:24 72-43-5 Toxaphene ND ug/L 3.0 1 09/03/08 00:00 09/04/08 21:24 8001-35-2 Decachlorobiphenyl (S) 79 % 10-138 1 09/03/08 00:00 09/04/08 21:24 2051-24-3 Tetrachloro-m-xylene (S) 33 % 10-110 1 09/03/08 00:00 09/04/08 21:24 877-09-8 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 2270 mg/kg 458 1 08/29/08 10:10 09/02/08 22:49 7429-90-5 Arsenic ND mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7440-38-2 Cadmium ND mg/kg 4.6 1 08/29/08 10:10 09/02/08 22:49 7440-43-9 Calcium 17800 mg/kg 458 1 08/29/08 10:10 09/02/08 22:49 7440-70-2 Chromium 87.0 mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7440-47-3 Copper 245 mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7440-50-8 Lead ND mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7439-92-1 Magnesium 3170 mg/kg 458 1 08/29/08 10:10 09/02/08 22:49 7439-95-4 Molybdenum ND mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7439-98-7 Nickel 36.2 mg/kg 22.9 1 08/29/08 10:10 09/02/08 22:49 7440-02-0 Potassium ND mg/kg 22900 1 08/29/08 10:10 09/02/08 22:49 7440-09-7 Selenium ND mg/kg 45.8 1 08/29/08 10:10 09/02/08 22:49 7782-49-2 Sodium ND mg/kg 22900 1 08/29/08 10:10 09/02/08 22:49 7440-23-5 Zinc 275 mg/kg 45.8 1 08/29/08 10:10 09/02/08 22:49 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Arsenic ND mg/L 0.025 1 09/04/08 14:27 09/05/08 12:56 7440-38-2 Banum ND mg/L 0.025 1 09/04/08 14:27 09/05/08 12:56 7440-39-3 Cadmium ND mg/L 0.0050 1 09/04/08 14:27 09/05/08 12:56 7440-43-9 Chromium ND mg/L 0.025 1 09/04/08 14:27 09/05/08 12:56 7440-47-3 Lead ND mg/L 0.025 1 09/04/08 14:27 09/05/08 12:56 7439-92-1 Selenium ND mg/L 0.050 1 09/04/08 14:27 09/05/08 12:56 7782-49-2 Silver ND mg/L 0.025 1 09/04/08 14:27 09/05/08 12:56 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Mercury ND ug/L 0.20 1 09/05/08 10:20 09/05/08 15:34 7439-97-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 2.1 mg/kg 0.22 1 08/29/08 11:40 08/30/08 10:53 7439-97-6 8270 MSSV TCLP Sep Funnel Analytical Method: EPA 8270 Preparation Method: EPA 3510 1,4-Dichlorobenzene ND ug/L 2,4-Dinitrotoluene ND ug/L Hexachloro-1,3-butadiene ND ug/L Hexachlorobenzene ND ug/L Date: 09/10/2008 05:26 PM 50.0 1 09/03/08 00:00 09/05/08 00:50 106-46-7 50.0 1 09/03/08 00:00 09/05/08 00:50 121-14-2 50.0 1 09/03/08 00:00 09/05/08 00:50 87-68-3 50.0 1 09/03/08 00:00 09/05/08 00:50 118-74-1 REPORT OF LABORATORY ANALYSIS Page 3 of 25 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ace Analytical w,vw.pacelabs.com Project SLUDGE ANALYSIS Pace Project No.: 9226439 Pace Analytical Services, Inc. 2225 Riverside Dr Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DIGESTER SLUDGE Lab ID: 9226439001 Results reported on a "dry -weight" basis Parameters Results Collected: 08/26/08 12:30 Received: 08/26/08 15:15 Matrix: Solid Units Report Limit DF Prepared Analyzed CAS No. Qual 8270 MSSV TCLP Sep Funnel Hexachloroethane 2-Methylphenol(o-Cresol) 3&4-Methylphenol(m&p Cresol) Nitrobenzene Pentachlorophenol Pyridine 2.4.5-Tnchlorophenol 2.4.6-Trichlorophenol Nitrobenzene-d5 (S) 2-Fluorobiphenyl (S) Terphenyl-d14 (S) Phenol-d6 (S) 2-Fluorophenol (S) 2.4.6-Tribromophenol (S) 8260 MSV TCLP Benzene 2-Butanone (MEK) Carbon tetrachloride Chlorobenzene Chloroform 1.4-Dichlorobenzene 1.2-Dichloroethane 1,1-Dichloroethene Tetrachloroethene Tnchloroethene Vinyl chloride 1.2-Dichloroethane-d4 (S) Toluene-d8 (S) 4-Bromofluorobenzene (S) Dibromofluoromethane (S) Percent Moisture Percent Moisture 2540G Total Percent Solids Total Solids 9045 pH Soil pH at 25 Degrees C Plant Available Nitrogen Plant Available Nitrogen Date' 09/10/2008 05:26 PM Analytical Method: EPA 8270 Preparation Method: EPA 3510 ND ug/L ND ug/L 951 ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 69 % 67 % 81 25 34 % 90 % Analytical Method: EPA 8260 ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L ND ug/L 111 % 121 % 99 ok 111 % 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 50.0 1 09/03/08 00:00 30-150 1 09/03/08 00:00 30-150 1 09/03/08 00:00 30-150 1 09/03/08 00:00 25-150 1 09/03/08 00:00 25-150 1 09/03/08 00:00 25-150 1 09/03/08 00:00 09/05/08 00:50 67-72-1 09/05/08 00:50 95-48-7 09/05/08 00:50 09/05/08 00:50 98-95-3 09/05/08 00.50 87-86-5 09/05/08 00-50 110-86-1 09/05/08 00:50 95-95-4 09/05/08 00:50 88-06-2 09/05/08 00:50 4165-60-0 09/05/08 00:50 321-60-8 09/05/08 00:50 1718-51-0 09/05/08 00:50 13127-88-3 09/05/08 00:50 367-12-4 09/05/08 00:50 118-79-6 125 25 09/07/08 11:11 71-43-2 250 25 09/07/08 11:11 78-93-3 125 25 09/07/08 11.11 56-23-5 125 25 09/07/08 11:11 108-90-7 125 25 09/07/08 11:11 67-66-3 125 25 09/07/08 11:11 106-46-7 125 25 09/07/08 11:11 107-06-2 125 25 09/07/08 11:11 75-35-4 125 25 09/07/08 11:11 127-18-4 125 25 09/07/08 11:11 79-01-6 125 25 09/07/08 11:11 75-01-4 79-120 25 09/07/08 11:11 17060-07-0 70-120 25 09/07/08 11:11 2037-26-5 S3 87-109 25 09/07/08 11:11 460-00-4 85-115 25 09/07/08 11:11 1868-53-7 Analytical Method: ASTM D2974-87 98.2 % 0.10 1 Analytical Method: SM 2540G 1.8 % 0.10 1 Analytical Method: EPA 9045 7.3 Std. Units 0.10 1 Analytical Method: 40CFR PART 503 2530 mg/kg 1.0 1 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent A�� of Pace Analytical Services, Inc.. 09/02/08 14:53 09/02/08 14:53 09/04/08 10:50 09/10/08 14:47 Page 4 of 25 ace Analytical www.pacelabs. com Project SLUDGE ANALYSIS Pace Project No.. 9226439 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: DIGESTER SLUDGE Lab ID: 9226439001 Collected: 08/26/08 12:30 Received: 08/26/08 15:15 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit. DF Prepared Analyzed CAS No. Qual Specific Oxygen Uptake Rate Oxygen, Dissolved 350.1 Ammonia Nitrogen. Ammonia 351.2 Total Kjeldahl Nitrogen Nitrogen. Kjeldahl, Total 353.2 Nitrogen, NO21NO3 Nitrogen. Nitrate Nitrogen, Nitrite Nitrogen, NO2 plus NO3 365.1 Phosphorus, Total Phosphorus 4500 Chloride in Soil Chlonde ASTM D516-90 Sulfate Soil Sulfate Analytical Method: 40CFR PART 503 1.72 mg/g/hr 0.010 1 Analytical Method: EPA 350.1 1660 mg/kg 275 1 Analytical Method: EPA 351.2 18700 mg/kg 3850 7 Analytical Method: EPA 353.2 ND mg/kg 585 1 ND mg/kg 585 1 ND mg/kg 585 1 Analytical Method: EPA 365.1 9230 mg/kg 726 7 Analytical Method: SM 4500-CI-E 12500 mg/kg 2640 1 Analytical Method: ASTM D516-90 14800 mg/kg 2750 1 08/26/08 12:20 7782-44-7 09/04/08 19:01 7764-41-7 09/06/08 15:44 7727-37-9 09/09/08 11:48 09/09/08 11:48 09/09/08 11:48 09/04/08 14:40 7723-14-0 09/10/08 13:20 16887-00-6 08/29/08 11:30 14808-79-8 Sample: DIGESTER SLUDGE (SAR) Lab ID: 9226439002 Collected: 08/26/08 12:20 Received: 08/26/08 15:15 Matrix: Water Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Calcium Magnesium Sodium Sodium Adsorption Ratio, SAR Sodium Adsorption Ratio Date 09/10/2008 05:26 PM Analytical Method: EPA 6010 Preparation Method: EPA 3010 405000 ug/L 51500 ug/L 274000 ug/L Analytical Method: EPA 6010 5000 100 250000 50 09/03/08 15:27 1 09/03/08 15:27 50 09/03/0815:27 09/05/08 12:21 09/04/08 15:48 09/05/08 12:21 3.4 meq/L 1 09/10/08 14:44 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1. IGiCLCr�: 7440-70-2 7439-95-4 7440-23-5 Page 5 of 25 Analytical Environmental Services, Inc. CLIENT: Pace Analytical Services, Inc. Client Sample ID: DIGESTER SLUDGE Project: 9226439 Collection Date: 8/26/2008 12:30:00 PM Lab ID: 0808H95-001 Matrix: SOLID Analyses Result Reporting Qual Units BatchlD Dilution Date Analyzed Limit Factor HERBICIDES, TCLP SW1311/8151A (SW3510B) Analyst: EGM 2,4,5-TP (Silvex) BRL 0.20 mg/L 103708 1 9/4/2008 3:16 PM 2.4-D BRL 0.20 mg/L 103708 1 9/4/2008 3:16 PM SUIT DCAA 103 44.7-146 %REC 103708 1 9/4/2008 3.16 PM Qualifiers: Date: 08-Sep-08 Value exceeds Maximum Contaminant Level E Estimated (Value above quantitation range) BRL Below Reporting Limit S Surrogate Recovery outside accepted recovery limns 1-1 Holding times for preparation or analysis exceeded Narr See Case Narrative N Analyte not NELAC certified NC Not Confirmed 13 Analyte detected in the associated Method Blank Page I of. I ' ANNUAL PATHOGEN AND VECTOR ATTRACTION REDUCTION FORM (02T Rules) Facility :Name: )Baxter Healthcare WQ Permit Number: W00031725 `Y WTP Name: Baxter Healthcare Monitoring Period: From 1 / I /2008 To NPUES Number: N0000656-I 12/31 /2008 'atho en Reduction (15A NCAC 02T .1106) - Please indicate level achieved and alternative performed: g Class A: Alt. A (time/temp) • Alt B (Alk Treatment) ■ 1 Alt. C (Prior Testing) ■ Alt.D (No Prior Test) • Process to Further Reduce Pathogengs • If applicable to alternative performed (Class A only) indicate "Process to Further Reduce Pathogens": Compost ■ Heat Drying • Heat Treatment • Thermophilic ■ Beta Ra\ ■ Gamma Ray ■ Pasteurization • Class B: Alt. (1) Fecal Density D Alt. (2) Process to Significantly Reduce Pathogens • If applicable to alternative performed (Class B only) indicate "Process to Significantly Reduce Pathogens": Lime Stabilization ■ Air Drying • Composting • Aerobic Digestion D Anaerobic Digestion ■ I If applicable to alternative performed (Class A or Class B) complete the following monitor'ng data: Parameter Allowable Level in Sludge Pathogen Density Number of- I.xcee- dences Frequency nt Analysis Sample -Type Analytical fech- ruut,e Minimum Geo. MeanMaximum Units Real 0olilorm 2 x 10 to the 6th power MPN 13372 16982 30303 MPN/g 0 7 grab sm922 I e per gram of total solids C Tll 1000 mpn per gram of total solid (dry weight) ;,Irnonella bacteria (in lien of fecal conform) 3 MPN per 4 grams total solid (dry weight) ctor Attraction Reduction (15A NCAC 02T .l 107) - Please indicate alternave perfo tir Alt. I ( VS reduction) D Alt. 2 (40-day bench) • Alt. 3 (30-day bench) ■ Alt. 4 (Spec. O, uptake) ■ Alt. 6 (Alk. Stabilization I Alt 7 (Drying - Stable) ■ Alt. 8 (Drying - Unstable) • Alt. 5 (I-t-Da\ Aerobic) • Alt. 10 (Incorporation) • No vector attraction reduction alternatives were performed IN Alt 9 ( Injection) • CERTIFICATION STATFMENT (please check the appropriate statement) 0 "I certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in 15A NCAC 02T .1107 have been met." ❑ "1 certify, under penalty of law, that the pathogen requirements in 15A NCAC 02T .1106 and the vector attraction reduction requirement in I5A NCAC 02T .1107 have not been met." (Please note if you check this statement attach an explanation why you have not met one or both of the requirements.) "This determination has been made under my direction and supervision in accordance with the system designed to ensure that qualified personnel properly gather and evaluate the information used to determine that the pathogen and vector attraction reduction requirements have been met. I am aware that there are significant penalties for false certification including fine and imprisonment." SILft( nl 6--o-u,(r(, Linslo,NiUa• rk.N T Prepare!. Name and Title (type or print) rF Signature of Preparer* ■ V� t^iCF-N ti6IZ J2b loC Date Dennis Key President Southern Soil Builders, Inc. )..and Applier Name and Title (if applicahle)(type or print) Signature of Land pplie r (if applicahle) 'Preparer is delined in 40 CFR Part 503.9(r) and I SA NCAC 2T .1102 (26) Date DENR FORM PVRF 02T (12/2006) .4 Analytical Results Pace Analytical 9800 Kincey Suite 100 Huntersville Entered 10/8/2008' Reported: 10/16/2008 Sample Remark NC 28078 For: 9229480 Sample ID Parameter Cust ID Result Units Method Da1te Analyzed Ain inlyst 08108-17.1 % Solids 922948001 1.69 % SM2540B '10/8/08 CIl. 08108-17.1 Fecal Coliform MTF 922948001 —17,751 MPN/g SM92210E '10/8/08 C 4. 08108-17.1 Geometric Mean 922948001 16,982 MPN/g dry wt. basis '10/9/08 (:::. 08108-17.2 % Solids 922948002 1.66 % SM2540B '10/8/08 C Il. 08108-17.2 Fecal Coliform MTF 922948002—43,855 MPN/g SM92210E '10/8/08 Cl.. 08108-17 3 % Solids 922948003 1.72 % SM2540B 'I 0/8/06 G I.. 08108-17.3 Fecal Coliform MTF 922948003 —13,372 MPN/g SM92210E "'0/8/08 CI. 08108-17,4 % Solids 922948004 1.73 % SM2540B '10/8/08 (:I. 08108-17.4 Fecal Coliform MTF 922948004—17,341 MPN/g SM92210E ' 0/8/08 Cl. 08108-17.5 % Solids 922948005 1.65 % SM2540B "0/8/08 (:1. 08108-17.5 Fecal Coliform MTF 922948005 —30,303 MPN/g SM92210E 10/8/a CI. 08108-17.6 % Solids 922948006 1.69 % SM2540B 10/8/08 CI. 08108-17.6 Fecal Coliform MTF 922948006 —13,609 MPN/g SM92210E 10/8/08 CI. 08108-17.7 % Solids 922948007 1.72 % SM2540B 10/8/08 Cl,. 08108-17.7 Fecal Coliform MTF 922948007 . 17,442 MPN/g SM92210E 10/8/08 C:1. Respectfully submitted, ,OuvA Dena Myers NC Cert #440, NCDW Cert #37755, EPA NC00909 P.Q. Box 228 • Statesville, North Carol, na 28687 4 04/872/469)7 1 Analytical Results Pace Analytical 9800 Kincey Suite 100 Huntersville Entered 8/27/2008 Reported: 9/3/2008 Sample Remark NC 28078 For: 9226439 STATESVILLE ANALYTICAL Sample ID Parameter Cust ID Result Units Method Date Analyzed Analyst 080827-1 % Solids 9226439001 1.69 % SM2540B 8/27/08 CL 080827-1 Fecal Coliform MTF 9226439001 53,254 MPN/g SM92210E 8/27/08 CL Respectfully submitted, Dena Myers NC Cert #440, NCDW Cert #37755, EPA NC0O909 P.O. Box 228 • Statesville, North Carolina 28687 • 704/872/4697 Analytical Results Pace Analytical 9800 Kincey Suite 100 Huntersville Entered 11/11/2008 Reported: 11/14/2008 Sample Remark NC 28078 For: 9231693 Sample ID Parameter Cust ID Result Units Method Dante Analyzed AtInlyst 081111-2.1 VSS 081111-2.2 VSS Respectfully submitted, kOzA Dena Myers NC Cert #440, NCDW Cert #37755, EPA NC00909 9231693003 3360 mg/L SM2540G 11/13/08 9231693004 12200 mg/L SM2540G 11/13/08 P.O. Box 228 • Statesville, North Carolina 28687 ':04/872/4697 Re ort No• 14S76 NCDA&CS Agronomic Division Phone: (919) 15.5-'Lb55 WCD �rte: www.ncagr.cuuvngl vuvuui P Grou 'r Southern Soil Builders, Inc. 958 !loots Rd Roaring River, NC 28669 Farm: Catawba County Copies To: 4 O A 4 , ' N s • � � r Soil , ... ro ;.rF.y�S ink '0 • ' 1.I/19/2008 . , 1',RUING 0 Report • Agronomist Comments C -- 12, $ Field Information Applied Lime Recommendations Sample No. Last Crop T1 Mo Yr T/A 6 2008 1.0 Crop or Year 1st Crop: Fes/OG/fim,M 2nd Crop: Lime .6T N P205 K20 120-200 50-70 40-60 Mg S 0 0 0 Cu 0 Zn 0 B .0 Mn 0 See Note 12 Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K-I MIN 1.14 0.98 8.9 73.0 2.4 5.4 34 43 Ca% Mg% 52.0 19.0 Mn-I Mn-AI(1)Mn-AI(2) Zn-I 63 55 200 Zn-AI 200 Cu=/ 159 S-1 51 SS -I NO3-N NH4-N Na 0.1 Field Information Applied Lime Recommendations . Sample No. Last Crop T2 Mo Yr TIA 6 2008 1.0 Crop or Year 1st Crop: Fes/OG/Tim,M 2nd Crop: Lime 0 N P205 K20 120-200 60-80 50-70 Mg S 0 0 0 Cu 0 Zn 0 B .0 Mn 0 See Note 12 Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K-1 MIN 1.19 1.08 6.7 75.0 1.7 5.5 27 38 Ca% Mg% 52.0 20.0 Mn-I Mn-AI(1)Mn-AI(2) Zn-1 61 61 117 Zn-AI 117 Cu-I 98 . - S-I 44 SS -I NO3-N NH4-N Na 0.1 Field Information . Applied Lime Recommendations Sample No. Last Crop Si Mo Yr TIA 6 2008 1.0 Crop or Year 1st Crop: Fes/OG/1'im,M 2nd Crop: Lime 0 N P205 K20 120-200 40-60 40-60 Mg S 0 0 0 Cu 0 Zn 0 B .0 Mn pli$ See Note 12 Test Results Soil Class HM% W/V CEC BS% Ac pH P-I K-I MIN 0.66 1.15 7.1 90.0 0.7 6.5 36 45 Ca% Mg% 54.0 33.0 Mn-I Mn-AI(1)Mn-A/(2) Zn-I 99 69 32 Zn-AI 32 Cu-I 102 - S-I 28 SS -I NO3-N NH4-N Na 0.1 Field Information Applied Lime Recommendations Sample No. Last Crop 52 Mo Yr TIA 6 2008 1.0 Crop or Year 1st Crop: Fes/OG/I'im,M 211d Crop: Lime .4T N P205 K20 120-200 20-40 0 Mg S 0 0 0 Cu 0 Zn 0 B .0 Mn 0 See Note 12 Test Results Soil Class HM% W/V CEC BS% Ac pH P-1 K-1 MIN 0.51 1.15 6.i 72.0 1.8 5.3 46 87 Ca% Mg% 41.0 24.0 Mn-I Mn-AI(1)Mn-AI(2) Zn-I 177 123 44 Zn-Al 44 Cu-I 124 , S-/ 34 SS -I NO3-N NH4-N Na 0.0