WQ0010689_Application_20140718

WATER QUALITY REGIONAL OPERATIONS SECTION
APPLICATION REVIEW REQUEST FORM
Date: July 18, 2014
To: ARO-WQROS: Chuck Cranford / Landon Davidson
From: David Goodrich, Water Quality Permitting Section - Non -Discharge Permitting Unit
Telephone: [phone] Fax: [phone] E Mail. [e-mail]
A. Permit Number: WQ0010689
B. Applicant: Baxter Healthcare Corporation
C. Facility Name: North Cove Steam Generation Plant Ash Distribution Program
D. Application:
Permit Type: Distribution of Residual Solids (503 Exempt)
Project Type: Renewal
E. Comments/Other Information:
❑ I would like to accompany you on a site visit.
Attached, you will find all information submitted in support of the above -referenced application for your
review, comment, and/or action. Within 45 calendar days, please take the following actions:
® Return a completed WQROSARR Form.
❑ Attach a classification rating sheet.
❑ Attach Attachment B for Certification.
® Return a completed WQROSRRR Staff Report
❑ Attach Well Construction Data Sheet.
❑ Issue an Attachment B Certification.
When you receive this request form, please write your name and dates in the spaces below, make a copy
of this sheet, and return it to the appropriate Central Office Water Quality Permitting Section contact
person listed above.
RO-WQROS Reviewer: Date:
RECEIVED
Division of Water Resources
J U L 2 1 2014
Water Quality Regional Operations
Asheville Regional Office_._
FORM: WQROSARR 02-14 Page 1 of 1

A=A
.
NCDENR
North Carolina Department of Environment and Natural Resources
Pat McCrory John E. Skvarla, III
Governor Secretary
July 18, 2014
Terry Foxx — Plant Manager
Baxter Healthcare Corporation
65 Pitt Station Rd.
Marion, NC 28752
Subject: Acknowledgement of
Application No.,WQ0010689
North Cover Stream Generation
Ash Distribution System
Rowan County
Dear Mr. Foxx:
The Water Quality Permitting Section acknowledges receipt of your permit application and
supporting documentation received on July 15, 2014. Your application package has been assigned the
number listed above, and the primary reviewer is David Goodrich.
Central and Asheville Regional Office staff will perform a detailed review of the provided
application, and may contact you with a request for additional information. To ensure maximum
efficiency in processing permit applications, the Division of Water Resources requests your assistance in
providing a timely and complete response to any additional information requests.
Please note that processing standard review permit applications may take as long as 60 to 90 days
after receipt of a complete application. If you have any questions, please contact
David Goodrich at [phone] or [e-mail].
Sincerely,
Jon isgaard, Supervisor
Division of Water Resources
cc: Asheville Regional Office, Water Quality Regional Operations. Section
Michael Pisarik — Baxter Healthcare Corp. P.O. Box 1390 Marion NC 28752
Permit File WQ0010689
1636 Mail Service Center, Raleigh, North Carolina 27699-1636
Phone: [phone] Internet: http://Portal.ncdenr.ora/web/wg
An Equal Opportunity 1 Affirmative Action Employer- Made in part with recycled paper

Central Files: APS — SWP
7/18/2014
Permit Number WQ0010689 Permit Tracking Slip
Program Category Status Project Type
Non -discharge In review Renewal
Permit Type Version Permit Classification
Distribution of Residual Solids (503 Exempt) D Individual
Primary Reviewer Permit Contact Affiliation
david.goodrich
Coastal SWRule
Permitted Flow
Facility
Facility Name Major/Minor Region
North Cove Steam Generation Plant Ash Distribution.Program Major Asheville
Location Address County
2859 Old Linville Rd McDowell
Facility Contact Affiliation
Marion NC 28752 Amanda Richcreek
Engineer Environmental
Owner
Owner Name Owner Type
Baxter Healthcare Corporation Non -Government
Owner Affiliation
Ricky Styles
2859 Old Linville Rd
Dates/Events Marion NC 28752
Scheduled
Orig Issue App Received Draft Initiated Issuance Public Notice Issue Effective Expiration
7/7/1995 7/15/2014
Regulated Activities Requested /Received Events
Commercial or industrial, other RO staff report received
RO staff report requested
Outfall
Waterbody Name Streamindex Number Current Class Subbasin

Baxter
July 9, 2014
NCDENR Division'of Water Resources
Water Quality Permitting Section
Non -Discharge Permitting Unit
1636 Mail Service Center
Raleigh, NC 27699-1636
RE: Permit No.WQ0010689 Permit Renewal Application for North Cove Steam Generation Plant Ash
Distribution Program .
Baxter Healthcare Corporation requests renewal of Permit No. WQ0010689. There have been no major
process changes or physical changes to equipment covered by this permit since our current permit was
issued. Please find the enclosed application which includes Form DCAR 11-13 and required
documentation for sections A, C, D, and H as instructed by Ms. Beverly Price in the NCDENR,
Asheville office. Also included is a current site map as directed in our current permit, paragraph I. 1.
Baxter Healthcare is submitting this application after the 180 day application deadline.due to the illness
and absence of our primary Environmental Engineer and turnover of key personnel. We sincerely
apologize for any inconvenience and have put measures in place to avoid a similar situation. in the
future.
If you have any questions regarding this application, please contact me at (W) 828-756-6017 or
michael pisarik@,baxter.com.
Sincerely,
Michael J. Pisarik
Sr. Environmental Engineer
Enclosures:
DCAR 11-13 and Supporting Documents- 1 Original & 2 Copies
DCAR 11-13
Residuals Source Certification
Program Information
Operations and Maintenance Plan
Ash Distribution Program Information Sheet
Analytical Reports
Steam Generation Plant Site Map
Baxter Healthcare Corporation
PO Box 1390, Marion, NC 28752
T 828.756.4151

State of North Carolina
Department of Environment and Natural Resources
. _
Division ofWater• Resources
Division of Water Resources 15A.NCAC 02T .1100 - DISTRIBUTION OF CLASS A RESIDUALS
INSTRUCTIONS FOR FORM: DCAR '11-13 '& SUPPORTING DOCUMENTATION
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the, amount of..additional
information requested., Failure to submit all of the required' items will lead to additional processing and review time for the
permit, application. Unless otherwise noted, -the Apblicant shall submit one original and two conies of -the application and
supporting documentation
For more' information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website at:
hap: 'portal.ncdenr.org/web/wg/aps/lau
General — This application is for treatment, storage, transport, distribution;' land application, and/or'.marketing of Class A (or
Equivalent) residuals under 15A NCAC 02T .11.00.
Unless otherwise noted, the Applicant shall submit one original and -two copies of the application and supporting documentation listed
below:
A. Distribution of Class A Residuals (FORM: DCAR 11-13):
Submit the completed and appropriately executed Distribution of Class A Residuals (FORM: DCAR.11-13) form. Please do
not make any unauthorized content changes to this -form. If necessary for clarity or due to space restrictions, attachments to
the application may be made,, as long as the attachments are numbered to correspond to the section and item to which they
refer.
The project name should be -consistent on the;plans, specifications; etc.
The Applicant's Certification on Page 3 of this form shall, be signed in accordance with 15A NCAC 02T .0106(b). An
alternate person may be designated as' the signing official . if a .delegation letter is provided from a person who meets the
criteria in 15A NCAC 02T ,0106(b).
0 If this project is fora modification of an existing permit, subi u"t one copy -of the existing permit.
Please submit this application form at least 180 days prior to the expiration date on the existing permit, or 90 days prior to
operation of proposed facility(ies) for application packages involving new or changes to treatment nand storage units.
B. Application Fee pp ' (New and Major Modification Application Packages) . • '
E3 Submit a check, money order or electronic funds transfer made, payable to: North Carolina Department of Environment and
Natural. Resources (NCDENR).
STANDARD'REVIEW — Submit the appropriate 'fee for all new and major modification applications as listed in the table
below.
STANDARD APPLICATION REVIEW FEES:
Facility Classification:.1
tY New Permit Major Modification
_i_i__
Major (residuals permitted for distribution > 3,000 dry tons/year) $1,310 ! $395
- _ Minor residuals permitted for distribution < 3' 000 dry tons/year) $810 $245
1- A major modification°'shall be defined as any permit modification that: increases the generating facility's residuals dry tonnage;
adds additional residuals ,sources; or includes the addition of new treatment or storage units/processes not previously permitted.
There is no fee for minor permit modifications.
C. Cover Letter (All Application Packages)
List all items included in the application package, as well as a brief descri tion of the requested permitting action.
JUL. 15 20'14
Permitting section
INSTRUCTIONS FOR FORM: DCAR 11-13' PaL7e 1 of 3

D. Program Information (All Application Packages)
Provide a narrative explaining the following:
How the materials will. be handled and transported from -where the residuals were produced to where it will be treated.
How the residuals will be processed/treated' (attach process flow diagram).
How leachate collection will be handled.
Where the residuals will be stored until processed.
t,How the final product will be distributed (packaging, bulk,, etc.)
What nutrients or other constituents (i.e. nitrogen, phosphorous, aluminum, calcium, etc.) are used or recommended as the
limiting parameter for determination of residuals loading rate to ensure that it does not overload the soil and cause
contravention of surface water or groundwater standards, limit crop growth, or adversely impact soil quality.
Attach,a marketability statement detailing destinations and approximate amounts of the final product to be distributed.
g[ Provide either a label that shall be affixed to the bagged processed residual or an information sheet that shall be provided to
the person who receives the processed residual. The label or information sheet shall contain,. at a minimum, the following
information:
Name and address of the person who prepared the residual that is sold or given away.
A statement that application of the residuals to the land shall be in accordance with the instructions on the label or
information sheet.
A statement that the residuals shall not be applied to any site that is flooded, frozen or snow-covered.
A statement that adequate procedures shall be provided to prevent surface runoff from carrying any disposed or stored
residuals into any surface waters.
Information on all applicable setbacks in accordance with 15A NCAC 02T .1108(b).
A statement that the residuals shall be applied at agronomic or recommended rates for intended uses.
E. Detailed Plans and Specifications (Application Involving New or Changes to Treatment or Storage Units)
Submit detailed plans and specifications that have been signed, sealed, and dated by a NC Professional Engineer per 15A
NCAC 02T .1104(a). Specifications for standard equipment may only be omitted for municipalities with approved standard
specifications, but use of the standard specifications must be noted on each sheet of the plans.
Plans must include the following minimum items: a general location map, a topographic map, plan and profile view of the
residuals treatment and storage units as well as the proximity of the residuals treatment and storage units to other utilities and
natural features within 500 feet of all treatment and storage facilities, and detail drawings of all items pertinent to the
residuals treatment and storage units. Depict minimum separations required in 15A NCAC 02T .1108(a) on the plans.
Specifications must include, at a minimum, the following for all items pertinent to residuals treatment and storage units:
description of materials to be used, method's of construction, quality of construction testing procedures to ensure the integrity
of the final product in accordance with 15A NCAC 02T .1104(a)(2)(B), including leakage and pressure testing as appropriate.
Plans and specifications must not be labeled with preliminary phrases (e.g., FOR REVIEW ONLY, NOT FOR
CONSTRUCTION, etc.) that indicate that they are anything other than final plans and specifications. However, the plans
and specifications may be labeled with the phrase: FINAL DESIGN — NOT RELEASED FOR CONSTRUCTION.
F. Engineering Calculations (Application Involving New or Changes to Treatment or Storage Units)
El Submit all design calculations that have been signed, sealed, and dated by a NC Professional Engineer per 15A NCAC 02T
.1104(a).
G. Environmental Assessments (May be Required — See 15A NCAC 1C .0300)
Submit a copy of the Findings of No Significant Impact (FONSI) or Environmental Impact Statement (EIS). Also, include
information on any mitigating factor(s) from the Environmental Assessment (EA) that impact the construction of the
residuals treatment and storage facilities. An EA may also be required for private systems if any public funds and/or lands
are used for the construction of the subject facilities.
INSTRUCTIONS FOR FORM: DCAR 11-13 Page 2 of 3

H. Operation and Maintenance Plan (New and Renewal Application Packages)
El For Modification Application, if there are any changes to the existing plan, submit an updated O&M plan.
Submit the O&M Plan in accordance with 1.5A NCAC 02T .1110 and include at a minimum:
Operational functions; describe the operation of the program to show what operations are necessary for the program to
function and by whom the functions are to be conducted.
Maintenance schedules; may include equipments calibration, maintenance of signs, etc.
Safety measures; may include safety training program, manuals, signs, etc.
Spill response plan; including control, containment, remediation, emergency contact information, etc.
Inspection plan including the following information;
® Names and titles of personnel responsible for conducting the inspections.
Frequency and location of inspections, including those to be conducted by the ORC, and procedures to assure that the
selected location(s) and inspection frequency are representative of the residuals management program.
Detailed description of inspection procedures including record keeping and actions to be taken by the inspector in the event
that noncompliance is observed.
Sampling and monitoring plan including the following information;
Names and titles of personnel responsible for conducting the sampling and monitoring.
Detailed description of monitoring procedures including parameters to be monitored.
Sampling frequency and procedures to assure that representative samples are being collected. Fluctuation in temperature,
flow, and other operating conditions can affect the quality of the residuals gathered during a particular sampling event. The
sampling plan shall account for any foreseen fluctuations in residuals quality and indicate the most limiting times for
residuals to meet pathogen and vector attraction reduction requirements (e.g. facilities that land apply multiple times per year
but have an annual sampling frequency, may need to sample during winter months when pathogen reduction is most likely to
be negatively affected by cold temperatures.
ONE ORIGINAL AND TWO COPIES OF THE COMPLETED APPLICATION PACKAGE, INCLUDING ALL
SUPPORTING INFORMATION AND MATERIALS, SHALL BE SENT TO THE FOLLOWING ADDRESS:
NORTH CAROLINA DEPARTMENT OF ENVIRONMENT AND NATURAL RESOURCES
DIVISION OF WATER RESOURCES
WATER QUALITY PERMITTING SECTION
NON -DISCHARGE PERMITTING UNIT
By U.S. Postal Service:
1636 MAIL SERVICE CENTER
RALEIGH, NORTH CAROLINA 27699-1636
TELEPHONE NUMBER: [phone]
By Courier/Special Delivery:
512 N. SALI8BURY STREET
RALEIGH, NORTH CAROLINA 27604
FAX NUMBER: [phone]
INSTRUCTIONS FOR FORM: DCAR 11-13 Page 3 of 3

State of North Carolina
Department of Environment and Natural Resources
Division of Water Resources
Division of Water Resources 15A NCAC 02T .1100 — DISTRIBUTION OF CLASS A RESIDUALS
FORM: DCAR 08-13
I. APPLICANT INFORMATION:
1. Applicant's name: Baxter Healthcare Corporation
Applicant type: [] Individual [g Corporation Ej General Partnership Q Privately -Owned Public Utility
❑ Federal ❑ State ❑ Municipal Q County
Signature authority's name per 15A NCAC 02T .0106: Terry Foxx Title: Plant Manager
Applicant's mailing address: 65 Pitt Station Rd.
City: Marion State: NC Zip: 28752-1 __ 1
Telephone number: 828 756-6530 Email Address: tegy foxxAbaxter.com
2. Consultant's name: NA License Number (for P.E.): _ l
Affiliation: [] On Staff: Retained (Firm: _)
Consultant's mailing address: F_
City: State: Zip:
Telephone number: (i 6 C_7V_1- 1 Email Address: iW
3. Fee submitted: I i (See Instruction B)
H. PERMIT INFORMATION:
1. Application is for (check all that apply): Q new, ❑ modified, 0 renewed permit
2. If this application is being submitted to renew or modify an existing permit, provide the following:
Permit number: WO0010689
Date of most -recently issued permit: June 7, 2010
Date of most -recently certified Attachment A (if different than the permit): r 1.
III. FACILITY INFORMATION:
1. Name of residuals processing facility: North Cove Steam Generation Plant
City: Marion State: NC Zip: 28752-1- a
Coordinates: Latitude: 35' 50' S" Longitude: 810 59' 40.7"
Datum: ' Level of accuracy: r` ----7
I I
Method of measurement: Google Earth
County where facility is located: McDowell
2. Facility contact (person familiar with residuals preparation):
Name: Rick Styles Title: Wood Boiler Superintendent
Mailing address: 65 Pitt Station Rd.
City: Marion State: NC
Telephone number: 828 756-6650
Zip: 287524`i
E-mail address: ricky styles ,baxter.com
FORM: DCAR 11-13 Page 1 of 3

3. Is the residual process facility also the generator? Yes; [] No
If No, please specify delivery frequency and quantity of residual to be processed: F.,i
4. Length of residuals storage at facility: <90 days (Note: the Division requires minimum 30 days storage in units that are
separate from treatment system, i.e. not in clarifiers, aeration basins, etc.)
IV. RESIDUALS QUALITY INFORMATION:
1. Specify how these residuals will be distributed:
sold or given away in bags or other containers; j] lawn (bulk); Q home garden (bulk);
El other (explain); Sold or given away in bulk for agricultural application
Note: Bulk residuals shall mean residuals that are transported and not sold or giving away in a bag or other receptacles with a
load capacity of one metric ton or less.
2. Complete the following if residuals are to be mixed with other materials:
Type of Materials
Amounts to be added
er 1.0 dry ton of residuals ton
Wood chips or saw dust
0.1-0.2 dry tons
3. Approximate amounts of the residuals received and processed at the facility: 2000 dry tons per year.
4. Approximate amounts of the final product (processed residuals) to be distributed: 2000 dry tons per year.
5. Provide a description of the onsite storage management plan for the treated residuals (including estimated average and
maximum storage times prior to distribution): Material stockpiles of approximately 500 tons are stored in basins or on the
cement apron until loaded onto bulk trucks for distribution Storage time depends on time of year and conditions of
application sites but is generally 30-60 days.
6. Does the facility have a stormwater management plan? Yes; Q No
Explain whether the treatment and storage areas are under,roof or how stormwater runoff will be handled: Treatment and
storage is not located under a roof. Stormwater runoff is directed into the basins and is either absorbed and distributed with
residuals or dewatered and added to the process water system
V. RESIDUALS SOURCE INFORMATION: (Not required if no new, renewed, or modified residuals source)
Complete and submit the attached Residuals Source Certification and all associated documentation.
Residuals Source
Certification
FORM: DCAR 11-13 Page 2 of 3

Professional Engineer's Certification: (Application Involving New or Changes to Treatment or Storage Units)
attest that this application for
has been reviewed by me and is accurate and complete to the best of my knowledge. I further attest that to the best of my knowledge
the proposed design has been prepared in accordance with the applicable regulations. Although certain portions of this submittal
package may have been developed by other professionals, inclusion of these materials under my signature and seal signifies that I
have reviewed this material and have judged it to be consistent with the proposed design.
North Carolina Professional Engineer's Seal, Signature, and Date:
Applicant's Certification:
The applicant or any affiliate has not been convicted of an environmental crime, has not abandoned a wastewater facility without
proper closure, does not have an outstanding civil penalty where all appeals have been exhausted or abandoned, are compliant with
any active compliance schedule, and do not have any overdue annual fees under Rule 15A NCAC 02T .0105.
I,
Yes El No, Explain;
(Signature Authorityts Name — PLEASE PRINT) (Title)
attest that this application for Baxter Healthcare North Cove Steam Generation Plant
(Facility Name)
has been reviewed by me and is accurate and complete to the best of my knowledge. I understand that the Division of Water
Resources may not conduct a technical review of this program and approval does not constitute a variance to any rules or statutes
unless specifically granted in the permit. Further, any discharge of residuals to surface waters or the land will result in an immediate
enforcement action, which may include civil penalties, injunctive relief, and/or criminal prosecution. I will make no claim against the
Division of Water Resources should a condition of this permit be violated. I also understand that if all required parts of this
application are not completed and that if all required supporting information and attachments are not included, this application
package will be returned to me as incomplete.
Note: In accordance with North Carolina General Statutes § 143-215.6A and § 143-215.6B, any person who knowingly makes any
false statement, representation, or certification in any application shall be guilty of a Class 2 misdemeanor, which may include a fine
not to exceed $10,000 as well as civil penalties up to $25,000 per violation.
Signature: Date: M//
FORM: DCAR 11-13 Page 3 of 3

State of North Carolina
Department of Environment and Natural Resources
Division of Water Resources
Divislon of Water Resources RESIDUALS SOURCE CERTIFICATION
INSTRUCTIONS FOR -FORM: RSC 11-13
Please use the following instructions as a checklist in order to ensure all required items are submitted. Adherence to these
instructions and checking the provided boxes will help produce a quicker review time and reduce the amount of additional
information requested. Failure to submit all of the required items will lead to additional processing and review time for the
permit application. Unless otherwise. noted, the Applicant shall submit one original and two copies of the application and
supporting documentation
For more information, visit the Water Quality Permitting Section's Non -Discharge Permitting Unit website at.,
http: //portal. ncdenr. org/weblwg/apsllau
General — This certification provides detailed information of residuals source generating facility and its residuals quality for land
application, distribution, or disposal in accordance with 15A NCAC 02T .1100. Do not submit this certification for review without
a corresponding application form (FORM: RLAP 11-13, FORM: DCAR 11-13, or FORM: SDR 11-13).
Unless otherwise noted, the Applicant shall submit one original and two copies of the application and supporting documentation listed
below.
A. Residuals Source Certification (FORM: RSC 11-13):
® Submit the completed and appropriately executed Residuals Source Certification (FORM: RSC 11-13) form. Please do not
make any unauthorized content changes to this form. If necessary for clarity or due to space restrictions, attachments to the
application may be made, as long as the attachments are numbered to correspond to the section and item to which they refer.
® For new or renewed permits, submit a separate certification for each source -facility.
❑ For.inodified permits, submit a separate certification for only those facilities that are affected by the proposed modification.
® Complete the residuals source facility summary page. List all new, renewed, or modified facilities.
B. Residuals Source -Generating Facility Information:
® For each source facility, attach the following:
® Vicinity map - A vicinity map that shows the location of the facility and meets all of the criteria in the "Map Guidance for
Residuals Land Application Permits".
Z -Process flow diagram and/or narrative - A detailed narrative and/or process flow diagram that describes how the residuals
are to be generated, treated, processed, and stored at the facility.
❑ Quantitative justification for residuals production rate - A quantitative justification for the value provided in Item 1. 8.
Ensure that the amount of residuals listed is the maximum amount expected to be generated by the facility for the life of
the permit. In addition, ensure that, this amount is equivalent to that which is actually to be land applied, distributed,
and/or disposed, including any chemicals, amendments, or other additives that are added to the residuals during
processing.
® Sampling plan - A detailed sampling plan for the residuals source -generating facility., Ensure that the plan identifies
sampling points, sampling frequency, sample type, as well as the Division -certified laboratory to -be used. In addition,
ensure that the plan details how the facility and/or the residuals are monitored for any applicable pathogen reduction and
vector attraction reduction requirements. Note that all sampling and monitoring must be completed on the residuals as
they are to be land applied, distributed, and/or disposed.
C. Residuals Quality Information:
® For each source facility, attach the following:
Z Laboratory analytical reports and operational data - reports for all laboratory analyses used to complete this certification.
0 Documentation that the facility complies and/or the residuals comply with any applicable pathogen reduction and vector
attraction reduction requirements.
❑ For new facility that may have not yet been constructed and analytical results of residuals cannot be obtained, please
attach analytical results of residuals generated from a similar facility along with the 'description of similarities of the two
facilities.
INSTRUCTIONS FOR FORM: RSC 11-13 Page 1 of 1

RESIDUALS SOURCE FACILITY SUMMARY
Applicant's name:
Status
Code'
Facility Permit Holder
Facility Name
County
Permit Number
Maximum Dry Tons Per Year
Current b
Proposed
R
Baxter Healthcare
Corporation
North Cove Steam-
Generation Plant
-
McDowell
WQ0010689
3200
3200
a Status Code for source facility are: ♦ N (New) ♦ R (Renewed) s M (Modified) ♦ D (Deleted)
b The amount of residuals currently permitted for distribution, land application, or disposal (i.e, not applicable to new facility).
SUMMARY FOR FORM: RSC 11-13 Page 1

State of North Carolina
Department of Environment and Natural Resources
Division of Water Resources
[vision of Water Resources RESIDUALS SOURCE CERTIFICATION
FORM: RSC 11-13
I. RESIDUALS SOURCE -GENERATING FACILITY INFORMATION (See Instruction.B.):
1. Facility Name: North Cove Steam Generator Plant
2: Facility permit holder is: 0, Federal, Ej State; [ Local'Government, or Private.
Facility permit issued by: Div. of Water Resources, Div. of Environmental Health,
or Other (explain .
3. Facility contact person and title: Rick Styles, Wood Boiler Superintendent
Complete mailing address: 65 Pitt Station Rd.
City: Marion State: NC
Zip: 28752
Telephone number: 828 756-6650 E-mail address: ricky stylesaa,baxter.com.
4. Facility physical address: 2859 Old Linville Rd.
City: Marion State: NC Zip: 28752-
Coordinates: Latitude: 350 50' 5" Longitude: 81' 59' 40.7"
Datum: Level of accuracy:
Method of measurement: GooQle Earth
5. Purpose of the facility:
treatment of municipal wastewater, treatment of 100% domestic wastewater,
treatment of potable water, treatment of 100% industrial wastewater,
treatment of industrial wastewater mixed with domestic wastewater,
(approximate percentages: % industrial and %,domestic)
other (explain: ).
6. Does the facility have an approved pretreatment program: Yes No
7. Facility permitted/design flow: 0.72 MGD and facility average daily flow: 0.72 MGD
8. Average amount of residuals being generated at this facility 1600 dry tons per year:
9. Specify the following regarding,treatment•and storage volumes available at the facility:
Type and volume of residuals treatment: 1600 ton ash
Type and volume of residuals storage (i.e., outside of residuals treatment units): 1600 ton ash
H. RESIDUALS QUALITY INFORMATION (See.Instruction C.):
1. Specify if residuals are regulated under:,
40 CFR Part 5.03 ' or 40 CFR Part 257.
Note: Only residuals that are generated during domestic/municipal wastewater treatment processes are'regulated under 40
CFR Part 503, otherwise, the residuals are regulated under 40 CFR Part 257.
2. Specify if residuals are defined under 15A NCAC 02T.1102(6) as:
l( Biological Non -Biological
Note: Biological residuals are residuals that have been generated •during the treatment of domestic wastewater, animal
processing wastewater, or the biological treatment of industrial wastewater (biological treatment is a system that utilizes,
biological processes including lagoons, activated sludge systems, extended aeration systems, and fixed film systems).
FORM: RSC 11-13 Page 1 of 5

3. Hazardous Waste' Determination: Complete the following to demonstrate that the residuals are non -hazardous under
RCRA: (Note - this item does not have to be completed for facilities that are less than 0.5 MGD in design flow that treat
100% non -municipal, domestic wastewater only)
a.. Are the residuals listed in 40,CFR,§261..3l-§26l.33: [] yes M no.
If yes, list the numbers)
b. Specify whether or not the residuals exhibit any of the characteristics defined by 40 CFR §261.21
261.24: yes no.
Fill in the following tables with the results of the latest toxicity characteristic leaching procedure (TCLP) analysis as
well as those for corrosivity, ignitability, and reactivity:
Laboratory: Pace Analytical Services and Date of analysis: 7/1/11
Passed corrosivity test: 0, yes no. pH: s.u. (2 < pH < 12.5)
Passed ignitability test: [D yes. no. Flashpoints >1.40 °F (> 140T)
Passed reactivity test:' Oyes no. HCN: ND mg/kg (<250) & H2S: ND mg/kg (<500)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
TCLP Parameter
Limit
(mg/1)
Result
(mg/1)
Arsenic
5.0
ND
Hexachlorobenzene
0.13
ND
Barium
100.0-
1.1
Hexachloro-1,3-Butadiene
0.5
ND
Benzene
0.5
ND
Hexachloroethane
3.0
ND
Cadmium
1.0
.037
Lead
5.0
ND
Carbon Tetrachloride
0.5
ND
Lindane
0.4
ND
Chlordane
0.03
ND
Mercury
0.2
ND
Chlorobenzene
100:0
ND
Methoxychlor
10.0
ND
Chloroform
6.0
ND
Methyl Ethyl Ketone
200.0
ND
Chromium
5.0
ND
Nitrobenzene
2.0
ND
m-Cresol
200.0
ND
Pentachlorophenol
100.0
ND
o-Cresol
200:0
ND
Pyridine
5.0
ND
p-Cresol
200.0
ND
Selenium
1.0
ND
Cresol
200.,0 A
Silver
5.0
ND
2,4-D
10.0
ND
Tetrachloroethylene
0.7
ND
1,4-Dichlorobenzene
7.5
ND
Toxaphene
.0.5 ,
ND
1,2-Dichloroethane
0.5
ND
Trichloroethylene
0.5
ND
1,1-Dichloroethylene
0.7
ND
2,4,5-Trich1orophenol
400.0
ND
2,4-Dinitrotoluene
0.13
ND
2,4,6-Trichlorophenol
2.0
ND
Endrin
0.02'
ND
2,4,5-TP (Silvex)
1.0
ND
Heptachlor and'its Hydroxide
0.008
'ND
Vinyl Chloride
• 0.2
ND
FORMc RSC 11-13 Page 2 of 5

4. Metals Determination: Complete one of the following tables (i.e., as applicable) to demonstrate that the residuals do not
violate the ceiling concentrations for metals regulated under 15A NCAC 02T .1105.
a. For Distribution/Land Application: Fill in the following table with.the results of the latest analyses (i.e., on a dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services and Date of analysis: 8/23/13
Parameter
Ceiling
Concentration Limits
(ClassA & C1assB)
(mg/kg)
Monthly Average
Concentration Limits
(Class A Only)
(mg/kg)
Result
(mglkg)
Arsenic
75
41
9.1
Cadmium
85,
39
1.9
Copper
4,300
1,500
75
Lead
840
300
22.6
Mercury
57
17
ND'
Molybdenum
75
n/a
1.6
Nickel
420
420
20.6
Selenium
100
100
ND
Zinc
7,500
2,800 .
197
b. For Surface Disposal Unit`(landfill): Fill in the following table with the results of the latest analyses (i.e., ona' dry weight
basis) for the following metal parameters:
Laboratory: Pace Analytical Services and Date of analysis: 8/24/13
Distance froin Disposal
Unit to Boundary to '
Closest Property Line
(meters, check one)
Arsenic
(mg/kg)
Chromium.
(mg/kg)
Nickel
(mg/kg)
�I > 0 but < 25
30
200
210
> 25 but < 50
34'
220
240
> 50 but < 75
39
260
270
> 75 but < 100
46
300
320
> 100 but < 125
53
360
390
> 125
62
450
-420
Result (mg/kg)
9.1
26.4
20.6
FORM: RSC 11-13 Page 3 of 5

5. Nutrient/Micronutrient Determination: Complete the following:
a. Total solids: 49.2 %.
b. Fill in the following table with the results of the latest analyses (i.e., on a dry weight basis) for the following nutrient and
micronutrient parameters:
Laboratory: Pace Analytical Services and Date of analysis: 8/28/13
Parameter
Result
(mg1kg)
Aluminum
Ammonia -Nitrogen
Calcium
84200
Magnesium
12900
Nitrate -Nitrite Nitrogen
pH (Standard Unit)
9.1
Phosphorus
3070
Potassium
21600
Sodium
6040
Total Kjeldahl Nitrogen
c. Using the results listed in Item II. 5b. above, calculate the sodium adsorption ration (SAR):
[Note: If residuals contain SAR of 10 or higher, the applicant shall obtain recommendations from the local Cooperative
Extension Office, the Department of Agriculture and Consumer Services, the Natural Resource Conservation Service, a
North Carolina Licensed Soil Scientist, or an agronomist, prior to land application of residuals. The recommendations shall
address the sodium application rate, soil amendments (e.g., gypsum, etc.), or a mechanism for maintaining site integrity
and conditions conducive to crop growth].
d. Specify the mineralization rate to be used in calculating the plant available nitrogen (PAN) of the residuals:" %.
This rate is a (check one): [ default value, or actually established.
If the residuals are not generated from the treatment of municipal or domestic wastewater, explain or provide technical
justification as to why the selected default value is appropriate to be applied to these residuals: F7
e. Calculate the PAN for the residuals (i.e., on a dry weight basis) and fill the results in the following table:
Application Method
First (1') Year PAN
Five -Year
(mg�g)
Maximum Adjusted PAN
(mg/kg)
Surface
Injection/Incorporation
6. Other Pollutants Determination: Specify whether or not there are any other pollutants of concern in the residuals and provide
the results of the latest analyses: =
FORM: RSC 11-13 Page 4 of 5

7. Pathogen Reduction: Per 15A NCAC 02T.1106, specify how residuals will meet the pathogen reduction requirements:
a. For Distribution/Land Application of Class A or Equivalent:
A fecal coliform density that is demonstrated to be less than 1,000 MPN per gram of total dry solids,
or
A salmonella sp. density that is demonstration to be less than 3 MPN per 4 grams of total dry solids.
AND one of the followings (except for non -biological residuals):
Alternative 1 [15A NCAC 02T.I 106(b)(3)(A)] - Time/Temperature Compliance.
Alternative 2 [15A NCAC 02T. 1 106(b)(3)(B)] -Alkaline Treatment.
]; Alternative 3 [15A NCAC 02T.I 106(b)(3)(C)] - Prior Testing for Enteric Virus/Viable Helminth Ova.
Alternative 4 [15A NCAC 02T.I 106(b)(3)(D)] - No Prior Testing for Enteric Virus/Viable Helminth Ova.
�] Alternative 5 [15A NCAC 02T.1106(b)(3)(E)-(K)] - Process to Further Reduce Pathogens (PFRP).
Specify one: composting, heat drying,] heat treatment,
thermophilic aerobic digestion, beta ray irradiation,
gamma ray irradiation, or pasteurization.
b. For Land Application of Class E:
[ J Alternative 1 [15A NCAC 02T.1106(c)(1)] -Fecal Coliform Density Demonstration.
li Alternative 2 [15A NCAC 02T.I 106(c)(2)] - Process to Significantly Reduce Pathogens (PSRP).
Specify one: aerobic digestion, air drying, []: anaerobic digestion,
composting, or lime stabilization.
c. For Surface Disposal:
Select One of the Class A or Equivalent Pathogen Reduction Alternatives in Item II. 7a. above.
Select One of the Class B or Equivalent Pathogen Reduction Alternatives in Item H. 7b. above.
Exempt - If Daily Cover Alternative is chosen in Item II.8. below [15A NCAC 02T.I 106(a)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
8. Vector Attraction Reduction (VAR): Per 15A NCAC 02T.1107, specify how residuals will meet the VAR requirements:
EJ Alternative 1 [15A NCAC 02T.1107(a)(1)] - 38% Volatile Solids Reduction (Aerobic/Anaerobic Digestion).
(' Alternative 2 [15A NCAC 02T. 1 107(a)(2)] - 40-Day Bench Scale Test (Anaerobic Digestion).
Alternative 3 [15A NCAC 02T.I 107(a)(3)] - 30-Day Bench Scale Test (Aerobic Digestion).
Alternative 4 [15A NCAC 02T. 1 107(a)(4)] - Specific Oxygen Uptake Rate Test (Aerobic Digestion).
Alternative 5 [15A NCAC 02T.I 107(a)(5)] - 14-Day Aerobic Processes.
Alternative 6 [15A NCAC 02T.I 107(a)(6)] - Alkaline Stabilization.
EJ Alternative 7 [15A NCAC 02T.I 107(a)(7)] - Drying of Stabilized Residuals.
Alternative 8 [15A NCAC 02T.I 107(a)(8)] - Drying of Unstabilized Residuals.
Alternative 9 [15A NCAC 02T. I 107(a)(9)] - Injection.
Alternative 10 [15A NCAC 02T. I 107(a)(1 0)] - Incorporation.
0. Alternative for Surface Disposal Units Only - Soil/Other Material Cover [15A NCAC 02T.I 107(b)(2)].
Not Applicable - Non -Biological Residuals with NO Domestic Wastewater Contribution.
Note: For animal processing residuals, only alternatives 9 or 10 may be chosen due to the nuisance conditions that typically
occur when these residuals are applied and left on the land surface.
FORM: RSC 11-13 Page 5 of 5

Baxter Healthcare
Permit Renewal Application: WQ0010689
Form DCAR 11-13
D. Program Information
Narrative: Residual ash solids are collected and treated in the same location. Process water is pumped
into one of two settling basins where the ash and water are separated. The water is drained from the
basin and pumped back into the emissions control process. When ash sludge reaches a sufficient depth,
the basin is taken out of service and drained of free liquid to the extent practicable. The remaining
residuals are further dewatered by mixing in wood flour and/or saw dust inside the basin using a loader
or similar piece of equipment. Dewatered material may be stored. in the basin or on the concrete apron
at the entrance to the basin to ensure any leachate drains back into one of the two basins and is ether
dewatered or returned to the process. A representative sample of the dewatered material is then
tested for metals, pH, and nutrient concentrations. Once the material is characterized, is loaded from
the basin or storage pile into trucks with a loader or similar equipment. Both calcium and phosphorus
concentrations are provided in the analytical data. The general application rate is three to four units by
weight of ash material for every one unit of agricultural lime recommended based on soil testing.
Marketability Statement: Baxter Healthcare anticipates production of less than 3,200 dry tons of ash
per year. Ash production for RY13 was approximately 1,576 dry tons. All ash residuals were distributed
to local recipients in accordance with Permit WQ0010689 for land application with the intended use of
agricultural soil improvement. Baxter anticipates similar activities during the next permit cycle.
1of1

Baxter Healthcare
Permit Renewal Application: WQ0010689
Ash Distribution Program O&M Plan
1. Maintenance Records: All scheduled maintenance, calibrations, and work orders are recorded
and managed through MAXIMO, a web based maintenance management and database system.
2. Safety: All personnel will receive instruction on assigned standard work, to include common and
special tasks, hazards present, and required PPE, in accordance with Baxter safety policy.
3. Storage and Handling:
a. All ash will be stored in the basins or on the apron in such a way that prevents runoff
prior to distribution and use to prevent contamination of surface waters. During dry
conditions, operators will spray water on stock piles to prevent wind erosion.
b. Handling and loading is conducted in the basin/apron area. Operators avoid creating
nuisance dust to the extent practicable.
c. Ash Distribution Program Information Sheets will be distributed to each receiver of ash
material outlining transport, storage, and application requirements.
4. Spill Response:
a. SPCC and SWPPP are incorporated in the corresponding plans for the overall plant.
5. Inspections:
a. Current Wood Boiler Superintendent is Rick Styles.
b. The Wood Boiler Superintendent is overall responsible for all inspections; however, he
may delegate inspections to operators. A visual inspection of both basins, ash storage
piles, and associated piping is performed at least once per day mechanical malfunctions,
operator errors, and discharges which may cause or lead to the release of waste to the
environment. A log is kept of all monthly inspections which include the date and time,
name of inspector, observations, and any corrective actions taken. Inspection forms are
kept with the Title V documentation. All maintenance work orders are recorded in
MAXIMO.
c. If non-compliance is discovered, personnel will follow instructions outlined in the plant
SPCC and/or SWPP plans.
6. Sampling and Monitoring:
1of2

Baxter Healthcare
Permit -Renewal Application: WQ0010689
a. The Wood Boiler Superintendent is overall responsible for the sampling and monitoring
program.
b. Composite samples are taken of material offered for shipment composed of
representative samples at different locations in the storage pile.
c. Samples are tested to demonstrate the material offered for shipment is non -hazardous
according to the Resource Conservation and Recovery Act (RCRA). All material offered
for shipment undergoes the following testing.
i. Full Toxicity Characteristics Leaching Procedure (Full TCLP ICP) once per permit
cycle.
ii. Total Metals from each basin cleaning
iii. TCLP Metals from each basin cleaning
iv. pH Corrosivity from each basin cleaning
d. Records of all ash distribution activities and sample results are maintained in the Wood
Boiler Superintendent's office.
7. Contact Information:
Wood Boiler Superintendent: Rick Styles 828-756-6650
Environmental Engineer: Mike Pisarik 828-756-6017
Plant Manager: John Weiler 828-756-6530
2 of 2

Baxter Healthcare,, Corp.
2859 Old Linville,Road
Marion, North -Carolina 28752
Ash Distribution Program Information Sheet — Return this sheet to Ricky Styles
Baxter 'Healthcare, Corp., is the generator of the-ash..provided to.
(Recipient). Application of the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport. Adequate provisions shall be .taken -to ensure that the transportation of ash does not cause
nuisances and, hazards to public health and safety or otherwise cause an adverse impact (e:g., transport
wet ash in leak -proof trucks or cover dry ash).
Storage: The ash shall be adequately stored to prevent wind erosion or surface runoff from carrying- ash
into any surface waters. Keeping the ash slightly •moistened will accomplish this objective under normal
conditions. However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The, ash application rates shall be. -limited to those that can be agronomically justified- (i.e., limited to
that needed to meet the liming requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one, foot of the seasonal, high water. table.
• Ash- shall not be placed within 1.00. feet of any water supply well -or spring unless underlain and
overlain by a liner with a.maximum hydraulic conductivity.of -10 1 centimeters .per second. If such a
liner/cover is provided, ash shall. not be.placed within 25 feet of any water supply well or spring.
• The ash shall not be applied -to any site that is flooded, frozen; or;snow-covered.
A summary of the ash chemical analyses is located on page '2 of the informatiow.sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from. Baxter Healthcare, Corp. to. Recipient upon delivery thereof. Thereafter,
Baxter Healthcare, Corp will have no responsibility and shall not be held liable by Recipient or any third
party for any spill, misuse, misapplication or other, mishandling of the ash: -Recipient acknowledges and
agrees that the ash is being delivered by Baxter Healthcare, .Corp to Recipient. as an, accommodation to
Recipient. In exchange therefore, Recipient agrees to indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any,and all liability, damage,.loss;,cost, expense (including: attorneys.'. fees),
claim, demand, suit, action, judgment or recovery asserted against Baxter, Healthcare, Corp by any third
party, including any governmental authority, whether for bodily injury (including death) or damage ,to
property, arising from or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient): Date:
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr:
Page 1 of 3
Updated: 3/5/12
Acres of Land:

Baxter Healthcare, Corp.
2859, O1d.Lin,%Ue_ -Road
Marion, -North Carolina18752
Ash.Distribution Program Information Sheet — Land OwneuCopy
Baxter Healthcare, Corp., is the generator- of the ash provided to
(Recipient).,, Application of - the aforementioned ash is prohibited except in accordance with the
instructions on this sheet.
Transport: Adequate provisions shall be taken to ensure that the transportation of ash does not cause
nuisances and hazards to public health and safety or otherwise cause an adverse impact (e.g., transport
wet ash in leak -proof trucks or cover dry ash). .
Storage: The ash shall be adequately stored to prevent wind erosion or surface -runoff from carrying ash
into'any.surface waters. Keeping the ash slightly moistened will accomplish this objective under normal
conditions: -However, berms, barriers, or tarps, may be necessary under windy or rainy conditions or if
erosion or runoff cannot be controlled.
Application: When using ash, the following shall apply:
• The -ash application rates shall be'limited to those that can be agronomically justified (i.e., limited to
that needed to meet the liming: requirements of the crops being grown on the land).
• Ash shall not be placed within 50 feet of any surface water.
• Ash shall not be placed within one foot of the seasonal high water table.
• Ash shall not be placed within 100 feet of any water- supply well or spring unless underlain and
overlain by a liner. with a maximum hydraulic conductivity of 10-6Centimeters per second. If such a
liner/cover is provided, ash shall -not be placed within 25 feet of any water supply well or spring.
• The ash shall not be applied to any site that is flooded, frozen, or snow-covered.
A summary ,of the: ash chemical analyses is located on page 2 of the information sheet. Detailed
laboratory results are available upon request.
Title to the ash will transfer from Baxter Healthcare, Corp to .Recipient upon delivery- thereof. Thereafter,
Baxter. Healthcare, :Corp willhave no,responsibility and shall mot be held liable by Recipient or any third
party for any spill, misuse, misapplication or other mishandling,of the ash. Recipient acknowledges and
agrees. that the ash is being: delivered by Baxter- Healthcare, Corp to Recipient as an accommodation :to
Recipient. In exchange therefore, Recipient agrees,to. indemnify, save and hold Baxter Healthcare, Corp
harmless from and against any and all liability, damage, loss, cost, expense (including attorneys' fees),
claim, demand, suit;,action, judgment or recovery asserted against Baxter Healthcare; Corp by any third
party; including ,any governmental authority, whether for bodily 'injury (including death) or damage to
property, arisingfrom or in connection with Recipient's receipt, transportation, handling or other use of
the ash.
Signed (Ash Recipient):
Ash Recipient's Address:
Intended Use of Ash:
Expected Qty/Yr:
Page 2 of 3
Updated: 3/5/12
Date:
Acres of Land:

Marion, North Carolina
Ash Distribution Program
Historical Analysis Average
Soil Amendment Properties
Parameter
Concentration
Calcium Carbonate Equivalent
42.0%
Potash (K2O)
3.6%
20-Mesh %
85.4%
100-Mesh %
44.7%
Metals (6010 MET ICP, EPA 6010)
Parameter
Concentration (mg/W
Arsenic
33.0
Barium
1,030
Cadmium
2.4
Calcium
63,500
Chromium
44.8
Copper
135
Lead
53.1
Magnesium
10,400
Manganese
2,450
Mercury
Less than 0.014
Nickel
21.3
Nitrogen
480
Phosphorus
1,600
Potassium
11,300
Selenium
Less than 0.092
Silver
0.37
Sodium
6,700
Zinc
100
TCLP RCRA Toxicity Metals (Lecahable Concentrations)
Parameter
Concentration (mg/L)
Arsenic
0.083
Barium
2.1
Cadmium
0.025
Chromium
Less than 0.025
Lead
Less than 0.025
Mercury
Less than 0.20
Selenium
Less than 0.050
Silver
Less than 0.025
EPA 9045 ph 8.9 std. units
Page 3 of 3
Updated: 3/5/12

aceAnalyical
wivw,pacelabs.com
�ry
September 12, 2013
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville. NC 28078
[phone]
Dear Mr. Styles:
Enclosed are the analytical results for sample(s) received by the laboratory on August 23, 2013. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards and the laboratory's Quality Assurance Manual, where applicable, unless
otherwise noted in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
Some analyses have been subcontracted outside of the Pace Network. The subcontracted
laboratory report has been attached.
If you have any questions concerning this report, please feel free to. contact me.
Sincerely,
Tom Williams
[e-mail]
Project Manager
Enclosures
�� of
o REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
9ewithout the written consent of Pace Analytical Services, Inc..
Page 1 of 16

acmnalXical
www.pacWabs.com
1
e
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Charlotte Certification IDS
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
South Carolina Certification M 99006001
Asheville Certification IDs
2225 Riverside Dr., Asheville, NC 28804
Florida/NELAP Certification #: E87648
Massachusetts Certification #: M-NC030
North Carolina Drinking Water Certification #: 37712
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Florida/NELAP Certification #: E87627
Kentucky UST Certification #: 84
West Virginia Certification #: 357
Vrginia/VELAP Certification #: 460221
North Carolina Wastewater Certification #: 40
South Carolina Certification M 99030001
West Virginia Certification #: 356
Vrginia/VELAP Certification #: 460222
REPORT OF LABORATORY ANALYSIS
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 2 of 16

anelftlj fecal
r www.pacelabs.com
t
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Lab ID Sample ID Method
Analysts
Analyses
Reported
Laboratory
92169897001 SP82313 ASH EPA 6010
JMW
17
PASI-A
EPA6010
JMW
7
PASI-A
EPA7470
SH1
1
PASI-A
EPA 7471
MTS
1
PASI-A
ASTM D2974-87
TNM
1
PASI-C
EPA 9045
AES2
1
PASI-A
EPA 365.1
JDA
1
PASI-A
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc.. Page 3 of 16

WeAnaljftal
WMpacelabacem
r
i
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205-East Meadow'Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 leincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Sample: SP82313 ASH Lab ID: 92169897001 Collected: 08/23/13 12:35 Received: 08/23/13 14:07 Matrix: Solid
Results reported on,a "dry -weight" basis
Parameters 'Results Units Report Limit DF Prepared Analyzed CAS'No. Qual
6.010 MET ICP Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
9.1 mg/kg
1.8
1
08124113141:30 08/25/13 17:13 7440-38-2
Barium
1300 mg/kg
0.91
1
08/24/13 14:30 08/25/13' 17:13 7440-39-3
Cadmium
1.9 mg/kg
0.18
1
08/24/13 14:30 08/25/13 17:13 7440-43-9
Calcium
84200 mg/kg
182
10
08/24/13 14:30 08/26/13 14:59 7440-70-2
Chromium
26.4 mg/kg
0.91
1
08/24/13 14:30 08/25/13 17:13 7440-47-3
Copper
75.0 mg/kg
0.91
1
08/24/13 14:30 08/25/13 17:13 7440-50-8
Iron
10700 mg/kg
18.2
1
08/24/13 14:30 08/25/13 17:13 7439-89-6
Lead "
22.6 mg/kg
0.91
1
08/24/13 14:30 08/25/13 17:13 7439-92-1
Magnesium
12900 mg/kg
18.2
1
08/24/13 14:30 08/25/13 17:13 7439-95-4
Manganese
2670 mg/kg
9.1
10
08/24/13 14:30 08/26/13 14:59 7439-96-5
Molybdenum
1.6 mg/kg
0.91
1
08/24/13 14:30 08/25/13 17:13 7439-98-7
Nickel
20.6 mg/kg
0.91
1
08/24/13 14:30 08/25/13 17:13 7440-02-0
Potassium
21600 mg/kg
9100
10
08/24/1314:30 08/26/13 14:59 7440-09-7
Selenium
ND mg/kg
1.8
1
08/24/13 14:30 08/25/13 17:13 7782-49-2
Silver
0.93 mg/kg
0.91
1
08/24/13 14:30 08/2511317:13 7440-22-4
Sodium
6040 mg/kg
910
1
08/24/13 14:30 08/26/13 14:41 7440-23-5
Zinc
197 mg/kg
1.8
1
08/24/13 14:30 08/25/13 17:13 7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA 1311; 08/28/13 16:55
Arsenic
ND mg/L
0.050
1
08/29/13 14:25 08/30/13 13:54 7440-38-2
Barium
3.5 mg/L
0.25
1
08/29/13 14:25 08/30/13 13:54 7440-39-3
Cadmium
ND mg/L
0.0050
1
08/29/13 14:25 08130/1313:54 7440-43-9
Chromium
ND mg/L
0.025
1
08/29/13 14:25 08/3011313:54 7440-47-3
Lead
ND mg/L
0.025
1
08/29/13 14:25 08/30/13 13:54 7439-92-1
Selenium.
ND mg/L
0.10
1
08/29/13 14:25 08/3011313:54 7782-49-2
Silver
ND mg/L
0.025
1
08129/13 14:25 08/30/13 13:54 7440-22-4
7470 Mercury, TCLP
Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 08/28/1316:55
Mercury
ND ug/L
0.20
1
08/29/13 17:15 08/30/1312:08 7439-97-6
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
ND mg/kg
0.0057
1
08/30/13 17:55 09/04/13 12:07 7439-97-6
Percent Moisture
AnalyticalMethod: ASTM D2974-87
Percent Moisture
49.2 %
0.10
1
09/03/13 08:48
9045 pH Soil
Analytical Method: EPA 9045
pH at 25 Degrees C
9.1 Std. Units
0.10
1
08/27/13 11:35
365.1 Phosphorus, Total
Analytical Method: EPA 365.1
Phosphorus
3070 mg/kg
151
50
08/30/13 16:49 7723-14-0
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except' in full,
without the written consent of Pace Analytical.Services, Inc..
Page 4 of 16

aceAnalyfical
www.pacelabs.com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
QC Batch: MERP/5536
QC Batch Method: EPA 7470
Associated Lab Samples: 92169897001
METHOD BLANK: 1038327
Associated Lab Samples: 92169897001
Parameter Units
ug/L
Mercury
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 7470
Analysis Description: 7470 Mercury TCLP
Matrix: Water
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.20 08/30/1311:18
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28076
[phone]
LABORATORY CONTROL SAMPLE: 1038328
Parameter Units
Spike
Cone.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Mercury ug/L
2.5
2.4
94
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1038329
1038330
MS
MSD
92168869001
Spike
Spike MS
MSD
MS MSD % Rec
Parameter Units Result
Cone.
Cone. Result
Result
% Rec % Rec Limits RPD Qual
Mercury ug/L ND
2.5
2.5 2.3
2.2
90 89 75-125 2
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 5 of 16

ViceAnaljftal
nwww.paoelpbs.com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/5541 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 92169897001
METHOD BLANK: 1039489
Associated Lab Samples: 92169897001
Parameter Units
Mercury mg/kg
LABORATORY CONTROL SAMPLE: 1039490
Parameter Units
Mercury mg/kg
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 09/04/1311:41
Spike LCS LCS % Rec
Cone. Result % Rec Limits Qualifiers
.067 0.055 82 80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1039491 1039492
MS MSD
92169384001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Cone. Cone. Result Result % Rec % Rec Limits RPD Qual
Mercury mg/kg 0.52 .05 .05 0.49 0.58 -51 129 75-125 17 M6
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 16

acuAnaijdical
/ www.pacelabs.com
I
1
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/14056 Analysis Method: EPA6010
QC Batch Method: EPA 3050 Analysis Description: 6010 MET
Associated Lab Samples: 92169897001
METHOD BLANK: 1035357
Associated Lab Samples: 92169897001
Parameter Units
Matrix: Solid
Blank Reporting
Result Limit
Analyzed
Arsenic
mg/kg
ND
1.0
08/25/1316:17
Barium
mg/kg
ND
0.50
08125/1316:17
Cadmium
mg/kg
ND
0.10
08/25/1316:17
Calcium
mg/kg
NO
10.0
08125/1316:17
Chromium
mg/kg
ND
0.50
08/25/1316:17
Copper
mg/kg
ND
0.50
08/25/1316:17
Iron
mg/kg
ND
10.0
08/25/1316:17
Lead
mg/kg
ND
0.50
08/2511316:17
Magnesium
mg/kg
ND
10.0
08/25/1316:17
Manganese
mg/kg
ND
0.50
08/25/1316:17
Molybdenum
mg/kg
ND
0.50
08/25/1316:17
Nickel
mg/kg
ND
0.50
08/25/1316:17
Potassium
mg/kg
ND
500
08/25/1316:17
Selenium
mg/kg
ND
1.0
08/25/1316:17
Silver
mg/kg
ND
0.50
08/25/1316:17
E Sodium
mg/kg
ND
500
08/25/1316:17
Zinc
mg/kg
ND
1.0
08125/1316:17
Qualifiers
LABORATORY CONTROL SAMPLE:
Parameter
1035358
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits
Arsenic
mg/kg
50
46.0
92
80-120
Barium
mg/kg
50
46.3
93
80-120
Cadmium
mg/kg
50
47.4
95
80-120
Calcium
mg/kg
500
486
97
80-120
Chromium
mg/kg
50
47.9
96
80-120
Copper
mg/kg
50
44.8
90
80-120
Iron
mg/kg
500
471
94
80-120
Lead
mg/kg
50
47.2
94
80-120
Magnesium
mg/kg
500
478
96
80-120
Manganese
mg/kg
50
47.3
95
80-120
Molybdenum
mg/kg
50
47.7
95
80-120
Nickel
mg/kg
50
48.0
96
80-120
Potassium
mg/kg
600
451J
90
80-120
Selenium
mg/kg
50
46.7
93
80-120
Silver
mg/kg
25
23.5
94
80-120
Sodium
mg/kg
500
444J
89
80-120
Zinc
mg/kg
50
47.6
95
80-120
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Qualifiers
Page 7 of 16

ac"Analytical
www.pacslabs:com
i
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1035359 .
MS
92168447001 Spike
Parameter Units Result Conc.
MSD
Spike
Conc.
1035360
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD Qual
Arsenic
mg/kg
ND
48.1
45.5
43.3
42.1
90
93
75-125
3
Barium
mg/kg
1.1
48.1
45.5
44.3
43.1
90
92
75-125
3
Cadmium
mg/kg
ND
48.1
45.5
43.8
42.4
91
93
75-125
3
Calcium
mg/kg
25.3
481
455
470
461
93
96
75-125
2
Chromium
mg/kg
ND
48.1
45.5
44.3
43.2
92
95
75-125
3
Copper
mg/kg
1.7
48.1
45.5
44.1
43.0
88
91
75-125
3
Iron
mg/kg
5330
481
455
5540
5570
42
53
75-125
1 M1
Lead
mg/kg
ND
48.1
45.5
42.8
41.5
.88
90
75-125
3
Magnesium
mg/kg
ND
481
455
439
427
90
93
75-125
3
Manganese
mg/kg
15.6
48.1
45.5
59.1
58.4
91
94
75-125
1
Molybdenum
mg/kg
ND
48.1
45.5
43.8
43.0
91
94
75-125
2
Nickel
mg/kg-
ND
48.1
45.5
44.6
43.4
92
95
75-125
3
Potassium
mg/kg
ND
481
455
452J
440J
93
95
75-125
Selenium
mg/kg
ND
48.1
45.5
44.6
43.0
92
94
75-125
4
Silver
mg/kg
ND
24
22.7
22.1
21.5
92
95
75-125
3
Sodium
mg/kg
ND
481
455
445J
434J
85
87
75-125
Zinc
mg/kg
ND
48.1
45.5
45.4
44.4
93
96
75-125
2
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 16

ceAnlyficl
wWw.pBcelabs.eom
1
Project: WOOD BOILER ASH
Pace Project No.: .92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/14085 . Analysis Method: EPA 6010
QC Batch Method: EPA 3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples: 92169897001
METHOD BLANK: 1038184 Matrix: Water
Associated Lab Samples: 92169897001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Pace Analytical Services, Inc.
9800 Kinsey Ave. Suite 100
Huntersville, NC 28078
[phone]
Arsenic
mg/L
ND
0.050
08/30/1312:43
Barium
mg/L
ND
0.25
08/30/1312:43
Cadmium
mg/L
ND
0.0050
08/30/1312:43
Chromium,
mg/L
ND _
0.025
.08/30/1312:43
Lead
mg/L
ND
0.025
08/30/1312:43
Selenium
mg/L
ND
0.10
08/30/1312:43
Silver
mg/L
ND
0.025
0813011312:43
LABORATORY CONTROL SAMPLE: 1038185
Spike
LCS
LCS % Rec
Parameter
Units Conc.
Result % Rec Limits
Qualifiers
Arsenic
mg/L
2.5
2.7
107
80-120
Barium
mg/L
2.5
2.4
96
80-120
Cadmium
mg/L
2.5
2.3
94
80-120
Chromium
mg/L
2.5
2.4
96
80-120
Lead
mg/L
2.5
2.2
90
80-120
Selenium
mg/L
2.5
2.8
112
80-120
Silver
mg/L
1.2
1.3
103
80-120
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
1038186
1038187
MS
MSD
92168869001 Spike
Spike
MS
MSD MS MSD
% Rec
Parameter
Units Result Conc.
Conc.
Result
Result % Rec % Rec
Limits
RPD Qual
Arsenic
mg/L
ND 2.5
2.5
2.7
2.8
109
111
75-125
2
Barium
mg/L
ND 2.5
2.5
2.5
2.5
98
99
75-125
1
Cadmium
mg/L
ND 2.5
2.5
2.4
2.4
97
96
75-125
0
Chromium
mg/L
0.26 2.5
2.5
2.7
2.7
98
97
75-125
1
Lead
mg/L
ND 2.5
2.5
2.3
2.3
93
93
75-125
0
Selenium
mg/L
ND 2.5
2.5
2.8
2.8
111
112
75-125
1
Silver
mg/L
ND 1.2
1.2
1.3
1.3
106
106
75-125
0
REPORT OF LABORATORY ANALYSIS
This report shall
not be reproduced, except in full,
Date: 09/12/2013 12:32 PM
without the written consent of Pace Analytical Services, Inc..
Page 9 of 16

aceAna�yfial
WWW..paeslsbs;com.
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical -Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
QC Batch: PMST/5793 Analysis Method: - ASTM D2974-87
QC Batch Method: ASTM D2974-87 Analysis Description: Dry Weight/Percent Moisture
Associated Lab Samples: 92169897001
SAMPLE DUPLICATE: 1037730
92170134001 Dup
Parameter Units Result Result RPD Qualifiers
Percent Moisture % 22.2 19.6 12
SAMPLE DUPLICATE: 1037731
92170066006 Dup
Parameter Units Result Result ROD Qualifiers
Percent Moisture % 6.9 6.3 9
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 10 of 16

aceAnaljftal
www.pacelabs.com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QC Batch: WET/26852
QC Batch Method: EPA 9045
Associated Lab Samples: 92169897001
SAMPLE DUPLICATE: 1035948
Parameter Units
pH at 25 Degrees C Std. Units
Date: 012/2013 12:32 PM
QUALITY CONTROL DATA
Analysis Method: EPA 9045
Analysis Description: 9045 pH
92169844001 Dup
Result Result RPD Qualifiers
10.2 10.6 4 D6
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 11 of 16

aeeAnal%cal
/ »'ww+t�a4elabs.com
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY. CONTROL DATA
QC Batch: WETA/16309 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total
Associated Lab Samples: 92169897001
METHOD BLANK: 1038955 Matrix: Solid
Associated Lab Samples: 92169897001
Blank Reporting
Parameter Units Result Limit Analyzed Qualifiers
Phosphorus mg/kg ND 2.0 08/30/1315:48
Pace Analytical Services, Inc.
9800 Kincey Ave., Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE: 1038956
Spike LCS LCS % Rec
Parameter Units Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 50 49.5 99 90-110
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 1038957 1038958
MS MSD
92169068001 Spike Spike MS MSD MS MSD % Rec
Parameter Units Result Conc. Conc. Result Result % Rec % Rec Limits RPD Qual
Phosphorus mg/kg 6580 3970 6650 4640 5200 -49 -21 90-110 11 M6
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report.shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 12 of 16

aceAnalyflcal
www.paWabs.com
�f
Project: WOOD BOILER ASH
Pace Project No.: 92169897
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
ND - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
PRL - Pace Reporting Limit.
RL - Reporting Limit.
S -.Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes toAzobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
N-Nitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Acid preservation may not be appropriate for 2-Chloroethylvinyl ether, Styrene, and Vinyl chloride.
Pace Analytical is TN accredited. Contact your Pace PM for the current list of accredited analytes.
TNI - The NELAC Institute.
LABORATORIES
PASI-A Pace Analytical Services - Asheville
PASI-C Pace Analytical Services - Charlotte
ANALYTE QUALIFIERS
D6 The relative percent difference (RPD) between the sample and sample duplicate exceeded laboratory control limits.
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Date: 09/12/201312:32 PM without the written consent of Pace Analytical Services, Inc.. Page 13 of 16

e
acmnalytical
wmpaolabscom
f
i
Pace Analytical'Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA CROSS REFERENCE TABLE
Pace Analytical Services, Inc.
9B00 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project: WOOD BOILER ASH
Pace Project No.: 92169897
Analytical
Lab ID Sample ID QC Batch Method QC Batch Analytical Method Batch
92169897001
SP82313 ASH
EPA 3050
MPRP/14056
EPA 6010
ICP/12793
92169897001
SP82313 ASH
EPA 3010
MPRP/14085
EPA 6010
ICP/12823
92169897001
SP82313 ASH
EPA 7470
MERP/5536
EPA 7470
MERC/5364
92169897001
SP82313 ASH
EPA 7471
MERP/5541
EPA 7471
MERC/5366
92169897001
SP82313 ASH
ASTM D2974-87
PMST/5793
92169897001
SP82313 ASH
EPA 9045
WET/26852
92169897001
SP82313 ASH
EPA 365.1
WETA/16309
Date: 09/12/2013 12:32 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 14 of 16

Baxter Healthcare - Wood Boiler Ash - Ricky Styles
Please test the sample(s) for the parameters as
- listed below.
Send original results to: email: [e-mail] & [e-mail]
Send invoice and copy of results to: email: [e-mail]
Ricky Styles
Baxter Healthcare Purchase Order # To Be Faxed
2859 Old Linville Rd.
Marion, NC 28752
[phone]
Rnmip-.tari r]na nnfs%.
Cam. 1- Al 1 1 10TC11
Sample #
Sample
.Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
As, Ba, Cd,
Ca, Or, Cu, Fe,
TCLP Metals
As, Ba, Cd,
Cr, Pb, Hg,
Ignitability,
Reactivity
pH
Corrosivity
Total -Arsenic
Full TCLP
Pb, Mg, Hg,
Se, Ag
Mn, Mo, NI, K,
Se, Ag, Na,
Zn, total
Phos horus
SP82313
ASH
8-23-1312:35PM
COMPOSITE
YES
YES
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NO 28804
c 828-254-7176
Chain of Custody
0
o�
Project Manager: Tom Williams
9800 Kincey Avenue, Suite 10(
Huntersville, NO 28078
(704) 875 - 9092 ext. 233
1/01, �' :3 f-5 tf : 6 ?

r^e
LABORATORY REPORT
Client
Pace Analytical Services, Inc.
2225 Riverside Drive
Asheville, NC 28804
Order Number
1113186
Project Number
9297122
Issued
Monday, July 11, 2011
Total Number of Pages
4 (excluding C.O.C. and cooler receipt form)
Approved By: -44-Al
QA Manager
NELAC Accreditation #E87688
"Analytical Integrity - EPA,Certified - NELAP Certified
3310 Win Street • Cuyahoga Falls, Ohio 44223 • Phone: [phone] Fax: [phone]
Web Site: www.settek.com

2
Sample Summary
Client: Pace Analytical Services, Inc.
Order Number: 1113186
Laboratory ID Client ID Matrix Sampling Date
1113186-01 9297122001 Solid 6/28/2011
"Analytical Integrity - EPA Certified - NELAP Certified
3310 WIn Street - Cuyahoga Faits, Ohio 44223 1 Phone: [phone] . Fair: 330-253-4488
Web Site: www.settek.com

mot,
i/
4-1 .
Report Narrative
Client: Pace Analytical Services, Inc.
Order Number: 1113186
3
Solid sample results are .reported on a wet weight basis except as noted.
No problems were encountered during analysis of this order number, except as noted.
Data Qualifiers:
13 = Analyte found in the method blank
J = Estimated concentration of analyte between MDL (LOD) and Reporting Limit (LOQ)
C = Analyte has been confirmed by another instrument or method'
E = Analyte exceeds the upper limit of the calibration curve.
D = Sample or extract was analyzed at a higher dilution
X = User defined data qualifier.
S = Surrogate out of control limits
U = Undetected
a = Not Accredited by NELAC
ND = Non Detected at LOQ
OF = Dilution Factor
Limit Of Quantitation (LOQ) = Laboratory Reporting Limit (not adjusted for dilution factor)
Limit Of Detection (LOD) = Laboratory Detection Limit
Estimated uncertainty values are available upon request,
Matrices:
A=Air
C = Cream
DW = Drinking Water
L = Liquid
0 = Oil
SL = Sludge
SO Soil
S = Solid
T ='Tablet
TC = TCLP Extract
WW = Waste Water
W ="Wipe
The test results meet the requirements of the NELAC standard, except where noted. The information contained in
this analytical report is the sole property of Summit Environmental Technologies, Inc. and that of the client. It cannot
be reproduced in any form without the consent of Summit Environmental Technologies, Inc. or the client for which this
report was issued. The results contained. in this report are only representative of the samples received. Conditions
can vary at different times and at different sampling conditions. Summit Environmental Technologies, Inc. is not
responsible for use or interpretation of the data included herein.
"Analytical Integrity" - EPA Certified - NELAP Certified
3310 Win' Street - Cuyahoga Falls, Ohio 44223 o Phone;: 330-253-8211 - Fax: [phone]
Web Site: www.settek.com

July 11, 2011
Client: Pace Analytical Services, Inc.
Address: 2225 Riverside Drive
Asheville, NC 29804
Received:7/1/2011
Project #:9297122
Client M
Lab 1D#
Collected Analvte
Result
Units
Matrix Method
DF
LOCI
Rua Analyst
9297122001
1113186-01
28-Jun-11 Flash Point
>140
°F
S , 1010
1
06-Jul-11 DVW
Client 1D
Lab M#
Collected AnaLyte
Result
Units
Matrix Method
DF
LONG
Run Analyst
9297122001
1113186-01
28-1un-11 Reactive Cyanide
ND
mg/kg
S 7.3.3.2
1
0.5
06-Jul-11 1111
Client 1D'#
Lab M#
Collected Analte
Result
JI&
afrix Method
DF
LOQ
Run Anal s
9297122001
1113186-01
28-Jun-11 Reactive Sulfide
ND
mg/kg
S 7.3.4.2
1
25
06-Jul-11 TIR
Page 4
"Analytical Integrity" • EPA Certified - NEL.AP Certified
3310 Min Street • Cuyahoga Falls, Ohio 44223 Phone: [phone] • Fan: 330-253.4489
Web Site; www.sett6k.com

aceAnaly ml
www.pmkb&oam
July 15, 2011
Mr. Ricky Styles
Baxter Healthcare
2859 Old Linville Road
Marion, NC 28752
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
RE: Project: Wood Boiler
Pace Project No.: 9297122
Dear Mr. Styles:
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
Enclosed are the analytical results for sample(s) received by the laboratory on June 28, 2011. The
results relate only to the samples included in this report. Results reported herein conform to the
most current TNI standards, where applicable, unless otherwise narrated in the body of the report.
Analyses were performed at the Pace Analytical Services location indicated on the sample analyte
page for analysis unless otherwise footnoted.
If you have any questions concerning this report, please feel free to contact me.
Sincerely,
/�24 _
Tom Williams
[e-mail]
Project Manager
Enclosures
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
[phone]
Page 1 of 21

aceAnaiytical
Wmpam4a6s.cam
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
Ormond Beach Certification IDs
8 East Tower Circle,.Ornond Beach, FL 32174
Alabama Certification #. 41320
Arizona Certification #. AZ0735
Colorado Certification: FL NELAC Reciprocity
Connecticut Certification #. PH 0216
Florida Certification #. E83079
Georgia Certification #: 955
Guam Certification: FL NELAC Reciprocity
Hawaii Certification: FL NELAC Reciprocity
Kansas Certification #: E-10383
Kentucky Certification #: 90050
Louisiana Certification #: LA090012
Louisiana Environmental Certificate #: 05007
Maine Certification #. FL1264
Massachusetts Certification M M-FL1264
Charlotte Certification IDs
9800 Kincey Ave. Ste 100, Huntersville, NC 28078
Louisiana/LELAP Certification #: 04034
New Jersey Certification M, NC012
North Carolina Drinking Water Certification #: 37706
North Carolina Field Services Certification #: 5342
North Carolina Wastewater Certification #: 12
Pennsylvania Certification M 68-00784
South Carolina Certification #: 99006001
Asheville Certification lDs
2225 Riverside Dr., Asheville, NC 28804
Connecticut Certification #. PH-0106
Flodda/NELAP Certification t E87648
Massachusetts Certification M M-NC030
New Jersey Certification #: NC011
North Carolina Bioassay Certification M 9
North Carolina Drinking Water Certification M 37712
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
CERTIFICATIONS
Michigan Certification M 9911
Mississippi Certification: FL NELAC Reciprocity
Montana Certification 9. Cert 0074
Nevada Certification: FL NELAC Reciprocity
New Hampshire Certification * 2958
New Jersey Certification #: FL765
New York Certification #. 11608
North Carolina Environmental Certificate #: 667
North Carolina Certification #: 12710
Pennsylvania Certification #. 68-547
Puerto Rico Certification t FLO1264
Tennessee Certification #: TN02974
Texas Certification: FL NELAC Reciprocity
Virginia Certification #: 00432
Wyoming Certification: FL NELAC Reciprocity
South Carolina Drinking Water Cert. #: 99006003
Virginia Certification #. 00213
Connecticut Certification #. PH-0104
Flodda/NELAP Certification #: E87627
Kentucky LIST Certification #: 84
Louisiana DHH Drinking Water# LA 100031
West Virginia Certification #: 357
North Carolina Wastewater Certification P 40
Pennsylvania Certification #. 68-03578
South Carolina Bioassay Certification #. 99030002
South Carolina Certification P 99030001
Virginia Certification #: 00072
West Virginia Certification #: 356
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800 KinceyAve_ Suite 100
Huntersville, NC 28078
[phone]
Page 2 of 21

aceAnalytical
www.pacelabs.com
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
SAMPLE ANALYTE COUNT
Pace Analytical Services, Inc.
9800 Kincey Ave. Suite 100
Huntersville, NC 28078
[phone]
Project:
Pace Project No.:
Lab ID
Wood Boiler
9297122
Sample ID
Method
Analysts
Analytts
Reported
9297122001
North Pond #WBNP628
EPA 8081
BAG
9
EPA 8151
UM
3
EPA6010
SHB
17
EPA6010
SHB
7
EPA7470
JMW
1
EPA7471
JMW
1
EPA 8270
PPM
18
EPA 8260
DLK
15
ASTM D2974-87
KDF
1
EPA 9045
SAJ
1
EPA 365.1
JDA
1
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
A
Laboratory
PASI-O
PASI-0
PASI-A
PAST -A
PASI-A
PASI-A
PAST-C
PASI-C
PASI-C
PASI-A
PASI-A
Page 3 of 21

aceAnalytical
www.pacebbs.com
Project: Wood Boiler
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
ANALYTICAL RESULTS
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Pace Project No.: 9297122
Sample: North Pond SWBNP628 Lab ID: 9207122001 Collected: 06/28/11 08:30 Received: 06/28/11 09:25 Matrix: Solid
Results reported on a dry -weight" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. t1ua1
8081 GCS Pesticides, TCLP
Analytical Method: EPA 8081
gamma-BHC (Lindane)
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14 58-89-9
Chlordane (Technical)
ND mg/L
0.0050
1
07/08/11 15:27
07/08/11 17:14 57-74-9
Endrin
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14 72-20-8
Heptachlor
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14 76-44-8
Heptachlor epoxide
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14 1024-57-3
Methoxychlor
ND mg/L
0.0010
1
07/08/11 15:27
07/08/11 17:14 72-43-5
Toxaphene
ND mg/L
0.0050
1 .
07/06/11 15:27
07/08/11 17:14 8001-35-2
Decachlorobiphenyl (S)
66 %
70-130
1
07/08/1115:27
07/08/11 17:14 2051-24-3 S1
Tetrachlom-m-xylene (S)
76 %
70-130
1
07/08/11 15:27
07/08/11 17:14 877-09-8
8151 Chlorinate Herbicide TCLP .
Analytical Method: EPA 8151
2,4-D
ND mg/L
0.010
1
07/07/11 14:00
07/12/11 20:17 94-75-7
2,4,5-TP (Silvex)
ND mg/L
0.010
1
07/07/11 14:00
07/12/11 20:17 93-72-1 M1
2,4-DCPA (S)
94 %
70-130
1
07/07/11 14:00
07/12/11 20:17 19719-28-9
6010 MET ICP _ Analytical Method: EPA 6010 Preparation Method: EPA 3050
Arsenic
14.4 mg/kg
0.88
1
07112/11 11.40
07/13/11 14:18
7440-38-2
Barium
1350' �mg/kg
0.88
1
07/12/11111.40
07/13/11 14:18
7440-39�3
Cadmium
2.2 mg"
0.18
1
07/12/11 11:40
07/13/11 14:18
744043=9
Calcium
64200 mg/kg
175
10
07/12/11 11:40
07/13/11 16:15
7440-70-2
Chromium
26.1 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-47-3
Copper
92.4 mg/kg
0.88
1
07/12/11.11:40
07/13/11 14:18
7440-50-8
Iron
14300 mg/kg
17.5
1
07/12/11 11.40
07/13/11 14:18
7439-89-6
Lead
32.4 ,mg/kg
0.88
1
07/12/11 11.40
07/13/11 14:18
7439-92-1
Magnesium
13000 mg/kg
17.5
1
07/12/11 11.40
07/13/11 14:18
7439-95-4
Manganese
2410 mg/kg
8.8
10
07/12/11 11:40
07/13/11 16:15
743946-5
Molybdenum
5.1 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7439-98-7
Nickel
16A mg/kg
0.88
1
07/12/11 11'.40
07/13/11 14:18
7440-02-0
Potassium
15800 mg/kg
8760
10
07/12/11 11:40
07/13/11 16:15
7440-09-7
Selenium
ND mg/kg
1.8
1
07/12/1f 11:40
07/13/11 14:18
7782-49-2
Silver
0.93 mg/kg
0.88
1
07/12/11 11:40
07/13/11 14:18
7440-22-4
Sodium
12300 mg/kg
8760
10
07/12/,11 11:40
07/13/11 16:15
7440-23-5
Zinc
254 mg/kg
1.8
1
07/12/11 11:40
07/13/11 14.18
7440-66-6
6010 MET ICP, TCLP
Analytical Method: EPA 6010 Preparation Method: EPA 3010
Leachate Method/Date: EPA
1311; 07/07/11 18:05
Arsenic
ND mg/L
0.025
1
07/08/11 15:45
07/11/11 13.43
7440-38-2
Barium
1.1 mg/L
0.50
1
07/08/11 15:45
07/11/11 13:43
7440.39-3
Cadmium
0.037 mg/L
0.0050
1
07/08/11 15*45
07/11/11 13:43
7440-43-9
Chromium
ND mg/L
0.025
1
07/08/11 15:45
07/11/11 13:43
7440-47-3
Lead
ND mg/L
0.025
1
07/08/11 15.,45
07/11/11 13:43
7439-92-1
Selenium
ND mg/L
0.10
1
07/08/11 15.45
07/11/11 13.43
7782-49-2
Silver
ND mg/L
0.025
1
07/08/11 15.45
07/11/11 13:43
7440-22-4
Date: 07/15/201105:47 PM REPORT OF LABORATORY ANALYSIS Page 4 of 21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAna1j&a1
w mpecakftcom
Project: Wood Boiler
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
ANALYTICAL RESULTS
[phone]
Pace Analytical, Services, Inc.
9800 lGrxeyAve. Suite 10o
Huntersviile, NC 28078
[phone]
Pace Project No.: 9297122
Sample: North Pond1-#WBNP628 Lab ID: 9297122001 . Collected: 06/28/11 08:30 Received: O6/28/11 09:25- Matrix: Solid
Results reported on a dry -weigh" basis
Parameters Results Units Report Limit DF Prepared Analyzed CAS No. Qual
7470 Mercury, TCLP Analytical Method: EPA 7470 Preparation Method: EPA 7470
Leachate Method/Date: EPA 1311; 07/07/11 18:05
Mercury
ND ug/L
0.20
1
07/08/11 17:10 07/11/11 13:16 7439-97-0
7471 Mercury
Analytical Method: EPA 7471 Preparation Method: EPA 7471
Mercury
0.022 mg/kg
0.0084
1
07/07/11 10:10 07/07/11 16:45 7439-97-0
8270 MSSV TCLP Sep Funnel
Analytical Method: EPA 8270 Preparation Method: EPA 3510
Leachate Method/Date: EPA 1311; 06/30/11 16:00
1,4-Dichlorobenzene
2exac
ND ug/L
50.0
1
07/01/11 10:00 07/01/1121:37 106�16-7
loco- ,3-b
Hexachlorobenzentadiene
ND ug/L
ND ug/L
50.0
1
07%01/11 10:00 07/0,11, 21:37 121-14-2
Hexachloroethane a
ND ug/L
50.0
1
07/01/11 10:00 07/01/11 21:37 87-68-3
Hexachloroethane
ND ug/L
50.0
1
07/01/11 10:00 07/01/1121:37 118-74-1
2-Methylphenol(6-Cresol)
ND ug/L
50,0
1
07/01/11 10:00 07/01/1121:37 67-72-1
3&4-Methylphenol(m8p Cresol)
ND ug/L
50.0
1
07/01/11 10:00 07/01/11 21:37 95-48 7
Nitrobenzene
ND ug/L
50.0
1
07/01/11 10:00 07/01/1121:37
Pentachlorophenol
ND uglL
50.0
1
07/01/11 10:00 07/01/1121:37 98-95-3
Pyridine
ND ug/L
100
1
07/011,,11 10:00 07/01/1121:37 87-86-5
2,4,5-Trichlorophenol
ND ug/L
50.0
1
07/01/11 10:00 07/01/11 21:37 110-86-1
2,4,6-Trichlorophenol
ND ug/L
50.0
1
07/01/11 10:00 07/01/1121:37 95-95-4
Nitrobenzene d5 (S)
84 %
50.0
1
07/01/11 10:00 07/01/1121:37 88-06 2
2-Fluorobiphenyl (S)
82 %
12-102
1
07/01/11 10:00 07/01/1121:37 4165-60-0
TerphenyM14 (S)
82 %
13-107
1
07/01/11 10:00 07/01/1121:37 321-60-8
Phenol-d6 (S)
30 1A
21-132
1
07/01/11 10:00 07/01/1121:37 1718-51-0
2-Fluorophenol (S)
44 %
10-110
1
07101/1' 10:00 07/01/11 21:37 13127 88-3
2,4,6-Tribromophenol (S)
87 %
10-110
1
07/01/11 10:00 07/01/11 21:37 367-12-4
27-108
1
07/01/11 10:00 07/01/11 21:37 118-79-6
8260 MSV TCLP
Analytical Method: EPA 8260
Benzene
2-Butanone (MEiq
ND ug/L
ND ug/L
190
38
07/01/11 10:23 71�t3-2
Carbon tetrachloride
ND ug/L
380
190
38
38
07/01111 10:23 78-93-3
Chlorobenzene
ND ug/L
07/01/11 10:23 56 23-5
Chloroform
ND ug/L
190
38
07/01/11 10:23 108-90-7
1,4-Dichlombenzene
ND ug/L
190
38
07/01/11 10:23 67-66-0
1,2-Dichloroethane
ND ug/L
190
190
38
38
07/01/11 10:23 106-46-7
1,1-Dichloroethene
ND ug/L
190
38
07/01/11 10:23 107-06-2
Tetrachloroethene
ND ug/L
07/01/11 10:23 75-354
Trichloroethene
ND ug/L
190
38
07/01/11 10:23 127-18-4
Vinyl chloride
ND ug/L
190
38
07/01/11 10:23 79-01-0
1,2-Dichlaroethane-d4 (S)
97 %
190
70-130
38
38
07/01/11 10:23 76-01-4
Toluene-d8 (S)
103 %
67-135
38
07/01/11 10:23 17060-07-0
4-Bromofluorobenzene (S)
95 %
07/01/11 10:23 2037-26-5
Dibromofluoromethane (S)
91 %
70-130
38
07/01/11 10:23 460-00-4
70-130
38
07/01/11 10:23 1868-53-7
Date: 07/15/2011 05:47 PM REPORT OF LABORATORY ANALYSIS
Page 5 of 21
This•report shall not be reproduce!, except in full, -
without the written consent.of Pace Analytical Services, Inc..

e
aeeftlx cad
Pace Analytical Services, Inc. Pace, Analytical &4vices,'Inc. =
205 East Meadow Road - Suite A
,PaceAnalyticaiServices; Inc.
2225 Riverside Dr.
'9800 KlnceyAve. Suie 100
mmPacelabs.cam
Eden, NC 27288
Asheville, NC 28804
Huntersville, NC 28078
[phone]
[phone]
[phone]
ANALYTICAL RESULTS
Project. Wood Boiler
Pace Project No.: 9297122
Sample: North Pond #WBNP628
Lab ID: 9297122001 Collected: 06/28/11 08:30
Received: 06/28/1109:25
Matrix. Solid
Results reported on a "dry -weight"
basis
Parameters
Results Units Report Limit DF
Prepared Analyzed
CAS No: Qual
Percent Moisture
Analytical Method: ASTM D2974-87
Percent Moisture
47.2 % 0.10. 1
06/3 0/1108:43
9045 pH Soil
Analytical Method: EPA 9045
PH at 25 Degrees C
9.4 Std..Units 0.10 1
07/05/11 16:19
36&1 Phosphorus, Total
Analytical Method: EPA 366.1 '
Phosphorus
3340 mg ft 105 10
&108111 16:04
7723-14-0
Date: 07/15/2011 05:47 PMREPORT-OF LABORATORY ANALYSIS
This report shall not be reproducer, except ihfull,
without the written consent of Pace Analytical Services, Inc..
Page 6 of 21

aceAnaljftal
w m..pacelabscam
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]'
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: GCSV/5111 'Analysis Method: • EPA 8081
QC Batch Method: EPA 8081 Analysis Description: 8081 GCS TCLP Pesticides
Associated Lab Samples: 9297122001
METHOD BLANK: 221091 Matrix: Water
Associated Lab Samples: 9297122001
Parameter
Units
Blank
Result
Reporting
Limit
Analyzed Qualifiers
Chlordane (Technical)
mg/L
ND
0.0050
07/08/11 15:58
Endrin
mg/L
ND
0.0010
07/08/1115:58
gamma-BHC (Lindane)
mg/L
ND
0.0010
07/08/11 15:58
Heptachlor
mg/L
ND
0:0010
07/0811115:58
Heptachlor epoxide
mg/L
ND
0.0010
07/08/11 15:58
Methoxychlor
mg/L
ND
0.0010
07/08/1115:58
Toxaphene
mg/L
ND
0.0050
07/08/1116:58
Decachlorobiphenyl IS)
%
105
70-130
07/08/11 15:58
Tetrachloro-m-xylene IS)
%
78
70-130
07/08/11 15:58
Pace Analytical Services, Inc.
9800 KinceyAve. Suite 100
Huntersville, NC 28078-
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
221092
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Endrin
mg/L
.005
0.0046
93
70-130
gamma-BHC (Lindane)
mg/L
.005
0.0041
82
70-130
Heptachlor
mg/L
.005
0.0041
83
70-130
Heptachlor epoxide
mg/L
.005
0.0047
94
70-130
Methoxychlor
mg/L
.005
0.0046
93
70-130
Decachlorobiphenyl (S)
%
101'
70-130
Tetrachloro-m-xylene IS)
%
86
70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 221336 221337
MS
9297122001
Spike
Parameter
Units
Result
Conc.
Endrin
mg/L
ND
' .005
gamma-BHC (Lindane)
mg/L
ND
.005
Heptachlor
mg/L
ND
.005
Heptachlor epoxide
mg/L
ND
.005
Methoxychlor
mg/L
ND
.005
Decachlorobiphenyl (S)
%
Tetrachloro-m-xylene (S)
%
Date: 07/15/2011 05:47 PM
MSD
Spike MS MSD MS MSD % Rec
Conc. Result Result % Rec % Rec Limits RPD
.005
0.0048
0.0046
.005
0.0042
0.0040
,.005
0.0043
0.0041
.005
0.0049
0.0046
.005
0.0050
0.0047
REPORT OF LABORATORY ANALYSIS
This report,shall not be reproduped,.except in full,
without the written consent of Pace Analytical Services, Inc..
96
92
70-130 4
84
81
70-130 4
86
82
70-130 5
98
93
70-130 6
100
95
70-130 5
80
77
70-130
87
82
70-130
Qual
Page 7 of 21

aceAnalytical
wmpaaelabacom
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: GCSV/5109
QC Batch Method: EPA 8151
Associated Lab Samples: 9297122001
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8151
Analysis Description: 8151 GCS Herbicides TCLP
Mt I MUu ULANK: 220563
Matrix: Water
Associated Lab Samples:
9297122001
Blank Reporting
Parameter
Units
Result Limit
Analyzed Qualifiers
2,4,5-TP (Silvex)
mg/L
ND 0.010
07/12/11 19:24
2,4-D
mg/L
ND 0.010
07/1211119:24
2,4-DCPA (S)
%
85 70-130
07/12/11 19:24
LABORATORY CONTROL SAMPLE: 220564
Pace Analytical Services, Inc.
98001Gncey Ave. Suite 100
Huntersville, NC 28078
(704)8759092
Spike
LCS LCS % Rec
Parameter
Units
Conc.
Result % Rec Limits Qualifiers
2,4,5-TP (Silvex)
mg/L
.012
0.011 88 70-130
2,4-D
mg/L'
.156
0.049 81 70-130
2,4-DCPA (S)
%
92 70-130
MATRIX SPIKE & MATRIX SPIKE DUPLICATE:
220565
220566
MS
MSD
9297122001
Spike
Spike
MS
MSD
MS
MSD
% Rec
Parameter Units
Result
Conc.
Conc.
Result
Result
% Rec
% Rec
Limits RPD Qual
2,4,5-TP (Silvex) mg/L
ND
.012
.012
0.016
0.011
131
93
70-130 34 M1
2,4-D mg/L
ND
.06
.06
0.077
0.056
129
94
70-130 32
2,4-DCPA (S) %
110
92
70-130
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not, be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 8 of 21

aceAnalytical
www.pawlabs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical, Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MPRP/8714 Analysis Method: EPA 6010
QC Batch Method: EPA3050 Analysis Description: 6010 MET
Associated Lab Samples: 9297122001
METHOD BLANK: 692215 Matrix: Solid
Associated Lab Samples: 9297122001
Parameter
Units
Arsenic
mg/kg
Barium
mg/kg
Cadmium
mg/kg
Calcium
mg/kg
Chromium
mg/kg
Copper
mg/kg
Iron
mg/kg
Lead
mg/kg
Magnesium
mg/kg
Manganese
mg/k9
Molybdenum
mg/kg
Nickel
mg/kg
Potassium
mg/kg
Selenium
mg/kg
Silver
mg/kg
Sodium
mg/kg
Zinc
mg/kg
Blank
Reporting
Result
Limit
Analyzed Qualifiers
ND
0.50
07/13/1114:06
ND
0.60
07/13/1114:06
ND
0.10
07/1311114:06
ND
10.0
07/13/11 14:06
ND
0.50
07/13/1114:06
ND
0.50
07113/1114:06
ND
10.0
07/13/11 14:06
ND
0.50
07113/1114:06
ND
10.0
07/13/11 14:06
ND
0.50
07/13/1114:06
ND
0.50
07/13/1114:06
ND
0.50
07/13/1114:06
ND
500
07/13/11 14:06
ND
1.0
07/13/1114:06
ND
0.50
07/1311114:06
ND
500
07/13/1114:06
ND
1.0
07/13/1114:06,
Pace Analytical Services, Inc.
9800IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
LABORATORY CONTROL SAMPLE:
Parameter
632216
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
50
47.4
95
80-120
Barium
mg/kg
50
48.0
96
80-120
Cadmium
mg/kg
50
49.6
99
80-120
Calcium
mg/kg
500
504
101
80-120
Chromium
mg/kg
50
50.2
100
80-120
Copper
mg/kg
50
47.2
94
80-120
Iron
mg/kg
500
516
103
80-120
Lead
mg/kg
50
49.1
98
80-120
Magnesium
mg/kg
Soo
496
99
80-120
Manganese
mg/kg
50
49.9
100
80-120
Molybdenum
mg/kg
50
49.3
99
80-120
Nickel
mg/kg
50
49.7
99
80-120
Potassium
mg/kg.
500
441J
88
80-120
Selenium
mg/kg
50
47.6
95
80-120
Silver
mg/kg
25
24.6
98
80-120
Sodium
mg/kg
500
459J
92
80-120
Zinc
mg/kg
50
50.7
101
80-120
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in frill,
without the written consent of Pace Analytical Services, Inc..
Page 9 of 21

aceAnalj(tical
www.pmkbs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC,28804
[phone]
QUALITY CONTROL DATA
Pace Analytical Services, Inc.
9800 lOncey Ave. Suite 100
Huntetsville, NC 28078
[phone]
MATRIX SPIKE SAMPLE:
Parameter
632217
Units
9297122001
Result
Spike
Conc.
MS
Result
MS
% Rec
% Rec
Limits Qualifiers
Arsenic
mg/kg
14.4
91
108
102
75-125
Barium
mg/kg
1350
91
1540
214
75-125 M1
Cadmium
mg/kg
. 2.2
91
84.6
91
75-125
Calcium
mg/kg
64200
910
68900
510
75-125 M6
Chromium
mg/kg
26.1
91
117
100
75-125
Copper
mg/kg
92A
91
190
107
75-125
Iron
mg/kg
14300
910
11800
-266
75-125 M1
Lead
mg/kg
32.4
91
110
85
75-125
Magnesium
mg/kg
13000
910
14700
189
75-125 M1
Manganese
mg/kg
2410
91
2650
262
75-125 M6
Molybdenum
mg/kg
5.1
91
86.5
89
75-125
Nickel
mg/kg
16.4
91
98.5
90
75-125
Potassium
mg/kg
15800
910
17500
190
75-125 M6
Selenium
mg/kg
ND
91
91:0
100
75-125
Silver
mg/kg
0.93
45.4
45.7
98
75-125
Sodium
mg/kg
12300
910
13600
147
75=125 M6
Zinc
mg/kg
254
91
367
124
75-125
SAMPLE DUPLICATE: 632218
Parameter
Arsenic
Barium
Cadmium
Calcium ,
Chromium
Copper
Iron
Lead
Magnesium
Manganese
Molybdenum
Nickel
Potassium
Selenium
Silver
Sodium
Zinc
Date: 07/15/2011 05:47 PM
Units
9297452002
Result
Dup
Result
RPD' Qualifiers
mg/kg
ND
ND
mg/kg
ND
.17J.
mg/kg
ND
ND
mg/kg
33.5
32.3
4
mg/kg
ND
.062J
mg/kg
ND
.052J
mg/kg
17.8
15.6
14
mg/kg
ND
ND
mg/kg
10.2
10.0
2
mg/kg
0.55
0.46
17
mg/kg
. ND
Ai
mg/kg
ND
ND
mg/kg
5700
5860
3
mg/kg
1.0
1.0
2
mg/kg
ND
.095J
mg/kg
2390
2470
3
Mg/kg
1.1
1.2
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 10 of 21

ICPAnalxical
www.pacelabacom
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East Meadow Road - SuiteA
Eden, NC 27288
[phone]'
Pace Analytical Services, Inc.
2225• Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
wu tiaicn: MPRP/8695 Analysis Method: EPA 6010
QC Batch Method: EPA3010 Analysis Description: 6010 MET TCLP
Associated Lab Samples` 9297122001
METHOD BLANK: ' 631475 Matrix., Water
Associated Lab Samples: 9297122001
Parameter
Units
Arsenic
mg/L
Barium
mg/L,
Cadmium
mg/L
Chromium
mg/L
Lead,
mg/L
Selenium
mg/L
Silver
mg/L
LPJ5L)KAI uKY (;UNTROL SAMPLE:
Parameter
631476
Units
Arsenic
mg/L
Barium
mg/L
Cadmium
mg/L
Chromium
mg/L
Lead
mg/L
Selenium
mg/L
Silver
mg/L
Pace Analytical Services, Inc.
9800IGnceyAve. Suite too
' Huntersville, NC 28078
[phone]
Blank
Reporting
Result
Limit
Analyzed
Qualifiers
ND
0.025
07/11/1112:41
ND
0.50
07/11/1112:41
ND
0.0050
07/11/1112:41
ND
0.025
07/11/1112.41
ND
0.025
07/11/1112:41
ND
0.10
07111/1112:41
ND
0.025
07/11/1112:41
Spike
LCS
LCS % Rec
Conc.
Result % Rec Limits Qualifiers
2.5
2.7
109
80-120
2.5
2.6
103
80-120
2.5
2.6
100
80-120
2.5
2.6
103
80-120
2.5
2.4
94
80-120
2.5
2.7
108
80-120
1.2 ,
1.3
102
80-120
MAI KIA,rIKE SAMPLE:
Parameter
631477
Units
9296142001
Result
Spike
Conc.
MS
Result
MS
% Rec
%Rec
Limits Qualifiers
Arsenic
mg/L
ND
2:5
2.5
001
7,,) 125
Barium
mg/L
ND
2.5
2.4
88
75-125
Cadmium
mg/L
ND
2.5
2.4
94
75-125
Chromium
mg/L
ND
2.5
2.4
97
'75-125
Lead
mg/L
257
2.5
217
=1600
75-125
Selenium
mg/L
ND
2.5
2.5
'99
75-125
Silver
mg/L
ND
1.2
1.2
97
75-125
SAMPLE DUPLICATE: 631478
Parameter
Units
9296514001
Result
Dup
Result RPD Qualifiers
Arsenic
mg/L
ND
ND
Barium
mg/L
1.2
1.2 0
Cadmium
mg/L
ND
ND
Chromium
mg/L
ND
ND
Lead
mg/L
ND
0.057
Date: 07/15/2011 05:47 PM REPORT OF LABORATORY ANALYSIS Page 11 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..

aceAnalytical
www.pacelabsx=
Project: Wood Boiler
Pace Project No.: 9297122 .
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc..
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY, CONTROL DATA
SAMPLE DUPLICATE: 631478
9296514001 Dup
Parameter Units Result Result RPD Qualifiers
Selenium mg/L ND ND
Silver mg/L ND ND
Date: 07/15/2011 05:47 PM
REPORT -OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
Without the written consent of Pace Analytical Services, Inc..
Pace Analytical Services, Inc.
9800IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Page 12 of 21

aceftij ical
www.*Wabs.com
Project: Wood Boiler
Pace Project No.: 9297122
Pace Analytical Services, Inc.
205 East, Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225•Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
QC Batch: MERP/3601 Analysis Method: EPA 7470
QC Batch Method: EPA 7470 Analysis Description: 7470 Mercury TCLP
Associated Lab Samples: 9297122001
METHOD BLANK: 631610 Matrix: Water
Associated Lab Samples: 9297122001
Blank Reporting
Parameter Units Result Limit Analyzed
Mercury ug/L ND 0.20 07/11/1112:39
LABORATORY CONTROL SAMPLE: 631611
Parameter Units
Mercury ug/L
MATRIX SPIKE SAMPLE: 631613
Parameter Units
Mercury ug/L
SAMPLE DUPLICATE: 631612
Parameter
Mercury
Date: 07/15/2011 05.47 PM
Qualifiers
Pace Analytical Services, Inc.
98001GnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
2.5 2.2 86 80-120
9296142001 Spike MS MS % Rec
Result Conc. Result %Rec Limits Qualifiers
ND 2.5 1.9 75 75-125
9296514001 Dup
Units Result Result RPD Qualifiers
ug/L ND ND
REPORT�OF LABORATORY ANALYSIS
This. report strall,not-be-reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
1 00 - I '
Page 13 of 21

® ' Pace Analytical Services, Inc. Pace Analytical Services, Inc. Pace Analytical Services, Inc.
ae19malytical 205 East Meadow Road - Suite A 2225 Riverside Dr. 9800 Wncey Ave. Suite 100
�,K, s— Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone] [phone]
QUALITY CONTROL DATA
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: MERP/3594 Analysis Method: EPA 7471
QC Batch Method: EPA 7471 Analysis Description: 7471 Mercury
Associated Lab Samples: 9297122001 .
METHOD BLANK: 630349
Associated Lab Samples: 9297122001
Parameter Units
mg/kg . .
Mercury
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 0.0050 07/07/1115:28
LABORATORY CONTROL SAMPLE:
630350
,Spike LCS
LCS
% Rec
Parameter
Units
Conc. Result
% Rec
Limits
Qualifiers
Mercury
mg/kg
..067 0.061
91
80-120
MATRIX SPIKE SAMPLE:
630351
9297121005 Spike -
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers '
Mercury
mg/kg
0.013 :076
0.085
94
75-125
MATRIX SPIKE SAMPLE:
630353
9297031012 Spike
MS
MS
% Rec
Parameter
Units
Result Conc.
Result
% Rec
Limits Qualifiers
Mercury
mg/kg
0.046 , - .075
0.11
92
75-125
SAMPLE DUPLICATE: 630352
9297167001
Dup
Parameter Units
Result
Result
Mercury mg/kg
ND
.00038J
SAMPLE DUPLICATE: 630354
9297031013
Dup
Parameter Units
Result
Result
Mercury mg/kg
0.036
0.032
Date: 07/15/2011 05:47 PM
RPD Qualifiers
RPD Qualifiers
11
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytipl Services, Inc..
Page 14 of 21

aceAnalXical
www.Pacew com
Project: Wood Boiler
Pace Project No.: 9297122
Pace AnalyticalZervices, Inc. Pace Analytica[Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY. CONTROL DATA
QC Batch: 'OEXT/14105 Analysis Method: EPA8270
QC Batch Method: EPA 3510 Analysis Description: 8270 TCLP MSSV
Associated Lab Samples: 9297122001
METHOD BLANK: 628862
Associated Lab Samples: 9297122001
Parameter Units
Matrix: Water
Blank Reporting
Result Limit
Analyzed Qualifiers
1,4-Dichlorobenzene
ug/L
ND
50.0
07/01/1120:15
2,4,5-Trichlorophenol
ug/L
ND
50.0
07/01/1120:15
2,4,6-Trichlorophenol
ug/L
ND
50.0
07101/1120:15
2,4-Dinifrotoluene
ug/L
ND
50.0
07/01/1120:15
2-Methylphenol(o-Cresol)''
ug/L
ND
50.0
07101/1120:15
3&4-Methylphenol(m&p Cresol)
ug/L
ND
50.0
07/01/1120:15
Hexac hloro-1,3-butadiene
ug/L
ND
50.0
07/01/1120:15
Hexachlorobenzene
ug/L
ND
50.0
07/01/1120:15
Hexachloroethane
ug/L
ND
50.0
07/01/1120:15
Nitrobenzene
uglL
ND
50.0
07/01/1120:15
Pentachlorophenol
ug/L
ND
100
07/01/1120:15
Pyridine
ug/L
ND
50:0
07/01/1120:15
2,4,6-Tribromophenol (S)
%84
27108
07/01/1120:15
2-Fluorobiphenyl (S)
%
82
13-107
07101/1120:15
2-Fluorophenol (S)
%
44
10-110
07/01/1120:15
Nitrobenzene-d5 (S)
%
85
12-102
07/01/1120:15
Phenol-d6 (S)
%
31
10-110
07/01/11 20:15•
Terphenyl-d14 (S)
%
74
21-132
07/01/1120:15
Pace Analytical Services, Inc.
9800IGnceyAve. Suite 100
Huntersville, NC 28078
LABORATORY CONTROL SAMPLE:
Parameter
628863
Units
Spike
Conc:
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers.
1,4-Dichtorobenzene
ug/L
500
312
62
10-110
2,4,5 Trichlorophenoi
ug/L
500
353
71
39-108
2,4,6-Trichiorophenol
4L
500
432
86
2,4-Dinitrotoluene
ug/L
500
384
77
.40-104
42-109
2-Methylphenol(o-Cresol)
ug/L
500
294
59
31-110
3&4-Methylphenol(m&p Cresol)
ug/L
500
262
52
30-110
Hexachloro-1,3-butadiene
ug/L
500
276
55
10-110
Hexachlorobenzene
ug/L
Soo
359
72
39-121
Hexachloroethane
ug/L
500
289
58
10-110
Nitrobenzene
ug/L
Soo
449
90
32-101
Pentachlorophenol
ug/L
1000
739 '
74
18-108
Pyridine
ug/L
500
264
53
10-110
2,4,6-Tribromophenol (S)
%
88
27-108
2-Fluorobiphenyl (S)
%
89
13-107
2-Fluorophenol (S)
%
49
10-110
Nitrobenzene-d5 (S)
%
92
12-102
Phenolwd6 (S)
%
31
10-110
TerphenyW14(S)
%
88
21-132
[phone]
Date: 07/15/2011 05A7 PM REPORT OF: LABORATORY ANALYSIS Page 15 of21
This report shall not be reproduced, except in full,
without the written consent of Pace Analyticaf: Services, Inc..

ace
Analj cal
www.pao"S.Cam
Pace Analytical Services, Inc.
205 East -Meadow Road - SuiteA
Eden, NC 27288
[phone]
Project: Wood Boiler
Paoe Project No.: 9297122
MATRIX SPIKE & MATRIX SPIKE DUPLICATE: 628864
'Parameter
1,4-Dichlorobenzene
2,4,5-Trichlorophenol
2,4,6-Trichlorophenol
2,4-Dinitrotoluene
2-Methylphenol(o-Cresol)
3&4-Methylphenol(m&p
Cresol)
Hexachloro-1,3-butadiene
Hexachlorobenzene
Hexachloroethane
Nitrobenzene
Pentachlorophenol
Pyridine
2,4,6-Tdbromophenol (S)
2-Fluorobiphenyl (S)
2-Ruorophenol(S)
Nitrobenzene-d5 (S)
Phenol-d6 (S)
Terphenyl-c114 (S)
Date: 07/15/2011 05:47 PM
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone].
QUALITY: CONTROL DATA
628865
Pace Analytical Services, Inc.
9800 IGnceyAve. Suite 100
Huntersville, NC 28078
[phone]
Units
9297187001
Result
MS
Spike
Cone.
MSD
Spike
Conc.
MS
Result
MSD
Result
MS
% Rec
MSD
% Rec
% Rec
Limits
RPD
ug/L
ND
500
500
300
290
60
58
30-150
3
ug/L
ND
500'
500
352
373
70
75
30-150
6
ug/L
ND
500
500
440,
453
88
91
30-150
3
ug/L
ND
500
500
375
412
75
82
30-150
10
ug/L
ND
500
500
299
281
60
56
30-150
6
ug/L
148
500
500
396
424
50
55
30-150
7
ug/L
'ND
500
500
281
279
56
56
30-150
1
ug/L
ND
500
500
359
358
72
72
30-150
0
ug/L
ND
500
500
287
272
57
54
30-150
5
ug/L
ND
500
500
479
463
96
93
30-150
3
ug/L
ND
1000
1000
764
809
76
81
30-150
6
ug/L
ND
500
500
266
230
53
46
30-150
14
%
85
85
27-108
%
87
85
13-107
%
46
44
10-110
%
87
85
12-102
%
30
28
10-110
%
80
83
21-132
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Qual
Page 16 of 21

aceftlXical
www.pa "Isom
Project: Wood Boiler
Pace Project No.: 9297122
QC -Batch: MSV/15868
QC Batch Method: EPA 8260
Associated Lab Samples: 9297122001
Pace Analytical Services, Inc. Pace Analytical Services, Inc.
205 East Meadow Road - Suite A 2225 Riverside Dr.
Eden, NC 27288 Asheville, NC 28804
[phone] [phone]
QUALITY CONTROL DATA
Analysis Method: EPA 8260
Analysis Description: 8260 MSV TCLP
METHOD BLANK: 628597 Matrbc Water
Associated Lab Samples:
Parameter
9297122001
Units
Blank
Result
Reporting
Limit
Analyzed hz Qualifiers
1,1-Dichloroethene
ug/L
ND
5.0
07/01/1100:41
1,2-Dichloroethane
ug/L
ND
5.0
07/0111100:41
1,4-Dichlorobenzene
ug/L
ND
5.0
07/01/1100:41
2-Butanone (MEK)
ug/L
ND
10.0
07/01/1.1 00.41
Benzene
Carbon tetrachloride
ug/L
ug/L
ND
5.0
07/01/1100:41
Chlorobenzene
ug/L
ND
5.0
07/01/11 00:41
Chloroform
ug/L
ND
ND
5.0
07/01/11 00:41
Tetrachloroethene
ug/L
5.0
07101/1100.41
Trichloroethene
ug/L
ND
5.0
0710111100:41
Vinyl chloride
ug/L
ND
5.0
07101/1100:41
1,2-Dichloroethane-d4 (S)
%
ND
5.0
07/01/1100:41
4-Bromofluorobenzene (S)
%
98
70-130
07/01/11 00:41
Dibromofluoromethane (S)
%
97
70-130
07/01/11 00:41
Toluene -dB (S)
%
104
70-130
07/01/1100:41
103
67-135
07/01/11 00.41
Pace Analytical Services, Inc.
9860IcnceyAve: Suite 100
Huntersville, NC 28078
LABORATORY CONTROL SAMPLE:
Parameter
628598
Units
Spike
Conc.
LCS
Result
LCS
% Rec
% Rec
Limits Qualifiers
1,1-Dichloroethene
ug/L
50
52.1
104
70-141
1,2-Dichloroethane
ug/L
50
54.1
108
70-139
1,4-Dichlorobenzene
ug/L
50
52A
105
70-141
2-Butanone (MEK)
ug/L
100
98.2
98
63-150
Benzene
Carbon tetrachloride
ug/L
ug/L
50
49.2
98
70-132
Chlorobenzene
ug/L
50
50
50.0
100
70-150
Chloroform
ug/L
50
54.4
54.4
109
70-134
Tetrachloroethene
ug/L
50
54.1
109
108
70-130
Tdchloroethene
ug/L
50
52.1
104
70-137
70-131
Vinyl chloride
ug/L
50
47.8
96
56-144
1,2-Dichloroethane-d4 (S)
%
4-Bromofluorobenzene (S)
%
99
70-130
Dibromofluoromethane (S)
%
103
70-130
Toluene -dB (S)
%
102
70-130
101
67-135
Date: 07/15/2011 05.47 PM REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 17 of 21

aceAnaoical
svbwpscebbs.com
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: PMST/4030
QC Batch Method: ASTM D2974-87
Associated Lab Samples: 9297122001
SAMPLE DUPLICATE: 628035
Parameter
Percent Moisture
SAMPLE DUPLICATE:. 628036
Parameter
Percent Moisture
Date: 07/15/2011 05:47 PM
o�
Pace Analytical Services, Inc.
205 East Meadow Road - Suite
Eden, NC 27288
[phone]
Units
Units
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
(.QUALITY CONTROL DATA
Analysis Method: ASTM D2974-87
Analysis Description: Dry Weight/Percent Moisture
9297061013 Dup
Result Result RPD Qualifiers
19.5 19.2 1
9297122001 Dup
Result Result RPD Qualifiers
47.2 47.9 2
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
qV
Pace Analytical Services, Inc.
9800 Kncey Ave. Suite 100
Huntersville, NC 28078
[phone]
Page 18 of 21

1k/��,n, Pace Analyycal•Services, Inc. Pare Analytical Services,.lnc. Pace Analytical Services, Inc.
eAna1 jdb® 205 East,Meadow Road - Suite A 2225 Riverside Dr. 98001Gncey Ave. Suite 100
www.pacelebs com Eden, NC 27288 Asheville, NC 28804 Huntersville, NC 28078
[phone] [phone]
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: WET/17032 Analysis. Method: - EPA 9045
QC Batch Method: EPA 9D45 Analysis Description: 9645 pH
Associated Lab Samples: 9297122001
SAMPLE DUPLICATE: 629698
9297061016 Dup.
Parameter Units Result Result RPD Qualifiers
pH at 25 Degrees C Std. Units 5.4 5.4
0
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This repart,shall not'be reproduced, except in full, '
without the written consent of Pace Analytical Services, Inc..
Page 19 of 21

aceAfflocal
wWW..paaelabsmm
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
Pace Analytical Services, Inc.
2225 Riverside Dr.
Asheville, NC 28804
[phone]
QUALITY CONTROL DATA
Project: Wood Boiler
Pace Project No.: 9297122
QC Batch: WETA/10057 Analysis Method: EPA 365.1
QC Batch Method: EPA 365.1 Analysis Description: 365.1 Phosphorus, Total.
Associated Lab Samples: 9297122001
Wit I t1w BLANK: 631125
Associated Lab Samples: 9297122001
Parameter Units
Phosphorus mg/kg
LABORATORY CONTROL SAMPLE: 631126
Parameter Units
Phosphorus mg1kg
Matrix: Solid
Blank Reporting
Result Limit Analyzed Qualifiers
ND 2.0 07/08/1115:55
Pace Analytical Services, Inc.
98001GnoeyAve. Suite too
Huntersville, NC 28078
[phone]
Spike LCS LCS % Rec
Conc. Result % Rec Limits Qualifiers
50 54.8 110 90-110
MATRIX SPIKE SAMPLE: 631127
9296826001 Spike MS MS % Rec
Parameter Units .Result Conc. Result % Rec Limits Qualifiers
Phosphorus mg/kg 11.1 127 134 97 90-110
bAMVLt UUPLIGATE: 631128
Parameter
Phosphorus
Date: 07/15/2011 05.47 PM
9296826002 Dup
Units Result Result
mg/kg 10.8 11.2
RPD Qualifiers
4
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
Page 20 of 21

aceAnapical
www.Pacelaftcarn -
Project: Wood Boiler
Pace Project No.: 9297122
DEFINITIONS
Pace Analytical Services, Inc.
205 East Meadow Road - Suite A
Eden, NC 27288
[phone]
QUALIFIERS
Pace Analytical Services, Inc.
,2225 Riverside Dr.
Asheville, NC 28804
[phone]
Pace Analytical Servlces, Inc.
9800IGnceyAve. Suite 100
Huntersville, NC 28078
DF - Dilution Factor, if reported, represents the factor applied to the reported data due to changes in sample preparation, dilution of
the sample aliquot, or moisture content.
NO - Not Detected at or above adjusted reporting limit.
J - Estimated concentration above the adjusted method detection limit'and below the adjusted reporting limit.
MDL -Adjusted Method Detection Limit.
S - Surrogate
1,2-Diphenylhydrazine (8270 listed analyte) decomposes to Azobenzene.
Consistent with EPA guidelines, unrounded data are displayed and have been used to calculate % recovery and RPD values.
LCS(D) - Laboratory Control Sample (Duplicate)
MS(D) - Matrix Spike (Duplicate)
DUP - Sample Duplicate
RPD - Relative Percent Difference
NC - Not Calculable.
SG - Silica Gel - Clean -Up
U - Indicates the compound was analyzed for, but not detected.
WNitrosodiphenylamine decomposes and cannot be separated from Diphenylamine using Method 8270. The result reported for
each analyte is a combined concentration.
Pace Analytical is TNI accredited. Contact your Pace PM for the current list of accredited analytes.
LABORATORIES
PASI-A Pace Analytical Services -Asheville
PASI-C Pace Analytical Services - Charlotte
PASI.O Pace Analytical Services - Ormond Beach
ANALYTE QUALIFIERS
M1 Matrix spike recovery exceeded QC limits. Batch accepted based on laboratory control sample (LCS) recovery.
M6 Matrix spike and Matrix spike duplicate recovery not evaluated against control limits due to sample dilution.
81 Surrogate recovery outside laboratory control limits (confirmed by re -analysis).
Date: 07/15/2011 05:47 PM
REPORT OF LABORATORY ANALYSIS
This report shall not be reproduced, except in full,
without the written consent of Pace Analytical Services, Inc..
[phone]
Page 21 of 21

Date: '
_ Analyst:
Facility:
Calihrnfinn
PH Analyses
- . 11IO sianaara s true value.

Baxter Healthcare - Wood Boiler
Please test the sample(s) for the parameters as listed below.
Send original results to: email: [e-mail]
Send Invoice and copy of results to: email: ricky_styles
Ricky Styles @baxter.com
Baxter Healthcare Purchase Order # 3 Z.5
�
2869 Old Linville Rd.
Marion, NC 28752
[phone]
email: [e-mail]
Ran"antad nima flaI®•
t5�O ( 114
Sample #
Sample
Description
Sample Date(s)
and time sample
collected
Grab or
Composite
Total Metals -
.As, Be, Cd,
Ca, Cr, Cu, Fe,
Pb, Mg, Hg,
Mn, Mo, NI, IC,
Se, Ag, Na,
Zn, total
Phosphorus
TCLP�Metala '
As, Ba, Cd,
Cr, Pb, Hg,
Se, Ag
Ignitabllity,
Reactivity
pH
Corroolvity
Total -Arsenic
Full TCLP
WB20TR2011
BOTTOM ASH
8-5-11 8:30AM
COMPOSITE
YES
YES
Sample sent to: Pace Analytical Services,
2225 Riverside Drive
Asheville, NC 28804
828-254-7176
Chain of Cumay
Project Manager: Tom Williams
9800 IGncey Avenue, Suite 10(
Huntersviile, NC 28078
(704) 875 - 9092 ext. 233
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