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Home My WebLink AboutWQ0010689_Annual Report_20130228Section 1 Form DMSDF RECEIVE MAR a6 0y Asheville Regional Office A .. Class A Annual Distribution and Marketing Surface Disposal Certification and Summary Form and Supplemental Information RECEIVENDENR/M FEB 2 8 2013 Aquifer Protection Section CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare Corporation North Cove Steam Generation Plant Ash PHONE: 828-756-6809 COUNTY: McDowell OPERATOR: Baxter Healthcare" FACILITY TYPE (please check one): ® Surface Disposal (complete Part A (Source(s) and "Residual In" Volume only) and Part C) R1 Distribution and Marketing (complete Parts A, B, and C) Was the facility in operation during the past calendar year? Yes R1 No ® —0� If No skip parts A, B, C and certify form below Part A*: Part B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information. Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) January See DMSDF sheet February supplemental for March breakdown April May June July August September October November December Total from FORM DMSDF (sup) _ 153.75 77188 927.63, 927.0 Totals: Annual (dry tons): 153.75 773.88 927.63' 927.63 Amendment(s) used: Bulking Agent(s) used: * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 Part C: Facility was compliant during the past calendar year with all conditions of the land application permit F0 Yes (including but not limited to items 1-3 below) issued by the Division of Water Quality: 13 No ► If No, Explain in Narritive 1. All monitoring was done in accordance with the permit and reported for the year as required and three (3) copies of certified laboratory results are attached. 2. All operation and maintenance requirements were compiled with or, in the case of a deviation, prior authorization was received from the Division of Water Quality. 3. No contravention of Ground Water Quality Standards occurred at a monitoring well. "I certify, under penalty of law, that the above information is, to the best of my knowledge and belief, true, accurate and complete. I am aware that there are ignicar penalties'for submitting false information, including the possibility of fines and imprisonment for knowing violations." ^ I A��n� - Signature of Permittee V Date **Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) Signature of Preparer** (if different from Permittee) RECEIVEDIDENR M FEB 2 8 2013 ione,i office ��vilie � �g otectt� AgWerProtedonSedon DENR FORM DMSDF (12/2006) CLASS A ANNUAL DISTRIBUTION AND MARKETING/ SURFACE DISPOSAL CERTIFICATION AND SUMMARY FORM Supplemental Information WQ PERMIT #: WQ0010689 FACILITY NAME: Baxter Healthcare' Corporation NorthCove Steam Generation Plant _Ash PHONE: 828-756-6809 COUNTY: :McDowell OPERATOR: Baxter Healthcare FACILITY TYPE (please check one): [3 Surface Disposal (complete Part A - "Month", "Source(s)" and "Residual In" columns only) RI Distribution and Marketing (complete Parts A, and B) Part A*: Part_B*: Month Sources(s) (include NPDES # if applicable) Volume (dry tons) Recipient Information Amendment/ Bulking Agent Residual In Product Out Name(s) Volume (dry tons) Intended use(s) March WQ0010689 2.08 9.44 11.52 Dean McClure 11.52 Land Application March WQ0010689 3.12 14.16 17.28 Bobby Boone 17.28 Land Application March WQ0010689 3.12 14.16 17.28 Dean McClure. 17.28 Land Application March WQ0010689 13.85 62.95 76.80 Bobby Boone 76.8 Land Application March WQ0010689 6.58 29.90 36.48 Bobby Boone 36.48 Land Application March WQ0010689 3.12 14.16 17.28 Dean McClure 17.28 Land Application April WQ0010689 6.23 28.33 34.56 Bobby Boone 34.56 Land Application April WQ0010689 4.15 18.89 23.04 Bobby Boone 23.04 Land Application April WQ0010689 6.23 28.33 34.56 Bobby Boone 34.56 Land Application April WQ0010689 1.04 4.72 5.76 James Barlowe 5.76 Land Application July WQ0010689 28.66 150.86 179.52 Kenneth Hughes 179.52 Land Application July WQ0010689 22.79 120.01 142.80 Jim Phillips 142.8 Land Application December WQ0010689 1.96 10.29 12.25 Bobby Boone 12.25 Land Application December WQ0010689 17.60 92.65 110.25 Jim Phillips 110.25 Land Application December WQ0010689 33.24 175..01 208.25 Max Holland 208.25 Land Application Totals: Annual (dry tons): 153.75 773.88 .................................... 927.63 927:63 ...................,... Amendment(s) used: I Bulking Agent(s) used: D Wood Chips * If more space is required, attach additional information sheets (FORM DMSDF (supp)): Total Number of Form DMSDF (Supp)l 1 DENR FORM DMSDF (Supp) (12/2006) Section 2,Form RSSF Annual Residual Sampling Summary Form and Form B ANNUAL RESIDUAL SAMPLING SUMMARY FORM ` Please note that your permit may contain additional parameters to be analyzed. The parameters can be reported in FORM RSSF - B WQ Permit Number: WQ0010689 Laboratory: Baxter Healthcare Corporation North Cove Facility Name: Steam Generation Plant Ash Residual Source WQ # or WQ0010689 NPDES #: WWTP Name: NA Recidunl Annlvcic Dgtn 1) Pace Analytical Services 2) 3) 4) 5) Parameter (mg/kg) Conc. Limit m a Sample or Composite Date 1NP22812 2NP22812 WBSP52512 WBNPOCT17 Percent Solids (%) NA Arsenic . 75 14.5 12.8 10.1 6.7 Cadmium 85 2.1 4.8 2 1.9 Copper 4,300 103 130 82.4 90.3 Chromium NA 23.4 20.3 22.1 23.6 Lead 840 18.5 16 18.9 18.4 Mercury 57 0.012 0.012 0.01 ND Molybdenum 75 ND 1.1 1.2 1.5 Nickel 420 15.9 13.5 13.7 29.3 Selenium 100 ND ND ND ND Zinc y 7,500 232 190 195 160 Total PhosphorusV NA 2710 2660 2680 3370 Barium NA 1650 1470 1340 1670 Calcium NA 78200 67500 76300 90100 Iron V NA 13700 11800 9130_ 23900 ror surrace aisposai racnities the ceiling concentration limits listed in this form are not applicable. Reference the individual permit for metals limits. "I certify, under penalty of law, that this document was prepared under my direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted: I am aware that there are significant penalties for asubmitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * o2-- 2-ce— le Date *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) DENR FORM RSSF (12/2006) ANNUAL RESIDUAL SAMPLING SUMMARY FORM - B Report all sampling analysis results for parameters not listed in FORM RSSF that are part of the WQ permit or were analyzed for over the past calendar year. Use additional forms as needed. WQ Permit Number: Facility Name: Residual Source NPDES # or WQ#: WWTP Name: Residual Analvsis Data WQ0010689 Baxter Healthcare Corporation North Cove Steam Generation Plant Ash WQ0010689 NA Laboratory: 1) Pace Analytical Services 2) 3) 4) 5) Parameter (mg/kg) Sample or Composite Date 1NP22812 2NP22812 WBSP52512 WBNPOCT17 Magnesium 14700 12700 9780 11900 Manganese 2720 2330 2410 2870 pH 9 9 8.7 9 Potassium 15500 14300 16900 16800 Silver o/ ND ND 1.1 ND Sodium ND 7000 8580 6070 "I certify, under penalty of law, that this document was prepared under my'direction or supervision in accordance with a system designed to assure that qualified personnel properly gathered and evaluated the information submitted. I am aware that there are significant penalties for submitting false information, including the possibility of fines and imprisonment for knowing violations." Signature of Preparer * (/ *Preparer is defined in 40 CFR Part 503.9(r) and 15A NCAC 2T .1102 (26) 6z— 24-(3 Date DENR FORM RSSF - B (12/2006) IN Section 3 Lab Sheets Sample 1- 1NP22812 February 28, 2012 AxAnaljdicalo mmpacelabs.com Project: , WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 1NP22812 Lab ID: 92112998002 Collected: 02/28/1210:35 Received: 02/28/12 13:24 Matrix: Solid Results reported on a "dry -weight' basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 17500 mg/kg 169 10 03/01/12 14:20 03/02/12 16:26 7429-90-5 Arsenic ✓14.5 mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7440-38-2 Barium 1650 mg/kg 8.4 10 03/01/12 14:20 03/02/12 16:26 7440-39-3 Cadmium ✓2.1 mg/kg 0.17 1 03/01/12 14:20 03/02/12 15:46 7440-43-9 Calcium 78200 mg/kg 169 10 03/01/12 14:20 03102/1216:26 7440-70-2 Chromium 23.4 mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7440-47-3 Copper 1-103 mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7440-50-8 Iron 13700 mg/kg 169 10 03/01/12 14:20 03/02/12 16:26 7439-89-6 Lead 08.5 mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7439-92-1 Magnesium 14700 mg/kg 169 10 03/01/12 14:20 03/02/12 16:26 7439-95-4 Manganese 2720 mg/kg 8.4 10 03/01/12 14:20 03/02/12 16:26 7439-96-5 Molybdenum AND mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7439-98-7 Nickel ✓15.9 mg/kg 0.84 1 03/01/12 14:20 03/02/12 15:46 7440-02-0 Potassium 15�5/000 mg/kg 8430 10 03/01/12 14:20 03/02/12 16:26 7440-09-7 Selenium LAND mg/kg 1.7 1 03/01/12 14:20 03/02/12 15:46 7782-49-2 Silver ND mg/kg 8.4 10 03/01/12 14:20 03/0211216:26 7440-22-4 Sodium ND mg/kg 8430 10 03/01/12 14:20 03/02/12 16:26 7440-23-5 Zinc (/232 mg/kg 1.7 1 03/01/12 14:20 03/02/12 15:46 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 03/02/12 17:15 Arsenic ND mg/L 0.025 1 03/05/12 10:55 03/06/12 13:51 7440-38-2 Barium 4.9 mg/L 0.50 1 03/05/12 10:55 03/06/12 13:51 7440-39-3 Cadmium 0.023 mg/L 0.0050 1 03/05/12 10:55 03/06/12 13:51 7440-43-9 Chromium 0.056 mg/L 0.025 1 03/05/12 10:55 03/06/12 13:51 7440-47-3 Lead 0.027 mg/L 0.025 1 03/05/12 10:55 03/06/12 13:51 7439-92-1 Selenium ND mg/L 0.10 1 03/05/12 10:55 03/06/12 13:51 7782-49-2 Silver ND mg/L 0.025 1 03/05/12 10:55 03/06/12 13:51 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA7470 Preparation Method: EPA7470 Leachate Method/Date: EPA 1311; 03/02/12 17:15 Mercury ND ug/L 0.20 1 03/05/12 12:35 03/06/12 10:58 7439-97-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury V0.012 mg/kg 0.0090 1 03/01/12 09:25 03/02/12 14:38 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 49.7 % 0.10 1 03/02/12 13:30 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 9.0 Std. Units 0.10 1 03/05/12 13:00 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 2710 mg/kg 174 50 03/12/12 16:31 7723-14-0 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, withoutthe written consent of Pace Analytical Services, Inc.. Page 6 of 18 1 . ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalytical 205 East Meadow Road - Suite 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www.pacelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: WOOD BOILER 2/28 Pace Project No.: 92112998 QC Batch: MERP14074 Analysis Method: EPA7471 QC Batch Method: EPA7471 Analysis Description: 7471 Mercury Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 728414 Matrix: Solid Associated Lab Samples: 92112998001, 92112998002, 92112998003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg ND 0.0050 03/01/1215:18 LABORATORY CONTROL SAMPLE: 728415 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg .067 0.061 92 80-120 MATRIX SPIKE SAMPLE: 728416 92112995006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury 'mg/kg 7.5 .061 9.0 2480 75-125 M6 MATRIX SPIKE SAMPLE: 728418 92112898003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.016 .072 0.074 81 75-125 SAMPLE DUPLICATE: 728417 92112728001 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg 0.0088 .0041 SAMPLE DUPLICATE: 728419 92112898004 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg 0.017 0.015 - 11 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 9 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. I )V?l 0 rac6Ana1Xica1 www.pacelabsxom Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Project: WOOD BOILER 2/28 Pace Project No.: 92112998 QC Batch: MPRP/10008 Analysis Method: EPA6010 QC Batch Method: EPA3050 Analysis Description: 6010 MET Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 729151 Matrix: Solid Associated Lab Samples: 92112998001, 92112998002, 92112998003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Aluminum mg/kg ND 10.0 03/02/1214:53 Arsenic mg/kg ND 0.50 03102/1214:53 Barium mg/kg ND 0.50 03/02/1214:53 Cadmium mg/kg ND 0.10 03102/1214:53 Chromium mg/kg ND 0.50 03/02/1214:53 Copper mg/kg ND 0.50 03/02/1214:53 Lead mg/kg ND 0.50 03/02/1214:53 Molybdenum mg/kg ND 0.50 03102/1214:53 Nickel mg/kg ND 0.50 03102/1214:53 Potassium mg/kg ND 500 03/02/1214:53 Selenium mg/kg ND 1.0 03/02/1214:53 Silver mg/kg ND 0.50 03/02/1214:53 Zinc mg/kg ND 1.0 03/02/1214:53 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 729152 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Aluminum mg/kg 500 509 102 80-120 Arsenic mg/kg 50 50.5 101 80-120 Barium mg/kg 50 50.6 101 80-120 Cadmium mg/kg 50 50.9 102 80-120 Chromium mg/kg 50 49.9 100 80-120 Copper mg/kg 50 50.5 101 80-120 Lead mg/kg 50 50.9 102 80-120 Molybdenum mg/kg 50 53.3 107 80-120 Nickel mg/kg 50 50.6 101 80-120 Potassium mg/kg 500 4871 97 80-120 Selenium mg/kg 50 49.6 99 80-120 Silver mg/kg 25 25.9 104 80-120 Zinc mg/kg 50 50.8 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 729153 729154 MS MSD 92112847005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Aluminum mg/kg 6880 462 470 7910 8400 224 324 75-125 6 J(M1) Arsenic mg/kg 0.76 46.2 47 45.6 47.4 97 99 75-125 4 Barium mg/kg 89.0 46.2 47 134 146 97 121 75-125 9 Cadmium mg/kg 0.31 46.2 47 42.8 43.8 92 93 75-125 2 Chromium mg/kg 8.8 46.2 47 50.2 52.6 90 93 75-125 5 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 10 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc aceAnalytical wvnvpacefabs.com Project: WOOD BOILER 2128 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 (QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 729153 729154 MS MSD 92112847005 Spike Spike MS MSD MS MSD % Rec - Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Copper mg/kg 32.4 46.2 47 80.5 110 104 165 75-125 31 J(D6),J(M1) Lead mg/kg 2.4 46.2 47 43.4 44.6 89 90 75-125 3 Molybdenum mg/kg 0.39 46.2 47 44.7 46.1 96 97 75-125 3 Nickel mg/kg 5.9 46.2 47 47.7 49.8 91 93 75-125 4 Potassium mg/kg 4220 462 470 4680 5250 99 219 75-125 12 J(M1) Selenium mg/kg ND 46.2 47 45.8 47.8 99 101 75-125 4 Silver mg/kg ND 23 23.5 23.5 24.3 102 103 75-125 3 Zinc mg/kg 47.1 46.2 47 . 89.3 110 91 134 75-125 21 J(D6),J(M1) Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 11 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. �aceAnalytkal www..pacelabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA QC Batch: PMST/4528 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92112998001, 92112998002, 92112998003 SAMPLE DUPLICATE: 728947 3560883001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 22.0 21.6 2 SAMPLE DUPLICATE: 729089 Parameter Percent Moisture 92113134002 Dup Units Result Result % 21.7 21.6 RPD Qualifiers 0 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 14 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. IeAnalydical www.pacelabs,com I Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET/19962 Analysis Method: EPA 9045 QC Batch Method: EPA 9045 Analysis Description: 9045 pH Associated Lab Samples: 92112998001, 92112998002, 92112998003 SAMPLE DUPLICATE: 730473 Parameter pH at 25 Degrees C 92112744001 Dup Units Result Result Std. Units 6.6 6.6 RPD Qualifiers 0 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 15 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnalXical 205 East Meadow Road -Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 www..ppdelabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: WOOD BOILER 2/28 Pace Project No.: 92112998 QC Batch: WETA/11711 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 733467 Matrix: Solid Associated Lab Samples: 92112998001, 92112998002, 92112998003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/kg ND 2.0 03/12/1216:11 LABORATORY CONTROL SAMPLE: 733468 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mg/kg 50 49.8 100 90-110 MATRIX SPIKE SAMPLE: 733469 92112998001 Spike MS MS % Rec Parameter Units Result Cone. Result % Rec Limits Qualifiers Phosphorus mg/kg 967 45.6 987 43 90-110 M6 SAMPLE DUPLICATE: 733470 92112998002 Dup Parameter Units Result Result RPD Qualifiers Phosphorus mg/kg 2710 2730 1 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 16 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalytical www.pacelabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. MDL -Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. J(M1) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 17 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aseAnal dical mmpacelabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification #: 37706 North Carolina Field Services Certification #: 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification #: 99006001 South Carolina Drinking Water Cert. #: 99006003 Virginia Drinking Water Certification #: 00213 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification M E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification M 37712 North Carolina Wastewater Certification #: 40 Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Connecticut Certification #: PH-0104 Florida/NELAP Certification #: E87627 Kentucky UST Certification #: 84 Louisiana DHH Drinking Water # LA 100031 West Virginia Certification #: 357 Virginia/VELAP Certification #: 460144 South Carolina Certification #: 99030001 Virginia Certification #: 00072 West Virginia Certification #: 356 Virgina/VELAP Certification #: 460147 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Page 3 of 18 Section 3 Lab Sheets Sample 2 — 2NP22812 February 28, 2012 aceAnalytical www.pacelabs,com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: 2NP22812 Lab ID: 92112998003 Collected: 02/28/12 10:35 Received: 02/28/12 13:24 Matrix: Solid Results reported on a "dry -weight' basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Aluminum 14900 mg/kg 138 10 03101/1214:20 03/02/12 16:29 7429-90-5 Arsenic V'12.8 mg/kg 0.69 1 03/01/12 14:20 03/02/12 15:53 7440-38-2 Barium 1470 mg/kg 6.9 10 03/01/12 14:20 03/02/12 16:29 7440-39-3 Cadmium &-/1.8 mg/kg 0.14 1 03/01/12 14:20 03/02/12 15:53 7440-43-9 Calcium 67500 mg/kg 138 10 03/01/12 14:20 03/02/12 16:29 7440-70-2 Chromium 20.3 mg/kg 0.69 1 03/01/12 14:20 03/02/12 15:53 7440-47-3 Copper ✓130 mg/kg 0.69 1 03/01/12 14:20 03/02/12 15:53 7440-50-8 Iron 11800 mg/kg 138 10 03101/1214:20 03/02/12 16:29 7439-89-6 Lead L-46.0 mg/kg 0.69 1 03/01/12 14:20 03/02/12 15:53 7439-92-1 Magnesium 12700 mg/kg 138 10 03/01/12 14:20 03/02/12 16:29 7439-95-4 Manganese 2330 mg/kg 6.9 10 03/01/12 14:20 03/02/12 16:29 7439-96-5. Molybdenum 0.1 mg/kg 0.69 1 03/01/12 14:20 03102/1215:53 7439-98-7 Nickel v13.5 mg/kg 0.69 1 03/01/12 14:20 03/02/12 15:53 7440-02-0 Potassium 14300 mg/kg 6910 10 03/01/12 14:20 03/02/12 16:29 7440-09-7 Selenium v ND mg/kg 1.4 1 03/01/12 14:20 03/02/12 15:53 7782-49-2 Silver ND.mg/kg 6.9 10 03/01/12 14:20 03/02/12 16:29 7440-22-4 Sodium 7000 mg/kg 6910 10 03/0111214:20 03/02/12 16:29 7440-23-5 Zinc --'190 mg/kg 1.4 1 03/01/12 14:20 03/0211215:53 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA3010 Leachate Method/Date: EPA 1311; 03/02/12 17:15 Arsenic ND mg/L 0.025 1 03/05/12 10:55 03/06/12 13:55 7440-38-2 Barium 5.1 mg/L 0.50 1 03105/1210:55 03/0611213:55 7440-39-3 Cadmium 0.023 mg/L 0.0050 1 03/05/12 10:55 03/06/12 13:55 7440-43-9 Chromium 0.027 mg/L 0.025 1 03/05/12 10:55 03/06/12 13:55 7440-47-3 Lead ND mg/L 0.025 1 03/05/12 10:55 03/06/12 13:55 7439-92-1 Selenium ND mg/L 0.10 1 03105/1210:55 03/06/12 13:55 7782-49-2 Silver ND mg/L 0.025 1 03/0511210:55 03/06/12 13:55 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA7470 Preparation Method: EPA7470 Leachate Method/Date: EPA 1311; 03/02/12 17:15 Mercury ND ug/L 0.20 1 03/05/12 12:35 03/06/12 11:09 7439-97-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury V10.012 mg/kg 0.0077 1 03/01/12 09:25 03/02/12 14:40 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 44.3 % 0.10 1 03/02/12 13:30 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 9.0 Std. Units 0.10 1 03/05/12 13:00 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 2660 mg/kg 176 50 03/12/12 16:32 7723-14-0 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 7 of 18 �aceAnaIXical0 mmoace..fabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MERP/4074 Analysis Method: EPA 7471 QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 728414 Matrix: Solid Associated Lab Samples: 92112998001, 92112998002, 92112998003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Mercury mg/kg ND 0.0050 03/01/1215:18 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 728415 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Mercury mg/kg .067 0.061 92 80-120 MATRIX SPIKE SAMPLE: 728416 92112995006 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury mg/kg 7.5 .061 9.0 2480 75-125 M6 MATRIX SPIKE SAMPLE: 728418 92112898003 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.016 .072 0.074 81 75-125 SAMPLE DUPLICATE: 728417 92112728001 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg 0.0088 .0041 SAMPLE DUPLICATE: 728419 92112898004 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg 0.017 0.015 11 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 9 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. vceAnalXical o wvnvpacelabs.cam Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MPRP/10008 Analysis Method: EPA 6010 QC Batch Method: EPA3050 Analysis Description: 6010 MET Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 729151 Associated Lab Samples: Parameter Matrix: 92112998001, 92112998002, 92112998003 Blank Units Result Solid Reporting Limit Analyzed Qualifiers Aluminum mg/kg ND 10.0 03/02/1214:53 Arsenic mg/kg ND 0.50 03/02/1214:53 Barium mg/kg ND 0.50 03/02/1214:53 Cadmium mg/kg ND 0.10 03/02/1214:53 Chromium mg/kg ND 0.50 03/02/1214:53 Copper mg/kg ND 0.50 03/02/1214:53 Lead mg/kg ND 0.50 03/02/1214:53 Molybdenum mg/kg ND 0.50 03/02/1214:53 Nickel mg/kg ND 0.50 03/02/1214:53 Potassium mg/kg ND 500 03102/1214:53 Selenium mg/kg ND 1.0 03/02/1214:53 Silver mg/kg ND 0.50 03/0211214:53 Zinc mg/kg ND 1.0 03/02/1214:53 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 729152 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Aluminum mg/kg 500 509 102 80-120 Arsenic mg/kg 50 50.5 101 80-120 Barium mg/kg 50 50.6 101 80-120 Cadmium mg/kg 50 50.9 102 80-120 Chromium mg/kg 50 49.9 100 80-120 Copper mg/kg 50 50.5 101 80-120 Lead mg/kg 50 50.9 102 80-120 Molybdenum mg/kg 50 53.3 107 80-120 Nickel mg/kg 50 50.6 101 80-120 Potassium mg/kg 500 4871 97 80-120 Selenium mg/kg 50 49.6 99 80-120 Silver mg/kg 25 25.9 104 80-120 Zinc mg/kg 50 50.8 102 80-120 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 729153 729154 MS MSD 92112847005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qua[ Aluminum mg/kg 6880 462 470 7910 8400 224 324 75-125 6 J(M1) Arsenic mg/kg 0.76 46.2 47 45.6 47.4 97 99 75-125 4 Barium mg/kg 89.0 46.2 47 134 146 97 121 75-125 9 Cadmium mg/kg 0.31 46.2 47 42.8 43.8 92 93 75-125 2 Chromium mg/kg 8.8 46.2 47 50.2 52.6 90 93 75-125 5 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 10 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc c6Ana1j&a1 wvm.pacelabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 729153 729154 MS MSD 92112847005 Spike Spike MS MSD MS MSD % Rec Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual Copper mg/kg 32.4 46.2 47 80.5 110 104 165 75-125 31 J(D6),J(M1) Lead , mg/kg 2.4 46.2 47 43.4 44.6 89 90 75-125 3 Molybdenum mg/kg 0.39 46.2 47 44.7 46.1 96 97 75-125 3 Nickel mg/kg 5.9 46.2 47 47.7 49.8 91 93 75-125 4 Potassium mg/kg 4220 462 470 4680 5250 99 219 75-125 12 J(MI) Selenium mg/kg ND 46.2 47 45.8 47.8 99 101 75-125 4 Silver mg/kg ND 23 23.5 23.5 24.3 102 103 75-125 3 Zinc mg/kg 47.1 46.2 47 89.3 110 91 134 75-125 21 J(D6),J(M1) Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 11 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc. �aceAnalytical wvtivpacelabs.com Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: PMST/4528 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92112998001, 92112998002, 92112998003 SAMPLE DUPLICATE: 728947 3550883001 Dup Parameter Units Result Result RPD Qualifiers Percent Moisture % 22.0 21.6 2 SAMPLE DUPLICATE: 729089 92113134002 Dup Parameter Units Result Result Percent Moisture % 21.7 21.6 RPD Qualifiers 0 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 14 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. _-4aceAna1j&a1 wwwpac91abscam Project: WOOD BOILER 2/28 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET/19962 Analysis Method: EPA 9045 QC Batch Method: EPA 9045 Analysis Description: 9045 pH Associated Lab Samples: 92112998001, 92112998002, 92112998003 SAMPLE DUPLICATE: 730473 Parameter pH at 25 Degrees C 92112744001 Dup Units Result Result Std. Units 6.6 6.6 RPD Qualifiers 0 Pace Analytical Services, Inc. 9800 KinceyAve Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 15 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. acter Analytical ( www.pacelabs.com 1 Project: WOOD BOILER 2128 Pace Project No.: 92112998 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/11711 Analysis Method: , EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92112998001, 92112998002, 92112998003 METHOD BLANK: 733467 Matrix: Solid Associated Lab Samples: 92112998001, 92112998002, 92112998003 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/kg ND 2.0 03/12/1216:11 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: 733468 Spike LCS LCS % Rec Parameter Units Cone. Result % Rec Limits Qualifiers Phosphorus mg/kg 50 49.8 100 90-110 MATRIX SPIKE SAMPLE: 733469 92112998001 Spike MS MS % Rec Parameter Units Result Cone. - Result % Rec Limits Qualifiers Phosphorus mg/kg 967 45.6 987 43 90-110 M6 SAMPLE DUPLICATE: 733470 92112998002 Dup Parameter Units Result Result RPD Qualifiers Phosphorus mg/kg 2710 2730 1 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 16 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ac6Ana1ytica1 ( www.pacelabs.cam Project: WOOD BOILER 2/28 Pace Project No.: 92112998 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. MDL-Adjusted Method Detection Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TN - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PASI-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS I The reported value is between the laboratory method detection limit and the laboratory practical quantitation limit. J(D6) Estimated Value. The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. i(MI) Estimated Value. Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. (704)875-9092 Date: 04/19/2012 05:19 PM REPORT OF LABORATORY ANALYSIS Page 17 of 18 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Section 3 Lab Sheets Sample 3 — WBSP52512 May 25, 2012 aC6Ana1j cal www.pacelabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. 205 East Meadow Road -Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 ANALYTICAL RESULTS Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: WBSPS2512 Lab ID: 92119396001 Collected: 05/25/12 08:45 Received: 05/25/12 10:09 Matrix: Solid Results reported on a "dry-weight"basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050 Arsenic L40.1 mg/kg 0.74 1 05/26/12 14:00 05/2911216:50 7440-38-2 Barium 1340 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7440-39-3 Cadmium ".0 mg/kg 0.15 1 05/26/12 14:00 05/29/12 16:50 7440-43-9 Calcium 76300 mg/kg 149 10 05/26/12 14:00 05/30/12 13:01 7440-70-2 Chromium 22.1 mg/kg 0.74 1 05/26/12 14:00 06/29/1216:50 7440-47-3 Copper �1182.4 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7440-50-8 Iron 9130 mg/kg 14.9 1 05/26/12 14:00 05/29/12 16:50 7439-89-6 Lead N8.9 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7439-92-1 Magnesium 9780 mg/kg 14.9 1 05/26/12 14:00 05/29/12 16:50 7439-95-4 Manganese 2410 mg/kg 7.4 10 05/26/12 14:00 05/30/12 13:01 7439-96-5 Molybdenum V1.2 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7439-98-7 Nickel v13.7 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7440-02-0 Potassium 16900 mg/kg 7430 10 05/26/12 14:00 05/30/12 13:01 7440-09-7 Selenium AID mg/kg 1.5 1 05/2611214:00 05/29/12 16:50 7782-49-2 Silver 1.1 mg/kg 0.74 1 05/26/12 14:00 05/29/12 16:50 7440-22-4 Sodium 8580 mg/kg 743 1 05/26/12 14:00 05/29/12 16:50 7440-23-5 Zinc IA95 mg/kg 1.5 1 05/2611214:00 05/29/12 16:50 7440-66-6 6010 MET ICP, TCLP Analytical Method: EPA 6010 Preparation Method: EPA 3010 Leachate Method/Date: EPA 1311; 06/06/12 16:20 Arsenic 0.069 mg/L 0.025 1 06/07/12 14:40 06/08/12 13:32 7440-38-2 Barium 4.9 mg/L 0.50 1 06/07/12 14:40 06/08/12 13:32 7440-39-3 Cadmium ND mg/L 0.0050 1 06/0711214:40 06/08/12 13:32 7440-43-9 Chromium ND mg/L 0.025 1 06/0711214:40 06108/1213:32 7440-47-3 Lead ND mg/L 0.025 1 06/07/12 14:40 06108/1213:32 7439-92-1 Selenium' ND mg/L 0.10 1 06/07/12 14:40 06/08/12 13:32 7782-49-2 Silver ND mg/L 0.025 1 06/07/12 14:40 06108/1213:32 7440-22-4 7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470 Leachate Method/Date: EPA 1311; 06/06/12 16:20 Mercury ND ug/L 0.20 1 06/08/1211:15 06/08/12 14:27 7439-97-6 7471 Mercury Analytical Method: EPA 7471 Preparation Method: EPA 7471 Mercury 1*"^ 0.010 mg/kg 0.0056 1 05/30/12 11:40 05/30/12 14:17 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 48.2 % 0.10 1 05/29/12 15:24 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 8.7 Std. Units 0.101 05/31/12 10:00 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 2680 mg/kg 179 25 06/12/12 10:41 7723-14-0 Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 4 of 15 aceAnal0cal ® www.pacelabq.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QC Batch: MERP/4255 QC Batch Method: EPA 7471 Associated Lab Samples: 92119396001 METHOD BLANK: 769960 Associated Lab Samples: 92119396001 Parameter Units Mercury mg/kg LABORATORY CONTROL SAMPLE: 769961 Parameter Units Mercury mg/kg MATRIX SPIKE SAMPLE: 769962 Parameter Units Mercury mg/kg QUALITY CONTROL DATA Analysis Method: EPA 7471 Analysis Description: 7471 Mercury Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 0.0050 05/30/1213:27 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers .067 0.057 85 80-120 92119402001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers 0.0076 .051 0.047 77 75-125 SAMPLE DUPLICATE: 769963 92119402002 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg 0.065 0.085 27 D6 Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS Page 6 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnatytical www.pacalabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA QC Batch: MPRP/10685 Analysis Method: EPA 6010 QC Batch Method: EPA3050 Analysis Description: 6010 MET Associated Lab Samples: 92119396001 METHOD BLANK: 769532 Associated Lab Samples: Parameter 92119396001 Units Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers Arsenic mg/kg ND 0.50 05129/1215:46 Barium mg/kg ND 0.50 05/29/1215:46 Cadmium mg/kg ND 0.10 05/29/1215:46 Calcium mg/kg ND 10.0 05/29/1215:46 Chromium mg/kg ND 0.50 05129/1215:46 Copper mg/kg ND 0.50 05/29/1215:46 Iron mg/kg ND 10.0 05/29/1215:46 Lead mg/kg ND 0.50 05/29/1215:46 Magnesium mg/kg ND 10.0 05/2911215:46 Manganese mg/kg ND 0.50 05/29/1215:46 Molybdenum mg/kg ND 0.50 05/29/1215:46 Nickel mg/kg ND 0.50 05/29/1215:46 Potassium mg/kg ND 500 05/29/1215:46 Selenium mg/kg ND 1.0 05/29/1215:46 Silver mg/kg ND 0.50 05/29/1215:46 Sodium mg/kg ND 500 05/29/1215:46 Zinc mg/kg ND 1.0 05/29/1215:46 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 LABORATORY CONTROL SAMPLE: Parameter 769533 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Qualifiers Arsenic mg/kg 50 49.4 99 80-120 Barium mg/kg 50 50.1 100 - 80-120 Cadmium mg/kg 50 48.6 97 80-120 Calcium mg/kg 500 479 96 80-120 Chromium mg/kg 50 48.1 96 80-120 Copper mg/kg 50 51.6 103 80-120 Iron mg/kg 500 506 101 80-120 Lead mg/kg 50 50.2 100 80-120 Magnesium mg/kg 500 513 103 80-120 Manganese mg/kg 50 48.5 97 80-120 Molybdenum mg/kg 50 49.6 99 80-120 Nickel mg/kg 50 48.8 98 80-120 Potassium mg/kg 500 484J 97 80-120 Selenium mg/kg 50 50.4 101 80-120 Silver mg/kg 25 24.4 98 80-120 Sodium mg/kg 500 511 102 80-120 Zinc mg/kg 50 47.8 96 80-120 Date: 06/13/201212:00 PM REPORT OF LABORATORY ANALYSIS Page 7 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalyiical� www.paWabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 MATRIX SPIKE SAMPLE: Parameter 769534 Units 92119358003 Result Spike Cone. MS Result MS % Rec . % Rec Limits Qualifiers Arsenic mg/kg ND 39.1 38.4 98 75-125 Barium mg/kg ND 39.1 39.1 100 75-125 Cadmium mg/kg ND 39.1 37.2 95 75-125 Calcium mg/kg 276 391 639 93 75-125 Chromium mg/kg ND 39.1 36.9 94 75-125 Copper mg/kg ND 39.1 41.1 105 75-125 Iron mg/kg ND 391 387 98 75-125 Lead mg/kg ND 39.1 38.6 99 75-125 Magnesium mg/kg ND 391 403 102 75-125 Manganese mg/kg ND 39.1 37.4 95 75-125 Molybdenum mg/kg ND 39.1 38.4 98 75-125 Nickel mg/kg ND 39.1 37.5 96 75-125 Potassium mg/kg ND 391 405 102 75-125 Selenium mg/kg ND 39.1 39.3 101 75-125 Silver mg/kg 1.0 19.5 20.7 101 75-125 Sodium mg/kg ND 391 427 107 75-125 Zinc mg/kg 1.9 39.1 38.0 92 75-125 SAMPLE DUPLICATE: 769535 92119392001 Dup Parameter Units Result Result RPD Qualifiers Arsenic mg/kg ND ND Barium mg/kg ND ND Cadmium mg/kg ND ND Calcium mg/kg 25.5 ug/g 28.6 11 Chromium mg/kg ND .075J Copper mg/kg ND .25J Iron mg/kg ND .81J Lead mg/kg ND ND Magnesium mg/kg ND 2.8J Manganese mg/kg ND .23J Molybdenum mg/kg ND ND Nickel mg/kg ND ND Potassium mg/kg ND 2.5J Selenium mg/kg 3.12 ug/g 2.9 7 Silver mg/kg ND ND Sodium mg/kg ND 136J Zinc mg/kg ND .62J Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS Page 8 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnaljNcal � www.pape)abs.com R Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA QC Batch: PMST/4780 Analysis Method: ASTM D2974-87 QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture Associated Lab Samples: 92119396001 SAMPLE DUPLICATE: 769717 Parameter Percent Moisture SAMPLE DUPLICATE: 769718 Parameter Percent Moisture 92119332001 Dup Units Result Result 19.3 19.0 92119396001 Dup Units Result Result 48.2 48.3 RPD Qualifiers 2 RPD Qualifiers 0 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 06/13/201212:00 PM REPORT OF LABORATORY ANALYSIS Page 11 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAna1Xica1 t www.pacalabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA QC Batch: WET/21017 Analysis Method: EPA 9045 QC Batch Method: EPA 9045 Analysis Description: 9045 pH Associated Lab Samples: 92119396001 SAMPLE DUPLICATE: 770001 92119358007 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C . Std. Units 3.5 3.5 1 SAMPLE DUPLICATE: 770002 92119358006 Dup Parameter Units Result Result RPD Qualifiers pH at 25 Degrees C Std. Units 5.2 5.4 2 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS Page 12 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceAnalj cal0 4 Wrw.pacelabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA QC Batch: WETA/12294 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total Associated Lab Samples: 92119396001 METHOD BLANK: 776339 Associated Lab Samples: 92119396001 Parameter Units Phosphorus mg/kg LABORATORY CONTROL SAMPLE: 776340 Parameter Units Phosphorus mg/kg MATRIX SPIKE SAMPLE: 776341 Parameter Units Phosphorus mg/kg SAMPLE DUPLICATE: 776342 Parameter Phosphorus Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 2.0 06/12/1210:10 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers 50 52.7 105 90-110 92119396001 Spike MS MS % Rec Result Conc. Result % Rec Limits Qualifiers 2680 201 3290 300 90-110 M6 92120635001 Dup Units Result Result RPD Qualifiers mg/kg 38.9 31.7 20 Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS Page 13 of 15 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. WeAnaiXicai® wwW.pacplabs.com Project: WOOD BOILER 5/25 Pace Project No.: 92119396 DEFINITIONS Pace Analytical Services, Inc. 205 East Meadow Road - Suite Eden, NC 27288 (336)623-8921 QUALIFIERS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL- Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG - Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. LABORATORIES PASI-A Pace Analytical Services -Asheville PAST-C Pace Analytical Services - Charlotte ANALYTE QUALIFIERS D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution. Date: 06/13/2012 12:00 PM REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. (704)875-9092 Page 14 of 15 aceAnalyllcal wmmw.pagelabsxom Project: WOOD BOILER 5/25 Pace Project No.: 92119396 Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 CERTIFICATIONS Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Charlotte Certification IDs 9800 KinceyAve. Ste 100, Huntersville, NC 28078 Connecticut Certification #: PH-0104 North Carolina Drinking Water Certification #: 37706 Florida/NELAP Certification #: E87627 North Carolina Field Services Certification #: 5342 Kentucky UST Certification M 84 North Carolina Wastewater Certification #: 12 Louisiana DHH Drinking Water # LA 100031 South Carolina Certification * 99006001 West Virginia Certification #: 357 South Carolina Drinking Water Cert. #: 99006003 Virginia/VELAP Certification M 460144 Virginia Drinking Water Certification M 00213 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 South Carolina Certification #: 99030001 Florida/NELAP Certification M E87648 Virginia Certification M 00072 Massachusetts Certification #: M-NC030 West Virginia Certification #: 356 North Carolina Drinking Water Certification #: 37712 UrginaNELAP Certification #: 460147 North Carolina Wastewater Certification M 40 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 15 Section 3 Lab Sheets Sample 4 — WBNPOCT17 October 17, 2012 Pace Analytical Services, Inc. Pace Analytical Services, Inc. aceAnaijdical 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacefabs.com Eden, NC 27288 Asheville, NC 2B804 (336)623-8921 (828)254-7176 ANALYTICAL RESULTS Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Sample: WBNPOCT17 Lab ID: 92135755002 Collected: 10/17/12 00:00 Received: 10/18/12 14:12 Matrix: Solid Results reported on a "dry -weight" basis Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual 6010 MET ICP Analytical Method: EPA6010 Preparation Method: EPA3050 Arsenic !/6.7 mg/kg 0.67 1 10/26/12 15:40 10129/1215:20 7440-38-2 Barium 1670 mg/kg 13.5 20 10/26/12 15:40 10/29/12 16:45 7440-39-3 Cadmium ".9 mg/kg 0.13 1 10/2611215:40 10/28/12 19:49 7440-43-9 Calcium 90100 mg/kg 269 20 10/26/12 15:40 10/29/12 16:45 7440-70-2 Chromium 23.6 mg/kg 0.67 1 10/26/12 15:40 10/28/12 19:49 7440-47-3 Copper 1-90.3 mg/kg 0.67 1 10/26/12 15:40 10/28/12 19:49 7440-50-8 Iron 23900 mg/kg 269 20 10/26/12 15:40 10/2911216:45 7439-89-6 Lead ✓18.4 mg/kg 0.67 1 10/26/12 15:40 10/28/12 19:49 7439-92-1 Magnesium 11900 mg/kg 13.5 1 10/26/12 15:40 10/28/12 19:49 7439-95-4 Manganese 2870 mg/kg 13.5 20 10/26/12 15:40 10/29/12 16:45 7439-96-5 Molybdenum V4.5 mg/kg 0.67 1 10/26/12 15:40 10/28/12 19:49 7439-98-7 Nickel t29.3 mg/kg 13.5 20 10/26/12 15:40 10/30/1216:27 7440-02-0 Potassium 16800 mg/kg 13500 20 10/26/12 15:40 10/29/12 16:45 7440-09-7 Selenium ✓ND mg/kg 1.3 1 10/26/12 15:40 10/28/12 19:49 7782-49-2 Silver ND mg/kg 0.67 1 10/26/12 15:40 10/28/12 19:49 7440-22-4 Sodium 6070 mg/kg 673 1 10/26/12 15:40 10/28/12 19:49 7440-23-5 Zinc Vf60 mg/kg 1.3 , 1 10/26/12 15:40 10/28/12 19:49 7440-66-6 7471 Mercury Analytical Method: EPA7471 Preparation Method: EPA7471 Mercury VND mg/kg 0.0095 1 10/25/12 12:15 10/25/12 15:43 7439-97-6 Percent Moisture Analytical Method: ASTM D2974-87 Percent Moisture 50.5 % 0.10 1 10/26/12 10:16 9045 pH Soil Analytical Method: EPA 9045 pH at 25 Degrees C 9.0 Sid. Units 0.10 1 10/28/12 14:30 365.1 Phosphorus, Total Analytical Method: EPA 365.1 Phosphorus 3370 mg/kg 194 25 10/28/12 16:47 7723-14-0 Date: 11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 6 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. aceArralytieal www.pacelabs.com 1 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 QC Batch: MERP/4616 QC Batch Method: EPA 7471 Associated Lab Samples: 92135755002 METHOD BLANK: 859191 Associated Lab Samples: 92135755002 Parameter Units Mercury mg/kg LABORATORY CONTROL SAMPLE: 859192 Parameter Units Mercury mg/kg QUALITY CONTROL DATA Analysis Method: EPA 7471 Analysis Description: 7471 Mercury Matrix: Solid Blank Reporting Result Limit Analyzed Qualifiers ND 0.0050 10/25/1214:26 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Spike LCS LCS % Rec Conc. Result % Rec Limits Qualifiers .067 0.061 91 80-120 MATRIX SPIKE SAMPLE: 859193 92136018001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Mercury mg/kg 0.0093 .052 0.024 29 75-125 M1 SAMPLE DUPLICATE: 859194 92136021001 Dup Parameter Units Result Result RPD Qualifiers Mercury mg/kg ND ND Date:11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 9 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. dei 0 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 161WAnaliftal 205 East Meadow Road - Suite A 2225 Riverside Dr. WW..pacelabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 QC Batch: MPRP/11824 QC Batch Method: EPA3050 Associated Lab Samples: 92135755002 Analysis Method: Analysis Description: EPA6010 6010 MET METHOD BLANK: 861104 Matrix: Solid Associated Lab Samples: 92135755002 Blank Reporting Parameter Units Result Limit Analyzed Arsenic mg/kg ND 0.50 10/28/1218:46 Barium mg/kg ND 0.50 10/28/1218:46 Cadmium mg/kg ND 0.10 10/28/1218:46 Calcium mg/kg ND 10.0 10/28/1218:46 Chromium mg/kg ND 0.50 10128/1218:46 Copper mg/kg ND 0.50 10/29/1214:29 Iron mg/kg ND 10.0 10/28/1218:46 Lead mg/kg ND 0.50 10/28/1218:46 Magnesium mg/kg ND 10.0 10/28/1218:46 Manganese mg/kg ND 0.50 10/28/1218:46 Molybdenum mg/kg ND 0.50 10/28/1218:46 Nickel mg/kg ND 0.50 10/28/1218:46 Potassium mg/kg ND 500 10/28/1218:46 Selenium mg/kg ND 1.0 10/28/1218:46 Silver mg/kg ND 0.50 10/28/1218:46 Sodium mglkg ND 500 10/28/1218:46 Zinc mg/kg ND 1.0 10/28/1218:46 Qualifiers LABORATORY CONTROL SAMPLE: Parameter 861105 Units Spike Conc. LCS Result LCS % Rec % Rec Limits Arsenic mg/kg 50 48.4 97 80-120 Barium mg/kg 50 48.8 98 80-120 Cadmium mg/kg 50 48.4 97 80-120 Calcium mg/kg 500 486 97 80-120 Chromium mg/kg 50 48.4 97 80' 120 Copper mg/kg 50 49.6 99 80-120 Iron mg/kg 500 504 101 80-120 Lead mg/kg 50 48.6 97 80-120 Magnesium mg/kg 500 491 98 80-120 Manganese mg/kg 50 48.8 98 80-120 Molybdenum mg/kg 50 48.7 97 80-120 Nickel mg/kg 50 48.4 97 80-120 Potassium mg/kg 500 473J 95 80-120 Selenium mg/kg 50 49.1 98 80-120 Silver mg/kg 25 24.4 98 80-120 Sodium mg/kg 500 479J 96 80-120 Zinc mg/kg 50 48.4 97 80-120 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Qualifiers Date: 11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 10 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. eAnapical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 �ac- www.pagslabs.com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 MATRIX SPIKE SAMPLE: 861174 92136087002 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Arsenic mg/kg ND 58.1 44.2 76 75-125 Barium mg/kg 112 58.1 185 126 75-125 M1 Cadmium mg/kg 3.4 58.1 53.8 87 75-125 Calcium mg/kg 378 581 893 89 75-125 Chromium mg/kg 65.1 58.1 95.1 52 75-125 M1 Copper mg/kg 46.0 58.1 105 101 75-125 Iron mg/kg 31300 581 30800 -94 75-125 M1 Lead mg/kg 13.4 58.1 66.8 92 75-125 Magnesium mg/kg 4260 581 5000 128 75-125 M1 Manganese mg/kg 917 58.1 1310 670 75-125 M1 Molybdenum mg/kg ND 58.1 48.3 83 75-125 Nickel mg/kg 17.6 58.1 68.5 88 75-125 Potassium mg/kg 8080 581 9350 218 75-125 M1 Selenium mg/kg 3.3 58.1 41.6 66 75-125 M1 Silver mg/kg ND 29 27.4 94 75-125 Sodium mg/kg ND 581 826 113 75-125 Zinc mg/kg 60.0 58.1 114 93 75-125 SAMPLE DUPLICATE: 861175 Parameter Units 92136087003 Result Dup Result RPD Qualifiers Arsenic mg/kg ND ND Barium mg/kg 96.8 98.7 2 Cadmium mg/kg 0.80 0.99 21 D6 Calcium mg/kg 2570 2150 18 Chromium mg/kg 20.1 18.9 6 Copper mg/kg 33.0 33.6 2 Iron mg/kg 22200 23100 4 Lead mg/kg 19.6 22.3 13 Magnesium mg/kg 2180 2700 21 D6 Manganese mg/kg 828 779 6 Molybdenum mg/kg 13.3 13.6 3 Nickel mg/kg 12.6 14.8 16 Potassium mg/kg 4620 5880 24 D6 Selenium mg/kg 1.7 1.4 19 Silver mg/kg ND ND Sodium mg/kg ND 595 Zinc mg/kg 31.9 39.5 21 D6 Date: 11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 11 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 0. aceftlytical® www.pacelabs.com j Pace Analytical Services, Inc. 205 East Meadow Road - Suite A Eden, NC 27288 (336)623-8921 Project: Wood Boiler WBNPOCT • Pace Project No.: 92135755 QC Batch: PMST/5083 QC Batch Method: ASTM D2974-87 Associated Lab Samples: 92135755001, 92135755002 SAMPLE DUPLICATE: 859793 Parameter Units Percent Moisture % SAMPLE DUPLICATE: 859794 Parameter Percent Moisture ova Units Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 QUALITY CONTROL DATA Analysis Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture 3571218006 Dup Result Result RPD Qualifiers 15.3 14.8 3 92136381003 Dup Result Result RPD Qualifiers 18.4 19.1 4 Pace Analytical Services, Inc. 9800 KinceyAve. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 11/02/2012 04:08'PM REPORT OF LABORATORY ANALYSIS Page 18 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. 1��IaceAnalj&cal •.0 Pace Analytical Services, Inc. Pace Analytical Services, Inc. 205 East Meadow Road - Suite A 2225 Riverside Dr. www.pacalabs.com Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 QUALITY CONTROL DATA Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 QC Batch: WET/22917 QC Batch Method: EPA 9045 Associated Lab Samples: 92135755002 SAMPLE DUPLICATE: 861901 Parameter Units pH at 25 Degrees C Std. Units SAMPLE DUPLICATE: 861902 Parameter Units pH at 25 Degrees C Std. Units Analysis Method: EPA 9045 Analysis Description: 9045 pH 92135468001 Dup Result Result RPD Qualifiers 7.3 7.3 0 92136406001 Dup Result Result RPD Qualifiers 5.6 5.6 0 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Date: 11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 19 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. ® Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc. l 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Kincey Ave. Suite 100 aeAnalytica www.pscalaica Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078 (336)623-8921 (828)254-7176 (704)875-9092 QUALITY CONTROL DATA Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 QC Batch: WETA/13594 Analysis Method: EPA 365.1 QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total .Associated Lab Samples: 92135755002 METHOD BLANK: 861558 - Matrix: Solid Associated Lab Samples: 92135755002 Blank Reporting Parameter Units Result Limit Analyzed Qualifiers Phosphorus mg/kg ND 2.0 10/28/1216:00 LABORATORY CONTROL SAMPLE: 861559 Spike LCS LCS % Rec Parameter Units Conc. Result % Rec Limits Qualifiers Phosphorus mg/kg 50 52.4 105 90-110 MATRIX SPIKE SAMPLE: 861560 92135468001 Spike MS MS % Rec Parameter Units Result Conc. Result % Rec Limits Qualifiers Phosphorus mg/kg 149 250 391 96 90-110 SAMPLE DUPLICATE: 861561 92135755002 Dup Parameter Units Result Result RPD Qualifiers Phosphorus mg/kg 3370 3240 4 Date: 11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 20 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. r ,t ® Pace Analytical Services, Inc. 80'AnalXica 205 East Meadow Road - Suite A wWwpabaa/a`bs.com Eden, NC 27288 (336)623-8921 QUALIFIERS Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 DEFINITIONS Pace Analytical Services, Inc. 2225 Riverside Dr. Asheville, NC 28804 (828)254-7176 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of the sample aliquot, or moisture content. ND - Not Detected at or above adjusted reporting limit. J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit. MDL -Adjusted Method Detection Limit. PRL - Pace Reporting Limit. RL - Reporting Limit. S - Surrogate 1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene. Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values. LCS(D) - Laboratory Control Sample (Duplicate) MS(D) - Matrix Spike (Duplicate) DUP - Sample Duplicate RPD - Relative Percent Difference NC - Not Calculable. SG Silica Gel - Clean -Up U - Indicates the compound was analyzed for, but not detected. N-Nitrosodiphenylamine decomposes and cannot be, separated from Diphenylamine using Method 8270. The result reported for each analyte is a combined concentration. Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride. Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes. TNI - The NELAC Institute. .LABORATORIES PASI-A Pace Analytical Services - Asheville PASI-C Pace Analytical Services - Charlotte PASI-O Pace Analytical Services - Ormond Beach ANALYTE QUALIFIERS 1g 8260 results are from a total analysis which show that analytes are not present or that they are present but at such low levels that the appropriate regulatory levels could not possibly be exceeded, per Section 1.2 of Method 1311. D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits. M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery. Date:11/02/2012 04:08 PM REPORT OF LABORATORY ANALYSIS Page 21 of 22 This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. n 1 t ;® Pace Analytical Services, Inc. Pace Analytical Services, Inc. �c AI al j i 1t+aJ205 East Meadow Road - Suite A 2225 Riverside Dr. www..pa4elobs.corn Eden, NC 27288 Asheville, NC 28804 (336)623-8921 (828)254-7176 CERTIFICATIONS Project: Wood Boiler WBNPOCT Pace Project No.: 92135755 Ormond Beach Certification IDs 8 East Tower Circle, Ormond Beach, FL 32174 Alabama Certification #: 41320 Arizona Certification #: AZ0735 Colorado Certification: FL NELAC Reciprocity Connecticut Certification #: PH-0216 Florida Certification #: E83079 Georgia Certification #: 955 Guam Certification: FL NELAC Reciprocity Hawaii Certification: FL NELAC Reciprocity Illinois Certification #. 200068 Indiana Certification: FL NELAC Reciprocity Kansas Certification #: E-10383 Kentucky Certification #: 90050 Louisiana Certification #: FL NELAC Reciprocity Louisiana Environmental Certificate M 05007 Maine Certification #: FL01264 Massachusetts Certification M M-FL1264 Michigan Certification M 9911 Mississippi Certification: FL NELAC Reciprocity Missouri Certification * 236 Charlotte Certification IDs 9800 Kincey Ave. Ste 100, Huntersville, NC 28078 North Carolina Drinking Water Certification M 37706 North Carolina Field Services Certification M 5342 North Carolina Wastewater Certification #: 12 South Carolina Certification M 99006001 Asheville Certification IDs 2225 Riverside Dr., Asheville, NC 28804 Florida/NELAP Certification * E87648 Massachusetts Certification #: M-NC030 North Carolina Drinking Water Certification #: 37712 Pace Analytical Services, Inc. 9800 Kincey Ave. Suite 100 Huntersville, NC 28078 (704)875-9092 Montana Certification #: Cert 0074 Nevada Certification: FL NELAC Reciprocity New Hampshire Certification #: 2958 New Jersey Certification #: FL765 New York Certification #: 11608 North Carolina Environmental Certificate M 667 North Carolina Certification #: 12710 Pace Analytical Services - Ormond certification number E83509 Pennsylvania Certification #: 68-00547 Puerto Rico Certification * FLO1264 Tennessee Certification #: TN02974 Texas Certification: FL NELAC Reciprocity US Virgin Islands Certification: FL NELAC Reciprocity Virginia Environmental Certification #: 460165 Washington Certification M C955 West Virginia Certification #: 9962C Wisconsin Certification M 399079670 Wyoming (EPA Region 8): FL NELAC Reciprocity Flonda/NELAP Certification M E87627 Kentucky UST Certification #: 84 West Virginia Certification M 357 VrginiaNELAP Certification #: 460221 North Carolina Wastewater Certification #: 40 South Carolina Certification M 99030001 West Virginia Certification #: 356 Vrginia/VELAP Certification M 460222 REPORT OF LABORATORY ANALYSIS This report shall not be reproduced, except in full, without the written consent of Pace Analytical Services, Inc.. Page 2 of 22 Section 4 Ash Receiver Signature Sheets Signed Ash Distribution Information Sheets Asti Distribution Prograin Inform8tio" Sheet Baxter Healthcare ........ ... -- ...... ........ CorTi.. is the Renermor of the ash Provided tQ (Rvcipient). Application of the aforementioned ash i�,; prohjl.Tlf��d except in accordance with the instructions on this sheet. Transpon; Adequate provisions shall be tahen to ensure that the tran5portation of ash, doe's not cause nuisances and hazards to public health and -;afeuy or otherwise cause an adverst jinpact (Qtrsuaspkrt. wet aQ-i in Icak-proofti-ticks or cover dry a-sh). Storage: The ash shall be adequately stored to prevent wind erosion or surface runalf from carrying ash into any surface waters. Keeping the ash slightly rnoistened will accomplish this olajective under nominal conditions. However. berms, harriers, or tarps, may be necessary Linder vvindy or rainy conditions or if crosion or runoff cannot be contrcillc& 4/ , �J)Hcation: When using ash. the following shall apply� o The ash application rates shall be limited to those that can be (i.e- limiwd to that needed to meet the liming, roquiremems of the crops being gown on the land.), a Ash shall nett he placed within 50 feet cif any surface water. * Ash shall not he placed within one f6.ot of the seasonal high water table. a Ash shall not be placed within 100 feet of any water supply well tier spring miless underfain and overlain by a liner vtiith a niaximum hydraulic: eondut;ovity of 10' centiriwtors pQr sccond, If such 41 liner/cover is provided, ash shall not be placed within 25 J-ee( ofany water supply well or spring, P The ash shall not. be applied to any sitethat is flooded. frozen. tar snow-covered. A. ,ummary of the ash chemical analyses is located on page 4 of the intbi-niation sheet. l3etailed laboratory results are available upon request. Title to the ash will transfer front Baxter healthcare, Corp to Rccipient upon delivery thereof. Thereafter. Baxter Healthcare, Corp will have no responsibility and ,;hall not tic held liable by Recipient or any third party for any spill, misuse, misapplication or other mishandling of the ash., Recipient acknowledges an(( agrees that. the ash is being delivered by Baxter I-lealthcare. Corp to Recipient as an accoinniodation to Rceipient. An exchange themfore ` Recipient aigrees to indernnif�y, save and hold Baxter Healthcare, (.'orp harmless fiom and against an), and all liability- damage,, loss. crest: CM)ewW (including attorneys" fl:es), claim, demand, suit, action...judgm-tent or recovery asserted against Baxter licaltheare, Corp by any third part),. including any governmental authority. whether R)r bodily injury (including death) or damage to property, arising; fron) or in connection with Recipient's receipt. transportation, hafiling ur Offiet use of the ash, .. ... . . .......... ........ - S vied (Asti P ... . ......... ............ Date .......... . ... . ........... Ash ReeipienCs Address: Intended Lj,,;e of Asti,. .......... ...... ........ . ........ .. . ......... . ...... . .. E-xpected --s of I anti. C Acre Page I of: WROW Nm1h Ash Disfrihildnil W"n Nth by- , lixg ANWAXI a0d m9no, v- nit,, homh mo cc V% 4A vme�q 0 low VC 00SP7 ,%holy, Sih AW A he a&qWm% -0, in C WA wm�q hcommW AqwkUmp, 'shoo "Ay AWL W" nllmsmw an wp � rMYN WAI 1--v !hai, 'O 4, plo. Nov mn of, mv two; nxQv"WNA'Q Tv szf� 0021 941AP 00 20 Lod; W AMN 51l SL PLUCK =Gn 1.00 All VA K, 0noy "IAV Owl,. inn ix V,ud -0pip 'A' .00 0 0 .0 C" cop qn p" 1 AC as Mai 0, an �v Anton. "NYqW1WxkW Wr aqui mnmmjkj.� & LY, ONO;", no! aymonG Inc ly. wComms lot" us jakinunh. mcmd N-A Wono oWn-, AWASIC T 000%, KA k 1: AVASIS 1A., '1:;'-.;o.i' hwj oy" xu q- onx LUIS! 04hym omho -or stud, ova, FWiWva 'WAY Lm:Ei _J 1 Y. v f V v I F, 2% Ash Distribution Program Information Sheet Baxter Healthcare. Corp.. is the; generator of the ash provided to ....... - _S_ f� rise lo a e, (Recipient). Application of The atbrementioned ash is prohibited except in accordance with the instructions ern this, sheet. Trwisl,iorl: Adequate provisions shall be taken to ensure that the transportation of ash does not cause nuisances and haziirds to public health and safety or otherwise cause an adverse impact (e.g_ transport wet ash in leak -proof trucks or cover dry ash). The ash shall be adequately stored to prevent vvind erosion or surfiace, runoff from carrying ash into anv surface waters. Keeping the ash slightly moistened will accomplish this objective under normal Conditions, However, bermsi, barriers, or tarps, may lie necessary under vvindy or rainy coridition,', or if erosion or runoff cannot be controlled. .41y.dication: When using ash, ifie -ficyllowing shall apply: * The ash application rates shall be limited to those that. can beawyrranorraiexally jrawtified Ge- limited to that needed to meet the firning requirements of the crops being gro-,,vii oil the land}. * Ash ,hall not he placed within 50 feet ofany Surface vvkner. * Ash sball not be placed within one fool of fficseasonal WO water table. * Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a liner with to maximuni hydraulic conductivity of i 0'7F' centimeters per second, I ['such a liner/cover is provided, ash shall not be placed within 25, fiat of any water supply well or spring * The ash shall not be applied to any site that isfloode(L frozen. or snow-covered. A summary of the ash clicrnical anaiyses is located on page 2 of the inl'ormation. Sheet. Detailed. laboratory results acre available upon request. Title to the ash will trawsfi:r from Baxter Healthcare. Corp to Recipient upon delivery thereof. Thereafter. 8 ax Jer (,"orp will baveno responsibility and shall not bt4 held liable by Recij)Wnt or any third - party tor any spill, misuse. misapplication or other mishandling ofthe ash, Recipient acknowledges and of reets that the ash is being, delivered by Baxter Healthcare. Corp to Recipient as an accommodation to Recipient. In exchanue therel"Ore. Recipient agrees to indernnif}', save and hold Baxter Healthcare. Corp harniless front and against any and all liability, damage, loss, cost, expense (includin.g attorneys' fees). claim, demand, suit. action, judgment or recovery asserted against. Batter Healthcare, Corp by any third party. uicludirq; any gOverninen(al ,:authority, whether fear bodily in ury (including death) or darnage to property. arising Born or in connection with Recipient's receipt, tran"portahon., handling or other use of the ash, Signed (Ash R.ecipient), Zi, �,5" D Ash Recipient's address Intended l se off h: /4"IVAe;/ l"xpected Qt);,' r. ( irdated'.. 1 5" 10 Acres off.and . .... Baxter Healthcare, Corp. 28.59 Old Linville Road Marion. North C'arolina 2,17:52 Ash Distribution Program Information Sheet Baxter Healthcare, Corp., is the generator of tile ash provided to (Recipient). Application of the aforementioned ash is prohibi ed except in accordant --with' the instructionsinstructions oil this sheet. Transport.- Adequate provisions shall be taken to ensure nsure that the transportation of ash does not cause nuisances and hazards to public health and safety or otherwise cause all adverse impact (e.g., transport wet ash in leak -proof trucks or cover dry ash). Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying ash into any surface waters. Keeping the asli slightly moistened will accomplish this objective under normal conditions. 14owever, bernis, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be controlled. Application: When using ash, the following shall apply- * The ash application rates shall be limited to those that can be agrozioni ical lyJustified (i.e., limited to that needed to meet the liming requirements of the crops being grown on the land). * Ash: shall not be'Placed within 50 feet of any surFace water. * Ash shall not he placed within one foot ofthe seasonal high water table. is Mh shall not, be placed within 100 feet of any water supply well or spring unless underlain and overlain by a liner with a maximum hydraulic conductivity of 19" centimeters per second. If such a liner/cover is provided., ash shall not be placed within 25 feet of any water supply well or spring. o The ash shall not be applied to any site that is flooded, frozen, or snow-covered. A summary of the ash chemical analyses is located on page 2 of the information sheet. Detailed laboratory results are available upon request. Title to the ash will transfer ftom..Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Flealtheare'. Corp will have no responsibility and shall not be field liable by Recipient or any third party for any spill, misuse, misapplication or other mishandling of the ash. Recipient acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare. Corp by any third party, including any governmental authority, whether for bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling or other use of the ash. Signed (Asti Recipient): Ash Recipient's Address: Intended Use of Ash: 4- c' 4!,! e Acres of Land: J,> Expected QtyfYr: 1 9 Page I of 3 Updated: M5110 Baxter Healthuare, Corp.. 2859 Old Linville Road Marion, North Carofisaa Ash Distribution Program baformation Sheet Baxter Healthcare, Corp., is the generator of the ash provided to -Nturs FWA5 (Recipient), Application of the aforementioned ash is prohibited except in accordance tvith the instructions on this Sheet. Transpori.- Adequate provisions shall be taken to ensure that the transportation of ash does not'causc nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport wet ash in leakproof trucks or cover ilty ash). Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from. carrying ash into Any surface waters. Keeping the ash slightly moistened will accomplish this objective under normal conditions. however, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if erosion or runoff cannot be controlled, Application: When using ash, the following shall apply, * "the ash application rates shall be limited to those that can be agronomically justified (i.e., limited to that needed to.tneet the liming requirementq of the crops being grown on the land), * Ash shall not be placed within 50feet of any surface water. * Ash shall not be placed within one foot of the seasonal high water table. * Ash shall not be placed within 100 feet of any water supply well or spring unless underlain and overlain by a. liner with a maximum hydraulic conductivity of 10-6 centimeters per second. If such a liner/cover is provided, ash shall not be placed within 25 feet of any water supply well or spring. * The ash shall not be applied to any site that is flooded, frozen, or snow-covered. A summary of the ash chemical analyses is located on page 2 of the information Sheet. Detailed laboratory results are available upon request. Title to the ash will transfer from Baxter Healthcare, Corp to Recipient upon delivery thereof. Thereafter, Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third party for. any spill, misuse, misapplication or other mishandling of the ash. Recipient. acknowledges and agrees that the ash is being delivered by Baxter Healthcare, Corp to Recipient as an accommodation to Recipient. In exchange, therefore, Recipient agrees to indemnify, save and hold. l3axterl-lealtheare. Corp harmless from. and against any and all liability, damage, loss, cost, expense (including attorneys' fees), claim, demand, suit, action, judgment or recovery asserted against Baxter Healthcare, Corp by any third party, including any governmental authority, whether for bodily injury (including death) or damage to property, arising from or in connection with Recipient's receipt, transportation, handling or other use of the ash. Signed (Ash Recipient): _J1111-841LOS --Bate: Ash Recipient's Address: '11?1?7 tylu V / 9F Intended Use of Ash, 11641a(LTUR-65 SUL I/VX�M_ Expected QtyiYr: Page I of 3 Updated.- 3/5/10 Acres of Land: -;- Nbriam Norch WiMm"i .Ash OfstdWon Pragmut Wbraiathe We( Sh "'d' 1 MY (Pit WYAO Wev, khroo It AXY CA * Wran"Oky v, vOwell nll. w'zr ioaj�: pmvogms AM ho Map w owwr Mt To sruiqlwaran caunk- �4 v d nunwaus ami Woods w We how; apa vv& — MOMMO C.Se an a&Nmc Ungm w P wmpw ?""'l w, ',roo"' *j- so Qvil .,W ausano a w0a -mn,W A= zmynp Aw or n.r W.-tw1--, 01% ask die fhllwyng Stott 0144', MH bu hmmy v? NNAC that cap N; io mcl-t the Yang "I'llid) lob AaH MI high .wi§'-'r r:.Ibh" AA, sh";P: jl')i Q fACS IM M ts f nwY =1o-nngui--ardWoans hncx "0 a nommum h, Mw cyAwhi m of IS wh MO Mw hu an�-kll A wwwow\ or 034K Go nowwwn not: 11100. We w) Au W m I Uwmlr a.EtRvoym upon d&;v--c,, 'Inc-kk.-Awr SOU We wo' ru-Spons�'Ntry ��.3vfj �;N.'tU r"o'f -v�'W bal�Ac 01 thi-rdl parly ftv an.% u;�wi"I. in f, aljos "All ..l am, ON 41OW'.'T agpifi:.�". azv`s aodll nu'i jMnM?y WAY WML danlagc' tot.answg t. AO RevroWy Was. .. .. ... . ......... . ANY(